Designation: C1580-15, ‘Standard Test Method for Water-Soluble Sulfate in Soil! ‘ea te in C80 ees ny ie tin ae a 1, Scope 1 This est mated 6 forte deteminion of war sole ste noi 1.2 Tis ot method was develop for connie of arabe safc sos bacon 0.02 and 329 mali tyme 13 This test meth doe ot rine sulin ay form exc ae 14 Sone goveing bade reuse te move of sis ‘rom oe rea ane Is sp the sre sn berate ta comply with leptons 15 The vas sain Sune at be repaid andor. No othe is of ment aloe is rd 1.6 This standard does no purpon 1 abies lof he sefety concer fa. asocoed ith ete te ‘sprain of he wer of thi andar eth eppes rte sry and heath pracces and to determin he plea of replay ltt prir to se 2 Referenced Documents 21 ASTM Siondande™ (i Terminology Relating to Conrete and Cone Ag ‘gees cies Meds for Chemical Analysis of Hyde Cones DIDS pete fn Reagent Weer ag mdchars npr nd Set penne bet grate ek pv lin pe now C0)“ DOE Bio Pratce for Analysis of Meal, Ores, and Reed Materals by Spectoptaony 1275 Prac for Desabing and Metaing Peformance of ‘Urwilt nd Visible Spctopomesre ‘3. Terminalogy 1. For tensors ed in thet mato fro ‘ernaaogy C128 4 Siguleance and Use 4.1 This st mtb can be ed to stein if si cold have an adver reaction with hy coment cont Apparatus 5. Phaomcer-One ofthe flowing given in oer of pcre ‘SLT Nephlonster or ubiimee, 51.2 Speophaamete To eset 20m with igh ph of Ato Semand 5:13 Fler planter wih vl er having & max ‘mum ner €20 nm and ight pa of 419 3m. Fer Pomel and potmetic paces preside hi et fthod ull confor to Practise B40, wecpotomect ates tl olor to Pacis EIS 52 Stopwatch, esse 0. mie 53 Measuring Spoon capicy 021903 mb. 34 Dring ven, cpl of coninuusy heing a se 55 Bone, shal be eagle of reproducing res widhin (90002 gh an acuaty of #00002 Dine icaig Tulane shall hae a senviy not excsting 0.0001 CConetioel tropa balances shal have smi ily eit of OOS Any pid weighing device tat ‘may be provides, suchas chain, dumped to hey ‘ier sal nt ies the Ba lcency by ee tha at any reting ad Wi ay ond wii th ed ‘pect he ane A Sm Chaps eo ope hea std ‘Sony AST wt pram Tce Tae ie Ady Mc Ws Ay pm A fi a inGp crs00-15 56 Sirer, magnetic viable speed, with a, THE- ‘torcaton costed mga ving oan overhear win propel. (6, Reagents and Materials ‘61 Party of Reagnte—AB renga sal confor to te specieaons the Commits on Aas Reagents of he ‘eensan Chemie! Sos 162 Paty of Weer—Unles eerie nde, reference to et shal Seu oman agent ecto te Speieson DI, Type Oder ape waer pe (See Nowe 1 my bens prove fist scene Ua the ‘we of suet ign yy to pits ose woe ‘Uherslyalfting the pit sd tes te tet etd “REN geet 163 Borin. Clorde—Coysals of baium chloride (ac 2,0) serene to AN 0 600 ym To pear te Ahora. seal spt oe 2 luge wach pus, dese {34h een feore ay esas Ul a ot 80 0 600 fi se ore, ‘4 Conditioning Reapet-Plce 30 mL of cocetacd Anrochone nit CL sp p19). 200 reagent wate, 10 IRL 884% hale propel an 5 gsm chide {SGCD i aso Add 30 ma perl a 165 Siete Sain, Sand (tm. = 0100 my SO, Dinatoe © 187 g of anys soi site (0,50. ‘te ud die wth aero Lina volume sk. 166 pH poper adil to eat 5p ws. 67 Sod Hyde, (OIN)—Dislve 4 of sium hone (N2OH) i rae nd te with wat fo HL 168 Hydrochloric Acid (218) 8.6m of concen trad ioc a O41 sp 1-19) tT with wae 17, Permit Variations 111 Both the ile meted snd quid methods as derived Tet Mets Cee permissible as aeratves tote tiie rose. 1, Callpraton and Standariization 1.1 Pepe sandr by dling 00,20, $0,100,150, 200,300 nd f0.0 mL of sada sli slion with wae ib Tod volume ie volume ass These soon wil vests