Beruflich Dokumente
Kultur Dokumente
Squeeze Cementing
with Coiled Tubing
i
All information contained in this publication is confidential and proprietary property of
Halliburton Energy Services, Inc. Any reproduction or use of these instructions, drawings, or
photographs without the express written permission of an officer of Halliburton Energy
Services, Inc. is forbidden.
1999, Halliburton Energy Services, Inc.
All Rights Reserved. Printed in the United States of America.
Printing History:
First Release (August 1999)
Revised (November 2001)
ii
Best Practices
Contents
Introduction ................................................................................................................. 1
Contents
Density .................................................................................................................. 16
Compatibility .......................................................................................................... 24
Contents
Summary ............................................................................................................... 28
Channels ............................................................................................................... 29
Figure 9Fresh water (85F, calculated critical flow rate = 0.02 bbl/min) ........ 32
Figure 1115.8-lb/gal Class H cement (PV = 27.5 cp; YP = 9.8 lb/100 ft2;
120F; calculated critical flow rate = 0.44 bbl/min) ........................................... 33
Equipment ............................................................................................................. 34
Contents
Underreaming ................................................................................................... 43
References ................................................................................................................ 44
Bibliography .............................................................................................................. 45
Contents
This manual describes the best practices and recommended slurry properties for squeeze
cementing with coiled tubing (CT). However, most of the laboratory and slurry behavior
information applies to all squeeze cementing. This chapter also presents information perti-
nent to the nodal buildup/washout squeeze method.
An extensive bibliography (Page 45) has been included for all subjects discussed. These
references are not limited to CT or squeeze cementing.
Introduction
Squeeze or remedial cementing is a common operation in the petroleum industry. Most
squeezes are performed with a drilling or workover rig and through threaded tubing or
drillpipe. Cement is the most common material used for squeezing and represents approxi-
mately 7 to 10% of the total cost of the squeeze. The remaining costs stem from well prepa-
ration, tools, waiting on cement (WOC), and drilling out excess cement left in the wellbore
after the squeeze. As reservoirs mature and production subsequently declines, the remedial
costs weigh heavily on the decision of remedial work or abandonment.
Techniques and cement properties developed or identified by British Petroleum (BP) and
Atlantic Richfield Company (ARCO) for Alaskan North Slope operations have served as the
foundation for CT squeezing worldwide. From this foundation, special techniques and
material properties have been developed that improve the probability of success and in-
crease the cost-saving potential.
Most recently, the advent of microfine cementing products and conformance technology has
enabled treatments to be performed through gravel-packed intervals without the costly
removal of downhole production equipment. Under certain situations, methods learned from
the nodal technique can apply to squeezing through a gravel pack.
CT offers significant benefits for slurry placement, control of the squeeze, and reduced
squeeze costs. However, the full potential offered by the technique depends on candidate
selection and preparation, cement slurry formulation, and job design. Small-volume and
nodal-buildup jobs require special and preferably on-location quality-control testing.
repair leaks in well tubulars and restore pressure integrity to the wellbore
raise the level of or restore a cement sheath behind the casing to support or protect well
tubulars
modify the production or injection profile of a well by sealing unwanted production or
thief zones
repair a poor primary cement job before well completion
Successful squeeze operations depend on accurate problem identification and careful selec-
tion of the appropriate sealant, mixing/pumping equipment, and placement technique. After
the job has been properly designed and the problem interval has been isolated, inject cement
slurry or another suitable sealant material into the interval to be sealed or filled. To ensure
success, apply pressure to hold the sealant in place until it hardens or takes set. When the
sealant is cement, pressure should be applied to remove (squeeze) fluid from the slurry and
to form an immovable, impermeable mass that will set and harden in place. The remaining
cement or other sealant should be removed from the interior of the wellbore to restore the
original inner diameter (ID) of the wellbore for future operations.
Note When in doubt about the actual circulating temperature, use the
static temperature at the squeeze depth.
Without cooling
With cooling
ccd01005
into the perforations during placement. In this case, always make sure a jet nozzle is used to
wash and clean up all the perforations after placement of the rathole material. The wash fluid
must also have sufficient carrying capacity to lift any solids encountered to the surface.
Failure to do so can result in solids bridging in the annulus around the CT string. Note that
this rathole fluid should be heavier than the planned cement slurry.
Problem Diagnosis
The following tools can help define a problem requiring a squeeze and the location to be
treated:
Production or injection logs for perforation evaluation help characterize the nature of the
contribution or injection from all intervals and can be used to troubleshoot repeat squeezes.
A typical log includes a flowmeter reading, the temperature, pressure, fluid density (from a
gradiometer or radioactive densiometer), neutron density, and resistivity probe. These logs
help determine the source of the fluid or gas entry. Potential alternatives (plugback, and
material and treatment-volume selection) can be developed, and the section to be
reperforated can be determined.
A pump-in survey with a temperature log can help determine the existence and direction of a
channel. The survey can also define the rate of temperature change. After injection or
circulation and pumping have stopped, the temperature slowly returns to the geothermal
gradient. At least 5 to 10F of initial cooling should be reached to obtain sufficient tempera-
ture shift for channel identification.
The temperature profile can also provide information vital to the thickening time for cement-
slurry design. The rate of warming after a certain amount of fluid is pumped is also helpful.
Knowledge of the thermal recovery after the treatment is placed allows job designers to
better estimate how long the fluid will remain pumpable if it is allowed to become static
(cement slurry or polymer treatment).
A pulsed-neutron log with borax brine water injected into the perforations also helps define
the extent of a channel. However, the log is omnidirectional and does not identify the
orientation or azimuth of a channel behind pipe.
A downhole video camera or casing-caliper log can be used in areas where severe corrosion
or erosion is suspected. Filter cakes form readily in perforations across permeable zones,
but the enlarged surface area of severely corroded casing may hamper long-term results
from a squeeze. Knowledge of the condition of the casing can help engineers determine the
operations feasibility and cost effectiveness.
Well Preparation
The preparation of the wells mechanical systems and the interval to be squeezed are critical
to success. Controlling other variables in the squeeze cannot compensate for improperly
preparing the well for the operation.
Completion Packers
A packer leak can also allow cement into the annulus and make future workovers difficult.
Packers can come unseated from applied squeeze pressure and tubing contraction because of
cooldown. These limitations must be considered as they would in any other squeeze.
Consider the presence of gas-lift valves when appropriate. Replace all gas-lift valves with
blanks, or take other appropriate measures to ensure that the valves are not damaged with
cement. To prevent valve exposure to cement during a planned reverse-out squeeze, replace
all but one valve with blanks, leaving the valve in the uppermost station for immediate
unloading.
Isolation Barriers
Physically isolate the interval to be treated to ensure controlled placement. Depending on the
design of the wellbore, complete isolation is sometimes impossible, but every attempt should
be made within the limits of the mechanical restrictions, cost, logistics, and risk.
If a significant rathole exists beneath the interval to be treated, large volumes of cement may
fall into the rathole instead of passing into the perforations. This occurrence has been proven
by field results and large-scale laboratory testing. Fill the rathole with sand, or use another
means to help prevent fluid swapping.
Note Often, pumping an extra volume of cement slurry to spot and fill
the rathole is the most cost-effective method for preventing fluid
swapping if the lower section of the well will not be re-entered.
Figure 2 shows a typical isolation method with multiple zones protected from the treatment.
In this complex situation, the intent was to treat a middle zone while protecting the upper
and lower zones. Variations of this situation could include the following:
Production tubing
and packer
Inflatable packer
Treatment fluid
Lower zone
Sand protected by sand
ccd01006
Cement or other sealant must penetrate into the leak path or unfilled area for a successful
squeeze job. Any injected fluid, especially a solids-laden one such as cement, always seeks
the path of least resistance. Therefore, removing all of the following types of nonsealing
debris is essential:
inorganic scale
pipe dope
organic deposits such as paraffin and asphaltenes
metallic debris caused by milling, perforating, and corrosion
The interval can be cleaned through one or more of the following techniques:
Pressure or chemical treatments (or a combination of) are common, effective ways to open a
leak path and prepare surfaces for sealant adhesion. Pressure surging alone may remove only
some debris, whereas chemical treatments may selectively remove other forms of debris.
Usually, a combination of a chemical treatment with one or more pressure-differential
techniques is most effective.
The combination of pressure from the hydrostatic column and the surface must initially be
equal to the formation pressure (i.e., the well has to be stabilized). In addition, if any fluid is
present, the fluid level must be low enough to provide an underbalance to the formation
pressure when the surface pressure is removed. If the fluid level in the well is unknown, it
can be estimated with the procedure in Appendix A (Page 47).
Perforation surging can be performed by setting a lock assembly in a profile nipple. The
assembly should include a nipple on the bottom adapted to hold a shear disk. After the
assembly is set near the bottom of the completion, the wellhead pressure (WHP) is decreased
until the differential pressure across the disk exceeds its shear value and fails. An instanta-
neous pressure surge occurs across the perforations, forcing out removable debris. An
alternative approach for assisting a well with insufficient BHP overcome the pressure in the
fluid column involves a coil-conveyed lock assembly (or packer) used with a circulating sub.
Positive differential pressure is also applied to the perforations during the application of
squeeze pressure during the cement job, causing filter-cake development. However, exces-
sive pressure too early in the treatment can fracture the formation or cause communication
with naturally occurring fractures, which can be difficult to heal.
Though formation fracturing can be detrimental, a pressure break at a pressure below the
fracture gradient indicates a perforation cleaning up during the squeeze. This diversion is
often the only way to clean out perforations. A high-pressure squeeze is designed to establish
a filter cake in all clean perforations during the initial pressure-increase stages of the
squeeze. As these first clean perforations are sealed with cement filter cake, any weaker
blockages caused by debris are removed, establishing communication with formation perme-
ability or channels behind pipe. Before continuing with the pressure increase, reduce pres-
sure to allow filter-cake development to resume. Filter-cake properties and associated slurry
requirements are discussed in detail in Interpreting Thickening-Time Test Results, (Page
17) and Fluid-Loss Testing and Filter-Cake Evaluation, (Page 17).
The potential advantage of this technique is to provide a differential across perforations that
cannot otherwise be cleaned of debris while other perforations are open. However, pressure
breaks are sometimes erroneously interpreted as a formation breakdown, and the slurry is
immediately pumped away in preparation for a second job. Job designers should be aware of
formation fracture gradients to prevent this misdiagnosis.
Chemical Treatments
Acidizing is commonly used as an integral part of cleanout. When the treatment procedure
does not provide for a prolonged flowback to enable the dissipation of residual acid,
overdisplace the treatment to protect the filter cake established during the squeeze from acid
attack. If the targeted problem is a channel behind pipe, a mud-acid or oxidizer treatment
may be required for removing clay-based solids or polymers, respectively.
Remove organic deposits such as pipe dope, paraffin, or asphaltenes that may be present in
the interval to be squeezed because cement does not bond well to these deposits. Chemical
treatments with xylene, diesel, paraffin solvents, etc. may be required. A mixture of xylene
or toluene in diesel with acetic acid and a mutual solvent effectively removes organic
deposits. Table 1 lists common generic cleaning formulas. For detailed information, consult
the Scale Removal and Control section under Frac/Acid Services on the HalWorld intranet
web site.
