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Article history: In this research, the overall heat transfer coefcient of CuO/water nanouids is investigated experi-
Received 23 May 2012 mentally under laminar ow regime (100 Re 1000) in a car radiator. The experimental system is
Received in revised form quite similar to cars cooling system. The nanouids in all the experiments have been stabilized with
26 November 2012
variation of pH and use of suitable surfactant. The results show that the overall heat transfer coefcient
Accepted 27 November 2012
Available online 2 January 2013
with nanouid is more than the base uid. The overall heat transfer coefcient increases with the
enhancement in the nanouid concentration from 0 to 0.4 vol.%. Conversely, the overall heat transfer
coefcient decreases with increasing the nanouid inlet temperature from 50 to 80 C. The imple-
Keywords:
Nanouid
mentation of nanouid increases the overall heat transfer coefcient up to 8% at nanouid concentration
Overall heat transfer coefcient of 0.4 vol.% in comparison with the base uid. In addition, the results are statistically analyzed using
CuO Taguchi method by implementing Qualitek-4 software. The maximum value of the overall heat transfer
Radiator coefcient with nanouid, effect of each operating parameter on the overall heat transfer coefcient and
Experimental design the optimum values of each parameter are determined.
Taguchi method 2012 Elsevier Masson SAS. All rights reserved.
1290-0729/$ e see front matter 2012 Elsevier Masson SAS. All rights reserved.
http://dx.doi.org/10.1016/j.ijthermalsci.2012.11.013
M. Naraki et al. / International Journal of Thermal Sciences 66 (2013) 82e90 83
developed region were found to increase by 17% and 27%, respec- In the literature, the tube-side heat transfer coefcients of
tively, for alumina/water nanouid at 6 vol.% with respect to pure different types of nanouids are usually reported which need the
water. The zirconia/water nanouid heat transfer coefcient temperature at the tube wall to be measured. The wall temperature
enhanced approximately 2% in the entrance region and 3% in the measurement involves operational difculties and has some
fully developed region at 1.32 vol.%. Farajollahi et al. [9] measured inherent errors which may result in inaccurate heat transfer coef-
the heat transfer characteristics of g-Al2O3/water and TiO2/water cient. Since the tube wall thickness is very small (especially in the
nanouids in a shell and tube heat exchanger under turbulent ow case of the car radiator), installing thermocouples inside the wall is
condition. According to their report, the maximum enhancement of almost impossible. Therefore, measurement of wall temperature is
the overall heat transfer coefcient of g-Al2O3/water nanouids very hard to perform and authors usually follow some calibration
was approximately 20% which occurred at 0.5% volume concen- procedure to revise their wall temperature. As a result, in this
tration and Peclet number about 50,000. At this Peclet number, the research, overall heat transfer coefcient is measured in a car
enhancements of the overall heat transfer coefcient at 0.3%, 0.75%, radiator which does not need the wall temperature measurement.
1%, and 2% nanoparticle volume concentrations were about 14%, In addition, the experimental results have been statistically
16%, 15%, and 9%, respectively. For TiO2/water nanouids the analyzed using Taguchi method by implementing Qualitek-4
maximum enhancement was observed at 0.3% particle volume software.
concentration. Fotukian and Esfahany [10] experimentally studied
convective heat transfer of dilute CuO/water nanouid inside 2. Nanouid preparation and stabilization
a circular tube. They used nanouids with nanoparticles volume
fractions less than 0.3%. The heat transfer coefcient increased Preparation of a stabilized nanouid is of great importance in
about 25% compared with pure water. Xie et al. [11] demonstrated heat transfer applications of nanouids. Poorly prepared nano-
that using Al2O3, ZnO, TiO2, and MgO nanouid with a mixture of uids will render biphasic heat transfer (i.e. solideliquid). Another
55 vol.% distilled water and 45 vol.% ethylene glycol as the base uid challenge is posed by nanoparticle aggregation which creates
in laminar ow inside a circular copper tube with constant wall larger particles (in micrometer order), thus eliminating the nano-
temperature could enhance the convective heat transfer. MgO, related discussions. Furthermore, particle instability results in
Al2O3, and ZnO nanouids exhibited superior enhancements of particle fouling in reservoir, pipes, pumps and other equipment of
heat transfer coefcient, with the highest enhancement up to 252% thermal cycle, all of which are considered undesirable factors in
at a Reynolds number of 1000 for MgO nanouid. Leong et al. [12] our experiment. The copper oxide nanoparticles used in this study
investigated the performance of Cu/EG nanouids in an automotive are approximately spherical with the diameter of about 60 nm.
car radiator. They revealed that in the nanouid-based coolants an Some other properties of the nanoparticle are shown in Table 1.
