Beruflich Dokumente
Kultur Dokumente
rmfield.co
g Teaching & Research Equipment
armfield
TH4
ISSUE 11
April 2016
PC-
0055698
1
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Armfield Ltd Instruction Manual TH4
1 Introduction
This manual contains instructions for the correct use and maintenance of the TH4 manufactured by Armfieid
Limited.
The information contained in this manual is intended for the user who is required to read it carefully and to
ensure that he has fully understood it before operating the machine.
The user manual must be available for ready consultation at all times.
If the manual is lost or damaged contact the manufacturer for a replacement copy.
WARNING - The manufacturer is not liable for consequences resulting from an improper use of the
machine due to the user’s failure to read this manual or incomplete reading of it.
The manual is an integral part of each piece of equipment and consequently must be kept throughout the
entire service life of the machine and accompany it at all times, even if transferred to another user.
This manual contains instructions required for the safety, receiving, installation, storage, correct operation and
maintenance of the TH4.
o
^J^WARNING - Armfield Limited reserves the right to modify the specifications referred to in this manual or
the characteristics of each machine. Some of the illustrations in this manual may include parts that are slightly
different to those mounted on your machine.
O
WARNING - All practical work areas and laboratories should be covered by local regulations which
must be followed at all times.
2 EC Conformity
Each machine is accompanied by an EC Declaration of Conformity signed by the representative of Armfield
Limited.
The equipment has been constructed in compliance with the essential health and safety requirements laid
down in the following applicable directives:
The following harmonised standards were also consulted for the design
o
WARNING - This declaration is only valid if the Equipment is installed, used and maintained in
compliance with the above mentioned directives and instructions and with the nstructions and equipment
described in this manual.
Table of Contents
1 Introduction ......................................................................................................................................................2
2 EC Conformity .................................................................................................................................................2
3 Disclaimer ......................................................................................................................................................... 6
4 Copyright and trademarks........................................................................................................................... 6
5 Symbols ............................................................................................................................................................. 7
6 Safety ............. ..................................................................................................................... .......... '■ ............. 8
6.1 Failure to comply with safety standards ........................................................................................ 8
6.2 Start up, operation and maintenance ............................................................................................ 8
6.3 Intended conditions of use ............................................................................................................... 9
6.4 Safety guidelines relating to maintenance, inspection and assembly work ........................ 9
6.5 Arbitrary production and transformation of spare parts .......................................................... 9
6.6 Noise ....................... . .............................................................................................................................10
6.7 Chemical Safety ...................................................................................................................................10
6.8 Control of Hazardous Substances ...................................................................... ..........................10
6.9 Water Borne Hazards .........................................................................................................................12
6.10 Hot/Cold Surfaces ...............................................................................................................................12
6.11 Hot/Cold Liquids .................................................................................................................................13
6.12 Leakage of hazardous fluids ............................................................................................................13
6.13 Protective clothing ..............................................................................................................................13
6.14 Machine maintenance .......................................................................................................................14
7 General Overview ......................................................................................................................................... 16
8 Equipment Diagrams ................................................................................................................................... 17
9 Description ..................................................................................................................................................... 21
9.1 Overview ................................................................................................................................................21
9.2 Rear of Unit .......................................................................................................................................... 22
9.3 Electrical Console ......... .................................................................................................................... 22
10 Installation ..................................................................................................................................................... 24
10.1 Advisory ................................................................................................................................................. 24
10.2 Electrical Supply .................................................................................................................................. 24
10.3 Cold water supply ............................................................................................................................... 25
10.4 Laboratory drain ................................................................................................................................. 25
10.5 Installing the optional TH Software ........................................................................................ ..... 25
10.6 Installing the Equipment ................................................................................................................... 25
10.7 Commissioning .................................................................................................................................... 25
10.8 Electrical Wiring Diagram ................................................................................................................. 27
11 Operation ....................................................................................................................................................... 28
11.1 Operating the optional TH Software........................................................ .................................... 28
11.2 Operating the Equipment ................................................................................................................ 28
11.2.1 Setting the cold water pressure regulator ......................................................................... 28
11.2.2 Priming the flow loop (When not using the clear acrylic reservoir) ........................... 28
11.2.3 Priming the flow loop (When using the clear acrylic reservoir) .................................. 28
11.2.4 Setting and measuring the water flowrate (Through flow) ........................................... 28
11.2.5 Setting and Measuring the water flowrate (Recycle flow)............................................. 29
11.2.6 Applying a step change to the heater ........................... .................................................... 29
11.2.7 Measuring the temperatures in the system ...................................................................... 29
12 Equipment Specifications ......................................................................................................... . .............. 30
12.1 USB Channel Numbers ..................................................................................................................... 30
12.2 Environmental Conditions ..............................................................................................................- 31
3 Disclaimer
This document and all the information contained within it are proprietary to Armfield Limited. This document
must not be used for any purpose other than that for which it is supplied and its contents must not be
reproduced, modified, adapted, published, translated or disclosed to any third party, in whole or in part,
without the prior written permission of Armfield Limited.
Should you have any queries or comments, please contact the Armfield Customer Support helpdesk (Monday
to Thursday: 0830 - 1730 and Friday: 0830 - 1300 UK time). Contact details are as follows:
t, • , International
United Kingdom
(0) 1425 478781 (calls charged at local rate) +44 (0) 1425 478781 (international
rates apply)
Email: support@armfield.co.uk
Any technical documentation made available by Armfield Limited is the copyright work of Armfield Limited
and wholly owned by Armfield Limited.
Brands and product names mentioned in this manual may be trademarks or registered trademarks of their
respective companies and are hereby acknowledged.