Table 1Cleaning Formulas for Common Chemical Deposits
Debris Type Formula Treatment Volume (gal/ft)
Calcium carbonate scale 10 to 15% HCl 20 to 30
Calcium sulfate (gyp) scale GYPSOL Process Consult acidizing manual
Cement or silica/silicate scale 12:3 mud acid 20 to 50
Paraffin/asphaltenes Paraffin solvent or xylene/toluene 20 to 40
Mixture of paraffin/asphaltenes 12% HCl + 10% xylene or 50:50 30 to 40
and scale xylene/toluene and 10 to 15%
HCl
Pipe dope or mixture of 70:20:10 volume ratio of xylene 30 to 50
paraffin/asphaltene with rust/metal or toluene (acetic acid: mutual
solvent)
Mechanical Methods
In some cases, the materials blocking an interval may not be soluble in acid or organic
solvents. In that case, mechanical methods of removal, including jetting or scraping, are
required before squeezing. Barium and strontium sulfate scales and high concentrations of
silicate scales are examples of these materials.
Injectivity Testing
Injectivity testing assesses the intervals capacity to accept fluid, which is vital for designing
and executing the operation. Accurate information from the injectivity test aids material
selection, squeeze-operation design, formulation of the cement slurry or other sealant, and
volume selection.
Injectivity testing before the squeeze operation helps the engineer identify the feasibility of a
treatment and aids in troubleshooting a producer well or an injector well. When numerous
squeezes are conducted in an area on a particular interval, a threshold injectivity is often
used as a guide for determining treatment options.
Clean, solids-free fluids are required for injectivity testing. If a solids-laden fluid is used,
fracturing the formation will probably be required for fluid injections into the interval,
unless the formation has vugs, natural fractures, acid-etched flow paths, or hydraulic frac-
tures from stimulations.
1. Pump the fluid into the target interval at a constant rate while monitoring surface pres-
sure. Record the rate and pressure pairs at each step for use in the squeeze design. (An
initial rate of about 1 bbl/min is often used.)
2. Continue pumping at this rate until the pressure has stabilized (is not increasing rapidly).
Use field experience in the area and fluid-friction simulation to help determine whether
or not perforation cleanup is required.
3. Repeat Steps 1 and 2 at various rates until you establish a profile. Use these data with
squeeze-slurry hydrostatics to help design the final surface-pumping pressure schedules.
4. If formation breakdown is evident at injection rates lower than expected, consider
performing a perforation cleanup treatment.
5. Use any indicated formation breakdown pressure plus a safety factor to help determine
the squeeze pressure to be applied during the early stages of the treatment.
Important The fluid should not form scale with the formation water, cause
swelling or migration of sensitive clay minerals, or form
emulsions or fluid blocks.
The fluid must be recoverable if the interval is to resume productivity. The formation may
inhibit matrix injection of permanent clear fluids such as PermSealTM or Injectrol sealants.
Some highly water-sensitive formations may require the use of nonaqueous fluids such as
diesel, mineral oil, or synthetics, and MOC/OneTM cement as the treatment system.
Clean, filtered fluids, such as filtered formation brine or weighted, artificial brines, are
typically recommended for injection tests. Surfactants, nonemulsifers, mutual solvents, and
clay stabilizers can be added to protect sensitive formations. Gas wells are prone to fluid
blocks, which may inhibit returned productivity. Surfactants can sometimes help reduce this
effect.
Krilov, et al.1 discuss the level of damage to formation permeability caused by the precipita-
tion of insoluble calcium salts by cement filtrate and migration of fine particulates caused by
clays released because of the high pH (generally >12) of cement filtrate. Though these
chemical and physical observations are significant, large pore volumes of filtrate flowed
through the cores (more than would probably result if a cement filter cake formed at the face
of the core), greatly reducing penetration distance. In most critical squeezes, slurry fluid loss
is low. The depth of penetration of the filtrate would be limited to a few millimeters, which
could be easily penetrated by perforating guns.
Wells with an injectivity between 1 and 3 bbl/min have been successfully squeezed with CT
with the cement properties and techniques described later in this section. An injectivity rate
greater than 3 bbl/min at low pressures may indicate the presence of high-permeability flow
paths, such as fractures, vugs, solution channels, etc. Larger treatment volumes and a rela-
tively higher slurry fluid loss (at least for a lead slurry) may be required in these cases.
Consider using reactive treatments, such as Flo-Chek service, before the cement squeeze.
Injectivity can also provide information about the possible extent of wellbore cooling. The
information can be used in designing and testing the cement slurry. Low injectivity may
preclude cooling the interval, thereby affecting the cement-slurry design in a hot well. A well
with a low injectivity and a high BHP may require a circulation kill before the squeeze. The
kill fluid should be dense enough to help reduce the surface pressure on the CT to acceptable
levels.
Material Selection
The variety of materials available for squeezes (Table 2, Page 12) can be mixed and pumped
with the same equipment commonly used with conventional cement slurries. CT operations
are not significantly restricted to the use of any of these materials.
The selection of the material for a particular squeeze should be based on present and ex-
pected future well conditions. In general, the selected material should
penetrate the area to be filled under the pressure limitations of the workstring (CT),
formation, well tubulars (casing and tubing), and wellbore equipment (packers,
valves, etc.)
adhere to surfaces to form an effective seal
withstand wellbore conditions (temperature and pressure), changes in wellbore stresses
(pressure or thermal cycling), and future treatments (acidizing, fracturing, and enhanced
recoveries)
Portland cements mixed with water and additives are the primary sealants for most squeezes,
but cement slurries are not suitable for all conditions and operations. The following para-
graphs briefly describe the materials listed in Table 2. For detailed coverage of sodium
silicates and other noncement fluids, refer to the Halliburton Conformance Technology
Manual2 or the appropriate bulletin.
Internally catalyzed sodium silicate systems (Injectrol service, Angard system, and Anjel
system) are low- or no-solids, low-viscosity fluids that can penetrate the natural permeability
of a formation a significant distance from the wellbore. These systems are used to form
barriers between zones. Crosslinking or gel times are adjusted by the mixture ratio of inter-
nal activators to sodium silicate. The cement slurry pumped behind the silicate provides a
high-strength barrier at the wellbore. These systems are usually used to control water-
injection wells, plug fractures, and help prevent water coning.
Most polymer treatments do not develop compressive or tensile strength and may not pro-
vide long-term durability if exposed to high differential pressures during production. Addi-
tionally, the positive pressures of most cement squeezes are not possible or even necessary in
the application of a solids-free polymer system. The systems are, therefore, often followed
by a cement slurry that helps seal the path close to the wellbore and helps provide a positive
squeeze pressure.
The following special formulations and types of Portland cements have been developed to
meet challenges presented by special squeeze-cementing requirements. The Halliburton
Cementing Technology Manual3 and the HalWorld intranet web site give detailed informa-
tion about these slurries.
Salt acts as a retarder or an accelerator, depending on its concentration. Salt also helps
prevent the swelling of water-sensitive clays and shales and promotes cement bonding to
salt formations.
Solid, granular, or flaked bridging agents (Flocele and walnut hulls) are used during a
squeeze to help limit cement penetration into a fracture.
Crystalline silica in different forms (SSA-1 and SSA-2 agents and MicroSand cement
additive) has different uses. Silica flour combats the retrogression of cement compres-
sive strength at temperatures > 230F. Coarse sand is also used as a bridging agent.
Latex (Latex 2000 additive) is used in a cement formulation that may be exposed to acid
or other corrosive elements to slow the rate of attack. Cases have shown that 50 to 75%
of wells squeezed with Class G cement failed during subsequent acid stimulations.
However, less than 30% failed with latex cements. True acid-resistant systems are also
available (Epseal sealant, FlexCemSM service, and StrataLock system).
Expansive additives (Super CBL and MicroBond cements) help enhance sealing
properties.
Non-Portland Cements
High-aluminate cements and refractory cements, such as Cement Fondu cement, are useful
for high temperatures. Magnesium-salt cements and high calcium carbonate blends, such as
FDP-C558, have become popular for workovers because they are completely soluble in
hydrochloric acid.
density
thickening time
fluid loss
rheology
free water and settling
compatibility
compressive strength
These tests represent a composite set of conditions and procedures based on the well depth,
type of cementing operation, and geothermal gradient. The most recent API recommended
practice4 has been expanded to cover the special considerations developed over the years for
critical cementing.
Although improved, the API recommended practices do not specifically address CT cement-
ing. Additional testing often considered for critical cementing and CT cementing include
filter-cake evaluation, HTHP gel strength, acid resistance, and slurry shear sensitivity.
Job-specific test procedures and schedules should be developed for modeling the planned CT
squeeze cementing as closely as possible. Job-specific information needed for formulating
customized test schedules includes the following:
Density
Density is usually based on compressive-strength needs, well control, formation fracture
pressure, and slurry stability requirements. For CT squeezes, consider the effect of the
cement-slurry density on CT stresses. Cement strength should not be a significant factor in
density selection for squeezing because a well-formed filter cake probably has the compres-
sive strength of several thousand pounds per square inch, even for lightweight slurries.
Variation always exists between calculated and measured density because of differences in
material-specific gravities and instrument error. Match the slurry density between that
measured in the laboratory and on the field slurry. Filter-cake development is affected by
slurry density. For critical situations, verify slurry density in the laboratory with a cali-
brated, pressurized mud balance. Follow the same procedure on the batch-mixed slurry on
location before pumping.
Thickening-Time Tests
Thickening time is a measure of how long a cement slurry or other sealant remains pumpable
during the squeeze under expected well conditions. The API4 defines thickening time as the
time it takes for the slurry to reach 70 or 100 Bearden units (Bc) under simulated well-
cementing conditions. The Bearden unit is a dimensionless value describing slurry consis-
tency.
Although 70 or 100 Bc is the API definition, some operators use different consistency
values, ranging from 40 to 70 Bc, to determine the thickening time. Although the values are
not the API-defined thickening time, they represent consistencies that are practical limits for
most situations. Halliburton normally defines thickening time as the time required for the
slurry to reach 70 Bc. A consistency over approximately 40 Bc is unpumpable for CT
applications.
The thickening-time test should model the well operation as closely as possible. Duplicate
the temperature, pressure, and pumping profile of the squeezes. For smaller CT sizes, surface
pressure during pumping results in an initial pumping pressure higher (as high as 5,000 psi)
than that normally used for cement testing.
In many CT operations, some static or hesitation periods occur during the job. These periods
can dramatically alter the slurry thickening time. If a hesitation technique is planned, simu-
late the static periods for hesitation when the slurry or other sealant is not sheared by pump-
ing. Modified test schedules4 have been designed to simulate hesitation squeezes, but they
should be adjusted to reflect CT operations. Other slurry effects to consider during these
static periods include fluid loss and gel-strength development, the latter of which is com-
pounded by temperature increases from a lack of fluid movement. In addition, an improperly
designed slurry may settle.
While the thickening-time profile in Figure 3 is preferred, many slurries differ, with the
slurry consistency increasing steadily over a longer period. This consistency profile is less
desirable for frictional pressure drop. Gelling cement slurries are also more difficult to
control and exhibit a less predictable filter-cake buildup. The causes of slow consistency
increases range from polymer effects to problems with the quality of the base cement. If the
consistency increases but then remains flat at an elevated level, do not use the slurry until the
problem is resolved, especially for CT applications. Similarly, if an unexplained viscosity
spike occurs during the test, do not use the slurry. Refer to cementing technology documents,
or contact the Halliburton Duncan Technology Center for more information on slurry gela-
tion and cement quality control.
