Second Soils Report Carolina Beach Lake

ECS Southeast, LLP
Geotechnical Engineering Report

Carolina Beach Lake
Carolina Beach, New Hanover County, North Carolina
ECS Project Number # 22:25877
October 9, 2017
October 9, 2017
Mr. Gregory R. Thompson, PE, PLS

SEPI Engineering & Construction
5030 New Centre Drive, Suite B
Wilmington, North Carolina 28403
ECS Project No. 22:25877
Reference: Geotechnical Engineering Report

Carolina Beach Lake
Carolina Beach, New Hanover County, North Carolina
Dear Mr. Thompson:
ECS Southeast (ECS) has completed the subsurface exploration, laboratory testing, and geotechnical
engineering analyses for the above-referenced project. Our services were performed in general
accordance with our Proposal No. 22.21909R1-GP, dated September 26, 2017. This report presents
our understanding of the geotechnical aspects of the project along, the results of the field
exploration and laboratory testing conducted, and our design and construction.
It has been our pleasure to be of service to SEPI Engineering & Constructions (SEPI) during the design
phase of this project. We would appreciate the opportunity to remain involved during the
continuation of the design phase, and we would like to provide our services during construction
phase operations as well to verify the assumptions of subsurface conditions made for this report.
Should you have any questions concerning the information contained in this report, or if we can be of
further assistance to you, please contact us.
Respectfully submitted,
ECS Southeast, LLP
Mike Ellis, E.I. Winslow Goins, PE

Project Manager Principal Engineer
MElllis@ecslimited.com WGoins@ecslimited.com
10/09/17
Carolina Beach Lake October 9, 2017
ECS Project No. 22:25877 Page i
TABLE OF CONTENTS
EXECUTIVE SUMMARY .................................................................................................................. 1

1.0 INTRODUCTION....................................................................................................................... 2
1.1 General ............................................................................................................................. 2
1.2 Scope of Services ............................................................................................................... 2
1.3 Authorization .................................................................................................................... 2
2.0 PROJECT INFORMATION ......................................................................................................... 3
2.1 Project Location ................................................................................................................ 3
2.2 Current Site Conditions ..................................................................................................... 3
2.3 Proposed Construction ...................................................................................................... 3
3.0 FIELD EXPLORATION ............................................................................................................... 4
3.1 Field Exploration Program ................................................................................................. 4
3.1.1 Vibracore Samples ................................................................................................... 4
3.1.2 Grab Samples ........................................................................................................... 4
3.2 Regional/Site Geology ....................................................................................................... 4
4.0 LABORATORY TESTING............................................................................................................ 6
5.0 SITE CONSTRUCTION RECOMMENDATIONS............................................................................ 7
6.0 CLOSING .................................................................................................................................. 8
ECS Project No. 22:25877 Page ii
APPENDICES
Appendix A Drawings & Reports

Site Location Diagram
Exploration Location Diagram
Appendix B Laboratory Testing

Laboratory Test Results Summary
TPH GRO tests (SW-846 5030+8015)
TPH DRO tests (SW-846 3550/8015)
SVOCs tests (EPA 625 / SW-846 8270D)
BETEX screens (8260)
RCRA Metals test (SW-846 6010 7470 / 7471)
Hexavalent Chromium tests (SM 3500 CRD / SW-846 7196)
TCL Volatile Organics tests (SW-846 8260)
TCL pesticides/PCB tests (SW-846 8081/8082)
Grain Size Analysis tests with hydrometer (ASTM D422)
Appendix C Supplemental Report Documents

ASFE Document
ECS Project No. 22:25877 Page 1
EXECUTIVE SUMMARY
The following summarizes the main findings of the field exploration and laboratory results for the
Carolina Beach Lake project in Carolina Beach, New Hanover County, North Carolina.
Three (3) grab samples were taken at the soil stockpile at the Carolina Beach Water
department. Additionally (3) vibracore samples were taken at approximately 12 feet
beneath the mudline in the existing lake.
The following tests were conducted on the soil samples:

o TPH GRO tests (SW-846 5030+8015)
o TPH DRO tests (SW-846 3550/8015)
o SVOCs tests (EPA 625 / SW-846 8270D)
o BETEX screens (8260)
o RCRA Metals test (SW-846 6010 7470 / 7471)
o Hexavalent Chromium tests (SM 3500 CRD / SW-846 7196)
o TCL Volatile Organics tests (SW-846 8260)
o TCL pesticides/PCB tests (SW-846 8081/8082)
o Grain Size Analysis tests with hydrometer (ASTM D422)
1.0 INTRODUCTION
1.1 GENERAL
The purpose of this study was to provide geotechnical and laboratory information for the
expected dredge soil at the existing Carolina Beach Lake in Carolina Beach, New Hanover County,
North Carolina.
The recommendations developed for this report are based on project information supplied SEPI.
This report contains the results of our subsurface explorations and laboratory analysis to aid in
planning for the project.
1.2 SCOPE OF SERVICES
To obtain the requested laboratory results, three (3) grab samples and three (3) vibracore
samples were obtained.
This report discusses our exploratory and testing procedures, presents our findings and
evaluations and includes the following:
A brief review and description of our field test procedures and the results of testing
conducted;
A review of surface topographical features and site conditions;
A review of area and site geologic conditions;
A review of subsurface soil stratigraphy with pertinent available physical properties;
Discussion of groundwater impact;
Laboratory test results;
Site vicinity map; and
Exploration location plan.
1.3 AUTHORIZATION
Our services were provided in accordance with our Proposal No. 22.21909R1-GP, dated
September 26, 2017, and includes the Terms and Conditions of Service outlined with our
Proposal.
2.0 PROJECT INFORMATION
2.1 PROJECT LOCATION
The proposed project site is located at the existing Carolina Beach lake Park in Carolina Beach,
New Hanover County, North Carolina. Figure 2.1.1 below shows an aerial image of the sites.
Figure 2.1.1. Site Location
2.2 CURRENT SITE CONDITIONS
The sites consist of an existing lake located at the existing Carolina Beach lake Park in Carolina
Beach, North Carolina.
2.3 PROPOSED CONSTRUCTION
The project consists of dredging the existing lake and using the soil from the lake as structural fill,
if possible.
3.0 FIELD EXPLORATION
3.1 FIELD EXPLORATION PROGRAM
The field exploration was planned with the objective of obtaining samples to perform the
requested laboratory tests.
3.1.1 Vibracore Samples
Three (3) vibracore samples (Zone 1, Zone 2, and Zone 4) were obtained at the existing lake at
approximately 12 feet below the waterline. The approximate test locations are shown on the
attached exploration diagram.
3.1.2 Grab Samples
Three (3) grab samples (Sp-1 through Sp-3) were taken at the stockpiled soil that was dredged
from the existing lake and stored at the Carolina Beach water department
3.2 REGIONAL/SITE GEOLOGY
The site is located in the Coastal Plain Physiographic Province of North Carolina. The Coastal Plain
is composed of seven terraces, each representing a former level of the Atlantic Ocean. Soils in
this area generally consist of sedimentary materials transported from other areas by the ocean or
rivers. These deposits vary in thickness from a thin veneer along the western edge of the region
to more than 10,000 feet near the coast. The sedimentary deposits of the Coastal Plain rest upon
consolidated rocks similar to those underlying the Piedmont and Mountain Physiographic
Provinces. In general, shallow unconfined groundwater movement within the overlying soils is
largely controlled by topographic gradients. Recharge occurs primarily by infiltration along higher
elevations and typically discharges into streams or other surface water bodies. The elevation of
the shallow water table is transient and can vary greatly with seasonal fluctuations in
precipitation.
Based on the U.S. Geological Survey1,2 the site of the proposed construction lies within the
Surficial Deposits (Qp) geologic formation. The formation generally consists of alluvial sands, silts
and clayss. An overview of the general site geology is illustrated in Figure 3.2.1 below.
1
The North Carolina Dept. of Environment, Health, and Natural Resources, Division of Land Resources, NC Geological
Survey, in cooperation with the NC Center for Geographic Information and Analysis, 1998, Geology - North Carolina
(1:250,000), coverage data file geol250. The data represents the digital equivalent of the official State Geology map
(1:500,000 scale), but was digitized from (1:250,000 scale) base maps.
2
Rhodes, Thomas S., and Conrad, Stephen G., 1985, Geologic Map of North Carolina: Department of Natural Resources
and Community Development, Division of Land Resources, and the NC Geological Survey, 1:500,000-scale, compiled by
Brown, Philip M., et al, and Parker, John M. III, and in association with the State Geologic Map Advisory Committee.
Figure 3.2.1
Geologic map for Figure 3.2.1 obtained from The North Carolina Dept. of Environment, Health, and Natural Resources, Division of Land
Resources, NC Geological Survey, in cooperation with the NC Center for Geographic Information and Analysis, 1998, Geology - North
Carolina (1:250,000), coverage data file geol250 and Google Earth.
4.0 LABORATORY TESTING

The laboratory testing performed by ECS for this project consisted of selected tests performed on
samples obtained during our field exploration operations. The following paragraphs briefly
discuss the results of the completed laboratory testing program.
Bulk soil samples were obtained at depths ranging from approximately 1 to 3 feet below the
existing ground surface and were subjected to moisture (ASTM D2974-87), pH (EPA 9045) sulfide
soil (SM 4500-S2d), sulfate ion (ASTM D 516-16) and chloride ion (ASTM D 512-12) testing. The
corrosion series testing results are shown in Table 4.1 below.
Perform six (6)TPH GRO tests (SW-846 5030+8015)
Perform six (6)TPH DRO tests (SW-846 3550/8015)
Perform six (6) SVOCs tests (EPA 625 / SW-846 8270D)
Perform six (6) BETEX screens (8260)
Perform six (6) RCRA Metals test (SW-846 6010 7470 / 7471)
Perform six (6) Hexavalent Chromium tests (SM 3500 CRD / SW-846 7196)
Perform six (6) TCL Volatile Organics tests (SW-846 8260)
Perform six (6) TCL pesticides/PCB tests (SW-846 8081/8082)
Perform six (6) Grain Size Analysis tests with hydrometer (ASTM D422)
5.0 SITE CONSTRUCTION RECOMMENDATIONS
Unsatisfactory Materials: Unsatisfactory fill materials include materials which to not satisfy the
requirements for suitable materials, as well as topsoil and organic materials (OH, OL), elastic Silt
(MH), and high plasticity Clay (CH) as encountered in Zone 1 and Zone 2 of the lake. The CEC can
consider allowing soils these soils to be used as Structural Fill at depths greater than 4 feet below
pavement subgrades outside the expanded building limits and within non-structural areas.
On-Site Borrow Suitability: Most materials contained within the on-site stockpiles as well as Zone
4 of the lake are expected to be suitable for use as fill. Limited moisture conditioning of the fill
lifts will be required to achieve compaction for the soils from the stockpile. Moisture conditioning
of the material of Zone 4 will be required prior to any fill placement.
Chemical Analysis: Based on the laboratory analysis, the samples tested positive for DROs,
arsenic, barium, chromium, lead, mercury. Based on the Inactive Hazardous Sites Branch (IHSB)
Preliminary Residential Health Based Soil Remediation Goal, the laboratory analysis detected
levels of arsenic above the IHSB PSRG values. Arsenic can typically occur naturally at elevated
levels above the IHSB levels.
6.0 CLOSING
ECS has prepared this report of findings, evaluations, and recommendations to guide
geotechnical-related design and construction aspects of the project.
The description of the proposed project is based on information provided to ECS by SEPI. If any of
this information is inaccurate, either due to our interpretation of the documents provided or site
or design changes that may occur later, ECS should be contacted immediately so that we can
review the report in light of the changes and provide additional or alternate recommendations as
may be required to reflect the proposed construction.
We recommend that ECS be allowed to review the projects plans and specifications pertaining to
our work so that we may ascertain consistency of those plans/specifications with the intent of the
geotechnical report.
Field observations, monitoring, and quality assurance testing during earthwork and foundation
installation are an extension of and integral to the geotechnical design recommendation. We
recommend that the owner retain these quality assurance services and that ECS be allowed to
continue our involvement throughout these critical phases of construction to provide general
consultation as issues arise. ECS is not responsible for the conclusions, opinions, or
recommendations of others based on the data in this report.
APPENDIX A Drawings & Reports
Site Location Diagram

Exploration Location Diagram
Service Layer Credits: USGS The National Map: Orthoimagery
SITE LOCATION DIAGRAM

ENGINEER
WEG
SCALE
CAROLINA BEACH LAKE NTS
PROJECT NO.
22:25877
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DATE
CAROLINA BEACH, NORTH CAROLINA 10/3/2017
Test
Location
Test
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Test
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APPENDIX B Laboratory Testing Results
TPH GRO tests (SW-846 5030+8015)

TPH DRO tests (SW-846 3550/8015)
SVOCs tests (EPA 625 / SW-846 8270D)
BETEX screens (8260)
RCRA Metals test (SW-846 6010 7470 / 7471)
Hexavalent Chromium tests (SM 3500 CRD / SW-846 7196)
TCL Volatile Organics tests (SW-846 8260)
TCL pesticides/PCB tests (SW-846 8081/8082)
Grain Size Analysis tests with hydrometer (ASTM D422)
#=CL#
Pace Analytical Services, LLC

9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LIMS USE: FR - FREDDIE WESCOTT

LIMS OBJECT ID: 92357321
October 06, 2017
Freddie Wescott
ECS Wilmington
6714 Netherlands Dr
Wilmington, NC 28405
RE: Project: CB-Site 9/29

Pace Project No.: 92357321
Dear Freddie Wescott:

Enclosed are the analytical results for sample(s) received by the laboratory on September 30, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
taylor.ezell@pacelabs.com
(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 77
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CERTIFICATIONS
Project: CB-Site 9/29

Charlotte Certification IDs

9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs

2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712

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SAMPLE ANALYTE COUNT

Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92357321001 ZONE 1 EPA 8015 Modified NU1 2 PASI-C

EPA 8081 PKS 24 PASI-C
EPA 8015 Modified WDV 2 PASI-C
EPA 6010 SER 7 PASI-A
EPA 7471 KAL 1 PASI-A
EPA 8270 RES 74 PASI-C
EPA 8260 DLK 70 PASI-C
ASTM D2974-87 CLW 1 PASI-C
EPA 7196 EWS 1 PASI-A
92357321004 SP-1 EPA 8015 Modified NU1 2 PASI-C

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SAMPLE ANALYTE COUNT

Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
EPA 8260 ZDO 70 PASI-C

EPA 8260 ZDO 70 PASI-C

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SUMMARY OF DETECTION

Lab Sample ID Client Sample ID

Method Parameters Result Units Report Limit Analyzed Qualifiers
92357321001 ZONE 1
EPA 8015 Modified Diesel Range Organics(C10-C28) 22.6 mg/kg 10.6 10/04/17 09:55
EPA 6010 Arsenic 2.1 mg/kg 1.5 10/03/17 18:25
EPA 6010 Barium 7.1 mg/kg 0.74 10/03/17 14:54
EPA 6010 Chromium 9.0 mg/kg 0.74 10/03/17 14:54
EPA 6010 Lead 16.8 mg/kg 0.74 10/03/17 14:54
EPA 7471 Mercury 0.013 mg/kg 0.0082 10/06/17 01:08
ASTM D2974-87 Percent Moisture 53.6 % 0.10 10/04/17 09:25
92357321002 ZONE 2
EPA 6010 Arsenic 3.4 mg/kg 3.2 10/03/17 18:37
EPA 6010 Barium 11.8 mg/kg 1.6 10/03/17 15:05
EPA 6010 Lead 15.2 mg/kg 1.6 10/03/17 15:05
92357321003 ZONE 4
EPA 6010 Barium 7.8 mg/kg 0.89 10/03/17 15:09
EPA 6010 Lead 9.1 mg/kg 0.89 10/03/17 15:09
EPA 7471 Mercury 0.014 mg/kg 0.0062 10/06/17 01:13
92357321004 SP-1
EPA 6010 Barium 5.9 mg/kg 0.53 10/03/17 15:12
EPA 6010 Lead 2.9 mg/kg 0.53 10/03/17 15:12
EPA 7471 Mercury 0.0057 mg/kg 0.0025 10/06/17 01:15
92357321005 SP-2
EPA 6010 Barium 3.8 mg/kg 0.45 10/03/17 15:16
EPA 6010 Lead 2.8 mg/kg 0.45 10/03/17 15:16
EPA 7471 Mercury 0.0028 mg/kg 0.0027 10/06/17 01:17
92357321006 SP-3
EPA 6010 Arsenic 0.79 mg/kg 0.72 10/03/17 19:09
EPA 6010 Barium 7.8 mg/kg 0.36 10/03/17 15:19
EPA 6010 Lead 2.6 mg/kg 0.36 10/03/17 15:19

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ANALYTICAL RESULTS

Sample: ZONE 1 Lab ID: 92357321001 Collected: 09/29/17 08:00 Received: 09/30/17 10:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28) 22.6 mg/kg 10.6 1 10/03/17 12:53 10/04/17 09:55
Surrogates
n-Pentacosane (S) 74 % 41-119 1 10/03/17 12:53 10/04/17 09:55 629-99-2
8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546
Aldrin ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 309-00-2

alpha-BHC ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 319-84-6
beta-BHC ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 319-85-7
delta-BHC ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 319-86-8
gamma-BHC (Lindane) ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 58-89-9
Chlordane (Technical) ND ug/kg 15.0 1 10/03/17 21:58 10/05/17 21:53 57-74-9
4,4'-DDD ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 72-54-8
4,4'-DDE ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 72-55-9
4,4'-DDT ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 50-29-3
Dieldrin ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 60-57-1
Endosulfan I ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 959-98-8
Endosulfan II ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 33213-65-9
Endosulfan sulfate ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 1031-07-8
Endrin ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 72-20-8
Endrin aldehyde ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 7421-93-4
Endrin ketone ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 53494-70-5
Heptachlor ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 76-44-8
Heptachlor epoxide ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 1024-57-3
Hexachlorobenzene ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 118-74-1
Methoxychlor ND ug/kg 10.7 1 10/03/17 21:58 10/05/17 21:53 72-43-5
Mirex ND ug/kg 10.7 1 10/03/17 21:58 10/05/17 21:53 2385-85-5
Toxaphene ND ug/kg 15.0 1 10/03/17 21:58 10/05/17 21:53 8001-35-2
Surrogates
Tetrachloro-m-xylene (S) 51 % 35-108 1 10/03/17 21:58 10/05/17 21:53 877-09-8
Decachlorobiphenyl (S) 48 % 21-123 1 10/03/17 21:58 10/05/17 21:53 2051-24-3
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016) ND ug/kg 70.6 1 10/03/17 21:58 10/04/17 13:34 12674-11-2
Surrogates
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gas Range Organics (C6-C10) ND mg/kg 12.6 1 10/03/17 14:30 10/05/17 04:27
Surrogates
4-Bromofluorobenzene (S) 86 % 70-167 1 10/03/17 14:30 10/05/17 04:27 460-00-4

