Beruflich Dokumente
Kultur Dokumente
Article history: Objectives: To assess by means of push-out test the post retentive potential of a new
Received 2 October 2011 flowable resin composite with low polymerization stress.
Received in revised form Methods: SureFil1 SDRTM (Dentsply, S) was compared with the resin cement Calibra (Dents-
16 January 2012 ply, C). S and C were used in combination with the adhesive XP Bond (Dentsply, XPB). In C
Accepted 17 January 2012 group the Self-Cure Activator was mixed with XPB. The following types of fibre posts were
luted into 30 extracted premolars: Radix Fiber Post (Dentsply, R), DT Light Post (RTD, LP), ER
Dentin Post (Komet, ER), DT Light SL (VDW, SL), FibreKleer (Jeneric Pentron, F). Six posted
Keywords: roots per group were tested. Each root provided three to five 1 mm-thick slices. Measured
Post push-out strengths were differentiated by post space level and statistically analysed
Luting ( p < 0.05). The failure mode of each debonded specimen was assessed.
Low-stress Results: Cement type did not have a significant effect on post retention ( p = 0.54). Post type
Resin composite was a significant factor for push-out strength ( p < 0.001). LP exhibited significantly higher
Push-out retentive strength than SL and F; push-out strengths of ER and R were significantly higher
Failure mode than those of F. Post retention was significantly influenced by post space level ( p < 0.001).
Significantly higher push-out strengths were recorded at the coronal third than at the
middle and apical levels. The postcement interaction was significant ( p = 0.002). Posts luted
with S most often failed at the cementpost interface.
Conclusions: When the new flowable low-stress composite was used to lute fibre posts,
similar retentive strengths to those of a marketed cement from the same manufacturer were
achieved.
Clinical significance: SureFil1 SDRTM, a flowable composite originally proposed for bulk filling
of posterior restorations, exhibited post retentive strengths similar to those of a cement by
the same manufacturer. With a relatively high filler load, yet a low curing stress, SureFil1
SDRTM may be adequate for both post cementation and core build-up.
# 2012 Elsevier Ltd. All rights reserved.
* Corresponding author at: Department of Dental Materials and Fixed Prosthodontics, Policlinico Le Scotte, viale Bracci, Siena 53100, Italy.
Tel.: +39 0577 233131; fax: +39 0577 233117.
E-mail address: cecilia.goracci@gmail.com (C. Goracci).
0300-5712/$ see front matter # 2012 Elsevier Ltd. All rights reserved.
doi:10.1016/j.jdent.2012.01.007
journal of dentistry 40 (2012) 322328 323
walls were etched with 34% phosphoric acid (Caulk Tooth Measured push-out strengths were differentiated by post
Conditioner Gel, Milford, DE USA) for 15 s using an intraca- space level (coronal, middle, and apical), and statistically
nalar tip. The gel was rinsed with water using endodontic analysed. The Three-Way Analysis of Variance was applied
needles. Excess water was removed from the post space using with push-out strength as the dependent variable, luting
absorbent paper points. In preparing the specimens of agent, post, and post space level as factors. The Tukey test was
subgroup 1, XP Bond was mixed with Self-Cure Activator. applied for pairwise comparisons as needed. In all the
The adhesive solution was applied on the post space walls analyses the level of significance was set at p < 0.05. Statistical
with a microbrush and left undisturbed for 20 s. Then, the calculations were handled by the software PASW Statistics 18
solvent was evaporated with the air stream from the airwater (SPSS Inc., Chicago, IL, USA).
syringe, and the adhesive was light-cured for 10 s with a The failure mode of each debonded specimen after the
quartz-tungsten-halogen light (VIP, Bisco, Schaumburg, IL, push-out test was assessed using a stereomicroscope (Nikon
USA; minimum output 550 mW/cm2). In subgroup 1 base and SMZ645, Tokyo, Japan) at 40 magnification and classified as
catalyst of Calibra were mixed and the mixed cement was follows: adhesive failure between dentin and cement, adhe-
placed into the post space with a Lentulo spiral. The cement sive failure between cement and post, cohesive failure within
was also applied onto the post surface and the post was seated the cement, cohesive failure within the post, mixed failure.
