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 PUBLICATIONS

A. Paper accepted in Journal

Micellar Effect on the oxidation of Norfloxacin by Chloramine-T in acidic
medium
Ref.: 20 September 2011/JDST 2012/164, DOI:10.1080/01932691.2011.629534.

B. Papers communicated
1. Micelle catalyzed kinetic assessment of the oxidative degradation of Norfloxacin
by chloramine-T.
2. Micelle catalyzed oxidative transformation of ciprofloxacin by chloramine-T: A
kinetic and mechanistic study
3. Effect of anionic micelle media on the oxidative transformation of
Fluoroquinolone drug Ciprofloxacin in acidic environment

C. Papers Presented
1. 14th National Conference on “Surfactants, Emulsions and Biocolloids
(NATCOSEB-XIV). Organised by University of Kashmir & Indian Society for
Surface Science and Technology, July 28-30, 2009. OP-18/54.
Micellar Effect on the oxidation of Norfloxacin by Chloramine-T in acidic
medium
2. 47th Annual Convention of Chemists-2010 & International Conference on Recent
Advances in Chemical Sciences. Organised by Indian Chemical Society, hosted
by School of Studies, RSU, Raipur, December 23-27, 2010. PHY(OP)-37.
Micelle catalyzed kinetic assessment of the oxidative degradation of
Norfloxacin by Chloramine-T
3. National Seminar on Recent Trends in Chemical Sciences and future prospects.
Sponsored by UGC-CRO, Bhopal & CCOST, at Govt V. Y. T. PG. Autonomous
college, Durg, October 11-12, 2011. OP-20/26.
Micelle catalysed oxidative transformation of ciprofloxacin by chloramine-T:
A kinetic and mechanistic study
4. AICON, All India Conference on Integrated Efforts for Sustainable Development
& Ecological Resilience. Organised by Chhatrapati Shivaji Institute of
technology, Durg, Jan 20-21, 2012. CheA 1220.
Cationic micelle catalyzed oxidative transformation of Ciprofloxacin by
Chloramine-T: A kinetic and mechanistic study

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Journal of Dispersion Science and Technology

Micellar Effect on Kinetic Assessment of the Oxidative Degradation

of Norfloxacin by Chloramine-T

DOI: 10.1080/01932691.2011.629534

Alpa Shrivastavaa, Ajaya Kumar Singhb*, Neerja Sachdevc, Dilip Raj Shrivastavad & Yokraj Katree
Available online: 27 Dec 2011

Abstract

The kinetics of oxidation of the Norfloxacin (NOR) by sodium salt of p-toluene

sulphonamide (Chloramine-T) has been studied in presence of an anionic surfactant, i.e.,
sodium dodecylsulphate (SDS) in perchloric acid medium at 308 K. The reactions show
first order, fractional order and inverse fractional order dependence of rate with respect to
NOR, chloramines-T and perchloric acid, respectively. Dilute micelle-forming anionic
surfactant slightly speed the reaction but the reaction rate decreases sharply with
increasing surfactant concentration. The kinetic data have been rationalized in terms of
various micelle kinetic models and binding parameters have been evaluated. The addition
of reduced product of the oxidant (phthalimide) has decreased the rate of reaction. The
rate of reaction also decreased with increase in salt concentrations. Effect of ionic
strength and solvent polarity of the medium on the rate of reaction were studied. The
oxidation products were identified by GC-MS analysis. Investigations of the reaction at
different temperatures allowed the determination of the activation parameters with
respect to the slow step of proposed mechanism.

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Keywords

• Micellar kinetics,
• norfloxacin,
• chloramine-T,
• oxidation

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