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ENVIRONMENTAL

SITE CHARACTERIZATION
REPORT
110 West Spruce Street, St. Charles, Michigan

PREPARED FOR Village of St. Charles


110 Spruce Street
St. Charles, Michigan 48655

PROJECT # 12716s

DATE December 21, 2017


Table of Contents

EXECUTIVE SUMMARY ....................................................................................................................... I

1.0 INTRODUCTION .........................................................................................................................1

2.0 SUBJECT PROPERTY OVERVIEW ..................................................................................................1


2.1 LOCATION AND LEGAL DISCRIPTION ....................................................................................... 1
2.2 VICINITY CHARACTERISTICS .................................................................................................... 1
2.3 DESCRIPTION OF STRUCUTURES AND OTHER IMPROVEMENTS............................................. 1
2.4 CURRENT USE OF THE SUBJECT PROPOERT ............................................................................ 2
2.5 UTILITIES AND MUNICIPAL SERVICES ...................................................................................... 2
2.6 CURRENT USES OF THE ADJOINING PROPERTIES ................................................................... 2

3.0 SUBJECT PROPERTY RECONNAISSANCE ......................................................................................3


3.1 METHODOLOGY AND LIMITING CONDITIONS ........................................................................ 3
3.2 GENERAL SUBJECT PROPERTY SETTING AND OPERATIONS .................................................... 3
3.3 RECONNAISSANCE OBSERVATIONS ......................................................................................... 4
3.3.1 Hazardous Substances and Petroleum Products .................................................... 4
3.3.2 Hazardous and Non-Hazardous Waste ................................................................... 4
3.3.3 Storage Tanks.......................................................................................................... 4
3.3.4 Unidentified Substances/Containers ...................................................................... 4
3.3.5 Potential Polychlorinated Biphenyl (PCB) Containing Electrical Equipment .......... 4
3.3.6 Interior Staining / Corrosion ................................................................................... 5
3.3.7 Drains and Sumps ................................................................................................... 5
3.3.8 Discharge Features ................................................................................................. 5
3.3.9 Pits, Ponds, and Lagoons ........................................................................................ 5
3.3.10 Solid Waste Dumping / Landfilling ......................................................................... 5
3.3.11 Stained Soil, Stressed Vegetation, Stained Pavement ............................................ 5
3.3.12 Well and Septic Systems ......................................................................................... 5
3.3.13 Material Issues of Non-Compliance ....................................................................... 6
3.3.14 Other Observations ................................................................................................ 6
3.3.15 Adjoining Properties ............................................................................................... 6

4.0 RECORDS REVIEW......................................................................................................................6


4.1 PHYSICAL SETTING SOURCES .................................................................................................. 6
4.2 STANDARD ENVIRONMENTAL RECORD SOURCES ................................................................... 8
4.2.1 Subject Property Listings ........................................................................................ 8
4.2.2 Adjoining Properties ............................................................................................... 8
4.2.3 Nearby Sites............................................................................................................ 9
4.3 ADDITIONAL ENVIRONMENTAL RECORD SOURCES ................................................................ 9
4.3.1 MDEQ Remediation and Redevelopment Division (RRD) ....................................... 9
4.3.2 Michigan Department of Licensing and Regulatory Affairs (LARA) ...................... 12

I
Table of Contents (continued)

4.3.3 Local Health Department ..................................................................................... 13


4.3.4 Local Fire Department .......................................................................................... 13
4.3.5 Assessing Department Records ............................................................................ 13
4.3.6 Building Department Records .............................................................................. 13
4.3.7 Other Historical Information ................................................................................ 13
4.4 OTHER RELEVANT ENVIRONMENTAL DOCUMENTS .............................................................. 13
4.5 HISTORICAL USE INFORMATION ........................................................................................... 13
4.5.1 Aerial Photographs ............................................................................................... 13
4.5.2 Fire Insurance Maps ............................................................................................. 14
4.5.3 City Directories ..................................................................................................... 14

5.0 CURRENT SITE EVALUATIONS ................................................................................................... 15


5.1 SUBSURFACE INVESTIGATION ............................................................................................... 15
5.2 SOIL AND GROUNDWATER ANALYTICAL RESULTS ................................................................. 15
5.2.1 Soil ........................................................................................................................ 15
5.2.2 Groundwater ........................................................................................................ 16
5.3 SUB-SLAB SOIL GAS AND INDOOR AIR ANALYTICAL MONITORING AND RESULTS ............... 16
5.3.1 Sub-Slab ................................................................................................................ 16
5.3.2 Indoor Air ............................................................................................................. 17
5.4 RADON ANALYTICAL RESULTS ............................................................................................... 17

6.0 CONCEPTUAL SITE MODEL ....................................................................................................... 17

7.0 SOIL EXPOSURE PATHWAY EVALUATION ................................................................................... 19

8.0 GROUNDWATER EXPOSURE PATHWAY EVALUATION ................................................................. 20

9.0 OPTIONAL TIER II EVALUATION................................................................................................. 21

10.0 SITE CLASSIFICATION ............................................................................................................... 21

11.0 WORKPLAN AND PROPOSED FOLLOW-UP ACTIVITES ................................................................ 21

12.0 CONCLUSIONS AND RECOMMENDATIONS ................................................................................ 23


12.1 CONCLUSIONS ....................................................................................................................... 23
12.2 RECOMMENDATIONS ............................................................................................................ 24

13.0 LIMITATIONS ........................................................................................................................... 24

14.0 SIGNATURES OF ENVIRONMENTAL PROFESSIONALS ................................................................. 24

II
Table of Contents (continued)

FIGURES
Figure 1 ................................................................................................................ Topographic Location Map
Figure 2 ........................................................................................................................ Sample Location Map
Figure 3 ........................................................................... Site Map with Soil Results Exceeding MDEQ NRCC
Figure 4 ........................................................... Site Map with Groundwater Results Exceeding MDEQ NRCC

TABLES
Table 1...................................................................................................... Summary of Soil Analytical Results
Table 2...................................................................................... Summary of Groundwater Analytical Results
Table 3.......................................................................Summary of Soil Gas – Site Specific Analytocal Results
Table 4........................................................................................... Summary of Inddor Air Analytical Results
Table Footnotes

APPENDICES
Appendix A ..................................................................................................................................Photographs
Appendix B ....................................................................................................................... Aerial Photographs
Appendix C ....................................................................................... Historical Fire Insurance Map Coverage
Appendix D ............................................................................................................................. Soil Boring Logs
Appendix B ........................................................................................................ Laboratory Analytical Report

III
ENVIRONMENTAL SITE CHARACTERIZATION
REPORT
110 West Spruce Street, St. Charles, Michigan
AKT Peerless Project No. 12716s

Executive Summary
AKT Peerless Environmental Services (AKT Peerless) conducted site characterization and investigation
activities for the non-residential property located at 110 West Spruce Street, St. Charles, Michigan. These
activities were conducted to determine the current site conditions related to the historic petroleum
release from an Underground Storage Tank (UST).

A review of historical data indicates no environmental concern associated with the Site, except for the
following:

• Village of St. Charles, 110 West Spruce Street is listed on the UST database. Two 1,000-gallon
gasoline USTs were installed on March 18, 1972, and March 19, 1975, respectively; and were
removed on May 26, 1992. One confirmed release of gasoline (C-0848-92) was reported on May
26, 1992, which remains open.

AKT Peerless reviewed historic data from previous investigations and conducted additional activities to
futher evaluate the nature and extent of the historic release. Results of the investigation indicated
impact above the MDEQ Part 213 Site Specific Non-Residential Soil Voliziation to Indoor Air Inhalation
Criteria and RBSLs criteria. Based on the findings of the additional sub-surface investigation, AKT
Peerless collected both sub-slab soil gas and the indoor air samples.

Analytical results for the sub-slab soil gas monitoring indicated all constiutants of concern were below
the site specific screening levels with the exception of Napthalene, which exceeds the Site-Specific
Non-Residential Criteria.

AKT Peerless also collected one indoor air sample from the interior of the building. Analytical results
indicated that all constituants of concern were reported as either non-detect or below the most
conseritive screening levels.

The results of the investigation indicated the presence of contamination in the soil, soil vapor, and
groundwater in exceedance of the MDEQ Part 201 and Part 213 Generic Non-Residential Cleanup
Criteria soley attributable to the open release.

AKT Peerless recommendiations include the following:

• Futher delineation of the soil and groundwater impact;


• Evaluate groundwater and soil characteristics;
• Futher evaluate potential exposure pathways; and
• Establish the appropriate cleanup objectives and the most feasible corrective actions to support
the closure of the release and remediate the source of the vapor intrusion pathway.

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page I


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
1.0 Introduction
The Village of St. Charles retained AKT Peerless Environmental Services (AKT Peerless) to conduct site
investigation activities for a commercial property located at 110 West Spruce Street, St. Charles,
Michigan (subject property). The purpose of site investigation activites is to determine current site
conditions relative to a historical release of petroleum hydrocarbons from a previously removed (1992)
underground storage tank (UST) system. Furthermore, site investigation activities also including a
historical site assessment to evaluate for other potential sources of contamination at the subject
property.

As a result of site investigation activities, AKT Peerless prepared this Environmental Site Characterization
Report of the subject property, which documents the historic site conditions, field activities, sampling
protocols, and laboratory results conducted as part of this assessment. This Environmental Site
Characterization Report was performed for the benefit of Village of St. Charles, who may rely on the
contents and conclusions of this report.

2.0 Subject Property Overview

2.1 Location and Legal Discription


The subject property is located in the northeast ¼ of the southwest ¼ of Section 5 in St. Charles (T10N,
R03E), Saginaw County, Michigan. The subject property is located on the north side of West Spruce Street.
See the following table for additional subject property details:

Subject Property Identifiers

Address Tax Identification Number Owner of Record Approximate Acreage

110 West Spruce Street 24-10-3-05-0330-700 Village of St. Charles Approximately 0.42 acres

Refer to Figure 1 for a topographic site location map. See Figure 2 for a sample location map.

2.2 Vicinity Characteristics


The subject property is currently zoned exempt (701) and is located in an area of St. Charles, Michigan that
is characterized by residential properties, surface roadways, municipal sewage and water, as well as
electrical and gas utilities.

2.3 Description of Strucutures and Other Improvements


General information regarding the on-site building is presented in the following table:

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page 1


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
Subject Building: 110 West Spruce Street

General Construction 1-story, gable roof, concrete and steel frame, concrete block and brick exterior,
concrete slab on grade foundation, no basement

Interior Finish Concrete, acoustical ceiling tiles, vinyl floor tiles, paint, wood, drywall, metal, glass,
carpet

Square Footage Approximately 6,420 square feet


(floor plan)

Construction and Other Constructed in the 1970s


Improvement Dates

Interior Operations Office spaces and garage areas with three overhead doors

The exterior of the subject property consists of an asphalt paved parking lot and landscaped areas.
2.4
2.4 Current Use of the Subject Property
The subject property is currently used as the Village of St. Charles administrative offices and police substation.

2.5 Utilities and Municipal Services


AKT Peerless identified the type and supplier of utilities provided to the subject property. These services
are described in the following table:

Subject Property Utility Data

Utility / Service Type Utility Company or Municipality

Heat Natural Gas Consumers Energy, connected 1972

Potable water Municipal Village of St. Charles

Electricity Electric lines Consumers Energy

Sewage disposal Municipal Village of St. Charles

Storm water County Saginaw County

2.6 Current Uses of the Adjoining Properties


The following table describes the current uses and/or occupants of the adjoining properties.

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page 2


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
Adjoining Property Data

Direction Address Current Use / Occupant

North 520 Cherry Street Residential

131 West Maple Street Residential

121 West Maple Street Residential

Northeast 100 Maple Street Tri-Township Fire Department

East 106 Spruce Street Tri-Township Fire Department

Southeast 109 West Spruce Street Residential

South 113 West Spruce Street Residential

117 West Spruce Street Residential

Southwest 203 West Spruce Street Residential

West 206 West Spruce Street Residential

3.0 Subject Property Reconnaissance

3.1 Methodology and Limiting Conditions


The subject property reconnaissance consisted of visual and physical observations of the subject property
and the periphery of the subject property. In addition, AKT Peerless observed the subject property from all
adjacent public thoroughfares. AKT Peerless viewed the subject property following a grid pattern
designed to cover representative portions of the unimproved areas.

Ms. Jacquelyn Luta of AKT Peerless conducted the subject property reconnaissance on August 17, 2017. AKT
Peerless did not encounter any project specific facts or conditions that limited our ability to access the
subject property.

Photographs taken during AKT Peerless’ subject property reconnaissance are provided in Appendix A.

3.2 General Subject Property Setting and Operations


The subject property consists of an office building, paved parking areas, and landscaped areas. The
subject building is utilized by the Village of St. Charles for administrative offices and a police substation.

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page 3


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
3.3 Reconnaissance Observations

3.3.1 Hazardous Substances and Petroleum Products


AKT Peerless did not observe hazardous substances or petroleum products at the subject property, except
for the following:

Hazardous Substances and Petroleum Products

Use/Location Material Quantity Observations

Storage area of Cleaning supplies 1-quart to 5-gallon The materials are stored within
subject building containers manufactures packaging on shelves. No
evidence of a release was observed.

3.3.2 Hazardous and Non-Hazardous Waste


AKT Peerless did not observe hazardous or non‐hazardous waste at the subject property, except for general
refuse stored within an on-site dumpster. No evidence of improper waste disposal was observed.

3.3.3 Storage Tanks


AKT Peerless did not observe evidence of any current UST systems (e.g., vent pipes, fill ports, dispensing
pumps, patched pavement, etc.) at the subject property.

AKT Peerless did not observe evidence of current aboveground storage tank (AST) systems (e.g., stands,
secondary containments, etc.) at the subject property.

3.3.4 Unidentified Substances/Containers


AKT Peerless did not observe evidence of unidentified substances or other suspect containers on the
subject property.

3.3.5 Potential Polychlorinated Biphenyl (PCB) Containing Electrical Equipment


AKT Peerless inspected the subject property for the presence of liquid-cooled electrical units such as
transformers and large capacitors. Such units are notable since they may be potential sources of PCBs.
AKT Peerless did not observe suspect PCB-containing equipment at the subject property, except for the
following:

Potential PCB-Containing Electrical Equipment

Source Description Source Location Responsibility Observations

Two pole-mounted Southeastern portion of subject Consumers Energy No evidence of a release


transformers property exterior

AKT Peerless observed two pole-mounted transformers on the northern portion of the subject property.
The transformers are the responsibility of Consumers Energy. In the event of a release incident,
Consumers Energy will repair the damaged or leaking electrical unit(s), and return the quality of the

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
affected soil and groundwater, if any, to its pre-release condition. AKT Peerless did not observe evidence
or indication of oil stains, leaks, or spills near the transformers.

3.3.6 Interior Staining / Corrosion


AKT Peerless did not observe interior staining or corrosion at the subject property.

3.3.7 Drains and Sumps


AKT Peerless did not observe drains or sumps at the subject property, except for the following:

Drains and Sumps

Description Location Observed Environmental Concerns

Floor drain Hallway along northern side of subject building None

Floor drains Two in garage located in the northeastern portion of None


the subject building

Sump Evidence room None

The floor drains led to the sump in the evidence room. No staining or odors were observed near the
floor drains. It is assumed that the drains discharge to the municipal sanitary sewer; however, this could
not be confirmed.

3.3.8 Discharge Features


Storm water that falls upon the subject property appears to evaporate, percolate directly into the ground
to discharge to storm water drains located within the parking lot of the subject property.

3.3.9 Pits, Ponds, and Lagoons


AKT Peerless did not observe pits, ponds, or lagoons at the subject property.

3.3.10 Solid Waste Dumping / Landfilling


AKT Peerless did not observe evidence of solid waste dumping or landfilling at the subject property.

3.3.11 Stained Soil, Stressed Vegetation, Stained Pavement


AKT Peerless did not observe any evidence of stained soil, stressed vegetation, or stained pavement at
the subject property.

3.3.12 Well and Septic Systems


AKT Peerless did not observe physical evidence or indication of wells or septic systems at the subject
property, with the exception of seven monitoring wells located throughout the parking lot of the subject
property and the northern adjoining property.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
3.3.13 Material Issues of Non-Compliance
Although AKT Peerless provides comments on obvious significant instances of non-compliance observed
in the course of performing its review, which could reasonably be expected to impair the value of the
subject property or result in a significant financial liability for the owner/operator of the site (i.e., non-
permitted discharges, over-accumulation of hazardous wastes by a small quantity geberator (SQG),
unregistered USTs, etc.), an environmental compliance audit or determination if the facility is in
compliance with all applicable regulations was not completed. Furthermore, an environmental
compliance inspection by a regulatory authority could reveal instances of non-compliance and/or
compliance deficiencies.

3.3.14 Other Observations


AKT Peerless did not observe obvious evidence of other potential environmental concerns at the subject
property.

3.3.15 Adjoining Properties


Based on AKT Peerless’ visual observations, the current uses of the adjoining properties do not appear to
pose an environmental concern to the subject property.

4.0 Records Review


The objective of the records review is to evaluate reasonably ascertainable databases, historical records,
and physical setting records to help identify environmental concerns at the subject property and, to the
extent identifiable, at surrounding properties.

4.1 Physical Setting Sources


AKT Peerless reviewed various available physical setting sources about the geologic, hydrogeologic,
hydrologic, and topographic characteristics that may affect potential contaminant migration to the
subject property, or within or from the subject property. The results of AKT Peerless' review are
presented in the following table:

Physical Setting Data

Physical Setting Information Data Sources

General Topography and Hydrogeology

Subject Property 590 feet above the National Geodetic Vertical Datum USGS’ Topographic Map of the
Elevation St. Charles Quadrangle (revised
1984)
Topographic Gradient Mostly flat

Closest Surface Water South Fork Bad River located approximately 558
feet south of the subject property.

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page 6


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
General Soil and Geology

Bedrock Saginaw Formation Unit of an unassigned group, MDNR Geological Survey


which is included in the Pottsville Series within the Division’s Bedrock Geology of
Pennsylvanian System of the Paleozoic Era. Southern Michigan (1987)

Quaternary Soils Lacustrine sand and gravel, described as pale Michigan Geological Survey
Description brown to pale reddish brown, fine to medium Division’s publication,
sand, commonly including beds or lenses of small Quaternary Geology of
gravel, chiefly quartz sand but gravel is rich in Southern Michigan (1982)
igneous and metamorphic rocks. These soils occur
chiefly as former beach and near-offshore littoral
deposits of glacial Great Lakes and may include
intercalated lacustrine clay. Locally veneered by
discontinuous sheets or small dunes of eolian
sand and may include areas of organic soils. In the
eastern part of the northern peninsula of
Michigan these sands commonly grade upstream
(north- or northwest- ward) into outwash
deposits. Soil thickness ranges from 3 to 100 feet.
Typically, lacustrine sand and gravel are
associated with moderate hydraulic permeability
and may allow the movement of contaminants
through groundwater.
County Soil Survey The soil at the subject property is classified as the USDA Soil Survey of Saginaw
Description Parkhill-Wixom Association, which is described as County, Michigan (1994)
nearly level and gently undulating, poorly drained
and somewhat poorly drained, loamy and sandy
soils on water-worked till plains.

Site‐Specific Geology and Hydrogeology

Physical Setting Information Data Sources

Soil and bedrock Fill to approximately 1.5’ below ground surface Expanded Triage Program Limited
characteristics (bgs), sand to approximately 2’ bgs, and clay to Site Investigation, Mannik Smith
approximately 15’ bgs Group, August 2014

Groundwater Approximately 5’ bgs 60-Day Initial Assessment Report,


characteristics CTI and Associates, February 1994

Based on the information presented above, AKT Peerless infers that groundwater in the vicinity of the
subject property flows toward the south, with potential influence from the South Fork Bad River. However,
local manmade structures (e.g., buildings, roads, sewer systems, and utility service lines) may influence
both surface water and groundwater flow. AKT Peerless was unable to precisely document the
groundwater flow direction beneath the subject property. To determine the site‐specific groundwater
flow direction, subsurface information would be necessary.

AKT Peerless did not identify any water supply wells at the subject property. Groundwater from the area of
the subject property does not serve as the primary drinking water source for properties in the Village of St.
Charles, which obtains its municipal water from Lake Huron.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
4.2 Standard Environmental Record Sources
AKT Peerless retained a third-party vendor to provide current environmental database information
compiled by a variety of federal and state regulatory agencies. The purpose of obtaining this data was to
evaluate potential environmental risks associated with the subject property, adjoining properties, and
nearby sites that are: (1) identified on target lists and (2) within varying distances of up to one mile from
the subject property.

4.2.1 Subject Property Listings


The database report does not identify the subject property on the referenced databases, except for the
following:

• Village of St. Charles, 110 West Spruce Street is listed on the UST database. Two 1,000-gallon
gasoline USTs were installed on March 18, 1972, and March 19, 1975, respectively; and were
removed on May 26, 1992. One confirmed release of gasoline (C-0848-92) was reported on May
26, 1992, which remains open.
• Village of St. Charles, 110 West Spruce Street is listed on the Waste database. No hazardous
waste violations or enforcement actions were reported.

4.2.2 Adjoining Properties


The database report does not identify any adjoining properties on the referenced databases, except for
the following:

Detail Table for Eastern Adjoining Property (106 West Spruce Street)

Known/Inferred Groundwater
Address Name Distance/Direction
Flow Direction:

106 West Spruce Street Tri Twp Fire District Adjoining/east Inferred south

Databases

LUST
One confirmed release (C-2470-91) of an unreported substance was reported on November 19, 1991, which was
granted closure by the MDEQ on April 21, 1994.

Resource Conservation and Recovery Act (RCRA) Non Generator (NonGen)


Waste
The eastern adjoining property was listed in the RCRA NonGen and waste databases (MID985629617). No
hazardous waste violations or enforcement actions associated with this database listing were reported.

UST
One 500-gallon gasoline UST was installed on April 16, 1976, and removed on November 19, 1991. A confirmed
release (C-2470-91) of an unreported substance was reported on November 19, 1991, which was granted
closure by the MDEQ on April 21, 1994.

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page 8


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
4.2.3 Nearby Sites
AKT Peerless’ review of the referenced databases also considered the potential or likelihood of
contamination from nearby sites. To evaluate which of the nearby sites identified in the database report
present an environmental risk to the subject property, AKT Peerless considered the following criteria:

• Type of database on which the site is identified.


• Topographic position of the identified site relative to the subject property.
• Direction and distance of the identified site from the subject property.
• Local soil conditions in the subject property area.
• Known or inferred groundwater flow direction in the subject property area.
• Status of the respective regulatory agency‐required investigation(s) of the identified site, if any.
• Surface and subsurface obstructions and diversions (e.g., buildings, roads, sewer systems, utility
service lines, rivers, lakes, and ditches) located between the identified site and the subject
property.

Only those nearby sites that are judged to present a potential environmental risk to the subject property
are further evaluated by reviewing agency file information. Using the above criteria, and based upon a
review of readily available information contained within the database report, AKT Peerless did not
identify nearby sites that present a potential environmental risk to the subject property.

4.3 Additional Environmental Record Sources

4.3.1 MDEQ Remediation and Redevelopment Division (RRD)


AKT Peerless reviewed the MDEQ RRD Perfected Lien List, dated July 25, 2017, to determine if
environmental cleanup liens had been filed against the subject property.

AKT Peerless also referenced the MDEQ Storage Tank Information Database (SID) for information
regarding the subject property and the adjoining property to the east.

In addition, AKT Peerless submitted a request to the MDEQ RRD to review available file information
regarding USTs, LUSTs, or other environmental records pertaining to the subject property and the
adjoining property to the east.

Subject Property

According to the Perfected Lien List, the MDEQ does not have record of environmental cleanup liens filed
against the subject property.

According to the SID, the following USTs are registered to the subject property:

Subject Property MDEQ RRD UST Details

Tank ID Installation Date Tank Contents Tank Capacity Removal Date* Tank Status

1 03/18/1972 Gasoline 1,000 gallons Unknown Removed

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page 9


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
Tank ID Installation Date Tank Contents Tank Capacity Removal Date* Tank Status

2 03/19/1975 Gasoline 1,000 gallons Unknown Removed

* Removal dates for USTs are not specified on the SID database.

The following file information was obtained from the MDEQ RRD pertaining to the subject property:

• 20-Day Initial Abatement Measures Report, prepared by CTI and Associates, June 9, 1992
• 45-Day Report, Prepared by CTI and Associates, July 8, 1992
• Free Product Removal Report, prepared by CTI and Associates, July 8, 1992
• Remedial Investigation Work Plan, prepared by CTI and Associates, July 8, 1992
• Site Characterization, prepared by CTI and Associates, July 8, 1992
• 60-Day Initial Assessment Report, prepared by CTI and Associates, February 21, 1994
• Phase I Hydrogeological Study Report/Phase II Hydrogeological Work Plan, prepared by CTI and
Associates, May 24, 1994
• Revised Phase II Hydrogeological Study Work Plan, prepared by RC Engineering, September 9,
1994
• Revised Phase II Hydrogeological Study Work Plan, prepared by RC Associates, September 30,
1994
• Additional Phase II Hydrogeological Investigation Work Plan, prepared by RC Associates, March
31, 1995
• Interim Phase II Hydrogeological Study, prepared by RC Engineering, March 31, 1995
• Additional Phase II Hydrogeological Investigation Report, prepared by RC Associates, June 30,
1995
• Vapor Intrusion and Indoor Air Investigation 2013 4th Quarter, prepared by Superior
Environmental, October 31, 2013
• Expanded Triage Program Limited Site Investigation, prepared by Mannik Smith Group, August 8,
2014

The above-listed reports were prepared to address a confirmed release of gasoline reported on May 26,
1992, during the removal of two 1,000-gallon gasoline USTs. During removal of the USTs, stained soil,
odors, and free product were observed. A total of twelve soil samples were collected from the two
excavation cavities. The samples were submitted for the analysis of benzene, toluene, ethylbenzene, and
xylenes (BTEX, collectively) and total lead. The analytical results indicated that BTEX and lead were
present along the sidewalls and bottom of the excavation cavities. Approximately, 96 cubic yards of
contaminated soil were disposed of at a licensed landfill.

During a subsequent investigation in April 1994, four soil borings were advanced, with the collection of
twelve soil samples for the analysis of BTEX and total lead. The four soil borings were converted to
monitoring wells. Three of the soil samples were detected for benzene at levels greater than the MDEQ
Type B Cleanup Standards. Four groundwater samples were collected for the analysis of BTEX and
dissolved lead. Two of the groundwater samples were detected for benzene, ethylbenzene, and xylenes
at levels greater than the MDEQ Type B Cleanup Standards.

In October 1994, eight soil borings were advanced and eight soil samples were collected for laboratory
analysis. Groundwater was collected from the eight borings. In addition, samples were collected from

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
five existing groundwater monitoring wells. Soil and groundwater samples were submitted for the
analysis of BTEX and total/dissolved lead. According to laboratory results, lead was detected in one
groundwater sample above the MDEQ Type B Cleanup Criteria, and benzene was detected in three of the
existing groundwater monitoring wells at levels, which exceed the MDEQ Type B Cleanup Criteria.

In May 1995, nine soil borings were advanced and eight soil samples were collected for laboratory
analysis. Groundwater was collected from the nine soil borings. Additional groundwater samples were
collected from four existing groundwater wells. The soil and groundwater samples were submitted for
analysis of BTEX and lead. Two soil samples and five groundwater samples reported detections of BTEX
compounds greater than the MDEQ Type B Cleanup Criteria.

During the July 2014 investigation, ten soil borings were advanced, with the collection of ten soil samples
for the analysis of volatile organic carbons (VOCs). Groundwater was collected from existing monitoring
wells. According to laboratory results, benzene, ethylbenzene, 2-methylnaphthalene, naphthalene,
toluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and xylenes were detected in soil samples
greater than the MDEQ Residential Tier 1 Drinking Water Protection Criteria, Groundwater Surface Water
Interface Protection Criteria, Direct Contact Criteria, and/or Soil Volatilization to Air Criteria. According to
laboratory results, benzene, ethylbenzene, 1,2,4-trimethylbenzene, and xylenes were detected in three
groundwater samples greater than the MDEQ Part 213 Residential Tier 1 Risk-Based Screening Levels
(RBSLs). Based on laboratory analytical results, the subject property meets the definition of a facility1, as
defined in Part 201 of the NREPA, Michigan Public Act (PA) 451, 1994, as amended.

As a result of the previously completed subsurface investigations, vapor intrusion and indoor air
investigations were conducted in January, April, July, and October 2016. The purpose of these sampling
activities was to evaluate for the presence of adverse indoor air quality conditions relative to the
presence of soil and groundwater contamination identified at the subject property. The sample results
were either not detected above the laboratory’s method detection limits or were detected below the
MDEQ Nonresidential Indoor Air Criteria for Vapor Intrusion.

Adjoining Properties

The adjoining properties were not identified on the MDEQ SID, except for the following:

Tri Twp Fire District, 106 West Spruce Street (eastern adjoining property)
According to the SID, the following USTs are registered to the eastern adjoining property:

Adjoining Properties MDEQ RRD UST Details

Tank ID Installation Date Tank Contents Tank Capacity Removal Date* Tank Status

1 04/16/1976 Gasoline 500 gallons Unknown Removed

*Removal dates for USTs are not specified on the SID database.

1
"Facility" means any area, place, or property where a hazardous substance in excess of the concentrations that
satisfy the cleanup criteria for unrestricted residential use has been released, deposited, disposed of, or otherwise
comes to be located.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
A confirmed release of gasoline (C-2470-91) was reported on November 19, 1991, which was granted
Type B closure by the MDEQ on April 21, 1994.

The following file information was obtained from the MDEQ RRD pertaining to the adjoining property to
the east:

Correspondence and Closure Summary for Tri Twp Fire Department, completed by Bierlein
Environmental, December 1991
On November 19, 1991, Bierlien Environmental removed a 500-gallon gasoline UST from the eastern
adjoining property. Photoionization readings at the time of excavation indicated soil contamination and a
confirmed release of gasoline (C-2470-91) was reported on November 19, 1991. Six soil samples were
collected from the excavation cavity and submitted for the analysis of BTEX, MTBE, and total lead.
Groundwater was not encountered in the excavation cavity. Based on laboratory results, further
excavation was conducted and an additional soil sample was collected and submitted for BTEX, methyl
tert-butyl ether (MTBE), and total lead. Laboratory analytical results were not detected or were detected
at levels less than MDEQ Type B Closure Criteria. A total of 57 cubic yards of contaminated soil were
removed and disposed of at a licensed facility. The MDEQ granted closure on April 21, 1994.

In AKT Peerless’ opinion, the eastern adjoining property does not present an environmental concern to
the subject property because: (1) the LUST incident was remediated and granted closure by the MDEQ
and (2) inferred groundwater flow is to the south.

4.3.2 Michigan Department of Licensing and Regulatory Affairs (LARA)


AKT Peerless contacted LARA’s Storage Tank Division (STD) to review available records regarding
registered storage tanks associated with the subject property and adjoining properties.

Subject Property

LARA provided AKT Peerless with UST registration and removal records for the subject property.
According to these records two 1,000-gallon gasoline USTs were formerly located on the northeast
portion of the subject property. These USTs were removed in May 1992. A confirmed release of gasoline
(C-0848-92) was reported on May 26, 1992, based on stained soil and odors.