with a slight finger pressure. Light-curing was performed One slice representative of each failure mode was
for 20 s through the post by placing the light tip onto the post processed for scanning electron microscopy (SEM) evaluation
coronal end. In subgroup 2, where SureFil1 SDRTM was used in order to obtain SEM images of the failure patterns. The slices
as the luting agent, cement application, post seating, and were rinsed in 96% alcohol solution for 1 min and air dried.
polymerization were performed in the same way as in Each slice was mounted on a metallic stub, sputter-coated
subgroup 1. with gold (Polaron Range SC7620; Quorum Technology,
After 24 h, the posted roots were transversely sectioned Newhaven, UK), and observed under a scanning electron
into 1 mm-thick serial slices using a low-speed saw (Isomet, microscope (JSM 6060 LV; JEOL, Tokyo, Japan).
Buehler, Lake Bluff, IL, USA) under water-cooling. Each root
provided three to five 1 mm-thick slices. The push-out test
was performed using a universal testing machine (Controls 3. Results
S.P.A., Milano, Italy), operating at a crosshead speed of
0.5 mm/min. On the loading machine each slice was posi- Descriptive statistics of the post push-out strengths are
tioned with the larger side of the post segment placed facing reported in Table 3. The Three-Way ANOVA indicated that
the punch tip. Bond failure was manifested by the dislodgment the type of luting agent did not have a significant effect on post
of the post fragment from the slice. Push-out strength data retention ( p = 0.54). Conversely, post type was a highly
were converted to MegaPascal (MPa) by dividing the load in significant factor for push-out strength ( p < 0.001). Particular-
Newton by the bonded surface area (SL) in mm2. SL was ly, DT Light Posts exhibited significantly higher retentive
calculated as the lateral surface area of a truncated cone using strength than DT Light SL and FibreKleer posts. Also, push-out
the formula: SL = p(R + r)[h2 + (R r)2]0.5, where p = 3.14, R is the strengths of ER Dentin Posts and Radix Fiber posts were
coronal post radius, r the apical post radius, and h the significantly higher than those of FibreKleer posts. Also post
thickness of the slice. The larger and the narrower diameters space level was a significant factor for push-out strength
of the post and the thickness of the slice were individually ( p < 0.001). Specifically, significantly higher push-out
measured using a digital calliper with 0.01 mm accuracy. strengths were recorded at the coronal third (12.1 4.1 MPa)
journal of dentistry 40 (2012) 322328 325
Table 3 Descriptive statistics of the post push-out strengths measured in MegaPascals. Different capital letters in the
Post column label statistically significant differences among the post types regardless of the luting agent and of the
dowel space level. Different small letters label statistically significant postcement interaction terms.
Post Luting agent Level N Mean Std. deviation
A ab
DT Light Post Calibra Coronal 4 11.6 1.8
Middle 5 7.3 2.2
Apical 2 10.4 6.4
Total 11 9.5 3.4
SureFil SDR a Coronal 4 15.8 1.3
Middle 6 13.3 4.6
Apical 2 13.9 4.1
Total 12 14.2 3.6
than at the middle (7.6 4.4 MPa) and apical (8.1 4 MPa) that had been restored with DT Light Posts failures were either
levels, that offered similar conditions for bonding. The post cohesive within cement or adhesive at the cementpost
cement interaction was significant ( p = 0.002). In Table 3 interface. Post fractures were observed only in the DT Light
different small letters label statistically significant interaction SL/Calibra group.
terms. The other between-factor interactions were not
statistically significant.