Date: 10/06/2017 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 77
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ANALYTICAL RESULTS

6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.1 mg/kg 1.5 1 09/30/17 19:10 10/03/17 18:25 7440-38-2

Barium 7.1 mg/kg 0.74 1 09/30/17 19:10 10/03/17 14:54 7440-39-3
Cadmium ND mg/kg 0.15 1 09/30/17 19:10 10/03/17 14:54 7440-43-9
Chromium 9.0 mg/kg 0.74 1 09/30/17 19:10 10/03/17 14:54 7440-47-3
Lead 16.8 mg/kg 0.74 1 09/30/17 19:10 10/03/17 14:54 7439-92-1
Selenium ND mg/kg 1.5 1 09/30/17 19:10 10/03/17 14:54 7782-49-2
Silver ND mg/kg 0.74 1 09/30/17 19:10 10/03/17 14:54 7440-22-4
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.013 mg/kg 0.0082 1 10/05/17 12:30 10/06/17 01:08 7439-97-6
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 83-32-9

Acenaphthylene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 208-96-8
Aniline ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 62-53-3
Anthracene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 120-12-7
Benzo(a)anthracene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 56-55-3
Benzo(a)pyrene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 50-32-8
Benzo(b)fluoranthene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 205-99-2
Benzo(g,h,i)perylene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 191-24-2
Benzo(k)fluoranthene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 207-08-9
Benzoic Acid ND ug/kg 3610 1 10/06/17 09:06 10/06/17 13:04 65-85-0
Benzyl alcohol ND ug/kg 1450 1 10/06/17 09:06 10/06/17 13:04 100-51-6
4-Bromophenylphenyl ether ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 101-55-3
Butylbenzylphthalate ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 85-68-7
4-Chloro-3-methylphenol ND ug/kg 1450 1 10/06/17 09:06 10/06/17 13:04 59-50-7
4-Chloroaniline ND ug/kg 3610 1 10/06/17 09:06 10/06/17 13:04 106-47-8
bis(2-Chloroethoxy)methane ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 111-91-1
bis(2-Chloroethyl) ether ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 111-44-4
2-Chloronaphthalene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 91-58-7
2-Chlorophenol ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 95-57-8
4-Chlorophenylphenyl ether ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 7005-72-3
Chrysene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 218-01-9
Dibenz(a,h)anthracene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 53-70-3
Dibenzofuran ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 132-64-9
1,2-Dichlorobenzene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 95-50-1
1,3-Dichlorobenzene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 541-73-1 L2
3,3'-Dichlorobenzidine ND ug/kg 3610 1 10/06/17 09:06 10/06/17 13:04 91-94-1
2,4-Dichlorophenol ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 120-83-2
Diethylphthalate ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 84-66-2
2,4-Dimethylphenol ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 105-67-9
Dimethylphthalate ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 131-11-3
Di-n-butylphthalate ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 84-74-2
4,6-Dinitro-2-methylphenol ND ug/kg 1450 1 10/06/17 09:06 10/06/17 13:04 534-52-1

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ANALYTICAL RESULTS

2,4-Dinitrophenol ND ug/kg 3610 1 10/06/17 09:06 10/06/17 13:04 51-28-5

2,4-Dinitrotoluene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 121-14-2
Di-n-octylphthalate ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 117-81-7
Fluoranthene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 206-44-0
Fluorene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 86-73-7
Hexachloro-1,3-butadiene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 87-68-3
Hexachlorobenzene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 118-74-1
Hexachlorocyclopentadiene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 77-47-4
Hexachloroethane ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 193-39-5
Isophorone ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 78-59-1
1-Methylnaphthalene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 90-12-0
2-Methylphenol(o-Cresol) ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 95-48-7
3&4-Methylphenol(m&p Cresol) ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 15831-10-4
Naphthalene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 91-20-3
2-Nitroaniline ND ug/kg 3610 1 10/06/17 09:06 10/06/17 13:04 88-74-4
Nitrobenzene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 98-95-3
2-Nitrophenol ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 88-75-5
N-Nitrosodimethylamine ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 62-75-9
N-Nitroso-di-n-propylamine ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 621-64-7
N-Nitrosodiphenylamine ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 86-30-6
2,2'-Oxybis(1-chloropropane) ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 108-60-1
Pentachlorophenol ND ug/kg 3610 1 10/06/17 09:06 10/06/17 13:04 87-86-5
Phenanthrene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 85-01-8
Phenol ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 108-95-2
Pyrene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 129-00-0 L2
1,2,4-Trichlorobenzene ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 120-82-1
2,4,5-Trichlorophenol ND ug/kg 723 1 10/06/17 09:06 10/06/17 13:04 95-95-4
Surrogates
Nitrobenzene-d5 (S) 31 % 23-110 1 10/06/17 09:06 10/06/17 13:04 4165-60-0
2-Fluorobiphenyl (S) 15 % 30-110 1 10/06/17 09:06 10/06/17 13:04 321-60-8 S2
Terphenyl-d14 (S) 21 % 28-110 1 10/06/17 09:06 10/06/17 13:04 1718-51-0 S2
Phenol-d6 (S) 33 % 22-110 1 10/06/17 09:06 10/06/17 13:04 13127-88-3
2-Fluorophenol (S) 31 % 13-110 1 10/06/17 09:06 10/06/17 13:04 367-12-4
2,4,6-Tribromophenol (S) 31 % 27-110 1 10/06/17 09:06 10/06/17 13:04 118-79-6
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 281 1 10/04/17 18:59 67-64-1

Benzene ND ug/kg 14.1 1 10/04/17 18:59 71-43-2

#=AR#

(704)875-9092
ANALYTICAL RESULTS

Bromobenzene ND ug/kg 14.1 1 10/04/17 18:59 108-86-1

Bromochloromethane ND ug/kg 14.1 1 10/04/17 18:59 74-97-5
Bromodichloromethane ND ug/kg 14.1 1 10/04/17 18:59 75-27-4
Bromoform ND ug/kg 14.1 1 10/04/17 18:59 75-25-2
Bromomethane ND ug/kg 28.1 1 10/04/17 18:59 74-83-9
2-Butanone (MEK) ND ug/kg 281 1 10/04/17 18:59 78-93-3
n-Butylbenzene ND ug/kg 14.1 1 10/04/17 18:59 104-51-8
sec-Butylbenzene ND ug/kg 14.1 1 10/04/17 18:59 135-98-8
tert-Butylbenzene ND ug/kg 14.1 1 10/04/17 18:59 98-06-6
Carbon tetrachloride ND ug/kg 14.1 1 10/04/17 18:59 56-23-5
Chlorobenzene ND ug/kg 14.1 1 10/04/17 18:59 108-90-7
Chloroethane ND ug/kg 28.1 1 10/04/17 18:59 75-00-3
Chloroform ND ug/kg 14.1 1 10/04/17 18:59 67-66-3
Chloromethane ND ug/kg 28.1 1 10/04/17 18:59 74-87-3
2-Chlorotoluene ND ug/kg 14.1 1 10/04/17 18:59 95-49-8
1,2-Dibromo-3-chloropropane ND ug/kg 14.1 1 10/04/17 18:59 96-12-8
Dibromochloromethane ND ug/kg 14.1 1 10/04/17 18:59 124-48-1
1,2-Dibromoethane (EDB) ND ug/kg 14.1 1 10/04/17 18:59 106-93-4
Dibromomethane ND ug/kg 14.1 1 10/04/17 18:59 74-95-3
1,2-Dichlorobenzene ND ug/kg 14.1 1 10/04/17 18:59 95-50-1
Dichlorodifluoromethane ND ug/kg 28.1 1 10/04/17 18:59 75-71-8
1,1-Dichloroethane ND ug/kg 14.1 1 10/04/17 18:59 75-34-3
1,1-Dichloroethene ND ug/kg 14.1 1 10/04/17 18:59 75-35-4
cis-1,2-Dichloroethene ND ug/kg 14.1 1 10/04/17 18:59 156-59-2
trans-1,2-Dichloroethene ND ug/kg 14.1 1 10/04/17 18:59 156-60-5
1,2-Dichloropropane ND ug/kg 14.1 1 10/04/17 18:59 78-87-5
1,1-Dichloropropene ND ug/kg 14.1 1 10/04/17 18:59 563-58-6
cis-1,3-Dichloropropene ND ug/kg 14.1 1 10/04/17 18:59 10061-01-5
trans-1,3-Dichloropropene ND ug/kg 14.1 1 10/04/17 18:59 10061-02-6
Diisopropyl ether ND ug/kg 14.1 1 10/04/17 18:59 108-20-3
Ethylbenzene ND ug/kg 14.1 1 10/04/17 18:59 100-41-4
Hexachloro-1,3-butadiene ND ug/kg 14.1 1 10/04/17 18:59 87-68-3
2-Hexanone ND ug/kg 141 1 10/04/17 18:59 591-78-6
Isopropylbenzene (Cumene) ND ug/kg 14.1 1 10/04/17 18:59 98-82-8
p-Isopropyltoluene ND ug/kg 14.1 1 10/04/17 18:59 99-87-6
Methylene Chloride ND ug/kg 56.2 1 10/04/17 18:59 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/kg 141 1 10/04/17 18:59 108-10-1
Methyl-tert-butyl ether ND ug/kg 14.1 1 10/04/17 18:59 1634-04-4
Naphthalene ND ug/kg 14.1 1 10/04/17 18:59 91-20-3
n-Propylbenzene ND ug/kg 14.1 1 10/04/17 18:59 103-65-1

#=AR#

(704)875-9092
ANALYTICAL RESULTS

Styrene ND ug/kg 14.1 1 10/04/17 18:59 100-42-5

1,1,1,2-Tetrachloroethane ND ug/kg 14.1 1 10/04/17 18:59 630-20-6
Tetrachloroethene ND ug/kg 14.1 1 10/04/17 18:59 127-18-4
Toluene ND ug/kg 14.1 1 10/04/17 18:59 108-88-3
1,2,3-Trichlorobenzene ND ug/kg 14.1 1 10/04/17 18:59 87-61-6
1,1,1-Trichloroethane ND ug/kg 14.1 1 10/04/17 18:59 71-55-6
Trichloroethene ND ug/kg 14.1 1 10/04/17 18:59 79-01-6
Trichlorofluoromethane ND ug/kg 14.1 1 10/04/17 18:59 75-69-4
1,2,3-Trichloropropane ND ug/kg 14.1 1 10/04/17 18:59 96-18-4
1,2,4-Trimethylbenzene ND ug/kg 14.1 1 10/04/17 18:59 95-63-6
Vinyl acetate ND ug/kg 141 1 10/04/17 18:59 108-05-4
Vinyl chloride ND ug/kg 28.1 1 10/04/17 18:59 75-01-4
Xylene (Total) ND ug/kg 28.1 1 10/04/17 18:59 1330-20-7
m&p-Xylene ND ug/kg 28.1 1 10/04/17 18:59 179601-23-1
o-Xylene ND ug/kg 14.1 1 10/04/17 18:59 95-47-6
Surrogates
Toluene-d8 (S) 89 % 70-130 1 10/04/17 18:59 2037-26-5 1g
4-Bromofluorobenzene (S) 72 % 70-130 1 10/04/17 18:59 460-00-4
1,2-Dichloroethane-d4 (S) 103 % 70-132 1 10/04/17 18:59 17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 53.6 % 0.10 1 10/04/17 09:25
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196 Modified
Chromium, Hexavalent ND mg/kg 9.6 1 10/03/17 15:00 10/03/17 16:12 18540-29-9
Surrogates
n-Pentacosane (S) 72 % 41-119 1 10/03/17 12:53 10/04/17 09:55 629-99-2
Aldrin ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 309-00-2

alpha-BHC ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 319-84-6
beta-BHC ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 319-85-7
delta-BHC ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 319-86-8

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Chlordane (Technical) ND ug/kg 263 10 10/05/17 14:59 10/06/17 11:09 57-74-9
4,4'-DDD ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 72-54-8
4,4'-DDE ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 72-55-9
4,4'-DDT ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 50-29-3
Dieldrin ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 60-57-1
Endrin ND ug/kg 75.1 10 10/05/17 14:59 10/06/17 11:09 72-20-8
Methoxychlor ND ug/kg 188 10 10/05/17 14:59 10/06/17 11:09 72-43-5
Mirex ND ug/kg 188 10 10/05/17 14:59 10/06/17 11:09 2385-85-5
Toxaphene ND ug/kg 263 10 10/05/17 14:59 10/06/17 11:09 8001-35-2
Surrogates
Tetrachloro-m-xylene (S) 0 % 35-108 10 10/05/17 14:59 10/06/17 11:09 877-09-8 D3,S4
Decachlorobiphenyl (S) 0 % 21-123 10 10/05/17 14:59 10/06/17 11:09 2051-24-3 S4
PCB-1016 (Aroclor 1016) ND ug/kg 124 1 10/05/17 14:59 10/06/17 09:39 12674-11-2
Surrogates
Surrogates
Arsenic 3.4 mg/kg 3.2 1 09/30/17 19:10 10/03/17 18:37 7440-38-2

Barium 11.8 mg/kg 1.6 1 09/30/17 19:10 10/03/17 15:05 7440-39-3
Cadmium ND mg/kg 0.32 1 09/30/17 19:10 10/03/17 15:05 7440-43-9
Chromium 19.6 mg/kg 1.6 1 09/30/17 19:10 10/03/17 15:05 7440-47-3
Lead 15.2 mg/kg 1.6 1 09/30/17 19:10 10/03/17 15:05 7439-92-1
Selenium ND mg/kg 3.2 1 09/30/17 19:10 10/03/17 15:05 7782-49-2
Silver ND mg/kg 1.6 1 09/30/17 19:10 10/03/17 15:05 7440-22-4

#=AR#

(704)875-9092
ANALYTICAL RESULTS

Mercury ND mg/kg 0.012 1 10/05/17 12:30 10/06/17 01:10 7439-97-6

Aniline ND ug/kg 1260 1 10/06/17 09:06 10/06/17 13:33 62-53-3
Chrysene ND ug/kg 1260 1 10/06/17 09:06 10/06/17 13:33 218-01-9
Fluorene ND ug/kg 1260 1 10/06/17 09:06 10/06/17 13:33 86-73-7

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Phenol ND ug/kg 1260 1 10/06/17 09:06 10/06/17 13:33 108-95-2
Pyrene ND ug/kg 1260 1 10/06/17 09:06 10/06/17 13:33 129-00-0 L2
Surrogates
Nitrobenzene-d5 (S) 13 % 23-110 1 10/06/17 09:06 10/06/17 13:33 4165-60-0 S2
Terphenyl-d14 (S) 20 % 28-110 1 10/06/17 09:06 10/06/17 13:33 1718-51-0 S2
Phenol-d6 (S) 15 % 22-110 1 10/06/17 09:06 10/06/17 13:33 13127-88-3 S2
2-Fluorophenol (S) 5 % 13-110 1 10/06/17 09:06 10/06/17 13:33 367-12-4 S2
Acetone ND ug/kg 537 1 10/04/17 19:18 67-64-1 M1

Benzene ND ug/kg 26.8 1 10/04/17 19:18 71-43-2

#=AR#

(704)875-9092
ANALYTICAL RESULTS


cis-1,3-Dichloropropene ND ug/kg 26.8 1 10/04/17 19:18 10061-01-5 M1
trans-1,3-Dichloropropene ND ug/kg 26.8 1 10/04/17 19:18 10061-02-6 M1
Hexachloro-1,3-butadiene ND ug/kg 26.8 1 10/04/17 19:18 87-68-3 M1
2-Hexanone ND ug/kg 268 1 10/04/17 19:18 591-78-6
Methylene Chloride ND ug/kg 107 1 10/04/17 19:18 75-09-2
Naphthalene ND ug/kg 26.8 1 10/04/17 19:18 91-20-3 M1
n-Propylbenzene ND ug/kg 26.8 1 10/04/17 19:18 103-65-1 M1
Styrene ND ug/kg 26.8 1 10/04/17 19:18 100-42-5 M1
Toluene ND ug/kg 26.8 1 10/04/17 19:18 108-88-3
1,2,3-Trichlorobenzene ND ug/kg 26.8 1 10/04/17 19:18 87-61-6 M1
1,2,4-Trichlorobenzene ND ug/kg 26.8 1 10/04/17 19:18 120-82-1 M1

#=AR#

(704)875-9092
ANALYTICAL RESULTS


1,3,5-Trimethylbenzene ND ug/kg 26.8 1 10/04/17 19:18 108-67-8 M1
Vinyl acetate ND ug/kg 268 1 10/04/17 19:18 108-05-4 M1
m&p-Xylene ND ug/kg 53.7 1 10/04/17 19:18 179601-23-1
o-Xylene ND ug/kg 26.8 1 10/04/17 19:18 95-47-6
Surrogates
Toluene-d8 (S) 88 % 70-130 1 10/04/17 19:18 2037-26-5 1g
Diesel Range Organics(C10-C28) ND mg/kg 14.5 1 10/03/17 12:53 10/04/17 10:19

Surrogates
n-Pentacosane (S) 84 % 41-119 1 10/03/17 12:53 10/04/17 10:19 629-99-2
Aldrin ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 309-00-2

alpha-BHC ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 319-84-6
beta-BHC ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 319-85-7
delta-BHC ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 319-86-8
Chlordane (Technical) ND ug/kg 201 10 10/05/17 14:59 10/06/17 11:27 57-74-9
4,4'-DDD ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 72-54-8
4,4'-DDE ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 72-55-9
4,4'-DDT ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 50-29-3
Dieldrin ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 60-57-1
Endrin ND ug/kg 57.5 10 10/05/17 14:59 10/06/17 11:27 72-20-8