5 Symbols
A
■ "Danger warning /\
£»Caution: Explosion Risk
Ac
aution: corrosive material
Do not remove safety guards from Do not repair or oil machine whilst in
rotating parts motion
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Wear safety shoes Wear breathing protection
6 Safety
o Failure to comply with the safety standards described in this manual and those relating to common sense
can cause danger to people and the environment and damage the Equipment.
Failure to observe and comply with these safety standards will invalidate the warranty.
Keep these instructions and all related documents together, ensure that they are legible and easily accessible
to all employees.
Do not remove any safety equipment before operating the Equipment or during its operation. Make sure
that there is no evident danger before powering up the Equipment. The system must be inspected regularly
to check for damage and to ensure that all safety devices are in good working order.
A
• ^The Equipment contains moving parts. Do not insert limbs or materials other than the processing material
while the Equipment is functioning. In the event of malfunction, danger or lack of appropriate safety systems,
shut down the Equipment immediately and inform the qualified personnel.
A<SA While the Equipment is being used the safety devices provided must be present and
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correctly installed. Do not carry out any operation on the safety devices while the Equipment is operating.
© The Equipment must always observe the operating limitations for which it was constructed and those
stated in the order confirmation: observe the temperature, pressure, capacity, viscosity and speed limits. Unless
otherwise stated in the order, the Equipment ,'-jst not be used in environments subject to the formation of
potentially explosive atmospheres.
A- k
i he user must ensure that all maintenance, inspection and assembly operations re:ated to the
Equipment are carried out by qualified technicians.
echnicians must carefully read this instruction manual before acting on the Equipment. Only authorised and
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-^Changes or modifications to the machine, within the limits that do not go beyond extraordinary
maintenance, are only permitted if agreed on beforehand with the manufacturer.
Only original spare parts or parts specifically declared as compatible by Armfield Limited must be used for
regular maintenance operations.
These parts have been designed specifically for the system. There is no guarantee that nonoriginal parts can
withstand the loads, and function correctly and safely.
6.6 Noise
The A-weighted sound power level emitted by the machine does not exceed 85dB(A).
This value is guaranteed if the Equipment is installed correctly, that is, in stable conditions with appropriate
fastenings and measured at a distance of 1 metre from the Equipment.
A
The unit is designed to use clean water during normal operation, but cleaning should be carried out
regularly as described in the maintenance section of this manual which may involve the use of
detergents/chemicals. In addition, under certain conditions causing algal growth, it may be necessary to use
disinfectants or biocides to avoid the possibility of waterborne infections as described above.
O
^CJFThe Control of Substances Hazardous to Health Regulations
The COSHH regulations impose a duty on employers to protect employees and others from substances used
at work which may be hazardous to health.
COSHH covers substances that are hazardous to health. Substances can take many forms and include:
• chemicals
• fumes
• dusts
• vapours
• mists
• nanotechnology
• germs that cause diseases such as leptospirosis or legionnaires disease and germs used in
laboratories.
The regulations require you to make an assessment of all operations which are liable to expose any person
to these hazards. You are also required to introduce suitable procedures for handling these substances and
keep appropriate records.
S -se the equipment supplied by Armfield Limited may involve the use of substances which :=- ce hazardous
(for example, cleaning fluids used for maintenance or chemicals used for part cu ar demonstrations) it is
essential that the responsible person in authority implements -e COSHH regulations or local equivalent.
Products you use may be 'dangerous for supply’. If so, they will have a label that has one or more hazard
symbols. These products include common substances in everyday use such as paint, bleach, solvent or fillers.
When a product is ‘dangerous for supply’, by law, the supplier must provide you with a safety data sheet.
Note: medicines, pesticides and cosmetic products have different legislation and don’t have a safety data
sheet. Ask the supplier how the product can be used safely.
Any such chemicals used must be stored, handled, prepared and used in accordance with the
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manufacturer’s instructions and with all applicable local regulations. Protective clothing (e.g. gloves, eye
protection) should be worn when appropriate, and users should be supplied with any relevant safety
information (e.g. the correct procedure in the event of contact with skin or eyes, the correct procedure in the
event of a spill, etc.).
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The equipment described in this instruction manual involves the use of water/fluid, which under certain
conditions can create a health hazard due to infection by harmful microorganisms.
For example, the microscopic bacterium called Legionella pneumophila will feed on any scale, rust, algae or
sludge in water and will breed rapidly if the temperature of water is between 20 and 45°C. Any water
containing this bacterium which is sprayed or splashed creating air-borne droplets can produce a form of
pneumonia called Legionnaires Disease which is potentially fatal.
Legionella is not the only harmful micro-organism which can infect water, but it serves as a useful example of
the need for cleanliness.
• Any water/fluid contained within the product must not be allowed to stagnate, i.e. the water must be
changed regularly.
• Any rust, sludge, scale or algae on which micro-organisms can feed must be removed regularly, i.e.
the equipment must be cleaned regularly.
• Where practicable the water/fluid should be maintained at a temperature below 20°C or the water
should be disinfected. In the TH4 water fresh water continuously flows through the system but water
may stagnate if left in the system after use. The reservoir will be especially prone to algal growth so
this should be drained after use and filled with fresh water for each run. Note that other hazards may
exist in the handling of biocides if these are used to disinfect the water.
• After use the water system should be filled and run with water containing a mild disinfectant such as
‘Milton’ to kill any micro-organisms or algal growth then flushed with clean water and left empty.
• A scheme should be prepared for preventing or controlling the risk incorporating all of the actions
listed above.
Further details on preventing infection are contained in the publication “The Control of Legionellosis including
Legionnaires Disease” - Health and Safety Series booklet HS (G) 70.
This unit contains components that that operate with a maximum temperature of 100°C and
minimum temperature of 5°C.
Do not touch any surfaces close to ‘Hot Surfaces’ warning labels, any of the interconnecting tubing or
components whilst the equipment is in use or returning to a safe temperature.