Table 4 illustrates the distribution of failure modes in 4. Discussion
the experimental groups. When SureFil1 SDRTM was used as a
luting agent in combination with all the posts except Based on the studys results, the null hypothesis has to be
FibreKleer posts, failures occurred consistently at the partly rejected, as post type and dowel space level were found
cementpost interface (Fig. 1A). When SureFil1 SDRTM was to have a significant influence on post retention. Conversely,
used with FibreKleer posts, failure was most often at the post push-out strength was not affected by the luting agent.
cementpost interface; however, also cohesive fractures The latter finding supports the use of SureFil1 SDRTM for
within the cement and mixed failures were reported. The intraradicular luting of FRC posts. SureFil1 SDRTM has been
majority of failures at the cementdentin interface were marketed for bulk-filling of posterior direct resin composite
exhibited by specimens that had been restored with Calibra restorations. As available in only one shade, SureFil1 SDRTM is
and ER Dentin Post or Radix Fiber posts (Fig. 1B). In specimens to be overlayed with a universal composite resin, replacing
326 journal of dentistry 40 (2012) 322328
missing enamel (SureFil1 SDRTM technical bulletin, Dentsply). system in unfilled and in variously filled formulations yielded
Beside the claim of a self-levelling adaptation, the new lower curing stress than a conventional marketed resin.
flowable composite features a polymerization modulator Regarding the degree of conversion of SureFil1 SDRTM, the
that, according to the manufacturer, provides the resin with a only available information is that provided by the manufac-
stress decreasing ability. The polymerization modulator is a turer (SureFil1 SDRTM technical bulletin, Dentsply). These
photoactive group, chemically embedded in urethane-based internal data indicate that at the bottom of a 5 mm-deep
methacrylate resin, that would interact with camphorqui- specimen of SureFil1 SDRTM, light-irradiated for 20 s (light
none. Such interaction would induce a slower modulus intensity 500550 mW/cm2), a degree of conversion of about
development that allows for a reduction in shrinkage stress, 50% was measured with Near-Infrared spectroscopy. More-
without affecting polymerization rate or degree of conversion over, at a 6 mm depth, following 20 s irradiation by a light
(SureFil1 SDRTM technical bulletin, Dentsply). In a recent curing unit with a power output of 650 mW/cm2, a degree
investigation the shrinkage behaviour and the micromecha- of conversion over 45% was measured for SureFil1 SDRTM
nical properties of SureFil1 SDRTM were compared with those through Fourier Transform spectroscopy (SureFil1 SDRTM
of two regular flowable methacrylate-based composites and of technical bulletin, Dentsply). The potential of SureFil1
a silorane-based composite.23 SureFil1 SDRTM had the lowest SDRTM for a slow stress development proposes this material
shrinkage stress, the longest pre-gel time, the lowest as hypothetically indicated also for FRC posts intraradicular
shrinkage rate. With regard to the micromechanical proper- luting, where stress due to constrained polymerization
ties, it emerged that SureFil1 SDRTM was less hard, more rigid, shrinkage remains a challenge. It was lately documented that
and more plastic than the other tested flowables.23 Koltisko stronger post retention and better intraradicular sealing were
et al.24 found for SureFil1 SDRTM a polymerization stress lower obtained with resin cements loaded by 30% and 50% in weight
than that of other universal and flowable composites, than when the filler load of the luting agent was increased to
although volumetric shrinkage (3.5 vol%) and flexular modu- 70%.18 The cited study provided evidence against the use of
lus were similar to those of the tested flowables. Burgess one same material for post luting and core build-up, recently
et al.22 stated that the chemistry of SureFil1 SDRTM is designed proposed by manufacturers for the purpose of simplification.
to slow the polymerization rate, thereby shrinkage stress is As a matter of fact, the relatively high filler load and elastic
reduced even though polymerization shrinkage remains modulus of resin composites typically used for abutments
comparable to that of other flowable composite resins would negatively affect curing stress when the same materials
(3.1 vol%). Jin et al.25 reported that the new SDRTM resin are employed for intraradicular post luting. In this regard it
Fig. 1 (A) Adhesive failure between post and luting agent in a specimen in which DT Light Post was used in combination
with SureFilW SDRTM (T50, bar = 500 mm). (B) Adhesive failure between cement and dentin in a Radix Fiber Post/Calibra
specimen (T50, bar = 500 mm).