coneatns of 00,2150, 10,130,200, 300, an 00 mg rrp Fallow the poste gen in Stcton9 wing sppopnte motto he andar sae Binion repr. tcteaee ah 5nd prepare first cave showing suf on cota it mg loti ‘inte canespontng plone rang oon Shige ropa i seein ro bes Ua etn Se Pr oat AST eed eM} RODENT 9 2A separ clraton carve must be prepare foreach ior nd ane curve rb prepa seca, {Dchange te sl arp or ter, oe any oe abn of Inorument or reagnts ne made. Chek he eave wih e2 ce fib roming two of more slatons of Known Shit snc nt range Yo 40mg SOL Non 2M spot cane my mea Ww rahe 0 ne soAtearase nae 1 Colt test 10 gf representative slo anal ‘ye simple for 18028 110°. Cra pas 600 Jimena 409m bela bled Sample A put ample sining of spose 30 p Tn a second 00 mesh IneledSupleB place ssl of spreaiatl 3p Record thems of ech ple to threat 0.001 g Add 280 ml of ‘Sooo wate fo ac Beste and ton & magnet ier forte 0 bb 0 more than 12h Pere extn through to ry sou etre er apr ude sein. Do fo wah the reside. Repeat te ato soln is not ou Chest the pi of te eae wing pH per and ode aul each leet pH of 7 = singer 0.18 Het or.N NaOH ‘92 Adj the temper of he solution in the veut task to Between 39 ted 25°C (55 1077 93 Use an alqut of 10 mL for specimen Al, 20 mL for spesimen a, 1m forpcinen BI, and 20m fr spimen Bite 6 wae of 100ml na volute Has od fan th poate tow or To Matode Cts, Por the Too mts a 280 ml boa, Ad 5.0m condoning tengo Ma by eg wih ss bat and apc ati. [Rad 3g of te pop BoC ess using meting {pon and act 94 Sir exacly 1.0 min athe same cons speed or all 195 Remove the beste rom th sie, poor sition ino tte col and pt te ell no the pometer. Record the tary at #0 ar poring the slain mt the oll ‘96 Determine the mg of $0, fom he ean curve 10, Caleaatin o Interpretation of Results 10 Cake the mt coment (% by mas) for ech posinen a flows 1 50, a died si Imo 950, scl fom eration carve tar fsa me 00m eae ue of alga specie. ns 102 Limits of vals fore ob va. See Note 3) on on neate =| PES ay a osname Ant Nf in sinWp c1500-15 1 Deemine which res fl within he above limits 2 Disa tone a et 4. Argel ie hat comply erSteW mph mda of ince sple pe when aon ieee rect pena 1 Report 1 Report the average oid 8% sue by mas of samp. Ilias alate mops of me SO hg Sei sea, many Salty 10 OM Repo ae ‘are: 001 o 10 mph 121 Prcson—Te standard devon was fou 0 vy ith concent, eee cuenta iain wt Sep th i. AST et ng ‘eet cos eco ‘sod fr the poke. The ingle operator cece 1 varation Wa oun be 8. Teer ol fo rope cndated es by the sae operate the ste Final shouldnt fer by more tan [24% of he verge The mullabortay cots fw was food tobe 212% Therefore esi of two dirt ibs dene sper of» tel shoslé no die fro ech ‘ter by ore tha 60 5 of tl averse 122 BiesSive tere & 90 scape reference male suinble for deteminng Bis, bas an 20 be dried, 13, Keywords 13. hyde coment si Sue; mite ANNEX ‘taney Information) ‘A, REDUCING THLE NUMUER OF SUD-SAMPLES AND SAMPLES OUT OF COMPLIANCE. AL. This proofre was wie to sccommote aon ‘itt are ot familar wit the a aoder tet per Toop caval alse number of sub sampe, nor ‘uns many be we AL2 If sample fils above 3.3 ali, hn iit ‘mpi mise dor itn canbe ued I is proce 'S flowed han he mg SO, rom the tins ead ‘all be manne win to 40 mgt saber procodare i usd, then vation wal be povided showing hat tbe ‘sls re win he nea geo he eabraon SUMMARY OF CHANGES Commiase C19 hs idee the loeation of selected changes w this et method soe the Int ae, (SH00F", ut may input he ue af Bs med. (Approved Ox |, 2013) 1) Ries Sesion So AST ard Ta 21 EDT NE ‘Seema