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Methoxychlor ND ug/kg 144 10 10/05/17 14:59 10/06/17 11:27 72-43-5
Mirex ND ug/kg 144 10 10/05/17 14:59 10/06/17 11:27 2385-85-5
Toxaphene ND ug/kg 201 10 10/05/17 14:59 10/06/17 11:27 8001-35-2
Surrogates
Surrogates
Surrogates
Arsenic ND mg/kg 1.8 1 09/30/17 19:10 10/03/17 18:42 7440-38-2

Barium 7.8 mg/kg 0.89 1 09/30/17 19:10 10/03/17 15:09 7440-39-3
Cadmium ND mg/kg 0.18 1 09/30/17 19:10 10/03/17 15:09 7440-43-9
Chromium 12.7 mg/kg 0.89 1 09/30/17 19:10 10/03/17 15:09 7440-47-3
Lead 9.1 mg/kg 0.89 1 09/30/17 19:10 10/03/17 15:09 7439-92-1
Selenium ND mg/kg 1.8 1 09/30/17 19:10 10/03/17 15:09 7782-49-2
Silver ND mg/kg 0.89 1 09/30/17 19:10 10/03/17 15:09 7440-22-4
Mercury 0.014 mg/kg 0.0062 1 10/05/17 12:30 10/06/17 01:13 7439-97-6

Aniline ND ug/kg 943 1 10/06/17 09:06 10/06/17 14:02 62-53-3

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Chrysene ND ug/kg 943 1 10/06/17 09:06 10/06/17 14:02 218-01-9
Fluorene ND ug/kg 943 1 10/06/17 09:06 10/06/17 14:02 86-73-7

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Phenol ND ug/kg 943 1 10/06/17 09:06 10/06/17 14:02 108-95-2
Pyrene ND ug/kg 943 1 10/06/17 09:06 10/06/17 14:02 129-00-0 L2
Surrogates
Nitrobenzene-d5 (S) 57 % 23-110 1 10/06/17 09:06 10/06/17 14:02 4165-60-0
2-Fluorobiphenyl (S) 42 % 30-110 1 10/06/17 09:06 10/06/17 14:02 321-60-8
Terphenyl-d14 (S) 25 % 28-110 1 10/06/17 09:06 10/06/17 14:02 1718-51-0 S2
Phenol-d6 (S) 60 % 22-110 1 10/06/17 09:06 10/06/17 14:02 13127-88-3
2-Fluorophenol (S) 58 % 13-110 1 10/06/17 09:06 10/06/17 14:02 367-12-4
Acetone ND ug/kg 309 1 10/04/17 19:38 67-64-1

Benzene ND ug/kg 15.5 1 10/04/17 19:38 71-43-2

#=AR#

(704)875-9092
ANALYTICAL RESULTS


2-Hexanone ND ug/kg 155 1 10/04/17 19:38 591-78-6
Styrene ND ug/kg 15.5 1 10/04/17 19:38 100-42-5
Toluene ND ug/kg 15.5 1 10/04/17 19:38 108-88-3
Vinyl acetate ND ug/kg 155 1 10/04/17 19:38 108-05-4

#=AR#

(704)875-9092
ANALYTICAL RESULTS

m&p-Xylene ND ug/kg 30.9 1 10/04/17 19:38 179601-23-1

o-Xylene ND ug/kg 15.5 1 10/04/17 19:38 95-47-6
Surrogates
Toluene-d8 (S) 89 % 70-130 1 10/04/17 19:38 2037-26-5 1g
Sample: SP-1 Lab ID: 92357321004 Collected: 09/29/17 11:00 Received: 09/30/17 10:35 Matrix: Solid
Surrogates
n-Pentacosane (S) 35 % 41-119 1 10/04/17 22:05 10/05/17 14:08 629-99-2 S2
Aldrin ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 309-00-2

alpha-BHC ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 319-84-6
beta-BHC ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 319-85-7
delta-BHC ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 319-86-8
4,4'-DDD ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 72-54-8
4,4'-DDE ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 72-55-9
4,4'-DDT ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 50-29-3
Dieldrin ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 60-57-1
Endrin ND ug/kg 23.4 10 10/03/17 21:58 10/05/17 22:29 72-20-8
Mirex ND ug/kg 58.4 10 10/03/17 21:58 10/05/17 22:29 2385-85-5

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Surrogates
PCB-1016 (Aroclor 1016) ND ug/kg 38.6 1 10/03/17 21:58 10/04/17 14:37 12674-11-2 M1
Surrogates
Surrogates
Arsenic ND mg/kg 1.1 1 09/30/17 19:10 10/03/17 18:46 7440-38-2

Barium 5.9 mg/kg 0.53 1 09/30/17 19:10 10/03/17 15:12 7440-39-3
Cadmium ND mg/kg 0.11 1 09/30/17 19:10 10/03/17 15:12 7440-43-9
Chromium 8.0 mg/kg 0.53 1 09/30/17 19:10 10/03/17 15:12 7440-47-3
Lead 2.9 mg/kg 0.53 1 09/30/17 19:10 10/03/17 15:12 7439-92-1
Selenium ND mg/kg 1.1 1 09/30/17 19:10 10/03/17 15:12 7782-49-2
Silver ND mg/kg 0.53 1 09/30/17 19:10 10/03/17 15:12 7440-22-4
Mercury 0.0057 mg/kg 0.0025 1 10/05/17 12:30 10/06/17 01:15 7439-97-6

Aniline ND ug/kg 389 1 10/03/17 15:52 10/05/17 16:10 62-53-3

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Chrysene ND ug/kg 389 1 10/03/17 15:52 10/05/17 16:10 218-01-9
Fluorene ND ug/kg 389 1 10/03/17 15:52 10/05/17 16:10 86-73-7

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Phenol ND ug/kg 389 1 10/03/17 15:52 10/05/17 16:10 108-95-2
Pyrene ND ug/kg 389 1 10/03/17 15:52 10/05/17 16:10 129-00-0
Surrogates
Nitrobenzene-d5 (S) 41 % 23-110 1 10/03/17 15:52 10/05/17 16:10 4165-60-0
Terphenyl-d14 (S) 58 % 28-110 1 10/03/17 15:52 10/05/17 16:10 1718-51-0
Phenol-d6 (S) 42 % 22-110 1 10/03/17 15:52 10/05/17 16:10 13127-88-3
2-Fluorophenol (S) 36 % 13-110 1 10/03/17 15:52 10/05/17 16:10 367-12-4
Acetone ND ug/kg 149 1 10/03/17 19:59 67-64-1

Benzene ND ug/kg 7.5 1 10/03/17 19:59 71-43-2

#=AR#

(704)875-9092
ANALYTICAL RESULTS


2-Hexanone ND ug/kg 74.7 1 10/03/17 19:59 591-78-6
4-Methyl-2-pentanone (MIBK) ND ug/kg 74.7 1 10/03/17 19:59 108-10-1
Styrene ND ug/kg 7.5 1 10/03/17 19:59 100-42-5
Toluene ND ug/kg 7.5 1 10/03/17 19:59 108-88-3
Vinyl acetate ND ug/kg 74.7 1 10/03/17 19:59 108-05-4 L2
m&p-Xylene ND ug/kg 14.9 1 10/03/17 19:59 179601-23-1
o-Xylene ND ug/kg 7.5 1 10/03/17 19:59 95-47-6
Surrogates
Toluene-d8 (S) 95 % 70-130 1 10/03/17 19:59 2037-26-5 1g

#=AR#

(704)875-9092
ANALYTICAL RESULTS

Surrogates
n-Pentacosane (S) 65 % 41-119 1 10/03/17 12:53 10/04/17 10:42 629-99-2
Aldrin ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 309-00-2

alpha-BHC ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 319-84-6
beta-BHC ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 319-85-7
delta-BHC ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 319-86-8
4,4'-DDD ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 72-54-8
4,4'-DDE ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 72-55-9
4,4'-DDT ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 50-29-3
Dieldrin ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 60-57-1
Endrin ND ug/kg 23.1 10 10/03/17 21:58 10/05/17 22:47 72-20-8
Mirex ND ug/kg 57.9 10 10/03/17 21:58 10/05/17 22:47 2385-85-5
Surrogates

#=AR#

(704)875-9092
ANALYTICAL RESULTS

Surrogates
Surrogates
Arsenic ND mg/kg 0.90 1 09/30/17 19:10 10/03/17 18:50 7440-38-2

Barium 3.8 mg/kg 0.45 1 09/30/17 19:10 10/03/17 15:16 7440-39-3
Cadmium ND mg/kg 0.090 1 09/30/17 19:10 10/03/17 15:16 7440-43-9
Chromium 6.5 mg/kg 0.45 1 09/30/17 19:10 10/03/17 15:16 7440-47-3
Lead 2.8 mg/kg 0.45 1 09/30/17 19:10 10/03/17 15:16 7439-92-1
Selenium ND mg/kg 0.90 1 09/30/17 19:10 10/03/17 15:16 7782-49-2
Silver ND mg/kg 0.45 1 09/30/17 19:10 10/03/17 15:16 7440-22-4
Mercury 0.0028 mg/kg 0.0027 1 10/05/17 12:30 10/06/17 01:17 7439-97-6

Aniline ND ug/kg 3830 10 10/03/17 15:52 10/05/17 16:39 62-53-3

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Chrysene ND ug/kg 3830 10 10/03/17 15:52 10/05/17 16:39 218-01-9
Fluorene ND ug/kg 3830 10 10/03/17 15:52 10/05/17 16:39 86-73-7
Phenol ND ug/kg 3830 10 10/03/17 15:52 10/05/17 16:39 108-95-2
Pyrene ND ug/kg 3830 10 10/03/17 15:52 10/05/17 16:39 129-00-0

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Surrogates
Nitrobenzene-d5 (S) 0 % 23-110 10 10/03/17 15:52 10/05/17 16:39 4165-60-0 D3,S4
Terphenyl-d14 (S) 0 % 28-110 10 10/03/17 15:52 10/05/17 16:39 1718-51-0 S4
Phenol-d6 (S) 0 % 22-110 10 10/03/17 15:52 10/05/17 16:39 13127-88-3 S4
2-Fluorophenol (S) 0 % 13-110 10 10/03/17 15:52 10/05/17 16:39 367-12-4 S4
2,4,6-Tribromophenol (S) 0 % 27-110 10 10/03/17 15:52 10/05/17 16:39 118-79-6 S4
Acetone ND ug/kg 127 1 10/03/17 18:40 67-64-1

Benzene ND ug/kg 6.4 1 10/03/17 18:40 71-43-2

#=AR#

(704)875-9092
ANALYTICAL RESULTS


2-Hexanone ND ug/kg 63.7 1 10/03/17 18:40 591-78-6
Styrene ND ug/kg 6.4 1 10/03/17 18:40 100-42-5
Toluene ND ug/kg 6.4 1 10/03/17 18:40 108-88-3
Vinyl acetate ND ug/kg 63.7 1 10/03/17 18:40 108-05-4 L2
m&p-Xylene ND ug/kg 12.7 1 10/03/17 18:40 179601-23-1
o-Xylene ND ug/kg 6.4 1 10/03/17 18:40 95-47-6
Surrogates
Toluene-d8 (S) 91 % 70-130 1 10/03/17 18:40 2037-26-5 1g

#=AR#

(704)875-9092
ANALYTICAL RESULTS

Surrogates
n-Pentacosane (S) 32 % 41-119 1 10/04/17 22:05 10/05/17 14:08 629-99-2 S2
Aldrin ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 309-00-2

alpha-BHC ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 319-84-6
beta-BHC ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 319-85-7
delta-BHC ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 319-86-8
4,4'-DDD ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 72-54-8
4,4'-DDE ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 72-55-9
4,4'-DDT ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 50-29-3
Dieldrin ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 60-57-1
Endrin ND ug/kg 10.7 5 10/03/17 21:58 10/05/17 23:23 72-20-8
Mirex ND ug/kg 26.8 5 10/03/17 21:58 10/05/17 23:23 2385-85-5
Surrogates
Surrogates
Surrogates

#=AR#

(704)875-9092
ANALYTICAL RESULTS

Arsenic 0.79 mg/kg 0.72 1 09/30/17 19:10 10/03/17 19:09 7440-38-2

Barium 7.8 mg/kg 0.36 1 09/30/17 19:10 10/03/17 15:19 7440-39-3
Cadmium ND mg/kg 0.072 1 09/30/17 19:10 10/03/17 15:19 7440-43-9
Chromium 7.1 mg/kg 0.36 1 09/30/17 19:10 10/03/17 15:19 7440-47-3
Lead 2.6 mg/kg 0.36 1 09/30/17 19:10 10/03/17 15:19 7439-92-1
Selenium ND mg/kg 0.72 1 09/30/17 19:10 10/03/17 15:19 7782-49-2
Silver ND mg/kg 0.36 1 09/30/17 19:10 10/03/17 15:19 7440-22-4
Mercury ND mg/kg 0.0045 1 10/05/17 19:05 10/05/17 23:23 7439-97-6 M1

Aniline ND ug/kg 340 1 10/03/17 15:52 10/05/17 17:08 62-53-3
Chrysene ND ug/kg 340 1 10/03/17 15:52 10/05/17 17:08 218-01-9

#=AR#

(704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/kg 340 1 10/03/17 15:52 10/05/17 17:08 86-73-7
Phenol ND ug/kg 340 1 10/03/17 15:52 10/05/17 17:08 108-95-2
Pyrene ND ug/kg 340 1 10/03/17 15:52 10/05/17 17:08 129-00-0
Surrogates
Nitrobenzene-d5 (S) 27 % 23-110 1 10/03/17 15:52 10/05/17 17:08 4165-60-0
Terphenyl-d14 (S) 46 % 28-110 1 10/03/17 15:52 10/05/17 17:08 1718-51-0
Phenol-d6 (S) 37 % 22-110 1 10/03/17 15:52 10/05/17 17:08 13127-88-3
2-Fluorophenol (S) 24 % 13-110 1 10/03/17 15:52 10/05/17 17:08 367-12-4
Acetone ND ug/kg 105 1 10/04/17 19:58 67-64-1

Benzene ND ug/kg 5.3 1 10/04/17 19:58 71-43-2

#=AR#

(704)875-9092
ANALYTICAL RESULTS


2-Hexanone ND ug/kg 52.6 1 10/04/17 19:58 591-78-6

#=AR#

(704)875-9092
ANALYTICAL RESULTS

Styrene ND ug/kg 5.3 1 10/04/17 19:58 100-42-5

Toluene ND ug/kg 5.3 1 10/04/17 19:58 108-88-3
Vinyl acetate ND ug/kg 52.6 1 10/04/17 19:58 108-05-4
m&p-Xylene ND ug/kg 10.5 1 10/04/17 19:58 179601-23-1
o-Xylene ND ug/kg 5.3 1 10/04/17 19:58 95-47-6
Surrogates
Toluene-d8 (S) 93 % 70-130 1 10/04/17 19:58 2037-26-5 1g

#=QC#

(704)875-9092
QUALITY CONTROL DATA

QC Batch: 380604 Analysis Method: EPA 8015 Modified

QC Batch Method: EPA 5035A/5030B Analysis Description: Gasoline Range Organics
Associated Lab Samples: 92357321001, 92357321002, 92357321003, 92357321004, 92357321005, 92357321006
METHOD BLANK: 2109167 Matrix: Solid

Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Gas Range Organics (C6-C10) mg/kg ND 6.0 10/03/17 17:44
4-Bromofluorobenzene (S) % 92 70-167 10/03/17 17:44
LABORATORY CONTROL SAMPLE: 2109168

Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Gas Range Organics (C6-C10) mg/kg 50 45.9 92 70-165
4-Bromofluorobenzene (S) % 95 70-167
MATRIX SPIKE SAMPLE: 2112426

92357396001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Gas Range Organics (C6-C10) mg/kg ND 57.6 52.5 90 47-187
SAMPLE DUPLICATE: 2109170

92357321002 Dup
Parameter Units Result Result RPD Qualifiers
Gas Range Organics (C6-C10) mg/kg ND ND
4-Bromofluorobenzene (S) % 93 97 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

#=QC#

(704)875-9092

QC Batch: 380651 Analysis Method: EPA 7471

QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92357321001, 92357321002, 92357321003, 92357321004, 92357321005

Blank Reporting
Mercury mg/kg ND 0.0060 10/05/17 23:32

Spike LCS LCS % Rec
Mercury mg/kg .083 0.089 106 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2109445 2109446

MS MSD
92356587001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.035 .056 .052 0.094 0.078 105 84 75-125 18

#=QC#

(704)875-9092


QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92357321006

Blank Reporting
Mercury mg/kg ND 0.0060 10/05/17 22:59

Spike LCS LCS % Rec
Mercury mg/kg .083 0.067 80 80-120

MS MSD
Mercury mg/kg ND .055 .059 0.036 0.035 58 53 75-125 1 M1

#=QC#

(704)875-9092


QC Batch Method: EPA 3050 Analysis Description: 6010 MET

Blank Reporting
Arsenic mg/kg ND 1.0 10/03/17 18:16
Barium mg/kg ND 0.50 10/03/17 14:37
Cadmium mg/kg ND 0.10 10/03/17 14:37
Chromium mg/kg ND 0.50 10/03/17 14:37
Lead mg/kg ND 0.50 10/03/17 14:37
Selenium mg/kg ND 1.0 10/03/17 14:37
Silver mg/kg ND 0.50 10/03/17 14:37

Spike LCS LCS % Rec
Arsenic mg/kg 50 47.8 96 80-120
Barium mg/kg 50 51.4 103 80-120
Cadmium mg/kg 50 48.8 98 80-120
Chromium mg/kg 50 49.1 98 80-120
Lead mg/kg 50 50.2 100 80-120
Selenium mg/kg 50 50.7 101 80-120
Silver mg/kg 25 24.6 98 80-120