Adjoining Properties

According to a response received, LARA STD does not have registered storage tank files for the adjoining
properties, except for the following:

Tri Twp Fire Department, 106 West Spruce street (eastern adjoining property)

LARA provided AKT Peerless with records for the eastern adjoining property. According to these records
a 500-gallon gasoline UST was formerly located on the southeast portion of this property. This UST was
removed in November 1991. A confirmed release of gasoline was reported on November 19, 1991,
based on odors.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
4.3.3 Local Health Department
AKT Peerless requested file information from the Saginaw County Health Department on August 29, 2017.
AKT received a response on September 1, 2017 dening the request because information associated with the
questionnaire did not exist.

4.3.4 Local Fire Department


The Tri Township Fire Department indicated knowledge of former USTs on site that were removed in 1991. No
other information regarding environmental concerns were identified.

4.3.5 Assessing Department Records


According to the Village of St. Charles Assessing Department, the parcel is an exempt government-owned parcel
and no records of the subject building’s construction were on file. According to previous environmental reports
described in Section 6.3.1, the subject building construction date is estimated to be in the 1970s.

4.3.6 Building Department Records


AKT Peerless requested building records for the subject property from the Village of St. Charles Building
Department. The building department indicated they did not have any records for the subject property.

4.3.7 Other Historical Information


AKT Peerless did not identify any other relevant historical information for the subject property.

4.4 Other Relevant Environmental Documents


The Village of St. Charles did not provide any other relevant environmental documents regarding the
environmental condition of the subject property, other than previously discussed.

4.5 Historical Use Information


The objective of reviewing historical sources is to develop a history of previous uses or specific
occupancies of the subject property, if possible, based on a limited historical use review.

4.5.1 Aerial Photographs


AKT Peerless obtained aerial photographs for the subject property from Environmental Data Resources
(EDR). AKT Peerless’ observations noted during the review of these photographs are summarized in the
following table. Photocopies of select aerial photographs are presented as Appendix B.

Subject Property Aerial Photography Summary

Photograph Observations Potential Environmental


Dates (Subject Property) Concerns

1937, 1941, The subject property appears to be undeveloped and not utilized None observed
1950, 1963, for any discernable purpose.
1970

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
Photograph Observations Potential Environmental
Dates (Subject Property) Concerns

1980, 1992, The subject property appears to be developed with the subject None observed
1997, 1998, building and a parking lot, consistent with current conditions.
2005, 2006

AKT Peerless’ review of historical aerial photographs of the adjoining properties is summarized in the
following table.

Adjoining Property Aerial Photography Summary

Photograph Potential Environmental Concerns


Dates (Adjoining Properties)

1937-2006 No obvious evidence or indications of environmental concerns were noted with respect to the
adjoining properties and nearby sites during AKT Peerless’ review of the referenced aerial
photographs.

4.5.2 Fire Insurance Maps


AKT Peerless’ research did not identify historical fire insurance map coverage of the subject property or
adjoining properties. A copy of the “No Coverage” statement provided by EDR is presented in Appendix
C.

4.5.3 City Directories


City Directories from various years between 1993 through 2016 were obtained from Environmental Risk
Information Services (ERIS). The purpose of this review was to determine the past occupancy of the subject
property. Directories were reviewed in approximately 5‐year intervals, or as available. Information
obtained from the reviewed directories is summarized in the following table:

City Directories Data

Year Address Listing


1993 110 West Spruce Street St. Charles Public Works Department

1998 110 West Spruce Street St. Charles Public Works Department, St. Charles Village Office, St.
Charles Police Department, St. Charles Chamber of Commerce
2001-2016 110 West Spruce Street St. Charles Public Works Department, St. Charles Village Office, St.
Charles Police Department

AKT Peerless also reviewed City Directories for select adjoining properties to determine their past
occupancy. No obvious or potential environmental concerns associated with historical occupants of the
adjoining properties were noted.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
5.0 Current Site Evaluations
In July 2017, AKT Peerless was contacted by the Client to evaluate historical data generated during
previous subsurface investigations in an effort to develop a scope of work to continue ongoing
monitoring of sub-slab and indoor air conditions. In addition to this evaluation, AKT Peerless proposed to
conduct other corrective actions as described in the following sections to evaluate the current nature
and extent of the historical petroleum release.

For the purpose of this assessment, AKT Peerless considerd laboratory analytical results obtained during
the 2014 and 2015 subsurface investigations as relevant and reliable. Therefore, these results are
depicted on the provided figures and included in the tables for comparison to MDEQ criteria.

5.1 Subsurface Investigation


To futher evlaute the nature and extent of the historical release, AKT Peerless conducted additional
subsurface investigation. Specifically, on August 22, 2017, AKT Peerless conducted a subsurface
investigation at the subject property that included the: 1) advancement of four soil borings (AKT-101,
AKT-102, AKT-103, and AKT-104), 2) installation of one temporary monitoring well, and 3) the collection
of soil and groundwater samples for laboratory analyses. Soil and groundwater samples were submitted
for laboratory analyses of VOCs.

See Appendix D for AKT Peerless’ soil boring logs.

5.2 Soil and Groundwater Analytical Results


AKT Peerless collected soil and groundwater samples for the purpose of evaluating the current nature
and extent of contamination at the site. Analytical results were compared with MDEQ Part 213
Nonresidential Cleanup Criteria (NRCC) provided in MDEQ Remediation and Redevelopment Division’s
Operational Memorandum No. 1, Tables 1 and 2. NRCC was selected based on the zoning and operation
of the site. Analytical data obtained from soil borings that were located offsite are compared to
Residential Cleanup Criteria (RCC) to appropriately characterize potential exposures at these locations.

As discussed in Section 4.3.1, previous investigations conducted at the site included the advancement of
eighteen soil borings and the installation of eight monitoring wells. Refer to Figures 2, 3, and 4 for
current and historical sample locations. Laboratory analytical results compared to Part 201 from the
2014 and 2015 subsurface investigations can be found in Tables 1 and 2.

5.2.1 Soil
AKT Peerless submitted seven soil samples, collected during the August 22, 2017 investigation activities
to Fibertec Environmental Services (Fibertec) analytical laboratory for analysis of VOCs. Soil analytical
results evidenced exceendances above Residential Drinking Water Protection Criteria and Risk Based
Screening Levels in three of the seven submitted soils samples. A site map depicting the locations and
analytical results of the soil analysis has been provided as Figure 3.

The following table summarizes the location, depth, matrix, and laboratory analysis for each sample.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
Soil Sample Collection Summary

Sample Location Sample Matrix Soil Sample Interval (feet, bgs) Laboratory Analytical Parameter(s)

AKT-101 Soil 0.5-1.5 VOCs


5.5-6.5
8.5-9.5
AKT-102 Soil 7.5-8.5 VOCs
AKT-103 Soil 1.5-2.5 VOCs
7.5-8.5
AKT-104 Soil 7-8 VOCs

The laboratory analyzed the samples for VOCs in accordance with USEPA Method 8260B

5.2.2 Groundwater
A groundwater sample was collected from one temporary well, installed at boring AKT-103 during
advancement. The samples was preserved in the field using hydrochloric acid and submitted for
laboratory analysis of VOC to Fibertec in Holt, Michigan for laboratory analysis. The sample was analyzed
using USEPA Methods 8260B/5035 for VOCs.

Refer to Tables 1 and 2 for a summary of soil and groundwater analytical results, respectively. Refer to
Appendix E for a complete analytical laboratory report.

5.3 Sub-Slab Soil Gas and Indoor Air Analytical Monitoring and Results

5.3.1 Sub-Slab
As discussed in Section 5.0, sub-slab soil vapor was historically evaluated utilizing one soil vapor pin (SEC-
VI-1). To further evaluate sub-slab soil vapor conditions AKT Peerless installed seven sub-slab vapor
monitoring pins, spaced equally throughout the building. The location of the monitoring points are
depicted on Figure 3.

On August 17, 2017, AKT Peerless collected seven sub-slab vapor samples from the monitoring pins
installed on August 15, 2017. The existing pin (SEC VI-1) was damaged and no sample was collected. The
seven sub-slab samples were collected in pre-cleaned Bottlevacs provided by Fibertec. The collected
samples were submitted to Fibertec for analysis of VOCs using TO-15 analytical methodology.

Laboratory analytical results indicated concentrations of Dichlorodifluoromethane were present in all


seven submitted samples, Tetrachloroethylene was detected in AKTVI-2, and Trichlorofluoromethane
was detected in three samples (AKTVI-2, AKTVI-4 and, AKTVI-5). To appropriately assess this exposure
pathway, AKT Peerless requested the calculation of site specific screening levels from MDEQ Toxicology.
Consequently, AKT Peerless has compared all sub-slab soil gas concentrations to the site specific
screening levels (TIASL12) as provided by MDEQ Toxicology. Based on this comparison, all detected
concentrations of VOCs were reported below the site specific screening levels. Refer to Table 3 for a
comparison of results to screening levels.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
On November 28, 2017, AKT Peerless returned to the site to conduct additional assessment activities
with respect to vapor intrusion. AKT Peerless utilized the existing seven sub-slab soil vapor monitoing
points and installed one additional point (AKT-VI-9) to replace the damaged historical point (SEC-VI-1).
As a result, AKT Peerless collected eight sub-slab vapor samples from AKT VI-1 through AKT VI-9. AKT VI-
9 Temp was located in the northeast corner of the building in the vicinity of the suspected source area.
The eight sub-slab samples were collected in pre-cleaned Bottlevacs provided by Fibertec. The collected
samples were submitted to Fibertec for analysis of VOCs using TO-15 analytical methodology. Analytical
results indicated all VOCs were reported below the site specific screening levels with the following
exception:

• Analytical results for AKT VI-9 evidanced at 85 µg/m3 Naphthalene, which exceeds the Site-
Specific Non-Residential VIAC of 59 µg/m3.

Refer to Table 3 for a comparison of soil gas specific site results to screening levels. Copies of laboratory
analytical reports are provided in Appendix E.

5.3.2 Indoor Air


As part of the monitoring activities conducted on November 28, 2017, AKT Peerless also collected one
Indoor Air Sample (Indoor Air-101). This sample was collected over an 8-hour period, using a Summa
Canister. The sample was collected in the Police Chief’s office located in the southest section of the
building ,at an elevation of approximately 3.5 feet above the ground level. The indoor air sample was
submitted to Fibertec for analysis of VOCs using TO-15 analytical methodology.

Laboratory analytical results indicated all consituations of concern were reported as non-detect at or
below the reporting limits with the exception of Acetone (110 µg/m3) and Trichloroethane (0.74 µg/m3).
Both of the detected constituants of concern were below the most conservative Media-Specific
Volatilization to Indoor Air Interm Action Screening Levels, Residential Recommended Interm Action
Screening Levels (RIASL), of 31,000 µg/m3 and 2.0 µg/m3, respectively. Refer to Table 4 for a comparison
of indoor air concentrations to screening levels.

5.4 Radon Analytical Results


As part of the air quality investigation, AKT Peerless collected one Radon sample from the evidence room
near the existing sump. The sample collection was started on October 6, 2017, and ended on October
10, 2017. Analytical resulted evidenced 0.8 pCi/L. The US EPA action level for indoor radon is 4.0 pCi/L.
The EPA indicates that there is little short-term risk with test results in this range (0.6 to 1.9 pCi/L).

6.0 Conceptual Site Model


Nature and Characteristics of Contaminants
Soil and groundwater have been impacted by petroleum contaminants at concentrations exceeding the
Nonresidential RBSLs and Screening Levels. Soil contaminants exceed Nonresidential Drinking Water
Protection Criteria and Groundwater Surface Water Interface Protection Criteria. Soil contamination is
located at depths ranging from 2 to 15 feet bgs. Soil contamination is present in two distinct areas on the
site. The first impacted area is located adjacent to the former UST cavity on the northern portion of the
site. The second impacted area is located on the southern portion of the site.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
No contaminants were identified in groundwater at concentrations exceeding the Residential Drinking
Water and Groundwater Surface Water Interface Criteria from the groundwater sample collected during
the August 22, 2017 sub-surface investiagtion. This groundwater appears to be present in a perched unit
that is continuous across the subject property. Groundwater is likely subject to seasonal fluctuations in
elevation, in which the shallow native clay identified beneath the site was excavated during the
construction of subsurface features (i.e. UST system, utilities).

Further investigation is necessary to: 1) delineate the vertical and lateral extent of soil and groundwater
contamination, 2) further evaluate the characteristics of the groundwater unit, and 3) further evaluate
the groundwater volatilization to indoor air inhalation exposure pathway. Therefore, for the purposes of
this exposure pathway evaluation, the known nature and extent of contamination was considered.

Table 7- Soil Exposure Pathway

Does Threat Exist


Exposure
to Potential
Pathway Explanation
Receptor(s)
(Yes or No)
Soil contaminants were identified at concentrations exceeding the Non-
Residential DWP. Shallow groundwater was identified in select borings
conducted at the subject property. Municipal water is provided by
Drinking Village of St Charles Department of Public Works. The impacted
Water groundwater unit is not developed for potable purposes and is reliably
No
Protection segregated by the presence of a confining clay layer. Therefore, based
on the presence of a confining clay layer, the absence of water wells on
or near the site, and presence of municipal water service, the drinking
water exposure pathway is incomplete.

Additional investigation is necessary to determine the groundwater flow


direction(s) beneath the subject property. The site and adjacent road
right-of-ways are serviced by the Saginaw County storm water sewer
GSI Protection
Yes system. Additional investigation will be necessary to define the lateral
extent of soil contamination, the presence of impacted groundwater,
and determine if contaminants threaten surface water quality.

Contaminants were identified that exceeded the criteria for this


pathway. Furthermore, sub-slab soil gas analytical results indicated one
Soil exceedance of site specific screening levels. This sample was located in
Volatilization the garage nearest to the contaminant plume. The commercial building
to Indoor Air on the site is concrete slab on-grade construction without a basement
Yes
Inhalation or other subsurface features, other than floor drains. However, the
(SVIAI) nature and extent of contamination has not yet been fully
characterized. Therefore, additional investigation is warranted to
further evaluate the potential completeness of this pathway.

Volatile Soil Contaminant concentrations do not exceed this pathway. However, the
Inhalation nature and extent of contamination has not yet been fully
(VSI-ambient No characterized. Additional investigation will be completed to further
air) evaluate the potential completeness of this pathway.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
Does Threat Exist
Exposure
to Potential
Pathway Explanation
Receptor(s)
(Yes or No)
Contaminant concentrations do not exceed this pathway and all known
Particulate impacted soil is located beneath asphalt or concrete paving. Therefore,
Soil Inhalation No impacted soil does not have the potential to become airborne under
the current conditions.

Contaminant concentrations do not exceed this pathway and all known


impacted soil is located beneath asphalt paving or vegetated topsoil.
Therefore, under the current conditions, impacted soil is reliably
Direct Contact covered with concrete or asphalt. In the event subsurface construction
Yes
becomes necessary within the area of impact, contractors should be
notified of the appropriate measures and procedures to prevent the
potential to exacerbate contaminants.

Based on the results of the laboratory analytical results, further investigation is necessary to delineate
soil and groundwater contamination related to the release. Potential receptors include commercial
workers on the property and construction/utility workers that may perform subsurface excavation
activities in the future. Furthermore, additional groundwater characterization is necessary to further
evaluate the characteristics of the groundwater (i.e. groundwater not in an aquifer, effects of seasonal
fluctuation, continuity, and movement).

7.0 Soil Exposure Pathway Evaluation


Drinking Water Protection
Contaminant concentrations in soil exceed the Drinking Water Protection Criteria. The site obtains
potable water exclusively from the Village of St. Charles Department of Public Works and municipal
potable water is obtained from Saginaw County. AKT Peerless reviewed the MDEQ Scanned Water Well
Record Retrieval Database for area surrounding the subject property (Section 26, Township 12N, Range
1E). Based on a review of these records, there are no recorded wells within 1 mile of the site. Based on
the documented soil types and AKT Peerless observations during the subsurface investigation, a clay unit
is present locally at a thicknesses ranging from 26 feet to over 100 feet. The shallow impacted
groundwater unit is not developed. Additional investigation activities are proposed to be completed to
define the extent of soil and groundwater contamination.

Groundwater Surface Water Interface Protection


The nearest surface water proximate to the site is Bad River, which is located approximately 600 feet
south of the subject property at its nearest point. Concentrations of contaminants were detected in soil
above the MDEQ Groundwater Surface Water Interface Protection Criteria. The subject property is
developed with concrete slab on-grade buildings, as well as associated paved and landscaped areas,
which cover the subject property. Additional investigation is necessary to define the lateral extent of soil
and groundwater contamination, as well as determine if contaminants have the potential to threaten
nearby surface water quality.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
Soil Volatilization to Indoor Air
Soil Volatilization to Indoor Air is a relevant exposure pathway. Presently, known contamination exceeds
the site specifc screening levels for this pathway. Additional investigation is warranted to define the
lateral extent of contamination, determine site hydrogeologic conditions, and potentially evaluate soil
gas conditions. Based on the findings of the proposed investigation, corrective actions may be warranted
to mitigate this exposure pathway.

Soil Volatilization to Ambient Air


Volatilization to Ambient Air is a relevant exposure pathway. However, contamination has not been
identified above their respective Volatilization to Ambient Air RBSLs. Additional investigation is
warranted to define the lateral extent of soil contamination and evaluate soil gas conditions. Based on the
findings of the proposed investigation, corrective actions may be warranted to mitigate this exposure
pathway.

Particulate Inhalation
Particulate Inhalation is a relevant exposure pathway. However, soils have not been identified above
their respective Particulate Inhalation RBSLs. Impacted soil is located beneath paving and vegetated
topsoil; therefore, this exposure pathway is not complete.

Direct Contact
Direct Contact is a relevant exposure pathway. Presently, known contamination does not exceed the
criteria for this pathway and contamination is located beneath asphalt paving. Based on the current
conditions, contamination is located at a depth of at least 3.0 feet bgs, beneath asphalt paving or
vegetated topsoil and is not readily accessible by users of the site. However, in the event excavation
activities become necessary this exposure route could potentially become complete. Additional
investigation activities are necessary to further define the nature and extent of contamination. Following
delineation, corrective actions and/or institutional controls will likely be appropriate to permanently
mitigate this exposure pathway.

8.0 Groundwater Exposure Pathway Evaluation


Drinking Water
Contaminant concentrations in groundwater exceed the Drinking Water Protection Criteria. The site
obtains potable water exclusively from the Village of St. Charles Department of Public Works. The
shallow impacted groundwater unit is not developed and is segregated from the groundwater unit used
for potable purposes. Therefore, human exposure through the ingestion of impacted groundwater does
not appear to be a complete exposure pathway. It is foreseeable that land use restrictions will be used to
reliably mitigate the potential for future groundwater development to support the closure of the release.
Furthermore, additional investigation is necessary to further characterize groundwater contamination.
The results of the proposed investigation activities will allow further evaluation of the this exposure
pathway.

Groundwater Surface Water Interface Protection


The nearest surface water proximate to the site is Bad River, which is located approximately 600 feet
south of the subject property at its nearest point. Concentrations of contaminants were detected in soil

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
above the MDEQ Groundwater Surface Water Interface Protection Criteria. The subject property is
developed with concrete slab on-grade buildings, as well as associated paved and landscaped areas that
cover the subject property. Additional investigation will be necessary to define the lateral extent of soil
and groundwater contamination and determine if contaminants have the potential to threaten nearby
surface water quality.

Groundwater Volatilization to Indoor Air

Groundwater Volatilization to Indoor Air is a relevant exposure pathway. Presently, known contamination
does exceed the site specific screening levels for this pathway. Additional investigation is warranted to
define the lateral extent of contamination, determine site hydrogeologic conditions, and further evaluate
potential vapor intrusion. As previously presented, groundwater is present at 3.0 to 4.0 feet bgs.
Contaminants have been identified in groundwater in near proximity to the onsite building at
concentrations exceeding the Site Specific Non-Residential Groundwater Vapor Intrusion Screening
Levels as provided by the MDEQ. Based on the findings of the proposed investigation, corrective actions
may be warranted to mitigate this exposure pathway.

Groundwater Volatilization to Ambient Air

Volatilization to Ambient Air is a relevant exposure pathway. However, contamination has not been
identified above their respective Volatilization to Ambient Air RBSLs. Additional investigation may be
warranted to define the lateral extent of soil contamination and evaluate soil gas conditions. Based on
the findings of the proposed investigation, corrective actions may be warranted to mitigate this exposure
pathway.

9.0 OPTIONAL TIER II EVALUATION


A Tier II or Tier III evaluation was not conducted as part of this report. Furthermore, based on the
findings of the proposed supplemental investigation to further characterize the nature, extent and
magnitude of contamination at the Subject Property, a Tier II and/or Tier III evaluations may be
conducted to support a Final Assessment Report (FAR) and Corrective Action Plan (CAP).

10.0 SITE CLASSIFICATION


No previous site classification levels have been reported for this release. Upon completion of additional
site characterization activities, the appropriate classification will be evaluated in accordance with MDEQ
LUST Site Classification System. If applicable, the site classification will be revised in a subsequent
submittal, likely included the FAR and CAP.

11.0 WORKPLAN AND PROPOSED FOLLOW-UP ACTIVITES


Additional investigations are necessary to further: 1) delineate the soil and groundwater contamination,
2) evaluate groundwater and soil characteristics, 3) evaluate potentially complete exposure pathways,
and 4) establish the appropriate cleanup objectives and the most feasible corrective actions to support
the closure of this release.

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
AKT Peerless has established the following scope of work to further evaluate the nature and extent of
soil contamination, evaluate for the presence of groundwater impact, and evaluate potential exposure
pathways. The scope of work was established in light of the following considerations:

1. Soil contamination has been identified at various locations across the site and is most notably
centralized adjacent to the former UST basin. Contamination has not been defined directionally
outward from the sample locations.
2. Groundwater was identified in select borings, at depths ranging from 1.0 to 3.0 feet bgs.
Additional monitoring wells are necessary to define the extent of the contaminant plume.
3. The vertical extent of contamination has been not been defined; contaminants were identified at
14.0 to 15.0 feet bgs in AKT-103 and AKT-104. Therefore, additional investigation is warranted to
evaluate the vertical extent.
4. Soil and groundwater contamination is present at concentrations exceeding Site Specific
Volatilization to Indoor Air Inhalation Screening Levels. Furthermore, sub-slab soil gas results
were reported above Site Specific Vapor Intrusion Screening Levels at one sample location AKT-
VI-9. Based on these conditions additional investigation and corrective actions are necessary to
mitigate this exposure.

Based on the above considerations, AKT Peerless established the following scope of work to characterize
the nature and extent of the release.

• Complete ten additional soil borings, radially outward from the locations of the identified soil
and groundwater contamination. Sample locations will be biased to evaluate for potential
migration pathways associated with any buried features (utility corridors).
• It is estimated that up to six monitoring wells will be installed at boring locations to evaluate
groundwater characteristics and the extent of the impact. The presence of groundwater will be
evaluated at each location and if present, samples will be collected using low-flow “minimal
drawdown” sampling procedures. Furthermore, to support the preparation of a FAR and the
associated CAP, groundwater flow direction, elevation, velocity, and recharge rates will also be
evaluated. These monitoring wells and borings will be place to evaluate the possible and/or
extent of off site migration to the north adjacent properties.
• Replace one sub-slab vapor sampling point within the existing building. One additional round of
vapor samples will be collected to further evaluate the vapor intrusion pathway.
• Soil, soil gas, and groundwater samples will be analyzed for VOCs in accordance with US
EPA/MDEQ approved analytical methods.

It should be noted that based on the findings of the above proposed investigation, additional
investigation activities may become warranted for various reasons including, but not limited to: 1)
identification of yet unknown preferential migration pathways, 2) identification of greater contamination
concentrations, requiring further source evaluation and exposure pathway evaluation, 3) identification of
groundwater impact, requiring additional lateral delineation and/or characterization, and 4)
identification of contamination with the potential to threaten indoor air quality nearer the onsite
buildings, requiring additional soil, groundwater, and/or soil gas evaluation.

To ensure the accuracy of data collected during on site activities, AKT Peerless recommends
implementing proper quality assurance/quality control (QA/QC) measures. The QA/QC procedures

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110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
should include, but not limited to: 1) decontamination of sampling equipment before and between
sampling locations/events, 2) calibration of field equipment, 3) documentation of field activities, and 4)
sample preservation techniques.

Documentation of Activities
During the completion of the future sampling activities, subject property conditions (i.e. soil boring
locations, weather conditions) will be documented. Soil should be visually inspected and a geologic log
should be prepared for each soil boring. These logs will include soil characteristics such as: 1) color, 2)
composition (e.g., sand, clay, or gravel), 3) soil moisture and water table depth, if applicable, and 4) signs
of possible contamination (i.e., stained or discolored soil, odors). Soil types should be classified in
accordance with ASTM publication D-2488 “Unified Soil Classification System.” All soil and groundwater
samples should be delivered to a laboratory under chain-of-custody documentation.

Sample Preservation Techniques


Soil and groundwater samples will be collected in laboratory-supplied containers, stored on ice or at
approximately 4 degrees Celsius, and submitted under chain-of-custody documentation.

Soil samples collected for volatile analyses will be field preserved with methanol in accordance with U.S.
EPA Method 5035.

Groundwater, if encountered, will be collected from the proposed monitor wells with a peristaltic pump
and dedicated tubing. Groundwater samples for VOC analyses should be collected with zero headspace
into 40 ml glass vials and preserved with hydrochloric acid.

12.0 Conclusions and Recommendations

12.1 Conclusions
Review of historical data indicats no environmental concern associated with the subject porperty with
the following exception:

• Village of St. Charles, 110 West Spruce Street is listed on the UST database. Two 1,000-gallon
gasoline USTs were installed on March 18, 1972, and March 19, 1975, respectively; and were
removed on May 26, 1992. One confirmed release of gasoline (C-0848-92) was reported on May
26, 1992, which remains open.

AKT Peerless reviewed historic data from previous investigations and conducted additional activities to
futher evaluate the nature and extent of the historic release. Results of the investigation indicated
impact above the MDEQ Part 213 Site Specific Non-Residential Soil Voliziation to Indoor Air Inhalation
and RBSLs criteria. Based on the findings of the additional sub-surface investigation, AKT Peerless
collected both sub-slab soil gas and the indoor air samples.

Analytical results for the sub-slab soil gas monitoring indicated all constiutants of concern were below
the site specific screening levels with the exception of Napthalene which exceeds the Site-Specific
Non-Residential Criteria.

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page 23


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
AKT Peerless also collected one indoor air sample from the interior of the building. Analytical results
indicated that all constituants of concern were reported as either non-detect or below the most
conseritive screening levels.

12.2 Recommendations
AKT Peerless recommendiations include the following:

• Futher delineation of the soil and groundwater impact


• Evaluate groundwater and soil characteristics
• Futher evaluate potential exposure pathways

Establish the appropriate cleanup objectives and the most feasible corrective actions to support the
closure of the release and remediate the source of the vapor intrusion pathway.

13.0 Limitations
The information and opinions obtained in this report are for the exclusive use of the Village of St.
Charles. No distribution to or reliance by other parties may occur without the express written permission
of AKT Peerless. AKT Peerless will not distribute this report without your written consent or as required
by law or by a Court order. The information and opinions contained in the report are given in light of that
assignment. The report must be reviewed and relied upon only in conjunction with the terms and
conditions expressly agreed upon by the parties and as limited therein. Any third parties, who have been
extended the right to rely on the contents of this report by AKT Peerless (which is expressly required
prior to any third-party release), expressly agrees to be bound by the original terms and conditions
entered into by AKT Peerless and Village of St. Charles.

Subject to the above and the terms and conditions, AKT Peerless accepts responsibility for the
competent performance of its duties in executing the assignment and preparing reports in accordance
with the normal standards of the profession, but disclaims any responsibility for consequential damages.
Although AKT Peerless believes that results contained herein are reliable, AKT Peerless cannot warrant or
guarantee that the information provided is exhaustive or that the information provided by Village of St.
Charles or third parties is complete or accurate.

14.0 Signatures of Environmental Professionals


The following individuals contributed to the completion of this report.

