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Contents
o Introduction
o Type of Filtration
o Filter media
o Design Equation for Batch Filtration
o Specific Cases of Filtration
o Industrial Filter Equipment
o Selection Criteria of various type of filter
FILTERATION
The separation of solids from a suspension in a liquid by means
of a porous medium or screen which retains the solids and
allows the liquid to pass is termed filtration.
Filtration
In the laboratory, the suspension is
poured into a conical funnel fitted with
a filter paper.
• Clarifying Filter
• Cross Flow
Filter cake
Clarifying Filter
• Any filter, such as a sand filter or a cartridge
filter, used to purify liquids with a low solid-liquid
ratio; in some instances colour may be removed as
well.
dL
L
Design Equation for Batch Filtration
Since the cake forms a porous bed over the filter medium, the flow of
filtrate through the accumulated cake is analogous to fluid flow
through a packed bed of granular solids.
• If the particles in the cake are uniformly wet by the filtrate then
Kozeny’s equations can be used to compute the pressure
drop across the cake (-P).
The velocity of fluid through the bed is:
Where,
Design…
is independent of
Incompressible pressure drop and
Filter cake position in the cake
Compressible
Formed when cake is not made up of individual rigid
particles
, sp/vp vary from layer to layer
varies with distance from filter medium
Cake nearest the surface of the media is subjected to the
greatest compressive force and has the lowest
Pressure gradient is non-linear and local value of may
vary with time
Design…
For the computation of Lc
Polyester
Multifilament
60x zoom
Design…
Rm is to be determined experimentally.
Rm may vary with P, as solid particles can be forced into the filter medium
But, since it is important only during early stages of filtration, can usually be
assumed as constant
Therefore, the total resistance of filtration is
Ruth correlation
Both these correlations are the functions of (-P) only. Therefore, for
compressible sludge also, is constant if the filtration is being conducted
at constant pressure.
Empirical Equation for Resistance of Compressible
Cakes
0 < n < 20
Generalized correlation
Specific cases of filtration
Final filtration equation
where ,
Where, and
Also
where,
-P
V or t
Specific cases of filtration
Constant pressure and compressible sludge
If 0 ( p) s
Then,
Where, -P2
and -P3
log-log plot
Kp’
If = 0 (-Pc)s Then
since
If
Then
Continuous Filtration
Continuous removal of the deposited cake.
The cake thickness is thus not allowed to increase to large
values and therefore the filtration process can be
conducted at a constant rate employing a constant
pressure difference.
• Filling Rotary drum filter
• Cake formation (vacuum filter)
• Dewatering
• Washing
• Dewatering
• Cake removal
f = fractional submergence of
the drum in the slurry.
V = volume of filtrate collected
during one rotation of the drum
and (V/tc) stands for the rate of
filtration.
For compressible cake, 0 (p) s
Industrial Filtration Equipment
Internal Structure
Rotary Drum Filter
• Horizontal drum that turns at 0.1-2 r/min in an agitated slurry trough
• Filter medium covers face of drum, which is partially submerged
• Vacuum and air are alternately applied as the drum rotates
• As panel leaves slurry zone, a wash liquid is drawn through filter, then cake
is sucked dry with air, and finally cake is scraped off
• From 30% up to 60-70% of filter area can be submerged
• Cakes usually 3-40 mm thick
• Drum sizes range from 0.3 m in diameter to 3 m in diameter
Rotary Drum Filter
Parts of a Rotary Drum filter
• The Drum:
The drum is supported by a large diameter trunion on the valve end
and a bearing on the drive end. The drum face is divided into
circumferential sectors each forming a separate vacuum cell. The
internal piping that is connected to each sector passes through the
trunion and ends up with a wear plate having ports that correspond to
the number of sectors.
Parts of Rotary Drum Filter
• The Valve: A valve with a bridge setting controls the sequence of the cycle so
that each sector is subjected to vacuum, blow and a dead zone. When a sector
enters submergence vacuum commences and continues through washing, if
required, to a point that it is cut-off and blow takes place to assist in discharging
the cake.
• The valve has on certain filters adjustable blocks and on others a fixed bridge ring.