MS MSD
Arsenic mg/kg 2.1 71.7 75.8 70.5 75.5 95 97 75-125 7
Barium mg/kg 7.1 71.7 75.8 78.5 82.0 99 99 75-125 4
Cadmium mg/kg ND 71.7 75.8 65.2 69.2 91 91 75-125 6
Chromium mg/kg 9.0 71.7 75.8 77.0 81.6 95 96 75-125 6
Lead mg/kg 16.8 71.7 75.8 88.2 91.6 99 99 75-125 4
Selenium mg/kg ND 71.7 75.8 74.1 77.8 102 101 75-125 5
Silver mg/kg ND 36 37.9 34.0 36.1 95 95 75-125 6

#=QC#

(704)875-9092


QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92357321004, 92357321005

Blank Reporting
1,1,1,2-Tetrachloroethane ug/kg ND 5.2 10/03/17 16:02
1,1,1-Trichloroethane ug/kg ND 5.2 10/03/17 16:02
1,1-Dichloroethane ug/kg ND 5.2 10/03/17 16:02
1,1-Dichloroethene ug/kg ND 5.2 10/03/17 16:02
1,1-Dichloropropene ug/kg ND 5.2 10/03/17 16:02
1,2,3-Trichlorobenzene ug/kg ND 5.2 10/03/17 16:02
1,2,3-Trichloropropane ug/kg ND 5.2 10/03/17 16:02
1,2,4-Trimethylbenzene ug/kg ND 5.2 10/03/17 16:02
1,2-Dibromo-3-chloropropane ug/kg ND 5.2 10/03/17 16:02
1,2-Dibromoethane (EDB) ug/kg ND 5.2 10/03/17 16:02
1,2-Dichlorobenzene ug/kg ND 5.2 10/03/17 16:02
1,2-Dichloropropane ug/kg ND 5.2 10/03/17 16:02
2-Butanone (MEK) ug/kg ND 104 10/03/17 16:02
2-Chlorotoluene ug/kg ND 5.2 10/03/17 16:02
2-Hexanone ug/kg ND 52.2 10/03/17 16:02
4-Methyl-2-pentanone (MIBK) ug/kg ND 52.2 10/03/17 16:02
Acetone ug/kg ND 104 10/03/17 16:02
Benzene ug/kg ND 5.2 10/03/17 16:02
Bromobenzene ug/kg ND 5.2 10/03/17 16:02
Bromochloromethane ug/kg ND 5.2 10/03/17 16:02
Bromodichloromethane ug/kg ND 5.2 10/03/17 16:02
Bromoform ug/kg ND 5.2 10/03/17 16:02
Bromomethane ug/kg ND 10.4 10/03/17 16:02
Carbon tetrachloride ug/kg ND 5.2 10/03/17 16:02
Chlorobenzene ug/kg ND 5.2 10/03/17 16:02
Chloroethane ug/kg ND 10.4 10/03/17 16:02
Chloroform ug/kg ND 5.2 10/03/17 16:02
Chloromethane ug/kg ND 10.4 10/03/17 16:02
cis-1,2-Dichloroethene ug/kg ND 5.2 10/03/17 16:02
cis-1,3-Dichloropropene ug/kg ND 5.2 10/03/17 16:02
Dibromochloromethane ug/kg ND 5.2 10/03/17 16:02

#=QC#

(704)875-9092


Blank Reporting
Dibromomethane ug/kg ND 5.2 10/03/17 16:02
Dichlorodifluoromethane ug/kg ND 10.4 10/03/17 16:02
Diisopropyl ether ug/kg ND 5.2 10/03/17 16:02
Ethylbenzene ug/kg ND 5.2 10/03/17 16:02
Hexachloro-1,3-butadiene ug/kg ND 5.2 10/03/17 16:02
Isopropylbenzene (Cumene) ug/kg ND 5.2 10/03/17 16:02
m&p-Xylene ug/kg ND 10.4 10/03/17 16:02
Methyl-tert-butyl ether ug/kg ND 5.2 10/03/17 16:02
Methylene Chloride ug/kg ND 20.9 10/03/17 16:02
n-Butylbenzene ug/kg ND 5.2 10/03/17 16:02
n-Propylbenzene ug/kg ND 5.2 10/03/17 16:02
Naphthalene ug/kg ND 5.2 10/03/17 16:02
o-Xylene ug/kg ND 5.2 10/03/17 16:02
p-Isopropyltoluene ug/kg ND 5.2 10/03/17 16:02
sec-Butylbenzene ug/kg ND 5.2 10/03/17 16:02
Styrene ug/kg ND 5.2 10/03/17 16:02
tert-Butylbenzene ug/kg ND 5.2 10/03/17 16:02
Tetrachloroethene ug/kg ND 5.2 10/03/17 16:02
Toluene ug/kg ND 5.2 10/03/17 16:02
trans-1,2-Dichloroethene ug/kg ND 5.2 10/03/17 16:02
trans-1,3-Dichloropropene ug/kg ND 5.2 10/03/17 16:02
Trichloroethene ug/kg ND 5.2 10/03/17 16:02
Trichlorofluoromethane ug/kg ND 5.2 10/03/17 16:02
Vinyl acetate ug/kg ND 52.2 10/03/17 16:02
Vinyl chloride ug/kg ND 10.4 10/03/17 16:02
Xylene (Total) ug/kg ND 10.4 10/03/17 16:02
1,2-Dichloroethane-d4 (S) % 109 70-132 10/03/17 16:02
Toluene-d8 (S) % 99 70-130 10/03/17 16:02

Spike LCS LCS % Rec
1,1,1,2-Tetrachloroethane ug/kg 53.3 55.7 104 74-137
1,1,1-Trichloroethane ug/kg 53.3 57.9 109 67-140
1,1,2,2-Tetrachloroethane ug/kg 53.3 52.8 99 72-141
1,1,2-Trichloroethane ug/kg 53.3 58.1 109 78-138
1,1-Dichloroethane ug/kg 53.3 60.0 113 69-134
1,1-Dichloroethene ug/kg 53.3 58.5 110 67-138
1,1-Dichloropropene ug/kg 53.3 58.7 110 69-139
1,2,3-Trichlorobenzene ug/kg 53.3 57.1 107 70-146
1,2,3-Trichloropropane ug/kg 53.3 59.9 112 69-144
1,2,4-Trichlorobenzene ug/kg 53.3 57.4 108 68-148
1,2,4-Trimethylbenzene ug/kg 53.3 56.2 105 74-137

#=QC#

(704)875-9092


Spike LCS LCS % Rec
1,2-Dibromo-3-chloropropane ug/kg 53.3 56.8 107 65-140
1,2-Dibromoethane (EDB) ug/kg 53.3 59.5 112 77-135
1,2-Dichlorobenzene ug/kg 53.3 55.8 105 77-141
1,2-Dichloroethane ug/kg 53.3 59.0 111 65-137
1,2-Dichloropropane ug/kg 53.3 56.5 106 72-136
1,3,5-Trimethylbenzene ug/kg 53.3 56.0 105 76-133
2-Butanone (MEK) ug/kg 107 124 116 58-147
2-Chlorotoluene ug/kg 53.3 55.9 105 73-139
2-Hexanone ug/kg 107 127 119 62-145
4-Chlorotoluene ug/kg 53.3 56.3 106 76-141
4-Methyl-2-pentanone (MIBK) ug/kg 107 128 120 64-149
Acetone ug/kg 107 139 130 53-153
Benzene ug/kg 53.3 57.2 107 73-135
Bromobenzene ug/kg 53.3 57.3 108 75-133
Bromochloromethane ug/kg 53.3 59.8 112 73-134
Bromodichloromethane ug/kg 53.3 56.6 106 71-135
Bromoform ug/kg 53.3 58.5 110 66-141
Bromomethane ug/kg 53.3 58.6 110 53-160
Carbon tetrachloride ug/kg 53.3 55.6 104 60-145
Chlorobenzene ug/kg 53.3 56.6 106 78-130
Chloroethane ug/kg 53.3 56.8 106 64-149
Chloroform ug/kg 53.3 55.2 104 70-134
Chloromethane ug/kg 53.3 60.0 113 52-150
cis-1,2-Dichloroethene ug/kg 53.3 58.5 110 70-133
cis-1,3-Dichloropropene ug/kg 53.3 58.6 110 68-134
Dibromochloromethane ug/kg 53.3 58.5 110 71-138
Dibromomethane ug/kg 53.3 57.7 108 74-130
Dichlorodifluoromethane ug/kg 53.3 48.9 92 40-160
Diisopropyl ether ug/kg 53.3 59.2 111 69-141
Ethylbenzene ug/kg 53.3 57.6 108 75-133
Hexachloro-1,3-butadiene ug/kg 53.3 53.4 100 68-143
Isopropylbenzene (Cumene) ug/kg 53.3 56.9 107 76-143
m&p-Xylene ug/kg 107 115 108 75-136
Methyl-tert-butyl ether ug/kg 53.3 60.2 113 68-144
Methylene Chloride ug/kg 53.3 51.8 97 45-154
n-Butylbenzene ug/kg 53.3 55.5 104 72-137
n-Propylbenzene ug/kg 53.3 55.4 104 76-136
Naphthalene ug/kg 53.3 64.0 120 68-151
o-Xylene ug/kg 53.3 58.0 109 76-141
p-Isopropyltoluene ug/kg 53.3 56.5 106 76-140
sec-Butylbenzene ug/kg 53.3 55.4 104 79-139
Styrene ug/kg 53.3 59.0 111 79-137
tert-Butylbenzene ug/kg 53.3 49.5 93 74-143

#=QC#

(704)875-9092


Spike LCS LCS % Rec
Tetrachloroethene ug/kg 53.3 51.0 96 71-138
Toluene ug/kg 53.3 58.2 109 74-131
trans-1,2-Dichloroethene ug/kg 53.3 60.3 113 67-135
trans-1,3-Dichloropropene ug/kg 53.3 59.3 111 65-146
Trichloroethene ug/kg 53.3 60.4 113 67-135
Trichlorofluoromethane ug/kg 53.3 59.1 111 59-144
Vinyl acetate ug/kg 107 24.4J 23 40-160 L2
Vinyl chloride ug/kg 53.3 57.3 107 56-141
Xylene (Total) ug/kg 160 173 108 76-137
1,2-Dichloroethane-d4 (S) % 107 70-132
Toluene-d8 (S) % 100 70-130

1,1,1,2-Tetrachloroethane ug/kg 2.2U 23.3 21.1 91 70-130
1,1,1-Trichloroethane ug/kg 1.9U 23.3 19.9 86 70-130
1,1,2,2-Tetrachloroethane ug/kg 2.0U 23.3 21.8 94 70-130
1,1,2-Trichloroethane ug/kg 2.2U 23.3 21.0 90 70-130
1,1-Dichloroethane ug/kg 1.6U 23.3 20.9 90 70-130
1,1-Dichloroethene ug/kg 1.9U 23.3 18.9 81 49-180
1,1-Dichloropropene ug/kg 1.6U 23.3 20.3 87 70-130
1,2,3-Trichlorobenzene ug/kg 2.4U 23.3 19.1 82 70-130
1,2,3-Trichloropropane ug/kg 1.7U 23.3 22.2 95 70-130
1,2,4-Trichlorobenzene ug/kg 1.7U 23.3 20.5 88 70-130
1,2,4-Trimethylbenzene ug/kg 2.1U 23.3 21.6 93 70-130
1,2-Dibromo-3-chloropropane ug/kg 3.8U 23.3 21.9 94 70-130
1,2-Dibromoethane (EDB) ug/kg 1.9U 23.3 22.1 95 70-130
1,2-Dichlorobenzene ug/kg 2.0U 23.3 21.5 92 70-130
1,2-Dichloroethane ug/kg 2.4U 23.3 19.4 83 70-130
1,2-Dichloropropane ug/kg 1.8U 23.3 21.2 91 70-130
1,3,5-Trimethylbenzene ug/kg 1.9U 23.3 22.8 98 70-130
2-Butanone (MEK) ug/kg 3.1U 46.5 41.5J 89 70-130
2-Chlorotoluene ug/kg 1.8U 23.3 22.0 95 70-130
2-Hexanone ug/kg 4.2U 46.5 44.1J 95 70-130
4-Chlorotoluene ug/kg 1.9U 23.3 21.8 94 70-130
4-Methyl-2-pentanone (MIBK) ug/kg 4.0U 46.5 43.8J 94 70-130
Acetone ug/kg 63.2J 46.5 49.5J -29 70-130 M1
Benzene ug/kg 0.0017U mg/kg 23.3 21.2 91 50-166
Bromobenzene ug/kg 2.1U 23.3 22.4 96 70-130

#=QC#

(704)875-9092


Bromochloromethane ug/kg 1.8U 23.3 21.8 94 70-130
Bromodichloromethane ug/kg 2.0U 23.3 19.7 85 70-130
Bromoform ug/kg 2.5U 23.3 20.9 90 70-130
Bromomethane ug/kg 2.7U 23.3 17.0 73 70-130
Carbon tetrachloride ug/kg 2.8U 23.3 19.9 85 70-130
Chlorobenzene ug/kg 2.0U 23.3 22.0 95 43-169
Chloroethane ug/kg 2.6U 23.3 18.5 79 70-130
Chloroform ug/kg 1.7U 23.3 21.6 93 70-130
Chloromethane ug/kg 2.6U 23.3 16.4 71 70-130
cis-1,2-Dichloroethene ug/kg 1.5U 23.3 21.9 94 70-130
cis-1,3-Dichloropropene ug/kg 1.9U 23.3 20.5 88 70-130
Dibromochloromethane ug/kg 1.9U 23.3 21.1 91 70-130
Dibromomethane ug/kg 2.7U 23.3 21.7 93 70-130
Dichlorodifluoromethane ug/kg 3.8U 23.3 9.3J 40 70-130 M1
Diisopropyl ether ug/kg 1.8U 23.3 20.3 87 70-130
Ethylbenzene ug/kg 0.0019U mg/kg 23.3 22.8 98 70-130
Hexachloro-1,3-butadiene ug/kg 2.1U 23.3 19.3 83 70-130
Isopropylbenzene (Cumene) ug/kg 2.0U 23.3 22.3 96 70-130
m&p-Xylene ug/kg 0.0038U mg/kg 46.5 44.4 95 70-130
Methyl-tert-butyl ether ug/kg 0.0016U mg/kg 23.3 20.7 89 70-130
Methylene Chloride ug/kg 3.5J 23.3 18.5J 65 70-130 M1
n-Butylbenzene ug/kg 1.9U 23.3 19.3 83 70-130
n-Propylbenzene ug/kg 1.8U 23.3 21.7 93 70-130
Naphthalene ug/kg 1.3U 23.3 26.6 115 70-130
o-Xylene ug/kg 0.0020U mg/kg 23.3 22.5 97 70-130
p-Isopropyltoluene ug/kg 1.8U 23.3 21.0 90 70-130
sec-Butylbenzene ug/kg 1.7U 23.3 21.8 94 70-130
Styrene ug/kg 1.9U 23.3 22.5 97 70-130
tert-Butylbenzene ug/kg 2.1U 23.3 19.4 84 70-130
Tetrachloroethene ug/kg 1.8U 23.3 21.0 90 70-130
Toluene ug/kg 0.0019U mg/kg 23.3 21.5 93 52-163
trans-1,2-Dichloroethene ug/kg 2.0U 23.3 20.0 86 70-130
trans-1,3-Dichloropropene ug/kg 1.6U 23.3 19.6 84 70-130
Trichloroethene ug/kg 2.2U 23.3 21.2 91 49-167
Trichlorofluoromethane ug/kg 2.4U 23.3 19.0 82 70-130
Vinyl acetate ug/kg 9.4U 46.5 ND 16 70-130 M0
Vinyl chloride ug/kg 1.9U 23.3 16.8 72 70-130
Toluene-d8 (S) % 98 70-130

92357386005 Dup
1,1,1,2-Tetrachloroethane ug/kg ND ND

#=QC#

(704)875-9092


92357386005 Dup
1,1,1-Trichloroethane ug/kg ND ND
1,1-Dichloroethane ug/kg ND ND
1,1-Dichloroethene ug/kg ND ND
1,1-Dichloropropene ug/kg ND ND
1,2,3-Trichlorobenzene ug/kg ND ND
1,2,3-Trichloropropane ug/kg ND ND
1,2,4-Trimethylbenzene ug/kg 102 88.0 15
1,2-Dibromo-3-chloropropane ug/kg ND ND
1,2-Dibromoethane (EDB) ug/kg ND ND
1,2-Dichlorobenzene ug/kg ND ND
1,2-Dichloropropane ug/kg ND ND
1,3,5-Trimethylbenzene ug/kg 63.8 57.4 11
2-Butanone (MEK) ug/kg ND 6.4J
2-Chlorotoluene ug/kg ND ND
2-Hexanone ug/kg ND ND
4-Methyl-2-pentanone (MIBK) ug/kg ND ND
Acetone ug/kg ND 35.9J
Benzene ug/kg ND ND
Bromobenzene ug/kg ND ND
Bromochloromethane ug/kg ND ND
Bromodichloromethane ug/kg ND ND
Bromoform ug/kg ND ND
Bromomethane ug/kg ND ND
Carbon tetrachloride ug/kg ND ND
Chlorobenzene ug/kg ND ND
Chloroethane ug/kg ND ND
Chloroform ug/kg ND 1.6J
Chloromethane ug/kg ND ND
cis-1,2-Dichloroethene ug/kg ND 2J
cis-1,3-Dichloropropene ug/kg ND ND
Dibromochloromethane ug/kg ND ND
Dibromomethane ug/kg ND ND
Dichlorodifluoromethane ug/kg ND ND
Diisopropyl ether ug/kg ND ND
Ethylbenzene ug/kg ND 2.7J
Hexachloro-1,3-butadiene ug/kg ND ND
Isopropylbenzene (Cumene) ug/kg 8.4 8.2 3
m&p-Xylene ug/kg ND 3.5J

