Beruflich Dokumente
Kultur Dokumente
020
1. GENERAL
1.1 Scope
The present standard establishes the methods of laboratory determination of physical and mechanical
characteristics of earthes with great bellies and shrinkages, from the foundation land.
The methods of the the present standard apply to earthes identified and classified according to STAS 1243-88.
1.2 Earthes with great bellies and shrinkages, called PUCM, are clay-bearing earthes, more or less
active, which have the property of modifying volume when their humidity oscillates.
1.4 Results interpretation of tests on earthes with big bellies and shrinkages can be made using the
identification diagram, made according to clause 7 and the status diagram, according to clause 8.
ASRO Entire or partial multiplication or use of this standard in any kind of publications and by any means (electronically, mechanically,
photocopy, micromedia etc.) is strictly forbidden without a prior written consent of ASRO
2 STAS 1913/12-88
2.2 Equipment.
-metallic grater
-technical balance with a 0.01 g weighing precision;
-oven with temperature regulator
-pestle mill (mechanic mortar)
-bolter (02)
-porcelain capsule 120mm
-80/80 mm celluloid plate.
-100 cm3 graduated cylinders
-calcium chloride exsiccator
-distilled water shower
-manual blender
2.3 Materials
-distilled water
-calcium chloride crystal solution (CaCl 2 ), 300g/l, filtered
The reading of the sediments final volume will be made with a 0.5 cm3 precision. The result will be recorded in
a table (as shown in annex A).
The sediments final volume for three samples will be determined.
2.6 Expression of results.
UL free belly will be calculated with the following relation:
V f Vi
U L= 100 [%]
Vi
where,
Vf the sediments final volume (cm3)
Vi earths initial volume (10 cm3)
As Ui = 10 cm3, the relation becomes:
UL=10 (Vf - 10) [%]
The UL values will be calculated for the three Vf determined values.
These values should not differ, exceeding 10% in the absolute value. If one of the results does not respect this
condition, the test will be repeated.
The tests result will be the arithmetic average of the calculated UL values.
3.2 Equipment
According to STAS 1913/4-86 plus:
-metal boxes, numbered and calibrated, with dimensions indicated in fig. 2
-technical balance with a 0.01 g weighing precision;
-anhydride calcium chloride exsiccator;
-cotton textile cloth pieces
-volume meter.
3.3 Materials
- distilled water
- consistent technical mineral butter
The calibrated and numbered metal boxes, well cleaned, will be lubricated in the interior with a thin consistent
technical mineral butter layer.
There will be extracted, on a spattle, a small earth quantity from the earth paste, which will be entered in the
metal box; the load will be made continuously and only next to the margin of the box.
In order to prevent the presence of air bubbles inside the earth paste, during the filling process, the metal box will
be subject to repeated shocks, by hitting the worktable.
The metal box will be filled up with earth paste. The earth paste will be leveled, with a clean spattle, 30o sloped
to the upper edge of the box, so that a perfectly plane surface shall be obtained.
The remaining of earth, if any, on the external side of the metal box shall be cleaned with a clean rag.
The metal box will be weighed; the weighing result will be recorded (as shown in the table from Annex B).
The earth test piece will be dried up, by keeping at the environment temperature, which must be maintained as
constant as possible, avoiding high heating places. By a 5-7 day slow drying, the earth test pieces will contract and if
the lubrication was made appropriately, it will detach of the metal box, on the whole outline. In this situation, the test
piece will be removed from the metal box and placed on clock glass and the box number will be written on the test
piece, with a soft pencil mine. The test piece shall be checked to see if there are any cracks of and then, the test piece
shall be dried in the oven, at a 105oC, for at least 12 hours.
The dry test piece shall be put in the exsiccator and after cooling, it will be weighed; the resulted mass will be
recoprded (as shown in the table from Annex B). The test piece volume will be determined, by mercury immersion,
using a volume meter; the measurement result will be recorded (as shown in the table from Annex B).
After the determination of the test piece volume, it will be broken, to control if there were inside any air pockets;
the test piece with air pocket will be excluded from the experiment.
The volume of three test pieces will be determined.
Ws and Cv values are calculated, for the 3 determined Vf values. They shall not differ between them with more
than:
15% in absolute value, in case of Ws shrinkage limit;
5% in absolute value, in case of Cv volume shrinkage.
In case none of the results comply with these respect these conditions, the test shall be repeated.
The test results represent the arithmetic average values of Ws and Cv, calculated.
4.2 Equipment.
-special device, obtained by the adaptation of a projection device.