Karl Primdahl
Project Manager
AKT Peerless
Saginaw, Michigan Office
Phone: 989.754.9896

ENVIRONMENTAL SITE CHARACTERIZATION REPORT Page 24


110 WEST SPRUCE STREET, ST. CHARLES, MICHIGAN
FIGURES
ST.CHARLES QUADRANGLE
MICHIGAN - SAGINAW COUNTY
7.5 MINUTE SERIES (TOPOGRAPHIC)

1 0 1 MILE

1000 0 1000 2000 3000 4000 5000 6000 7000 FEET

1 0 1 KILOMETER

MICHIGAN
QUADRANGLE LOCATION

IMAGE TAKEN FROM 1975 U.S.G.S. TOPOGRAPHIC MAP

TOPOGRAPHIC LOCATION MAP DRAWN BY: OGO


DATE: 12/15/2017
110 WEST SPRUCE STREET
ST. CHARLES TOWNSHIP, MICHIGAN
www.aktpeerless.com PROJECT NUMBER: 12716s
FIGURE 1
AKT-103/TMW

MW-8/SEC-15
PARKING LOT
AKT-102
RESIDENTIAL 100 WEST MAPLE STREET
RESIDENTIAL 121 WEST MAPLE STREET
131 WEST MAPLE STREET MW-4/SEC-11
MW-9/SEC-16

SEC-05
FORMER 1,000 GALLON
GASOLINE USTs

SB-01 SB-02
SEC-04
MW-3/SEC-10

AKT-104/MW-10
SEC-06 TRI TOWNSHIP FIRE DEPARTMENT
ASPHALT PARKING AREA SB-03 AKT-101 106 WEST SPRUCE STREET
SEC-07 SB-04

GARAGE MW-1
CH

SEC-08 SEC-03
ER

MW-2/SEC-9
SB-05 SB-10
RY

GARAGE
ST

SB-09
RE
ET

SEC-01 SEC-02 MW-5/SEC-12


SUBJECT BUILDING

SB-06 SB-08

MW-6/SEC-13

SB-07
ASPHALT PARKING AREA

RESIDENTIAL
206 WEST SPRUCE STREET RESIDENTIAL
ET 109 WEST SPRUCE STREET
CE STRE
TS PRU
WES RESIDENTIAL
113 WEST SPRUCE STREET LEGEND
= PROPERTY LINE
RESIDENTIAL = POLE MOUNTED TRANSFORMER
203 WEST SPRUCE STREET = CATCH BASIN
= OVERHEAD DOOR
= SOIL BORING BY SUPERIOR
RESIDENTIAL = SOIL BORING BY MANNIK SMITH
117 WEST SPRUCE STREET = MONITORING WELL
= SOIL BORING
RESIDENTIAL DRAWN BY: OGO
SAMPLE LOCATION MAP
DATE: 12/15/2017
110 WEST SPRUCE STREET
0 20 40
ST. CHARLES TOWNSHIP, MICHIGAN SCALE: 1" = 40'
www.aktpeerless.com PROJECT NUMBER: 12716s
FIGURE 2
12/15/2017

40
SEC-05 (6-7') SEC-11 (7-8')
SB-02 (5')
SB-01 (2') AKT-102 (7.5-8.5') 9/11/2015 AKT-104 (7-8')
7/7/2015

SCALE: 1" = 40'


OGO
7/10/2014

FIGURE 3
7/10/2014 2-Methylnaphthalene 15,000 ug/Kg (2) 2-Methylnaphthalene 23,200 ug/Kg (2,3) 8/22/2017
2-Methylnaphthalene 20,300 ug/Kg (2) 8/22/2017
Ethylbenzene 25,300 ug/Kg (1,2,3,4)

20
2-Methylnaphthalene 7,700 ug/Kg (2) Benzene 3,700 ug/Kg (1,3,4) Ethylbenzene 26,900 ug/Kg (1,2,3,4) 2-Methylnaphthalene 16,000 ug/Kg (2)
Ethylbenzene 200 ug/Kg (4) Naphthalene 11,100 ug/Kg (2,3)

DRAWN BY:
Ethylbenzene 340 ug/Kg (2,3,4) Ethylbenzene 7,300 ug/Kg (1,2,3,4) Naphthalene 10,100 ug/Kg (2,3) n-Butylbenzene 7,400 ug/Kg (1)
1,2,4-Trimethybenzene 2,900 ug/Kg (1,2,3,4) 1,2,4-Trimethybenzene 11,100 ug/Kg (1,2,3,4)
1,2,4-Trimethybenzene 42,000 ug/Kg (1,2,3,4) 1,2,4-Trimethybenzene 68,000 ug/Kg (1,2,3,4) 1,2,4-Trimethybenzene 116,000 ug/Kg (1,2,3,4) Ethylbenzene 4,500 ug/Kg (1,2,3,4)
1,3,5-Trimethybenzene 960 ug/Kg (4) 1,3,5-Trimethybenzene 46,600 ug/Kg (1,2,3,4)
1,3,5-Trimethybenzene 12,000 ug/Kg (1,2,3,4) 1,3,5-Trimethybenzene 20,000 ug/Kg (1,2,3,4) 1,3,5-Trimethybenzene 28,400 ug/Kg (1,2,3,4) Naphthalene 4,700 ug/Kg (2,3)
Xylenes 570 ug/Kg (4) Xylenes 111,000 ug/Kg (1,2,3,4)

DATE:
Xylenes 6,500 ug/Kg (1,2,3,4) Xylenes 27,600 ug/Kg (1,2,3,4) n-Propylbenzene 5,500 ug/Kg (1)
1,2,3-Trimethybenzene 8,000 ug/Kg (3,4)
1,2,4-Trimethybenzene

0
43,000 ug/Kg (1,2,3,4)
1,3,5-Trimethybenzene 13,000 ug/Kg (1,2,3,4)
Xylenes 19,000 ug/Kg (1,2,3,4)

AKT-103/TMW AKT-104 (8.5-9.5')


SEC-06 (2-3') 8/22/2017
Ethylbenzene 310 ug/Kg (4)
MW-8/SEC-15
PARKING LOT 7/7/2015 1,2,3-Trimethybenzene 680 ug/Kg (4)
AKT-102 1,2,4-Trimethybenzene 3,600 ug/Kg (1,2,3,4)
RESIDENTIAL 100 WEST MAPLE STREET 2-Methylnaphthalene 61,600 ug/Kg (2,3)
1,3,5-Trimethybenzene 1,100 ug/Kg (4)
Benzene 3,140 ug/Kg (1,3,4)
RESIDENTIAL 121 WEST MAPLE STREET Ethylbenzene 48,800 ug/Kg (1,2,3,4) Xylenes 2,600 ug/Kg (2,4)
Naphthalene 37,000 ug/Kg (2,3)
131 WEST MAPLE STREET MW-4/SEC-11 Toluene 105,000 ug/Kg (1,2,3)
MW-9/SEC-16

SITE MAP WITH SOIL RESULTS EXCEEDING MDEQ NRCC


1,2,4-Trimethybenzene 230,000 ug/Kg (1,2,3,4)
SB-03 (6') 1,3,5-Trimethybenzene 62,900 ug/Kg (1,2,3,4)
Xylenes 375,000 ug/Kg (1,2,3,4)
SEC-05 7/10/2014
Ethylbenzene 19,000 ug/Kg (1,2,3,4) SEC-06 (4-5')
FORMER 1,000 GALLON Naphthalene 9,600 ug/Kg (2,3)
GASOLINE USTs Toluene 21,000 ug/Kg (1,2)
7/7/2015

ST. CHARLES TOWNSHIP, MICHIGAN


2-Methylnaphthalene 10,100 ug/Kg (2)
SB-01 SB-02 Xylenes 107,000 ug/Kg (1,2,3,4)
Benzene 337 ug/Kg (1,3,4)
SEC-04 Ethylbenzene 7,070 ug/Kg (1,2,3,4)

PROJECT NUMBER: 12716s-


MW-3/SEC-10

110 WEST SPRUCE STREET


Naphthalene 5,200 ug/Kg (2,3)
1,2,4-Trimethybenzene 42,200 ug/Kg (1,2,3,4)
AKT-104/MW-10
SEC-06 TRI TOWNSHIP FIRE DEPARTMENT 1,3,5-Trimethybenzene
Xylenes
12,300 ug/Kg (1,2,3,4)
42,200 ug/Kg (1,2,3,4)
ASPHALT PARKING AREA SB-03 AKT-101 106 WEST SPRUCE STREET
SEC-07 SB-04

GARAGE MW-1
CH

SEC-08 SEC-03
ER

MW-2/SEC-9
SB-05 SB-10
RY

GARAGE
S

SB-04 (5')
TR

SB-09
EE

7/10/2014
T

SEC-01 SEC-02 MW-5/SEC-12


SUBJECT BUILDING Ethylbenzene 1,500 ug/Kg (2,3,4)
Naphthalene 1,700 ug/Kg (2)

SB-06 SB-08

MW-6/SEC-13

SB-07
ASPHALT PARKING AREA

RESIDENTIAL SEC-02 (6-7')


206 WEST SPRUCE STREET RESIDENTIAL 7/7/2015
T 109 WEST SPRUCE STREET
TREE
Benzene 181 ug/Kg (1,3,4)
E S
T SP RUC
WES RESIDENTIAL
113 WEST SPRUCE STREET SEC-08 (7-8')
7/7/2015
RESIDENTIAL Benzene 954 ug/Kg (1,3,4)
203 WEST SPRUCE STREET

RESIDENTIAL
117 WEST SPRUCE STREET

RESIDENTIAL LEGEND

www.aktpeerless.com
203 WEST SPRUCE STREET
= PROPERTY LINE
SEC-01 (7-8') = POLE MOUNTED TRANSFORMER
SB-05 (9')
7/7/2015 = CATCH BASIN
7/10/2014 Benzene 560 ug/Kg (1,3,4) = OVERHEAD DOOR
Benzene 980 ug/Kg (1,3,4) Naphthalene 1,750 ug/Kg (2) = SOIL BORING BY SUPERIOR
Ethylbenzene 1,600 ug/Kg (2,3,4)
Naphthalene 1,900 ug/Kg (2) = SOIL BORING BY MANNIK SMITH
= MONITORING WELL
= SOIL BORING
SEC-07 (4-5')
7/7/2015 CRITERIA NOTE
Benzene 961 ug/Kg (1,3,4)
Ethylbenzene 1,890 ug/Kg (1,2,3,4) (1) - Exceeds Non-Residential Drinking Water Protection Criteria and RBSLs
Naphthalene 1,930 ug/Kg (2) (2) - Exceeds Groundwater Surface Water Interface Protection Criteria and RBSLs
1,2,4-Trimethybenzene 4,480 ug/Kg (1,2,3,4)
1,3,5-Trimethybenzene 583 ug/Kg (4) (3) - Exceeds Site Specific Non-Residential Soil Volatilization to Indoor Air Inhalation Criteria and RBSLs
Xylenes 4,010 ug/Kg (2,4) (4) - Exceeds Recommended Interim Action Screening Levels (RIASLs)
AKT-103/TMW

MW-8/SEC-15
PARKING LOT
AKT-102
RESIDENTIAL 100 WEST MAPLE STREET
RESIDENTIAL 121 WEST MAPLE STREET
131 WEST MAPLE STREET MW-4/SEC-11
MW-9/SEC-16 MW-4
9/18/2015
SEC-05 1,2,4-Trimethybenzene 20.4 ug/L (2)
Xylenes 136 ug/L (2)
FORMER 1,000 GALLON
GASOLINE USTs

SB-01 SB-02
SEC-04
MW-3/SEC-10

AKT-104/MW-10
SEC-06 TRI TOWNSHIP FIRE DEPARTMENT
ASPHALT PARKING AREA SB-03 AKT-101 106 WEST SPRUCE STREET
SEC-07 SB-04

GARAGE MW-1 MW-1


CH

7/7/2015
SEC-08 SEC-03
ER

MW-2/SEC-9 Benzene 148 ug/L (1)


SB-05 SB-10 33.9 ug/L (2)
RY

Ethylbenzene

GARAGE MW-1
S
TR

SB-09
9/18/2017
EE

Benzene 262 ug/L (1,2)


T

SEC-01 SEC-02 MW-5/SEC-12 Ethylbenzene 41.9 ug/L (2)


SUBJECT BUILDING

SB-06 SB-08

MW-6/SEC-13

SB-07
ASPHALT PARKING AREA

RESIDENTIAL
206 WEST SPRUCE STREET RESIDENTIAL
ET 109 WEST SPRUCE STREET
CE STRE
TS PRU
LEGEND
WES RESIDENTIAL
= PROPERTY LINE 113 WEST SPRUCE STREET
= POLE MOUNTED TRANSFORMER
= CATCH BASINRESIDENTIAL
= OVERHEAD DOOR
= SOIL BORING BY SUPERIOR CRITERIA NOTE
= SOIL BORING BY MANNIK SMITH
= MONITORING WELL (1) - Exceeds Non-Residential Drinking Water Criteria
= SOIL BORING (2) - Exceeds Groundwater Surface Water Interface Criteria

DRAWN BY: OGO


SITE MAP WITH SOIL RESULTS EXCEEDING MDEQ NRCC
DATE: 12/15/2017
110 WEST SPRUCE STREET
0 20 40
ST. CHARLES TOWNSHIP, MICHIGAN SCALE: 1" = 40'
www.aktpeerless.com PROJECT NUMBER: 12716s
FIGURE 4
TABLES
Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample


SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7 SB-8 SB-9 SB-10
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth 2' 5' 6' 5' 9' 2' 1' 2'-3' 2.5' 7'
data)
RBSLs

Semivolatiles, PNAs
2-Methylnaphthalene 91-57-6 57,000 1.7E+5 4,200 30,000 1.8E+6 2.9E+8 2.6E+7 NC NA 61,600 7,700 15,000 1,300 <TDL 1,900 <TDL <TDL <TDL <TDL <TDL

Volatiles
Acetone (I) 67-64-1 15,000 42,000 34,000 3.10E+06 1.6E+8 1.7E+11 7.3E+7 2.6E+05 1.1E+8 <1500 NS NS NS NS NS NS NS NS NS NS
Acrylonitrile (I) 107-13-1 100 (M); 52 220 100 (M); 40 NC 17,000 5.8E+7 74,000 NC 8.3E+6 <1500 NS NS NS NS NS NS NS NS NS NS
Benzene (I) 71-43-2 100 100 4,000 (X) 47 (M) 45,000 4.7E+8 8.4E+5 (C) 1.7 (M) 4.0E+5 3700 <TDL 3,700 <TDL <TDL 980 <TDL <TDL <TDL <TDL <TDL
Bromobenzene (I) 108-86-1 550 1,500 NA NC 5.4E+5 2.4E+8 1.7E+6 (C) NC 7.6E+5 <740 NS NS NS NS NS NS NS NS NS NS
Bromodichloromethane 75-27-4 1,600 (W) 1,600 (W) ID NC 31,000 1.1E+8 4.9E+5 NC 1.5E+6 <370 NS NS NS NS NS NS NS NS NS NS
Bromoform 75-25-2 1,600 (W) 1,600 (W) ID NC 3.1E+6 3.6E+9 3.8E+6 (C) NC 8.7E+5 <1500 NS NS NS NS NS NS NS NS NS NS
Bromomethane 74-83-9 200 580 700 NC 13,000 1.5E+8 1.0E+6 NC 2.2E+6 <300 NS NS NS NS NS NS NS NS NS NS
2-Butanone (MEK) (I) 78-93-3 2.6E+5 7.6E+5 44,000 NC 3.5E+7 2.9E+10 7.0E+8 (C,DD) NC 2.7E+7 <750 NS NS NS NS NS NS NS NS NS NS
n-Butylbenzene 104-51-8 1,600 4,600 ID NC ID 8.8E+8 8.0E+6 NC 1.0E+7 7,400 NS NS NS NS NS NS NS NS NS NS
sec-Butylbenzene 135-98-8 1,600 4,600 ID NC ID 1.8E+8 8.0E+6 NC 1.0E+7 1,400 NS NS NS NS NS NS NS NS NS NS
tert-Butylbenzene (I) 98-06-6 1,600 4,600 ID NC ID 2.9E+8 8.0E+6 NC 1.0E+7 <370 NS NS NS NS NS NS NS NS NS NS
Carbon disulfide (I,R) 75-15-0 16,000 46,000 ID 920 1.6E+6 2.1E+10 4.3E+7 (C,DD) NC 2.8E+5 <370 NS NS NS NS NS NS NS NS NS NS
Carbon tetrachloride 56-23-5 100 100 900 (X) NC 12,000 1.7E+8 4.4E+5 (C) NC 3.9E+5 <370 NS NS NS NS NS NS NS NS NS NS
Chlorobenzene (I) 108-90-7 2,000 2,000 500 NC 9.2E+5 2.1E+9 1.4E+7 (C) 82 2.6E+5 <370 NS NS NS NS NS NS NS NS NS NS
Chloroethane 75-00-3 8,600 34,000 22,000 (X) NC 3.6E+7 2.9E+11 1.2E+7 (C) 330 9.5E+5 <370 NS NS NS NS NS NS NS NS NS NS
Chloroform 67-66-3 1,600 (W) 1,600 (W) 7,000 7.4 (M) 1.5E+5 1.6E+9 5.5E+6 (C) 0.26 (M) 1.5E+6 <370 NS NS NS NS NS NS NS NS NS NS
Chloromethane (I) 74-87-3 5,200 22,000 ID NC 1.2E+5 2.6E+9 7.4E+6 (C) 6.9 (M) 1.1E+6 <370 NS NS NS NS NS NS NS NS NS NS
o-Chlorotoluene (I) 95-49-8 3,300 9,300 ID NC 1.5E+6 2.1E+9 1.5E+7 (C) NC 5.0E+5 <370 NS NS NS NS NS NS NS NS NS NS
Dibromochloromethane 124-48-1 1,600 (W) 1,600 (W) ID NC 80,000 1.6E+8 5.0E+5 NC 6.1E+5 <370 NS NS NS NS NS NS NS NS NS NS
Dibromochloropropane 96-12-8 10 (M); 4.0 10 (M); 4.0 ID NC 900 7.0E+5 20,000 (C) NC 1,200 <370 NS NS NS NS NS NS NS NS NS NS
Dibromomethane 74-95-3 1,600 4,600 NA NC ID ID 8.0E+6 (C) NC 2.0E+6 <370 NS NS NS NS NS NS NS NS NS NS
1,2-Dichlorobenzene 95-50-1 14,000 14,000 280 NC 4.6E+7 4.4E+10 6.3E+7 (C) NC 2.1E+5 <370 NS NS NS NS NS NS NS NS NS NS
1,3-Dichlorobenzene 541-73-1 170 480 680 NC 94,000 8.8E+7 6.6E+5 (C) 10 (M) 1.7E+5 <370 NS NS NS NS NS NS NS NS NS NS
1,4-Dichlorobenzene 106-46-7 1,700 1,700 360 NC 2.6E+5 5.7E+8 1.9E+6 23 (M) NA <740 NS NS NS NS NS NS NS NS NS NS
Dichlorodifluoromethane 75-71-8 95,000 2.7E+5 ID 220 (M) 6.3E+7 1.5E+12 1.7E+8 (C) NC 1.0E+6 <370 NS NS NS NS NS NS NS NS NS NS
1,1-Dichloroethane 75-34-3 18,000 50,000 15,000 220 2.5E+6 1.5E+10 8.7E+7 (C) 2.6 (M) 8.9E+5 <370 NS NS NS NS NS NS NS NS NS NS
1,2-Dichloroethane (I) 107-06-2 100 100 7,200 (X) NC 21,000 1.5E+8 4.2E+5 NC 1.2E+6 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
cis-1,2-Dichloroethylene 156-59-2 1,400 1,400 12,000 37 (M) 2.1E+5 1.0E+9 8.0E+6 (C) 2.1 (M) 6.4E+5 <370 NS NS NS NS NS NS NS NS NS NS
trans-1,2-Dichloroethylene 156-60-5 2,000 2,000 30,000 (X) 1,400 (SE) 3.3E+5 2.1E+9 1.2E+7 (C) 39 (M) 1.4E+6 <370 NS NS NS NS NS NS NS NS NS NS
1,1-Dichloroethylene (I) 75-35-4 140 140 2,600 NC 3,700 7.8E+7 6.6E+5 (C) 12 (M) 5.7E+5 <370 NS NS NS NS NS NS NS NS NS NS
Ethylbenzene (I) 100-41-4 1,500 1,500 360 340 2.4E+6 1.3E+10 7.1E+7 (C) 12 (M) 1.4E+5 48,800 340 7,300 19,000 1,500 1,600 <TDL <TDL <TDL <TDL <TDL
Ethylene dibromide 106-93-4 20 (M); 1.0 20 (M); 1.0 110 (X) NC 5,800 1.8E+7 430 NC 8.9E+5 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
2-Hexanone 591-78-6 20,000 58,000 ID NC 1.3E+6 1.2E+9 1.0E+8 (C) NC 2.5E+6 <2,500 NS NS NS NS NS NS NS NS NS NS
Isopropyl benzene 98-82-8 91,000 2.6E+5 3,200 NC 2.0E+6 2.6E+9 8.0E+7 (C) NC 3.9E+5 1,300 NS NS NS NS NS NS NS NS NS NS
4-Methyl-2-pentanone (MIBK) (I) 108-10-1 36,000 1.0E+5 ID 1.5E+05(SE) 5.3E+7 6.0E+10 1.8E+8 (C) NC 2.7E+6 <2500 NS NS NS NS NS NS NS NS NS NS
Methylene chloride 75-09-2 100 100 30,000 (X) NC 7.0E+5 8.3E+9 5.8E+6 (C) 130 2.3E+6 <370 NS NS NS NS NS NS NS NS NS NS
Methyl-tert-butyl ether (MTBE) 1634-04-4 800 800 1.4E+5 (X) 2,100 3.0E+7 8.8E+10 7.1E+6 (C) 74 (M) 5.9E+6 <250 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
Naphthalene 91-20-3 35,000 1.0E+5 730 1,900 3.5E+5 8.8E+7 5.2E+7 NC NA 37,000 <TDL <TDL 9,600 1,700 1,900 <TDL <TDL <TDL <TDL <TDL
n-Propylbenzene (I) 103-65-1 1,600 4,600 ID NC ID 5.9E+8 8.0E+6 NC 1.0E+7 5,500 NS NS NS NS NS NS NS NS NS NS
Styrene 100-42-5 2,700 2,700 2,100 (X) NC 3.3E+6 6.9E+9 1.9E+6 (C) NC 5.2E+5 <740 NS NS NS NS NS NS NS NS NS NS
1,1,1,2-Tetrachloroethane 630-20-6 1,500 6,400 ID NC 1.2E+5 5.3E+8 2.2E+6 (C) NC 4.4E+5 <370 NS NS NS NS NS NS NS NS NS NS

AKT Peerless Environmental and Energy Services


Page 1 of 10
Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample


SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7 SB-8 SB-9 SB-10
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014 7/10/2014
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth 2' 5' 6' 5' 9' 2' 1' 2'-3' 2.5' 7'
data)
RBSLs

1,1,2,2-Tetrachloroethane 79-34-5 170 700 1,600 (X) NC 34,000 6.8E+7 2.4E+5 NC 8.7E+5 <370 NS NS NS NS NS NS NS NS NS NS
Tetrachloroethylene 127-18-4 100 100 1,200 (X) 74 2.1E+5 1.2E+9 9.3E+5 (C) 6.2 (M) 88,000 <370 NS NS NS NS NS NS NS NS NS NS
Toluene (I) 108-88-3 16,000 16,000 5,400 64,000 (SE) 3.3E+6 1.2E+10 1.6E+8 (C) 105,000 2.5E+5 <370 <TDL <TDL 21,000 <TDL <TDL <TDL <TDL <TDL <TDL <TDL
1,2,4-Trichlorobenzene 120-82-1 4,200 4,200 5,900 (X) NC 3.4E+7 1.1E+10 5.8E+6 (C,DD) 53 (M) 1.1E+6 <740 NS NS NS NS NS NS NS NS NS NS
1,1,1-Trichloroethane 71-55-6 4,000 4,000 1,800 7,500 (SE) 4.5E+6 2.9E+10 1.0E+9 (C,D) 450 4.6E+5 <370 NS NS NS NS NS NS NS NS NS NS
1,1,2-Trichloroethane 79-00-5 100 100 6,600 (X) NC 57,000 2.5E+8 8.4E+5 NC 9.2E+5 <370 NS NS NS NS NS NS NS NS NS NS
Trichloroethylene 79-01-6 100 100 4,000 (X) 4.0 (M) (SE) 14,000 5.9E+7 6.6E+5 (C,DD) 0.33 (M) 5.0E+5 <370 NS NS NS NS NS NS NS NS NS NS
Trichlorofluoromethane 75-69-4 52,000 1.5E+5 NA 340 1.1E+8 1.7E+12 2.6E+8 (C) NC 5.6E+5 <1,500 NS NS NS NS NS NS NS NS NS NS
1,2,3-Trichloropropane 96-18-4 840 2,400 NA NC 11,000 8.8E+6 4.2E+6 (C) NC 8.3E+5 <740 NS NS NS NS NS NS NS NS NS NS
1,2,3-Trimethylbenzene 526-73-8 1800 1800 570 4,800 1.9E+7 3.6E+10 1.0E+8 (C) 270 94,000 8,000 NS NS NS NS NS NS NS NS NS NS
1,2,4-Trimethylbenzene (I) 95-63-6 2,100 2,100 570 2,600 2.5E+7 3.6E+10 1.0E+8 (C) 150 1.1E+5 230,000 42,000 68,000 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
1,3,5-Trimethylbenzene (I) 108-67-8 1,800 1,800 1,100 1,800 1.9E+7 3.6E+10 1.0E+8 (C) 100 94,000 62,900 12,000 20,000 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
Vinyl chloride 75-01-4 40 40 260 (X) 8.2 (M) 29,000 8.9E+8 34,000 8.2E+02 4.9E+5 <370 NS NS NS NS NS NS NS NS NS NS
Xylenes (I) 1330-20-7 5,600 5,600 820 5,000 5.4E+7 1.3E+11 1.0E+9 (C,D) 280 1.5E+5 375,000 170 6,500 107,000 650 160 <TDL <TDL <TDL <TDL <TDL

AKT Peerless Environmental and Energy Services


Page 2 of 10
Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample


SEC-01 SEC-01 SEC-02 SEC-02 SEC-03 SEC-03 SEC-04 SEC-04 SEC-05
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth 7'-8' 9'-10' 6'-7' 9'-10' 5'-6' 9'-10' 4'-5' 9'-10' 6'-7'
data)
RBSLs

Semivolatiles, PNAs
2-Methylnaphthalene 91-57-6 57,000 1.7E+5 4,200 30,000 1.8E+6 2.9E+8 2.6E+7 NC NA 61,600 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL 23,200

Volatiles
Acetone (I) 67-64-1 15,000 42,000 34,000 3.10E+06 1.6E+8 1.7E+11 7.3E+7 2.6E+05 1.1E+8 <1500 NS NS NS NS NS NS NS NS NS
Acrylonitrile (I) 107-13-1 100 (M); 52 220 100 (M); 40 NC 17,000 5.8E+7 74,000 NC 8.3E+6 <1500 NS NS NS NS NS NS NS NS NS
Benzene (I) 71-43-2 100 100 4,000 (X) 47 (M) 45,000 4.7E+8 8.4E+5 (C) 1.7 (M) 4.0E+5 3700 560 <TDL 181 <TDL <TDL <TDL <TDL <TDL <TDL
Bromobenzene (I) 108-86-1 550 1,500 NA NC 5.4E+5 2.4E+8 1.7E+6 (C) NC 7.6E+5 <740 NS NS NS NS NS NS NS NS NS
Bromodichloromethane 75-27-4 1,600 (W) 1,600 (W) ID NC 31,000 1.1E+8 4.9E+5 NC 1.5E+6 <370 NS NS NS NS NS NS NS NS NS
Bromoform 75-25-2 1,600 (W) 1,600 (W) ID NC 3.1E+6 3.6E+9 3.8E+6 (C) NC 8.7E+5 <1500 NS NS NS NS NS NS NS NS NS
Bromomethane 74-83-9 200 580 700 NC 13,000 1.5E+8 1.0E+6 NC 2.2E+6 <300 NS NS NS NS NS NS NS NS NS
2-Butanone (MEK) (I) 78-93-3 2.6E+5 7.6E+5 44,000 NC 3.5E+7 2.9E+10 7.0E+8 (C,DD) NC 2.7E+7 <750 NS NS NS NS NS NS NS NS NS
n-Butylbenzene 104-51-8 1,600 4,600 ID NC ID 8.8E+8 8.0E+6 NC 1.0E+7 7,400 NS NS NS NS NS NS NS NS NS
sec-Butylbenzene 135-98-8 1,600 4,600 ID NC ID 1.8E+8 8.0E+6 NC 1.0E+7 1,400 NS NS NS NS NS NS NS NS NS
tert-Butylbenzene (I) 98-06-6 1,600 4,600 ID NC ID 2.9E+8 8.0E+6 NC 1.0E+7 <370 NS NS NS NS NS NS NS NS NS
Carbon disulfide (I,R) 75-15-0 16,000 46,000 ID 920 1.6E+6 2.1E+10 4.3E+7 (C,DD) NC 2.8E+5 <370 NS NS NS NS NS NS NS NS NS
Carbon tetrachloride 56-23-5 100 100 900 (X) NC 12,000 1.7E+8 4.4E+5 (C) NC 3.9E+5 <370 NS NS NS NS NS NS NS NS NS
Chlorobenzene (I) 108-90-7 2,000 2,000 500 NC 9.2E+5 2.1E+9 1.4E+7 (C) 82 2.6E+5 <370 NS NS NS NS NS NS NS NS NS
Chloroethane 75-00-3 8,600 34,000 22,000 (X) NC 3.6E+7 2.9E+11 1.2E+7 (C) 330 9.5E+5 <370 NS NS NS NS NS NS NS NS NS
Chloroform 67-66-3 1,600 (W) 1,600 (W) 7,000 7.4 (M) 1.5E+5 1.6E+9 5.5E+6 (C) 0.26 (M) 1.5E+6 <370 NS NS NS NS NS NS NS NS NS
Chloromethane (I) 74-87-3 5,200 22,000 ID NC 1.2E+5 2.6E+9 7.4E+6 (C) 6.9 (M) 1.1E+6 <370 NS NS NS NS NS NS NS NS NS
o-Chlorotoluene (I) 95-49-8 3,300 9,300 ID NC 1.5E+6 2.1E+9 1.5E+7 (C) NC 5.0E+5 <370 NS NS NS NS NS NS NS NS NS
Dibromochloromethane 124-48-1 1,600 (W) 1,600 (W) ID NC 80,000 1.6E+8 5.0E+5 NC 6.1E+5 <370 NS NS NS NS NS NS NS NS NS
Dibromochloropropane 96-12-8 10 (M); 4.0 10 (M); 4.0 ID NC 900 7.0E+5 20,000 (C) NC 1,200 <370 NS NS NS NS NS NS NS NS NS
Dibromomethane 74-95-3 1,600 4,600 NA NC ID ID 8.0E+6 (C) NC 2.0E+6 <370 NS NS NS NS NS NS NS NS NS
1,2-Dichlorobenzene 95-50-1 14,000 14,000 280 NC 4.6E+7 4.4E+10 6.3E+7 (C) NC 2.1E+5 <370 NS NS NS NS NS NS NS NS NS
1,3-Dichlorobenzene 541-73-1 170 480 680 NC 94,000 8.8E+7 6.6E+5 (C) 10 (M) 1.7E+5 <370 NS NS NS NS NS NS NS NS NS
1,4-Dichlorobenzene 106-46-7 1,700 1,700 360 NC 2.6E+5 5.7E+8 1.9E+6 23 (M) NA <740 NS NS NS NS NS NS NS NS NS
Dichlorodifluoromethane 75-71-8 95,000 2.7E+5 ID 220 (M) 6.3E+7 1.5E+12 1.7E+8 (C) NC 1.0E+6 <370 NS NS NS NS NS NS NS NS NS
1,1-Dichloroethane 75-34-3 18,000 50,000 15,000 220 2.5E+6 1.5E+10 8.7E+7 (C) 2.6 (M) 8.9E+5 <370 NS NS NS NS NS NS NS NS NS
1,2-Dichloroethane (I) 107-06-2 100 100 7,200 (X) NC 21,000 1.5E+8 4.2E+5 NC 1.2E+6 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
cis-1,2-Dichloroethylene 156-59-2 1,400 1,400 12,000 37 (M) 2.1E+5 1.0E+9 8.0E+6 (C) 2.1 (M) 6.4E+5 <370 NS NS NS NS NS NS NS NS NS
trans-1,2-Dichloroethylene 156-60-5 2,000 2,000 30,000 (X) 1,400 (SE) 3.3E+5 2.1E+9 1.2E+7 (C) 39 (M) 1.4E+6 <370 NS NS NS NS NS NS NS NS NS
1,1-Dichloroethylene (I) 75-35-4 140 140 2,600 NC 3,700 7.8E+7 6.6E+5 (C) 12 (M) 5.7E+5 <370 NS NS NS NS NS NS NS NS NS
Ethylbenzene (I) 100-41-4 1,500 1,500 360 340 2.4E+6 1.3E+10 7.1E+7 (C) 12 (M) 1.4E+5 48,800 131 <TDL <TDL <TDL <TDL <TDL <TDL <TDL 26,900
Ethylene dibromide 106-93-4 20 (M); 1.0 20 (M); 1.0 110 (X) NC 5,800 1.8E+7 430 NC 8.9E+5 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
2-Hexanone 591-78-6 20,000 58,000 ID NC 1.3E+6 1.2E+9 1.0E+8 (C) NC 2.5E+6 <2,500 NS NS NS NS NS NS NS NS NS
Isopropyl benzene 98-82-8 91,000 2.6E+5 3,200 NC 2.0E+6 2.6E+9 8.0E+7 (C) NC 3.9E+5 1,300 NS NS NS NS NS NS NS NS NS
4-Methyl-2-pentanone (MIBK) (I) 108-10-1 36,000 1.0E+5 ID 1.5E+05(SE) 5.3E+7 6.0E+10 1.8E+8 (C) NC 2.7E+6 <2500 NS NS NS NS NS NS NS NS NS
Methylene chloride 75-09-2 100 100 30,000 (X) NC 7.0E+5 8.3E+9 5.8E+6 (C) 130 2.3E+6 <370 NS NS NS NS NS NS NS NS NS
Methyl-tert-butyl ether (MTBE) 1634-04-4 800 800 1.4E+5 (X) 2,100 3.0E+7 8.8E+10 7.1E+6 (C) 74 (M) 5.9E+6 <250 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
Naphthalene 91-20-3 35,000 1.0E+5 730 1,900 3.5E+5 8.8E+7 5.2E+7 NC NA 37,000 1,750 <TDL <TDL <TDL <TDL <TDL <TDL <TDL 10,100
n-Propylbenzene (I) 103-65-1 1,600 4,600 ID NC ID 5.9E+8 8.0E+6 NC 1.0E+7 5,500 NS NS NS NS NS NS NS NS NS
Styrene 100-42-5 2,700 2,700 2,100 (X) NC 3.3E+6 6.9E+9 1.9E+6 (C) NC 5.2E+5 <740 NS NS NS NS NS NS NS NS NS
1,1,1,2-Tetrachloroethane 630-20-6 1,500 6,400 ID NC 1.2E+5 5.3E+8 2.2E+6 (C) NC 4.4E+5 <370 NS NS NS NS NS NS NS NS NS