Adjustable bridge blocks enable the optimization of form to dry ratio within the
filtration cycle as well as the "effective submergence" of the drum when the slurry
level in the tank is at the maximum.
a. cake formation
b. cake washing & drying
c. cake blow discharge b
a c
Parts of Rotary Drum Filter
The Internal piping:
Cloth Locking
Roll
Cloth
Tensioning Roll
Fixed Trays
3-Way Valves
Cloth Wash
Manifold
Pneumatic
Cylinder
Fixed roll with "on-off" motor actuator:
• In this system the discharge roll is mounted on the frame in a fixed
position and a timer controlled pulley moves the cloth at "vacuum off" to
allow cake discharge and "vacuum on" during filtration. A special tilting
feed box pours the slurry onto the filter deck when the cloth moves at
"vacuum off".
Selection Criteria for Tray Filter
• They may be built from synthetic materials of construction which makes them
suitable to withstand highly corrosive applications without the use of exotic
and expensive alloys.
• The sealing against loss of vacuum is simple as opposed to the rubber belt
filters which use sacrificial moving belts to seal between the underside of the
main belt and the top flanges that run along the vacuum box.
• They are built in a modular construction which enables expansion when
circumstances so require.
• The separation of mother and wash filtrates is sharp and accurate since, as
opposed to partitions in a vacuum box of a rubber belt filter, the filtrate is
contained in a tray.
• They lend themselves better than rubber belt filters when two vacuum zones
are required such as high vacuum for the feed and wash zones and low
vacuum with high air rates for the drying zone.
• The power consumption is lower since the rubber belt filters require special
arrangements to support the heavy belt and reduce friction.
• Features are found more often on tray filters such as gas tight
enclosures, compression rolls and blankets, thermal drying, vibrating trays to
seal cracks in the cake and ultrasonic or chemical cloth cleaning.
• They are however less in use for very thick and heavy cakes since, contrary to
rubber belt filters, the friction during indexing due to the cake weight between
the supporting grids that cover the trays and the backside of the cloth may
cause extensive wear.
The Disc Filter
• A disk filter is a type of water filter used primarily in
irrigation, similar to a screen filter , except that the filter cartridge is
made of a number of disks stacked on top of each other like a pile
of poker chips. The water passes through the small grooves in
between and the impurities are trapped behind. Some types of disk
filters can be backflushed in such a way that the disks are able to
separate and spin during the cleaning cycle.
1. The Vessel:
There are two types of vessel configuration:
• Vessels with conical bottom for cake filtration and polishing.
• Vessels with dished bottom for slurry thickening.
Candle filter
The Cake Discharge Mechanism:
There are two methods to discharge the cake at the end of the
cycle:
• Snap blow
. • Vibrating mechanism
For cakes that discharge readily a snap blow from the backside of
the medium is sufficient to release the cake but cakes that are
difficult to discharge require a mechanism that assists release by
vibrating the entire pack of candles. In this instance it is good
practice to incorporate special headers with high impact sprays
in the upper part of the vessel to clean the candles and dislodge
entrained particles.
Candle filter
Candle Filters are best selected in the following instances:
• When minimum floor space for large filtration areas is required.
• When the liquids are volatile and may not be subjected to vacuum.
• When there is a risk of environmental hazard from toxic, flammable
or volatile cakes specially secured discharge mechanisms may be
incorporated.
• When high filtrate clarity is required for polishing applications.
• When handling saturated brines that require elevated temperatures
the tank may be steam jacketed.
• When the cake may be discharged either dry or as a thickened
slurry.
Since the centrifugal forces are many-fold larger in magnitude than the
gravitational forces, the effectively pressure difference driving force for
filtration may be assumed to be due to centrifugal action only. Thus
Centrifugal filtration
We can therefore use an equation for constant pressure provided the
inherent assumptions such as the flow of filtrate through the cake is laminar
and the voids of the cake are completely filled with the filtrate ( no
channeling ) are kept alive. Thus,
Time(min) 10 20 30 45 60
for i=1:n
t(i)=t(i)*60;
end
for i=1:4
Continue…
dt(i)=t(i+1)-t(i); tw=vw/rw;
dfv(i)=fv(i+1)-fv(i); disp('t wash=');disp(tw);disp('sec');disp('
dtf(i)=dt(i)/dfv(i);
av(i)=fv(i)+.5*dfv(i);
');disp((tw/60));disp('min');
end
delta t=
600 600 900 900
delta V=
2.1000 1.5600 1.9800 1.7000
delta t/delta V=
285.7143 384.6154 454.5455 529.4118
Output:
V avg= 5.0400 6.8700 8.6400 10.4800
t wash= 1.8418e+003sec
30.6967 min
ratio= 0.2443
2.2529 hr