-matrix (figure 3, 2nd position);
-counter matrix (fig. 3, 3rd position);
-sample dressing cutter
-calibrated and numbered watch glass;
-porous plates
-vacuum pump;
-vacuum exsiccator;
-covering capsules 40mm and h-40mm;
5 STAS 1913/12-88
-thermo-adjustable oven;
-technical balance with a 0.01 gram weighing precision.
Thickness 1.5
6 STAS 1913/12-88
Vf test pieces volume, when volume changes no longer occur, in cubic centimeters;
Cv earths volume shrinkage, in percents.
Using the data obtained, a diagram is elaborated, setting w test piece moisture in the x-ordinate and V100 volume
in the y-coordinate (the usage of a grid indicated in annex C is recommended).
The obtained diagram represents the earths shrinkage curve; for comparison purpose, it is drawn the saturation
line (Su=1), originating in point V100=100/ and placed at 45o, in which stands for the solid frames density, expressed
in grams per cubic centimeter.
The moisture value corresponding to the intersection point of the constant volume level and the saturation line,
represents the shrinkage limit, determined graphically.
5.2 Equipment
-according to STAS 1913/4-86 and also:
-numbered and calibrated metallic boxes, with sizes according to figure 4.
-technical balance with a 0.01 g weighing precision.
-calcium chloride exsiccator.
-cotton textile cloth pieces.
-length measuring device (gauge), with a 0.5 mm precision
5.3 Materials
According to subclause 3.3
The long sides of the test piece are measured and then it is calculated their arithmetical average. The result is
considered the length of the dry test piece.
If the test piece bent during the drying process, the distances between the end surfaces are measured. The
arithmetical average of these distances is considered the length of the dry test piece.
The length of the three test pieces is determined.
The weighing and measuring results are recorded in a table shown in annex D.
where
B the length of the dry test piece (cm);
A the initial length of the test piece (cm);
Cl values are calculated for the three determined lengths.
The test result is the arithmetic average of Cl calculated values.
NOTE- The moisture of equilibrium is established according to the technical appropriate specifications, on basis of retaining curve of the
water by land, in different suctions, determined according to STAS 9180-73 and according to the volume shrinkage curve,
determined according to clause 4 of this standard.
6.2 Equipment.
According to STAS 8942/1-84.
6.3 Materials.
According to STAS 8942/1-84
the flooded
sample curve
Un-flooded ssample
translated curve
Un-flooded
sample curve
e differences between the coordinates of the two curves, corresponding to various pressures applied allow the
establishing of the volume variations, , expected after the flooding with various pressures.
Where e0 represents the pores index of the un-flooded sample corresponding to the applied pressure.
The initial volume of the un-flooded sample V1 corresponding to 100 g of the solid frame is determined with the
relation:
V f = V s (1 + e 0 )
Where Vs=100/s and corresponds to the volume dislocated by 100 grams of solid frame.
The final volume of the flooded sample, corresponding to 100grams of solid frame, under pressure, is
determined with the relation:
V f = V f (1 + )
By processing the data obtained after the double test in edometer, it is drawn the status modification road, by
raising moisture, from the initial value, corresponding to the un-flooded test piece, to the final value, corresponding to
the flooded test piece (approximately when Sr=0.9), for various values of the applied pressure. (fig. 6).
10 STAS 1913/12-88
In order to establish the probable field of the status modification roads under the action of various modifications
of moisture and pressure, as well as the equilibrium status curves, corresponding to various pressures applied, there are
used several un-flooded test pieces (multiple test in edometer), with various initial moistures and then the edometric
curves corresponding to these test pieces are compared to the curve corresponding to a single flooded test piece.
The use of at least three un-flooded test pieces is necessary, with the following guiding values of the initial
moisture:
- Ws shrinkage limit;
- Wp the inferior plasticity limit (determined according to STAS 1913/4-86);
- moisture=1/2 (Wp+Wsat).
7. IDENTIFICATION DIAGRAM
7.1 The identification diagram provides with an image of the earths activity, which is more active as its
impression has a wider area.
8. STATUS DIAGRAM
The status diagram (fig. 8) has a w moisture in its x- axis, in percents, and the V volume in the y-axis,
corresponding to 100 grams of dry material, expressed in cm3/ 100 grams.
As between the apparent dry density and volume it is the relation:
100
V=
d
on th y-axis the corresponding d values can be marked. The lines of apparent dry equal density are parallel with
the x- axis.
