Code No: 117AK Set No.

1
JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD
IV B .Tech. I Sem., I Mid-Term Examinations, September -2017
ANALYTICAL INSTRUMENTATION
Objective Exam
Name: ______________________________ Hall Ticket No. A
Answer All Questions. All Questions Carry Equal Marks. Time: 20 Min. Marks: 10.

I. Choose the correct alternative:

1. When the reading of a pH meter changes from 5 to 7, the hydrogen ion concentration of the solution is
[ ]
a) Halved b) doubled c) increases 100 times d) decreased 100 times

2. In the Sodium analyzer we add Ammonia in order to [ ]

a) maintain the pH constant b) standardize the sample solution
c) Because it is essential component with ISE d) All

3. Glass Electrode has a measurement range of _______. [ ]

A) PH 1 TO PH 11 B) PH 0 TO PH 11 C) PH 1 TO PH 15 D) PH 0TO PH 15

4. Colorimetry is used to analyze [ ]

a) NO B) NITROGEN C) NO3 D) NOX

5. The transmittance of a particular solution measured is T. The concentration of the solution is now doubled.
Assuming that Beer Lamberts law holds good for both the cases, the transmittance for the second would
be__________ . [ ]
2 1/2
a)T/2 b) 2T c)T d)(T)
6. For the measurement of Conductance [ ]
a) Direct reading instrument are preferred over the null balance type instrument.
b) Null balance instrument are preferred over the Direct reading type instrument.
c) Direct reading instrument and null balance type instrument are equally preferred.
d) Both instruments cannot be used.

7. Match the instrument to the characteristics [ ]

A)Interferometer i) wavelength dispersion
B) monochromator ii) magnifying power
iii) Flatness measurement
a) A-i ; B-ii b) A-ii ; B-iii c) A-iii ; B-i d) A-iii ; B-ii

8. A Gas Chromatograph is used for [ ]

a) Measuring flow rate of a gas b) measuring the temp of a gas
c) Measuring the pressure of a gas d) analysing the composition of a gas
9. IR Spectroscopy [ ]
a) Has a useful range of radiation from 2.5 to 15 microns b) is unsuitable for analysis of mixture of metals
c) is unsuitable for analysis of organic gases d) Uses bolometer as one of the detectors

10. A Photodiode functions as [ ]

a) Photoconductive device while working with reverse volt
b) Photovoltaic device while working without a reverse volt
c)photovoltaic device while working with or without reverse volt d)None of the above

Cont..2
Code No:117AK :2: Set No. 1

II Fill in the Blanks

11. The potential of pH electrode is given by__________.

12. Chromatograph can be used for body fluids. (T/F)

13. In Chromatogram , the area under the peak gives ___________ indication .

14. NOx when passed into an evacuated flask containing a solution of H2O2 in Sulphuric acid, the oxides of
nitrogen is converted into ____________.

15. Chemiluminescence is ______________.

16. A Combination electrode can be used within the temperature range _____________.

17. Despite the addition of an acid or base, the pH remains constant in __________ solution.

18. Paramagnetism can be used for the analysis of _______.

19. _____________ correction is employed in Beckman pH meter.

20. For good efficiency the column preferred is ____________

-oOo-
Code No: 117AK Set No. 2
JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD
IV B .Tech. I Sem., I Mid-Term Examinations, September -2017
ANALYTICAL INSTRUMENTATION
Objective Exam
Name: ______________________________ Hall Ticket No. A
Answer All Questions. All Questions Carry Equal Marks. Time: 20 Min. Marks: 10.

I. Choose the correct alternative:

1. Colorimetry is used to analyze [ ]
a) NO B) NITROGEN C) NO3 D) NOX

2. The transmittance of a particular solution measured is T. The concentration of the solution is now doubled.
Assuming that Beer Lamberts law holds good for both the cases, the transmittance for the second would
be__________ . [ ]
2 1/2
a)T/2 b) 2T c)T d)(T)
3. For the measurement of Conductance [ ]
a) Direct reading instrument are preferred over the null balance type instrument.
b) Null balance instrument are preferred over the Direct reading type instrument.
c) Direct reading instrument and null balance type instrument are equally preferred.
d) Both instruments cannot be used.