overall heat transfer coefcient of 164 W/m2 K can be achieved for The nanouid has been stabilized with variations of pH and using
2 vol.% Cu/EG nanouid compared with 142 W/m2 K for the base SDS (Sodium Dodecyl Sulfonate) surfactant. For stabilization of
uid. Peyghambarzadeh et al. [13] investigated the forced convec- nanouid, the pH of suspension was changed to obtain the
tive heat transfer of Al2O3/water nanouid in an automobile radi- optimum value (the pH in which the suspension is more stable)
ator. They concluded that the heat transfer enhancement was about using NaOH 1 M solution. At the mentioned pH, nanouid samples
45% compared with pure water at the concentration of 1 vol.%. In were made in different concentrations of surfactant. According
other work, Peyghambarzadeh et al. [14] measured forced to the previous studies to nd out the optimal pH, samples with
convective heat transfer coefcient of Al2O3/mixture of water and pH of 6.2, 8.2, 9.14, 10.1, 11 and 12.1 were prepared. The sample
EG in a car radiator. They reported that in the best conditions, the with pH 10.1 showed more stability than the others. At the
heat transfer enhancement of about 40% compared with the base optimum pH (pH 10.1), samples with different concentrations of
uids has been recorded. Zamzamian et al. [15] investigated 0.04, 0.08, 0.1, 0.2, 0.3 and 0.4 wt.% of SDS surfactant were
experimentally the forced convective heat transfer coefcient in prepared. As shown in Fig. 1, the sample with concentration of
Al2O3/EG and CuO/EG nanouids in a double pipe and plate heat 0.2 wt.% SDS surfactant and at pH 10.1 had the lowest nano-
exchangers under turbulent ow. Their ndings indicated consid- particle sedimentation and highest stability after 60 h in
erable enhancement in convective heat transfer coefcient of the a stationary state.
nanouids as compared with the base uid, ranging from 2% to 50%.
Moreover, the results indicated that the convective heat transfer
3. Experimental setup
coefcient of nanouid increases with enhancing nanoparticles
concentration and nanouid temperature. Leong et al. [16] revealed
As shown in Fig. 2, the schematic of experimental system used
the convective heat transfer coefcients and the overall heat
in this research includes ow lines, a reservoir tank, two heaters,
transfer coefcients of copper/water nanouid were higher than
a centrifugal pump, ow meter, a forced draft fan, an air ow
that of base uid in a shell and tube heat recovery exchanger. They
channel, a temperature controller, four thermocouples and a cross
reported that about 16.9% enhancement was recorded for ethylene
ow heat exchanger. The test section is a cross ow heat
glycol with 1% copper nanoparticles compared with base uid.
exchanger (an automobile radiator) which was installed inside the
Saeedinia et al. [17] reported that CuO nanoparticles suspended in
air ow channel and its conguration is the louvered n-and-tube
base oil increase the heat transfer coefcient even for a very low
particle concentration of 0.2 wt.%. The maximum heat transfer
coefcient enhancement of 12.7% is obtained for 2 wt.% nanouid at Table 1
highest Reynolds number compared with that of base oil. Sundar Some characteristics of copper oxide nanoparticle.
et al. [18] evaluated experimentally the convective heat transfer Copper oxide (CuO) nanopowder
coefcient of Fe3O4 nanouid for ow in a circular tube at the range Appearance Black powder
of 3000 < Re < 22,000 and the volume concentration range of Purity 98%
0 < C < 0.6%. Nanouid heat transfer was higher compared with Grain size (nm) 60 nm
water and increased with volume concentration. The heat transfer Specic surface area (m2/g) 80
Actual density (gr/cm3) 6.4
coefcient was enhanced by 30.96% at 0.6% volume concentration Appearance density (gr/cm3) 0.79
compared with the ow of water at similar operating conditions.
84 M. Naraki et al. / International Journal of Thermal Sciences 66 (2013) 82e90
type. Nanouid passes through the 34 vertical tubes with working uid, two electrical heaters (6000 W) and a temperature
stadium-shaped cross section. The ns and the tubes are made controller were used to vary the temperature between 40 and
with aluminum. The size and dimensions of the radiator is shown 80 C. Four RTDs (Pt-100U) were implemented on the ow line to
in Table 2. For cooling the liquid, a forced draft fan (Techno Pars record air ow and radiator uid inlet and outlet temperatures.