100
The volume dislocated by 100 grams of solid frame V s = is represented by the barred square, in the
s
diagram. In such a representation, the expressions of the main indices are calculated with the following relations:
- Porosity:
Vs
n = (1- )100 [%]
V
- Pores index:
V
e= -1
Vs
- Saturation moisture:
w sat = w (V - V s ) [%]
3
Where w =1g/cm , water density.
- Moisture for a certain moisture degree Sr
w = S r w sat = S r w (V - V s ) [%]
- 0 volume moisture (Vw water volume, per V total volume), in percents;
12 STAS 1913/12-88
Vw w 100
= 100 =
V w V
Or
100 3
V= w [cm /100g]
w
- volume mass:
100 w
= (1 + )
V 100
or
100 w
V = (1 + ) 3
[cm /100g]
100
In the diagram (w,V), the equal index curves Sr, , , which become linear and correspond to line fascicles that
pass through the points A, O and respectively D.
The change of earth status during the belly-shrinkage processes is indicated by the movement of M point on the
shrinkage curve, which becomes identical with the saturation line, as long as the earth is dry.
For w=wsat, the volume resulting in the change of status has the following expression:
V
V = V + V = V(1 + ) = (V s + w sat )(1 + )
V
Where represents the relative volume change.
Curves with an equal represent a line fascicle, which passes through the point B.
For the tests in edometer, where relative volume variations correspond to relative deformations, the module
deformation expression may be deduced on basis of values, considering relation:
M=
Or for:
1
= 1 M=
Fig.8
13 STAS 1913/12-88
This diagram allows the assessment of changes for the moisture and ramming status during various mechanical
stresses or temperature, hydrological conditions and can be used as a base for representing the changes of various
geotechnical indices, depending on the status changes, indices that can be read in the diagram, no further calculations
necessary.
The use of the diagram in the laboratory is also useful for checking the correspondence between various physical
indices determined in the lab.
ANNEX A
GEOTECHNICAL LABORATORY
Order
Site
Boring
Sample...
Depth.
UL=10(Vf-10) %
Average %
ANNEX B
GEOTECHNICAL LABORATORY
Order
Site
Boring
Sample...
Depth.
MEASURI
DETERMINATIONS 1w 2 3 4 AVERAGE
NG UNIT
m Wet test piece mass + mc box mass g
mc box mass g
Wet test piece mass m u g
Dry test piece mass m d g
Mass of contained water m w = m u - m d g
Initial volume V i Cubic cm
Final volume V f Cubic cm
Shrinkage V i - V f Cubic cm
mw
Moisture w = 100 %
md
Vi V f
Volume shrinkage C V = 100 %
Vf
Vi V f
Shrinkage limit w s = w L - 100 %
md
Glass mass g
Description of material..
Performed by.. Date.
15 STAS 1913/12-88
ANNEX C
GEOTECHNICAL LABORATORY
Order
Site
Sample......
Depth.
VOLUME SHRINKAGE
Magnification ratio..
Day
Time
tare m c (g)
Dry piece mass
m d + tare m c (g)
Tare m c (g)
ANNEX C
SHRINKAGE LIMIT AND VOLUME SHRINKAGE
Ws graphic
Ws calculated
Vi V f
w s = w sat - 100
md
Volume shrinkage
Vi V f
CV = 100
Vf
Axis shrinkage
hi h f
100
hf
Transversal shrinkage:
di d f
100
df
Description of material.
Performed by.
Date..
17 STAS 1913/12-88
ANNEX D
GEOTECHNICAL LABORATORY
Order
Site
Boring
Sample...
Depth.
Measure
Determinations 1 2 3 4 Average
unit
Wet test piece mass m u + tare m c g
Dry test piece mass m d + tare m c g
Tare m c g
Wet test piece mass m u g
Dry test piece mass m d g
Contained water mass m w = m u - m d g
Initial length A cm
Final length B cm
B
Linear shrinkage C L = (1- )100 %
A
mu m d
Moisture w = 100 %
md
Description of material.
Performed by.
Date
18 STAS 1913/12-88
ANNEX E
E.1 It is taken into consideration a clay for which were obtained the following:
-from the granulometric analysis:
Table 1
Diameter 2 5 50 200 500 2mm
- plasticity limits:
the superior plasticity limit w L = 67%;
the inferior plasticity limit w P = 23%;
- plasticity index I P = 44%
3
-bulk mass s= 2.73 g/ cm
For the same clay, the edometric test led to the following height values of the sample, in mm:
Table 2
The sample diameter d was 70 mm and the dry mass was 128.22 grams.