AA This unit is designed to operate with a maximum liquid temperature of 70°C and
e s also a potential risk of scalding from hot liquids or vapours (e.g. steam).
. Check that the temperature of the Equipment and liquid is at a safe level
Do not touch any surfaces close to ‘Hot Surfaces’ warning labels, any of the interconnecting tuning or
components whilst the equipment is in use or returning to a safe temperature.
A A ^
f * H - J V / ^ 8r | f the Equipment is used to pump/operate with hazardous liquids (toxic, corrosive,
flammable, etc.), the volumes of fluid that leak through the seals must be collected and disposed of without
endangering human health or the environment and in accordance to local legislation.
Safety gloves
Wear suitable gloves to protect your hands from various types of possible hazards: mechanical, electrical,
chemical and high/low temperatures.
Clothing
Footware
Eye Protection
Wear suitable eye protection to protect your eyes from various types of possible hazards: mechanical debris,
chemicals and hot water/steam.
Ear Protection
Wear suitable ear protection to protect your ears from excessive noise.
ta'i
Breathing Protection
Wear suitable breathing protection to protect your respiratory system from fumes.
Do not disassemble the Equipment before emptying the contents/fluids (if applicable).
Even if the tubes are all empty, some liquid could remain in the unit. The fluid(s) can be hazardous to human
health and the environment, and can be very hot/cold.
A
■ 1 ■ "*All maintenance work must be carried out with the machine isolated from the power supply.
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'LFTO give increased operator protection, the unit incorporates a Residual Current Device (RCD), alternatively
called an Earth Leakage Circuit Breaker, as an integral part of this equipment. If through misuse or accident
the equipment becomes electrically compromised, the RCD will switch off the electrical supply and reduce the
severity of any electric shock
received by an operator to a level which, under normal circumstances, will not cause injury to that person.
AA At least once each month, check that the RCD is operating correctly by pressing the TEST button.
The circuit breaker MUST trip when the button is pressed. Failure to trip —eans that the operator is not
protected and the equipment must be checked and repaired by a competent electrician before it is used.
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7 General Overview
The TH range is designed to introduce the fundamental principles of thermodynamics to the student. The
range of equipment starts at basic concepts such as temperature and pressure measurement and leads on to
introducing the relationships between these fundamentals, the first and second law of thermodynamics, the
principles of reversibility, entropy, enthalpy etc.
The equipment allows the student to gain a true understanding of these principles. The small scale of the
equipment allows the relevant teaching exercises to be carried out in a relatively short period of time.
This instruction manual describes the operation of the TH4 'Recycle Loops' apparatus that has been designed
by Armfield to demonstrate clearly, both visually and experimentally, what recycle is and to allow mass and
energy balances to be performed under steady state and unsteady state conditions. Recycle is a simple
phenomenon which occurs in many aspects of everyday life but a concept that can lead to confusion in
engineering applications when combined with other principles such as mass and energy balances and the use
of the steady flow energy equation.
The application modelled is typical of a heating arrangement in the chemical, food or pharmaceutical
industries whereby the temperature of product is raised or lowered offline by recirculating some of the product
through a heat exchanger.
8 Equipment Diagrams
PC-0055698 17 issue 11
April 2016
Arm field Ltd instruction
Manual TH4
PC-0055698 19
Arm field
Ltd instruc
tion Manual TH4
Recycle
loop
pump
j 4X
F1
PC-
0055698
20 issue 11 April 2016
Arm field Ltd
Fx = Flow sensor Tx = instruction Manual TH4
Temperature sensor
9 Description
Where necessary, refer to the drawings in Equipment Diagrams section 8.
9.1 Overview
The TH4 Recycle Loops apparatus s a bench top unit designed to introduce students to the characteristics of
a recycle loop, ano the typical responses under steady state and unsteady conditions. The apparatus is
ffrrtttttnuuuinuntrrm
mounted on a moulded ABS support plinth (1). The components associated with the flow loop are mounted
on a plastic plate (2) that is located on top of the support plinth by four knurled fixings.
The apparatus consists of a through pipe (5) conveying water from the cold water mains supply (4) to a
suitable drain (6), with a loop of pipework in parallel with the inlet and outlet connections. This recycle loop
incorporates a circulating pump (10) which transfers water from the through pipe just before the drain
connection (7), and returns the water back to the tnrough pipe downstream of the supply connection (8). A
heater in the recycle loop (11) raises the temperature of the water in the loop, which then mixes with fresh cold
water entering the system.
_
~e : xulating pump (10) is a gear pump with an external bypass arrangement incorporating a casing valve (9),
which allows the flow rate through the loop to be varied using a simple ~dw control valve (13). The pump is
turned on/off by the switch (25) on the console. The s~2 scale of the loop ensures that time constants are
short enough to allow responses to be fully evaluated in a normal laboratory session.
~ne water heater (11) consists of a 2 kW cylindrical cartridge heater mounted concentrically within an insulated
tube, so that water flows along the annulus and over the surface of the neater. A switch (24) on the console
allows the heater to be switched on or off, to generate step changes when investigating the transient
responses of the recycle loop. To prevent overheating, the heater cannot operate unless the circulating pump
is switched on and fiowrates F1 and F2 are at least 1 l/min. The ‘Heater On’ LED (23) on the console is not
Ruminated if power to the heater has been cut by the protection circuit because the flow rates are too low.
To allow the volume of the loop to be changed, and hence to demonstrate the effect of residence time, a pair
of self-sealing fittings (14) allow a short length of pipe or a reservoir (18) to be connected in series with the
recycle loop. The arrangement permits different lengths of flexible tubing to be connected in series with the
loop, if it is required to create further changes in residence time. The clear acrylic reservoir incorporates an air
bleed screw (41) on the top to aid priming and draining.