AKT Peerless Environmental and Energy Services


Page 3 of 10
Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample


SEC-01 SEC-01 SEC-02 SEC-02 SEC-03 SEC-03 SEC-04 SEC-04 SEC-05
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth 7'-8' 9'-10' 6'-7' 9'-10' 5'-6' 9'-10' 4'-5' 9'-10' 6'-7'
data)
RBSLs

1,1,2,2-Tetrachloroethane 79-34-5 170 700 1,600 (X) NC 34,000 6.8E+7 2.4E+5 NC 8.7E+5 <370 NS NS NS NS NS NS NS NS NS
Tetrachloroethylene 127-18-4 100 100 1,200 (X) 74 2.1E+5 1.2E+9 9.3E+5 (C) 6.2 (M) 88,000 <370 NS NS NS NS NS NS NS NS NS
Toluene (I) 108-88-3 16,000 16,000 5,400 64,000 (SE) 3.3E+6 1.2E+10 1.6E+8 (C) 105,000 2.5E+5 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
1,2,4-Trichlorobenzene 120-82-1 4,200 4,200 5,900 (X) NC 3.4E+7 1.1E+10 5.8E+6 (C,DD) 53 (M) 1.1E+6 <740 NS NS NS NS NS NS NS NS NS
1,1,1-Trichloroethane 71-55-6 4,000 4,000 1,800 7,500 (SE) 4.5E+6 2.9E+10 1.0E+9 (C,D) 450 4.6E+5 <370 NS NS NS NS NS NS NS NS NS
1,1,2-Trichloroethane 79-00-5 100 100 6,600 (X) NC 57,000 2.5E+8 8.4E+5 NC 9.2E+5 <370 NS NS NS NS NS NS NS NS NS
Trichloroethylene 79-01-6 100 100 4,000 (X) 4.0 (M) (SE) 14,000 5.9E+7 6.6E+5 (C,DD) 0.33 (M) 5.0E+5 <370 NS NS NS NS NS NS NS NS NS
Trichlorofluoromethane 75-69-4 52,000 1.5E+5 NA 340 1.1E+8 1.7E+12 2.6E+8 (C) NC 5.6E+5 <1,500 NS NS NS NS NS NS NS NS NS
1,2,3-Trichloropropane 96-18-4 840 2,400 NA NC 11,000 8.8E+6 4.2E+6 (C) NC 8.3E+5 <740 NS NS NS NS NS NS NS NS NS
1,2,3-Trimethylbenzene 526-73-8 1800 1800 570 4,800 1.9E+7 3.6E+10 1.0E+8 (C) 270 94,000 8,000 NS NS NS NS NS NS NS NS NS
1,2,4-Trimethylbenzene (I) 95-63-6 2,100 2,100 570 2,600 2.5E+7 3.6E+10 1.0E+8 (C) 150 1.1E+5 230,000 <TDL 179 <TDL 203 <TDL <TDL <TDL <TDL 116,000
1,3,5-Trimethylbenzene (I) 108-67-8 1,800 1,800 1,100 1,800 1.9E+7 3.6E+10 1.0E+8 (C) 100 94,000 62,900 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL 28,400
Vinyl chloride 75-01-4 40 40 260 (X) 8.2 (M) 29,000 8.9E+8 34,000 8.2E+02 4.9E+5 <370 NS NS NS NS NS NS NS NS NS
Xylenes (I) 1330-20-7 5,600 5,600 820 5,000 5.4E+7 1.3E+11 1.0E+9 (C,D) 280 1.5E+5 375,000 <TDL 297 <TDL <TDL <TDL <TDL <TDL <TDL 27,600

AKT Peerless Environmental and Energy Services


Page 4 of 10
Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample


SEC-05 SEC-06 SEC-06 SEC-06 SEC-07 SEC-07 SEC-07 SEC-08 SEC-08 SEC-08
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth 9'-10' 2'-3' 4'-5' 14'-15' 4'-5' 8'-9' 14'-15' 2'-3' 7'-8' 14'-15'
data)
RBSLs

Semivolatiles, PNAs
2-Methylnaphthalene 91-57-6 57,000 1.7E+5 4,200 30,000 1.8E+6 2.9E+8 2.6E+7 NC NA 61,600 <TDL 61,600 10,100 <TDL 2,220 <TDL <TDL <TDL <TDL <TDL

Volatiles
Acetone (I) 67-64-1 15,000 42,000 34,000 3.10E+06 1.6E+8 1.7E+11 7.3E+7 2.6E+05 1.1E+8 <1500 NS NS NS NS NS NS NS NS NS NS
Acrylonitrile (I) 107-13-1 100 (M); 52 220 100 (M); 40 NC 17,000 5.8E+7 74,000 NC 8.3E+6 <1500 NS NS NS NS NS NS NS NS NS NS
Benzene (I) 71-43-2 100 100 4,000 (X) 47 (M) 45,000 4.7E+8 8.4E+5 (C) 1.7 (M) 4.0E+5 3700 <TDL 3,140 337 <TDL 961 <TDL <TDL <TDL 954 <TDL
Bromobenzene (I) 108-86-1 550 1,500 NA NC 5.4E+5 2.4E+8 1.7E+6 (C) NC 7.6E+5 <740 NS NS NS NS NS NS NS NS NS NS
Bromodichloromethane 75-27-4 1,600 (W) 1,600 (W) ID NC 31,000 1.1E+8 4.9E+5 NC 1.5E+6 <370 NS NS NS NS NS NS NS NS NS NS
Bromoform 75-25-2 1,600 (W) 1,600 (W) ID NC 3.1E+6 3.6E+9 3.8E+6 (C) NC 8.7E+5 <1500 NS NS NS NS NS NS NS NS NS NS
Bromomethane 74-83-9 200 580 700 NC 13,000 1.5E+8 1.0E+6 NC 2.2E+6 <300 NS NS NS NS NS NS NS NS NS NS
2-Butanone (MEK) (I) 78-93-3 2.6E+5 7.6E+5 44,000 NC 3.5E+7 2.9E+10 7.0E+8 (C,DD) NC 2.7E+7 <750 NS NS NS NS NS NS NS NS NS NS
n-Butylbenzene 104-51-8 1,600 4,600 ID NC ID 8.8E+8 8.0E+6 NC 1.0E+7 7,400 NS NS NS NS NS NS NS NS NS NS
sec-Butylbenzene 135-98-8 1,600 4,600 ID NC ID 1.8E+8 8.0E+6 NC 1.0E+7 1,400 NS NS NS NS NS NS NS NS NS NS
tert-Butylbenzene (I) 98-06-6 1,600 4,600 ID NC ID 2.9E+8 8.0E+6 NC 1.0E+7 <370 NS NS NS NS NS NS NS NS NS NS
Carbon disulfide (I,R) 75-15-0 16,000 46,000 ID 920 1.6E+6 2.1E+10 4.3E+7 (C,DD) NC 2.8E+5 <370 NS NS NS NS NS NS NS NS NS NS
Carbon tetrachloride 56-23-5 100 100 900 (X) NC 12,000 1.7E+8 4.4E+5 (C) NC 3.9E+5 <370 NS NS NS NS NS NS NS NS NS NS
Chlorobenzene (I) 108-90-7 2,000 2,000 500 NC 9.2E+5 2.1E+9 1.4E+7 (C) 82 2.6E+5 <370 NS NS NS NS NS NS NS NS NS NS
Chloroethane 75-00-3 8,600 34,000 22,000 (X) NC 3.6E+7 2.9E+11 1.2E+7 (C) 330 9.5E+5 <370 NS NS NS NS NS NS NS NS NS NS
Chloroform 67-66-3 1,600 (W) 1,600 (W) 7,000 7.4 (M) 1.5E+5 1.6E+9 5.5E+6 (C) 0.26 (M) 1.5E+6 <370 NS NS NS NS NS NS NS NS NS NS
Chloromethane (I) 74-87-3 5,200 22,000 ID NC 1.2E+5 2.6E+9 7.4E+6 (C) 6.9 (M) 1.1E+6 <370 NS NS NS NS NS NS NS NS NS NS
o-Chlorotoluene (I) 95-49-8 3,300 9,300 ID NC 1.5E+6 2.1E+9 1.5E+7 (C) NC 5.0E+5 <370 NS NS NS NS NS NS NS NS NS NS
Dibromochloromethane 124-48-1 1,600 (W) 1,600 (W) ID NC 80,000 1.6E+8 5.0E+5 NC 6.1E+5 <370 NS NS NS NS NS NS NS NS NS NS
Dibromochloropropane 96-12-8 10 (M); 4.0 10 (M); 4.0 ID NC 900 7.0E+5 20,000 (C) NC 1,200 <370 NS NS NS NS NS NS NS NS NS NS
Dibromomethane 74-95-3 1,600 4,600 NA NC ID ID 8.0E+6 (C) NC 2.0E+6 <370 NS NS NS NS NS NS NS NS NS NS
1,2-Dichlorobenzene 95-50-1 14,000 14,000 280 NC 4.6E+7 4.4E+10 6.3E+7 (C) NC 2.1E+5 <370 NS NS NS NS NS NS NS NS NS NS
1,3-Dichlorobenzene 541-73-1 170 480 680 NC 94,000 8.8E+7 6.6E+5 (C) 10 (M) 1.7E+5 <370 NS NS NS NS NS NS NS NS NS NS
1,4-Dichlorobenzene 106-46-7 1,700 1,700 360 NC 2.6E+5 5.7E+8 1.9E+6 23 (M) NA <740 NS NS NS NS NS NS NS NS NS NS
Dichlorodifluoromethane 75-71-8 95,000 2.7E+5 ID 220 (M) 6.3E+7 1.5E+12 1.7E+8 (C) NC 1.0E+6 <370 NS NS NS NS NS NS NS NS NS NS
1,1-Dichloroethane 75-34-3 18,000 50,000 15,000 220 2.5E+6 1.5E+10 8.7E+7 (C) 2.6 (M) 8.9E+5 <370 NS NS NS NS NS NS NS NS NS NS
1,2-Dichloroethane (I) 107-06-2 100 100 7,200 (X) NC 21,000 1.5E+8 4.2E+5 NC 1.2E+6 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL NS NS NS
cis-1,2-Dichloroethylene 156-59-2 1,400 1,400 12,000 37 (M) 2.1E+5 1.0E+9 8.0E+6 (C) 2.1 (M) 6.4E+5 <370 NS NS NS NS NS NS NS NS NS NS
trans-1,2-Dichloroethylene 156-60-5 2,000 2,000 30,000 (X) 1,400 (SE) 3.3E+5 2.1E+9 1.2E+7 (C) 39 (M) 1.4E+6 <370 NS NS NS NS NS NS NS NS NS NS
1,1-Dichloroethylene (I) 75-35-4 140 140 2,600 NC 3,700 7.8E+7 6.6E+5 (C) 12 (M) 5.7E+5 <370 NS NS NS NS NS NS NS NS NS NS
Ethylbenzene (I) 100-41-4 1,500 1,500 360 340 2.4E+6 1.3E+10 7.1E+7 (C) 12 (M) 1.4E+5 48,800 <TDL 48,800 7,070 <TDL 1,890 <TDL <TDL <TDL <TDL <TDL
Ethylene dibromide 106-93-4 20 (M); 1.0 20 (M); 1.0 110 (X) NC 5,800 1.8E+7 430 NC 8.9E+5 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
2-Hexanone 591-78-6 20,000 58,000 ID NC 1.3E+6 1.2E+9 1.0E+8 (C) NC 2.5E+6 <2,500 NS NS NS NS NS NS NS NS NS NS
Isopropyl benzene 98-82-8 91,000 2.6E+5 3,200 NC 2.0E+6 2.6E+9 8.0E+7 (C) NC 3.9E+5 1,300 NS NS NS NS NS NS NS NS NS NS
4-Methyl-2-pentanone (MIBK) (I) 108-10-1 36,000 1.0E+5 ID 1.5E+05(SE) 5.3E+7 6.0E+10 1.8E+8 (C) NC 2.7E+6 <2500 NS NS NS NS NS NS NS NS NS NS
Methylene chloride 75-09-2 100 100 30,000 (X) NC 7.0E+5 8.3E+9 5.8E+6 (C) 130 2.3E+6 <370 NS NS NS NS NS NS NS NS NS NS
Methyl-tert-butyl ether (MTBE) 1634-04-4 800 800 1.4E+5 (X) 2,100 3.0E+7 8.8E+10 7.1E+6 (C) 74 (M) 5.9E+6 <250 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
Naphthalene 91-20-3 35,000 1.0E+5 730 1,900 3.5E+5 8.8E+7 5.2E+7 NC NA 37,000 <TDL 37,000 5,200 <TDL 1,930 <TDL <TDL <TDL <TDL <TDL
n-Propylbenzene (I) 103-65-1 1,600 4,600 ID NC ID 5.9E+8 8.0E+6 NC 1.0E+7 5,500 NS NS NS NS NS NS NS NS NS NS
Styrene 100-42-5 2,700 2,700 2,100 (X) NC 3.3E+6 6.9E+9 1.9E+6 (C) NC 5.2E+5 <740 NS NS NS NS NS NS NS NS NS NS
1,1,1,2-Tetrachloroethane 630-20-6 1,500 6,400 ID NC 1.2E+5 5.3E+8 2.2E+6 (C) NC 4.4E+5 <370 NS NS NS NS NS NS NS NS NS NS

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Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample


SEC-05 SEC-06 SEC-06 SEC-06 SEC-07 SEC-07 SEC-07 SEC-08 SEC-08 SEC-08
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015 7/7/2015
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth 9'-10' 2'-3' 4'-5' 14'-15' 4'-5' 8'-9' 14'-15' 2'-3' 7'-8' 14'-15'
data)
RBSLs

1,1,2,2-Tetrachloroethane 79-34-5 170 700 1,600 (X) NC 34,000 6.8E+7 2.4E+5 NC 8.7E+5 <370 NS NS NS NS NS NS NS NS NS NS
Tetrachloroethylene 127-18-4 100 100 1,200 (X) 74 2.1E+5 1.2E+9 9.3E+5 (C) 6.2 (M) 88,000 <370 NS NS NS NS NS NS NS NS NS NS
Toluene (I) 108-88-3 16,000 16,000 5,400 64,000 (SE) 3.3E+6 1.2E+10 1.6E+8 (C) 105,000 2.5E+5 <370 <TDL 105,000 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
1,2,4-Trichlorobenzene 120-82-1 4,200 4,200 5,900 (X) NC 3.4E+7 1.1E+10 5.8E+6 (C,DD) 53 (M) 1.1E+6 <740 NS NS NS NS NS NS NS NS NS NS
1,1,1-Trichloroethane 71-55-6 4,000 4,000 1,800 7,500 (SE) 4.5E+6 2.9E+10 1.0E+9 (C,D) 450 4.6E+5 <370 NS NS NS NS NS NS NS NS NS NS
1,1,2-Trichloroethane 79-00-5 100 100 6,600 (X) NC 57,000 2.5E+8 8.4E+5 NC 9.2E+5 <370 NS NS NS NS NS NS NS NS NS NS
Trichloroethylene 79-01-6 100 100 4,000 (X) 4.0 (M) (SE) 14,000 5.9E+7 6.6E+5 (C,DD) 0.33 (M) 5.0E+5 <370 NS NS NS NS NS NS NS NS NS NS
Trichlorofluoromethane 75-69-4 52,000 1.5E+5 NA 340 1.1E+8 1.7E+12 2.6E+8 (C) NC 5.6E+5 <1,500 NS NS NS NS NS NS NS NS NS NS
1,2,3-Trichloropropane 96-18-4 840 2,400 NA NC 11,000 8.8E+6 4.2E+6 (C) NC 8.3E+5 <740 NS NS NS NS NS NS NS NS NS NS
1,2,3-Trimethylbenzene 526-73-8 1800 1800 570 4,800 1.9E+7 3.6E+10 1.0E+8 (C) 270 94,000 8,000 NS NS NS NS NS NS NS NS NS NS
1,2,4-Trimethylbenzene (I) 95-63-6 2,100 2,100 570 2,600 2.5E+7 3.6E+10 1.0E+8 (C) 150 1.1E+5 230,000 <TDL 230,000 42,200 <TDL 4,480 <TDL <TDL <TDL <TDL <TDL
1,3,5-Trimethylbenzene (I) 108-67-8 1,800 1,800 1,100 1,800 1.9E+7 3.6E+10 1.0E+8 (C) 100 94,000 62,900 <TDL 62,900 12,300 <TDL 583 <TDL <TDL <TDL <TDL <TDL
Vinyl chloride 75-01-4 40 40 260 (X) 8.2 (M) 29,000 8.9E+8 34,000 8.2E+02 4.9E+5 <370 NS NS NS NS NS NS NS NS NS NS
Xylenes (I) 1330-20-7 5,600 5,600 820 5,000 5.4E+7 1.3E+11 1.0E+9 (C,D) 280 1.5E+5 375,000 <TDL 375,000 42,200 <TDL 4,010 <TDL <TDL <TDL <TDL <TDL

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Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample


SEC-09 SEC-10 SEC-11 SEC-14 SEC-14 SEC-15 SEC-15 SEC-16 SEC-16
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 9/11/2015 9/11/2015 9/11/2015 10/26/2015 10/26/2015 10/26/2015 10/26/2015 10/26/2015 10/26/2015
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth 7'-8' 6.5'-7.5' 7'-8' 3'-3.5' 13' 3'-3.5' 13' 3'-3.5' 13'
data)
RBSLs

Semivolatiles, PNAs
2-Methylnaphthalene 91-57-6 57,000 1.7E+5 4,200 30,000 1.8E+6 2.9E+8 2.6E+7 NC NA 61,600 <TDL <TDL 20,300 <TDL <TDL <TDL <TDL <TDL <TDL

Volatiles
Acetone (I) 67-64-1 15,000 42,000 34,000 3.10E+06 1.6E+8 1.7E+11 7.3E+7 2.6E+05 1.1E+8 <1500 NS NS NS NS NS NS NS NS NS
Acrylonitrile (I) 107-13-1 100 (M); 52 220 100 (M); 40 NC 17,000 5.8E+7 74,000 NC 8.3E+6 <1500 NS NS NS NS NS NS NS NS NS
Benzene (I) 71-43-2 100 100 4,000 (X) 47 (M) 45,000 4.7E+8 8.4E+5 (C) 1.7 (M) 4.0E+5 3700 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
Bromobenzene (I) 108-86-1 550 1,500 NA NC 5.4E+5 2.4E+8 1.7E+6 (C) NC 7.6E+5 <740 NS NS NS NS NS NS NS NS NS
Bromodichloromethane 75-27-4 1,600 (W) 1,600 (W) ID NC 31,000 1.1E+8 4.9E+5 NC 1.5E+6 <370 NS NS NS NS NS NS NS NS NS
Bromoform 75-25-2 1,600 (W) 1,600 (W) ID NC 3.1E+6 3.6E+9 3.8E+6 (C) NC 8.7E+5 <1500 NS NS NS NS NS NS NS NS NS
Bromomethane 74-83-9 200 580 700 NC 13,000 1.5E+8 1.0E+6 NC 2.2E+6 <300 NS NS NS NS NS NS NS NS NS
2-Butanone (MEK) (I) 78-93-3 2.6E+5 7.6E+5 44,000 NC 3.5E+7 2.9E+10 7.0E+8 (C,DD) NC 2.7E+7 <750 NS NS NS NS NS NS NS NS NS
n-Butylbenzene 104-51-8 1,600 4,600 ID NC ID 8.8E+8 8.0E+6 NC 1.0E+7 7,400 NS NS NS NS NS NS NS NS NS
sec-Butylbenzene 135-98-8 1,600 4,600 ID NC ID 1.8E+8 8.0E+6 NC 1.0E+7 1,400 NS NS NS NS NS NS NS NS NS
tert-Butylbenzene (I) 98-06-6 1,600 4,600 ID NC ID 2.9E+8 8.0E+6 NC 1.0E+7 <370 NS NS NS NS NS NS NS NS NS
Carbon disulfide (I,R) 75-15-0 16,000 46,000 ID 920 1.6E+6 2.1E+10 4.3E+7 (C,DD) NC 2.8E+5 <370 NS NS NS NS NS NS NS NS NS
Carbon tetrachloride 56-23-5 100 100 900 (X) NC 12,000 1.7E+8 4.4E+5 (C) NC 3.9E+5 <370 NS NS NS NS NS NS NS NS NS
Chlorobenzene (I) 108-90-7 2,000 2,000 500 NC 9.2E+5 2.1E+9 1.4E+7 (C) 82 2.6E+5 <370 NS NS NS NS NS NS NS NS NS
Chloroethane 75-00-3 8,600 34,000 22,000 (X) NC 3.6E+7 2.9E+11 1.2E+7 (C) 330 9.5E+5 <370 NS NS NS NS NS NS NS NS NS
Chloroform 67-66-3 1,600 (W) 1,600 (W) 7,000 7.4 (M) 1.5E+5 1.6E+9 5.5E+6 (C) 0.26 (M) 1.5E+6 <370 NS NS NS NS NS NS NS NS NS
Chloromethane (I) 74-87-3 5,200 22,000 ID NC 1.2E+5 2.6E+9 7.4E+6 (C) 6.9 (M) 1.1E+6 <370 NS NS NS NS NS NS NS NS NS
o-Chlorotoluene (I) 95-49-8 3,300 9,300 ID NC 1.5E+6 2.1E+9 1.5E+7 (C) NC 5.0E+5 <370 NS NS NS NS NS NS NS NS NS
Dibromochloromethane 124-48-1 1,600 (W) 1,600 (W) ID NC 80,000 1.6E+8 5.0E+5 NC 6.1E+5 <370 NS NS NS NS NS NS NS NS NS
Dibromochloropropane 96-12-8 10 (M); 4.0 10 (M); 4.0 ID NC 900 7.0E+5 20,000 (C) NC 1,200 <370 NS NS NS NS NS NS NS NS NS
Dibromomethane 74-95-3 1,600 4,600 NA NC ID ID 8.0E+6 (C) NC 2.0E+6 <370 NS NS NS NS NS NS NS NS NS
1,2-Dichlorobenzene 95-50-1 14,000 14,000 280 NC 4.6E+7 4.4E+10 6.3E+7 (C) NC 2.1E+5 <370 NS NS NS NS NS NS NS NS NS
1,3-Dichlorobenzene 541-73-1 170 480 680 NC 94,000 8.8E+7 6.6E+5 (C) 10 (M) 1.7E+5 <370 NS NS NS NS NS NS NS NS NS
1,4-Dichlorobenzene 106-46-7 1,700 1,700 360 NC 2.6E+5 5.7E+8 1.9E+6 23 (M) NA <740 NS NS NS NS NS NS NS NS NS
Dichlorodifluoromethane 75-71-8 95,000 2.7E+5 ID 220 (M) 6.3E+7 1.5E+12 1.7E+8 (C) NC 1.0E+6 <370 NS NS NS NS NS NS NS NS NS
1,1-Dichloroethane 75-34-3 18,000 50,000 15,000 220 2.5E+6 1.5E+10 8.7E+7 (C) 2.6 (M) 8.9E+5 <370 NS NS NS NS NS NS NS NS NS
1,2-Dichloroethane (I) 107-06-2 100 100 7,200 (X) NC 21,000 1.5E+8 4.2E+5 NC 1.2E+6 <370 NS NS <TDL <TDL <TDL <TDL <TDL <TDL <TDL
cis-1,2-Dichloroethylene 156-59-2 1,400 1,400 12,000 37 (M) 2.1E+5 1.0E+9 8.0E+6 (C) 2.1 (M) 6.4E+5 <370 NS NS NS NS NS NS NS NS NS
trans-1,2-Dichloroethylene 156-60-5 2,000 2,000 30,000 (X) 1,400 (SE) 3.3E+5 2.1E+9 1.2E+7 (C) 39 (M) 1.4E+6 <370 NS NS NS NS NS NS NS NS NS
1,1-Dichloroethylene (I) 75-35-4 140 140 2,600 NC 3,700 7.8E+7 6.6E+5 (C) 12 (M) 5.7E+5 <370 NS NS NS NS NS NS NS NS NS
Ethylbenzene (I) 100-41-4 1,500 1,500 360 340 2.4E+6 1.3E+10 7.1E+7 (C) 12 (M) 1.4E+5 48,800 <TDL <TDL 25,300 <TDL <TDL <TDL <TDL <TDL <TDL
Ethylene dibromide 106-93-4 20 (M); 1.0 20 (M); 1.0 110 (X) NC 5,800 1.8E+7 430 NC 8.9E+5 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
2-Hexanone 591-78-6 20,000 58,000 ID NC 1.3E+6 1.2E+9 1.0E+8 (C) NC 2.5E+6 <2,500 NS NS NS NS NS NS NS NS NS
Isopropyl benzene 98-82-8 91,000 2.6E+5 3,200 NC 2.0E+6 2.6E+9 8.0E+7 (C) NC 3.9E+5 1,300 NS NS NS NS NS NS NS NS NS
4-Methyl-2-pentanone (MIBK) (I) 108-10-1 36,000 1.0E+5 ID 1.5E+05(SE) 5.3E+7 6.0E+10 1.8E+8 (C) NC 2.7E+6 <2500 NS NS NS NS NS NS NS NS NS
Methylene chloride 75-09-2 100 100 30,000 (X) NC 7.0E+5 8.3E+9 5.8E+6 (C) 130 2.3E+6 <370 NS NS NS NS NS NS NS NS NS
Methyl-tert-butyl ether (MTBE) 1634-04-4 800 800 1.4E+5 (X) 2,100 3.0E+7 8.8E+10 7.1E+6 (C) 74 (M) 5.9E+6 <250 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
Naphthalene 91-20-3 35,000 1.0E+5 730 1,900 3.5E+5 8.8E+7 5.2E+7 NC NA 37,000 <TDL <TDL 11,100 <TDL <TDL <TDL <TDL <TDL <TDL
n-Propylbenzene (I) 103-65-1 1,600 4,600 ID NC ID 5.9E+8 8.0E+6 NC 1.0E+7 5,500 NS NS NS NS NS NS NS NS NS
Styrene 100-42-5 2,700 2,700 2,100 (X) NC 3.3E+6 6.9E+9 1.9E+6 (C) NC 5.2E+5 <740 NS NS NS NS NS NS NS NS NS
1,1,1,2-Tetrachloroethane 630-20-6 1,500 6,400 ID NC 1.2E+5 5.3E+8 2.2E+6 (C) NC 4.4E+5 <370 NS NS NS NS NS NS NS NS NS

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Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample


SEC-09 SEC-10 SEC-11 SEC-14 SEC-14 SEC-15 SEC-15 SEC-16 SEC-16
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 9/11/2015 9/11/2015 9/11/2015 10/26/2015 10/26/2015 10/26/2015 10/26/2015 10/26/2015 10/26/2015
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth 7'-8' 6.5'-7.5' 7'-8' 3'-3.5' 13' 3'-3.5' 13' 3'-3.5' 13'
data)
RBSLs

1,1,2,2-Tetrachloroethane 79-34-5 170 700 1,600 (X) NC 34,000 6.8E+7 2.4E+5 NC 8.7E+5 <370 NS NS NS NS NS NS NS NS NS
Tetrachloroethylene 127-18-4 100 100 1,200 (X) 74 2.1E+5 1.2E+9 9.3E+5 (C) 6.2 (M) 88,000 <370 NS NS NS NS NS NS NS NS NS
Toluene (I) 108-88-3 16,000 16,000 5,400 64,000 (SE) 3.3E+6 1.2E+10 1.6E+8 (C) 105,000 2.5E+5 <370 <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL <TDL
1,2,4-Trichlorobenzene 120-82-1 4,200 4,200 5,900 (X) NC 3.4E+7 1.1E+10 5.8E+6 (C,DD) 53 (M) 1.1E+6 <740 NS NS NS NS NS NS NS NS NS
1,1,1-Trichloroethane 71-55-6 4,000 4,000 1,800 7,500 (SE) 4.5E+6 2.9E+10 1.0E+9 (C,D) 450 4.6E+5 <370 NS NS NS NS NS NS NS NS NS
1,1,2-Trichloroethane 79-00-5 100 100 6,600 (X) NC 57,000 2.5E+8 8.4E+5 NC 9.2E+5 <370 NS NS NS NS NS NS NS NS NS
Trichloroethylene 79-01-6 100 100 4,000 (X) 4.0 (M) (SE) 14,000 5.9E+7 6.6E+5 (C,DD) 0.33 (M) 5.0E+5 <370 NS NS NS NS NS NS NS NS NS
Trichlorofluoromethane 75-69-4 52,000 1.5E+5 NA 340 1.1E+8 1.7E+12 2.6E+8 (C) NC 5.6E+5 <1,500 NS NS NS NS NS NS NS NS NS
1,2,3-Trichloropropane 96-18-4 840 2,400 NA NC 11,000 8.8E+6 4.2E+6 (C) NC 8.3E+5 <740 NS NS NS NS NS NS NS NS NS
1,2,3-Trimethylbenzene 526-73-8 1800 1800 570 4,800 1.9E+7 3.6E+10 1.0E+8 (C) 270 94,000 8,000 NS NS NS NS NS NS NS NS NS
1,2,4-Trimethylbenzene (I) 95-63-6 2,100 2,100 570 2,600 2.5E+7 3.6E+10 1.0E+8 (C) 150 1.1E+5 230,000 <TDL <TDL 11,100 <TDL <TDL <TDL <TDL <TDL <TDL
1,3,5-Trimethylbenzene (I) 108-67-8 1,800 1,800 1,100 1,800 1.9E+7 3.6E+10 1.0E+8 (C) 100 94,000 62,900 <TDL <TDL 46,600 <TDL <TDL <TDL <TDL <TDL <TDL
Vinyl chloride 75-01-4 40 40 260 (X) 8.2 (M) 29,000 8.9E+8 34,000 8.2E+02 4.9E+5 <370 NS NS NS NS NS NS NS NS NS
Xylenes (I) 1330-20-7 5,600 5,600 820 5,000 5.4E+7 1.3E+11 1.0E+9 (C,D) 280 1.5E+5 375,000 <TDL <TDL 111,000 <TDL <TDL <TDL <TDL <TDL <TDL

AKT Peerless Environmental and Energy Services


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Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample AKT-104 8.5- AKT-103 7.5- AKT-101 0.5- AKT-103 1.5- AKT-102 7.5- AKT-101 5.5- AKT-104 7-
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location 9.5 8.5 1.5 2.5 8.5 6.5 8
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 8/22/2017 8/22/2017 8/22/2017 8/22/2017 8/22/2017 8/22/2017 8/22/2017
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth (8.5' - 9.5') (7.5' - 8.5') (0.5' - 1.5') (1.5' - 2.5') (7.5' - 8.5') (5.5' - 6.5') (7' - 8')
data)
RBSLs