3,500 260
80 240
3,000
220
Consistency (Bc)
Temperature (F)
Pressure
Pressure (psi)
2,500 60 200
Temperature
2,000 Consistency 180
1,500 40 160
140
1,000
20 120
500 100
0 80
ccd01009
0 1 2 3 4 5 6 7 8 9
Time (hr)
Two slightly different techniques discussed in existing literature6, 7 explore the derivation and
application of equations that describe filter-cake deposition in a perforation and the spheri-
cally shaped node that can result inside the casing.
The API operating fluid-loss test is a static filtration test used for determining the amount of
filtrate removable from a slurry under specific conditions. The test is performed with a
known filter medium under 1,000-psi differential pressure at the expected well temperature
for the squeeze. For API tests, the filter medium is a 325-mesh, stainless-steel screen with an
effective permeability of >1 darcy and an overall filtration area of 3.5 in2.
In the special case of fluid-loss testing for microfine cement slurries, the slurries flow
through the 325-mesh screen. The procedure requires the filter medium to be either a 600-
mesh screen or a Whatman 50 filter paper placed on top of the standard 325-mesh screen.
Table 3 shows the average results of comparative testing.8 The slurry in this 1993 test is no
longer recommended because the introduction of Micro Fly Ash cement component elimi-
nated the need for 40% MicroSand cement additive at temperatures below 230F. Reference
9 has up-to-date microfine slurry data.
Table 3Fluid Loss vs. Filter-Cake Thickness
Filter Medium API Reported Filter-Cake Thickness
Fluid Loss (cc) (in.)
9
400-md Berea sandstone 56 /16
1
600-mesh screen 49 /2
1
325-mesh screen with filter paper 27 /4
Slurry descriptionMicro Matrix cement + 40% MicroSand additive + 1% KCl (bwow) +
3.2% CFR-3 friction reducer + 1.8 gal/sk Latex 2000 additive + 1.2 gal/sk FDP-C485
stabilizer + 0.15 gal/sk D-Air 3 defoamer + 0.1 gal/sk Micro Matrix cement retarder +
6.55 gal/sk fresh water mixed at 12 lb/gal
For most cement-slurry designs, the fluid loss value of interest is the amount of fluid re-
moved from the slurry after 30 minutes of exposure to the conditions listed in Table 3.
However, for nodal squeezes, the thickness or volume of filter cake produced during the test
is also of interest. Filter-cake formation and properties are a function of
Figure 4 (Page 19) shows the effects of different fluid-loss ranges on filter-cake thickness for
a typical Class G or H cement mixed at normal density. Uncontrolled fluid loss can result in
rapid buildup of a thick, relatively permeable filter cake capable of prematurely bridging the
ID of the casing. This effect frequently leads to the conclusion that a squeeze has been
achieved across an entire interval. However, if hydraulic communication, and thus the
pressure differential required for filter-cake building, are lost to the lower perforations, those
perforations are not squeezed. After drillout and pressure testing, the perforations do not
sustain a positive or negative test and are deemed a failure when, in fact, the perforations
were never squeezed.
75 cc Fluid-loss slurry
ccd01010
25 cc Fluid-loss slurry
CT applications pose an additional concern for the nodal buildup and washout technique. If
too much filter cake is built on the perforations, the washout of remaining liquid slurry may
be hindered. Additionally, even if the washout is accomplished without damage to the nodes,
any wireline-conveyed tools, such as perforating guns, may not pass freely through the
squeezed interval.
Figure 5, a photograph from a downhole video, shows properly built nodes on perforations
inside a casing. Note the concave shape of the node around the perforation.
differential pressure
filter-medium permeability
filtration time
Some limitations can be overcome by modifications to the API test procedure or the test
equipment. Table 4 provides a comparison of API recommended procedures to those that
may be considered for nodal applications.
Even with the modifications in Table 4, initially run the standard API tests for comparison,
especially with inexperienced laboratory personnel or with a new, unique slurry.
Preconditioning a slurry for only 20 minutes allows the slurry to reach the design tempera-
ture. The 20 minutes does not allow time for potential polymer breakdown or other chemical
or physical interactions, such as sedimentation, that may affect fluid-loss properties. Some
slurries may show excellent fluid-loss control when conditioned in this manner, only to fall
apart because of polymer destruction when conditioned at a higher temperature than an
atmospheric consistometer can reach. Alternatively, use a high-temperature, high-pressure
(HTHP) stirring fluid-loss cell.
Time plays a critical role in building a node of cement solids. With the factors that affect
filter-cake formation and the importance of creating the required filter cake, laboratory
modeling should reflect the history of the cement slurry. The history should include time
estimates for the mixing, pumping, placement, and any subsequent washouts. Increasing the
pressure schedule in the laboratory with a regulator instead of instantly applying the maxi-
mum differential pressure results in a lower spurt (initial) loss, improved packing of the
cement grains and polymer, and thus a lower permeability per linear thickness of cake. This
process ultimately helps provide a lower total volume of filtrate recorded and a thinner filter
cake.
Differential Pressure
Pressure applied during a CT squeeze can be higher than 1,000 psi, particularly when
excess cement is washed out. In these cases, the filter cake must withstand the pressure
differentials and erosion in the wellbore during the cleanout of excess cement, and the future
differential pressure if the squeeze is to be followed with hydraulic fracturing. However,
laboratory testing has shown that, for a properly designed slurry, additional differential
pressure (above the 1,000-psi standard) applied to the fluid-loss cell results in little or no
incremental change in filter-cake characteristics. Although the validity of increasing the
maximum differential has been debated, the test may be performed if requested by the
customer.
Filter-Medium Permeability
The permeability of the filter medium used in the API test is higher than that of many forma-
tions, especially carbonates. Core or synthetic (aluminum oxide) disks of varying
permeabilities can be inserted in some test cells with an adapter. Contact the Duncan
Technology Center for information on building or obtaining an adapter.
Filtration Time
Filtration time, or the time of applied squeeze pressure, often exceeds the 30 minutes of an
API test. Thus, the filter-cake volume produced under downhole CT conditions can signifi-
cantly exceed the filter-cake volume generated during an API test at a single pressure. For
slurries with higher fluid-loss values, the API fluid-loss cell may not have enough volume to
accommodate all the filtrate generated from a CT in-place test because of the extended
squeezing time and sometimes the higher differential pressures. Cement slurries with filtrate
volumes >60 ml may cause all the slurry to become dehydrated, forming filter cake in the
API cell. Continued filtration only purges water from the pore spaces, giving an inaccurate
measure of the fluid loss of the slurry under downhole conditions. An obvious indicator of
these effects is the lack of any liquid slurry remaining above the filter cake at the conclusion
of the test. The simplest solution is to use a longer fluid-loss cell, such as one built by Baroid
Drilling Fluids. The fluid loss of the slurry is probably too high for nodal applications.
Slurry Volume
Standard API procedures require only the final filtrate volume to be recorded. While this
measurement is acceptable for most situations, if difficulties occur in achieving the required
filter cake (thickness or friability), knowledge of the fluid-loss rate at different points in the
test can help the chemist determine which fluid-loss additives can be adjusted or substituted.
Determining the thickness of the filter cake and its friability is the ultimate goal of the test.
Example fluid-loss volumes and resulting filter-cake characteristics are shown in Table 5.
Generally, initial fluid-loss values should be between 70 and 130 ml API (35 to 65 ml of
actual filtrate collected) for obtaining a filter cake between 0.4 and 1.0 in. This range
Figures 6 and 7 show typical steps needed for measuring filter-cake characteristics in the
cell. The instrument shown can be easily made from various hardware components. In
Figure 6, a tool is made to fit in the top of a fluid-loss cell and is calibrated (distance h)
against the screen before the test. After the fluid-loss test, the tool is placed on top of the cell
(Figure 7), and the added height is noted (h + dh). Several heights can be recorded, starting
with the level of remaining liquid slurry, followed by the height of soft filter cake and the
height of firm filter cake. Placing a known weight on the top of the device and comparing the
resulting penetration into the filter cake allows the friability of different filter-cakes to be
compared. Calculating the force-per-unit area needed for penetrating a given distance into
the firm filter cake is possible if the cross-sectional area of the device in contact with the
filter cake is known.
Weight platform
h h + dh
Alignment plate
Liquid slurry
Soft cake
325-Mesh screen
ccd01012
Hard cake
Examine the cake after it has been forced from the cell and allowed to stand unconfined for
a few minutes. If the cake slumps under its own weight, it will not remain in place on a
perforation, and it most likely will not withstand the jetting from the washout.
Rheological Properties
Free water, sedimentation, and frictional pressure drop are all functions of rheology.
Multitemperature rheology data are required for performing job simulations (OptiCem job
simulator) and calculating the surface pressures. The relatively higher frictional pressure
drop with small-diameter CT strings prompts many to strive immediately for the lowest
rheology possible, sacrificing slurry stability. The ideal balance is to have the rheology as
low as possible without sacrificing slurry stability. Synthetic polymers normally provide a
more consistent, predictable rheology.
correlations have been developed for adjusting data measured at lower temperatures for
temperatures above the testing limits of laboratory equipment. In addition, some equipment
can measure the rheology of cement slurries at downhole temperatures and elevated pres-
sures.
A shortcut HTHP method not discussed in the API recommended practice includes running a
thickening-time test for the expected placement time, turning the stirring motor off for a
period at HTHP conditions, and then either observing the consistency deflection on startup
or cooling the machine and opening the slurry can for visual observation. Free oil or water in
the top of the can is the first indication of slurry instability, and hard sedimentation in the
bottom of the can is an immediate pass/fail indication for sedimentation. Final pass/fail
criteria are determined by the specific application. The Mini MACS analyzer is the HTHP
machine most suited to gelation and sedimentation testing under static conditions.
Compatibility
Compatibility is defined as the ability of two or more fluids to mix together without undesir-
able chemical or physical reactions. All fluids that will be pumped in the well must be
compatible, including cements, spacers, muds, and brines. Fluid incompatibility can result in
severe gelation, fluid separation, and sedimentation. The final outcome can range from a
nuisance to a job-terminating event.
Section 16 of API Recommended Practice 10B4 provides detailed procedures for compatibil-
ity testing. Aspects such as contaminated rheology, thickening times, compressive strength,
settling, and static gel strength are discussed for general cementing. These guidelines apply
especially to CT cementing because a CT unit may not be able to pull the tubing string
through a severely gelled fluid mixture in the annulus. In addition, the pressure limitation of
a CT string may not allow severely gelled fluids to be displaced.
For instance, attempts have been made to correlate TLME to FETME by ratio or scaling the
TLME to an equivalent FETME at similar operating conditions. A single-pass jet mixer
(ground mixer) operates at less than 5% of the API mixing energy [the energy (5.9 J/g)
imparted to the cement powder while it is mixed with water].5 A scale-down of TLME of this
magnitude does not provide enough energy for wetting the cement particles, and does not
allow the slurry to reach a state of equilibrium before physical testing (rheology and thicken-
ing time).