Water temperatures at the inlet (T1), at the outlet (T3), and within the recycle loop after the heater (T2) are
measured using type K thermocouples (15), installed in tappings in the pipework. The flow rates are measured
at the inlet (F1), at the outlet (F3) and in the recycle loop (F2) using miniature turbine-type flow sensors (16).
Flow in the recycle loop can be varied from 0 to 3 l/min. The 'through flow' of water can be varied from 0 to
3 l/min. However, power to the heater will be cut if the flow in either stream is less than 1 l/min.
Cold fluid for the equipment is provided by an external cold water supply. A pressure regulator (17) after the
cold water supply inlet (4) minimises fluctuations in the supply pressure to maintain the flow at a steady rate.
A strainer built into the pressure regulator
traps particles in the water which could damage the regulator or flow sensors. A manual control valve ( 12)
allows the through flow of cold water to be varied as required.
Drain valves located at the rear left-hand side and front right-hand side of the pipework on the plinth top
allow the front and rear sections of the flow loop to be drained after use. A drain valve, located in a recess at
the left-hand end of the ABS support, allows the channel in the top of the moulded support plinth to be
drained, when necessary.
A mains switch (32), located on the front of the plinth below the control console, allows the TH4 to be turned
on and off as required and isolates all of the individual electrical circuits inside the plinth when switched off.
The Residual Current Device (33) is a device for the protection of personnel in the event of an electrical fault
or short to earth. All electrical circuits inside the plinth are protected by this device. The operation, purpose
and testing of the Residual Current Device are explained in more detail on page 4 of this manual. Normal
operation of the equipment is achieved with the switch in the UP position.
The miniature circuit breakers (34, 35 & 36) are re-settable devices which protect individual electrical circuits
inside the plinth and console. These three circuit breakers protect the water heater (34), the low voltage DC
supplies (35) and the mains output socket (36). If any of these breakers are activated, this indicates a fault in
the particular circuit and if the breaker will not reset, further investigation will be required by a competent
electrician. Normal operation of the equipment is achieved with these switches in the UP position.
The service unit is provided with a 4-metre length of mains cable which is fitted with a plug to suit the mains
power input socket (39). The cable allows connection of the unit to an appropriate electrical supply.
The mains power output socket (40) is an extra mains power source used for driving external ancillary
equipment up to 1 Amp maximum.
The low voltage DC output socket (37) is used to provide 18 V dc for the motor on the circulating pump ( 10)
in the recycle loop.
The heater socket (38) is used to provide mains electrical power to the electrical heater (11) incorporated in
the recycle loop.
The three turbine type flow sensors (F1, F2 & F3) installed on the equipment are numbered to allow
connections to the appropriate sockets (29, 30 & 31) on the front of the console. The required flow reading is
selected via a switch (22) and displayed on the adjacent LCD panel meter (21). Readings are displayed directly
on the meter in units of litres per minute (flow measurement ranges are 1.0 to 3.00 l/min for F1, F2 & F3).
A 50 way IDC socket on the right hand side of the console (the Data I/O Port) allows all of the temperature
and flow measurements to be connected simultaneously to a PC via an optional Armfield interface device
which is supplied with the Data Logging Accessory. (The Data Logging Accessory includes Windows™ based
data logging software with appropriate teaching exercises to suit the TH4).
10 Installation
10.1 Advisory
Before operating the equipment, it must be unpacked, assembled and installed as described in the steps that
follow. Safe use of the equipment depends on following the correct installation procedure.
GREEN/YELLOW - EARTH
BLUE - NEUTRAL
GREEN/YELLOW - EARTH
BLUE - NEUTRAL
GREEN/YELLOW - EARTH
BLUE - NEUTRAL
A drain valve in the base of the plinth on the left-hand side also requires connection to a sink or floor drain
and is normally left open. This drain allows any water spilled on the plinth top to ce rrained from the collecting
channel in the plinth top.
Carefully remove any transit packaging, taking care not to discard any of the loose items.
The equipment is supplied fully assembled and ready for operation with the exception of the clear acrylic
reservoir that is packed separately to avoid damage in transit. Place the reservoir on the support bracket that
is located behind the electrical console on the plinth top.
10.7 Commissioning
Refer to Figures 1, 2, & 3 in Equipment Diagrams section 8.
Note: When commissioning the TH4 apparatus, it is strongly recommended that flow readings are taken
using the built-in console display and NOT the optional data logging
software. The maximum flow rate measurable by the software is restricted due to signal voltage limitations.
Ensure that the flexible pipe is connected between the quick release fittings (14) in the recycle loop. Close the
cold water flow control valve (12).
Connect the cold water inlet (4) to the cold water supply using flexible tubing (not supplied). Secure the tubing
to the inlet using a pipe clip. Connect the hot water outlet ( 6) to a suitable drain using flexible tubing (not
supplied). Turn on the cold water supply.
Set the selector switch (22) on the console to position F1. Open the cold water flow control valve (12) fully. Pull
the grey knob on the pressure regulator (17) upwards - towards the right - then adjust the regulator until the
display (21) indicates 3.2 l/min (rotate the knob anticlockwise to decrease the flow, clockwise to increase the
flow).
Push the grey knob on the pressure regulator down to lock the setting.
With water flowing through the apparatus to drain, half-open the recycle flow control valve (13) then start the
circulating pump using the switch (25) on the console.
Slowly open then close the recycle flow control valve several times to force water through the pump bypass
(9) and remove all air from the pipe loop. Allow water to flow through the flow loop until all air has been
expelled.
Set the selector switch (22) position F1. Adjust the cold water flow control valve until the display ( 21) indicates
2.00 litre/min (do not vary the flow by changing the setting of the pressure regulator).
Set the selector switch (22) to position F2. Adjust the recycle flow control valve (13) until the display ( 21)
indicates 2.00 l/min.