Semivolatiles, PNAs
2-Methylnaphthalene 91-57-6 57,000 1.7E+5 4,200 30,000 1.8E+6 2.9E+8 2.6E+7 NC NA 61,600 750 <390 <370 <380 1,000 <390 16,000

Volatiles
Acetone (I) 67-64-1 15,000 42,000 34,000 3.10E+06 1.6E+8 1.7E+11 7.3E+7 2.6E+05 1.1E+8 <1500 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,500
Acrylonitrile (I) 107-13-1 100 (M); 52 220 100 (M); 40 NC 17,000 5.8E+7 74,000 NC 8.3E+6 <1500 <150 <160 <150 <150 <150 <150 <1,500
Benzene (I) 71-43-2 100 100 4,000 (X) 47 (M) 45,000 4.7E+8 8.4E+5 (C) 1.7 (M) 4.0E+5 3700 <50 <50 <50 <50 <50 <50 <180
Bromobenzene (I) 108-86-1 550 1,500 NA NC 5.4E+5 2.4E+8 1.7E+6 (C) NC 7.6E+5 <740 <100 <100 <100 <100 <100 <100 <740
Bromodichloromethane 75-27-4 1,600 (W) 1,600 (W) ID NC 31,000 1.1E+8 4.9E+5 NC 1.5E+6 <370 <100 <100 <100 <100 <100 <100 <370
Bromoform 75-25-2 1,600 (W) 1,600 (W) ID NC 3.1E+6 3.6E+9 3.8E+6 (C) NC 8.7E+5 <1500 <150 <160 <150 <150 <150 <150 <1,500
Bromomethane 74-83-9 200 580 700 NC 13,000 1.5E+8 1.0E+6 NC 2.2E+6 <300 <300 <320 <300 <300 <310 <310 <3,000
2-Butanone (MEK) (I) 78-93-3 2.6E+5 7.6E+5 44,000 NC 3.5E+7 2.9E+10 7.0E+8 (C,DD) NC 2.7E+7 <750 <750 <750 <750 <750 <750 <750 <1,500
n-Butylbenzene 104-51-8 1,600 4,600 ID NC ID 8.8E+8 8.0E+6 NC 1.0E+7 7,400 490 <50 <50 <50 640 <50 7,400
sec-Butylbenzene 135-98-8 1,600 4,600 ID NC ID 1.8E+8 8.0E+6 NC 1.0E+7 1,400 120 <50 <50 <50 180 <50 1,400
tert-Butylbenzene (I) 98-06-6 1,600 4,600 ID NC ID 2.9E+8 8.0E+6 NC 1.0E+7 <370 <50 <50 <50 <50 <50 <50 <370
Carbon disulfide (I,R) 75-15-0 16,000 46,000 ID 920 1.6E+6 2.1E+10 4.3E+7 (C,DD) NC 2.8E+5 <370 <250 <250 <250 <250 <250 <250 <370
Carbon tetrachloride 56-23-5 100 100 900 (X) NC 12,000 1.7E+8 4.4E+5 (C) NC 3.9E+5 <370 <50 <50 <50 <50 <50 <50 <370
Chlorobenzene (I) 108-90-7 2,000 2,000 500 NC 9.2E+5 2.1E+9 1.4E+7 (C) 82 2.6E+5 <370 <50 <50 <50 <50 <50 <50 <370
Chloroethane 75-00-3 8,600 34,000 22,000 (X) NC 3.6E+7 2.9E+11 1.2E+7 (C) 330 9.5E+5 <370 <370 <390 <370 <380 <390 <390 <3,700
Chloroform 67-66-3 1,600 (W) 1,600 (W) 7,000 7.4 (M) 1.5E+5 1.6E+9 5.5E+6 (C) 0.26 (M) 1.5E+6 <370 <50 <50 <50 <50 <50 <50 <370
Chloromethane (I) 74-87-3 5,200 22,000 ID NC 1.2E+5 2.6E+9 7.4E+6 (C) 6.9 (M) 1.1E+6 <370 <250 <250 <250 <250 <250 <250 <370
o-Chlorotoluene (I) 95-49-8 3,300 9,300 ID NC 1.5E+6 2.1E+9 1.5E+7 (C) NC 5.0E+5 <370 <50 <50 <50 <50 <50 <50 <370
Dibromochloromethane 124-48-1 1,600 (W) 1,600 (W) ID NC 80,000 1.6E+8 5.0E+5 NC 6.1E+5 <370 <100 <100 <100 <100 <100 <100 <370
Dibromochloropropane 96-12-8 10 (M); 4.0 10 (M); 4.0 ID NC 900 7.0E+5 20,000 (C) NC 1,200 <370 <250 <250 <250 <250 <250 <250 <370
Dibromomethane 74-95-3 1,600 4,600 NA NC ID ID 8.0E+6 (C) NC 2.0E+6 <370 <250 <250 <250 <250 <250 <250 <370
1,2-Dichlorobenzene 95-50-1 14,000 14,000 280 NC 4.6E+7 4.4E+10 6.3E+7 (C) NC 2.1E+5 <370 <100 <100 <100 <100 <100 <100 <370
1,3-Dichlorobenzene 541-73-1 170 480 680 NC 94,000 8.8E+7 6.6E+5 (C) 10 (M) 1.7E+5 <370 <100 <100 <100 <100 <100 <100 <370
1,4-Dichlorobenzene 106-46-7 1,700 1,700 360 NC 2.6E+5 5.7E+8 1.9E+6 23 (M) NA <740 <100 <100 <100 <100 <100 <100 <740
Dichlorodifluoromethane 75-71-8 95,000 2.7E+5 ID 220 (M) 6.3E+7 1.5E+12 1.7E+8 (C) NC 1.0E+6 <370 <370 <390 <370 <380 <390 <390 <3,700
1,1-Dichloroethane 75-34-3 18,000 50,000 15,000 220 2.5E+6 1.5E+10 8.7E+7 (C) 2.6 (M) 8.9E+5 <370 <50 <50 <50 <50 <50 <50 <370
1,2-Dichloroethane (I) 107-06-2 100 100 7,200 (X) NC 21,000 1.5E+8 4.2E+5 NC 1.2E+6 <370 <50 <50 <50 <50 <50 <50 <370
cis-1,2-Dichloroethylene 156-59-2 1,400 1,400 12,000 37 (M) 2.1E+5 1.0E+9 8.0E+6 (C) 2.1 (M) 6.4E+5 <370 <50 <50 <50 <50 <50 <50 <370
trans-1,2-Dichloroethylene 156-60-5 2,000 2,000 30,000 (X) 1,400 (SE) 3.3E+5 2.1E+9 1.2E+7 (C) 39 (M) 1.4E+6 <370 <50 <50 <50 <50 <50 <50 <370
1,1-Dichloroethylene (I) 75-35-4 140 140 2,600 NC 3,700 7.8E+7 6.6E+5 (C) 12 (M) 5.7E+5 <370 <50 <50 <50 <50 <50 <50 <370
Ethylbenzene (I) 100-41-4 1,500 1,500 360 340 2.4E+6 1.3E+10 7.1E+7 (C) 12 (M) 1.4E+5 48,800 310 <50 <50 <50 200 <50 4,500
Ethylene dibromide 106-93-4 20 (M); 1.0 20 (M); 1.0 110 (X) NC 5,800 1.8E+7 430 NC 8.9E+5 <370 <50 <50 <50 <50 <50 <50 <370
2-Hexanone 591-78-6 20,000 58,000 ID NC 1.3E+6 1.2E+9 1.0E+8 (C) NC 2.5E+6 <2,500 <2,500 <2,500 <2,500 <2,500 <2,500 <2,500 <2,500
Isopropyl benzene 98-82-8 91,000 2.6E+5 3,200 NC 2.0E+6 2.6E+9 8.0E+7 (C) NC 3.9E+5 1,300 <250 <250 <250 <250 <250 <250 1,300
4-Methyl-2-pentanone (MIBK) (I) 108-10-1 36,000 1.0E+5 ID 1.5E+05(SE) 5.3E+7 6.0E+10 1.8E+8 (C) NC 2.7E+6 <2500 <2,500 <2,500 <2,500 <2,500 <2,500 <2,500 <2,500
Methylene chloride 75-09-2 100 100 30,000 (X) NC 7.0E+5 8.3E+9 5.8E+6 (C) 130 2.3E+6 <370 <100 <100 <100 <100 <100 <100 <370
Methyl-tert-butyl ether (MTBE) 1634-04-4 800 800 1.4E+5 (X) 2,100 3.0E+7 8.8E+10 7.1E+6 (C) 74 (M) 5.9E+6 <250 <250 <250 <250 <250 <250 <250 <250
Naphthalene 91-20-3 35,000 1.0E+5 730 1,900 3.5E+5 8.8E+7 5.2E+7 NC NA 37,000 380 <330 <330 <330 <330 <330 4,700
n-Propylbenzene (I) 103-65-1 1,600 4,600 ID NC ID 5.9E+8 8.0E+6 NC 1.0E+7 5,500 520 <100 <100 <100 590 <100 5,500
Styrene 100-42-5 2,700 2,700 2,100 (X) NC 3.3E+6 6.9E+9 1.9E+6 (C) NC 5.2E+5 <740 <74 <79 <74 <76 <77 <77 <740
1,1,1,2-Tetrachloroethane 630-20-6 1,500 6,400 ID NC 1.2E+5 5.3E+8 2.2E+6 (C) NC 4.4E+5 <370 <100 <100 <100 <100 <100 <100 <370

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Table 1, Summary of Soil Analytical Results
110 Spruce Street
St Charles, Michigan
AKT Peerless Project No. 12716s

Site Specific Sample AKT-104 8.5- AKT-103 7.5- AKT-101 0.5- AKT-103 1.5- AKT-102 7.5- AKT-101 5.5- AKT-104 7-
Parameters* Non- Groundwater Non-Residential Non-Residential Non- Location 9.5 8.5 1.5 2.5 8.5 6.5 8
Residential Non-
Chemical Residential Surface Water Soil Infinite Source Residential Recommended
Drinking Water Residential Soil Saturation Maximum
Abstract Drinking Water Interface Volatilization to Volatile Soil Particulate Soil Interim Action
Protection Direct Contact Concentration Concentration Collection Date 8/22/2017 8/22/2017 8/22/2017 8/22/2017 8/22/2017 8/22/2017 8/22/2017
Service Protection Protection Indoor Air Inhalation Inhalation Screening Levels
*(Refer to detailed laboratory Criteria & Criteria and Screening Levels Detected
Number Criteria & Criteria & Inhalation Criteria (VSIC) Criteria and (RIASLs)
report for method reference RBSLs RBSLs
RBSLs RBSLs Criteria and and RBSLs RBSLs Depth (8.5' - 9.5') (7.5' - 8.5') (0.5' - 1.5') (1.5' - 2.5') (7.5' - 8.5') (5.5' - 6.5') (7' - 8')
data)
RBSLs

1,1,2,2-Tetrachloroethane 79-34-5 170 700 1,600 (X) NC 34,000 6.8E+7 2.4E+5 NC 8.7E+5 <370 <50 <50 <50 <50 <50 <50 <370
Tetrachloroethylene 127-18-4 100 100 1,200 (X) 74 2.1E+5 1.2E+9 9.3E+5 (C) 6.2 (M) 88,000 <370 <50 <50 <50 <50 <50 <50 <370
Toluene (I) 108-88-3 16,000 16,000 5,400 64,000 (SE) 3.3E+6 1.2E+10 1.6E+8 (C) 105,000 2.5E+5 <370 <50 <50 <50 <50 <50 <50 <370
1,2,4-Trichlorobenzene 120-82-1 4,200 4,200 5,900 (X) NC 3.4E+7 1.1E+10 5.8E+6 (C,DD) 53 (M) 1.1E+6 <740 <250 <250 <250 <250 <250 <250 <740
1,1,1-Trichloroethane 71-55-6 4,000 4,000 1,800 7,500 (SE) 4.5E+6 2.9E+10 1.0E+9 (C,D) 450 4.6E+5 <370 <50 <50 <50 <50 <50 <50 <370
1,1,2-Trichloroethane 79-00-5 100 100 6,600 (X) NC 57,000 2.5E+8 8.4E+5 NC 9.2E+5 <370 <50 <50 <50 <50 <50 <50 <370
Trichloroethylene 79-01-6 100 100 4,000 (X) 4.0 (M) (SE) 14,000 5.9E+7 6.6E+5 (C,DD) 0.33 (M) 5.0E+5 <370 <50 <50 <50 <50 <50 <50 <370
Trichlorofluoromethane 75-69-4 52,000 1.5E+5 NA 340 1.1E+8 1.7E+12 2.6E+8 (C) NC 5.6E+5 <1,500 <150 <160 <150 <150 <150 <150 <1,500
1,2,3-Trichloropropane 96-18-4 840 2,400 NA NC 11,000 8.8E+6 4.2E+6 (C) NC 8.3E+5 <740 <100 <100 <100 <100 <100 <100 <740
1,2,3-Trimethylbenzene 526-73-8 1800 1800 570 4,800 1.9E+7 3.6E+10 1.0E+8 (C) 270 94,000 8,000 680 <100 <100 <100 110 <100 8,000
1,2,4-Trimethylbenzene (I) 95-63-6 2,100 2,100 570 2,600 2.5E+7 3.6E+10 1.0E+8 (C) 150 1.1E+5 230,000 3,600 <100 <100 <100 2,900 <100 43,000
1,3,5-Trimethylbenzene (I) 108-67-8 1,800 1,800 1,100 1,800 1.9E+7 3.6E+10 1.0E+8 (C) 100 94,000 62,900 1,100 <100 <100 <100 960 <100 13,000
Vinyl chloride 75-01-4 40 40 260 (X) 8.2 (M) 29,000 8.9E+8 34,000 8.2E+02 4.9E+5 <370 <40 <40 <40 <40 <40 <40 <370
Xylenes (I) 1330-20-7 5,600 5,600 820 5,000 5.4E+7 1.3E+11 1.0E+9 (C,D) 280 1.5E+5 375,000 2,600 <150 <150 <150 570 <150 19,000

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Table 2, Summary of Groundwater Analytical Results
110 Spruce Street
St. Charles, Michigan
AKT Peerless Project No. 12716s

Sample AKT-103 GW
Parameters* Residential Residential Location 6-11
Flammability
Chemical Residential Groundwater Groundwater Recommended
and Maximum
Abstract Drinking Surface Water Volatilization to Water Interim Action Collection
Explosivity Concentration 8/22/2017
Service Water Interface Indoor Air Solubility Screening Date
*(Refer to detailed laboratory Inhalation Screening Detected
Number Criteria Criteria Levels
report for method reference Criteria Level
(RIASLs)
data) Depth 0

Semivolatiles, PNAs
2-Methylnaphthalene 91-57-6 260 19 25,000 (S) 24,600 ID NC <5.0 <5.0

Volatiles
Acetone (I) 67-64-1 730 1,700 1.0E+9 (D,S) 1.0E+9 1.5E+7 1.2E+07 <50 <50
Acrylonitrile (I) 107-13-1 2.6 2.0 (M); 1.2 34,000 7.50E+7 6.4E+6 NC <2.0 <2.0
Benzene (I) 71-43-2 5.0 (A) 200 (X) 5,600 1.75E+6 68,000 14 <1.0 <1.0
Bromobenzene (I) 108-86-1 18 NA 1.8E+5 4.13E+5 ID NC <1.0 <1.0
Bromodichloromethane 75-27-4 80 (A,W) ID 4,800 6.74E+6 ID NC <1.0 <1.0
Bromoform 75-25-2 80 (A,W) ID 4.7E+5 3.10E+6 ID NC <1.0 <1.0
Bromomethane 74-83-9 10 35 4,000 1.45E+7 ID NC <5.0 <5.0
2-Butanone (MEK) (I) 78-93-3 13,000 2,200 2.4E+8 (S) 2.40E+8 ID NC <25 <25
n-Butylbenzene 104-51-8 80 ID ID NA ID NC <1.0 <1.0
sec-Butylbenzene 135-98-8 80 ID ID NA ID NC <1.0 <1.0
tert-Butylbenzene (I) 98-06-6 80 ID ID NA ID NC <1.0 <1.0
Carbon disulfide (I,R) 75-15-0 800 ID 2.5E+5 1.19E+6 13,000 NC <5.0 <5.0
Carbon tetrachloride 56-23-5 5.0 (A) 45 (X) 370 7.93E+5 ID NC <1.0 <1.0
Chlorobenzene (I) 108-90-7 100 (A) 25 2.1E+5 4.72E+5 1.6E+5 540 <1.0 <1.0
Chloroethane 75-00-3 430 1,100 (X) 5.7E+6 (S) 5.74E+6 1.1E+5 6,700 <5.0 <5.0
Chloroform 67-66-3 80 (A,W) 350 28,000 7.92E+6 ID 7.6 <1.0 <1.0
Chloromethane (I) 74-87-3 260 ID 8,600 6.34E+6 36,000 160 <5.0 <5.0
o-Chlorotoluene (I) 95-49-8 150 ID 2.2E+5 3.73E+5 ID NC <5.0 <5.0
Dibromochloromethane 124-48-1 80 (A,W) ID 14,000 2.60E+6 ID NC <5.0 <5.0
Dibromochloropropane 96-12-8 0.2 (A) ID 220 1,230 NA NC <1.0 <1.0
Dibromomethane 74-95-3 80 NA ID 1.10E+7 ID NC <5.0 <5.0
1,2-Dichlorobenzene 95-50-1 600 (A) 13 1.6E+5 (S) 1.56E+5 NA NC <1.0 <1.0
1,3-Dichlorobenzene 541-73-1 6.6 28 18,000 1.11E+5 ID 52 <1.0 <1.0
1,4-Dichlorobenzene 106-46-7 75 (A) 17 16,000 73,800 NA 120 <1.0 <1.0
Dichlorodifluoromethane 75-71-8 1,700 ID 2.2E+5 3.00E+5 ID NC <5.0 <5.0
1,1-Dichloroethane 75-34-3 880 740 1.0E+6 5.06E+6 3.8E+5 67 <1.0 <1.0
1,2-Dichloroethane (I) 107-06-2 5.0 (A) 360 (X) 9,600 8.52E+6 2.5E+6 NC <1.0 <1.0
cis-1,2-Dichloroethylene 156-59-2 70 (A) 620 93,000 3.50E+6 5.3E+5 48 <1.0 <1.0
trans-1,2-Dichloroethylene 156-60-5 100 (A) 1,500 (X) 85,000 6.30E+6 2.3E+5 650 <1.0 <1.0
1,1-Dichloroethylene (I) 75-35-4 7.0 (A) 130 200 2.25E+6 97,000 170 <1.0 <1.0
1,2-Dichloropropane (I) 78-87-5 5.0 (A) 230 (X) 16,000 2.80E+6 5.5E+5 NC <1.0 <1.0
Ethylbenzene (I) 100-41-4 74 (E) 18 1.1E+5 1.69E+5 43,000 45 <1.0 <1.0
Ethylene dibromide 106-93-4 0.05 (A) 5.7 (X) 2,400 4.20E+6 ID NC <1.0 <1.0
2-Hexanone 591-78-6 1,000 ID 4.2E+6 1.60E+7 NA NC <50 <50
Isopropyl benzene 98-82-8 800 28 56,000 (S) 56,000 29,000 NC <5.0 <5.0
4-Methyl-2-pentanone (MIBK) (I) 108-10-1 1,800 ID 2.0E+7 (S) 2.00E+7 ID NC <50 <50
Methylene chloride 75-09-2 5.0 (A) 1,500 (X) 2.2E+5 1.70E+7 ID 3,900 <5.0 <5.0
Methyl-tert-butyl ether (MTBE) 1634-04-4 40 (E) 7,100 (X) 4.7E+7 (S) 4.68E+7 ID 4,000 <5.0 <5.0
Naphthalene 91-20-3 520 11 31,000 (S) 31,000 NA NC <5.0 <5.0
n-Propylbenzene (I) 103-65-1 80 ID ID NA ID NC <1.0 <1.0
Styrene 100-42-5 100 (A) 80 (X) 1.7E+5 3.10E+5 1.4E+5 NC <1.0 <1.0
1,1,1,2-Tetrachloroethane 630-20-6 77 ID 15,000 1.10E+6 ID NC <1.0 <1.0
1,1,2,2-Tetrachloroethane 79-34-5 8.5 78 (X) 12,000 2.97E+6 ID NC <1.0 <1.0
Tetrachloroethylene 127-18-4 5.0 (A) 60 (X) 25,000 2.0E+5 ID 96 <1.0 <1.0
Toluene (I) 108-88-3 790 (E) 270 5.3E+5 (S) 5.26E+5 61,000 23,000 <1.0 <1.0

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Page 1 of 2 Project No.: 12716s
Table 2, Summary of Groundwater Analytical Results
110 Spruce Street
St. Charles, Michigan
AKT Peerless Project No. 12716s

Sample AKT-103 GW
Parameters* Residential Residential Location 6-11
Flammability
Chemical Residential Groundwater Groundwater Recommended
and Maximum
Abstract Drinking Surface Water Volatilization to Water Interim Action Collection
Explosivity Concentration 8/22/2017
Service Water Interface Indoor Air Solubility Screening Date
*(Refer to detailed laboratory Inhalation Screening Detected
Number Criteria Criteria Levels
report for method reference Criteria Level
(RIASLs)
data) Depth 0

1,2,4-Trichlorobenzene 120-82-1 70 (A) 99 (X) 3.0E+5 (S) 3.00E+5 NA 95 <5.0 <5.0


1,1,1-Trichloroethane 71-55-6 200 (A) 89 6.6E+5 1.33E+6 ID 8,600 <1.0 <1.0
1,1,2-Trichloroethane 79-00-5 5.0 (A) 330 (X) 17,000 4.42E+6 NA NC <1.0 <1.0
Trichloroethylene 79-01-6 5.0 (A) 200 (X) 2,200 1.10E+6 ID 6.1 <1.0 <1.0
Trichlorofluoromethane 75-69-4 2,600 NA 1.1E+6 (S) 1.10E+6 ID NC <1.0 <1.0
1,2,3-Trichloropropane 96-18-4 42 NA 8,300 1.90E+6 NA NC <1.0 <1.0
1,2,4-Trimethylbenzene (I) 95-63-6 63 (E) 17 56,000 (S) 55,890 56,000 (S) 440 <1.0 <1.0
1,3,5-Trimethylbenzene (I) 108-67-8 72 (E) 45 61,000 (S) 61,150 ID 310 <1.0 <1.0
Vinyl chloride 75-01-4 2.0 (A) 13 (X) 1,100 2.76E+6 33,000 0.96 (M) <1.0 <1.0
Xylenes (I) 1330-20-7 280 (E) 41 1.9E+5 (S) 1.86E+5 70,000 1,200 <3.0 <3.0

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Table 3 - Summary of Soil Gas Analytical Results - Site Specific
110 Spruce Street,
Village of St. Charles, Michigan
AKT Peerless Project No.: 12716s

Sample AKT VI-9


AKTV1-2 AKTV1-2 AKTV1-3 AKT VI-3 AKTV1-4 AKT VI-4 AKTV1-5 AKT VI-5 AKTV1-6 AKT VI-6 AKTV1-7 AKT VI-7 AKTV1-8 AKT VI-8
Location (Temp)
Hazardous Substance (a) Site-Specific Non-
Residential
Chemical Maximum
Volatilization to Collection
Abstract Service Concentration 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 11/28/17
Indoor Air Date
Number Detected
*(Refer to detailed laboratory report for Criteria (VIAC)
method reference data) (µg/m3)
Depth Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab

Chemicals of Concerns (µg/m3)


Acetone 67641 1.0E+06 <TDL <52 <96 <24 <57 <41 <57 <24 <93 <24 <57 <24 <57 <24 <57 <57
Benzene 71432 260 95 <6.0 <19 <6.0 <19 <6.0 <19 <6.0 <19 <6.0 <19 <6.0 <19 <6.0 <19 95
Carbon disulfide 75150 36,000 <TDL <31 <37 <12 <37 <25 <74 <12 <37 <12 <37 <12 <37 <12 <37 <37
Chloroform 67663 87 <TDL <1.2 <9.4 <1.2 <5.9 <1.2 <6.0 <1.2 <9.1 <1.2 <5.9 <1.2 <5.9 <1.2 <5.9 <5.9
Dibromochloromethane 124481 17,000 <TDL <1.1 <16 <0.48 <4.6 <0.84 <10 <0.48 <16 <0.48 <4.1 <0.48 <4.6 <0.48 <4.1 <4.6
1,1-Dichloroethane 75343 10,000 <TDL <6.0 <24 <6.0 <24 <6.0 <24 <6.0 <24 <6.0 <24 <6.0 <24 <6.0 <24 <24
cis-1,2-Dichloroethylene 156592 410 <TDL <10 <32 <6.0 <24 <8.3 <24 <6.0 <31 <6.0 <24 <6.0 <24 <6.0 <24 <24
trans-1,2 - Dichloroethylene 156605 26,000 (SE) <TDL <6.0 <24 <6.0 <24 <6.0 <24 <6.0 <24 <6.0 <24 <6.0 <24 <6.0 <24 <24
Ethyl tertiary butyl ether (ETBE) 637923 19,000 <TDL ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Ethylbenzene 100414 8.0E+02 150 <32 <110 <12 <52 <26 <64 <13 <100 <12 <52 <12 <52 <12 <52 150
n-Heptane 142825 1.80E+05 420 <12 <49 <12 <49 <12 <60 <12 <49 <12 <49 <12 <49 <12 <49 420
n-Hexane 110543 36,000 570 <12 <42 <12 <42 <12 <85 <12 <42 <12 <42 <12 <42 <12 <42 570
Isopropanol 67630 10,000 <TDL <32 <61 <12 <29 <26 <36 <13 <59 <12 <29 <12 <29 <12 <29 <29
4-Methyl-2-pentanone (MIBK) 108101 1.00E+05 <TDL <32 <100 <12 <49 <25 <99 <12 <97 <12 <49 <12 <49 <12 <49 <49
Methyl-tert-butyl ether (MTBE) 1634044 7,700 <TDL <11 <30 <6.0 <24 <8.5 <53 <6.0 <29 <6.0 <22 <6.0 <24 <6.0 <22 <24
2-Methylnaphthalene 91576 510 <TDL <110 <480 <24 <140 <85 <140 <42 <470 <24 <140 <24 <140 <24 <140 <140
Naphthalene 91203 59 85 <11 <43 <5.3 <28 <8.5 <28 <5.3 <42 <5.3 <28 <5.3 <28 <5.3 <28 85
Tetrachloroethylene 127184 1400 (SE) 48 48 <41 <6.0 <41 <6.0 <41 <6.0 <41 <6.0 <41 <6.0 <41 <6.0 <41 <41
Toluene 108883 2.5E+05 380 <6.0 <23 <6.0 <23 <6.0 <23 <6.0 <23 <6.0 <23 <6.0 <23 <6.0 <23 380
1,1,1-Trichloroethane 71556 2.3E+05 <TDL <6.0 <33 <6.0 <33 <6.0 <33 <6.0 <33 <6.0 <33 <6.0 <33 <6.0 <33 <33
Trichloroethylene 79016 67 <TDL <1.1 <4.4 <0.30 <1.6 <0.84 <2.6 <0.41 <4.2 <0.30 <1.6 <0.30 <1.6 <0.30 <1.6 <1.6
Trichlorofluoromethane 75694 22,000 86 86 66 <6.0 <34 49 82 74 150 <6.0 <34 <6.0 <34 <6.0 <34 <34

Page 1 of 2
Table 3 - Summary of Soil Gas Analytical Results - Site Specific
110 Spruce Street,
Village of St. Charles, Michigan
AKT Peerless Project No.: 12716s

Sample AKT VI-9


AKTV1-2 AKTV1-2 AKTV1-3 AKT VI-3 AKTV1-4 AKT VI-4 AKTV1-5 AKT VI-5 AKTV1-6 AKT VI-6 AKTV1-7 AKT VI-7 AKTV1-8 AKT VI-8
Location (Temp)
Hazardous Substance (a) Site-Specific Non-
Residential
Chemical Maximum
Volatilization to Collection
Abstract Service Concentration 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 8/17/2017 11/28/17 11/28/17
Indoor Air Date
Number Detected
*(Refer to detailed laboratory report for Criteria (VIAC)
method reference data) (µg/m3)
Depth Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab Sub-slab

1,2,4-Trimethylbenzene 95636 3,100 640 <11 <40 <6.0 <29 <8.4 <29 <6.0 <39 <6.0 <29 <6.0 <29 <6.0 <29 640
1,3,5-Trimethylbenzene 108678 3,100 230 <11 <40 <6.0 <29 <8.4 <29 <6.0 <39 <6.0 <29 <6.0 <29 <6.0 <29 230
Vinyl chloride 75014 450 <TDL <6.0 <15 <6.0 <15 <6.0 <15 <6.0 <15 <6.0 <15 <6.0 <15 <6.0 <15 <15
Xylenes 1330207 11,000 890 <96 <320 <24 <100 <76 <190 <37 <310 <24 <100 <24 <100 <24 <100 890
Footnotes:
(a) - Part 201 Hazardous substances without inhalation toxicity values at this time are not included in this
table.
(b) - The IAVI and SGVI presented in this table are health-based values. The applicable IAVI and SGVI are
based on the higher of the health-based value and the appropriate analytical reporting limit.
(c) - Conversion from ug/m³ to parts per billion by volume (ppbv) uses this equation: ppbv =
([ug/m³]x(283.15°K)) / 12.187xMolecular Weight(f/mol))

(e) - TCE IURs for different scenarios as follows: Residential mutagenic = 1.0E-06; Residential cancer =
3.1E-06; Nonresidential cancer = 4.1E-06 (see EPA VISL calculator). IRIS suggests that the kidney risk be
assessed using he mutagenic equations and the liver and non-Hodgkin lymphoma (NHL) be addressed using
the standard cancer equations. In order to generate cancer-based RSLs for land uses involving multiple age
receptors using the RSL calculator, multiple steps need to be performed.
http://www/epa.gov/oswer/riskassessment/sghandbook/chemicals.htm
(f) - "IAVIres cancer" for vinyl chloride is based on EPA recommendation to apply an uncertainty factor of 2
(i.e., multiply IURF by 2) to quantify risk from continuous exposure during childhood. The final "IAVIres"
is based on updated EPA methodology specifically for vinyl chloride to address mutagenicity. The
algorithm is found in the U.S. EPA Regional Screening Level User's Guide.
(g) - Risk-based criteria are not available for methane due to insufficient toxicity data/ An acceptable soil
gas concentration (presented for both residential and nonresidential land uses) was derived utilizing 25
percent of the lower explosive level for methane. This equates to 1.25 percent or 8.4E+6 ug/m³.
(h) - Screening level based on FESL
"ID" - means "insufficient data" to develop a criterion at the date of publication of these tables (5/23/2013)
NC - No Criteria Calculated
ND - Not Detected
TDL - Target Detection Limits

Page 2 of 2
Table - Summary of Non-Residential Indoor Air
110 Spruce Street,
Village of St. Charles, Michigan
AKT Peerless Project No.: 12716s

Sample Indoor Air -


Location 101
Time-Sensitive
Hazardous Substance (a)
Recommended
Chemical Maximum Collection
Interm Action 11/28/2017
Abstract Service Concentration Date
Screening Levels
*(Refer to detailed laboratory report for Number TSRISL12 Detected
method reference data) Indoor Air
(µg/m3) Depth