#=QC#

(704)875-9092


92357386005 Dup
Methyl-tert-butyl ether ug/kg ND ND
Methylene Chloride ug/kg ND ND
n-Butylbenzene ug/kg 15.5 12.5 21
n-Propylbenzene ug/kg 14.4 14.2 1
Naphthalene ug/kg 10.1 9.3 7
o-Xylene ug/kg 9.1 9.0 1
p-Isopropyltoluene ug/kg 60.9 33.3 59 D6
sec-Butylbenzene ug/kg 17.5 16.7 5
Styrene ug/kg ND ND
tert-Butylbenzene ug/kg 9.7 9.2 5
Tetrachloroethene ug/kg ND ND
Toluene ug/kg ND ND
trans-1,2-Dichloroethene ug/kg ND ND
trans-1,3-Dichloropropene ug/kg ND ND
Trichloroethene ug/kg ND ND
Trichlorofluoromethane ug/kg ND ND
Vinyl acetate ug/kg ND ND
Vinyl chloride ug/kg ND ND
Xylene (Total) ug/kg 9.1 9J
1,2-Dichloroethane-d4 (S) % 113 98 9
4-Bromofluorobenzene (S) % 187 196 11 S2
Toluene-d8 (S) % 102 99 3

#=QC#

(704)875-9092


QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92357321001, 92357321002, 92357321003, 92357321006

Blank Reporting
1,1-Dichloroethene ug/kg ND 5.4 10/04/17 11:43
1,1-Dichloropropene ug/kg ND 5.4 10/04/17 11:43
1,2,3-Trichloropropane ug/kg ND 5.4 10/04/17 11:43
1,2-Dibromo-3-chloropropane ug/kg ND 5.4 10/04/17 11:43
1,2-Dibromoethane (EDB) ug/kg ND 5.4 10/04/17 11:43
2-Butanone (MEK) ug/kg ND 108 10/04/17 11:43
2-Hexanone ug/kg ND 53.8 10/04/17 11:43
4-Methyl-2-pentanone (MIBK) ug/kg ND 53.8 10/04/17 11:43
Acetone ug/kg ND 108 10/04/17 11:43
Benzene ug/kg ND 5.4 10/04/17 11:43
Bromobenzene ug/kg ND 5.4 10/04/17 11:43
Bromochloromethane ug/kg ND 5.4 10/04/17 11:43
Bromodichloromethane ug/kg ND 5.4 10/04/17 11:43
Bromoform ug/kg ND 5.4 10/04/17 11:43
Bromomethane ug/kg ND 10.8 10/04/17 11:43
Carbon tetrachloride ug/kg ND 5.4 10/04/17 11:43
Chlorobenzene ug/kg ND 5.4 10/04/17 11:43
Chloroethane ug/kg ND 10.8 10/04/17 11:43
Chloroform ug/kg ND 5.4 10/04/17 11:43
Chloromethane ug/kg ND 10.8 10/04/17 11:43
cis-1,2-Dichloroethene ug/kg ND 5.4 10/04/17 11:43
cis-1,3-Dichloropropene ug/kg ND 5.4 10/04/17 11:43
Dibromochloromethane ug/kg ND 5.4 10/04/17 11:43

#=QC#

(704)875-9092


Blank Reporting
Dibromomethane ug/kg ND 5.4 10/04/17 11:43
Dichlorodifluoromethane ug/kg ND 10.8 10/04/17 11:43
Diisopropyl ether ug/kg ND 5.4 10/04/17 11:43
Ethylbenzene ug/kg ND 5.4 10/04/17 11:43
Hexachloro-1,3-butadiene ug/kg ND 5.4 10/04/17 11:43
Isopropylbenzene (Cumene) ug/kg ND 5.4 10/04/17 11:43
m&p-Xylene ug/kg ND 10.8 10/04/17 11:43
Methyl-tert-butyl ether ug/kg ND 5.4 10/04/17 11:43
Methylene Chloride ug/kg ND 21.5 10/04/17 11:43
n-Butylbenzene ug/kg ND 5.4 10/04/17 11:43
n-Propylbenzene ug/kg ND 5.4 10/04/17 11:43
Naphthalene ug/kg ND 5.4 10/04/17 11:43
o-Xylene ug/kg ND 5.4 10/04/17 11:43
p-Isopropyltoluene ug/kg ND 5.4 10/04/17 11:43
sec-Butylbenzene ug/kg ND 5.4 10/04/17 11:43
Styrene ug/kg ND 5.4 10/04/17 11:43
tert-Butylbenzene ug/kg ND 5.4 10/04/17 11:43
Tetrachloroethene ug/kg ND 5.4 10/04/17 11:43
Toluene ug/kg ND 5.4 10/04/17 11:43
trans-1,2-Dichloroethene ug/kg ND 5.4 10/04/17 11:43
trans-1,3-Dichloropropene ug/kg ND 5.4 10/04/17 11:43
Trichloroethene ug/kg ND 5.4 10/04/17 11:43
Trichlorofluoromethane ug/kg ND 5.4 10/04/17 11:43
Vinyl acetate ug/kg ND 53.8 10/04/17 11:43
Vinyl chloride ug/kg ND 10.8 10/04/17 11:43
Xylene (Total) ug/kg ND 10.8 10/04/17 11:43
1,2-Dichloroethane-d4 (S) % 96 70-132 10/04/17 11:43
Toluene-d8 (S) % 97 70-130 10/04/17 11:43

Spike LCS LCS % Rec
1,1,1,2-Tetrachloroethane ug/kg 53 52.7 100 74-137
1,1,1-Trichloroethane ug/kg 53 50.5 95 67-140
1,1,2,2-Tetrachloroethane ug/kg 53 50.5 95 72-141
1,1,2-Trichloroethane ug/kg 53 50.8 96 78-138
1,1-Dichloroethane ug/kg 53 51.3 97 69-134
1,1-Dichloroethene ug/kg 53 51.3 97 67-138
1,1-Dichloropropene ug/kg 53 51.6 97 69-139
1,2,3-Trichlorobenzene ug/kg 53 56.4 106 70-146
1,2,3-Trichloropropane ug/kg 53 52.3 99 69-144
1,2,4-Trichlorobenzene ug/kg 53 58.0 110 68-148
1,2,4-Trimethylbenzene ug/kg 53 56.0 106 74-137

#=QC#

(704)875-9092


Spike LCS LCS % Rec
1,2-Dibromo-3-chloropropane ug/kg 53 54.6 103 65-140
1,2-Dibromoethane (EDB) ug/kg 53 55.5 105 77-135
1,2-Dichlorobenzene ug/kg 53 53.8 102 77-141
1,2-Dichloroethane ug/kg 53 48.5 92 65-137
1,2-Dichloropropane ug/kg 53 51.6 97 72-136
1,3,5-Trimethylbenzene ug/kg 53 55.8 105 76-133
2-Butanone (MEK) ug/kg 106 101J 95 58-147
2-Chlorotoluene ug/kg 53 54.7 103 73-139
2-Hexanone ug/kg 106 111 104 62-145
4-Chlorotoluene ug/kg 53 55.6 105 76-141
4-Methyl-2-pentanone (MIBK) ug/kg 106 108 102 64-149
Acetone ug/kg 106 108 102 53-153
Benzene ug/kg 53 52.8 100 73-135
Bromobenzene ug/kg 53 55.9 105 75-133
Bromochloromethane ug/kg 53 54.0 102 73-134
Bromodichloromethane ug/kg 53 51.7 98 71-135
Bromoform ug/kg 53 54.1 102 66-141
Bromomethane ug/kg 53 51.4 97 53-160
Carbon tetrachloride ug/kg 53 52.5 99 60-145
Chlorobenzene ug/kg 53 54.9 104 78-130
Chloroethane ug/kg 53 48.9 92 64-149
Chloroform ug/kg 53 52.2 99 70-134
Chloromethane ug/kg 53 54.8 103 52-150
cis-1,2-Dichloroethene ug/kg 53 52.4 99 70-133
cis-1,3-Dichloropropene ug/kg 53 54.5 103 68-134
Dibromochloromethane ug/kg 53 54.8 103 71-138
Dibromomethane ug/kg 53 53.2 100 74-130
Dichlorodifluoromethane ug/kg 53 48.2 91 40-160
Diisopropyl ether ug/kg 53 50.5 95 69-141
Ethylbenzene ug/kg 53 56.2 106 75-133
Hexachloro-1,3-butadiene ug/kg 53 56.2 106 68-143
Isopropylbenzene (Cumene) ug/kg 53 55.1 104 76-143
m&p-Xylene ug/kg 106 111 105 75-136
Methyl-tert-butyl ether ug/kg 53 51.8 98 68-144
Methylene Chloride ug/kg 53 43.4 82 45-154
n-Butylbenzene ug/kg 53 56.4 106 72-137
n-Propylbenzene ug/kg 53 55.0 104 76-136
Naphthalene ug/kg 53 60.6 114 68-151
o-Xylene ug/kg 53 56.5 107 76-141
p-Isopropyltoluene ug/kg 53 56.5 107 76-140
sec-Butylbenzene ug/kg 53 54.9 104 79-139
Styrene ug/kg 53 56.7 107 79-137
tert-Butylbenzene ug/kg 53 48.8 92 74-143

#=QC#

(704)875-9092


Spike LCS LCS % Rec
Tetrachloroethene ug/kg 53 51.1 97 71-138
Toluene ug/kg 53 53.8 102 74-131
trans-1,2-Dichloroethene ug/kg 53 52.0 98 67-135
trans-1,3-Dichloropropene ug/kg 53 53.3 101 65-146
Trichloroethene ug/kg 53 55.9 106 67-135
Trichlorofluoromethane ug/kg 53 53.0 100 59-144
Vinyl acetate ug/kg 106 77.6 73 40-160
Vinyl chloride ug/kg 53 51.1 96 56-141
Xylene (Total) ug/kg 159 168 106 76-137
Toluene-d8 (S) % 99 70-130

1,1,1,2-Tetrachloroethane ug/kg ND 92.5 96.0 104 70-130
1,1,1-Trichloroethane ug/kg ND 92.5 98.6 107 70-130
1,1,2,2-Tetrachloroethane ug/kg ND 92.5 79.0 85 70-130
1,1,2-Trichloroethane ug/kg ND 92.5 76.8 83 70-130
1,1-Dichloroethane ug/kg ND 92.5 103 112 70-130
1,1-Dichloroethene ug/kg ND 92.5 106 114 49-180
1,1-Dichloropropene ug/kg ND 92.5 96.9 105 70-130
1,2,3-Trichlorobenzene ug/kg ND 92.5 22.8J 25 70-130 M1
1,2,3-Trichloropropane ug/kg ND 92.5 88.3 96 70-130
1,2,4-Trichlorobenzene ug/kg ND 92.5 28.4 31 70-130 M1
1,2,4-Trimethylbenzene ug/kg ND 92.5 115 124 70-130
1,2-Dibromo-3-chloropropane ug/kg ND 92.5 101 109 70-130
1,2-Dibromoethane (EDB) ug/kg ND 92.5 104 112 70-130
1,2-Dichlorobenzene ug/kg ND 92.5 69.9 76 70-130
1,2-Dichloroethane ug/kg ND 92.5 84.4 91 70-130
1,2-Dichloropropane ug/kg ND 92.5 90.3 98 70-130
1,3,5-Trimethylbenzene ug/kg ND 92.5 121 131 70-130 M1
1,3-Dichloropropane ug/kg ND 92.5 114 123 70-130
2,2-Dichloropropane ug/kg ND 92.5 103 112 70-130
2-Butanone (MEK) ug/kg ND 185 204J 95 70-130
2-Chlorotoluene ug/kg ND 92.5 120 130 70-130
2-Hexanone ug/kg ND 185 217J 117 70-130
4-Chlorotoluene ug/kg ND 92.5 112 121 70-130
4-Methyl-2-pentanone (MIBK) ug/kg ND 185 168J 91 70-130
Acetone ug/kg ND 185 335J 64 70-130 M1
Benzene ug/kg ND 92.5 98.4 106 50-166
Bromobenzene ug/kg ND 92.5 120 130 70-130

#=QC#

(704)875-9092


Bromochloromethane ug/kg ND 92.5 103 111 70-130
Bromodichloromethane ug/kg ND 92.5 77.6 84 70-130
Bromoform ug/kg ND 92.5 68.8 74 70-130
Bromomethane ug/kg ND 92.5 73.4 79 70-130
Carbon tetrachloride ug/kg ND 92.5 92.7 100 70-130
Chlorobenzene ug/kg ND 92.5 90.0 97 43-169
Chloroethane ug/kg ND 92.5 109 118 70-130
Chloroform ug/kg ND 92.5 99.2 107 70-130
Chloromethane ug/kg ND 92.5 113 123 70-130
cis-1,2-Dichloroethene ug/kg ND 92.5 97.4 105 70-130
cis-1,3-Dichloropropene ug/kg ND 92.5 40.4 44 70-130 M1
Dibromochloromethane ug/kg ND 92.5 88.5 96 70-130
Dibromomethane ug/kg ND 92.5 86.1 93 70-130
Dichlorodifluoromethane ug/kg ND 92.5 95.3 103 70-130
Diisopropyl ether ug/kg ND 92.5 101 109 70-130
Ethylbenzene ug/kg ND 92.5 105 113 70-130
Hexachloro-1,3-butadiene ug/kg ND 92.5 28.3 31 70-130 M1
Isopropylbenzene (Cumene) ug/kg ND 92.5 86.0 93 70-130
m&p-Xylene ug/kg ND 185 207 112 70-130
Methyl-tert-butyl ether ug/kg ND 92.5 96.5 104 70-130
Methylene Chloride ug/kg ND 92.5 102 89 70-130
n-Butylbenzene ug/kg ND 92.5 77.2 84 70-130
n-Propylbenzene ug/kg ND 92.5 139 151 70-130 M1
Naphthalene ug/kg ND 92.5 38.8 42 70-130 M1
o-Xylene ug/kg ND 92.5 95.2 103 70-130
p-Isopropyltoluene ug/kg ND 92.5 104 112 70-130
sec-Butylbenzene ug/kg ND 92.5 111 120 70-130
Styrene ug/kg ND 92.5 25.9 28 70-130 M1
tert-Butylbenzene ug/kg ND 92.5 112 121 70-130
Tetrachloroethene ug/kg ND 92.5 107 116 70-130
Toluene ug/kg ND 92.5 87.3 94 52-163
trans-1,2-Dichloroethene ug/kg ND 92.5 92.4 100 70-130
trans-1,3-Dichloropropene ug/kg ND 92.5 43.3 47 70-130 M1
Trichloroethene ug/kg ND 92.5 91.2 99 49-167
Trichlorofluoromethane ug/kg ND 92.5 116 126 70-130
Vinyl acetate ug/kg ND 185 ND 19 70-130 M1
Vinyl chloride ug/kg ND 92.5 108 117 70-130
Toluene-d8 (S) % 89 70-130

92357321001 Dup

#=QC#

(704)875-9092


92357321001 Dup
1,1-Dichloroethene ug/kg ND ND
1,1-Dichloropropene ug/kg ND ND
1,2,3-Trichloropropane ug/kg ND ND
1,2,4-Trimethylbenzene ug/kg ND ND
1,2-Dibromo-3-chloropropane ug/kg ND ND
1,2-Dibromoethane (EDB) ug/kg ND ND
1,3,5-Trimethylbenzene ug/kg ND ND
2-Butanone (MEK) ug/kg ND 19.6J
2-Hexanone ug/kg ND ND
4-Methyl-2-pentanone (MIBK) ug/kg ND ND
Acetone ug/kg ND 144J
Benzene ug/kg ND ND
Bromobenzene ug/kg ND ND
Bromochloromethane ug/kg ND ND
Bromodichloromethane ug/kg ND ND
Bromoform ug/kg ND ND
Bromomethane ug/kg ND ND
Carbon tetrachloride ug/kg ND ND
Chlorobenzene ug/kg ND ND
Chloroethane ug/kg ND ND
Chloroform ug/kg ND ND
Chloromethane ug/kg ND ND
cis-1,2-Dichloroethene ug/kg ND ND
cis-1,3-Dichloropropene ug/kg ND ND
Dibromochloromethane ug/kg ND ND
Dibromomethane ug/kg ND ND
Dichlorodifluoromethane ug/kg ND ND
Diisopropyl ether ug/kg ND ND
Ethylbenzene ug/kg ND ND
Hexachloro-1,3-butadiene ug/kg ND ND
Isopropylbenzene (Cumene) ug/kg ND ND
m&p-Xylene ug/kg ND ND

#=QC#

(704)875-9092


92357321001 Dup
Methyl-tert-butyl ether ug/kg ND ND
Methylene Chloride ug/kg ND ND
n-Butylbenzene ug/kg ND ND
n-Propylbenzene ug/kg ND ND
Naphthalene ug/kg ND ND
o-Xylene ug/kg ND ND
p-Isopropyltoluene ug/kg ND ND
sec-Butylbenzene ug/kg ND ND
Styrene ug/kg ND ND
tert-Butylbenzene ug/kg ND ND
Tetrachloroethene ug/kg ND ND
Toluene ug/kg ND ND
trans-1,2-Dichloroethene ug/kg ND ND
trans-1,3-Dichloropropene ug/kg ND ND
Trichloroethene ug/kg ND ND
Trichlorofluoromethane ug/kg ND ND
Vinyl acetate ug/kg ND ND
Vinyl chloride ug/kg ND ND
Xylene (Total) ug/kg ND ND
1,2-Dichloroethane-d4 (S) % 103 99 2
4-Bromofluorobenzene (S) % 72 72 6
Toluene-d8 (S) % 89 89 6 1g

#=QC#

(704)875-9092


QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV

Blank Reporting
Diesel Range Organics(C10-C28) mg/kg ND 5.0 10/04/17 09:32
n-Pentacosane (S) % 90 41-119 10/04/17 09:32

Spike LCS LCS % Rec
Diesel Range Organics(C10-C28) mg/kg 65.1 38.5 59 49-113
n-Pentacosane (S) % 81 41-119

92357418001 Dup
Diesel Range Organics(C10-C28) mg/kg ND ND
n-Pentacosane (S) % 51 63 19

#=QC#

(704)875-9092


QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV

Blank Reporting
Diesel Range Organics(C10-C28) mg/kg ND 4.9 10/04/17 17:00
n-Pentacosane (S) % 86 41-119 10/04/17 17:00