To expand this discussion to modern mixers such as the RCM mixing system, consider an
RCM I mixing system mixing at a rate of 6 bbl/min. Because at this volumetric rate the
RCM I mixing system produces about 13 to 20% of the mixing energy imparted by the API
laboratory procedure (equivalent to 0.77 to 1.2 J/g), some researchers have suggested that
laboratory tests be run at this equivalent energy level. Laboratory mixing energy is propor-
tional to time in the laboratory blender, so the 35-second mixing time at 12,000 rev/min
would be cut to 5 to 7 seconds. An extension of this logic would be to apply 17 seconds of
mixing in the laboratory to simulate the 50 to 75% of energy imparted by an RCM II mixing
system. Years of laboratory testing have shown this level of TLME to be insufficient.
Many polymers are used in cements primarily as viscosifiers and fluid-loss additives. Testing
has shown that some of these polymers are more susceptible to changing with extended
residence time in a mixer. Specifically, the additives based on natural hydroxethyl cellulose
(HEC), such as Halad-9, Halad-22A, and Halad-322 additives, seem to be the most
susceptible and exhibit primarily decreased viscosity. Synthetic materials, such as Halad-
344, Halad-361A, Halad-413, and Latex 2000 additives, are least affected.
Particle-Wetting Efficiency
For the design criteria to be met and the test data to be repeatable, efficient wetting of all
materials is required. A critical stage of the wetting of cement particles requires that enough
mechanical energy be applied to deflocculate amorphous, hydroscopic cement, and additive
aggregates fully. Further, reducing TLME, and thus wetting efficiency, directly affect the
transient state of slurry properties. Transient effects refers to the fact that energy reduction
greatly reduces the available time for additives to go into solution. For polymer hydration,
this effect can introduce significant error between tests. When cement and its associated
additives are placed in water, chemical reactions begin immediately (starting with many
components going into solution) and do not stop. However, the reaction rates can be affected
by shear. When particles cannot be contacted by water because they are inside agglomerates
of dry, unwetted cement as a result of poor dispersion, all required chemical interactions are
further inhibited. Only marginal improvements can be made by the addition of dispersants,
such as CFR-3 friction reducer. Adding too much dispersant can affect critical slurry proper-
ties, such as free water and settling.
A poorly wetted slurry requires significantly more energy downstream for reaching the same
result (measured by physical slurry properties) as a slurry initially mixed efficiently. At-
tempts made to repair a poorly wetted slurry with chokes and screening devices10 have
exhibited little success. Mixing energy is also a function of throughput rate, so less time in a
mixer because of smaller volume tubs or higher pumping (downhole) rates yields lower
specific mixing-energy values, producing a less wetted and somewhat unstable slurry.
Test data suggest that modern field-mixing equipment does not require as much FETME for
obtaining the same results as standard API laboratory procedures.11 Paper SPE 2521811 shows
that, for the RCM II mixing system, FETME values from 50 to 75% normally produce
slurries with properties similar to those mixed in the laboratory with standard API proce-
dures. The RCM II and the RCM IIe mixing systems performed better than previous
mixers because the axial flow mixer design provides greater wetting efficiency when the
cement is initially wetted.
This third-party research indicates that the properties (thickening time, fluid loss, and
rheology) of the slurries mixed in yard tests had already departed dramatically from labora-
tory-prepared slurries even before they were pumped through the CT spool. We believe that
the slurry was undergoing physical changes because of poor mixing, improper slurry design,
or other reasons. To conclude that further changes were caused by pumping through the CT
spool is misguided. They presented other hypotheses for the drastic changes to slurry proper-
ties, such as the adsorption of retarders on steel surfaces or chemical deterioration. However,
slurry design or thermal effects during mixing were not presented as possible causes.
Though enough energy must be applied when the cement particles are initially wetted, well-
maintained and properly functioning recirculating mixing equipment provides ample energy
for providing a stable, well-mixed slurry. Further, our studies show that pumping a cement
slurry through CT has no effect on physical properties, except dilution effects on the leading
and trailing edges, and that rheology decreases when natural polymers are used instead of
synthetics. Halliburton did similar work for a major operator in 199211 and with another
operator for a specific application (Micro Matrix cement).8 In both cases, nothing resembling
the previous report was observed. Since then, other major operators have done internal
research and reported essentially the same results as ours. A properly designed slurry that
takes into account all possible variables, including surface-mixing temperatures, performs as
expected, regardless of the batch size, mixer size, or CT length.
Cement Strength
The cement strength is the amount of compressive load that cement withstands before
failure. The compressive strength of a cement slurry can be determined by the API procedure
in which an unconfined 2-in. cube (nominal dimensions) is loaded in compression uniaxially
until the cement fails. This convenient method of compressive-strength testing is similar to
failure-testing procedures used in the construction industry, from which the API methods
were developed.
The API approved the use of the ultrasonic cement analyzer (UCA) for well-simulation
tests.4 The UCA offers the advantage of a continuous measure of compressive strength vs.
time. The strength is determined from correlations of sonic transit time vs. compressive
strength. Therefore, the results must be calibrated with destructive API tests.
The mode of cement failure can be compressive, tensile, or shear. Failure may stem from the
following:
The compressive strength of the set cement itself is of little relevance for squeeze cementing
except for the estimate of drillout time. However, the API compressive-strength test indicates
whether uncontaminated cement will set under well conditions. For most slurries, a compres-
sive strength of at least 500 psi is sufficient.
The API compressive-strength test does not measure the strength of the filter cake for
squeeze cementing. Cement filer-cake density for a well-dehydrated normal-density slurry is
> 20 lb/gal. In the elapsed time of applied squeeze pressure, some cement blends can build
filter-cake compressive strengths of 5,000 psi before the liquid slurry itself develops any
measurable strength. Under most conditions, the compressive strength of the final, fully set
filter cake from a squeeze cementing job is two to five times greater than the compressive
strength of the set cement resulting from the original slurry.
Acid Resistance
The chemical resistance or the rate of solubility of the set cement is a concern in many
squeezes. Portland cements are subject to attack by various well fluids, such as acid, certain
components in formation waters, and carbon dioxide. For the sake of repeatability and
presumably for worst-case evaluation, acid-solubility testing is normally performed on cubes
of set cement instead of cement filter cake. The testing covered in this section and in all
literature refers to testing cubes of set slurry.
Latex 2000 additive (styrene-butadiene) has successfully decreased the rate of solubility of
Portland cement in acids. In general, 2 gal/sk of Latex 2000 additive in a slurry at normal
density lowers acid solubility to approximately 10% by weight when a 2-in. cube is exposed
for 1 hour in 12% HCl/3% HF in a stirring bath at 190F. Previously published literature
reports acid solubilities approaching 95% for nonlatex slurries. Acid-solubility testing is a
strong function of the test procedures, and some tests are performed with cement chips or
ground samples.
Although a styrene-butadiene latex slurry does not provide total acid resistance, it does
provide a solubility rate that allows enough safe contact time for performing a small matrix
acid cleanup. However, because of the low fluid loss of slurries that have sufficient latex for
providing low-acid solubility rates, care must be taken to ensure that node competency is not
jeopardized when latex slurries are used for node applications.
For detailed study of cement acid solubility and specific laboratory-test procedures, refer to
additional references.8,14-17
Summary
Because the API tests were not designed for the specialized needs of some CT cementing
operations, the API tests and testing equipment often must be modified for a more accurate
simulation of CT operations. If equipment is not available or cannot be readily modified,
contact the Duncan Technology Center for immediate assistance.
For larger CT workovers in which numerous squeezes are performed, procuring modified
equipment for the local laboratory is highly recommended. The following guidelines briefly
summarize the information covered so far:
Model the planned CT procedure in the laboratory as closely as possible. Include the
squeeze pressure, temperature profiles, and hesitation. Modify API procedures and
equipment, if possible, to simulate the operation.
Job Design
Obtaining the best, most economical job under a given set of conditions depends on applying
the problem diagnosis, slurry design, and laboratory testing that we have discussed so far in
a logical sequence. Indiscriminately applying a cement squeeze without fully understanding
the problem can worsen the situation, especially with CT operations. The problem should be
diagnosed with one of the techniques discussed unless knowledge of local trends can take
precedence. After the wellbore has been cleaned and preparations have been made, materials
and volumes should be selected. With problems such as water or gas coning or early break-
through on enhanced oil-recovery projects, near-wellbore solutions may be insufficient.
Techniques of radial treatment for a distance around the wellbore may be required. See the
Halliburton Conformance Technology Manual2 for guidance.
Guidelines do not exist for choosing job volumes for simple, near-wellbore cement squeez-
ing. The volumes are usually chosen based on local experience, injection rates and volumes,
and whether the application is designed to squeeze off perforations or to place a larger
volume of cement into the annulus.
Squeezing Perforations
Perforations are often enlarged because of erosion during high-rate production. The intervals
are also often characterized by large voids behind pipe because of sand production. Case
histories show a high failure rate of nodal squeeze technology attempted on washed-out
perforations. Washed-out perforations are as difficult to squeeze as casing damage caused by
corrosion or splits in the casing. Cement dehydration is more difficult over these enlarged
surface areas. Achieving a seal may require repetitive squeezes, regardless of the technique.
Pretreatments with conformance chemicals can be useful in these situations.
Channels
The direction and length of a channel should be determined to aid slurry and job designers and
subsequently enhance the potential for success in sealing the channel. Perforations may also be
squeezed after an extensive channel has been filled with a sealant. Slurry penetration along the
length of the channel depends on cement fluid loss and rheology. A low API fluid-loss value
(40 to 60 ml) is commonly used for obtaining passage of a cement slurry through a channel,
especially if permeable formations are present. Low fluid-loss, microfine slurries have success-
fully traversed channels that exhibit low injectivity (less than 1 bbl/min at maximum allowable
pressure). Further, microfine slurries applied as lead slurries followed by moderate fluid-loss,
conventional slurries have successfully achieved the squeeze. For low-injection profiles,
consider using solids-free, internally activated conformance chemicals.
Cement Volume
The selection of cement volume depends on several factors, and experience is often the best
guide for selecting the initial volume to use in any squeeze. The parameter most difficult to
quantify is the volume of cement to be placed behind the pipe. The following factors affect
the estimate and sources of information:
Historically, cement volumes for CT squeezes using a hesitation technique and the nodal
technique are less than volumes for performing a squeeze in which continuous pumping is
applied. Also, treatment-volume reductions can be achieved because of less dilution of slurry
in surface equipment when certain procedures are followed (Cement Mixing and Pumping,
Page 38) and during pumping and spotting (Job Simulation, Page 31). Testing has shown
that a slurry pumped through 10,000 ft of 1 -in. CT has 0.5 to 0.75 bbl of dilution at both
the leading and trailing edges of the slurry, compared with 1 to 2 bbl when pumped through
2 7/8-in. tubing.
Injectivity tests can serve as a guide, but they should be refined as other information be-
comes available. Table 6 (Page 31) provides guidelines for cement volumes based on
injectivity-test data.
The data in Table 6 are based on historical field data from non-CT squeeze work only. The
table also does not account for the added friction pressures encountered with CT less than
2 in. in diameter.