Chemicals of Concerns (µg/m3)


Acetone 67641 31,000 110 110
Ammonia 7664417 1,200 ND
Benzene 71432 54 ND
Chlordane 57749 1 ND
Chlorobenzene 108907 460 ND
Chloroethane 75003 36,000 ND
Chloroform 67663 52 ND
Chloromethane 74873 410 ND
1,3-Dichlorobenzene 541731 28 ND
1,4-Dichlorobenzene 106467 300 ND
1,1-Dichloroethane 75343 740 ND
1,1-Dichloroethylene 75354 1,900 ND
cis-1,2-Dichloroethylene 156592 72 ND
trans-1,2 - Dichloroethylene 156605 790 ND
Ethylbenzene 100414 480 ND
n-Hexane 110543 6,600 ND
Methyl-tert-butyl ether (MTBE) 1634044 4,600 ND
Methylene chloride 75092 2,900 ND
Tetrachloroethylene 127184 82 ND
Toluene 108883 7,500 ND
1,2,4-Trichlorobenzene 120821 19 ND
1,1,1-Trichloroethane 71556 7,000 ND
Trichloroethylene 79016 12 0.74 0.74
1,2,3-Trimethylbenzene 526738 560 ND
1,2,4-Trimethylbenzene 95636 560 ND
1,3,5-Trimethylbenzene 108678 560 ND

Page 1 of 2
Table - Summary of Non-Residential Indoor Air
110 Spruce Street,
Village of St. Charles, Michigan
AKT Peerless Project No.: 12716s

Sample Indoor Air -


Location 101
Time-Sensitive
Hazardous Substance (a)
Recommended
Chemical Maximum Collection
Interm Action 11/28/2017
Abstract Service Concentration Date
Screening Levels
*(Refer to detailed laboratory report for Number TSRISL12 Detected
method reference data)
(µg/m3) Depth Indoor Air

Vinyl acetate 108054 1,900 ND


Vinyl chloride 75014 280 ND
Xylenes 1330207 2,000 ND
Footnotes:
(a) - Part 201 Hazardous substances without inhalation toxicity values at this time are not included in this
table.
(b) - The IAVI and SGVI presented in this table are health-based values. The applicable IAVI and SGVI are
based on the higher of the health-based value and the appropriate analytical reporting limit.
(c) - Conversion from ug/m³ to parts per billion by volume (ppbv) uses this equation: ppbv =
([ug/m³]x(283.15°K)) / 12.187xMolecular Weight(f/mol))

(e) - TCE IURs for different scenarios as follows: Residential mutagenic = 1.0E-06; Residential cancer =
3.1E-06; Nonresidential cancer = 4.1E-06 (see EPA VISL calculator). IRIS suggests that the kidney risk be
assessed using he mutagenic equations and the liver and non-Hodgkin lymphoma (NHL) be addressed using
the standard cancer equations. In order to generate cancer-based RSLs for land uses involving multiple age
receptors using the RSL calculator, multiple steps need to be performed.
http://www/epa.gov/oswer/riskassessment/sghandbook/chemicals.htm
(f) IAVIres cancer for vinyl chloride is based on EPA recommendation to apply an uncertainty factor of 2
(i.e., multiply IURF by 2) to quantify risk from continuous exposure during childhood. The final "IAVIres"
is based on updated EPA methodology specifically for vinyl chloride to address mutagenicity. The
algorithm is found in the U.S. EPA Regional Screening Level User's Guide. y
(g) p
gas concentration (presented for both residential and nonresidential land uses) was derived utilizing 25
percent of the lower explosive level for methane. This equates to 1.25 percent or 8.4E+6 ug/m³.
(h) - Screening level based on FESL
"ID" - means "insufficient data" to develop a criterion at the date of publication of these tables (5/23/2013)
NC - No Criteria Calculated
ND - Not Detected
TDL - Target Detection Limits

Page 2 of 2
R 299.49 FOOTNOTES
(as last revised by MDEQ on December 30, 2013)
FOR GENERIC CLEANUP CRITERIA TABLES
Cleanup Criteria Requirements for Response Activity (formerly the Part 201 Generic Cleanup Criteria and Screening Levels)

(A) Criterion is the state of Michigan drinking water standard established pursuant to Section 5 of 1976 PA 399, MCL 325.1005.
(B) Background, as defined in R 299.1(b), may be substituted if higher than the calculated cleanup criterion. Background levels may be less than criteria for some inorganic compounds.
(C) The criterion developed under R 299.20 to R 299.26 exceeds the chemical-specific soil saturation screening level (Csat). The person proposing or implementing response activity shall document whether
additional response activity is required to control free-phase liquids or NAPL to protect against risks associated with free-phase liquids by using methods appropriate for the free-phase liquids present.
Development of a site-specific Csat or methods presented in R 299.22, R 299.24(5), and R 299.26(8) may be conducted for the relevant exposure pathways.
(D) Calculated criterion exceeds 100 percent, hence it is reduced to 100 percent or 1.0E+9 parts per billion (ppb).
(E) Criterion is the aesthetic drinking water value, as required by Section 20120a(5) of the Natural Resources and Environmental Protection Act, 1994 PA 451, as amended (NREPA). A notice of aesthetic impact
may be employed as an institutional control mechanism if groundwater concentrations exceed the aesthetic drinking water criterion, but do not exceed the applicable health-based drinking water value [as
provided in the table in Footnote (E) in R 299.49].
(F) Criterion is based on adverse impacts to plant life and phytotoxicity.
(G) Groundwater surface water interface (GSI) criterion depends on the pH or water hardness, or both, of the receiving surface water. The final chronic value (FCV) for the protection of aquatic life shall be
calculated based on the pH or hardness of the receiving surface water. Where water hardness exceeds 400 mg CaCO3/L, use 400 mg CaCO3/L for the FCV calculation. The FCV formula provides values in units of
ug/L or ppb. The generic GSI criterion is the lesser of the calculated FCV, the wildlife value (WV), and the surface water human non-drinking water value (HNDV). The soil GSI protection criteria for these
hazardous substances are the greater of 20 times the GSI criterion or the GSI soil-water partition values using the GSI criteria developed with the procedure described in this footnote. [See table in Footnote
(G) in R 299.49].
(H) Valence-specific chromium data (Cr III and Cr VI) shall be compared to the corresponding valence-specific cleanup criteria. If both Cr III and Cr VI are present in groundwater, the total concentration of both
cannot exceed the drinking water criterion of 100 ug/L. If analytical data are provided for total chromium only, they shall be compared to the cleanup criteria for Cr VI. Cr III soil cleanup criterion for protection
of drinking water can only be used at sites where groundwater is prevented from being used as a public water supply, currently and in the future, through an approved land or resource use restriction.

(I) Hazardous substance may exhibit the characteristic of ignitability as defined in 40 C.F.R. §261.21 (revised as of July 1, 2001), which is adopted by reference in these rules.
(J) Hazardous substance may be present in several isomer forms. Isomer-specific concentrations shall be added together for comparison to criteria.
(K) Hazardous substance may be flammable or explosive, or both.
(L) Criteria for lead are derived using a biologically based model, as allowed for under Section 20120a(9) of the NREPA, and are not calculated using the algorithms and assumptions specified in pathway-specific
rules. The generic residential drinking water criterion of 4 ug/L is linked to the generic residential soil direct contact criterion of 400 mg/kg. A higher concentration in the drinking water, up to the state action
level of 15 ug/L, may be allowed as a site-specific remedy and still allow for drinking water use, under Section 20120a(2) of the NREPA if soil concentrations are appropriately lower than 400 mg/kg. If a site-
specific criterion is approved based on this subdivision, a notice shall be filed on the deed for all property where the groundwater concentrations will exceed 4 ug/L to provide notice of the potential for
unacceptable risk if soil or groundwater concentrations increase. Acceptable concentrations of site-specific soil and drinking water concentrations are presented in the [table in Footnote (L) in R 299.49].

(M) Calculated criterion is below the analytical target detection limit, therefore, the criterion defaults to the target detection limit.
(N) The concentrations of all potential sources of nitrate-nitrogen (e.g., ammonia-N, nitrite-N, nitrate-N) in groundwater that is used as a source of drinking water shall not, when added together, exceed the
nitrate drinking water criterion of 10,000 ug/L. Where leaching to groundwater is a relevant pathway, soil concentrations of all potential sources of nitrate-nitrogen shall not, when added together, exceed the
nitrate drinking water protection criterion of 2.0E+5 ug/kg.
(O) The concentration of all polychlorinated and polybrominated dibenzodioxin and dibenzofuran isomers present at a facility, expressed as an equivalent concentration of 2,3,7,8-tetrachlorodibenzo-p-dioxin
based upon their relative potency, shall be added together and compared to the criteria for 2,3,7,8-tetrachlorodibenzo-p-dioxin. The generic cleanup criteria for 2,3,7,8-tetrachlorodibenzo-p-dioxin are not
calculated according to the algorithms presented in R 299.14 to R 299.26. The generic cleanup criteria are being held at the values that the DEQ has used since August 1998, in recognition of the fact that
national efforts to reassess risks posed by dioxin are not yet complete. Until these studies are complete, it is premature to select a revised slope factor and/or reference dose for calculation of generic cleanup
criteria
(P) Amenable cyanide methods or method OIA-1677 shall be used to quantify cyanide concentrations for compliance with all groundwater criteria. Total cyanide methods or method OIA-1677 shall be used to
quantify cyanide concentrations for compliance with soil criteria. Nonresidential direct contact criteria may not be protective of the potential for release of hydrogen cyanide gas. Additional land or resource
use restrictions may be necessary to protect for the acute inhalation concerns associated with hydrogen cyanide gas.
(Q) Criteria for carcinogenic polycyclic aromatic hydrocarbons were developed using relative potential potencies to benzo(a)pyrene.
(R) Hazardous substance may exhibit the characteristic of reactivity as defined in 40 C.F.R. §261.23 (revised as of July 1, 2001), which is adopted by reference in these rules.
(S) Criterion defaults to the hazardous substance-specific water solubility limit.
(T) Refer to the federal Toxic Substances Control Act (TSCA), 40 C.F.R. §761, subpart D and 40 C.F.R. §761, Subpart G, to determine the applicability of TSCA cleanup standards. Subpart D and subpart G of 40
C.F.R. §761 (July 1, 2001) are adopted by reference in these rules. Alternatives to compliance with the TSCA standards listed below are possible under 40 C.F.R. §761 Subpart D. New releases may be subject to
the standards identified in 40 C.F.R. §761, Subpart G. Use Part 201 soil direct contact cleanup criteria in the following table if TSCA standards are not applicable. [See table in Footnote (T) in R 299.49].

(U) Hazardous substance may exhibit the characteristic of corrosivity as defined in 40 C.F.R. §261.22 (revised as of July 1, 2001), which is adopted by reference in these rules.
(V) Criterion is the aesthetic drinking water value as required by Section 20120(a)(5) of the NREPA. Concentrations up to 200 ug/L may be acceptable, and still allow for drinking water use, as part of a site-specific
cleanup under Section 20120a(2) and 20120b of the NREPA.
(W) Concentrations of trihalomethanes in groundwater shall be added together to determine compliance with the Michigan drinking water standard of 80 ug/L. Concentrations of trihalomethanes in soil shall be
added together to determine compliance with the drinking water protection criterion of 1,600 ug/kg.
(X) The GSI criterion shown in the generic cleanup criteria tables is not protective for surface water that is used as a drinking water source. For a groundwater discharge to the Great Lakes and their connecting
waters or discharge in close proximity to a water supply intake in inland surface waters, the generic GSI criterion shall be the surface water human drinking water value (HDV) listed in the [table in Footnote (X)
in R 299.49], except for those HDV indicated with an asterisk. For HDV with an asterisk, the generic GSI criterion shall be the lowest of the HDV, the WV, and the calculated FCV. See formulas in [the table in
Footnote (G) in R 299.49]. Soil protection criteria based on the HDV shall be as listed in the [table in Footnote (X) in R 299.49], except for those values with an asterisk. Soil GSI protection criteria based on the
HDV shall be as listed in the [table in Footnote (X) in R 299.49], except for those values with an asterisk. Soil GSI protection criteria for compounds with an asterisk shall be the greater of 20 times the GSI
criterion or the GSI soil-water partition values using the GSI criteria developed with the procedure described in this footnote.

(Y) Source size modifiers shown in the [table in Footnote (Y) in R 299.49] shall be used to determine soil inhalation criteria for ambient air when the source size is not one-half acre. The modifier shall be multiplied
by the generic soil inhalation criteria shown in the table of generic cleanup criteria to determine the applicable criterion. See Footnote (C) [in R 299.49].
(Z) Mercury is typically measured as total mercury. The generic cleanup criteria, however, are based on data for different species of mercury. Specifically, data for elemental mercury, chemical abstract service
(CAS) number 7439976, serve as the basis for the soil volatilization to indoor air criteria, groundwater volatilization to indoor air, and soil inhalation criteria. Data for methyl mercury, CAS number 22967926,
serve as the basis for the GSI criterion; and data for mercuric chloride, CAS number 7487947, serve as the basis for the drinking water, groundwater contact, soil direct contact, and the groundwater protection
criteria. Comparison to criteria shall be based on species-specific analytical data only if sufficient facility characterization has been conducted to rule out the presence of other species of mercury.

(AA) Use 10,000 ug/L where groundwater enters a structure through the use of a water well, sump or other device. Use 28,000 ug/L for all other uses.
(BB) The state drinking water standard for asbestos (fibers greater than 10 micrometers in length) is in units of a million fibers per liter of water (MFL). Soil concentrations of asbestos are determined by polarized
light microscopy.
(CC) Groundwater: The generic GSI criteria are based on the toxicity of unionized ammonia (NH3); the criteria are 29 ug/L and 53 ug/L for cold water and warm water surface water, respectively. As a result, the GSI
criterion shall be compared to the percent of the total ammonia concentration in the groundwater that will become NH3 in the surface water. This percent NH3 is a function of the pH and temperature of the
receiving surface water and can be estimated using the [table in Footnote (CC) in R 299.49], taken from Emerson, et al., (Journal of the Fisheries Research Board of Canada, Volume 32(12):2382, 1975). The
generic approach for estimating NH3 assumes a default pH of 8 and default temperatures of 68 °F and 85 °F for cold water and warm water surface water, respectively. The resulting NH3 is 3.8 percent and 7.2
percent for cold water and warm water, respectively. This default percentage shall be multiplied by the total ammonia-nitrogen (NH3-N) concentration in the groundwater and the resulting NH3 concentration
compared to the applicable GSI criterion. As an alternative, the maximum pH and temperature data from the specific receiving surface water can be used to estimate, from the [table in Footnote (CC) in R
299.49], a lower percent unionized ammonia concentration for comparison to the generic GSI.
Soil: The generic soil GSI protection criteria for unionized ammonia are 580 ug/kg and 1,100 ug/kg for cold water and warm water surface water, respectively.
(DD) Hazardous substance causes developmental effects. Residential direct contact criteria are protective of both prenatal and postnatal exposure. Nonresidential direct contact criteria are protective for a
pregnant adult receptor.
(EE) The [values listed in the table in Footnote (EE) in 299.49] are applicable generic GSI criteria as required by Section 20120e of the NREPA.
(FF) The chloride GSI criterion shall be 125 mg/L when the discharge is to surface waters of the state designated as public water supply sources or 50 mg/L when the discharge is to the Great Lakes or connecting
waters. Chloride GSI criteria shall not apply for surface waters of the state that are not designated as a public water supply source, however, the total dissolved solids criterion is applicable.

(GG) Risk-based criteria are not available for methane due to insufficient toxicity data. An acceptable soil gas concentration (presented for both residential and nonresidential land uses) was derived utilizing 25
percent of the lower explosive level for methane. This equates to 1.25 percent or 8.4E+6 ug/m3.
(HH) The residential criterion for sodium is 230,000 ug/L in accordance with the Sodium Advisory Council recommendation and revised Groundwater Discharge Standards.
ID Insufficient data to develop criterion.
NA A criterion or value is not available or, in the case of background and CAS numbers, not applicable.
NLL Hazardous substance is not likely to leach under most soil conditions.
NLV Hazardous substance is not likely to volatilize under most conditions.
ug/kg Micrograms per kilogram
ug/L Micrograms per liter
NS Not sampled
<TDL Below Laboratory Target Detection Limits
BOLD Exceeds highlighted criteria.
Appendix A
Photographs
VIEW OF SUBJECT BUILDING FACING NORTH

VIEW OF SUBJECT BUILDING FACING EAST

TAKEN BY: J. LUTA


PROPERTY PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
VIEW OF SUBJECT BUILDING FACING WEST

VIEW OF SUBJECT BUILDING FACING SOUTH

TAKEN BY: J. LUTA


PROPERTY PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
INTERIOR VIEW OF SUBJECT BUILDING

INTERIOR VIEW OF SUBJECT BUILDING

TAKEN BY: J. LUTA


PROPERTY PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
INTERIOR VIEW OF SUBJECT BUILDING UTILITY ROOM

INTERIOR VIEW OF SUBJECT BUILDING EVIDENCE ROOM WITH SUMP

TAKEN BY: J. LUTA


PROPERTY PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
VIEW OF MONITORING WELL ON NORTHEASTERN PORTION OF SUBJECT PROPERTY

VIEW OF MONITORING WELL ON NORTHERN ADJOINING PROPERTY

TAKEN BY: J. LUTA


PROPERTY PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
VIEW OF NORTHERN ADJOINING PROPERTY

VIEW OF NORTHERN ADJOINING PROPERTY

TAKEN BY: J. LUTA


PROPERTY PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
VIEW OF EASTERN ADJOINING PROPERTY

VIEW OF SOUTHEASTERN ADJOINING PROPERTY

TAKEN BY: J. LUTA


RECONNAISSANCE PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
VIEW OF SOUTHERN ADJOINING PROPERTY

VIEW OF SOUTHERN ADJOINING PROPERTY

TAKEN BY: J. LUTA


PROPERTY PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
VIEW OF SOUTHWESTERN ADJOINING PROPERTY

VIEW OF WESTERN ADJOINING PROPERTY

TAKEN BY: J. LUTA


PROPERTY PHOTOGRAPHS DATE: 08/17/17

110 WEST SPRUCE STREET


PROJECT NUMBER: 12716s
VILLAGE OF ST. CHARLES, MICHIGAN
Appendix B
Aerial Photographs
INQUIRY #: 3283320.4

YEAR: 1937

= 500'
INQUIRY #: 3283320.4

YEAR: 1941

= 500'
INQUIRY #: 3283320.4

YEAR: 1950

= 500'
INQUIRY #: 3283320.4

YEAR: 1963

= 500'
INQUIRY #: 3283320.4

YEAR: 1970

= 600'
INQUIRY #: 3283320.4

YEAR: 1980

= 600'
INQUIRY #: 3283320.4

YEAR: 1992

= unknown
INQUIRY #: 3283320.4

YEAR: 1997

= unknown
INQUIRY #: 3283320.4

YEAR: 1998

= 500'
INQUIRY #: 3283320.4

YEAR: 2005

= 500'
INQUIRY #: 3283320.4

YEAR: 2006

= 500'
Appendix C
Historical Fire Insurance Map Coverage
FIRE INSURANCE MAP RESEARCH RESULTS
Date: 2017-08-15

Order Number:20170815022
110 W Spruce St, Saint Charles, MI, 48655

ERIS has searched our in-house collection of close to 1 million Fire Insurance Maps for the address at
110 W Spruce St, Saint Charles, MI, 48655.

Please note that no information was found for your site or adjacent properties.

If you have any questions regarding the enclosed information, please do not hesitate to contact us.

Individual Fire Insurance Maps for the subject property and/or adjacent sites are included with the ERIS environmental
database report to be used for research purposes only and cannot be resold for any other commercial uses other than
for use in a Phase I environmental assessment.

Address: 38 Lesmill Road Unit 2, Toronto, ON M3B 2T5


Phone: 416-510-5204 Fax: 416-510-5133
info@erisinfo.com www.erisinfo.com
Appendix D
Soil Boring Logs
BORING LOG
110 Spruce Street
AKT-101
St. Charles, Michigan Drawn By: John Warner
AKT Peerless Project No: 12716s Date: 8/24/2017
DRILLING COMPANY: AKT Peerless WEATHER: 79° Partly Sunny
TECHNICIAN: Karl Primdahl BORING DEPTH: 8'
DATE DRILLED: 08/22/17 DEPTH TO GW: NA
DRILLING METHOD: Push Probe SCREEN INTERVAL: NA
FIELD GEOLOGIST: Karl Primdahl SCREEN MATERIAL: NA
SAMPLE INTERVAL

USCS SOIL CLASS.


% RECOVERY
DEPTH FEET

MOISTURE
PID VALUE

COLOR

TEMPORARY WELL
GEOLOGIC DESCRIPTION DIAGRAM
Black Asphalt
SM Dark Grayish Brown Silty Sand-With Gravel, Strong Odor M

CL Dark Grayish Brown Sandy Clay M


2 90% <.01

4
CL Light Brownish Gray Clay-Medium Plasticity M

6 90% <.01

8
End of Boring

10

12

14

16

18

20
BORING LOG
110 Spruce Street
B-2
St. Charles, Michigan Drawn By: John Warner
AKT Peerless Project No: 12716s Date: 8/24/2017
DRILLING COMPANY: AKT Peerless WEATHER: 79° Partly Sunny
TECHNICIAN: Karl Primdahl BORING DEPTH: 11'
DATE DRILLED: 08/22/17 DEPTH TO GW: 7.5'
DRILLING METHOD: Push Probe SCREEN INTERVAL: NA
FIELD GEOLOGIST: Karl Primdahl SCREEN MATERIAL: NA
SAMPLE INTERVAL

USCS SOIL CLASS.


% RECOVERY
DEPTH FEET

MOISTURE
PID VALUE

COLOR

TEMPORARY WELL
GEOLOGIC DESCRIPTION DIAGRAM
Brown Topsoil M
SM Brown Silty Sand-With Trace Gravel M

CL Dark Grayish Brown Clay M


2 90% <.01

<.01
6 90%
CL Mottled Brown Clay M

CL Grey Clay-Stiff, With Strong Odor M


8 106
CL Grey Clay M
CL Brown Clay M
<.01
10

End of Boring
12

14

16

18

20
BORING LOG
110 Spruce Street
AKT-103
St. Charles, Michigan Drawn By: John Warner
AKT Peerless Project No: 12716s Date: 8/24/2017
DRILLING COMPANY: AKT Peerless WEATHER: 79° Partly Sunny
TECHNICIAN: Karl Primdahl BORING DEPTH: 12'
DATE DRILLED: 08/22/17 DEPTH TO GW: 7.5'
DRILLING METHOD: Push Probe SCREEN INTERVAL: 6-11'
FIELD GEOLOGIST: Karl Primdahl SCREEN MATERIAL: PVC
SAMPLE INTERVAL

USCS SOIL CLASS.


% RECOVERY
DEPTH FEET

MOISTURE
PID VALUE

COLOR

TEMPORARY WELL
GEOLOGIC DESCRIPTION DIAGRAM
Brown Grass/Organic Topsoil M

90% <.01 SM Dark Brown Silty Sand-With Trace Gravel M PVC


2
RISER

CL Mottled Gray Brown Clay M


4

90% <.01
6

CL Brown Clay-Soft, Medium Plasticity M


8

90% <.01
10

12
End of Boring

14

16

18

20
BORING LOG
110 Spruce Street
AKT-104
St. Charles, Michigan Drawn By: John Warner
AKT Peerless Project No: 12716s Date: 8/24/2017
DRILLING COMPANY: AKT Peerless WEATHER: 79° Partly Sunny
TECHNICIAN: Karl Primdahl BORING DEPTH: 11'
DATE DRILLED: 08/22/17 DEPTH TO GW: NA
DRILLING METHOD: Push Probe SCREEN INTERVAL: NA
FIELD GEOLOGIST: Karl Primdahl SCREEN MATERIAL: NA
SAMPLE INTERVAL

USCS SOIL CLASS.


% RECOVERY
DEPTH FEET

MOISTURE
PID VALUE

COLOR

TEMPORARY WELL
GEOLOGIC DESCRIPTION DIAGRAM
Black Asphalt
90% 300 SM Brown Silty Sand-Stained, Strong Odor M
SM Brown Sand-Strong Odor M
2 60% 180

CL Brown Clay-Lean, Strong Odor M


4

90% <.01
6

8
CL Brownish Gray Clay-Medium Plasticity M

10

End of Boring
12

14

16

18

20
Appendix E
Laboratory Analytical Report
Wednesday, August 30, 2017

Fibertec Project Number: 80436


Project Identification: St. Charles/127165 /127165
Submittal Date: 08/24/2017

Mr. Karl Primdahl


AKT Peerless Environ. Svcs, Inc. - Saginaw
214 South Janes Ave.
Saginaw, MI 48607

Dear Mr. Primdahl,

Thank you for selecting Fibertec Environmental Services as your analytical laboratory. The samples you submitted have
been analyzed in accordance with NELAC standards and the results compiled in the attached report. Any exceptions to
NELAC compliance are noted in the report. These results apply only to those samples submitted. Please note TO-15
samples will be disposed of 10 calendar days after the reporting date. All other samples will be disposed of 30 days after the
reporting date.

If you have any questions regarding these results or if we may be of further assistance to you, please contact me at (517)
699-0345.

Sincerely,

By Emily Kennedy at 4:06 PM, Aug 30, 2017

For Daryl P. Strandbergh


Laboratory Director

Enclosures

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 2 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-001

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-104 8.5-9.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 1 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 12:05

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Water (Moisture) Content Dried at 105 ± 5°C Aliquot ID: 80436-001 Matrix: Soil/Solid
Method: ASTM D2216-10 Description: AKT-104 8.5-9.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Percent Moisture (Water Content) 20 % 1 1.0 08/25/17 MC170825 08/28/17 MC170825 BMG

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-001A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-104 8.5-9.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

1. Acetone U µg/kg 1000 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


‡ 2. Acrylonitrile U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
3. Benzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
4. Bromobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
5. Bromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
6. Bromodichloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
7. Bromoform U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
8. Bromomethane U µg/kg 300 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
9. 2-Butanone U µg/kg 750 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
10. n-Butylbenzene 490 µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
11. sec-Butylbenzene 120 µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
12. tert-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
13. Carbon Disulfide U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
14. Carbon Tetrachloride U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
15. Chlorobenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
16. Chloroethane U µg/kg 370 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
17. Chloroform U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
18. Chloromethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
19. 2-Chlorotoluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
20. Dibromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 21. 1,2-Dibromo-3-chloropropane (SIM) U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
22. Dibromomethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
23. 1,2-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
24. 1,3-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
25. 1,4-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
26. Dichlorodifluoromethane U µg/kg 370 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
27. 1,1-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
28. 1,2-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
29. 1,1-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
30. cis-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 3 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-001

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-104 8.5-9.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 1 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 12:05

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-001A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-104 8.5-9.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

31. trans-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


32. 1,2-Dichloropropane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
33. cis-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
34. trans-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
35. Ethylbenzene 310 µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
36. Ethylene Dibromide U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
37. 2-Hexanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
38. Isopropylbenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
39. Methylene Chloride U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 40. 2-Methylnaphthalene 750 µg/kg 370 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
41. 4-Methyl-2-pentanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
42. MTBE U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
43. Naphthalene 380 µg/kg 330 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
44. n-Propylbenzene 520 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
45. Styrene U µg/kg 74 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
46. 1,1,1,2-Tetrachloroethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
47. 1,1,2,2-Tetrachloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
48. Tetrachloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
49. Toluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
50. 1,2,4-Trichlorobenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
51. 1,1,1-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
52. 1,1,2-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
53. Trichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
54. Trichlorofluoromethane U L+ µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
55. 1,2,3-Trichloropropane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 56. 1,2,3-Trimethylbenzene 680 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
57. 1,2,4-Trimethylbenzene 3600 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
58. 1,3,5-Trimethylbenzene 1100 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
59. Vinyl Chloride U µg/kg 40 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
60. m&p-Xylene 2000 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
61. o-Xylene 640 µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 62. Xylenes 2600 µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 4 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-002

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-103 7.5-8.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 2 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 11:00

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Water (Moisture) Content Dried at 105 ± 5°C Aliquot ID: 80436-002 Matrix: Soil/Solid
Method: ASTM D2216-10 Description: AKT-103 7.5-8.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Percent Moisture (Water Content) 22 % 1 1.0 08/25/17 MC170825 08/28/17 MC170825 BMG

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-002A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-103 7.5-8.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

1. Acetone U µg/kg 1000 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


‡ 2. Acrylonitrile U µg/kg 160 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
3. Benzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
4. Bromobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
5. Bromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
6. Bromodichloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
7. Bromoform U µg/kg 160 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
8. Bromomethane U µg/kg 320 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
9. 2-Butanone U µg/kg 750 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
10. n-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
11. sec-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
12. tert-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
13. Carbon Disulfide U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
14. Carbon Tetrachloride U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
15. Chlorobenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
16. Chloroethane U µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
17. Chloroform U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
18. Chloromethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
19. 2-Chlorotoluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
20. Dibromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 21. 1,2-Dibromo-3-chloropropane (SIM) U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
22. Dibromomethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
23. 1,2-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
24. 1,3-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
25. 1,4-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
26. Dichlorodifluoromethane U µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
27. 1,1-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
28. 1,2-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
29. 1,1-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
30. cis-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 5 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-002

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-103 7.5-8.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 2 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 11:00

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-002A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-103 7.5-8.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

31. trans-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


32. 1,2-Dichloropropane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
33. cis-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
34. trans-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
35. Ethylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
36. Ethylene Dibromide U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
37. 2-Hexanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
38. Isopropylbenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
39. Methylene Chloride U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 40. 2-Methylnaphthalene U µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
41. 4-Methyl-2-pentanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
42. MTBE U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
43. Naphthalene U µg/kg 330 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
44. n-Propylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
45. Styrene U µg/kg 79 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
46. 1,1,1,2-Tetrachloroethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
47. 1,1,2,2-Tetrachloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
48. Tetrachloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
49. Toluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
50. 1,2,4-Trichlorobenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
51. 1,1,1-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
52. 1,1,2-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
53. Trichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
54. Trichlorofluoromethane U L+ µg/kg 160 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
55. 1,2,3-Trichloropropane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 56. 1,2,3-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
57. 1,2,4-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
58. 1,3,5-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
59. Vinyl Chloride U µg/kg 40 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
60. m&p-Xylene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
61. o-Xylene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 62. Xylenes U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 6 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-003

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-101 0.5-1.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 3 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 09:35

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Water (Moisture) Content Dried at 105 ± 5°C Aliquot ID: 80436-003 Matrix: Soil/Solid
Method: ASTM D2216-10 Description: AKT-101 0.5-1.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Percent Moisture (Water Content) 15 % 1 1.0 08/25/17 MC170825 08/28/17 MC170825 BMG

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-003A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-101 0.5-1.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