E.2 The obtaining of A impression is made on cross-section paper, on which the axes are marked, the lines and
symbols mentioned below and in fig. 9.
For WL, Ip, and xd, it can be adopted the scale:
100%10 cm.
For the equivalent diameter d, it is used a logarithmic scale so that for changing the size order, for instance
between 0.1 cm and 1 cm, or between 1 and 10 , there is a 5 cm correspondence (50%), on the other three axes.
The correspondence between the number and the decimal logarithm is in conformity with table 3.
Table 3
Number 1 2 3 4 5 6 7 8 9 10
Decimal
0 0,3 0,47 0,6 0,7 0,78 0,84 0,9 0,95 1,0
logarithm
It is marked afterwards, on the negative x-axis, the values corresponding to diameters of 1cm=10mm ((in the
origin point of the coordinate axis), 5, 2, 1 mm 500, 200, 100, 50, 20, 10, 5, and 2 , drawing if necessary, the
horizontal lines corresponding to separation limits between the main fractions.
It is represented, in dial I, point P1, with x-coordinate WL=67% and y-coordinate=44%, and in dial II, point P2,
with x-coordinate 2 =67% and y-coordinate Ip=44%.In the dial III it is represented the granulometric composition
according to data indicated in table 1, limited to point P3, corresponding to a 2 diameter and to point P90,
corresponding to xd=90%. In the dial IV, point P4, situated on the horizontal line, corresponding to 2 and having a
WL=67% x-axis.
19 STAS 1913/12-88
By the union of points P1, P2, P3, P90, P4 and P1, it is obtained the impression of the considered clay. (figure 9).
Any other earth with an impression close to the one of the considered clay is supposed to have an analog
structure and is supposed to have an analog behavior.
Point P2, of the obtained impressions being situated in the active zone and in the important area of the
impression indicates that the considered earth presents the danger of great bellies and shrinkages, under conditions of
important seasonal variations.
E.3 Volume V, corresponding to 100 grams is calculated, depending on the sample dimensions and dry mass.
Table 4.
Moisture Pressure applied , MPa
0.0125 0.025 0.05 0.10 0.20 0.40 0.80 1.60
V volume cubic centimeters/100 g
Natural (w=12.1%) 59.52 59.4 59.16 58.79 58.35 57.91 57.32 56.59
By flooding (Sr 0.9 66.44 66.19 65.50 64.32 62.57 60.46 57.91 55.38
These results may be represented in the status diagram, which has moisture w (%) in its x-axis and volume V
(cubic centimeters/100 grams), in its y-axis( fig. 10).
In this situation, the following scales are convenient:
W = 10% 10 cm
3
V = 10 cm /100g . 10 cm.
V=Vs+w
Which has a slope V/ w=1 and which reaches the y- axis in point:
V s = 100/
3
s = 100/2,73 = 36,63 cm /100g
By the union of these points, it is obtained the saturation line and then it can easily be drawn the lines with an
equal saturation degree, considering relation:
W = S r w sat
E.4 In the same status diagram, (fig 10), it can be drawn the shrinkage curve (fig. 11) that indicates the connection
between moisture w(%) and volume V100, corresponding to 100 grams of solid frame. As it can be seen in figure 1, the
shrinkage curve is made up in fact of two joined parts. The slope of the tangent to the shrinkage curve indicates the
extent in which the applied pressure, , is transmitted to the water in the pores:
u = -h +
where u is the water pressure in the pores and h is the suction in the earth pores.
For the right part, bent to 45 degrees, parallel/ covering the saturation line (Sr=1), slope=1, that is the whole
pressure applied is transmitted to the water within the pores (u=1. , since h=0).
For the other right part, parallel to w axis, coeficient=0, which is that because of the earth advanced dryness,
the whole applied pressure is taken over by the mineral frame.
The above mentioned relation and therefore the knowledge of values deduced from the shrinkage curve are
necessary to the calculus of the moisture equilibrium distribution, under water-proof pavements or under radiation.
The shrinkage curve also allows the forecast of volume variations related to moisture variations.
For instance, for a raise of moisture, from 20% to 30%, it results as indicated in fig. 10 a belly + V=V1-
V2=67.2-56.8=+10.4 cm3/100 grams (Cv=18.3%), while a moisture lowering, from 20% to 10%, leads to a shrinkage
- V=V2-V0=51-56.8=-5.8 cm3/100 grams (Cv=-10.2%).
Less active
Very active
inactive