Large cement volumes required for filling big channels or fractures may be reduced with
thixotropic cements. These high-gel-strength cements build resistance and enable squeeze
pressure to build. Sand can be pumped into the formation before the cement, partially filling
the area to be squeezed and forming a high-permeability bridge against which a filter cake
can be formed. In high-injectivity situations, reactive fluids, such as sodium silicate, can be
pumped ahead of the cement slurry with freshwater spacers between the two materials.
When simulators are used for a CT job, frictional pressure predictions may depart from the
simulated data after the slurry enters turbulent flow. The departure has a different slope for
the portion of the CT spooled on the reel because of the unusual flow profile, as shown in
Figure 8. Flow in a curved pipe causes secondary circulations in a plane perpendicular to the
pipe axis. These secondary circulations are caused by the centrifugal acceleration of the
axial flow because of the pipe curvature, thus influencing the mean axial profile so that it is
no longer symmetrical about the axis.
ccd01014
As a result, the friction pressures predicted by currently used, dynamic pumping simulators
differ from what is seen on the job. Figures 9 to 12 (Pages 32 to 33) show sample pressure
data recorded during large-scale testing of both straight and spooled sections of 1 -in. CT
with a nominal wall thickness of 0.087 in. and an ID of 1.076 in. The diameter of the spooled
section of CT used was 82.75 in.
1,800 25
1,600
20
Friction Pressure, psi/1,000 ft
1,400
1,200
Reynolds Number
15 Spool
1,000 Straight pipe
800 CemFlo program
10
OptiCem program
600
Reynolds number
400 5
200
0 0
ccd01016
0.3 0.5 0.7 0.9 1.2 1.4 1.7 1.8
Flow Rate, bbl/min
Figure 9Fresh water (85F, calculated critical flow rate = 0.02 bbl/min)
1,800 16,000
1,600 14,000
Friction Pressure, psi/1,000 ft
1,400
12,000
Reynolds Number
1,200 Spool
10,000
1,000 Straight pipe
8,000 CemFlo program
800
6,000 OptiCem program
600
Reynolds number
4,000
400
200 2,000
0 0
ccd01017
Figure 1016.4-lb/gal Class H cement (PV = 23 cp; YP = 9 lb/100 ft2; 100F; calculated
critical flow rate = 0.38 bbl/min)
1,800 14,000
1,600
12,000
Friction Pressure, psi/1,000 ft
1,400
10,000
Reynolds Number
1,200 Spool
1,000 8,000 Straight pipe
CemFlo program
800 6,000 OptiCem program
600 Reynolds number
4,000
400
2,000
200
0 0
ccd01018
0.2 0.4 0.5 0.6 0.7 0.9 1.1 1.2 1.3 1.4
Flow Rate, bbl/min
Figure 1115.8-lb/gal Class H cement (PV = 27.5 cp; YP = 9.8 lb/100 ft2; 120F; calculated
critical flow rate = 0.44 bbl/min)
1,800 6,000
1,600
5,000
Friction Pressure, psi/1,000 ft
1,400
Reynolds Number
400
1,000
200
ccd01019
0 0
0.2 0.4 0.5 0.6 0.7 0.8 1.0
Flow Rate, bbl/min
Figure 1215.8-lb/gal Class H cement (PV = 41 cp; YP = 14.7 lb/100 ft2; 120F; calculated
critical flow rate = 1.05 bbl/min)
Table 7 summarizes the differences between spooled and straight pipe and between straight
pipe and OptiCem program at 0.5 and 1.0 bbl/min (the most common operating range for
pumping cement through 1-in. CT).
Error exists between simulator data and actual pressure data. The significance of the error
depends on the job. Unless the job is on a well at underbalanced hydrostatic conditions
where a danger of approaching the working-pressure limitations of the CT exists, or if a
running squeeze will be attempted through a choke during circulation above the treatment,
the error is usually not a concern. Previously published literature covers flow in curved pipes
with high Reynolds numbers. Some mathematical models may be included in a future
OptiCem update. Finally, no model exists for simulating the effects of the welded bead on
the ID of smaller CT strings.
Job Design
Thus far, this manual has concentrated on concepts and job planning. We now cover the
logistics of job design and execution in more detail.
Equipment
Equipment used for CT squeezes is almost the same as that used for other cementing opera-
tions. However, the following items help the job run more smoothly:
the CT unit and any necessary auxiliary cranes or hydraulic power packages
the squeeze manifold and two adjustable chokes equipped with pressure gauges
bleedoff and diverter valving at the entry side of the CT
cement mixing equipment (Batch mixing is preferred when slurry quality is critical.)
high-pressure pumping equipment and any necessary transfer or additive pumps
fluid-storage and mixing tanks for contaminating fluid (if used)
fluid filters (Filtering fluids before injectivity testing or squeezing is recommended. A
filtering unit should have differential pressure gauges on the filter and be able to deliver
high rates for killing the well.)
a nitrogen pump (The pump is recommended for inflow and negative testing if the
reservoir pressure is insufficient for providing an inflow test at flowing differentials with
a full column of fluid to the surface. The pump is also used for foam cementing.)
Cementing Nozzles
Some situations, such as the nodal-washout technique, require the use of a specialized nozzle
on the end of the CT. Figure 13 shows a complex nozzle, but variations exist, depending on
the job pumped. Simpler nozzles consist of a ported sub. When building the nozzles, make
sure that all shoulders are beveled. This design will help prevent the nozzle from hanging
when it passes through narrow restrictions.
Section A-ASix
each of 1/8-in. ports
drilled tangential to
the internal 60
circumference 3-in OD
Gauge
Contam
Water
CTU
Pump
Batch
mixer
ccd01008
Clod filter
Centrifugal
Pump
1. Place a bleedoff or bypass valve in the high-pressure line ahead of the coil.
2. Prime all pumps.
3. Calibrate the flowmeters by pumping known volumes of fluid from measuring tanks.
4. Open the bypass valve ahead of the coil, and fill the high-pressure treating lines.
5. Record the volume of the system.
6. Close the bypass valve.
7. Measure the volume required for filling the coil.
8. Record the required volume.
The procedure also allows a check that helps ensure that the CT is clear of debris before it is
started in the wellbore. After completion, the volume counters on the cementing unit are
calibrated to the CT and all surface equipment. If significant errors are found and are not
acceptable to the upcoming job, service or replace the flowmeters.
Viscous Prepad
Steps in Cement Mixing and Pumping (Page 38) help minimize dilution of the cement
slurry because of surface equipment. However, these steps do not help prevent dilution in the
CT string or in the annulus. Although large-scale testing has shown that slurry dilution at
both the leading and trailing edges of the slurry typically is no more than 1 bbl when the
slurry is pumped through 10,000 ft of 1 -in. CT spooled at the surface, no testing has been
done to verify the intermixing length in the string while the string is in the wellbore.
Field data20 indicate that, based on pressure responses observed during jobs, significant
contamination does occur. However, large-scale plug-cementing research has shown that the
degree of intermixing depends on factors such as density difference, flow regimes, veloci-
ties, and hydraulic flow areas. Instead of attempting to model these complex factors, it is
common to run a volume of viscous prepad ahead of a squeeze slurry, especially when small
volumes of slurry are used and significant volumetric contamination cannot be tolerated.
Avoid weighted spacers because the solids typically associated with conventional cement
spacers can bridge and interfere with the placement of the slurry in some situations, such as
a nodal squeeze or squeeze into low-injectivity openings.
Viscous prepads can be prepared with the same polymers discussed in Contamination
Procedure (Page 41). Concentrations of 2 to 3 lb/bbl of HEC-based polymers usually
provide an adequate viscosity and yield point for solids transport and minimize retardation of
the cement. Filtering the solutions helps prevent plugging of perforations with any fish-eyes
present.
Another technique for minimizing contamination while pumping involves isolating selected
fluids mechanically. Foam balls have been used successfully. This technique requires spe-
cialized ball or plug-releasing devices at the entry of the CT unit. Verify that these isolation
techniques will not interfere with the final outcome of the job. The items cannot be circu-
lated out of the well and must be easily drillable if removal is required.
Job Execution
Depth Control and Correlation
Accurate information about depth is necessary for a successful squeeze. Most CT units have
counters that indicate the depth of the end of the coil. These counters have limited accuracy
and do not account for stretch in the tubing or residual bend effects. Stretch in the tubing can
be calculated by Hookes law:
S = (F L) (E A)
where
S = stretch (ft)
F = force (lb)
L = length of tubing (ft)
E = Youngs Modulus (typically 30 106 psi)
A = cross-sectional area of the CT (in.)
When possible, calibrate or correlate the depth with casing-collar locators, tubing-end
locators (TELs), or tubing-nipple locators (TNLs). Tagging bottom may be useful if the
squeeze interval is near total depth. TELs or TNLs are useful if the squeeze interval is close
to the end of the tubing.
Tagging bottom is a good technique for most squeezes, but it provides accurate depth
correlations only if used properly. In addition, if significant solids are in the rathole and are
circulated into the annulus between the CT and production tubing, the CT can become stuck.
Never stop circulating, and avoid letting the CT become static during bottom tagging.
The procedure for correlating counters with the actual depth through tagging bottom follows:
1. Check and record the weight just before tagging bottom. This should be done approxi-
mately every 1,000 ft as you RIH unless a good record exists from previous and recent
CT work.
2. Tag the bottom, and notice the weight slack (an indication that the CT string is com-
pressing).
3. Pull up the CT string until the weight is the same as the weight just before tagging
bottom. Put the CT in tension, with stretch accounted for, just as the end moves off
bottom. Pull uphole 10 ft and place a flag on the pipe to avoid running back in the hole
past this point until the squeeze is complete and you are making your cleanout passes.
4. Note the depth difference, and correlate to correct the counter for depth.
1. Use a batch mixer with an RCM II mixing system to help provide a homogeneous
slurry. For smaller jobs, the 25-bbl mixing tub on the AdvantageTM skid is useful. Some
Halliburton batch mixers also have an RCM mixing system.
2. Continuously mix the slurry with the RCM II mixing system equipped with ADCTM
control system for most jobs that do not involve node building or otherwise require
critical control of slurry properties.
After the slurry has been mixed and has met any necessary on-location quality-control
measures, it is ready to go in the CT. At the start of pumping the slurry into the CT, you may
need to divert flow at the entry side of the unit until good-quality slurry is observed. This
step minimizes the amount of diluted slurry in the CT string. The same procedure can also be
used at the end of the slurry volume. Normally, 1 to 2 bbl of slurry are diluted on the leading
edge because of pumping through surface equipment, particularly the suction manifolds.
The recommended procedure for spotting cement with CT designed to minimize contamina-
tion of the cement with the fluid in the wellbore follows:
3. Begin pumping spacer and cement through the CT according to the planned procedures.
4. After the leading edge of cement has entered the annulus, allow it to rise a short distance
above the end of the CT before you pull the CT up. The volume of slurry between the
end of the CT and the top of cement is the contamination interface.
5. Pull the CT up at a rate equal to or slower than the fluid rise in the annulus to permit the
end of the CT nozzle to remain 5 to 10 ft below the top of the cement (TOC).
6. As the last of the treatment volume exits the CT, accelerate the CT pulling rate to place
the end of the CT nozzle above the planned TOC.
7. Begin the squeeze either after clearing the CT by reversing or circulating bottoms up or
simultaneously by using surface chokes. Simultaneous pumping and squeezing requires
communication, prejob planning, and computer pressure simulation.