Spike LCS LCS % Rec
Diesel Range Organics(C10-C28) mg/kg 67.1 41.6 62 49-113

Diesel Range Organics(C10-C28) mg/kg ND 77.1 34.8 45 10-146 H3

#=QC#

(704)875-9092


QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides

Blank Reporting
4,4'-DDD ug/kg ND 2.0 10/05/17 20:24
4,4'-DDE ug/kg ND 2.0 10/05/17 20:24
4,4'-DDT ug/kg ND 2.0 10/05/17 20:24
Aldrin ug/kg ND 2.0 10/05/17 20:24
alpha-BHC ug/kg ND 2.0 10/05/17 20:24
beta-BHC ug/kg ND 2.0 10/05/17 20:24
Chlordane (Technical) ug/kg ND 7.1 10/05/17 20:24
delta-BHC ug/kg ND 2.0 10/05/17 20:24
Dieldrin ug/kg ND 2.0 10/05/17 20:24
Endosulfan I ug/kg ND 2.0 10/05/17 20:24
Endosulfan II ug/kg ND 2.0 10/05/17 20:24
Endosulfan sulfate ug/kg ND 2.0 10/05/17 20:24
Endrin ug/kg ND 2.0 10/05/17 20:24
Endrin aldehyde ug/kg ND 2.0 10/05/17 20:24
Endrin ketone ug/kg ND 2.0 10/05/17 20:24
gamma-BHC (Lindane) ug/kg ND 2.0 10/05/17 20:24
Heptachlor ug/kg ND 2.0 10/05/17 20:24
Heptachlor epoxide ug/kg ND 2.0 10/05/17 20:24
Hexachlorobenzene ug/kg ND 2.0 10/05/17 20:24
Methoxychlor ug/kg ND 5.1 10/05/17 20:24
Mirex ug/kg ND 5.1 10/05/17 20:24
Toxaphene ug/kg ND 7.1 10/05/17 20:24
Decachlorobiphenyl (S) % 87 21-123 10/05/17 20:24
Tetrachloro-m-xylene (S) % 82 35-108 10/05/17 20:24

Spike LCS LCS % Rec
4,4'-DDD ug/kg 8.3 8.3 100 63-126
4,4'-DDE ug/kg 8.3 8.5 103 62-126
4,4'-DDT ug/kg 8.3 8.5 103 65-135
Aldrin ug/kg 8.3 7.3 88 40-120
alpha-BHC ug/kg 8.3 6.4 78 37-123
beta-BHC ug/kg 8.3 6.7 82 51-113
delta-BHC ug/kg 8.3 8.3 101 25-139
Dieldrin ug/kg 8.3 8.5 103 54-125
Endosulfan I ug/kg 8.3 8.6 105 54-125
Endosulfan II ug/kg 8.3 9.4 114 62-121
Endosulfan sulfate ug/kg 8.3 8.7 106 39-121
Endrin ug/kg 8.3 8.2 99 65-134

#=QC#

(704)875-9092


Spike LCS LCS % Rec
Endrin aldehyde ug/kg 8.3 7.3 89 44-121
Endrin ketone ug/kg 8.3 8.7 106 59-124
gamma-BHC (Lindane) ug/kg 8.3 7.0 85 41-121
Heptachlor ug/kg 8.3 6.9 84 43-120
Heptachlor epoxide ug/kg 8.3 8.4 102 47-118
Hexachlorobenzene ug/kg 8.3 6.2 75 50-150
Methoxychlor ug/kg 24.8 25.9 105 68-125
Mirex ug/kg 24.8 25.0 101 59-114
Decachlorobiphenyl (S) % 107 21-123
Tetrachloro-m-xylene (S) % 77 35-108

4,4'-DDD ug/kg ND 17.4 17.1 98 50-150
4,4'-DDE ug/kg ND 17.4 17.6 101 50-150
4,4'-DDT ug/kg ND 17.4 17.3 99 50-150
Aldrin ug/kg ND 17.4 16.6 95 50-150
alpha-BHC ug/kg ND 17.4 14.9 85 50-150
beta-BHC ug/kg ND 17.4 15.3 88 50-150
delta-BHC ug/kg ND 17.4 15.4 88 50-150
Dieldrin ug/kg ND 17.4 17.1 98 50-150
Endosulfan I ug/kg ND 17.4 17.7 101 50-150
Endosulfan II ug/kg ND 17.4 18.0 103 50-150
Endosulfan sulfate ug/kg ND 17.4 17.4 100 50-150
Endrin ug/kg ND 17.4 16.8 96 50-150
Endrin aldehyde ug/kg ND 17.4 14.8 84 50-150
Endrin ketone ug/kg ND 17.4 16.9 97 50-150
gamma-BHC (Lindane) ug/kg ND 17.4 16.5 94 50-150
Heptachlor ug/kg ND 17.4 14.1 80 50-150
Heptachlor epoxide ug/kg ND 17.4 16.7 96 50-150
Hexachlorobenzene ug/kg ND 17.4 14.9 85 50-150
Methoxychlor ug/kg ND 52.3 52.2 100 50-150
Mirex ug/kg ND 52.3 51.2 98 50-150
Tetrachloro-m-xylene (S) % 60 35-108

92357321005 Dup
4,4'-DDD ug/kg ND ND
4,4'-DDE ug/kg ND ND
4,4'-DDT ug/kg ND ND
Aldrin ug/kg ND ND

#=QC#

(704)875-9092


92357321005 Dup
alpha-BHC ug/kg ND ND
beta-BHC ug/kg ND ND
Chlordane (Technical) ug/kg ND ND
delta-BHC ug/kg ND ND
Dieldrin ug/kg ND ND
Endosulfan I ug/kg ND ND
Endosulfan II ug/kg ND ND
Endosulfan sulfate ug/kg ND ND
Endrin ug/kg ND ND
Endrin aldehyde ug/kg ND ND
Endrin ketone ug/kg ND ND
gamma-BHC (Lindane) ug/kg ND ND
Heptachlor ug/kg ND ND
Heptachlor epoxide ug/kg ND ND
Hexachlorobenzene ug/kg ND ND
Methoxychlor ug/kg ND ND
Mirex ug/kg ND ND
Toxaphene ug/kg ND ND
Decachlorobiphenyl (S) % 0 65
Tetrachloro-m-xylene (S) % 0 75

#=QC#

(704)875-9092


QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides

Blank Reporting
4,4'-DDD ug/kg ND 2.0 10/06/17 11:44
4,4'-DDE ug/kg ND 2.0 10/06/17 11:44
4,4'-DDT ug/kg ND 2.0 10/06/17 11:44
Aldrin ug/kg ND 2.0 10/06/17 11:44
alpha-BHC ug/kg ND 2.0 10/06/17 11:44
beta-BHC ug/kg ND 2.0 10/06/17 11:44
Chlordane (Technical) ug/kg ND 6.8 10/06/17 11:44
delta-BHC ug/kg ND 2.0 10/06/17 11:44
Dieldrin ug/kg ND 2.0 10/06/17 11:44
Endosulfan I ug/kg ND 2.0 10/06/17 11:44
Endosulfan II ug/kg ND 2.0 10/06/17 11:44
Endosulfan sulfate ug/kg ND 2.0 10/06/17 11:44
Endrin ug/kg ND 2.0 10/06/17 11:44
Endrin aldehyde ug/kg ND 2.0 10/06/17 11:44
Endrin ketone ug/kg ND 2.0 10/06/17 11:44
gamma-BHC (Lindane) ug/kg ND 2.0 10/06/17 11:44
Heptachlor ug/kg ND 2.0 10/06/17 11:44
Heptachlor epoxide ug/kg ND 2.0 10/06/17 11:44
Hexachlorobenzene ug/kg ND 2.0 10/06/17 11:44
Methoxychlor ug/kg ND 4.9 10/06/17 11:44
Mirex ug/kg ND 4.9 10/06/17 11:44
Toxaphene ug/kg ND 6.8 10/06/17 11:44
Tetrachloro-m-xylene (S) % 79 35-108 10/06/17 11:44
LABORATORY CONTROL SAMPLE & LCSD: 2111749 2111750

Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
4,4'-DDD ug/kg 8.1 7.7 7.8 95 94 63-126 1 30
4,4'-DDE ug/kg 8.1 7.8 8.0 97 97 62-126 2 30
4,4'-DDT ug/kg 8.1 8.0 8.0 98 97 65-135 1 30
Aldrin ug/kg 8.1 7.3 7.7 90 93 40-120 5 30
alpha-BHC ug/kg 8.1 6.6 7.2 82 86 37-123 8 30
beta-BHC ug/kg 8.1 6.4 6.6 79 80 51-113 4 30
delta-BHC ug/kg 8.1 7.7 7.9 95 95 25-139 3 30
Dieldrin ug/kg 8.1 7.8 8.1 97 97 54-125 3 30
Endosulfan I ug/kg 8.1 8.0 8.3 99 101 54-125 4 30
Endosulfan II ug/kg 8.1 8.4 8.4 104 102 62-121 1 30
Endosulfan sulfate ug/kg 8.1 8.0 8.1 99 98 39-121 1 30
Endrin ug/kg 8.1 7.6 7.8 93 95 65-134 4 30

#=QC#

(704)875-9092


Endrin aldehyde ug/kg 8.1 7.1 7.2 88 87 44-121 2 30
Endrin ketone ug/kg 8.1 7.7 7.9 96 95 59-124 1 30
gamma-BHC (Lindane) ug/kg 8.1 7.0 7.4 86 90 41-121 6 30
Heptachlor ug/kg 8.1 7.0 7.4 87 90 43-120 5 30
Heptachlor epoxide ug/kg 8.1 7.9 8.3 98 100 47-118 5 30
Hexachlorobenzene ug/kg 8.1 6.7 7.2 83 87 50-150 7 30
Methoxychlor ug/kg 24.3 23.2 23.8 96 96 68-125 3 30
Mirex ug/kg 24.3 22.9 23.5 94 95 59-114 2 30
Decachlorobiphenyl (S) % 100 100 21-123
Tetrachloro-m-xylene (S) % 83 88 35-108

#=QC#

(704)875-9092


QC Batch Method: EPA 3546 Analysis Description: 8082 GCS PCB

Blank Reporting
PCB-1016 (Aroclor 1016) ug/kg ND 33.6 10/04/17 12:28

Spike LCS LCS % Rec
PCB-1016 (Aroclor 1016) ug/kg 167 148 89 31-120
PCB-1260 (Aroclor 1260) ug/kg 167 124 75 32-120

PCB-1016 (Aroclor 1016) ug/kg ND 194 704 364 49-150 M1
PCB-1260 (Aroclor 1260) ug/kg ND 194 96.3 50 50-150

92357321005 Dup
PCB-1016 (Aroclor 1016) ug/kg ND ND
Decachlorobiphenyl (S) % 58 56 5

#=QC#

(704)875-9092


QC Batch Method: EPA 3546 Analysis Description: 8082 GCS PCB

Blank Reporting

PCB-1016 (Aroclor 1016) ug/kg 163 108 127 66 78 31-120 16 30
PCB-1260 (Aroclor 1260) ug/kg 163 95.4 98.4 59 61 32-120 3 30
Decachlorobiphenyl (S) % 87 85 21-132

#=QC#

(704)875-9092


QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92357321004, 92357321005, 92357321006

Blank Reporting
1,2,4-Trichlorobenzene ug/kg ND 326 10/05/17 13:45
1,2-Dichlorobenzene ug/kg ND 326 10/05/17 13:45
1-Methylnaphthalene ug/kg ND 326 10/05/17 13:45
2,2'-Oxybis(1-chloropropane) ug/kg ND 326 10/05/17 13:45
2,4,5-Trichlorophenol ug/kg ND 326 10/05/17 13:45
2,4-Dichlorophenol ug/kg ND 326 10/05/17 13:45
2,4-Dimethylphenol ug/kg ND 326 10/05/17 13:45
2,4-Dinitrophenol ug/kg ND 1630 10/05/17 13:45
2,4-Dinitrotoluene ug/kg ND 326 10/05/17 13:45
2-Chloronaphthalene ug/kg ND 326 10/05/17 13:45
2-Chlorophenol ug/kg ND 326 10/05/17 13:45
2-Methylphenol(o-Cresol) ug/kg ND 326 10/05/17 13:45
2-Nitroaniline ug/kg ND 1630 10/05/17 13:45
2-Nitrophenol ug/kg ND 326 10/05/17 13:45
3&4-Methylphenol(m&p Cresol) ug/kg ND 326 10/05/17 13:45
3,3'-Dichlorobenzidine ug/kg ND 1630 10/05/17 13:45
4,6-Dinitro-2-methylphenol ug/kg ND 651 10/05/17 13:45
4-Bromophenylphenyl ether ug/kg ND 326 10/05/17 13:45
4-Chloro-3-methylphenol ug/kg ND 651 10/05/17 13:45
4-Chloroaniline ug/kg ND 1630 10/05/17 13:45
4-Chlorophenylphenyl ether ug/kg ND 326 10/05/17 13:45
Acenaphthene ug/kg ND 326 10/05/17 13:45
Acenaphthylene ug/kg ND 326 10/05/17 13:45
Aniline ug/kg ND 326 10/05/17 13:45
Anthracene ug/kg ND 326 10/05/17 13:45
Benzo(a)anthracene ug/kg ND 326 10/05/17 13:45
Benzo(a)pyrene ug/kg ND 326 10/05/17 13:45
Benzo(b)fluoranthene ug/kg ND 326 10/05/17 13:45
Benzo(g,h,i)perylene ug/kg ND 326 10/05/17 13:45
Benzo(k)fluoranthene ug/kg ND 326 10/05/17 13:45
Benzoic Acid ug/kg ND 1630 10/05/17 13:45
Benzyl alcohol ug/kg ND 651 10/05/17 13:45
bis(2-Chloroethoxy)methane ug/kg ND 326 10/05/17 13:45

#=QC#

(704)875-9092


Blank Reporting
bis(2-Chloroethyl) ether ug/kg ND 326 10/05/17 13:45
bis(2-Ethylhexyl)phthalate ug/kg ND 326 10/05/17 13:45
Butylbenzylphthalate ug/kg ND 326 10/05/17 13:45
Chrysene ug/kg ND 326 10/05/17 13:45
Di-n-butylphthalate ug/kg ND 326 10/05/17 13:45
Di-n-octylphthalate ug/kg ND 326 10/05/17 13:45
Dibenz(a,h)anthracene ug/kg ND 326 10/05/17 13:45
Dibenzofuran ug/kg ND 326 10/05/17 13:45
Diethylphthalate ug/kg ND 326 10/05/17 13:45
Dimethylphthalate ug/kg ND 326 10/05/17 13:45
Fluoranthene ug/kg ND 326 10/05/17 13:45
Fluorene ug/kg ND 326 10/05/17 13:45
Hexachloro-1,3-butadiene ug/kg ND 326 10/05/17 13:45
Hexachlorobenzene ug/kg ND 326 10/05/17 13:45
Hexachlorocyclopentadiene ug/kg ND 326 10/05/17 13:45
Hexachloroethane ug/kg ND 326 10/05/17 13:45
Indeno(1,2,3-cd)pyrene ug/kg ND 326 10/05/17 13:45
Isophorone ug/kg ND 326 10/05/17 13:45
N-Nitroso-di-n-propylamine ug/kg ND 326 10/05/17 13:45
N-Nitrosodimethylamine ug/kg ND 326 10/05/17 13:45
N-Nitrosodiphenylamine ug/kg ND 326 10/05/17 13:45
Naphthalene ug/kg ND 326 10/05/17 13:45
Nitrobenzene ug/kg ND 326 10/05/17 13:45
Pentachlorophenol ug/kg ND 1630 10/05/17 13:45
Phenanthrene ug/kg ND 326 10/05/17 13:45
Phenol ug/kg ND 326 10/05/17 13:45
Pyrene ug/kg ND 326 10/05/17 13:45
2,4,6-Tribromophenol (S) % 86 27-110 10/05/17 13:45
2-Fluorobiphenyl (S) % 78 30-110 10/05/17 13:45
2-Fluorophenol (S) % 73 13-110 10/05/17 13:45
Nitrobenzene-d5 (S) % 78 23-110 10/05/17 13:45
Phenol-d6 (S) % 80 22-110 10/05/17 13:45
Terphenyl-d14 (S) % 80 28-110 10/05/17 13:45

Spike LCS LCS % Rec
1,2,4-Trichlorobenzene ug/kg 1680 1380 82 36-120
1,2-Dichlorobenzene ug/kg 1680 1400 83 41-120
1-Methylnaphthalene ug/kg 1680 1500 89 40-120
2,2'-Oxybis(1-chloropropane) ug/kg 1680 1150 68 17-120
2,4,5-Trichlorophenol ug/kg 1680 1580 94 37-120