1. Acetone U µg/kg 1000 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


‡ 2. Acrylonitrile U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
3. Benzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
4. Bromobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
5. Bromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
6. Bromodichloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
7. Bromoform U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
8. Bromomethane U µg/kg 300 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
9. 2-Butanone U µg/kg 750 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
10. n-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
11. sec-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
12. tert-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
13. Carbon Disulfide U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
14. Carbon Tetrachloride U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
15. Chlorobenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
16. Chloroethane U µg/kg 370 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
17. Chloroform U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
18. Chloromethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
19. 2-Chlorotoluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
20. Dibromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 21. 1,2-Dibromo-3-chloropropane (SIM) U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
22. Dibromomethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
23. 1,2-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
24. 1,3-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
25. 1,4-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
26. Dichlorodifluoromethane U µg/kg 370 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
27. 1,1-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
28. 1,2-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
29. 1,1-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
30. cis-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 7 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-003

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-101 0.5-1.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 3 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 09:35

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-003A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-101 0.5-1.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

31. trans-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


32. 1,2-Dichloropropane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
33. cis-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
34. trans-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
35. Ethylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
36. Ethylene Dibromide U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
37. 2-Hexanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
38. Isopropylbenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
39. Methylene Chloride U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 40. 2-Methylnaphthalene U µg/kg 370 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
41. 4-Methyl-2-pentanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
42. MTBE U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
43. Naphthalene U µg/kg 330 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
44. n-Propylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
45. Styrene U µg/kg 74 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
46. 1,1,1,2-Tetrachloroethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
47. 1,1,2,2-Tetrachloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
48. Tetrachloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
49. Toluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
50. 1,2,4-Trichlorobenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
51. 1,1,1-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
52. 1,1,2-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
53. Trichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
54. Trichlorofluoromethane U L+ µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
55. 1,2,3-Trichloropropane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 56. 1,2,3-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
57. 1,2,4-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
58. 1,3,5-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
59. Vinyl Chloride U µg/kg 40 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
60. m&p-Xylene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
61. o-Xylene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 62. Xylenes U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 8 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-004

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-103 1.5-2.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 4 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 10:50

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Water (Moisture) Content Dried at 105 ± 5°C Aliquot ID: 80436-004 Matrix: Soil/Solid
Method: ASTM D2216-10 Description: AKT-103 1.5-2.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Percent Moisture (Water Content) 16 % 1 1.0 08/25/17 MC170825 08/28/17 MC170825 BMG

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-004A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-103 1.5-2.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

1. Acetone U µg/kg 1000 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


‡ 2. Acrylonitrile U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
3. Benzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
4. Bromobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
5. Bromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
6. Bromodichloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
7. Bromoform U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
8. Bromomethane U µg/kg 300 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
9. 2-Butanone U µg/kg 750 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
10. n-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
11. sec-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
12. tert-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
13. Carbon Disulfide U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
14. Carbon Tetrachloride U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
15. Chlorobenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
16. Chloroethane U µg/kg 380 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
17. Chloroform U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
18. Chloromethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
19. 2-Chlorotoluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
20. Dibromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 21. 1,2-Dibromo-3-chloropropane (SIM) U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
22. Dibromomethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
23. 1,2-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
24. 1,3-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
25. 1,4-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
26. Dichlorodifluoromethane U µg/kg 380 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
27. 1,1-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
28. 1,2-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
29. 1,1-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
30. cis-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 9 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-004

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-103 1.5-2.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 4 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 10:50

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-004A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-103 1.5-2.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

31. trans-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


32. 1,2-Dichloropropane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
33. cis-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
34. trans-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
35. Ethylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
36. Ethylene Dibromide U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
37. 2-Hexanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
38. Isopropylbenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
39. Methylene Chloride U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 40. 2-Methylnaphthalene U µg/kg 380 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
41. 4-Methyl-2-pentanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
42. MTBE U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
43. Naphthalene U µg/kg 330 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
44. n-Propylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
45. Styrene U µg/kg 76 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
46. 1,1,1,2-Tetrachloroethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
47. 1,1,2,2-Tetrachloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
48. Tetrachloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
49. Toluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
50. 1,2,4-Trichlorobenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
51. 1,1,1-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
52. 1,1,2-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
53. Trichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
54. Trichlorofluoromethane U L+ µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
55. 1,2,3-Trichloropropane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 56. 1,2,3-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
57. 1,2,4-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
58. 1,3,5-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
59. Vinyl Chloride U µg/kg 40 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
60. m&p-Xylene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
61. o-Xylene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 62. Xylenes U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 10 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-005

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-102 7.5-8.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 5 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 10:30

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Water (Moisture) Content Dried at 105 ± 5°C Aliquot ID: 80436-005 Matrix: Soil/Solid
Method: ASTM D2216-10 Description: AKT-102 7.5-8.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Percent Moisture (Water Content) 20 % 1 1.0 08/25/17 MC170825 08/28/17 MC170825 BMG

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-005A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-102 7.5-8.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

1. Acetone U µg/kg 1000 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


‡ 2. Acrylonitrile U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
3. Benzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
4. Bromobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
5. Bromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
6. Bromodichloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
7. Bromoform U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
8. Bromomethane U µg/kg 310 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
9. 2-Butanone U µg/kg 750 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
10. n-Butylbenzene 640 E µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
11. sec-Butylbenzene 180 µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
12. tert-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
13. Carbon Disulfide U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
14. Carbon Tetrachloride U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
15. Chlorobenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
16. Chloroethane U µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
17. Chloroform U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
18. Chloromethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
19. 2-Chlorotoluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
20. Dibromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 21. 1,2-Dibromo-3-chloropropane (SIM) U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
22. Dibromomethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
23. 1,2-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
24. 1,3-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
25. 1,4-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
26. Dichlorodifluoromethane U µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
27. 1,1-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
28. 1,2-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
29. 1,1-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
30. cis-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 11 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-005

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-102 7.5-8.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 5 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 10:30

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-005A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-102 7.5-8.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

31. trans-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


32. 1,2-Dichloropropane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
33. cis-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
34. trans-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
35. Ethylbenzene 200 µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
36. Ethylene Dibromide U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
37. 2-Hexanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
38. Isopropylbenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
39. Methylene Chloride U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 40. 2-Methylnaphthalene 1000 µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
41. 4-Methyl-2-pentanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
42. MTBE U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
43. Naphthalene U µg/kg 330 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
44. n-Propylbenzene 590 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
45. Styrene U µg/kg 77 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
46. 1,1,1,2-Tetrachloroethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
47. 1,1,2,2-Tetrachloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
48. Tetrachloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
49. Toluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
50. 1,2,4-Trichlorobenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
51. 1,1,1-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
52. 1,1,2-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
53. Trichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
54. Trichlorofluoromethane U L+ µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
55. 1,2,3-Trichloropropane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 56. 1,2,3-Trimethylbenzene 110 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
57. 1,2,4-Trimethylbenzene 2900 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
58. 1,3,5-Trimethylbenzene 960 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
59. Vinyl Chloride U µg/kg 40 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
60. m&p-Xylene 570 µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
61. o-Xylene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 62. Xylenes 570 µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 12 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-006

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-101 5.5-6.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 6 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 09:45

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Water (Moisture) Content Dried at 105 ± 5°C Aliquot ID: 80436-006 Matrix: Soil/Solid
Method: ASTM D2216-10 Description: AKT-101 5.5-6.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Percent Moisture (Water Content) 20 % 1 1.0 08/25/17 MC170825 08/28/17 MC170825 BMG

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-006A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-101 5.5-6.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

1. Acetone U µg/kg 1000 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


‡ 2. Acrylonitrile U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
3. Benzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
4. Bromobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
5. Bromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
6. Bromodichloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
7. Bromoform U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
8. Bromomethane U µg/kg 310 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
9. 2-Butanone U µg/kg 750 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
10. n-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
11. sec-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
12. tert-Butylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
13. Carbon Disulfide U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
14. Carbon Tetrachloride U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
15. Chlorobenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
16. Chloroethane U µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
17. Chloroform U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
18. Chloromethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
19. 2-Chlorotoluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
20. Dibromochloromethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 21. 1,2-Dibromo-3-chloropropane (SIM) U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
22. Dibromomethane U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
23. 1,2-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
24. 1,3-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
25. 1,4-Dichlorobenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
26. Dichlorodifluoromethane U µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
27. 1,1-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
28. 1,2-Dichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
29. 1,1-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
30. cis-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 13 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-006

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-101 5.5-6.5 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 6 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 09:45

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-006A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-101 5.5-6.5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

31. trans-1,2-Dichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


32. 1,2-Dichloropropane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
33. cis-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
34. trans-1,3-Dichloropropene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
35. Ethylbenzene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
36. Ethylene Dibromide U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
37. 2-Hexanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
38. Isopropylbenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
39. Methylene Chloride U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 40. 2-Methylnaphthalene U µg/kg 390 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
41. 4-Methyl-2-pentanone U µg/kg 2500 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
42. MTBE U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
43. Naphthalene U µg/kg 330 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
44. n-Propylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
45. Styrene U µg/kg 77 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
46. 1,1,1,2-Tetrachloroethane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
47. 1,1,2,2-Tetrachloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
48. Tetrachloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
49. Toluene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
50. 1,2,4-Trichlorobenzene U µg/kg 250 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
51. 1,1,1-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
52. 1,1,2-Trichloroethane U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
53. Trichloroethene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
54. Trichlorofluoromethane U L+ µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
55. 1,2,3-Trichloropropane U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 56. 1,2,3-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
57. 1,2,4-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
58. 1,3,5-Trimethylbenzene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
59. Vinyl Chloride U µg/kg 40 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
60. m&p-Xylene U µg/kg 100 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
61. o-Xylene U µg/kg 50 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 62. Xylenes U µg/kg 150 1.0 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 14 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-007

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-104 7-8 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 7 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 11:45

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Water (Moisture) Content Dried at 105 ± 5°C Aliquot ID: 80436-007 Matrix: Soil/Solid
Method: ASTM D2216-10 Description: AKT-104 7-8

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Percent Moisture (Water Content) 19 % 1 1.0 08/25/17 MC170825 08/28/17 MC170825 BMG

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-007A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-104 7-8

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

1. Acetone U µg/kg 1500 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


‡ 2. Acrylonitrile U µg/kg 1500 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
3. Benzene U µg/kg 180 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
4. Bromobenzene U µg/kg 740 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
5. Bromochloromethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
6. Bromodichloromethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
7. Bromoform U µg/kg 1500 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
8. Bromomethane U µg/kg 3000 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
9. 2-Butanone U µg/kg 1500 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
10. n-Butylbenzene 7400 E µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
11. sec-Butylbenzene 1400 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
12. tert-Butylbenzene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
13. Carbon Disulfide U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
14. Carbon Tetrachloride U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
15. Chlorobenzene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
16. Chloroethane U µg/kg 3700 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
17. Chloroform U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
18. Chloromethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
19. 2-Chlorotoluene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
20. Dibromochloromethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 21. 1,2-Dibromo-3-chloropropane (SIM) U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
22. Dibromomethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
23. 1,2-Dichlorobenzene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
24. 1,3-Dichlorobenzene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
25. 1,4-Dichlorobenzene U µg/kg 740 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
26. Dichlorodifluoromethane U µg/kg 3700 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
27. 1,1-Dichloroethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
28. 1,2-Dichloroethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
29. 1,1-Dichloroethene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
30. cis-1,2-Dichloroethene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 15 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-007

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-104 7-8 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 7 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Soil/Solid Collect Time: 11:45

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS, 5035 Aliquot ID: 80436-007A Matrix: Soil/Solid
Method: EPA 5035A/EPA 8260B Description: AKT-104 7-8

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

31. trans-1,2-Dichloroethene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB


32. 1,2-Dichloropropane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
33. cis-1,3-Dichloropropene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
34. trans-1,3-Dichloropropene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
35. Ethylbenzene 4500 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
36. Ethylene Dibromide U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
37. 2-Hexanone U µg/kg 2500 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
38. Isopropylbenzene 1300 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
39. Methylene Chloride U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 40. 2-Methylnaphthalene 16000 µg/kg 3700 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
41. 4-Methyl-2-pentanone U µg/kg 2500 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
42. MTBE U µg/kg 250 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
43. Naphthalene 4700 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
44. n-Propylbenzene 5500 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
45. Styrene U µg/kg 740 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
46. 1,1,1,2-Tetrachloroethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
47. 1,1,2,2-Tetrachloroethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
48. Tetrachloroethene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
49. Toluene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
50. 1,2,4-Trichlorobenzene U µg/kg 740 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
51. 1,1,1-Trichloroethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
52. 1,1,2-Trichloroethane U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
53. Trichloroethene U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
54. Trichlorofluoromethane U L+ µg/kg 1500 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
55. 1,2,3-Trichloropropane U µg/kg 740 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 56. 1,2,3-Trimethylbenzene 8000 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
57. 1,2,4-Trimethylbenzene 43000 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
58. 1,3,5-Trimethylbenzene 13000 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
59. Vinyl Chloride U µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
60. m&p-Xylene 18000 µg/kg 740 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
61. o-Xylene 1100 µg/kg 370 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB
‡ 62. Xylenes 19000 µg/kg 1100 10 08/25/17 VI17H25A 08/25/17 VI17H25A ANB

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 16 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-008

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-103 GW 6-11 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 8 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Surface Water Collect Time: 11:15

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS Aliquot ID: 80436-008A Matrix: Surface Water
Method: EPA 0624 Description: AKT-103 GW 6-11

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U µg/L 50 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES


2. Acrylonitrile U µg/L 2.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
3. Benzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 4. Bromobenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 5. Bromochloromethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
6. Bromodichloromethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
7. Bromoform U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
8. Bromomethane U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 9. 2-Butanone U µg/L 25 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 10. n-Butylbenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 11. sec-Butylbenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 12. tert-Butylbenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 13. Carbon Disulfide U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
14. Carbon Tetrachloride U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
15. Chlorobenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
16. Chloroethane U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
17. Chloroform U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
18. Chloromethane U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 19. 2-Chlorotoluene U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
20. Dibromochloromethane U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 21. 1,2-Dibromo-3-chloropropane (SIM) U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 22. Dibromomethane U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 23. 1,2-Dichlorobenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
24. 1,3-Dichlorobenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
25. 1,4-Dichlorobenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 26. Dichlorodifluoromethane U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
27. 1,1-Dichloroethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
28. 1,2-Dichloroethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
29. 1,1-Dichloroethene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 30. cis-1,2-Dichloroethene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
31. trans-1,2-Dichloroethene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
32. 1,2-Dichloropropane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
33. cis-1,3-Dichloropropene U µg/L 0.50 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
34. trans-1,3-Dichloropropene U µg/L 0.50 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
35. Ethylbenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 36. Ethylene Dibromide U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 37. 2-Hexanone U µg/L 50 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 17 of 18
Laboratory Project Number: 80436
Date: 08/30/17
Laboratory Sample Number: 80436-008

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT-103 GW 6-11 Chain of Custody: 156816
Inc. - Saginaw
Client Project Name: St. Charles/127165 Sample No: 8 Collect Date: 08/22/17

Client Project No: 127165 Sample Matrix: Surface Water Collect Time: 11:15

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

Volatile Organic Compounds (VOCs) by GC/MS Aliquot ID: 80436-008A Matrix: Surface Water
Method: EPA 0624 Description: AKT-103 GW 6-11

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 38. Isopropylbenzene U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
39. Methylene Chloride U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 40. 2-Methylnaphthalene U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 41. 4-Methyl-2-pentanone U µg/L 50 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 42. MTBE U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 43. Naphthalene U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 44. n-Propylbenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 45. Styrene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 46. 1,1,1,2-Tetrachloroethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
47. 1,1,2,2-Tetrachloroethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
48. Tetrachloroethene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
49. Toluene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 50. 1,2,4-Trichlorobenzene U µg/L 5.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
51. 1,1,1-Trichloroethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
52. 1,1,2-Trichloroethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
53. Trichloroethene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
54. Trichlorofluoromethane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 55. 1,2,3-Trichloropropane U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 56. 1,2,3-Trimethylbenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 57. 1,2,4-Trimethylbenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 58. 1,3,5-Trimethylbenzene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
59. Vinyl Chloride U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 60. m&p-Xylene U µg/L 2.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 61. o-Xylene U µg/L 1.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES
‡ 62. Xylenes U µg/L 3.0 1.0 08/28/17 VM17H28A 08/28/17 VM17H28A MES

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Analytical Laboratory Report Order: 80436
Page: 18 of 18
Laboratory Project Number: 80436
Date: 08/30/17

Definitions/ Qualifiers:

A: Spike recovery or precision unusable due to dilution.


B: The analyte was detected in the associated method blank.
E: The analyte was detected at a concentration greater than the calibration range, therefore the result is estimated.
J: The concentration is an estimated value.
M: Modified Method
U: The analyte was not detected at or above the reporting limit.
X: Matrix Interference has resulted in a raised reporting limit or distorted result.
W: Results reported on a wet-weight basis.
*: Value reported is outside QC limits

Exception Summary:
E : This flag identifies compounds whose response exceed the response of the highest standard in the initial calibration
range of the instrument for that specific analysis.
L+ : Recovery in the associated laboratory sample (LCS) exceeds the upper control limit. Results may be biased high.

Accreditation Number(s):

T104704518-17-6 (TX)

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80436-170830160458


Friday, August 25, 2017

Fibertec Project Number: 80326


Project Identification: Village Of St. Charles/127165 /127165
Submittal Date: 08/18/2017

Mr. Karl Primdahl


AKT Peerless Environ. Svcs, Inc. - Saginaw
214 South Janes Ave.
Saginaw, MI 48607

Dear Mr. Primdahl,

Thank you for selecting Fibertec Environmental Services as your analytical laboratory. The samples you submitted have
been analyzed in accordance with NELAC standards and the results compiled in the attached report. Any exceptions to
NELAC compliance are noted in the report. These results apply only to those samples submitted. Please note TO-15
samples will be disposed of 10 calendar days after the reporting date. All other samples will be disposed of 30 days after the
reporting date.

If you have any questions regarding these results or if we may be of further assistance to you, please contact me at (517)
699-0345.

Sincerely,

By Emily Kennedy at 10:39 AM, Aug 25, 2017

For Daryl P. Strandbergh


Laboratory Director

Enclosures

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 2 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-001

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-3 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2195 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 11:27

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-001 Matrix: Air


Method: EPA TO-15 Description: AKTV1-3

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


2. Benzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
3. Benzyl Chloride U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
4. Bromodichloromethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
5. Bromoform U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
6. Bromomethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
7. 1,3-Butadiene U ppbv 0.30 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
8. 2-Butanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 9. Carbon Disulfide U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
10. Carbon Tetrachloride U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
11. Chlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
12. Chloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
13. Chloroform U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
14. Chloromethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
15. Cyclohexane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
16. Dibromochloromethane U ppbv 0.48 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
17. 1,2-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
20. Dichlorodifluoromethane 45 ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
21. 1,1-Dichloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
22. 1,2-Dichloroethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
23. 1,1-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
24. cis-1,2-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
26. 1,2-Dichloropropane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
27. cis-1,3-Dichloropropene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
28. trans-1,3-Dichloropropene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
29. 1,4-Dioxane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 30. Ethyl Acetate U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
31. Ethylbenzene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
32. Ethylene Dibromide U ppbv 0.12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
33. n-Heptane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
34. Hexachlorobutadiene U ppbv 3.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
35. n-Hexane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 36. 2-Hexanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 37. Isopropanol U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 3 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-001

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-3 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2195 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 11:27

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-001 Matrix: Air


Method: EPA TO-15 Description: AKTV1-3

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 39. 2-Methylnaphthalene U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
40. 4-Methyl-2-pentanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
41. MTBE U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 42. Naphthalene U ppbv 5.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
43. Styrene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
45. Tetrachloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 46. Tetrahydrofuran U ppbv 3.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
47. Toluene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
48. 1,2,4-Trichlorobenzene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
50. 1,1,2-Trichloroethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
51. Trichloroethene U ppbv 0.30 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
52. Trichlorofluoromethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
54. 1,2,4-Trimethylbenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
55. 1,3,5-Trimethylbenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
56. Vinyl Acetate U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
57. Vinyl Chloride U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
58. m&p-Xylene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
59. o-Xylene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 60. Xylenes U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 4 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-002

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-6 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2496 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 11:55

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-002 Matrix: Air


Method: EPA TO-15 Description: AKTV1-6

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


2. Benzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
3. Benzyl Chloride U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
4. Bromodichloromethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
5. Bromoform U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
6. Bromomethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
7. 1,3-Butadiene U ppbv 0.30 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
8. 2-Butanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 9. Carbon Disulfide U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
10. Carbon Tetrachloride U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
11. Chlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
12. Chloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
13. Chloroform U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
14. Chloromethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
15. Cyclohexane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
16. Dibromochloromethane U ppbv 0.48 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
17. 1,2-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
20. Dichlorodifluoromethane 15 ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
21. 1,1-Dichloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
22. 1,2-Dichloroethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
23. 1,1-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
24. cis-1,2-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
26. 1,2-Dichloropropane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
27. cis-1,3-Dichloropropene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
28. trans-1,3-Dichloropropene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
29. 1,4-Dioxane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 30. Ethyl Acetate U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
31. Ethylbenzene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
32. Ethylene Dibromide U ppbv 0.12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
33. n-Heptane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
34. Hexachlorobutadiene U ppbv 3.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
35. n-Hexane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 36. 2-Hexanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 37. Isopropanol U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 5 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-002

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-6 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2496 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 11:55

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-002 Matrix: Air


Method: EPA TO-15 Description: AKTV1-6

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 39. 2-Methylnaphthalene U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
40. 4-Methyl-2-pentanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
41. MTBE U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 42. Naphthalene U ppbv 5.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
43. Styrene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
45. Tetrachloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 46. Tetrahydrofuran U ppbv 3.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
47. Toluene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
48. 1,2,4-Trichlorobenzene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
50. 1,1,2-Trichloroethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
51. Trichloroethene U ppbv 0.30 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
52. Trichlorofluoromethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
54. 1,2,4-Trimethylbenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
55. 1,3,5-Trimethylbenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
56. Vinyl Acetate U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
57. Vinyl Chloride U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
58. m&p-Xylene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
59. o-Xylene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 60. Xylenes U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 6 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-003

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-8 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2495 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 12:23

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-003 Matrix: Air


Method: EPA TO-15 Description: AKTV1-8

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


2. Benzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
3. Benzyl Chloride U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
4. Bromodichloromethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
5. Bromoform U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
6. Bromomethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
7. 1,3-Butadiene U ppbv 0.30 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
8. 2-Butanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 9. Carbon Disulfide U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
10. Carbon Tetrachloride U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
11. Chlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
12. Chloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
13. Chloroform U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
14. Chloromethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
15. Cyclohexane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
16. Dibromochloromethane U ppbv 0.48 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
17. 1,2-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
20. Dichlorodifluoromethane 100 ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
21. 1,1-Dichloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
22. 1,2-Dichloroethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
23. 1,1-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
24. cis-1,2-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
26. 1,2-Dichloropropane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
27. cis-1,3-Dichloropropene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
28. trans-1,3-Dichloropropene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
29. 1,4-Dioxane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 30. Ethyl Acetate U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
31. Ethylbenzene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
32. Ethylene Dibromide U ppbv 0.12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
33. n-Heptane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
34. Hexachlorobutadiene U ppbv 3.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
35. n-Hexane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 36. 2-Hexanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 37. Isopropanol U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 7 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-003

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-8 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2495 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 12:23

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-003 Matrix: Air


Method: EPA TO-15 Description: AKTV1-8

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 39. 2-Methylnaphthalene U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
40. 4-Methyl-2-pentanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
41. MTBE U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 42. Naphthalene U ppbv 5.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
43. Styrene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
45. Tetrachloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 46. Tetrahydrofuran U ppbv 3.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
47. Toluene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
48. 1,2,4-Trichlorobenzene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
50. 1,1,2-Trichloroethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
51. Trichloroethene U ppbv 0.30 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
52. Trichlorofluoromethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
54. 1,2,4-Trimethylbenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
55. 1,3,5-Trimethylbenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
56. Vinyl Acetate U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
57. Vinyl Chloride U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
58. m&p-Xylene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
59. o-Xylene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 60. Xylenes U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 8 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-004

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-7 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2390 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 12:05

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-004 Matrix: Air


Method: EPA TO-15 Description: AKTV1-7

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


2. Benzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
3. Benzyl Chloride U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
4. Bromodichloromethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
5. Bromoform U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
6. Bromomethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
7. 1,3-Butadiene U ppbv 0.30 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
8. 2-Butanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 9. Carbon Disulfide U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
10. Carbon Tetrachloride U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
11. Chlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
12. Chloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
13. Chloroform U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
14. Chloromethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
15. Cyclohexane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
16. Dibromochloromethane U ppbv 0.48 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
17. 1,2-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
20. Dichlorodifluoromethane 83 ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
21. 1,1-Dichloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
22. 1,2-Dichloroethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
23. 1,1-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
24. cis-1,2-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
26. 1,2-Dichloropropane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
27. cis-1,3-Dichloropropene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
28. trans-1,3-Dichloropropene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
29. 1,4-Dioxane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 30. Ethyl Acetate U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
31. Ethylbenzene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
32. Ethylene Dibromide U ppbv 0.12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
33. n-Heptane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
34. Hexachlorobutadiene U ppbv 3.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
35. n-Hexane U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 36. 2-Hexanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 37. Isopropanol U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 9 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-004

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-7 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2390 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 12:05

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-004 Matrix: Air


Method: EPA TO-15 Description: AKTV1-7

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 39. 2-Methylnaphthalene U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
40. 4-Methyl-2-pentanone U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
41. MTBE U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 42. Naphthalene U ppbv 5.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
43. Styrene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
45. Tetrachloroethene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 46. Tetrahydrofuran U ppbv 3.3 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
47. Toluene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
48. 1,2,4-Trichlorobenzene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
50. 1,1,2-Trichloroethane U ppbv 1.2 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
51. Trichloroethene U ppbv 0.30 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
52. Trichlorofluoromethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
54. 1,2,4-Trimethylbenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
55. 1,3,5-Trimethylbenzene U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
56. Vinyl Acetate U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
57. Vinyl Chloride U ppbv 6.0 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
58. m&p-Xylene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
59. o-Xylene U ppbv 12 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 60. Xylenes U ppbv 24 4.0 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 10 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-005

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-2 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 497 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 10:51

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-005 Matrix: Air


Method: EPA TO-15 Description: AKTV1-2

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 52 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


2. Benzene U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
3. Benzyl Chloride U ppbv 2.7 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
4. Bromodichloromethane U ppbv 1.2 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
5. Bromoform U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
6. Bromomethane U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
7. 1,3-Butadiene U ppbv 2.7 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
8. 2-Butanone U ppbv 12 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 9. Carbon Disulfide U ppbv 31 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
10. Carbon Tetrachloride U ppbv 2.7 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
11. Chlorobenzene U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
12. Chloroethane U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
13. Chloroform U ppbv 1.2 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
14. Chloromethane U ppbv 10 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
15. Cyclohexane U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
16. Dibromochloromethane U ppbv 1.1 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
17. 1,2-Dichlorobenzene U ppbv 11 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
20. Dichlorodifluoromethane 2200 ppbv 63 78 08/23/17 VK17H23A 08/23/17 VK17H23A LDS
21. 1,1-Dichloroethane U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
22. 1,2-Dichloroethane U ppbv 2.7 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
23. 1,1-Dichloroethene U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
24. cis-1,2-Dichloroethene U ppbv 10 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
26. 1,2-Dichloropropane U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
27. cis-1,3-Dichloropropene U ppbv 11 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
28. trans-1,3-Dichloropropene U ppbv 10 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
29. 1,4-Dioxane U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 30. Ethyl Acetate U ppbv 12 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
31. Ethylbenzene U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
32. Ethylene Dibromide U ppbv 1.1 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
33. n-Heptane U ppbv 12 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
34. Hexachlorobutadiene U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
35. n-Hexane U ppbv 12 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 36. 2-Hexanone U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 37. Isopropanol U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 11 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-005

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-2 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 497 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 10:51

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-005 Matrix: Air


Method: EPA TO-15 Description: AKTV1-2

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 51 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


‡ 39. 2-Methylnaphthalene U ppbv 110 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
40. 4-Methyl-2-pentanone U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
41. MTBE U ppbv 11 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 42. Naphthalene U ppbv 11 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
43. Styrene U ppbv 54 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 1.1 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
45. Tetrachloroethene 7.0 ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 46. Tetrahydrofuran U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
47. Toluene U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
48. 1,2,4-Trichlorobenzene U ppbv 53 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
50. 1,1,2-Trichloroethane U ppbv 1.2 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
51. Trichloroethene U ppbv 1.1 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
52. Trichlorofluoromethane 15 ppbv 11 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
54. 1,2,4-Trimethylbenzene U ppbv 11 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
55. 1,3,5-Trimethylbenzene U ppbv 11 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
56. Vinyl Acetate U ppbv 54 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
57. Vinyl Chloride U ppbv 6.0 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
58. m&p-Xylene U ppbv 63 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
59. o-Xylene U ppbv 32 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 60. Xylenes U ppbv 96 39 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 12 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-006

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-5 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 484 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 11:11

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-006 Matrix: Air


Method: EPA TO-15 Description: AKTV1-5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


2. Benzene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
3. Benzyl Chloride U ppbv 1.2 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
4. Bromodichloromethane U ppbv 1.2 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
5. Bromoform U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
6. Bromomethane U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
7. 1,3-Butadiene U ppbv 1.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
8. 2-Butanone U ppbv 12 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 9. Carbon Disulfide U ppbv 12 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
10. Carbon Tetrachloride U ppbv 1.2 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
11. Chlorobenzene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
12. Chloroethane U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
13. Chloroform U ppbv 1.2 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
14. Chloromethane U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
15. Cyclohexane U ppbv 13 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
16. Dibromochloromethane U ppbv 0.48 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
17. 1,2-Dichlorobenzene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
20. Dichlorodifluoromethane 650 ppbv 15 19 08/23/17 VK17H23A 08/23/17 VK17H23A LDS
21. 1,1-Dichloroethane U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
22. 1,2-Dichloroethane U ppbv 1.2 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
23. 1,1-Dichloroethene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
24. cis-1,2-Dichloroethene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
26. 1,2-Dichloropropane U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
27. cis-1,3-Dichloropropene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
28. trans-1,3-Dichloropropene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
29. 1,4-Dioxane U ppbv 12 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 30. Ethyl Acetate U ppbv 12 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
31. Ethylbenzene U ppbv 13 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
32. Ethylene Dibromide U ppbv 0.42 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
33. n-Heptane U ppbv 12 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
34. Hexachlorobutadiene U ppbv 13 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
35. n-Hexane U ppbv 12 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 36. 2-Hexanone U ppbv 13 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 37. Isopropanol U ppbv 13 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 13 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-006

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-5 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 484 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 11:11

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-006 Matrix: Air


Method: EPA TO-15 Description: AKTV1-5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 20 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


‡ 39. 2-Methylnaphthalene U ppbv 42 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
40. 4-Methyl-2-pentanone U ppbv 12 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
41. MTBE U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 42. Naphthalene U ppbv 5.3 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
43. Styrene U ppbv 21 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
45. Tetrachloroethene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 46. Tetrahydrofuran U ppbv 12 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
47. Toluene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
48. 1,2,4-Trichlorobenzene U ppbv 21 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
50. 1,1,2-Trichloroethane U ppbv 1.2 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
51. Trichloroethene U ppbv 0.41 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
52. Trichlorofluoromethane 13 ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
54. 1,2,4-Trimethylbenzene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
55. 1,3,5-Trimethylbenzene U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
56. Vinyl Acetate U ppbv 21 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
57. Vinyl Chloride U ppbv 6.0 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
58. m&p-Xylene U ppbv 25 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
59. o-Xylene U ppbv 13 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 60. Xylenes U ppbv 37 15 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 14 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-007

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-4 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2332 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 11:37

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-007 Matrix: Air


Method: EPA TO-15 Description: AKTV1-4

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 41 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


2. Benzene U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
3. Benzyl Chloride U ppbv 2.1 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
4. Bromodichloromethane U ppbv 1.2 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
5. Bromoform U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
6. Bromomethane U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
7. 1,3-Butadiene U ppbv 2.1 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
8. 2-Butanone U ppbv 12 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 9. Carbon Disulfide U ppbv 25 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
10. Carbon Tetrachloride U ppbv 2.1 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
11. Chlorobenzene U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
12. Chloroethane U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
13. Chloroform U ppbv 1.2 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
14. Chloromethane U ppbv 8.3 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
15. Cyclohexane U ppbv 26 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
16. Dibromochloromethane U ppbv 0.84 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
17. 1,2-Dichlorobenzene U ppbv 8.4 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
20. Dichlorodifluoromethane 1200 ppbv 25 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
21. 1,1-Dichloroethane U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
22. 1,2-Dichloroethane U ppbv 2.1 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
23. 1,1-Dichloroethene U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
24. cis-1,2-Dichloroethene U ppbv 8.3 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
26. 1,2-Dichloropropane U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
27. cis-1,3-Dichloropropene U ppbv 8.5 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
28. trans-1,3-Dichloropropene U ppbv 8.2 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
29. 1,4-Dioxane U ppbv 25 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 30. Ethyl Acetate U ppbv 12 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
31. Ethylbenzene U ppbv 26 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
32. Ethylene Dibromide U ppbv 0.87 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
33. n-Heptane U ppbv 12 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
34. Hexachlorobutadiene U ppbv 26 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
35. n-Hexane U ppbv 12 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 36. 2-Hexanone U ppbv 26 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 37. Isopropanol U ppbv 26 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 15 of 16
Laboratory Project Number: 80326
Date: 08/25/17
Laboratory Sample Number: 80326-007

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKTV1-4 Chain of Custody: 156822
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: 2332 Collect Date: 08/17/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 11:37

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 80326-007 Matrix: Air


Method: EPA TO-15 Description: AKTV1-4

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 40 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS


‡ 39. 2-Methylnaphthalene U ppbv 85 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
40. 4-Methyl-2-pentanone U ppbv 25 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
41. MTBE U ppbv 8.5 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 42. Naphthalene U ppbv 8.5 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
43. Styrene U ppbv 43 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.87 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
45. Tetrachloroethene U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 46. Tetrahydrofuran U ppbv 25 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
47. Toluene U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
48. 1,2,4-Trichlorobenzene U ppbv 42 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
50. 1,1,2-Trichloroethane U ppbv 1.2 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
51. Trichloroethene U ppbv 0.84 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
52. Trichlorofluoromethane 8.8 ppbv 8.5 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
54. 1,2,4-Trimethylbenzene U ppbv 8.4 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
55. 1,3,5-Trimethylbenzene U ppbv 8.4 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
56. Vinyl Acetate U ppbv 43 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
57. Vinyl Chloride U ppbv 6.0 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
58. m&p-Xylene U ppbv 50 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
59. o-Xylene U ppbv 26 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS
‡ 60. Xylenes U ppbv 76 31 08/22/17 VK17H22A 08/22/17 VK17H22A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Analytical Laboratory Report Order: 80326
Page: 16 of 16
Laboratory Project Number: 80326
Date: 08/25/17

Definitions/ Qualifiers:

A: Spike recovery or precision unusable due to dilution.