Actual Squeeze
After spotting the cement and positioning the end of the CT nozzle a safe distance above the
TOC (at least 50 to 75 ft), increase pressure to initiate filter-cake building. Some filter cake
usually exists because of differentials induced by the equivalent circulating density (ECD)
and hydrostatic effects during placement. Generally, the differential pressure at the perfora-
tion is gradually built to 1,000 and 1,500 psi above the initial bottomhole pump-in pressure
for the squeeze.
After an initial filter cake has been formed, the pressure is increased, which in turn increases
the filter-cake node height and compresses or densifies the filter cake. Densifying the filter
cake helps protect the squeeze while excess cement is being washed out.
The maximum allowable squeeze pressure can be above or below the fracture pressure of the
formation, depending on the application. For most applications, the job ends at this point.
Subsequent steps may include recompleting another zone after waiting a specified time for
the cement to set or returning with the CT and drilling out the squeeze before pressure
testing.
A detailed pressure, volume, and time schedule helps ensure adequate node buildup. If low
differential pressures are used and the cement nodes did not form properly, the filter cake
may be fragile, and a successful squeeze may not result. High differential squeeze pressures,
often above the formation fracture pressure, normally ensure that the nodes are competent
and all perforations have opened and accepted cement slurry. However, the squeeze may
break down, requiring another squeeze if the higher squeeze pressure is attempted too early
in the schedule or if the perforations are severely eroded. The nodal squeeze example
problems in Appendix B (Page 48) have job worksheets that exhibit the types of schedules
that can be prepared.
As filter-cake integrity is increased (lower permeability and higher bulk density), the filter
cakes capability to resist differential pressure and thus protect the formation from fracturing
increases. More often, some breakdown occurs as medium-range pressures are reached.
Breakdown usually indicates a perforation opening and accepting cement slurry if fracture
pressure has not been reached. A careful increase of the pressure in the later stages of
pressurization can increase filter-cake integrity and node height, further protecting the
formation from fracturing and improving the potential for a successful squeeze. The final
pressure in many CT nodal squeezes can be between 500 and 1,500 psi above fracture
pressure, depending on the formation and the condition of the well and perforations.
1. Maintain a running-in-hole (RIH) speed with the CT to enable lifting or dilution of the
cement slurry and to prevent excessive WHP.
2. After clean returns are observed at the surface, make at least one more jetting pass.
3. Maintain adequate overbalance pressure across the squeezed interval while performing
these operations when appropriate (underbalanced fluid column).
Contamination Procedure
Contamination washout is commonly used for removing slurry after a nodal squeeze. The
procedure involves contaminating the unset cement during washing and also increasing the
hydration time of the cement because of chemical retarding. Dilution also minimizes the
effects of cement hydration.
If contamination is used, simulate the process first in the laboratory by exposing the slurry to
various contamination levels at bottomhole temperature (BHT), which helps ensure compat-
ibility. Avoid gelation spikes.
The primary design criteria of the washout and contamination fluids are to provide solids
suspension of the cement slurry under low velocity in the annulus and, if necessary, to retard
the hydration reactions of the cement. Contamination can be accomplished with single- or
dual-gel polymer systems that achieve these criteria. Mildly retarding xanthan biopolymers,
such as welan gums are commonly used. Dual systems with welan gums, cellulose-based
fluid-loss additives for drilling muds, and high-temperature cement-settling control additives
have also been used, as well as guars. The total polymer loading on the first pass volume of
fluid usually is about
2.5 lb/bbl of water. A minimum volume for this pass is typically 1.5 times the expected slurry
volume. After the first pass has been made and the bulk of the slurry has been mobilized,
polymer loadings in subsequent wash fluids can be dropped to about 0.75 to 1.5 lb/bbl,
depending on the formulation used. The dual systems are sometimes designed around
specific temperature ranges, compatibility, and improvement of the economics of the wash
fluid.
An additional design step is to examine the effects of the contaminant on ultimate filter-cake
integrity. Exposing the filter cake made during a fluid-loss test to the contaminant allows the
examination of these effects. Some of the early work used powerful cement retarders, such as
borax, in the washout fluid. This practice is no longer recommended. The retarders extend
the WOC time before the perforations are pressure-tested, and the chemicals can permeate
the filter cake, causing it to soften and slump so that it eventually falls off the perforation.
Mild cement retarders, such as those used in the slurry itself, or even some viscosifiers that
impart longer hydration times, are usually sufficient.
Node Hardening
Even when mildly retarding to nonretarding wash fluids are used, node degradation is
possible because of cement-particle diffusion into the wellbore brine or water remaining
after the washout. Accelerator solutions are commonly spotted across the perforations after
all cement slurry is safely out of the wellbore. This procedure helps offset the weakening of
the cement node. These solutions penetrate the remaining permeability of the cement node
and accelerate the hydration of the cement. Economical solutions include completion brines,
various salts, such as calcium chloride, triethanolamine (TEA), and blends of both TEA and
salts. A 5 to 20% solution of TEA is typically most effective at temperatures above 130F.
Testing21 shows that a 5% TEA solution mixed in fresh water can completely penetrate a 2-
in. cement cube in less than 24 hours, producing >50% of ultimate compressive strength.
Comparative testing on the same slurry with fresh water resulted in unset cement in 24
hours. However, even when deep penetration is not achieved, the hard shell of hydrated
cement on the node surface provides support that helps prevent slumping while the interior
of the node undergoes hydration at normal rates. Laboratory testing of accelerator solutions
on filter cake is recommended before use.
1. Circulate the first heavy polymer-loading fluid to the nozzle, and start the jetting from
the expected TOC.
2. Run in the hole while jetting at the maximum rate, decreasing the rate to 1.5 bbl/min
across the perforations. Use enough volume to achieve at least a 1:1 volume dilution of
the cement slurry with the contamination fluid until reaching the previous CT total
depth.
3. Ensure that all the diluted cement is above the nozzle by pulling the CT and circulating
at 80% of the pump rate used while going in the well. Continue until returns are accept-
ably clean.
4. Repeat the jetting twice with a solution with a lower polymer loading. During this stage,
some jetting-nozzle profiles, such as the one shown previously, can be altered by drop-
ping a ball to activate high-velocity tangential side jets. On the last pass, circulate a
TEA solution in place (if required) across the perforations while pulling out of the hole.
5. If well-control conditions permit, switch to slick water (clean water with a friction
reducer), and pull out of the hole (POOH), washing all downhole equipment.
Reverse Circulation
Treatment fluids (cement slurries or polymers) must sometimes be reversed, which can be
more advantageous than normal circulation. You may also want to avoid exposing produc-
tion equipment, such as gas-lift tools, to the fluids. Large solids, such as gun debris or high
sand concentrations, can cause annular bridging, which can result in lost circulation or
sticking of the CT string.
Low annular velocities resulting from pressure restrictions of small-diameter CT, combined
with large-diameter tubing or casing during normal circulation, can prohibit effective cement
contamination and cleanout. Reverse circulation, however, can effectively remove the
cement slurry in the presence of poor annular hydraulics. Circulation is performed down the
backside as returns (cement slurry and debris) are taken from the CT. Reverse circulation
also minimizes hydraulic agitation across the perforated interval during cleanout. However,
this method can expose the cement nodes to elevated pressure.
Control the RIH speed to help prevent the formation of high-density slugs in the CT during
reverse circulation, which may increase circulating pressure on the backside to unacceptable
limits. If the increase occurs, purge the CT while pulling by applying direct circulation
before repeating the process.
Underreaming
Small completion IDs require the use of small-diameter motors, which have a lower rate and
torque output than the full-sized equipment used in conventional drilling. The underreamer
includes a full-gauge hole at or near the bottom of the tool. This hole helps prevent side
loading as a pilot hole is established.
Squeeze Failure
If testing indicates squeeze failure, a resqueeze may be required. A production or injection
well can be recompleted and monitored for effectiveness before it is resqueezed. However, if
the squeeze fails to meet regulations, a resqueeze is mandatory. Before resqueezing, we
recommend that you perform an injectivity test to help determine the magnitude of the
failure. Running logs is also helpful for determining the location of the failure.
References
1. Krilov, Z., Romic, L., Celap, S., and Cabrajac, S.: Permeability Damage Due to Precipi-
tation of Insoluble Salts From Cement Slurry Filtrates, paper SPE 25218 presented at
the SPE International Symposium on Oilfield Chemistry, New Orleans, March 25.
2. Halliburton Conformance Technology Manual, Manual No. F3373 (1993).
3. Halliburton Cementing Technology Manual, Part No. 516.99001(1996).
4. RP10B, Recommended Practice for Testing Well Cements, twenty-second edition, API,
Dallas (1997).
5. Spec. 10, Specification for Material and Testing for Well Cements, fifth edition, API,
Dallas (1990).
6. Binkley, G.W., Dumbauld, G.K., and Collins, R.E.: Factors Affecting the Rate of
Deposition of Cement in Unfractured Perforations During Squeeze-Cementing Opera-
tions, Trans., AIME (1958) 213, 5158.
7. Flow of Fluids through Porous Materials, R.E. Collins, Pennwell Books, Tulsa (1976).
8. Heathman, J.F., Carpenter, R.B., Sanders, G.S., and Wedman, M.L.: Acid-Resistant
Microfine Squeeze Cement: From Conception to Viable Technology, paper SPE 26571
presented at the 1993 SPE Annual Technical Conference and Exhibition, Houston, Oct.
36.
9. Microfine Cementing Products, Halliburton Best Practices Series, Halliburton Energy
Services, bibliography H00727 (Oct. 1997).
10. Heathman, J.F., Sands, F.L., Sas-Jaworsky, A., and Badalamenti, A.M.: A Study of the
Effects of Mixing Energy Imparted on Cement Slurries by Field Equipment and Coiled
Tubing, paper SPE 26573 presented at the 1993 SPE Annual Technical Conference and
Exhibition, Houston, Oct. 36.
11. Automatic Density Control and Specific Mixing Energy Deliver Consistent High-
Quality Cement Slurries, OTC paper 7068 presented at the 1992 Offshore Technology
Conference, Houston.
12. Vidick, B., Nash, F.D., and Hartley, I.: Cementing Through Coiled Tubing and Its
Influence on Slurry Properties, paper SPE 20959 presented at the 1990 Europe 90, The
Hague, The Netherlands, Oct. 2224.
13. Hibbert, A.P., Kellingray, D.J., and Vidick, B.: Effect of Mixing Energy Levels During
Batch Mixing of Cement Slurries, Drilling and Completion (March 1995) 49.
14. Halliburton Research Laboratory Report, bibliography C32-E001-92.
15. Brady, J.L., Gantt, L.L., Fife, D.M., and Rich, D.A.: Cement Solubility in Acids, paper
SPE 18986 presented at the 1989 Joint Rocky Mountain Regional/Low Permeability
Reservoirs Symposium and Exhibition, Denver, Mar. 68.
16. Blount, C.G., Brady, J.L., Fife, D.M., Gantt, L.L., Huesser, J.M., and Hightower, C.M.:
HCl-HF Acid-Resistant Cement Blend: Model Study and Field Application, paper SPE
19541 presented at the 1989 SPE Annual Technical Conference and Exhibition, San
Antonio, Oct. 811.