Set the selector switch (22) to position T1 and observe that the display (21) indicates a sensible temperature
for the water in °C. Check that T2 and T3 are the same (no heating).
Note: If the heater is switched on with no water in the system or the flow of water in either loop is less than
1 l/min then a protection circuit will operate and turn off the power to the heater to prevent damage to the
equipment. The ‘Heater On’ LED (23) on the console will not be illuminated if F1 or F2 is set below 1 l/min. The
protection circuit will automatically restore power to the heater when normal operating conditions are
restored - by turning on or increasing the flow of cold water through the equipment.
Observe that the temperature of the water in the loop gradually rises and stabilises at an elevated value.
Check that T2 > T3 >T1.
Switch off the heater and observe that the temperatures gradually return to ambient values. Check operation
equipment and connect it to the quick release fittings. Ensure that the reservoir is located correctly over the
two fittings then press downwards until the fittings latch.
Remove the air bleed screw (located on top of the clear acrylic reservoir). Open the cold water flow control
valve (12) fully to allow water to flow through the apparatus to drain. Halfopen the recycle flow control valve
(13) then start the circulating pump. While the reservoir is filling with water adjust the position of the recycle
flow control valve to ensure that the clear stand-pipe inside the reservoir remains filled with water (if the level
falls near to the bottom close the recycle valve until the stand-pipe remains filled). When the level inside the
r
eservoir is above the stand-pipe, refit and tighten the air bleed screw.
Slowly open then close the recycle flow control valve several times to force water through the pump bypass
(9) and remove all air from the pipe loop. Allow water to flow through the flow loop until all air has been
expelled.
Close the cold water flow control valve and switch off the circulating pump. Remove the air bleed screw on
top of the reservoir, open the drain valve at the rear of the apparatus (left hand side of heater assembly) then
allow the reservoir to drain. When empty the reservoir can be removed by pressing the catch on both quick
release connectors at the same time. ~ne reservoir should be replaced on the bracket at the rear of the
console. The air bleed screw should be replaced on the top of the reservoir. The flexible pipe should be
connected zer.seen the two quick release connectors.
_
-e :asic operation of the 'Recycle Loops' apparatus has been confirmed. Refer to the Ope'=:ion section for
further information.
Connect the cold water inlet (4) to the cold water supply using flexible tubing (not supplied). Secure the tubing
to the inlet using a pipe clip. Connect the hot water outlet ( 6) to a suitable drain using flexible tubing (not
supplied). Turn on the cold water supply.
Set the selector switch (22) on the console to position F1. Open the cold water flow control valve (12) fully. Pull
the grey knob on the pressure regulator (17) upwards - towards the right - then adjust the regulator until the
display (21) indicates 3.2 l/min (3.0 l/min if using the optional software). Rotate the knob anticlockwise to
decrease the flow, clockwise to increase the flow.
Push the grey knob on the pressure regulator down to lock the setting.
11.2.2 Priming the flow loop (When not using the clear acrylic reservoir)
Ensure that the loop of pipe is fitted between the two self-sealing fittings (14). With water flowing through the
apparatus to drain, half-open the recycle flow control valve (13) then start the circulating pump using the
switch (25) on the console. Slowly open then close the recycle flow control valve (13) several times to force
water through the pump bypass (9). Allow water to flow through the flow loop until all air has been expelled.
11.2.3 Priming the flow loop (When using the clear acrylic reservoir)
Ensure that the reservoir is securely fitted by pressing it down onto the self-sealing fittings until they both
latch. Ensure that with water is flowing through the apparatus to drain. Remove the air bleed screw (located
on the top of the clear acrylic reservoir). Open the recycle flow control valve (13) half-way then operate the
pump and allow the vessel to fill with water. Adjust the recycle flow control flow control valve if necessary to
ensure that the stand-pipe inside the reservoir does not empty completely. When the reservoir has filled to a
level above the stand-pipe replace and tighten the air bleed screw. Slowly open then close the recycle flow
control valve several times to force water through the pump bypass. Allow water to flow through the flow
loop until all air has been expelled.
regulator. The minimum 'through flow1 (F1) is limited to 1.00 l/min to prevent excessive temperatures in the
equipment. If the ‘Heater On’ LED is not illuminated when the heater is switched on then the 'through-flow'
or the 'recycle flow' must be increased as appropriate to prevent over-heating.
Note: When fully primed, the inflow (F1) and outflow (F2) must always be the same.
Note: £ the heater is switched on with no water in the system, or the flow of water is not a:ei_=:e then a
protection circuit will operate and turn off the power to the heater to prevent ; = ~age to the equipment.
The ‘Heater On' LED (23) on the console will not illuminate if or F2 is less than 1.00 l/min. The protection
h circuit will automatically restore :: the heater when normal operating conditions are restored - by turning on
or
- —ess Tg the flow of cold water through the equipment.
11.2.7 Measuring the temperatures in the system
Set the selector switch (22) to position T1, T2 or T3 as required. The display (21) indicates the appropriate
temperature in the range 4 - 1 0 0 °C. Maximum operating temperature is typically 70 °C at T2.
IJJ JJJJ
12 Equipment Specifications
6 Ch 2 Return
8 Ch 3 Return
10 Ch 4 Return
12 Ch 5 Return
14 Ch 6 Return
16 Ch 7 return
a. Indoor use;
b. Altitude up to 2000 m;
c. Temperature 5 °C to 40 °C;
d. Maximum relative humidity 80 % for temperatures up to 31 °C, decreasing linearly to 50 % relative
humidity at 40 °C;
Note: The normal level of transient over-voltages is impulse withstand (over-voltage) category II of
IEC 60364-4-443;
g. Pollution degree 2.