4. Match the instrument to the characteristics [ ]

A)Interferometer i) wavelength dispersion
B) monochromator ii) magnifying power
iii) Flatness measurement
a) A-i ; B-ii b) A-ii ; B-iii c) A-iii ; B-i d) A-iii ; B-ii

5. A Gas Chromatograph is used for [ ]

a) Measuring flow rate of a gas b) measuring the temp of a gas
c) Measuring the pressure of a gas d) analysing the composition of a gas
6. IR Spectroscopy [ ]
a) Has a useful range of radiation from 2.5 to 15 microns b) is unsuitable for analysis of mixture of metals
c) is unsuitable for analysis of organic gases d) Uses bolometer as one of the detectors

7. A Photodiode functions as [ ]
a) Photoconductive device while working with reverse volt
b) Photovoltaic device while working without a reverse volt
c)photovoltaic device while working with or without reverse volt d)None of the above
8. When the reading of a pH meter changes from 5 to 7, the hydrogen ion concentration of the solution is
[ ]
a) Halved b) doubled c) increases 100 times d) decreased 100 times

9. In the Sodium analyzer we add Ammonia in order to [ ]

a) maintain the pH constant b) standardize the sample solution
c) Because it is essential component with ISE d) All

10. Glass Electrode has a measurement range of _______. [ ]

A) PH 1 TO PH 11 B) PH 0 TO PH 11 C) PH 1 TO PH 15 D) PH 0TO PH 15

Cont..2
Code No:117AK :2: Set No. 2

II Fill in the Blanks

11. NOx when passed into an evacuated flask containing a solution of H2O2 in Sulphuric acid, the oxides of
nitrogen is converted into ____________.

12. Chemiluminescence is ______________.

13. A Combination electrode can be used within the temperature range _____________.

14. Despite the addition of an acid or base, the pH remains constant in __________ solution.

15. Paramagnetism can be used for the analysis of _______.

16. _____________ correction is employed in Beckman pH meter.

17. For good efficiency the column preferred is ____________

18. The potential of pH electrode is given by__________.

19. Chromatograph can be used for body fluids. (T/F)

20. In Chromatogram , the area under the peak gives ___________ indication .

-oOo-
Code No: 117AK Set No. 3
JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD
IV B .Tech. I Sem., I Mid-Term Examinations, September -2017
ANALYTICAL INSTRUMENTATION
Objective Exam
Name: ______________________________ Hall Ticket No. A
Answer All Questions. All Questions Carry Equal Marks. Time: 20 Min. Marks: 10.

I. Choose the correct alternative:

1. For the measurement of Conductance [ ]
a) Direct reading instrument are preferred over the null balance type instrument.
b) Null balance instrument are preferred over the Direct reading type instrument.
c) Direct reading instrument and null balance type instrument are equally preferred.
d) Both instruments cannot be used.

2. Match the instrument to the characteristics [ ]

A)Interferometer i) wavelength dispersion
B) monochromator ii) magnifying power
iii) Flatness measurement
a) A-i ; B-ii b) A-ii ; B-iii c) A-iii ; B-i d) A-iii ; B-ii

3. A Gas Chromatograph is used for [ ]

a) Measuring flow rate of a gas b) measuring the temp of a gas
c) Measuring the pressure of a gas d) analysing the composition of a gas
4. IR Spectroscopy [ ]
a) Has a useful range of radiation from 2.5 to 15 microns b) is unsuitable for analysis of mixture of metals
c) is unsuitable for analysis of organic gases d) Uses bolometer as one of the detectors

5. A Photodiode functions as [ ]
a) Photoconductive device while working with reverse volt
b) Photovoltaic device while working without a reverse volt
c)photovoltaic device while working with or without reverse volt d)None of the above
6. When the reading of a pH meter changes from 5 to 7, the hydrogen ion concentration of the solution is
[ ]
a) Halved b) doubled c) increases 100 times d) decreased 100 times

7. In the Sodium analyzer we add Ammonia in order to [ ]

a) maintain the pH constant b) standardize the sample solution
c) Because it is essential component with ISE d) All