1400 rpm) which is capable of adjusting the air ow speed from The temperatures from the thermocouples were measured by four
low to high, was installed close and face to face to the radiator at digital multimeters, SU-105PRR, SAMWON ENG, with an accuracy
the beginning of the air ow channel and consequently air and of 0.1 C.
water have indirect cross ow contact and there is heat exchange
between hot water owing in the tube-side and air across the 3.1. Uncertainty analysis
tube bundle. The inlet air temperature was about 35 C 0.2 C in
the whole experiments. The pump gives a constant ow rate of Uncertainty analysis is carried out by calculating the error of the
0.6 m3/h, the ow rate to the test section is regulated by appro- measurements. The uncertainty range of Reynolds number comes
priate adjusting of a globe valve on the recycle line. The working from the errors in the measurement of volumetric ow rate and
uid lls 35% of the reservoir tank whose total volume is hydraulic diameter of the tubes and the uncertainty of overall heat
approximately 20 l (height of 30 cm and diameter of 30 cm). The transfer coefcient refers to the errors in the measurements of
total volume of the circulating liquid is constant in all the volumetric ow rate, hydraulic diameter, and all the temperatures.
experiments. Five layer insulated tubes (Isopipe 0.75 in diameter) According to standard uncertainty analysis, the measurement
have been used as connecting lines and covered with glass wool uncertainty in liquid side Re number is 5.2% and for the overall
to reduce heat loss to the surrounding. A ow meter (Technical heat transfer coefcient is 15.1%. Furthermore, to check the
Group LZM-15Z Type) was used to control and manipulate the reproducibility of the experiments, some runs were repeated later
liquid ow rate with the precision of 0.006 m3/h. For heating the which proved to have excellent repeatability.
By assuming that the nanoparticles are well dispersed within 5. Calculation of heat transfer coefcient
the base uid, i.e. the particle concentration can be considered
uniform throughout the system; the effective thermophysical In these experiments, the nanouid owing inside the tube
properties of the mixtures can be evaluated using some classical transfers heat to the outside air owing in the air ow channel. The
formulas as usually used for two phase ow. The following corre- air-side and the tube-side heat transfer rates can be calculated as:
lation has been used to predict nanouid density at different
temperatures and concentrations [12e14]: _ a Cp;a Ta;o Ta;i
Qa m (5)
Nu 0:951 Re0:173
D Pr1=3 (14)
Af
ho 1 1 h (15)
Ao
Ao Af Ab (16)
Ao is the total surface area of the nned tube, Af is surface area of the Fig. 3. Comparison between the measured overall heat transfer coefcient and the
n, Ab is surface area of the bare tube. The n efciency, h, can be predicted values for distilled water.
approximated from the Schmidt approximation [25] as follows:
ow rate increases with nanoparticle concentration compared with
tanhml
h ; (17) the base uid. The maximum enhancement of the overall heat
ml
transfer coefcient of CuO/water nanouids occurs at 0.4 vol.%
where concentration of nanoparticle which is approximately 8%
comparing with the base uid. The enhancement of the overall heat
s
2ho transfer coefcient at the concentration of 0.15 vol.% of the nano-
m ; (18) particle is about 6%.
kf ft
These increases in the overall heat transfer coefcient with
nanouid can be explained by the increase of heat transfer ef-
where kf is the thermal conductivity of the n, l is the n length and
ciency due to the enhancement of thermal conductivity, the acti-
ft is the n thickness. The air-side heat transfer coefcient can be
vation of convective heat transfer or the thinning of thermal
calculated from Vithayasai et al. [22] correlation suggested for the
boundary layer. In addition, there will be one important mecha-
radiator as:
nism for this enhancement on thermal conductivity of nanouid in
the piping ow. That is the non-uniform particle concentration in
Nua 10:145 LnRea 46:081 Pra0:33 (19)
the cross-section of the tube. Ding and Wen [26] investigated that
the particle migration by shear rate gradient, viscosity gradient, and
Brownian motion causes non-uniformity in particle concentration
6. Results and discussions
Fig. 5. Effect of inlet nanouid temperature on the overall heat transfer coefcient Fig. 7. Effect of nanouid volumetric ow rate on the overall heat transfer coefcient
with nanouid. of CuO/water nanouid in the car radiator.
88 M. Naraki et al. / International Journal of Thermal Sciences 66 (2013) 82e90
the overall heat transfer coefcient with nanouid are 79.30 and Table 3
81.23 W/m2 K at the nanouid volumetric ow rate of 0.4 and Number of factors and levels in each factor.
Table 4
L9 array selected for experiments and the corresponding experimental results.
Columns U (W/m2 K)
Trial 1 1 1 1 1 72.13
Trial 2 1 2 2 2 76.44
Trial 3 1 3 3 3 82.54
Trial 4 2 1 2 3 88.19
Trial 5 2 2 3 1 79.60
Trial 6 2 3 1 2 73.91
Trial 7 3 1 3 2 91.61
Trial 8 3 2 1 3 78.74
Fig. 8. Effect of air Reynolds number to heat transfer coefcient of CuO/water nano-
Trial 9 3 3 2 1 76.68
uid in car radiator.
M. Naraki et al. / International Journal of Thermal Sciences 66 (2013) 82e90 89
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