#=QC#

(704)875-9092


Spike LCS LCS % Rec
2,4,6-Trichlorophenol ug/kg 1680 1450 86 40-120
2,4-Dichlorophenol ug/kg 1680 1460 87 33-120
2,4-Dimethylphenol ug/kg 1680 1560 93 36-120
2,4-Dinitrophenol ug/kg 8420 7080 84 22-121
2,4-Dinitrotoluene ug/kg 1680 1600 95 60-120
2,6-Dinitrotoluene ug/kg 1680 1680 100 54-120
2-Chloronaphthalene ug/kg 1680 1480 88 41-120
2-Chlorophenol ug/kg 1680 1470 88 39-120
2-Methylnaphthalene ug/kg 1680 1500 89 26-120
2-Methylphenol(o-Cresol) ug/kg 1680 1750 104 41-120
2-Nitroaniline ug/kg 3370 2820 84 45-120
2-Nitrophenol ug/kg 1680 1460 87 35-120
3&4-Methylphenol(m&p Cresol) ug/kg 1680 1650 98 35-120
3,3'-Dichlorobenzidine ug/kg 3370 3120 93 16-125
4,6-Dinitro-2-methylphenol ug/kg 3370 3420 102 46-120
4-Bromophenylphenyl ether ug/kg 1680 1520 90 36-120
4-Chloro-3-methylphenol ug/kg 3370 3030 90 37-120
4-Chloroaniline ug/kg 3370 2740 81 35-120
4-Chlorophenylphenyl ether ug/kg 1680 1450 86 30-120
4-Nitrophenol ug/kg 8420 7880 94 43-120
Acenaphthene ug/kg 1680 1470 87 46-120
Acenaphthylene ug/kg 1680 1530 91 46-120
Aniline ug/kg 1680 1410 83 33-120
Anthracene ug/kg 1680 1520 90 63-120
Benzo(a)anthracene ug/kg 1680 1500 89 61-120
Benzo(a)pyrene ug/kg 1680 1460 87 59-120
Benzo(b)fluoranthene ug/kg 1680 1400 83 55-120
Benzo(g,h,i)perylene ug/kg 1680 1380 82 57-120
Benzo(k)fluoranthene ug/kg 1680 1350 80 56-120
Benzoic Acid ug/kg 8420 5670 67 13-120
Benzyl alcohol ug/kg 3370 3110 92 34-120
bis(2-Chloroethoxy)methane ug/kg 1680 1450 86 21-120
bis(2-Chloroethyl) ether ug/kg 1680 1420 84 25-120
bis(2-Ethylhexyl)phthalate ug/kg 1680 1740 103 56-123
Butylbenzylphthalate ug/kg 1680 1740 103 57-120
Chrysene ug/kg 1680 1460 87 64-120
Di-n-butylphthalate ug/kg 1680 1720 102 58-120
Di-n-octylphthalate ug/kg 1680 1920 114 47-121
Dibenz(a,h)anthracene ug/kg 1680 1420 84 56-120
Dibenzofuran ug/kg 1680 1440 85 43-120
Diethylphthalate ug/kg 1680 1620 96 55-120
Dimethylphthalate ug/kg 1680 1670 99 54-120
Fluoranthene ug/kg 1680 1540 91 61-120
Fluorene ug/kg 1680 1510 90 51-120
Hexachloro-1,3-butadiene ug/kg 1680 1350 80 22-120

#=QC#

(704)875-9092


Spike LCS LCS % Rec
Hexachlorobenzene ug/kg 1680 1520 90 53-120
Hexachlorocyclopentadiene ug/kg 1680 1180 70 18-150
Hexachloroethane ug/kg 1680 1370 81 39-120
Indeno(1,2,3-cd)pyrene ug/kg 1680 1430 85 58-120
Isophorone ug/kg 1680 1560 93 38-120
N-Nitroso-di-n-propylamine ug/kg 1680 1670 99 30-120
N-Nitrosodimethylamine ug/kg 1680 1320 78 32-120
N-Nitrosodiphenylamine ug/kg 1680 1560 93 50-120
Naphthalene ug/kg 1680 1400 83 38-120
Nitrobenzene ug/kg 1680 1390 83 37-120
Pentachlorophenol ug/kg 3370 2850 85 10-120
Phenanthrene ug/kg 1680 1500 89 62-120
Phenol ug/kg 1680 1610 96 37-120
Pyrene ug/kg 1680 1340 79 63-120
2,4,6-Tribromophenol (S) % 93 27-110
2-Fluorobiphenyl (S) % 85 30-110
2-Fluorophenol (S) % 81 13-110
Nitrobenzene-d5 (S) % 80 23-110
Phenol-d6 (S) % 91 22-110
Terphenyl-d14 (S) % 78 28-110

#=QC#

(704)875-9092


QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave

Blank Reporting
1,2,4-Trichlorobenzene ug/kg ND 325 10/06/17 11:39
2,2'-Oxybis(1-chloropropane) ug/kg ND 325 10/06/17 11:39
2,4-Dichlorophenol ug/kg ND 325 10/06/17 11:39
2,4-Dimethylphenol ug/kg ND 325 10/06/17 11:39
2,4-Dinitrophenol ug/kg ND 1620 10/06/17 11:39
2-Chloronaphthalene ug/kg ND 325 10/06/17 11:39
2-Chlorophenol ug/kg ND 325 10/06/17 11:39
2-Methylphenol(o-Cresol) ug/kg ND 325 10/06/17 11:39
3&4-Methylphenol(m&p Cresol) ug/kg ND 325 10/06/17 11:39
3,3'-Dichlorobenzidine ug/kg ND 1620 10/06/17 11:39
4,6-Dinitro-2-methylphenol ug/kg ND 649 10/06/17 11:39
4-Bromophenylphenyl ether ug/kg ND 325 10/06/17 11:39
4-Chloro-3-methylphenol ug/kg ND 649 10/06/17 11:39
4-Chloroaniline ug/kg ND 1620 10/06/17 11:39
4-Chlorophenylphenyl ether ug/kg ND 325 10/06/17 11:39
Acenaphthene ug/kg ND 325 10/06/17 11:39
Acenaphthylene ug/kg ND 325 10/06/17 11:39
Aniline ug/kg ND 325 10/06/17 11:39
Anthracene ug/kg ND 325 10/06/17 11:39
Benzo(a)anthracene ug/kg ND 325 10/06/17 11:39
Benzo(a)pyrene ug/kg ND 325 10/06/17 11:39
Benzo(b)fluoranthene ug/kg ND 325 10/06/17 11:39
Benzo(g,h,i)perylene ug/kg ND 325 10/06/17 11:39
Benzo(k)fluoranthene ug/kg ND 325 10/06/17 11:39
Benzoic Acid ug/kg ND 1620 10/06/17 11:39
Benzyl alcohol ug/kg ND 649 10/06/17 11:39
bis(2-Chloroethoxy)methane ug/kg ND 325 10/06/17 11:39

#=QC#

(704)875-9092


Blank Reporting
bis(2-Chloroethyl) ether ug/kg ND 325 10/06/17 11:39
bis(2-Ethylhexyl)phthalate ug/kg ND 325 10/06/17 11:39
Butylbenzylphthalate ug/kg ND 325 10/06/17 11:39
Chrysene ug/kg ND 325 10/06/17 11:39
Di-n-butylphthalate ug/kg ND 325 10/06/17 11:39
Di-n-octylphthalate ug/kg ND 325 10/06/17 11:39
Dibenz(a,h)anthracene ug/kg ND 325 10/06/17 11:39
Dibenzofuran ug/kg ND 325 10/06/17 11:39
Diethylphthalate ug/kg ND 325 10/06/17 11:39
Dimethylphthalate ug/kg ND 325 10/06/17 11:39
Fluoranthene ug/kg ND 325 10/06/17 11:39
Fluorene ug/kg ND 325 10/06/17 11:39
Hexachloro-1,3-butadiene ug/kg ND 325 10/06/17 11:39
Hexachlorobenzene ug/kg ND 325 10/06/17 11:39
Hexachlorocyclopentadiene ug/kg ND 325 10/06/17 11:39
Hexachloroethane ug/kg ND 325 10/06/17 11:39
Indeno(1,2,3-cd)pyrene ug/kg ND 325 10/06/17 11:39
Isophorone ug/kg ND 325 10/06/17 11:39
N-Nitroso-di-n-propylamine ug/kg ND 325 10/06/17 11:39
N-Nitrosodimethylamine ug/kg ND 325 10/06/17 11:39
N-Nitrosodiphenylamine ug/kg ND 325 10/06/17 11:39
Naphthalene ug/kg ND 325 10/06/17 11:39
Nitrobenzene ug/kg ND 325 10/06/17 11:39
Pentachlorophenol ug/kg ND 1620 10/06/17 11:39
Phenanthrene ug/kg ND 325 10/06/17 11:39
Phenol ug/kg ND 325 10/06/17 11:39
Pyrene ug/kg ND 325 10/06/17 11:39
2,4,6-Tribromophenol (S) % 66 27-110 10/06/17 11:39
2-Fluorobiphenyl (S) % 60 30-110 10/06/17 11:39
2-Fluorophenol (S) % 61 13-110 10/06/17 11:39
Nitrobenzene-d5 (S) % 63 23-110 10/06/17 11:39
Phenol-d6 (S) % 68 22-110 10/06/17 11:39
Terphenyl-d14 (S) % 63 28-110 10/06/17 11:39

1,2,4-Trichlorobenzene ug/kg 836 519 547 62 65 36-120 5 30
1,2-Dichlorobenzene ug/kg 836 533 556 64 66 41-120 4 30
1,3-Dichlorobenzene ug/kg 836 512 539 61 64 66-120 5 30 L2
1,4-Dichlorobenzene ug/kg 836 528 541 63 64 42-120 2 30
1-Methylnaphthalene ug/kg 836 578 596 69 71 40-120 3 30
2,2'-Oxybis(1-chloropropane) ug/kg 836 464 471 56 56 17-120 1 30
2,4,5-Trichlorophenol ug/kg 836 554 572 66 68 37-120 3 30

#=QC#

(704)875-9092


2,4,6-Trichlorophenol ug/kg 836 534 549 64 65 40-120 3 30
2,4-Dichlorophenol ug/kg 836 571 571 68 68 33-120 0 30
2,4-Dimethylphenol ug/kg 836 590 607 71 72 36-120 3 30
2,4-Dinitrophenol ug/kg 4180 2720 2730 65 65 22-121 0 30
2,4-Dinitrotoluene ug/kg 836 628 683 75 81 60-120 8 30
2,6-Dinitrotoluene ug/kg 836 636 635 76 76 54-120 0 30
2-Chloronaphthalene ug/kg 836 532 560 64 67 41-120 5 30
2-Chlorophenol ug/kg 836 583 582 70 69 39-120 0 30
2-Methylnaphthalene ug/kg 836 573 597 69 71 26-120 4 30
2-Methylphenol(o-Cresol) ug/kg 836 713 724 85 86 41-120 1 30
2-Nitroaniline ug/kg 1670 1100J 1200J 66 71 45-120 30
2-Nitrophenol ug/kg 836 561 566 67 67 35-120 1 30
3&4-Methylphenol(m&p Cresol) ug/kg 836 667 701 80 84 35-120 5 30
3,3'-Dichlorobenzidine ug/kg 1670 1200J 1110J 72 66 16-125 30
3-Nitroaniline ug/kg 1670 1120J 1190J 67 71 45-120 30
4,6-Dinitro-2-methylphenol ug/kg 1670 1340 1260 80 75 46-120 6 30
4-Bromophenylphenyl ether ug/kg 836 581 551 69 66 36-120 5 30
4-Chloro-3-methylphenol ug/kg 1670 1200 1220 72 73 37-120 1 30
4-Chloroaniline ug/kg 1670 1080J 1030J 65 61 35-120 30
4-Chlorophenylphenyl ether ug/kg 836 535 558 64 67 30-120 4 30
4-Nitroaniline ug/kg 1670 1200 1450 72 86 48-120 19 30
4-Nitrophenol ug/kg 4180 3360 3760 80 90 43-120 11 30
Acenaphthene ug/kg 836 541 568 65 68 46-120 5 30
Acenaphthylene ug/kg 836 556 574 66 68 46-120 3 30
Aniline ug/kg 836 560 543 67 65 33-120 3 30
Anthracene ug/kg 836 577 605 69 72 63-120 5 30
Benzo(a)anthracene ug/kg 836 581 606 69 72 61-120 4 30
Benzo(a)pyrene ug/kg 836 588 593 70 71 59-120 1 30
Benzo(b)fluoranthene ug/kg 836 555 579 66 69 55-120 4 30
Benzo(g,h,i)perylene ug/kg 836 588 569 70 68 57-120 3 30
Benzo(k)fluoranthene ug/kg 836 545 544 65 65 56-120 0 30
Benzoic Acid ug/kg 4180 1940 1840 46 44 13-120 5 30
Benzyl alcohol ug/kg 1670 1220 1180 73 71 34-120 3 30
bis(2-Chloroethoxy)methane ug/kg 836 568 581 68 69 21-120 2 30
bis(2-Chloroethyl) ether ug/kg 836 568 555 68 66 25-120 2 30
bis(2-Ethylhexyl)phthalate ug/kg 836 704 713 84 85 56-123 1 30
Butylbenzylphthalate ug/kg 836 690 711 83 85 57-120 3 30
Chrysene ug/kg 836 565 590 68 70 64-120 4 30
Di-n-butylphthalate ug/kg 836 653 741 78 88 58-120 13 30
Di-n-octylphthalate ug/kg 836 775 816 93 97 47-121 5 30
Dibenz(a,h)anthracene ug/kg 836 596 596 71 71 56-120 0 30
Dibenzofuran ug/kg 836 556 567 67 68 43-120 2 30
Diethylphthalate ug/kg 836 650 686 78 82 55-120 5 30
Dimethylphthalate ug/kg 836 636 684 76 82 54-120 7 30
Fluoranthene ug/kg 836 563 674 67 80 61-120 18 30
Fluorene ug/kg 836 574 604 69 72 51-120 5 30
Hexachloro-1,3-butadiene ug/kg 836 513 566 61 67 22-120 10 30

#=QC#

(704)875-9092


Hexachlorobenzene ug/kg 836 549 568 66 68 53-120 3 30
Hexachlorocyclopentadiene ug/kg 836 431 383 51 46 18-150 12 30
Hexachloroethane ug/kg 836 540 548 65 65 39-120 2 30
Indeno(1,2,3-cd)pyrene ug/kg 836 613 608 73 72 58-120 1 30
Isophorone ug/kg 836 627 618 75 74 38-120 1 30
N-Nitroso-di-n-propylamine ug/kg 836 689 688 82 82 30-120 0 30
N-Nitrosodimethylamine ug/kg 836 507 542 61 65 32-120 7 30
N-Nitrosodiphenylamine ug/kg 836 595 578 71 69 50-120 3 30
Naphthalene ug/kg 836 528 561 63 67 38-120 6 30
Nitrobenzene ug/kg 836 549 566 66 67 37-120 3 30
Pentachlorophenol ug/kg 1670 1090J 1080J 65 64 10-120 30
Phenanthrene ug/kg 836 558 592 67 71 62-120 6 30
Phenol ug/kg 836 640 659 77 79 37-120 3 30
Pyrene ug/kg 836 517 535 62 64 63-120 3 30 L2
2,4,6-Tribromophenol (S) % 69 68 27-110
2-Fluorobiphenyl (S) % 63 63 30-110
2-Fluorophenol (S) % 66 68 13-110
Nitrobenzene-d5 (S) % 63 66 23-110
Phenol-d6 (S) % 74 75 22-110
Terphenyl-d14 (S) % 62 65 28-110

#=QC#

(704)875-9092

QC Batch: 380581 Analysis Method: ASTM D2974-87

QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture

92357321001 Dup
Percent Moisture % 53.6 57.1 6

92357337001 Dup
Percent Moisture % 81.9 82.0 0

#=QC#

(704)875-9092


QC Batch Method: EPA 7196 Modified Analysis Description: 7196 Chromium, Hexavalent

Blank Reporting
Chromium, Hexavalent mg/kg ND 5.0 10/03/17 16:12

Spike LCS LCS % Rec
Chromium, Hexavalent mg/kg 25 25.3 101 90-110

MS MSD
Chromium, Hexavalent mg/kg ND 16.3 15.2 16.0 14.9 98 98 75-125 7

#=QL#

(704)875-9092
QUALIFIERS

DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville

PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
1g The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.
D3 Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M0 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.

#=CR#

(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE

Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92357321001 ZONE 1 EPA 3546 380582 EPA 8015 Modified 380745

92357321004 SP-1 EPA 3546 380743 EPA 8015 Modified 380974
92357321001 ZONE 1 EPA 3546 380713 EPA 8081 380810
92357321002 ZONE 2 EPA 3546 381068 EPA 8081 381160

92357321003 ZONE 4 EPA 3546 381068 EPA 8081 381160
92357321004 SP-1 EPA 3546 380713 EPA 8081 380810

92357321005 SP-2 EPA 3546 380713 EPA 8081 380810
92357321006 SP-3 EPA 3546 380713 EPA 8081 380810
92357321001 ZONE 1 EPA 3546 380714 EPA 8082 380811
92357321002 ZONE 2 EPA 3546 381088 EPA 8082 381161
92357321003 ZONE 4 EPA 3546 380714 EPA 8082 380811

92357321004 SP-1 EPA 3546 380714 EPA 8082 380811
92357321005 SP-2 EPA 3546 380714 EPA 8082 380811
92357321006 SP-3 EPA 3546 380714 EPA 8082 380811
92357321001 ZONE 1 EPA 5035A/5030B 380604 EPA 8015 Modified 381037

92357321004 SP-1 EPA 5035A/5030B 380604 EPA 8015 Modified 380791
92357321001 ZONE 1 EPA 3050 380282 EPA 6010 380308

92357321002 ZONE 2 EPA 3050 380282 EPA 6010 380308
92357321003 ZONE 4 EPA 3050 380282 EPA 6010 380308
92357321004 SP-1 EPA 3050 380282 EPA 6010 380308
92357321005 SP-2 EPA 3050 380282 EPA 6010 380308
92357321006 SP-3 EPA 3050 380282 EPA 6010 380308
92357321001 ZONE 1 EPA 7471 380651 EPA 7471 380727

92357321002 ZONE 2 EPA 7471 380651 EPA 7471 380727
92357321003 ZONE 4 EPA 7471 380651 EPA 7471 380727
92357321004 SP-1 EPA 7471 380651 EPA 7471 380727
92357321005 SP-2 EPA 7471 380651 EPA 7471 380727
92357321006 SP-3 EPA 7471 380665 EPA 7471 380728
92357321001 ZONE 1 EPA 3546 381174 EPA 8270 381198

92357321002 ZONE 2 EPA 3546 381174 EPA 8270 381198
92357321003 ZONE 4 EPA 3546 381174 EPA 8270 381198
92357321004 SP-1 EPA 3546 380637 EPA 8270 380848

92357321005 SP-2 EPA 3546 380637 EPA 8270 380848

#=CR#

(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE

Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92357321006 SP-3 EPA 3546 380637 EPA 8270 380848
92357321001 ZONE 1 EPA 8260 380786

92357321002 ZONE 2 EPA 8260 380786
92357321003 ZONE 4 EPA 8260 380786
92357321004 SP-1 EPA 8260 380595

92357321005 SP-2 EPA 8260 380595
92357321006 SP-3 EPA 8260 380786
92357321001 ZONE 1 ASTM D2974-87 380581

92357321002 ZONE 2 ASTM D2974-87 380581
92357321003 ZONE 4 ASTM D2974-87 380581
92357321004 SP-1 ASTM D2974-87 380581
92357321005 SP-2 ASTM D2974-87 380581
92357321006 SP-3 ASTM D2974-87 380581
92357321001 ZONE 1 EPA 7196 Modified 380601 EPA 7196 380659

92357321004 SP-1 EPA 7196 Modified 380601 EPA 7196 380659

Page 75 of 77
Page 76 of 77
Page 77 of 77
Particle Size Distribution Report
1 in.
3/8 in.
#100
#140
#200
in.
in.
6 in.
3 in.
2 in.
1 in.
#10
#20
#30
#40
#60
#4
100 0
90 10
80 20
70 30
PERCENT COARSER
PERCENT FINER
60 40
50 50
40 60
30 70
20 80
10 90
0 100
100 10 1 0.1 0.01 0.001
GRAIN SIZE - mm.

