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Accelerator Technology 1
TUP269 Proceedings of 2011 Particle Accelerator Conference, New York, NY, USA
by the manufacturer and must clearly correlate to each may demonstrate that UT is non-mandatory for RRR
aspect of the user specification. niobium e-beam welds.
Reference [3] provides useful guidance on creating this
specification Pressure Testing Requirements
SRF cavities do not use the test requirements for a
FABRICATION vacuum vessel because they must have a MAWP above
14.7 psi. Div. 2, Part 8.1.1(b) allows selecting pneumatic
Material Specifications testing over hydrostatic testing if the hydrostatic test
A suitable material specification must be created for could cause permanent visible distortion in the SRF
RRR niobium by the end user. All material tests should cavity. The cavity design must ensure that testing does
include at least two samples for each heat used in cavity not result in a permanent geometry change.
construction. Tensile testing (ASTM E8) should be
performed at each applicable material state (as received, ANALYSIS PARAMETERS
welded, and post bake-out). Testing and analysis can be
simplified by ordering the material in a fully annealed Material Mechanical Properties
state and returning it to that state after manufacturing. The literature shows a wide range of RRR niobium
The code imposes toughness testing for the mechanical properties [6,7]. Analysis should use
determination of the minimum design material minimum values based on the purchasing material
temperature (MDMT). For non-ferrous alloys Section specification. All analysis results should be checked
3.11.5 of Div. II, allows the MDMT to be based on against the actual material mechanical test results.
material testing that convinces the user of sufficient It is possible that the external surface of the cavity
ductility at its design temperaturesuch testing could receives a flaw during fabrication. It is suggested that a
include a Charpy V-notch impact test (ASTM E23), a fracture mechanics evaluation is used to calculate the
fracture toughness test (ASTM E399) and/or a tensile test allowable stress at 4.22 K using a conservative flaw
(ASTM E1450). size.
Welding Qualification Pressure Loads
All weld joints and welders must be qualified according The chosen MAWP must have margin above actual
to the provisions in Section IX of the code. This requires operating conditions in order to prevent accidental
qualifying welds and documenting the results in a triggering of pressure relief devices. Pressure relief has to
Procedure Qualification Report(s) (PQR). Each PQR coincide with the highest MAWP of the cavity. Therefore,
covers a small range of weld parameters. The PQRs in the cavity must be designed for the most severe
turn support a Welding Procedure Specification (WPS) conditions of concurrent loads and temperature.
that is associated with each weld. Weld design experience
is of paramount importance to the successful construction Manufacturing Complications
of an SRF cavityweld preparations affect the vessel SRF cavities go through a number of manufacturing
integrity and internal RF volume. processes. Analyses must take into account: (1) thickness
reduction due to buffered chemical polishing (BCP)
INSPECTION AND TESTING and/or electro-polishing, (2) Plastic strain induced by
initial tuning, (3) Annealing due to bake-out temperatures,
Inspection (4) Heat affected zones at welds, and (5) Tuner preload.
Div. 2 imposes 100% inspection criteria upon the
majority of welds. All electron beam welds are specified DESIGN BY ANALYSIS
to be 100% ultrasonically inspected in addition to visual The design by analysis requirements of Div. 2, Part 5
inspection (Div. 2, Part 7.4.3.3 (a)). However, inspection requires demonstrating protection against five failure
methods for SRF cavities may be limited by material mechanisms: plastic collapse, local plastic failure,
thickness and geometry. The thin curved structure of an buckling, fatigue, and ratcheting. For each failure
SRF cavity is a difficult geometry for ultrasonic mechanism, there is a choice to use at least one of three
inspection. Yet, a phased array ultrasonic system may be different material models: elastic, elastic-perfectly plastic,
capable of sufficient clarity and resolution. and elastic-plastic. The vessel needs to meet code criteria
Ultrasonic and radiographic inspections are equally for only one material model. It should be noted there are
capable of detecting volumetric flaws. However, cases were a vessel will not pass under all three models.
ultrasonic inspection is best suited for planar flaw
detection [5]. It is reasoned that the code presumes that Plastic Collapse and Buckling
electron beam welding results in higher incidents of Plastic collapse and buckling are highly related failure
planar flaws, but that may not be true for niobium welds mechanisms. In both cases, the goal is to determine
prepared and processed in clean room environments. A sufficient margin against structural instability. Buckling
thorough characterization of niobium e-beam weld flaws only applies under compressive stress conditions, whereas
2 Accelerator Technology
Proceedings of 2011 Particle Accelerator Conference, New York, NY, USA TUP269
plastic collapse can occur under tension or compression. The code provides a formulation for determining
These analyses, for an SRF cavity, must consider both forming strains but it does not account for a reversal in
stress stiffening (coupling of in plane displacements to curvaturesuch as in the forming of the iris. If peak
out of plane displacements) and applied tuner strains occur near the curvature of the iris, it is suggested
displacement. to perform a rigorous evaluation of the forming strains.