8. Glass Electrode has a measurement range of _______. [ ]

A) PH 1 TO PH 11 B) PH 0 TO PH 11 C) PH 1 TO PH 15 D) PH 0TO PH 15

9. Colorimetry is used to analyze [ ]

a) NO B) NITROGEN C) NO3 D) NOX

10. The transmittance of a particular solution measured is T. The concentration of the solution is now doubled.
Assuming that Beer Lamberts law holds good for both the cases, the transmittance for the second would
be__________ . [ ]
a)T/2 b) 2T c)T2 d)(T)1/2

Cont..2
Code No:117AK :2: Set No. 3

II Fill in the Blanks

11. A Combination electrode can be used within the temperature range _____________.

12. Despite the addition of an acid or base, the pH remains constant in __________ solution.

13. Paramagnetism can be used for the analysis of _______.

14. _____________ correction is employed in Beckman pH meter.

15. For good efficiency the column preferred is ____________

16. The potential of pH electrode is given by__________.

17. Chromatograph can be used for body fluids. (T/F)

18. In Chromatogram , the area under the peak gives ___________ indication .

19. NOx when passed into an evacuated flask containing a solution of H2O2 in Sulphuric acid, the oxides of
nitrogen is converted into ____________.

20. Chemiluminescence is ______________.

-oOo-
Code No: 117AK Set No. 4
JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD
IV B .Tech. I Sem., I Mid-Term Examinations, September -2017
ANALYTICAL INSTRUMENTATION
Objective Exam
Name: ______________________________ Hall Ticket No. A
Answer All Questions. All Questions Carry Equal Marks. Time: 20 Min. Marks: 10.

I. Choose the correct alternative:

1. A Gas Chromatograph is used for [ ]
a) Measuring flow rate of a gas b) measuring the temp of a gas
c) Measuring the pressure of a gas d) analysing the composition of a gas
2. IR Spectroscopy [ ]
a) Has a useful range of radiation from 2.5 to 15 microns b) is unsuitable for analysis of mixture of metals
c) is unsuitable for analysis of organic gases d) Uses bolometer as one of the detectors

3. A Photodiode functions as [ ]
a) Photoconductive device while working with reverse volt
b) Photovoltaic device while working without a reverse volt
c)photovoltaic device while working with or without reverse volt d)None of the above
4. When the reading of a pH meter changes from 5 to 7, the hydrogen ion concentration of the solution is
[ ]
a) Halved b) doubled c) increases 100 times d) decreased 100 times

5. In the Sodium analyzer we add Ammonia in order to [ ]

a) maintain the pH constant b) standardize the sample solution
c) Because it is essential component with ISE d) All

6. Glass Electrode has a measurement range of _______. [ ]

A) PH 1 TO PH 11 B) PH 0 TO PH 11 C) PH 1 TO PH 15 D) PH 0TO PH 15

7. Colorimetry is used to analyze [ ]

a) NO B) NITROGEN C) NO3 D) NOX

8. The transmittance of a particular solution measured is T. The concentration of the solution is now doubled.
Assuming that Beer Lamberts law holds good for both the cases, the transmittance for the second would
be__________ . [ ]
2 1/2
a)T/2 b) 2T c)T d)(T)
9. For the measurement of Conductance [ ]
a) Direct reading instrument are preferred over the null balance type instrument.
b) Null balance instrument are preferred over the Direct reading type instrument.
c) Direct reading instrument and null balance type instrument are equally preferred.
d) Both instruments cannot be used.

10. Match the instrument to the characteristics [ ]

A)Interferometer i) wavelength dispersion
B) monochromator ii) magnifying power
iii) Flatness measurement
a) A-i ; B-ii b) A-ii ; B-iii c) A-iii ; B-i d) A-iii ; B-ii

Cont..2
Code No:117AK :2: Set No. 4

II Fill in the Blanks

11. Paramagnetism can be used for the analysis of _______.

12. _____________ correction is employed in Beckman pH meter.

13. For good efficiency the column preferred is ____________

14. The potential of pH electrode is given by__________.

15. Chromatograph can be used for body fluids. (T/F)

16. In Chromatogram , the area under the peak gives ___________ indication .

17. NOx when passed into an evacuated flask containing a solution of H2O2 in Sulphuric acid, the oxides of
nitrogen is converted into ____________.

18. Chemiluminescence is ______________.

19. A Combination electrode can be used within the temperature range _____________.

20. Despite the addition of an acid or base, the pH remains constant in __________ solution.

-oOo-