% Gravel % Sand % Fines
% +3"
Coarse Fine Coarse Medium Fine Silt Clay
0.0 0.0 0.0 0.0 3.8 43.1 35.0 18.1
SIEVE PERCENT SPEC.* PASS? Soil Description

SIZE FINER PERCENT (X=NO) Black, Silt, with Moderate Organic Material
#4 100.0
#10 100.0
#20 99.8
#40 96.2 Atterberg Limits
PL= LL= PI=
#60 85.2
#100 63.6 Coefficients
#200 53.1 D90= 0.2926 D85= 0.2489 D60= 0.1328
0.0327 mm. 45.1 D50= 0.0521 D30= 0.0106 D15= 0.0031
0.0211 mm. 39.8 D10= Cu= Cc=
0.0124 mm. 32.5
Classification
0.0089 mm. 27.2 USCS= AASHTO=
0.0064 mm. 21.9
0.0046 mm. 17.3 Remarks
0.0032 mm. 15.2
0.0013 mm. 13.3
* (no specification provided)
Location: Zone 1
Sample Number: S-1 Date: 10/6/17
Client: SEPI Engineering Construction
Project: Carolina Beach Lake
Project No: 25877 Figure
Tested By: KEL

1 in.
3/8 in.
#100
#140
#200
in.
in.
6 in.
3 in.
2 in.
1 in.
#10
#20
#30
#40
#60
#4
100 0
90 10
80 20
70 30
PERCENT COARSER
PERCENT FINER
60 40
50 50
40 60
30 70
20 80
10 90
0 100
100 10 1 0.1 0.01 0.001
GRAIN SIZE - mm.

% +3"
0.0 0.0 0.0 0.0 10.0 26.5 32.7 30.8

SIZE FINER PERCENT (X=NO) Black, Silt, with Heavy Organic Material
#4 100.0
#10 100.0
#20 99.5
PL= LL= PI=
#60 77.6
#200 63.5 D90= 0.4250 D85= 0.3400 D60= 0.0469
0.0317 mm. 54.3 D50= 0.0255 D30= 0.0047 D15=
0.0207 mm. 46.1 D10= Cu= Cc=
0.0122 mm. 39.8
Classification
0.0063 mm. 33.4
0.0045 mm. 29.3 Remarks
0.0031 mm. 25.2
0.0013 mm. 19.2
Location: Zone 2
Tested By: KEL

1 in.
3/8 in.
#100
#140
#200
in.
in.
6 in.
3 in.
2 in.
1 in.
#10
#20
#30
#40
#60
#4
100 0
90 10
80 20
70 30
PERCENT COARSER
PERCENT FINER
60 40
50 50
40 60
30 70
20 80
10 90
0 100
100 10 1 0.1 0.01 0.001
GRAIN SIZE - mm.

% +3"
0.0 0.0 1.5 0.9 19.7 66.2 5.3 6.4

SIZE FINER PERCENT (X=NO) Black, Fine to Medium Sand, with Silt, Some Organic Material
3/8 100.0
#4 98.5
#10 97.6
PL= LL= PI=
#40 77.9
#100 19.0 D90= 0.6200 D85= 0.5126 D60= 0.3049
#200 11.7 D50= 0.2603 D30= 0.1891 D15= 0.1107
0.0362 mm. 10.9 D10= 0.0233 Cu= 13.11 Cc= 5.04
0.0230 mm. 10.0
Classification
0.0094 mm. 8.2
0.0067 mm. 7.2 Remarks
0.0047 mm. 6.3
0.0033 mm. 5.9
0.0014 mm. 5.2
Location: Zone 4
Tested By: EG Checked By: KEL

1 in.
3/8 in.
#100
#140
#200
in.
in.
6 in.
3 in.
2 in.
1 in.
#10
#20
#30
#40
#60
#4
100 0
90 10
80 20
70 30
PERCENT COARSER
PERCENT FINER
60 40
50 50
40 60
30 70
20 80
10 90
0 100
100 10 1 0.1 0.01 0.001
GRAIN SIZE - mm.

% +3"
0.0 0.0 0.0 0.6 15.7 73.8 5.5 4.4

SIZE FINER PERCENT (X=NO) Very Dark Brown, Fine to Medium Sand, with Silt, Slight
#4 100.0 Organic Material
#10 99.4
#20 98.1
PL= LL= PI=
#60 46.0
#200 9.9 D90= 0.4929 D85= 0.4363 D60= 0.2994
0.0364 mm. 8.3 D50= 0.2633 D30= 0.1991 D15= 0.1403
0.0231 mm. 7.4 D10= 0.0764 Cu= 3.92 Cc= 1.73
0.0134 mm. 6.4
Classification
0.0067 mm. 5.3
0.0033 mm. 4.1
0.0014 mm. 3.4
Location: SP-1
Tested By: KEL

1 in.
3/8 in.
#100
#140
#200
in.
in.
6 in.
3 in.
2 in.
1 in.
#10
#20
#30
#40
#60
#4
100 0
90 10
80 20
70 30
PERCENT COARSER
PERCENT FINER
60 40
50 50
40 60
30 70
20 80
10 90
0 100
100 10 1 0.1 0.01 0.001
GRAIN SIZE - mm.

% +3"
0.0 0.0 0.6 0.8 18.2 72.6 3.4 4.4

3/8 100.0 Organic Material
#4 99.4
#10 98.6
PL= LL= PI=
#40 80.4
#100 12.1 D90= 0.5283 D85= 0.4637 D60= 0.3223
#200 7.8 D50= 0.2862 D30= 0.2197 D15= 0.1640
0.0366 mm. 7.2 D10= 0.1146 Cu= 2.81 Cc= 1.31
0.0232 mm. 6.3
Classification
0.0095 mm. 5.2
0.0048 mm. 4.3
0.0033 mm. 4.3
0.0014 mm. 4.3
Location: SP-2
Tested By: KEL

1 in.
3/8 in.
#100
#140
#200
in.
in.
6 in.
3 in.
2 in.
1 in.
#10
#20
#30
#40
#60
#4
100 0
90 10
80 20
70 30
PERCENT COARSER
PERCENT FINER
60 40
50 50
40 60
30 70
20 80
10 90
0 100
100 10 1 0.1 0.01 0.001
GRAIN SIZE - mm.

% +3"
0.0 0.0 0.0 0.2 14.7 74.0 4.1 7.0

#4 100.0 Organic Material
#10 99.8
#20 98.4
PL= LL= PI=
#60 46.5
#200 11.1 D90= 0.4752 D85= 0.4245 D60= 0.2961
0.0363 mm. 10.1 D50= 0.2614 D30= 0.1990 D15= 0.1397
0.0230 mm. 9.2 D10= 0.0350 Cu= 8.47 Cc= 3.83
0.0134 mm. 8.1
Classification
0.0067 mm. 7.1
0.0033 mm. 6.0
0.0014 mm. 5.3
Location: SP-3
Tested By: KEL

APPENDIX C Supplemental Report Documents
ASFE Document
Important Information About Your
Geotechnical Engineering Report
Subsurface problems are a principal cause of construction delays, cost overruns, claims, and disputes
The following information is provided to help you manage your risks.
Geotechnical Services Are Performed for elevation, configuration, location, orientation, or weight of the
Specific Purposes, Persons, and Projects proposed structure,
Geotechnical engineers structure their services to meet the specific needs of composition of the design team, or
their clients. A geotechnical engineering study conducted for a civil engineer project ownership.
may not fulfill the needs of a construction contractor or even another civil
engineer. Because each geotechnical engineering study is unique, each geo- As a general rule, always inform your geotechnical engineer of project
technical engineering report is unique, prepared solely for the client. No one changes - even minor ones - and request an assessment of their impact.
except you should rely on your geotechnical engineering report without first Geotechnical engineers cannot accept responsibility or liability for problems
conferring with the geotechnical engineer who prepared it. And no one - not that occur because their reports do not consider developments of which they
even you - should apply the report for any purpose or project except the one were not informed.
originally contemplated.
Subsurface Conditions Can Change
Read the Full Report A geotechnical engineering report is based on conditions that existed at the
Serious problems have occurred because those relying on a geotechnical time the study was performed. Do not rely on a geotechnical engineering
engineering report did not read it all. Do not rely on an executive summary. report whose adequacy may have been affected by: the passage of time; by
Do not read selected elements only. man-made events, such as construction on or adjacent to the site; or by natu-
ral events, such as floods, earthquakes, or groundwater fluctuations. Always
A Geotechnical Engineering Report Is Based on contact the geotechnical engineer before applying the report to determine if it
A Unique Set of Project-Specific Factors is still reliable. A minor amount of additional testing or analysis could prevent
Geotechnical engineers consider a number of unique, project-specific factors major problems.
when establishing the scope of a study. Typical factors include: the clients
goals, objectives, and risk management preferences; the general nature of the Most Geotechnical Findings Are Professional
structure involved, its size, and configuration; the location of the structure Opinions
on the site; and other planned or existing site improvements, such as access Site exploration identifies subsurface conditions only at those points where
roads, parking lots, and underground utilities. Unless the geotechnical engi- subsurface tests are conducted or samples are taken. Geotechnical engineers
neer who conducted the study specifically indicates otherwise, do not rely on review field and laboratory data and then apply their professional judgment
a geotechnical engineering report that was: to render an opinion about subsurface conditions throughout the site. Actual
not prepared for you, subsurface conditions may differ-sometimes significantly from those indi-
not prepared for your project, cated in your report. Retaining the geotechnical engineer who developed your
not prepared for the specific site explored, or report to provide construction observation is the most effective method of
completed before important project changes were made. managing the risks associated with unanticipated conditions.
Typical changes that can erode the reliability of an existing geotechnical A Reports Recommendations Are Not Final
engineering report include those that affect: Do not overrely on the construction recommendations included in your re-
the function of the proposed structure, as when its changed from a port. Those recommendations are not final, because geotechnical engineers
parking garage to an office building, or from alight industrial plant develop them principally from judgment and opinion. Geotechnical engineers
to a refrigerated warehouse, can finalize their recommendations only by observing actual
subsurface conditions revealed during construction. The geotechnical engi- to disappointments, claims, and disputes. To help reduce the risk of such
neer who developed your report cannot assume responsibility or liability for outcomes, geotechnical engineers commonly include a variety of explanatory
the reports recommendations if that engineer does not perform construction provisions in their reports. Sometimes labeled limitations many of these
observation. provisions indicate where geotechnical engineers responsibilities begin
and end, to help others recognize their own responsibilities and risks. Read
A Geotechnical Engineering Report Is Subject to these provisions closely. Ask questions. Your geotechnical engineer should
Misinterpretation respond fully and frankly.
Other design team members misinterpretation of geotechnical engineer-
ing reports has resulted in costly problems. Lower that risk by having your Geoenvironmental Concerns Are Not Covered
geotechnical engineer confer with appropriate members of the design team The equipment, techniques, and personnel used to perform a geoenviron-
after submitting the report. Also retain your geotechnical engineer to review mental study differ significantly from those used to perform a geotechnical
pertinent elements of the design teams plans and specifications. Contractors study. For that reason, a geotechnical engineering report does not usually re-
can also misinterpret a geotechnical engineering report. Reduce that risk by late any geoenvironmental findings, conclusions, or recommendations; e.g.,
having your geotechnical engineer participate in prebid and preconstruction about the likelihood of encountering underground storage tanks or regulated
conferences, and by providing construction observation. contaminants. Unanticipated environmental problems have led to numerous
project failures. If you have not yet obtained your own geoenvironmental in-
Do Not Redraw the Engineers Logs formation, ask your geotechnical consultant for risk management guidance.
Geotechnical engineers prepare final boring and testing logs based upon Do not rely on an environmental report prepared for someone else.
their interpretation of field logs and laboratory data. To prevent errors or
omissions, the logs included in a geotechnical engineering report should Obtain Professional Assistance To Deal with Mold
never be redrawn for inclusion in architectural or other design drawings. Diverse strategies can be applied during building design, construction, op-
Only photographic or electronic reproduction is acceptable, but recognize eration, and maintenance to prevent significant amounts of mold from grow-
that separating logs from the report can elevate risk. ing on indoor surfaces. To be effective, all such strategies should be devised
for the express purpose of mold prevention, integrated into a comprehensive
Give Contractors a Complete Report and plan, and executed with diligent oversight by a professional mold prevention
Guidance consultant. Because just a small amount of water or moisture can lead to
Some owners and design professionals mistakenly believe they can make the development of severe mold infestations, a number of mold prevention
contractors liable for unanticipated subsurface conditions by limiting what strategies focus on keeping building surfaces dry. While groundwater, wa-
they provide for bid preparation. To help prevent costly problems, give con- ter infiltration, and similar issues may have been addressed as part of the
tractors the complete geotechnical engineering report, but preface it with a geotechnical engineering study whose findings are conveyed in-this report,
clearly written letter of transmittal. In that letter, advise contractors that the the geotechnical engineer in charge of this project is not a mold prevention
report was not prepared for purposes of bid development and that the reports consultant; none of the services performed in connection with
accuracy is limited; encourage them to confer with the geotechnical engineer the geotechnical engineers study were designed or conducted
who prepared the report (a modest fee may be required) and/or to conduct ad- for the purpose of mold prevention. Proper implementation of
ditional study to obtain the specific types of information they need or prefer. the recommendations conveyed in this report will not of itself
A prebid conference can also be valuable. Be sure contractors have sufficient be sufficient to prevent mold from growing in or on the struc-
time to perform additional study. Only then might you be in a position to give ture involved.
contractors the best information available to you, while requiring them to at
least share some of the financial responsibilities stemming from unantici- Rely on Your ASFE-Member Geotechnical
pated conditions. Engineer For Additional Assistance
Membership in ASFE/The Best People on Earth exposes geotechnical engi-
Read Responsibility Provisions Closely neers to a wide array of risk management techniques that can be of genuine
Some clients, design professionals, and contractors do not recognize that benefit for everyone involved with a construction project. Confer with your
geotechnical engineering is far less exact than other engineering disciplines. ASFE-member geotechnical engineer for more information.
This lack of understanding has created unrealistic expectations that have led
The Best People on Earth
8811 Colesville Road/Suite G106, Silver Spring, MD 20910

Telephone: 301/565-2733 Facsimile: 301/589-2017
e-mail: info@asfe.org www.asfe.org
Copyright 2004 by ASFE, Inc. Duplication, reproduction, or copying of this document, in whole or in part, by any means whatsoever, is strictly prohibited, except with ASFEs specific
written permission. Excerpting, quoting, or otherwise extracting wording from this document is permitted only with the express written permission of ASFE, and only for purposes
of scholarly research or book review. Only members of ASFE may use this document as a complement to or as an element of a geotechnical engineering report. Any other firm,
individual, or other entity that so uses this document without being anASFE member could be committing negligent or intentional (fraudulent) misrepresentation.
IIGER06045.0M

Second Soils Report Carolina Beach Lake

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Second Soils Report Carolina Beach Lake

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ECS Southeast, LLP

Geotechnical Engineering Report

Carolina Beach, New Hanover County, North Carolina

ECS Project Number # 22:25877

Mr. Gregory R. Thompson, PE, PLS

Reference: Geotechnical Engineering Report

Dear Mr. Thompson:

ECS Southeast, LLP

Mike Ellis, E.I. Winslow Goins, PE

EXECUTIVE SUMMARY .................................................................................................................. 1

Appendix A Drawings & Reports

Appendix B Laboratory Testing

Appendix C Supplemental Report Documents

The following tests were conducted on the soil samples:

1.2 SCOPE OF SERVICES

2.0 PROJECT INFORMATION

2.1 PROJECT LOCATION

Figure 2.1.1. Site Location

2.2 CURRENT SITE CONDITIONS

2.3 PROPOSED CONSTRUCTION

3.0 FIELD EXPLORATION

3.1 FIELD EXPLORATION PROGRAM

3.1.1 Vibracore Samples

3.1.2 Grab Samples

3.2 REGIONAL/SITE GEOLOGY

4.0 LABORATORY TESTING

5.0 SITE CONSTRUCTION RECOMMENDATIONS

Site Location Diagram

SITE LOCATION DIAGRAM

TPH GRO tests (SW-846 5030+8015)

Pace Analytical Services, LLC

LIMS USE: FR - FREDDIE WESCOTT

October 06, 2017

RE: Project: CB-Site 9/29

Dear Freddie Wescott:

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, LLC

Project: CB-Site 9/29

Charlotte Certification IDs

Asheville Certification IDs

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, LLC

SAMPLE ANALYTE COUNT

Project: CB-Site 9/29

92357321001 ZONE 1 EPA 8015 Modified NU1 2 PASI-C

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, LLC

SAMPLE ANALYTE COUNT

Project: CB-Site 9/29

EPA 8260 ZDO 70 PASI-C

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, LLC

Project: CB-Site 9/29

Lab Sample ID Client Sample ID

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, LLC

Project: CB-Site 9/29

Aldrin ND ug/kg 4.3 1 10/03/17 21:58 10/05/17 21:53 309-00-2

REPORT OF LABORATORY ANALYSIS

Pace Analytical Services, LLC

Project: CB-Site 9/29

Arsenic 2.1 mg/kg 1.5 1 09/30/17 19:10 10/03/17 18:25 7440-38-2

Mercury 0.013 mg/kg 0.0082 1 10/05/17 12:30 10/06/17 01:08 7439-97-6