13 Routine Maintenance
13.1 Responsibility
To preserve the life and efficient operation of the equipment it is important that the equipment is properly
maintained. Regular maintenance of the equipment is the responsibility of the end user and must be performed
by qualified personnel who understand the operation of the equipment.
13.2 General
In addition to regular maintenance the following notes should be observed:
1. The equipment should be disconnected from the electrical supply when not in use.
2. The pipework and reservoir associated with the recycle loop and the channel in the support plinth base
should be drained after use. Drain valves located at the rear left- hand side and front right-hand side of
the pipework on the plinth top allow the front and rear sections of the flow loop to be drained after use.
A drain valve, located in a recess at the left-hand end of the ABS support, allows the channel in the top
of the moulded support plinth to be drained, when necessary.
Note: Before removing the reservoir close the cold water flow control valve, switch off the circulating
pump, open the rear drain valve then unscrew the bleed screw on the top of the reservoir until the
reservoir has drained. Press the latches on both quick release fittings at the base of the reservoir to detach
it.
3. The various plugs and sockets on the equipment should be given a light spray of de- moisturising
lubricant at regular intervals to ensure smooth and reliable connections.
4. Test the RCD by pressing the TEST button at least once a month. If the RCD does not trip when the TEST
button in pressed then the equipment must not be used and should be checked by a competent
electrician.
A Type K thermocouple simulator should be connected to each socket in turn on the front of the console
and the corresponding zero and span potentiometers adjusted to calibrate the circuit. Calibration at 0°C
(zero potentiometer) and 100°C (span potentiometer) is recommended.
If a thermocouple simulator is not available then a Type K thermocouple (E.g. a thermocouple can be
removed from the quick release fitting at one of the measuring points) can be used with crushed ice and
boiling water as the reference points.
Note: Maintenance of the TH4 Recycle Loops apparatus does not require access to the electrical circuits or
components located inside the moulded plinth. However, in the event of an electrical problem, it may be
necessary for a competent electrician to gain access to the inside of the moulding as follows:
Ensure that the equipment is disconnected from the electrical supply (not just switched off).
Disconnect the electrical leads to the heater and circulating pump from the electrical panel at the rear oTthe
plinth.
Carefully remove the front panel from the electrical console by unscrewing the four fixings.
Disconnect the electrical connections between the top and bottom plinth sections by disconnecting the
appropriate connectors.
Unscrew the six fixings around the periphery of the plinth top.
Carefully lift the top moulded section away from the bottom moulded section and place the top section in a
suitable location.
The electrical circuits inside the bottom moulded plinth section are accessible for working on.
A circuit diagram showing the mains and DC electrical circuits inside the plinth is included in Electrical Wiring
Diagram section 10.8 to assist in fault finding.
Should it be necessary to remove the PCB from inside the electrical console then the PCB Connections diagram
below shows the location and function of the electrical connectors on the PCB to aid re-assembly. Re-assembly
of the equipment is the inverse of the above instructions.
OVERTEMP HEATER
FLOW (irt4nin)
I! El B IE
TEMPERATURE ("O
PCB Connections
ZERO
SPAN
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Armfield Ltd Instruction Manual TH4
rates
When using the appropriate Armfield Teaching Software (optional accessory) the Teaching Exercises may
differ, particularly in the suggested flow rates, and it is recommended that reference is made to the help text
incorporated in the software rather than this manual.
Due to voltage limits on the sensor signals, the software cannot measure flow rates above
3.0 l/min. Flow rates higher than this will be displayed as 3.0 l/min. When operating at flows close to this
value, it is recommended that the flow rate displayed on the integrated control console is also monitored, to
ensure that any deviation above the 3.0 l/min software limit is noted.
14.2 Nomenclature
The following nomenclature has been used for the theory presented in this manual:
Recorded inlet Fi l/min Recorded Flow rate at inlet, recorded from flow
flow rate meter display
Recorded outlet F3 l/min Recorded Flow rate at outlet, recorded from flow
flow rate meter display
Recycle mass Qm2 kg/s Calculated Mass flow rate through the recycle
flow rate loop
Qm2 = P QV2
Outlet mass flow Qm3 kg/s Calculated Mass flow rate at outlet
rate
Qm3 = p QV3
Recycle flow U2 m/s Calculated Velocity of the fluid in the recycle loop
velocity - „ Qv2 u2 = —
Heat transfer QT J/s Calculated Rate of heat transfer from heater and
rate pump to fluid.
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Density of Water
PC-0055698 41 Issue
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14.4 Data Sheet 2
Armfield Ltd Instruction
Manual TH4
Temp. Temp. Specific Temp. Temp. Specific
water water heat water water water heat water
°C K J/kg/K °C K J/kg/K
itfwirnmrmmxmrnirnjmrmnimmw
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Armfield Ltd Instruction
Manual TH4
PC-0055698 43 Issue
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14.5 Data Sheet 3
Armfield Ltd Instruction
Manual TH4
Temp. Temp. Enthalpy Temp. Temp. Enthalpy
water water of water J1 water water of water J
°C K kg °C K / kg
x 103 x 103
28.96 302.11 121.46 130.0 403.15 546.31
PC-0055698 44 Issue
11 April 2016
n rmtit m tr i m t mt m tm tmmtr t
Recycle
loop
pump
Fx = Flow sensor Tx =
Temperature sensor
Objective
To demonstrate the effect of recycle on the total mass flow rate of a system Method
To vary the flow through a recycle loop, while observing the inlet and outlet flow rates of the whole system.
Theory
The recycle loop apparatus may be simply modelled as a generic system, with an inflow (from the water
supply) and an outflow (to the drain).
Under steady state conditions, for equilibrium, the rate of mass flow entering a system must equal the rate of
mass flow leaving a system. The mass flow rate, Qm, is the mass of fluid passing a point in a given time. It may
be calculated as:
V = volume of fluid, in m3
Inlet
Outlet Flow
However, the mass balance for
Check that the inlet is connected to the water supply, and the outlet to a suitable drain.