journal of dentistry 40 (2012) 322328 327
should be noticed that SureFil1 SDRTM could provide the of conversion33,34 and bond strength to dentin,35 are enhanced
favourable combination of relatively high filler load (68 wt%) by exposure to light. Beside opacity, other properties of
and low curing stress. The shrinkage stress measured by FibreKleer posts may have played a role in determining the
SureFil1 SDRTM in the study by Ilie et al.23 was 1.1 .01 MPa. relatively weak retention observed for these dowels in the
Similarly low values of curing stress were measured in the present study. Differently from the other posts on trial, that all
study by Ferrari et al.18 for a luting agent filled by 10 wt% feature an epoxy resin matrix, in FibreKleer posts the matrix is
(1.19 .25 MPa), while the curing stress of the 70 wt% made of methacrylate resin. It can therefore be speculated
filled cement was 2.36 .004 MPa. Nevertheless, it should that the methacrylated-based matrix of FibreKleer is less
also be considered that SureFil1 SDRTM is a light-cured resin receptive to the bonding of Calibra and SureFil1 SDRTM. In a
composite, while it has been demonstrated that dual-cure previous investigation it was reported that the pull-out
materials are the most appropriate for intraradicular luting, as strength of FibreKleer posts was significantly increased by
light transmission through the post is a critical issue.2631 post surface sandblasting with aluminium oxide and Cojet
Thereby, the idea to test the ability of the new flowable treatment.32 It could therefore be interesting to verify whether
material to intraradicularly retain several types of FRC posts, such post surface treatments may also enhance the adhesion
with different degrees of translucency. The push-out mea- of SureFil1 SDRTM and Calibra.
surements demonstrated that, irrespective of the post type, It is also worth mentioning that the use of post and cement
SureFil1 SDRTM yielded post retentive strengths similar to from the same manufacturer did not bring any particular
those of Calibra, that was tested as control. It would also be of benefit to post retention, as Radix Fiber Posts measured push-
interest to investigate whether the slower modulus develop- out strengths similar to those of the other translucent dowels
ment and the consequent low shrinkage stress of SureFil1 under test.
SDRTM result in improved interfacial sealing within the Also the handling characteristics of the materials deserve
posted root. some comments. In this regard it should be considered that
When considering the influence of the dowel space level on SureFil1 SDRTM would have the advantage of not requiring any
push-out strength, the coronal third was found to offer the mixing step. Furthermore, having a relatively high filler load in
most favourable conditions for post retention. This observa- comparison with other flowable composites, its use could be
tion is in line with the results of several previous investiga- proposed also for building up the abutment. The performance
tions, and could be related to the increasingly difficult access, of the new material in this application should however be
to changes in dentin tubules orientation, as well as to light preliminarily verified with in vitro tests of bond strength and
attenuation, proceeding from the coronal to the apical level of interfacial adaptation.
the dowel space.1,4,28,29 It should finally be mentioned that this study provided
Concerning post types, DT Light Post, Radix Fiber, ER Dentin information on early post retention. It is understood that
Post, DT Light SL posts, although differing in chemical the evidence collected in the present investigation should
composition and shape, all exhibit relatively high degrees of ideally be strengthened by the outcome of dynamic tests
translucency according to recent spectrophotometric mea- simulating the clinical function and ultimately by in vivo
surements,26 and were selected for the test in consideration of observations.
the light-curing mode of SureFil1 SDRTM. Notwithstanding the
decline in cement retentive strength with light attenuation at
the middle and apical levels, it can be inferred from this 5. Conclusions
studys findings that the amount of light reaching SureFil1
SDRTM through the above mentioned translucent posts was Within the limitation of this in vitro test, it can be concluded
sufficient to induce proper cement polymerization and the that SureFil1 SDRTM, a new light-cured flowable resin
development of adequate post retentive strengths. Therefore, composite originally proposed for bulk filling of posterior
there is evidence that SureFil1 SDRTM can be safely used for restorations, when used to lute fibre posts achieved retentive
intraradicular luting in combination with translucent posts. strengths similar to those of Calibra, a dual-cure luting agent
Conversely, significantly lower push-out strengths were marketed by the same manufacturer. As a one-component
measured in the present study by FibreKleer posts. These material, SureFil1 SDRTM does not require any mixing step,
dowels are made of glass fibres embedded in a methacrylate- thus further simplifying the handling. However, being a light-
based resin matrix and have a cylindrical shape with coronal cured resin composite, for a safe use of SureFil1 SDRTM as a
serrations. In a previous study FibreKleer posts measured luting agent, fibre posts of knowingly adequate translucency
significantly lower post pull-out strengths than the titanium should be preferred.