17. Carpenter, R.B., and Edwards, T.M.: A Proven Methodology for Comparison of Cement
Acid Solubility, paper SPE 27683 presented at the 1994 SPE Permian Basin Oil and
Gas Recovery Conference, Midland, Texas, Mar. 1618.
18. Drillable Tools Manual (Part No. 802.2000), Section 16 (March 1997).
19. Walker, E.J., Gantt., L., and Crow, W.: Coiled Tubing Operations and Services, World
Oil (June 1992) 213, No. 6, 69.
20. Carpenter, R.B.: New Technologies Address the Problem Areas of Coiled-Tubing
Cementing, paper SPE 20426 presented at the 1990 SPE Annual Technical Conference
and Exhibition, New Orleans, Sept. 2326.
Bibliography
Barry, T.S., Beck, D.L., and Putnam, J.S.: Offshore Coiled-Tubing Cement Squeezes,
Forties Field, paper SPE 23144 presented at the 1991 Annual Technical Conference and
Exhibition, Aberdeen, Sept. 36.
Bond, A., and BP Alaska Authors: Latex Acid Resistant Cement and Various New or
Existing Placement Techniques, paper presented at the 1995 3rd International Conference
and Exhibition on Coiled Tubing Technology: Operations, Services, Practices, Houston,
Mar. 1316.
Brookey, J.B., and Garrett, C.: Use of Drilling Fluid Additives to Improve Drilling and
Remedial Operations with Coiled Tubing, Proc. Paper No. 24 presented at the 1994 2nd
International Conference and Exhibition on Coiled Tubing Technology: Operations, Ser-
vices, Practices, Houston, March 2931.
Brookey, T., Bird, J., and Garrett, C.: Copolymer Beads Aid Drilling and Remedial Opera-
tions by Reducing Wellbore Friction, Proc., Second Annual Coiled Tubing Technology
International Management Conference, Dallas (1994) Paper 22.
Fram, J.H., and Eberhard, M.J.: Use of Coiled Tubing for Abandoning Shallow Thermal
Wells, South Belridge Field, Kern County, California, paper SPE 26087 presented at the
1993 SPE Western Regional Meeting, Anchorage, May 1618.
Gantt, L.L., and Smith, B.E.: Advancements in the Coiled Tubing Cement Squeeze Process
at Prudhoe Bay, Proc. Paper No. 21 presented at the 1994 2nd International Conference and
Exhibition on Coiled Tubing Technology: Operations, Services, Practices, Houston, Mar.
2931, 1994.
Haney, J., and Folmnsbee, G.: Coiled Tubing Improves North Sea Squeeze Cementing,
Petroleum Engineer International (August 1991) 2834.
Krause, R.E., and Reem, D.C.: New Coiled-Tubing Cementing Techniques at Prudhoe
Developed to Withstand Higher Differential Pressure, SPE Production and Facilities
(November 1993) 26062.
Mody, R.K., Coronado, M.P., and Craig, G.C.: Coiled Tubing Conveyed Inflatable
Workover Systems, Proc., Coiled Tubing Operations and Slimhole Drilling Practices
Conference (1993).
Noles, J., Bays, B., Browning, G., and Knecht, B.: Small-Capacity Cement Procedure
Reduces Failure Potential, World Oil (May 1996) 5355.
Oliver, A., Calvert, G., and Gavin, B.: Coiled Tubing Cement Squeeze with Wash Through
Operation. SPE Production Engineering (May 1992) 13743.
Pavlich, J.P., Greaves, C., and Edwards, T.M.: Designing Slurries for Coiled Tubing Ce-
ment Squeezes, CTH (1993) 11620.
Teel, M.E.: Coiled Tubing 1994 Update: Expanding Applications, World Oil (June 1994)
3945.
Vrokinn, P.B., and Sanders, G.S.: Cement Slurry Qualification, Field Mixing, and Quality
Assurance Procedures for Coiled-Tubing Squeeze Operations in Prudhoe Bay, Alaska,
paper SPE 26089 presented at the 1993 Western Regional Meeting, Anchorage, May 2628.
Walker, E.J., Gantt, L., and Crow, W.: Coiled Tubing . . . Operations and Services, World
Oil Coiled Tubing Handbook (1993) 5157.
Yang, S.Y.: Equation Determines Pressure Drop in Coiled Tubing, Oil & Gas Journal
(December 4, 1995) 6768.
The data in Table B-1 is used in the sample calculations on Page 49.
Volumes
Tubing
78.5 bbl
Casing
Behind casing (top perforation to aquifer)0.0226 bbl/ft (7,670 to 7,600) = 1.3 bbl
CT volume = 19 bbl
Fluid Column
Fill casing from plugback total depth (PBTD) to at least 100 ft above the perforations.
Sump 3 bbl
Perforations 5.6 bbl
100 ft above perforations 3.7 bbl
12.3 bbl [Use 15 bbl (170 ft above top perforation).]
Worst-case top of cement (WCTOC) = PBTD cement height
WCTOC = 7,900 ft (15 bbl/0.0371 bbl/ft) = 7,495 ft MD
Gel contaminant volume = 3 casing volume
= 3 24.9 bbl = 75 bbl (Mix 150 bbl for contingency of lost
circulation.)
Sample Problem 1
a
No. MD Fluid Rate Vol CTP WHP At Nozzle Comments
(bbl/min) (bbl) (psi) (psi) Fluid/Vol
1 7,900 FSW b 1.5 ++ 3,500 0 FSW / ++ Clean out sand with well flowing on
GL and perform TD check. Injectivity
test down BS.
2 7,900 CMTc 1.5 0 4,000 Vac FSW / ++ Shut in well. Begin cement down CT.
3 7,900 CMT 1.5 10 4,000 Vac FSW / ++
4 7,900 CMT/ 1.5 15 4,000 Vac FSW / ++ Finish pumping cement. Switch to FSW.
FSW /0
5 7,900 FSW 1.5 / 4 1,500 Vac CMT / 0 Cement at nozzle. Decrease rate and
1.0 begin POOH at 27 ft/min.
6 7,765 FSW 1.0 9 1,500 Vac CMT / 5
7 7,660 FSW 1 13 1,500 0 CMT / 9 Cement covering perfs. Begin filling
production tubing. Any increase in fluid
height is applying squeeze pressure.
8 7,495 FSW 1 19 1,500 0 CMT / 15 All cement out nozzle. Continue POOH
FSW / 0 to 7,400 ft at 60 ft/min and decrease
to minimum rate.
9 7,400 FSW 0.3 20 200 0 FSW / 1 Stop CT at 7,400 and resume maximum
pump rate down CT.
10 7,400 FSW/ 1.5 51.0 4,000 0 FSW / 25 Production tubing filled. Begin to
GELd /0 (1,000) see positive pressure indication
at surface. Control squeeze pressure with
choke. Approximately 20 minutes have
elapsed since perforations were covered
with cement; 1,000-psi effective
squeeze pressure with WHP = 0.
Switch to gel and decrease rate
to 0.5 bbl/min.
11 7,400 GEL 0.5 10 1,000 1,000 FSW / 35 Build surface squeeze pressure to 1,000 psi;
2,000-psi effective squeeze
pressure. Maintain pressure for 60 minutes
total time.
12 7,400 GEL 0.5 19 1,000 1,000 FSW / 44 Gel contaminant at nozzle. Slowly release
GEL / 0 squeeze pressure. Then increase rate to
maximum and RIH contaminating cement.
13 7,500 GEL 1.5 20 4,000 0 GEL / 1 Reciprocate down to PBTD and up to EOTe
three times. Decrease rate to 1 bbl/min
across perfs.
14 7,900 GEL/ 1.5 75 4,000 0 GEL / 75 Final downward pass to TD. Displace well
FSW FSW / 0 to FSW while POOH.
a
Measured depth
b
Field salt water
c
Cement
d
Gelled water
e
End of Tubing
Example Problem 2
Diagnostics (Figure B-2)
Reservoir pressure = 4,800 psi. Reservoir temperature = 160F.
1
4 /2-in. Tubing
(0.0149 bbl/ft)
1
1 /2-in. OD CT
Capacity: 20 bbl
Packer 9,200 ft
Perforations: 9,800 ft
to 9,900 ft MD/TVD
Casing
Sump0.0371 bbl/ft (10,000 to 9,900) = 3.7 bbl
Perforations0.0371 bbl/ft (9,900 to 9,800) = 3.7 bbl
Tailpipe to top perforations0.0371 bbl/ft (9,800 to 9,200) = 22.2 bbl
Overall (inside casing)0.0371 bbl/ft (9,200 to 10,000) = 29.6 bbl
CT volume20 bbl (12,000 ft of 1.5-in. 0.109-in. wall thickness)
Cement Volume
Expected WHP with 8.5 lbm/gal brine (or the underbalance with 8.5 lbm/gal brine):
= Formation pressure hydrostatic pressure
= 4,800 psi (8.5 lbm/gal 0.052 9,800 ft)
= 470 psi
Maximum surface squeeze pressure to prevent fracturing:
= Fracture gradient hydrostatic 500-psi safety margin
= (9,800 ft 0.8 psi/ft) 4,330 psi 500 psi
= 3,010 psi
To obtain 2,000-psi formation overbalance,
= Formation pressure hydrostatic + 2,000-psi
overbalance
= 4,800 psi 4,330 psi + 2,000 psi
= 2,470 psi (use 2,500 psi)
To obtain 500-psi negative differential pressure test on squeeze:
= Formation pressure hydrostatic 500 psi
= 4,800 psi 4,330 psi 500 psi
= -30 psi (use WHP = 0 psi)
Sample Problem 2
No. MDa Fluid Rate Vol CTP WHP At Nozzle Comments
(bbl/min) (bbl) (psi) (psi) Fluid/Vol
1 10,000 FSW b 1.5 ++ 3,500 200 FSW / ++ Clean out with well flowing on GL and perform
TD check. Injectivity test down BS.
2 10,000 CMTc 1.5 CMT/0 4,000 500 FSW / ++ Shut in well. Begin cement down CT.
3 10,000 CMT / 1.5 CMT/1 4,000 500 FSW / ++ Switch to FSW spacer.
FSW 1FSW/0
4 10,000 1.5 /1.0 8 4,000 500 CMT / 0 Cement at nozzle. Continue pumping FSW at
decreased rate of 1.0 bbl/min.
5 10,000 1.0 9 3,500 500 CMT / 1
1 bbl cement out nozzle. Continue pumping
FSW and begin POOH at 27 ft/min.
6 9,850 1.0 16.4 3,500 500 CMT / 7.4 Cement covering perforations. Continue to
POOH to the top perforations.
7 9,770 1.0 18 3,500 500 / CMT / 9
700 Stop CT near the top perforation (9,770). At
18 bbl FSW, begin to build pressure to
indicate perforations sealed. Begin squeeze.
(Estimated 1.6-bbl cement behind pipe)
8 9,770 / 1.0 18 3,500 500 / CMT / 9 Resume POOH when initial pressure is
POOH 700 developed. Choke well returns to maintain
700 psi.
9 9,715 / 1.0 / 0.25 20 3,500 / 700 CMT / 11 Continue pumping while POOH to new
POOH 500 FSW / 0 WCTOC (9,715 ft). Decrease rate when all
cement has exited the nozzle. CT should be
at 9,715 ft when FSW is at the nozzle. CTP
will decrease from the decreased rate.