Check that the heater switch and the pump switch are both in the off (up) position.
Switch on the console, and fully open both the inlet and recycle loop valves.
Use the rotary selector switch on the console to display the output from the inlet flow meter F1 on the digital
meter. Turn on the water supply and increase the pressure slowly to give an indicated flow rate of
approximately 3.5 l/min, then close the pressure regulator to give a flow rate of approximately 3.2 l/min.
Switch on the recycle pump, and allow about five minutes for the air in the system to disperse. Open and
close the recycle loop valve a few times to help in this process.
Switch off the recycle loop pump and close both valves until you are ready to begin the experiment.
Procedure
Turn the rotary selector switch on the console to select the output from the inlet flow meter F1 on the display.
Adjust the inlet valve to give an indicated flowrate of about 1 litre/min.
Change the display to give the output from the recycle loop flow meter F2. Turn on the recycle loop pump,
and open the recycle loop valve to give an indicated recycle flowrate of about 1 litre/min. Wait for the flow
velocities to stabilise.
Record the flowrates for the inlet, the outlet, and the recycle loop.
Continue to open the recycle loop valve to give recycle flow rate increments of approximately 0.5 l/min,
recording the flowrates at each step. Do not exceed 3 l/min as readings will not be accurate from the flow
meter.
Repeat the whole experiment for a range of inlet flowrates. Do not exceed 3.0 l/min as readings will not be
accurate from the flow meter.
Results
Tabulate yoUr results under the following headings:
kg/m3
Conclusions
Describe the effect on the inlet and outlet mass flow rates when the recycle rate is changed. Does this agree
with the theoretical result for the steady state mass balance?
i
I Pressure regulator
Recycle
loop
pump
Fx = Flow sensor Tx =
Temperature sensor
Objective
To investigate the Steady State Heat Balance equation applied to a recycle loop.
Method
To vary the flow rate through a recycle loop, whilst heating the recycle fluid and observing the temperatures
of the inlet, outlet, and recycle loop flow.
Theory
A heat balance over the whole system shows that
Qvi is the volume flow rate at the inlet ( = Qvo, from Exercise A)
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Armfield Ltd TH4
Equipment Set Up
To set up the recycle loop apparatus, you will need to complete the recycle loop. Use the short length of
tubing provided to con-ect the two self-sealing couplings on the unit.
Check that the inlet is connected to the water supply, and the outlet to a suitable drain.
Check that the heater switch and the pump switch are both in the off (up) position.
Switch on the console, and fully open both the inlet and recycle loop valves.
Use the rotary selector switch on the console to display the output from the inlet flow meter F1 on the digital
meter. Turn on the water supply and increase the pressure slowly to give an indicated flow rate of
approximately 3.5 l/min, then close the pressure regulator to give a flow rate of approximately 3.2 l/min.
Switch on the recycle pump, and allow about five minutes for the air in the system to disperse. Open and
close the recycle loop valve a few times to help in this process.
Switch off the recycle loop pump and close both valves until you are ready to begin the experiment.
Procedure
Open the inlet valve to give an inlet flow rate of approximately 1.5 l/min.
Open the recycle loop valve, and then switch on the recycle loop pump. Adjust the recycle oop valve to give
a low flow rate through the recycle loop (typically 1 l/min).
Record the inlet flow rate and temperature. These can be assumed to be constants for each set of results.
Record the recycle loop flow rate, and the recycle loop and outlet temperatures.
Open the recycle loop valve in stages, to give a series of recycle rates. At each step, record the recycle loop
flow rate and temperature, and the outlet temperature.
Results
Convert the gauge temperatures from Celsius into Kelvin (add 273.15).
For each constant inlet flow rate, plot a graph of the recycle temperature, T 2 (in Kelvin), against (1/Qvi + 1/Qv2).
From Equation (2) in the theory, under steady-state conditions the gradient of this graph will be (H/C) and the
intercept with the y-axis will be (T1 + (H/QX)). H can then be found by obtaining the specific heat of water at
the recycle temperature, using the table provided in Data Sheet 2 section 14.4.
Conclusion
Does the recycle rate affect the temperature of the outlet flow, for constant inlet flow rate? Comment
Pressure regulator
Fx = Flow sensor Tx =
Temperature sensor
In unsteady state experiments both the inlet flow and recycle flow are fixed, and the heater is switched either
on or off. The apparatus takes several minutes to respond.
Theory
A heat balance for a small time interval, dt, in which the outlet temperature, T3, changes by dT gives
where
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Armfield Ltd Instruction Manual TH4
Using Eq. (1) from Exercise B to eliminate H, and then integrating from T1 at time 0 gives
Equipment Set Up
To set up the recycle loop apparatus, you will need to complete the recycle loop. Use the short length of
tubing provided to connect the two self-sealing couplings on the unit.
Check that the inlet pipe is connected to the water supply, and the outlet pipe runs to a suitable drain.
Switch on the console, and fully open both the inlet and recycle loop valves.
Turn on the water supply, wait until water is flowing through the system, and then switch on the recycle loop
pump.
Open and close the recycle loop valve a few times to help disperse any air present.
Wait a few seconds until all the air is pumped from the system, then switch off the recycle loop pump and
close both valves until you are ready to begin the experiment.
Procedure
Open the irHet valve and the recycle loop valve. Switch on the recycle loop pump, and wait a few moments
for the system to stabilise.
If using automatic data logging, set the data logger or computer to log at five-second intervals.
If recording manually, note the inlet flow rate and temperature and the recycle rate; these may be assumed
constant for each set of results.
Begin logging or manual recording of the outlet and recycle loop temperatures as the heater is switched on.