dowels ParaPost.32 Moreover, despite the manufacturers
claim of translucency, no light transmission was recorded
references
through FibreKleer serrated posts using a spectrophotome-
ter.26 The impairment in light transmission may reasonably
explain the low retentive strengths demonstrated by posts
1. Goracci C, Ferrari M. Current perspectives on post systems:
luted with SureFil1 SDRTM, that is a light-cured material.
a literature review. Australian Dental Journal 2011;56(Suppl.
Similarly low push-out strengths were measured also when 1):7783.
Calibra was used to lute FibreKleer posts. Although Calibra is 2. Bitter K, Kielbassa AM. Post-endodontic restorations with
a dual-cure luting agent, previous studies have pointed adhesively luted fiber-reinforced composite post systems: a
out that relevant properties of the cement, such as degree review. American Journal of Dentistry 2007;20:35360.
328 journal of dentistry 40 (2012) 322328
3. Cagidiaco MC, Goracci C, Garcia-Godoy F, Ferrari M. Clinical canal with and without fibre post insertion. Journal of
studies of fiber posts: a literature review. International Journal Dentistry 2011;39:4229.
of Prosthodontics 2008;21:32836. 20. Davidson CL, Feilzer AJ. Polymerization shrinkage and
4. Goracci C, Grandini S, Bossu` M, Bertelli E, Ferrari M. polymerization shrinkage stress in polymer-based
Laboratory assessment of the retentive potential of restoratives. Journal of Dentistry 1997;25:43540.
adhesive posts: a review. Journal of Dentistry 2007;35:82735. 21. Van Ende A, De Munck J, Mine A, Lambrechts P, Van
5. Naumann M, Blankenstein F, Dietrich T. Survival of glass Meerbeek B. Does a low-shrinking composite induce less
fibre reinforced composite post restorations after 2 years- stress at the adhesive interface? Dental Materials
an observational clinical study. Journal of Dentistry 2010;26:21522.
2005;33:30512. 22. Burgess J, Cakir D. Comparative properties of low-shrinkage
6. Dietschi D, Duc O, Krejci I, Sadan A. Biomechanical composite resins. Compendium of Continuing Education in
considerations for the restoration of endodontically treated Dentistry 2010;31:105. (Spec Iss 2).
teeth: a systematic review of the literature. Part II 23. Ilie N, Hickel R. Investigation on a methacrylate-based
(Evaluation of fatigue behavior, interfaces, and in vivo flowable composite based on the SDRTM technology. Dental
studies). Quintessence International 2008;39:11729. Materials 2011;27:34855.
7. Cagidiaco MC, Goracci C, Garcia-Godoy F, Ferrari M. Clinical 24. Koltisko B, Dai Q, Jin X, Bertrand S. The polymerization
trials of fiber posts: a literature review. In: Ferrari M, Breschi stress of flowable composites. Journal of Dental Research
L, Grandini S, editors. Fiber posts and endodontically treated 2010;89:321.
teeth: a compendium of scientific and clinical perspectives. 25. Jin X, Bertrand S, Hammesfahr PD. New radically
Wendywood: Modern Dentistry Media; 2008. p. 14963. polymerizable resins with remarkably low curing stress.
8. Ferrari M. Introduction. In: Ferrari M, Breschi L, Grandini S, Journal of Dental Research 2009;88:1651.
editors. Fiber posts and endodontically treated teeth: a 26. Goracci C, Corciolani G, Vichi A, Ferrari M. Light
compendium of scientific and clinical perspectives.. Wendywood: transmission ability of marketed fiber posts. Journal of Dental
Modern Dentistry Media; 2008. p. 913. Research 2008;87:11228.
9. Asmussen E, Peutzfeldt A, Heitmann T. Stiffness, elastic 27. Ho YC, Lai YL, Chou IC, Yang SF, Lee SY. Effects of light
limit, and strength of newer types of endodontic posts. attenuation by fibre posts on polymerization of a dual-cured
Journal of Dentistry 1999;27:2758. resin cement and microleakage of post-restored teeth.