B: The analyte was detected in the associated method blank.
E: The analyte was detected at a concentration greater than the calibration range, therefore the result is estimated.
J: The concentration is an estimated value.
M: Modified Method
U: The analyte was not detected at or above the reporting limit.
X: Matrix Interference has resulted in a raised reporting limit or distorted result.
W: Results reported on a wet-weight basis.
*: Value reported is outside QC limits

Exception Summary:

Accreditation Number(s):

T104704518-17-6 (TX)

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 80326-170825103102


Thursday, December 07, 2017

Fibertec Project Number: 82097


Project Identification: Village Of St. Charles/127165 /127165
Submittal Date: 11/30/2017

Mr. Karl Primdahl


AKT Peerless Environ. Svcs, Inc. - Saginaw
214 South Janes Ave.
Saginaw, MI 48607

Dear Mr. Primdahl,

Thank you for selecting Fibertec Environmental Services as your analytical laboratory. The samples you submitted have
been analyzed in accordance with NELAC standards and the results compiled in the attached report. Any exceptions to
NELAC compliance are noted in the report. These results apply only to those samples submitted. Please note TO-15
samples will be disposed of 10 calendar days after the reporting date. All other samples will be disposed of 30 days after
the reporting date.

If you have any questions regarding these results or if we may be of further assistance to you, please contact me at (517)
699-0345.

Sincerely,

By Natalie Zaleski at 2:41 PM, Dec 07, 2017

For Daryl P. Strandbergh


Laboratory Director

Enclosures

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 2 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-001

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-8 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 08:49

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-001 Matrix: Air


Method: EPA TO-15 Description: AKT VI-8

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG


2. Benzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
3. Benzyl Chloride U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
4. Bromodichloromethane U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
5. Bromoform U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
6. Bromomethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
7. 1,3-Butadiene U ppbv 0.30 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
8. 2-Butanone U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 9. Carbon Disulfide U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
10. Carbon Tetrachloride U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
11. Chlorobenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
12. Chloroethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
13. Chloroform U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
14. Chloromethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
15. Cyclohexane U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
16. Dibromochloromethane U ppbv 0.48 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
17. 1,2-Dichlorobenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
18. 1,3-Dichlorobenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
19. 1,4-Dichlorobenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
20. Dichlorodifluoromethane 25 ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
21. 1,1-Dichloroethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
22. 1,2-Dichloroethane U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
23. 1,1-Dichloroethene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
24. cis-1,2-Dichloroethene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
25. trans-1,2-Dichloroethene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
26. 1,2-Dichloropropane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
27. cis-1,3-Dichloropropene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
28. trans-1,3-Dichloropropene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
29. 1,4-Dioxane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 30. Ethyl Acetate U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
31. Ethylbenzene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
32. Ethylene Dibromide U ppbv 0.12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
33. n-Heptane U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
34. Hexachlorobutadiene U ppbv 0.48 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
35. n-Hexane U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 36. 2-Hexanone U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 37. Isopropanol U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 3 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-001

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-8 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 08:49

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-001 Matrix: Air


Method: EPA TO-15 Description: AKT VI-8

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 39. 2-Methylnaphthalene U ppbv 24 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
40. 4-Methyl-2-pentanone U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
41. MTBE U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 42. Naphthalene U ppbv 5.3 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
43. Styrene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
45. Tetrachloroethene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 46. Tetrahydrofuran U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
47. Toluene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
48. 1,2,4-Trichlorobenzene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
49. 1,1,1-Trichloroethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
50. 1,1,2-Trichloroethane U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
51. Trichloroethene U ppbv 0.30 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
52. Trichlorofluoromethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
54. 1,2,4-Trimethylbenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
55. 1,3,5-Trimethylbenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
56. Vinyl Acetate U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
57. Vinyl Chloride U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
58. m&p-Xylene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
59. o-Xylene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 60. Xylenes U ppbv 24 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 4 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-002

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-3 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 09:29

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-002 Matrix: Air


Method: EPA TO-15 Description: AKT VI-3

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG


2. Benzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
3. Benzyl Chloride U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
4. Bromodichloromethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
5. Bromoform U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
6. Bromomethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
7. 1,3-Butadiene U ppbv 0.54 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
8. 2-Butanone U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 9. Carbon Disulfide U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
10. Carbon Tetrachloride U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
11. Chlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
12. Chloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
13. Chloroform U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
14. Chloromethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
15. Cyclohexane U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
16. Dibromochloromethane U ppbv 0.54 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
17. 1,2-Dichlorobenzene U ppbv 6.5 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
18. 1,3-Dichlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
19. 1,4-Dichlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
20. Dichlorodifluoromethane 160 ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
21. 1,1-Dichloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
22. 1,2-Dichloroethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
23. 1,1-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
24. cis-1,2-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
25. trans-1,2-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
26. 1,2-Dichloropropane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
27. cis-1,3-Dichloropropene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
28. trans-1,3-Dichloropropene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
29. 1,4-Dioxane U ppbv 6.5 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 30. Ethyl Acetate U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
31. Ethylbenzene U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
32. Ethylene Dibromide U ppbv 0.22 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
33. n-Heptane U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
34. Hexachlorobutadiene U ppbv 0.48 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
35. n-Hexane U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 36. 2-Hexanone U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 37. Isopropanol U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 5 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-002

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-3 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 09:29

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-002 Matrix: Air


Method: EPA TO-15 Description: AKT VI-3

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 39. 2-Methylnaphthalene U ppbv 24 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
40. 4-Methyl-2-pentanone U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
41. MTBE U ppbv 6.6 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 42. Naphthalene U ppbv 5.3 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
43. Styrene U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
45. Tetrachloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 46. Tetrahydrofuran U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
47. Toluene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
48. 1,2,4-Trichlorobenzene U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
49. 1,1,1-Trichloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
50. 1,1,2-Trichloroethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
51. Trichloroethene U ppbv 0.30 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
52. Trichlorofluoromethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
54. 1,2,4-Trimethylbenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
55. 1,3,5-Trimethylbenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
56. Vinyl Acetate U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
57. Vinyl Chloride U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
58. m&p-Xylene U ppbv 13 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
59. o-Xylene U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 60. Xylenes U ppbv 24 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 6 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-003

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-6 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 09:41

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-003 Matrix: Air


Method: EPA TO-15 Description: AKT VI-6

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG


2. Benzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
3. Benzyl Chloride U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
4. Bromodichloromethane U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
5. Bromoform U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
6. Bromomethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
7. 1,3-Butadiene U ppbv 0.30 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
8. 2-Butanone U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 9. Carbon Disulfide U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
10. Carbon Tetrachloride U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
11. Chlorobenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
12. Chloroethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
13. Chloroform U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
14. Chloromethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
15. Cyclohexane U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
16. Dibromochloromethane U ppbv 0.48 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
17. 1,2-Dichlorobenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
18. 1,3-Dichlorobenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
19. 1,4-Dichlorobenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
20. Dichlorodifluoromethane 17 ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
21. 1,1-Dichloroethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
22. 1,2-Dichloroethane U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
23. 1,1-Dichloroethene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
24. cis-1,2-Dichloroethene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
25. trans-1,2-Dichloroethene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
26. 1,2-Dichloropropane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
27. cis-1,3-Dichloropropene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
28. trans-1,3-Dichloropropene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
29. 1,4-Dioxane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 30. Ethyl Acetate U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
31. Ethylbenzene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
32. Ethylene Dibromide U ppbv 0.12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
33. n-Heptane U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
34. Hexachlorobutadiene U ppbv 0.48 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
35. n-Hexane U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 36. 2-Hexanone U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 37. Isopropanol U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 7 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-003

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-6 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 09:41

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-003 Matrix: Air


Method: EPA TO-15 Description: AKT VI-6

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 39. 2-Methylnaphthalene U ppbv 24 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
40. 4-Methyl-2-pentanone U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
41. MTBE U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 42. Naphthalene U ppbv 5.3 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
43. Styrene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
45. Tetrachloroethene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 46. Tetrahydrofuran U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
47. Toluene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
48. 1,2,4-Trichlorobenzene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
49. 1,1,1-Trichloroethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
50. 1,1,2-Trichloroethane U ppbv 1.2 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
51. Trichloroethene U ppbv 0.30 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
52. Trichlorofluoromethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
54. 1,2,4-Trimethylbenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
55. 1,3,5-Trimethylbenzene U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
56. Vinyl Acetate U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
57. Vinyl Chloride U ppbv 6.0 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
58. m&p-Xylene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
59. o-Xylene U ppbv 12 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 60. Xylenes U ppbv 24 4.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 8 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-004

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-4 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 09:48

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-004 Matrix: Air


Method: EPA TO-15 Description: AKT VI-4

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG


2. Benzene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
3. Benzyl Chloride U ppbv 1.2 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
4. Bromodichloromethane U ppbv 1.2 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
5. Bromoform U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
6. Bromomethane U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
7. 1,3-Butadiene U ppbv 1.2 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
8. 2-Butanone U ppbv 25 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 9. Carbon Disulfide U ppbv 24 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
10. Carbon Tetrachloride U ppbv 1.2 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
11. Chlorobenzene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
12. Chloroethane U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
13. Chloroform U ppbv 1.2 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
14. Chloromethane U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
15. Cyclohexane U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
16. Dibromochloromethane U ppbv 1.2 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
17. 1,2-Dichlorobenzene U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
18. 1,3-Dichlorobenzene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
19. 1,4-Dichlorobenzene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
20. Dichlorodifluoromethane 700 ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
21. 1,1-Dichloroethane U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
22. 1,2-Dichloroethane U ppbv 1.2 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
23. 1,1-Dichloroethene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
24. cis-1,2-Dichloroethene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
25. trans-1,2-Dichloroethene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
26. 1,2-Dichloropropane U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
27. cis-1,3-Dichloropropene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
28. trans-1,3-Dichloropropene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
29. 1,4-Dioxane U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 30. Ethyl Acetate U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
31. Ethylbenzene U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
32. Ethylene Dibromide U ppbv 0.50 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
33. n-Heptane U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
34. Hexachlorobutadiene U ppbv 0.50 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
35. n-Hexane U ppbv 24 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 36. 2-Hexanone U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 37. Isopropanol U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 9 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-004

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-4 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 09:48

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-004 Matrix: Air


Method: EPA TO-15 Description: AKT VI-4

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 23 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG


‡ 39. 2-Methylnaphthalene U ppbv 25 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
40. 4-Methyl-2-pentanone U ppbv 24 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
41. MTBE U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 42. Naphthalene U ppbv 5.3 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
43. Styrene U ppbv 25 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
44. 1,1,2,2-Tetrachloroethane U ppbv 0.50 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
45. Tetrachloroethene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 46. Tetrahydrofuran U ppbv 1.9 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
47. Toluene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
48. 1,2,4-Trichlorobenzene U ppbv 24 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
49. 1,1,1-Trichloroethane U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
50. 1,1,2-Trichloroethane U ppbv 1.2 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
51. Trichloroethene U ppbv 0.48 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
52. Trichlorofluoromethane 15 ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
54. 1,2,4-Trimethylbenzene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
55. 1,3,5-Trimethylbenzene U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
56. Vinyl Acetate U ppbv 25 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
57. Vinyl Chloride U ppbv 6.0 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
58. m&p-Xylene U ppbv 29 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
59. o-Xylene U ppbv 15 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 60. Xylenes U ppbv 44 18 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 10 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-005

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-9 (Temp) Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 10:06

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-005 Matrix: Air


Method: EPA TO-15 Description: AKT VI-9 (Temp)

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG


2. Benzene 30 ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
3. Benzyl Chloride U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
4. Bromodichloromethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
5. Bromoform U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
6. Bromomethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
7. 1,3-Butadiene 10 ppbv 0.54 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
8. 2-Butanone U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 9. Carbon Disulfide U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
10. Carbon Tetrachloride U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
11. Chlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
12. Chloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
13. Chloroform U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
14. Chloromethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
15. Cyclohexane 48 ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
16. Dibromochloromethane U ppbv 0.54 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
17. 1,2-Dichlorobenzene U ppbv 6.5 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
18. 1,3-Dichlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
19. 1,4-Dichlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
20. Dichlorodifluoromethane 27 ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
21. 1,1-Dichloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
22. 1,2-Dichloroethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
23. 1,1-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
24. cis-1,2-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
25. trans-1,2-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
26. 1,2-Dichloropropane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
27. cis-1,3-Dichloropropene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
28. trans-1,3-Dichloropropene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
29. 1,4-Dioxane U ppbv 6.5 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 30. Ethyl Acetate U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
31. Ethylbenzene 35 ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
32. Ethylene Dibromide U ppbv 0.22 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
33. n-Heptane 100 ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
34. Hexachlorobutadiene U ppbv 0.48 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
35. n-Hexane 160 ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 36. 2-Hexanone U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 37. Isopropanol U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 11 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-005

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-9 (Temp) Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 10:06

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-005 Matrix: Air


Method: EPA TO-15 Description: AKT VI-9 (Temp)

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 39. 2-Methylnaphthalene U ppbv 24 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
40. 4-Methyl-2-pentanone U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
41. MTBE U ppbv 6.6 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 42. Naphthalene 16 ppbv 5.3 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
43. Styrene U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
45. Tetrachloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 46. Tetrahydrofuran U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
47. Toluene 100 ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
48. 1,2,4-Trichlorobenzene U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
49. 1,1,1-Trichloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
50. 1,1,2-Trichloroethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
51. Trichloroethene U ppbv 0.30 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
52. Trichlorofluoromethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
54. 1,2,4-Trimethylbenzene 130 ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
55. 1,3,5-Trimethylbenzene 47 ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
56. Vinyl Acetate U ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
57. Vinyl Chloride U ppbv 6.0 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
58. m&p-Xylene 140 ppbv 13 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
59. o-Xylene 67 ppbv 12 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG
‡ 60. Xylenes 210 ppbv 24 8.0 12/04/17 VA17L04A 12/04/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 12 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-006

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-5 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 10:12

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-006 Matrix: Air


Method: EPA TO-15 Description: AKT VI-5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 39 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS


2. Benzene U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
3. Benzyl Chloride U ppbv 2.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
4. Bromodichloromethane U ppbv 1.9 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
5. Bromoform U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
6. Bromomethane U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
7. 1,3-Butadiene U ppbv 2.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
8. 2-Butanone U ppbv 12 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 9. Carbon Disulfide U ppbv 12 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
10. Carbon Tetrachloride U ppbv 2.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
11. Chlorobenzene U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
12. Chloroethane U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
13. Chloroform U ppbv 1.9 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
14. Chloromethane U ppbv 7.8 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
15. Cyclohexane U ppbv 24 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
16. Dibromochloromethane U ppbv 1.9 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
17. 1,2-Dichlorobenzene U ppbv 8.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
20. Dichlorodifluoromethane 750 ppbv 24 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
21. 1,1-Dichloroethane U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
22. 1,2-Dichloroethane U ppbv 2.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
23. 1,1-Dichloroethene U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
24. cis-1,2-Dichloroethene U ppbv 7.8 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
26. 1,2-Dichloropropane U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
27. cis-1,3-Dichloropropene U ppbv 8.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
28. trans-1,3-Dichloropropene U ppbv 7.7 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
29. 1,4-Dioxane U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 30. Ethyl Acetate U ppbv 12 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
31. Ethylbenzene U ppbv 24 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
32. Ethylene Dibromide U ppbv 0.82 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
33. n-Heptane U ppbv 12 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
34. Hexachlorobutadiene U ppbv 2.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
35. n-Hexane U ppbv 12 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 36. 2-Hexanone U ppbv 24 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 37. Isopropanol U ppbv 24 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 13 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-006

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-5 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 10:12

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-006 Matrix: Air


Method: EPA TO-15 Description: AKT VI-5

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 38 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS


‡ 39. 2-Methylnaphthalene U ppbv 80 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
40. 4-Methyl-2-pentanone U ppbv 24 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
41. MTBE U ppbv 8.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 42. Naphthalene U ppbv 8.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
43. Styrene U ppbv 40 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.82 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
45. Tetrachloroethene U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 46. Tetrahydrofuran U ppbv 24 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
47. Toluene U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
48. 1,2,4-Trichlorobenzene U ppbv 40 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
50. 1,1,2-Trichloroethane U ppbv 1.8 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
51. Trichloroethene U ppbv 0.79 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
52. Trichlorofluoromethane 26 ppbv 8.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
54. 1,2,4-Trimethylbenzene U ppbv 7.9 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
55. 1,3,5-Trimethylbenzene U ppbv 8.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
56. Vinyl Acetate U ppbv 12 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
57. Vinyl Chloride U ppbv 6.0 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
58. m&p-Xylene U ppbv 47 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
59. o-Xylene U ppbv 24 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 60. Xylenes U ppbv 71 29 12/05/17 VK17L05A 12/06/17 VK17L05A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 14 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-007

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-7 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 10:23

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-007 Matrix: Air


Method: EPA TO-15 Description: AKT VI-7

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 24 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG


2. Benzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
3. Benzyl Chloride U ppbv 1.2 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
4. Bromodichloromethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
5. Bromoform U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
6. Bromomethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
7. 1,3-Butadiene U ppbv 0.54 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
8. 2-Butanone U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
‡ 9. Carbon Disulfide U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
10. Carbon Tetrachloride U ppbv 1.2 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
11. Chlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
12. Chloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
13. Chloroform U ppbv 1.2 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
14. Chloromethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
15. Cyclohexane U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
16. Dibromochloromethane U ppbv 0.54 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
17. 1,2-Dichlorobenzene U ppbv 6.5 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
18. 1,3-Dichlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
19. 1,4-Dichlorobenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
20. Dichlorodifluoromethane 220 ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
21. 1,1-Dichloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
22. 1,2-Dichloroethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
23. 1,1-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
24. cis-1,2-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
25. trans-1,2-Dichloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
26. 1,2-Dichloropropane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
27. cis-1,3-Dichloropropene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
28. trans-1,3-Dichloropropene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
29. 1,4-Dioxane U ppbv 6.5 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
‡ 30. Ethyl Acetate U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
31. Ethylbenzene U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
32. Ethylene Dibromide U ppbv 0.22 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
33. n-Heptane U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
34. Hexachlorobutadiene U ppbv 0.48 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
35. n-Hexane U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
‡ 36. 2-Hexanone U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
‡ 37. Isopropanol U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 15 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-007

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-7 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 10:23

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-007 Matrix: Air


Method: EPA TO-15 Description: AKT VI-7

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
‡ 39. 2-Methylnaphthalene U ppbv 24 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
40. 4-Methyl-2-pentanone U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
41. MTBE U ppbv 6.6 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
‡ 42. Naphthalene U ppbv 5.3 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
43. Styrene U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
44. 1,1,2,2-Tetrachloroethane U ppbv 0.48 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
45. Tetrachloroethene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
‡ 46. Tetrahydrofuran U ppbv 1.2 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
47. Toluene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
48. 1,2,4-Trichlorobenzene U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
49. 1,1,1-Trichloroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
50. 1,1,2-Trichloroethane U ppbv 1.2 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
51. Trichloroethene U ppbv 0.30 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
52. Trichlorofluoromethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
54. 1,2,4-Trimethylbenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
55. 1,3,5-Trimethylbenzene U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
56. Vinyl Acetate U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
57. Vinyl Chloride U ppbv 6.0 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
58. m&p-Xylene U ppbv 13 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
59. o-Xylene U ppbv 12 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG
‡ 60. Xylenes U ppbv 24 8.0 12/04/17 VA17L04A 12/05/17 VA17L04A KRG

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 16 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-008

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-2 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 09:10

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-008 Matrix: Air


Method: EPA TO-15 Description: AKT VI-2

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone U ppbv 40 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS


2. Benzene U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
3. Benzyl Chloride U ppbv 2.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
4. Bromodichloromethane U ppbv 1.9 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
5. Bromoform U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
6. Bromomethane U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
7. 1,3-Butadiene U ppbv 2.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
8. 2-Butanone U ppbv 12 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 9. Carbon Disulfide U ppbv 12 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
10. Carbon Tetrachloride U ppbv 2.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
11. Chlorobenzene U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
12. Chloroethane U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
13. Chloroform U ppbv 1.9 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
14. Chloromethane U ppbv 8.1 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
15. Cyclohexane U ppbv 25 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
16. Dibromochloromethane U ppbv 1.9 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
17. 1,2-Dichlorobenzene U ppbv 8.2 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
18. 1,3-Dichlorobenzene U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
19. 1,4-Dichlorobenzene U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
20. Dichlorodifluoromethane 740 ppbv 24 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
21. 1,1-Dichloroethane U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
22. 1,2-Dichloroethane U ppbv 2.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
23. 1,1-Dichloroethene U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
24. cis-1,2-Dichloroethene U ppbv 8.1 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
25. trans-1,2-Dichloroethene U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
26. 1,2-Dichloropropane U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
27. cis-1,3-Dichloropropene U ppbv 8.3 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
28. trans-1,3-Dichloropropene U ppbv 8.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
29. 1,4-Dioxane U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 30. Ethyl Acetate U ppbv 12 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
31. Ethylbenzene U ppbv 25 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
32. Ethylene Dibromide U ppbv 0.84 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
33. n-Heptane U ppbv 12 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
34. Hexachlorobutadiene U ppbv 2.1 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
35. n-Hexane U ppbv 12 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 36. 2-Hexanone U ppbv 25 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 37. Isopropanol U ppbv 25 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 17 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-008

Client Identification: AKT Peerless Environ. Svcs, Sample Description: AKT VI-2 Chain of Custody: 148612
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 09:10

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Bottle-Vac) Aliquot ID: 82097-008 Matrix: Air


Method: EPA TO-15 Description: AKT VI-2

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 39 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS


‡ 39. 2-Methylnaphthalene U ppbv 83 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
40. 4-Methyl-2-pentanone U ppbv 24 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
41. MTBE U ppbv 8.3 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 42. Naphthalene U ppbv 8.3 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
43. Styrene U ppbv 41 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.84 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
45. Tetrachloroethene U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 46. Tetrahydrofuran U ppbv 25 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
47. Toluene U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
48. 1,2,4-Trichlorobenzene U ppbv 41 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
49. 1,1,1-Trichloroethane U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
50. 1,1,2-Trichloroethane U ppbv 1.9 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
51. Trichloroethene U ppbv 0.81 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
52. Trichlorofluoromethane 12 ppbv 8.3 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
54. 1,2,4-Trimethylbenzene U ppbv 8.1 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
55. 1,3,5-Trimethylbenzene U ppbv 8.2 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
56. Vinyl Acetate U ppbv 12 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
57. Vinyl Chloride U ppbv 6.0 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
58. m&p-Xylene U ppbv 49 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
59. o-Xylene U ppbv 25 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS
‡ 60. Xylenes U ppbv 73 30 12/05/17 VK17L05A 12/06/17 VK17L05A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 18 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-009

Client Identification: AKT Peerless Environ. Svcs, Sample Description: Indoor Air-101 Chain of Custody: 148613
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 08:45

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Summa) Aliquot ID: 82097-009 Matrix: Air


Method: EPA TO-15 Description: Indoor Air-101

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

‡ 1. Acetone 48 ppbv 15 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS


2. Benzene U ppbv 0.90 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
3. Benzyl Chloride U ppbv 0.080 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
4. Bromodichloromethane U ppbv 0.12 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
5. Bromoform U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
6. Bromomethane U ppbv 0.90 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
7. 1,3-Butadiene U ppbv 0.080 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
8. 2-Butanone U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
‡ 9. Carbon Disulfide U ppbv 6.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
10. Carbon Tetrachloride U ppbv 0.12 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
11. Chlorobenzene U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
12. Chloroethane U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
13. Chloroform U ppbv 0.12 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
14. Chloromethane U ppbv 6.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
15. Cyclohexane U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
16. Dibromochloromethane U ppbv 0.080 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
17. 1,2-Dichlorobenzene U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
18. 1,3-Dichlorobenzene U ppbv 0.30 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
19. 1,4-Dichlorobenzene U ppbv 0.30 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
20. Dichlorodifluoromethane U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
21. 1,1-Dichloroethane U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
22. 1,2-Dichloroethane U ppbv 0.12 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
23. 1,1-Dichloroethene U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
24. cis-1,2-Dichloroethene U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
25. trans-1,2-Dichloroethene U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
26. 1,2-Dichloropropane U ppbv 0.30 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
27. cis-1,3-Dichloropropene U ppbv 0.30 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
28. trans-1,3-Dichloropropene U ppbv 0.30 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
29. 1,4-Dioxane U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
‡ 30. Ethyl Acetate U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
31. Ethylbenzene U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
32. Ethylene Dibromide U ppbv 0.030 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
33. n-Heptane U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
34. Hexachlorobutadiene U ppbv 0.080 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
35. n-Hexane U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
‡ 36. 2-Hexanone U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
‡ 37. Isopropanol U ppbv 6.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 19 of 20
Laboratory Project Number: 82097
Date: 12/07/17
Laboratory Sample Number: 82097-009

Client Identification: AKT Peerless Environ. Svcs, Sample Description: Indoor Air-101 Chain of Custody: 148613
Inc. - Saginaw
Client Project Name: Village Of St. Charles/127165 Sample No: Collect Date: 11/28/17

Client Project No: 127165 Sample Matrix: Air Collect Time: 08:45

Sample Comments:

Definitions: Q: Qualifier (see definitions at end of report) NA: Not Applicable ‡ : Parameter not included in NELAC Scope of Analysis.

TO-15 (Summa) Aliquot ID: 82097-009 Matrix: Air


Method: EPA TO-15 Description: Indoor Air-101

Preparation Analysis
Parameter(s) Result Q Units Reporting Limit Dilution P. Date P. Batch A. Date A. Batch Init.

38. Methylene Chloride U ppbv 6.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
‡ 39. 2-Methylnaphthalene U ppbv 6.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
40. 4-Methyl-2-pentanone U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
41. MTBE U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
‡ 42. Naphthalene U ppbv 0.30 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
43. Styrene U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
44. 1,1,2,2-Tetrachloroethane U ppbv 0.030 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
45. Tetrachloroethene U ppbv 0.90 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
‡ 46. Tetrahydrofuran U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
47. Toluene U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
48. 1,2,4-Trichlorobenzene U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
49. 1,1,1-Trichloroethane U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
50. 1,1,2-Trichloroethane U ppbv 0.12 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
51. Trichloroethene 0.14 ppbv 0.030 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
52. Trichlorofluoromethane U ppbv 1.5 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
53. 1,1,2-Trichlorotrifluoroethane U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
54. 1,2,4-Trimethylbenzene U ppbv 0.90 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
55. 1,3,5-Trimethylbenzene U ppbv 0.90 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
56. Vinyl Acetate U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
57. Vinyl Chloride U ppbv 0.30 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
58. m&p-Xylene U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
59. o-Xylene U ppbv 3.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS
‡ 60. Xylenes U ppbv 6.0 1.0 12/06/17 VK17L06A 12/06/17 VK17L06A LDS

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746


Analytical Laboratory Report Order: 82097
Page: 20 of 20
Laboratory Project Number: 82097
Date: 12/07/17

Definitions/ Qualifiers:

A: Spike recovery or precision unusable due to dilution.


B: The analyte was detected in the associated method blank.
E: The analyte was detected at a concentration greater than the calibration range, therefore the result is estimated.
J: The concentration is an estimated value.
M: Modified Method
U: The analyte was not detected at or above the reporting limit.
X: Matrix Interference has resulted in a raised reporting limit or distorted result.
W: Results reported on a wet-weight basis.
*: Value reported is outside QC limits

Exception Summary:

Accreditation Number(s):

T104704518-17-6 (TX)

1914 Holloway Drive Holt, MI 48842 T: (517) 699-0345 F: (517) 699-0388


11766 E. Grand River Brighton, MI 48116 T: (810) 220-3300 F: (810) 220-3311
8660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368 F: (231) 775-8584

DCSID: G-610.16 (01/06/16) lab@fibertec.us RSN: 82097-171207143746

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