Continue POOH to 100 ft above the new
WCTOC (9,615) at + speed.
10 9,615 FSW 1.0 / 0.25 22 1,000 / 700 FSW / 2 Continue to ramp squeeze pressure at
300 approximately 250 psi each for 10 minutes
while holding the CT at 9,615 ft.
11 9,615 Geld 0.25 / 1.6 24 / 0 300 / 700 FSW / 4
4,000 Squeeze pressure building good. Decide to
switch to gel. Increase rate but control
squeeze pressure with choke. RIH to 9,715 ft.
13 Contamination
14 9,715 FSW 1.5 0 4,000 2,500 / Gel / 0 Gel at nozzle. Switch to FSW. Release
1500 squeeze pressure slowly to 1,500 psi. RIH
jetting at 40 FPM/1.5 bbl/min and
contaminating cement. Decrease rate to
1.0 bbl/min across the perforations.
a
Measured depth
b
Field salt water
c
Cement
d
Gelled water
Justification: This well has been shut in due to high water production. Isolation from
these water sands will allow production and fracturing of the hydrocar-
bon producing sands, which are not projected as depleted.
Expected BHP: 3,000 psi at 7,000 ft, or approximately 0.43 psi/ft gradient
1. Mix all fluids for the location one day before CTU cement squeeze operations. Take
samples of water and perform complete laboratory tests, including thickening time, to
confirm that properties for the cement have not been altered by the current materials.
Wellbore flush volume: X bbl filtered water
X bbl acid, specific to well conditions
Mix water volume: 50 bbl filtered fresh water should be available by the start of the
day for sampling and testing with the cement blend.
Fluid column spacer: 30 bbl dead crude. Determine if needed at the end of the
acid treatment.
2. Before RIH with CT, evaluate WHP. If required, pump filtered water to sweep wellbore
gas and fluid back into the formation. This can be done while RIH or after CT is on the
bottom if the wellhead pressure is low enough to allow entry to the well.
3. While RIH, make PU weight checks every 1,000 ft. Note and record all weight-check
values to ensure no problems exist when the CT is filled with cement. Make dry tag to
confirm PBTD. Do not pump down CT while making tag. PU 10 ft and flag CT.
4. Jet wash across perforations with acid to clean up perforations. Volume to pump should
be calculated based on one down pass and one up pass, running at 80% of fluid rate.
5. Reconfirm tag location, again without pumping. Determine PU weight and then pull
uphole 5 ft. Slowly pump down the CT (approximately 0.5 bpm) with water to flush the
rathole fluids. PU to 15 ft off the bottom and pump down the CT at 1 bpm and 1.5 bpm.
Make sure the CT is well away form the bottom before pumping. If CT annulus pressure
falls off to 0 psi or goes on vacuum during this test, crude oil will be required for lower-
ing backside hydraulics during the cement squeeze. POOH and prepare for Day 2.
1. Confirm that the fluids required for the job are on location and in proper condition. The
cleanout fluids can be prepared on location or made up and brought to the location by a
mud company. Required fluids include the following:
200 bbl filtered water
30 bbl dead crude (if needed, based on injection rate and pressure after acid work
from Step 5 in Day 1)
50 bbl mix water (filtered fresh water) retained from Day 1
X bbl 1.5 lb/bbl Biozan cleanout fluid
X bbl 0.5 lb/bbl Biozan cleanout fluid
35 bbl 10% TEA solution
RIH with combo jet swirl nozzle (confirm ball-drop nozzle design and ball size before
RIH), dry tag PBTD, and confirm the flag set from Day 1. Repeat string weight tests at
1,000-ft intervals past 4,000 ft to confirm that no changes from the Day 1 acid job are
present. As soon as the nozzle is through the tubing, begin batch-mixing the designed
volume of cement slurry (allow for excess due to surface equipment sumps and dilution)
of Latex Acid Resistant Cement.
When the cement is up to weight, begin flushing the CT Tubing annulus with the
filtered water to remove all gas from the wellbore and to condition the bottom of the
well. While cement is being prepared, establish stable injection pressure by shutting in
the CT x Tubing annulus and pump down the CT at 1 bpm and 1.5 bpm. Be well off the
bottom before switching to all injection down the CT. If the annulus goes on vacuum or
does not show sufficient WHP, pump degassed crude down the annulus to lighten the
backside fluid column. This should confirm the results from Step 5 in Day 1.
2. After the cement slurry has been mixed at weight for 15 minutes and thoroughly sheared,
catch a sample to conduct QC testing. Condition slurry in an atmospheric Howco at
200F (or lower to match the appropriate BHCT) for 20 minutes before conducting a full
30-min API fluid-loss test. Measure the filter cake to ensure that the field blend is
acceptable and have the engineer confirm cement quality. Fluid properties are listed in
Appendix C-1.
3. Pressure-test the cementing lines to maximum squeeze pressure plus 1,000 to 3,000 psi.
Pump the following fluids down the coil:
5 bbl fresh water spacer
42 bbl cement (zero cement volume at reel with bypass setup)
5 bbl fresh water
1.5 lb Biozan gel (follow fresh water spacer for cleanout)
4. Continue to pump filtered water or crude oil down the backside if necessary to ensure
that the well remains fluid packed. If possible, shut in the backside injection and monitor
WHP with a static column.
Locate the CT to flag depth (10 ft above TD or PBTD) as cement reaches the nozzle.
Begin POOH with CT when the cement top reaches 50 to 75 ft above the nozzle.
Pull CT uphole at 1:1 (for every barrel pumped, pull the CT the distance equivalent
of 1 barrel of casing volume)
Continue to stack cement while maintaining the nozzle at 50 to 75 ft below the top
of cement. Begin taking returns if WHP shows a significant pressure bump, usually
500 psi above the stable injection pressure determined earlier. Take returns through
choke, holding backpressure (referred to as bump pressure) as preplanned. The
engineer will define this pressure as the job is performed.
5. Pull the nozzle above top perforations only when bump pressure is observed and the
cement is being stacked above the perforations by taking returns with the bump pressure
on the annulus.
If bump pressure is not observed and the nozzle has been pulled to within 50 ft of
the top perforations, RIH with the nozzle and continue to reciprocate the nozzle
across approximately the top 150 ft of the perforations until bump pressure is
observed. Do not stop CT for any period of time while pumping and laying in
cement.
6. When bump pressure has been achieved, stack the remaining cement above the perfora-
tions. Lay the cement 1 for 1, keeping the nozzle below the top of the cement, until the
last bbl of cement leaves the nozzle. As the last 3 bbl leave the nozzle, increase running
speed to try and pull out of cement.
7. Determine the safety depth (the depth at which the nozzle is 500 to 1,000 ft above the
cement, based on calculations for cement placed behind the pipe).
As the last bbl of cement leaves the nozzle, pull uphole at 80% of fluid and shut
down the CT.
Ensure that 3 bbl Biozan fluid are out the end of the nozzle before shutting down the CT.
Node Building Sequencing. Accurate pressure monitoring and the use of good pressure-
buildup sequencing procedures are key to obtaining cement nodes with strong perforation/
formation bonds. Attempting to obtain squeeze pressure by pinching the choke while circu-
lating does not allow accurate monitoring of pressure leakoff and accurate determination of
cement volumes pumped behind pipe during the node-building process. Remember that a
node cannot be built unless fluid is lost from the slurry as indicated by pressure leakoff.
Pressure leakoff while static indicates that nodes are building.
8. When the CT nozzle is at a safe depth and a minimum of 3 bbl of 1.5-lb Biozan has
exited the nozzle, shut in returns and raise the WHP to an equivalent of 1,200 psi +
hydrostatic calculated at the top perforation. This is the desired first pressure step for the
node-building sequence. Calculate the additional pressure generated by the cement
column and the CT Tubing annulus fluid to adjust WHP for an equivalent of 1,200 psi
surface pressure with water to the top of the perforations.
1,200 psi + TVD Top Perf 0.43 psi/ft = (TVD Top Perf Cement Top TVD) Cement Density psi/ft +
(Cement Top TVD Backside Fluid Density psi/ft) + Desired Pressure Step 1 WHP
Pressure levelingPressure leveling indicates that no further fluid is being lost through the
node that has been built to that point. Once the pressure levels for a minute or two, nodes are
no longer being built and the next pressure increment can begin. This process usually takes
15 to 20 minutes.
Pressure breakbackIf the squeeze pressure breaks back, immediately stop pumping and
allow the pressure to stabilize and repeat pressure sequencing. If no signs of immediate
healing exist, reduce the pressure increment and increase waiting time between stages.
9. With the choke still closed, walk squeeze pressure up to maximum ssqueeze pressure in
300- to 500-psi increments. The engineer should determine the pressure steps.
Hold and maintain maximum squeeze pressure for 1 hour.
Maximum squeeze pressure is calculated at 1,500 psi over the calculated surface
fracturing pressure with water in the hole. Remember to make the same surface-
pressure adjustment for the cement in the hole as calculated earlier.
10. After holding the maximum squeeze pressure for 1 hour, slowly bleed the WHP to 500
psi. From this point until the job is complete, the choke operator should attempt to
maintain 500-psi WHP through all rate changes.
Launch the ball to modify the nozzle-jet configuration.
Chase the ball to the nozzle with 1.5-lb/bbl Biozan gel.
11. For the down pass, begin the cleanout procedure by RIH jetting with 1.5 lb/bbl Biozan
gel at maximum injection rate. Lower the rate as the ball approaches the nozzle. Do not
jet across the perforations until the ball has reached the nozzle.
With the ball seated in the nozzle, begin cement cleanout procedure across perfo-
rations by RIH with the coil at 1:1 speed. The pumping rate should be to 1.5 bpm
(or < 5 hhp as calculated from jet-bit hydraulics for the nozzle design).
Important Warn the choke operator before all rate changes occur.
Increase jetting rate to maximum injection pressure while RIH at 1:1 speed from
bottom perforation to TD or PBTD.
Take a barrel count to ensure 1:1 returns.
12. For the up-pass, pull uphole at 80% speed while jetting at maximum injection pressure
to bottom squeeze perforation.
Reduce the jetting rate to 1.5 bpm (or < 5 hhp) across squeeze perforations while
POOH at 80% speed.
Increase the jetting rate to maximum injection pressure while POOH at 80% speed
from top of the squeeze perforations to the tubing tail.
13. Perform three down-passes and two up-passes with 1.5-lb/bbl Biozan gel, again limiting
your pump rate and thus the hhp exerted on the nodes to less than 1.5 bpm or 5 hhp.
14. Switch to 10% TEA solution on the third down-pass to ensure that it reaches flag depth.
Lay 10% TEA on the third up-pass in the rathole and across perforations.
Note Three passes are needed to adequately clean the wellbore in 7-in.
casing. If a sufficient number of passes is not conducted, the
nodes may be difficult to clean and cement stringers may be left
in the wellbore.
15. Reduce the Biozan concentration to 0.5 lb/bbl after the 10% TEA and increase the pump
rate to maximum from the top of the perforations to the surface.
POOH at 80% running speed at maximum CT injection pressure while being
careful to thoroughly jet across any downhole tubing equipment (specifically, gas
lift mandrels).
Post-Squeeze Test
After three days, perform a pressure test on the squeeze to 1,000 psi.