10. Baba NZ, Golden G, Goodacre CJ. Nonmetallic prefabricate Journal of Dentistry 2011;39:30915.
dowels: a review of compositions, properties, laboratory, and 28. Radovic I, Corciolani G, Magni E, Krstanovic G, Pavlovic V,
clinical test results. Journal of Prosthodontics 2009;18:52736. Vulicevic ZR, et al. Light transmission through fiber post: the
11. Hatta M, Shinya A, Vallittu OK, Shinya A, Lassila LV. High effect on adhesion, elastic modulus and hardness of dual-
volume individual fibre post versus low volume fibre post: cure resin cement. Dental Materials 2009;25:83744.
the fracture load of the restored tooth. Journal of Dentistry 29. Navarra CO, Goracci C, Breschi L, Vichi A, Corciolani G,
2011;39:6571. Cadenaro M, Ferrari M. Influence of post type on degree of
12. Monticelli F, Ferrari M, Toledano M. Cement system and conversion of a resin-based luting agent. American Journal of
surface treatment selection for fiber post luting. Medicina Dentistry, 2012, in press.
Oral Patologia Oral y Cirurgia Bucal 2008;13:E21421. 30. Giachetti L, Scaminaci Russo D, Bertini F, Giuliani V.
13. Radovic I, Monticelli F, Goracci C, Vulicevic ZR, Ferrari M. Translucent fiber post cementation using a light-curing
Self-adhesive resin cements: a literature review. Journal of adhesive/composite system: SEM analysis and pull-out test.
Adhesive Dentistry 2008;10:2518. Journal of Dentistry 2004;32:62934.
14. Bagheri R, Mese A, Burrow MF, Tyas MJ. Comparison of the 31. Teixeira CS, Silva-Sousa YC, Sousa-Neto MD. Effects of light
effect of storage media on shear punch strength of resin exposure time on composite resin hardness after root
luting cements. Journal of Dentistry 2010;38:8207. reinforcement using translucent fibre post. Journal of
15. Breschi L, Mazzoni A, Ferrari M. Adhesion to intra-radicular Dentistry 2008;36:5208.
dentin. In: Ferrari M, Breschi L, Grandini S, editors. Fiber 32. Kelsey WP, Latta MA, Kelsey MR. A comparison of the
posts and endodontically treated teeth: a compendium of scientific retention of three endodontic dowel systems following
and clinical perspectives. Wendywood: Modern Dentistry different surface treatments. Journal of Prosthodontics
Media; 2008. p. 1537. 2008;17:26973.
16. Lindblad RM, Lassila LV, Salo V, Vallittu PK, Tjaderhane L. 33. Arrais CA, Giannini M, Rueggeberg FA. Effect of sodium
Effect of chlorhexidine on initial adhesion of fiber-reinforced sulfinate salts on the polymerization characteristics of dual-
post to root canal. Journal of Dentistry 2010;38:796801. cured resin cement systems exposed to attenuated light-
17. Tay FR, Loushine RJ, Lambrechts P, Weller RN, Pashley DH. activation. Journal of Dentistry 2009;37:21927.
Geometric factors affecting dentin bonding in root canals: a 34. Arrais CA, Rueggeberg FA, Waller JL, de Goes MF, Giannini
theoretical modeling approach. Journal of Endodontics M. Effect of curing mode on the polymerization
2005;31:5849. characteristics of dual-cured resin cement systems. Journal
18. Ferrari M, Carvalho CA, Goracci C, Antoniolli F, Mazzoni A, of Dentistry 2008;36:41826.
Mazzotti G, et al. Influence of luting material filler content 35. Latta MA, Kelsey 3rd WP, Kelsey 5th WP. Effect of
on post cementation. Journal of Dental Research 2009;88:9516. polymerization mode of adhesive and cement on shear
19. Aksornmuang J, Nakajima M, Senawongse P, Tagami J. bond strength to dentin. American Journal of Dentistry
Effects of C-factor and resin volume on the bonding to root 2006;19:96100.