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Catalog Description:
Chemistry 405. Instrumental Analysis. 3-3-0 Prerequisite or co-requisite: Chemistry 306, co-requisite: Chemistry
407. A course in the theory and practice of modern instrumental methods of analysis, with emphasis on
spectrophotometric, chromatographic, mass spectrometric, and electrochemical methods of analysis. (40.0502)
H. Microcomputer Software
WEB SITES
http://www.cem.msu.edu/~cem333/LectureMenu.html SIMON GARRETT, MICHIGAN STATE USES OUR
TEXT BOOK. MANY OF SKOOG'S DIAGRAMS, ORGANIZED BY CHAPTER IN OUR BOOK, 2000
http://www.chemistry.msu.edu/courses/cem333/ GREAT SITE, USES OUR TEXT, HAS REVIEW SHEETS FOR
TESTS, NOTES ON EACH CHAPTER MICHIGAN STATE, PDF FILES Dr. Greg M. Swain, 2004
4. http://science.widener.edu/~svanbram/chem366/chem366.html GREAT SITE, WIDENER STATE, GREAT
LINKS i.e. S/N, T.C. O' HAVER, Problem Sets Sample Abstracts, Writing Guides, more
http://www.chemguide.co.uk/analysismenu.html#top EXCELLENT FOR ALL CHEMISTRY, 405 NMR, IR, MS
Course Goals:
The student should demonstrate knowledge of the basic concepts involved in the theory and practice of modern
instrumental analysis.
http://www.chemistry.org/portal/a/c/s/1/acsdisplay.html?DOC=education%5Ccpt%5Cts_anlchem.html
"This instrumental analysis course is part of a sequence of courses that also includes modern quantitative analytical
chemistry and presents an integrated view of the theories, chemical methods, and instrumental techniques for
solving a variety of real problems in chemical analysis. Students receive a coherent and progressive treatment of the
various aspects of problem definition, selection of analytical method, experimental design, and data collection and
evaluation. The problem-oriented role of chemical analysis is emphasized throughout the student's experience.
The student should emerge from this instrumental analysis course with the following competencies:
2 Understand comparison and critical selection of methods for elemental and molecular analyses
8 Understand theory and operational principles of analytical instruments including electronic components
11 Fundamental understanding of the principles of and instrumentation for atomic, molecular, and mass
spectrometry, magnetic resonance spectrometry, chromatography and other methods of separation, electroanalytical
methods, and thermal methods
12 Understand basic concepts of stoichiometry and basic chemical reactions involving analytes and ordinary
reagents
The La. State Grade Level Expectations (GLE) for Chemistry (Grades 11/12) covered in this course can be
found at http://www.doe.state.la.us/lde/ssa/1842.html#Chemistry
Course Content
The student is expected to master and apply the following concepts to problem solving:
Course Requirements:
Required reading: Assigned readings in textbooks and supplements
Graduate students taking this course for graduate credit are also required to do an oral presentation and write a
comprehensive paper (approximately 10 pages) based on an independent study.
Methods of Evaluation
Tests- Three (3) 80 minute tests - approximately every 5-6 weeks. 300 pts
Daily work (in class activities and writing assignments) 50 pts
Paper (graduate students only) 100 pts
Final exam, comprehensive standardized test 200 pts
Grading Scale: A 90-100%, B 90-80%, C 80-65%, D 65-50%, F below 50%
Late/Missed Assignments: No makeup exams. Late assignments are penalized one letter grade/day late.
Attendance Policy: Regular attendance is required.
Semester Withdrawls: The last day to withdraw form the class with a W is Friday March 30th, 2007.
NOTE This syllabus is not a contract and no part of it should be construed as such. The syllabus is subject to
change. Students will be notified of these changes in a timely manner.
Attachment: Scoring Rubric for Discussion Questions, Calendar
Scoring Rubric for Discussion Questions
Level of Achievement General Approach Comprehension
1. Addresses the question.
Exemplary 15. Demonstrates a clear
2. States a correct,
(3 pts) and complete
relevant, justifiable understanding of the
answer. question.
3. Presents arguments in a 16. Backs conclusions
logical order. with data and warrants
4. Uses acceptable style (justification).
and grammar (no errors) 17. Uses 2 or more ideas,
examples and/or arguments
that support the answer.
Adequate 5. Does not address the 18. Demonstrates only
(2 pts) question explicitly, adequate understanding of
although does so question because does not
tangentially. back conclusions with
6. States a correct, warrants and data.
relevant and justifiable 19. Uses only one idea to
answer. support the answer.
7. Presents arguments in a 20. Less thorough than
logical order. above.
8. Uses acceptable style
and grammar (one error).
Needs Improvement 9. Does not address the 21. Does not demonstrate
(1 pt) question. understanding of the
10. States no correct, question.
relevant answers 22. Does not provide
11. Indicates evidence to support their
misconceptions. answer to the question.
12. Is not clearly or
logically organized.
13. Fails to use acceptable
style and grammar (2 or
more errors).
No answer (0 pts) 14. No answer OR
illegible
21 X3 22 CH 14 23 X4 24 CH 11, 20 25
28 X4 3/1/2004 CH 2 X4 3 CH 20 4
20
7 Midsem (MS) 8 MS 3T MS 9 MS 6M MS 10 MS Ch 26 11 MS
4M MS X5 TEST 2 LAB MID
SEM
14 MS grades due 15 ch 26 15 x6 17 ch 27 18
X5
21 x7 22 ch 28 23 x7 24 ch 28 25
Easter
Break
28 29 30 31 1-Apr
11 X9 12 CH 17 13 X9 14 CH 19 15
18 X10 19 CH 19 20 X 11 21 EC 22
25 EC 26 TEST 4 27 LAB 28 Last Class 29
FINAL Day REVIEW
May 2 3 4 4M 5 6 3T
Finals begin Final 8-10 Final
am 8-10
9 Final 10 11 12 13
grades due
16 Spring
Semester
Ends
405 Ch
1 Intro
SECT II AT. SPEC.
6. Intro. Spec.
7. Comp. Opt. Inst.
8. Intro. Opt. At. Spec.
9. At. Abs.& At. Fluor.
10.At. Em.
12.At. X-Ray
TEST 1
SECT. III MOL. SPEC.
13. Intro. uv/vis Mol.Abs.
14. Ap. uv/vis Mol. Abs.
15. Mol. Luminescence
20&11 Mass Spec.
TEST 2
SECT. V SEP.METH.
26. Intro. Chrom. Sep.
27. GC
28. HPLC
TEST 3
16.Intro. Infrared (IR)
17. Appl. IR
19. NMR
SECT. IV EL.CHEM
22.
Intro
23. Potentiometry
24. Coulometry
25. Voltammetry
TEST 4