Fatigue and Ratcheting
OPERATIONAL CONSIDERATIONS
Fatigue cycles result from temperature excursions (2 K
Cavities may require a procedure for warm-up that
to 293 K) and tuner travel. The active tuner displacement
limits the coarse tuner displacement so that the niobium is
over the mean stress imposed by tuner preload is not
not yielded during transitions from 4.22 K to 293 K.
significant for continuous wave operation but could have
Additionally, cool-down must occur slowly in order to
an effect over the cavity life in pulsed configurations.
maintain a T 28oC across the cavity surface because
The allowable number of cycles for integral
the code allows temperature variations below 28oC to be
construction, which exempts a vessel from fatigue
ignored as a load contributing to a fatigue failure.
analysis, is 1000. The code addresses cyclic loads due to
pressure variations as well as both local and global
temperature changes. Additionally, displacement induced CONCLUSION
stress cycles, such as from tuner travel, are not The requirements of the ASME Boiler and Pressure
specifically addressed and must be considered. Vessel code provide a framework for designing safe and
A ratcheting analysis should always be performed when reliable equipment. Due to the uniqueness of addressing
yielding occurs due to cyclic loads. Plastic strains are SRF cavities as pressure vessels, an SRF community
typically developed during temperature transitions by committee could be formed to qualify niobium and
material CTE mismatchsuch as a cavity constrained in clearly address the unique aspects of SRF cavity pressure
a vertical test fixture and at stainless steel flanges. safety within the code.
As of the publishing of this paper, the analyses were
Local Plastic Failure completed which demonstrate that the SPL cavity design
The code requires evaluation for local plastic failure at meets the Div. II, Section VIII Design by Analysis
1.7*MAWP. However, plastic strain accumulates in the requirements during vertical testing.
cavity mostly due to initial forming and tuning. If the
manufacturing bakeout temperature is 800oC for 2 REFERENCES
hours it can be assumed that all forming and tuning
[1] ASME, 2007, 2008 & 2009 addenda, ASME Boiler and
strains are relieved. However, this means a reduction in Pressure Vessel Code, Section VIII Div. 2, ASME, New
strength for parts that did not begin annealed. The code York, NY
recommends using an elastic-plastic model instead of the [2] ASME, 2010, ASME Boiler and Pressure Vessel Code,
elastic evaluation. The use of an elastic-perfectly plastic Appendix 5 of Section II, Part D, Mandatory Appendix 5,
model is conservative for this analysis. Guideline on the Approval of New Materials under the
The strain limit criterion against plastic rupture is based ASME Boiler and Pressure Vessel Code, ASME, New
upon the triaxiality of stress, material crystal structure, York, NY.
uniaxial strain limit, and the strain hardening exponent. [3] T. Seipp and S. George, User's Design Specification
Recommendations for ASME Section VIII, Div. 2, ASME
The triaxiality of stress is presented as a simple equation;
Conf. Proc.,(2010).
however, the other variables require some discrimination [4] D. Osage and M. Prager, Technical Basis of Material
in their selection. The basis for the uniaxial strain limit in Toughness Requirements in the ASME B&PV Code,
order of accuracy is: percent area reduction at failure, Section VIII, Div. 2, ASME Conf. Proc. (2010)
percent elongation at failure, strain hardening exponent [5] Jack Spanner, Effectiveness of Substituting Ultrasonic
[8]. An evaluation of the uniaxial strain limit equations Testing for Radiographic Testing for Repair/Replacement
shows that reduction of area specified is the same ASME Conf. Proc. 2005, 33 (2005)
formulation for all material. If another uniaxial strain [6] T.J. Peterson, H.F. Carter, M.H. Foley, et. al., Pure
limit formulation is used the BCC crystal structure of Niobium as a Pressure Vessel Material, Advances in
Cryogenic Engineering: Transactions of the Cryogenic
niobium suggests using ones for aluminum or copper.
Engineering Conference, Vol. 55 (2010)
The strain hardening exponent (slope of the plastic stress- [7] Walsh, R.P. et al., "Low Temperature Tensile and Fracture
strain curve) as calculated from available data at room Toughness Properties of SCRF Cavity Structural Material",
temperature is ~0.2 (welded+formed) and ~0.3 SCRF99, Santa Fe, 1999.
(annealed). Those values should be used as a guideline [8] Wolf Reinhardt, Investigation of the Elastic-Plastic
since the material data does not meet ASME Design Method in Section VIII Div. 2 ASME Conf. Proc.
requirements. There is not adequate data for estimating 2009, 41 (2009)
the strain hardening exponent for 4.22 K.
Accelerator Technology 3