If using manual recording, record the values at five-second intervals until the outlet temperature reaches a
constant or near-constant value. This is the steady-state temperature, Ts. If using automatic logging, the inlet
flow rate and temperature and the recycle rate may also be monitored.
Start a new results table, and begin logging or manual recording of the same parameters, this time as the
heater is switched off. Record or log at five-second intervals until the outlet temperature stabilises again.
Results
Tabulate your results under the following headings:
°c
T2
K °C
Outlet temperature
Instruction Manual T3
K
In [ ’ T3 )~|
,(VTi)
TH4
For each set of results, Tind TheTinal outlet temperature, and use this value as the value of
Ts.
Convert the gauge temperatures from Celsius into Kelvin (add 273.15).
Choose two example sets of results, one where the heater was switched off, and a second where the heater
was switched on. For these two results, plot a graph of T3 against elapsed time.
(TS-T3)~
In (VT-I).
For each inlet flow rate, plot a graph of For against time.
AVVVVV1
Additional
volume
Fx = Flow sensor Tx =
Temperature sensor
Objective
To investigate the steady flow energy equation applied to a recycle loop.
Method
To calculate the heat transfer rate at a range of recycle rates, using the steady flow energy equation.
Theory
where
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Issue 11 April 2016
and theLtdsubscripts
Armfield 1 and 3 refer to the inlet and the outlet
Instmction of the control volume respectively (the control
Manual TH4
volume can be considered to coincide with temperature sensors T1 and T3).
With the TH4 apparatus, some assumptions may be made to simplify this equation:
The inlet and outlet are at the same height, so the potential energy term g(z3 - Zi) goes to zero.
The system does no work, so the Qw term becomes negligible. The equation then becomes:
(hi - QT =QI
h3)+i ^32 -U!2)
Qt may be determined fry •experiment, by measuring the inlet and outlet flow rates and
temperatures, providing that the pipe diameter at inlet and outlet of the control volume is known.
Equipment^et Up
To set up the recycle loop apparatus, you will need to complete the recycle loop. Use the short length of
tubing provided to connect the two self-sealing couplings on the unit.
Check that the inlet pipe is connected to the water supply, and the outlet pipe runs to a suitable drain.
Switch on the console, and fully open both the inlet and recycle loop valves.
Turn on the water supply, wait until water is flowing through the system, and then switch on the recycle loop
pump.
Open and close the recycle loop valve a few times to help disperse any air present.
Wait a few seconds until all the air is pumped from the system, then switch off the recycle loop pump and
close both valves until you are ready to begin the experiment.
Procedure
Open the inlet valve and the recycle loop valve. Switch on the recycle loop pump and the heater, and wait
for the outlet temperature to reach a steady value.
Take readings from each of the flow meters and temperature sensors.
Close the recycle valve a little to reduce the recycle rate, and repeat the readings.
Continue to close the recycle valve a little at a time, taking readings at each recycle rate.
Change the flow rate using the inlet valve, and repeat the experiment.
Continue to close the inlet valve a little at a time, and repeat the experiment until readings have been obtained
for a full range of inlet flow rates.
Determine the inlet and outlet enthalpies from the temperatures measured, using the reference table
provided in Data Shes- ? section 14.5. The inlet and outlet velocities may be determined from the inlet and ou
t f: v ate nd the pipe diameter:
Ul = u3 =
d2/4
and
A value for the pipe diameter at the point of flow measurement has been provided in the
nomenclature.
The inlet mass flow rate may be determined from the inlet flow rate and the inlet flow density. The density
may be found from the inlet temperature, using the reference table provided in Data Sheet 1 section 14.3.
Diameter of pipe:
CO co
jij
aj
c=
03 I
Pd
t=f E
O h-
E
o aj
a> "
IZ
JTO
- ja o-s;
2 to » ll a ° E
“ S" is
o ° to (-« «
a) u
ll Oi E a.
c ir SE O ”p
S'S aj u_ re LL E
Q:
Conclusion
Describe any relationship found between recycle rate and heat transfer rate.
Comment on the assumptions made in the steady flow energy equation. What factors might affect the validity
of these assumptions?
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Armfield Ltd Instruction Manual TH4
What other factors may be affecting the results that have not been accounted for in the equation?
Fx = Flow sensor Tx =
Temperature sensor
Objective
To investigate the effect of parameter changes on response rates.
Method
To vary parameters such as heater power and recycle loop volume, and investigate any subsequent change
in system response.
Theory
Following a change to the system input or parameters the system will take some time to return to equilibrium
conditions. The speed of this response and the shape of the response curve is of some importance in an
industrial situation, as it will affect how quickly the system can be matched to the required conditions.
Three system parameters will be investigated in this experiment. Each parameter will be varied independently,
and the corresponding effect on system response investigated:
Through flow, the total volume flow rate through the whole system, which determines the total mass
of fluid in the heat balance equation.
Recycle flow, the volume flow rate through the recycle loop.
Loop volume, the total volume of fluid that is contained in the recycle loop.
Equipment Set Up
To set up the recycle loop apparatus, you will need to complete the recycle loop. Use the clear Perspex
reservoir provided to connect the two self-sealing couplings on the unit.
Switch on the console, and fully open both the inlet and recycle loop valves.
Turn on the water supply, wait until water is flowing through the system, and then switch on the recycle loop
pump.
Open and close the recycle loop valve a few times to help disperse any air present.
Wait a few seconds until all the air is pumped from the system, then switch off the recycle loop pump and
close both valves until you are ready to begin the experiment.
Procedure
Open the inlet valve and the recycle loop valve and then switch on the recycle loop pump. Response rate
measurement procedure:
If using automatic data logging, set the data logger or computer to log at five-second intervals. ~
Note the inlet temperature. This can be assumed constant for each set of measurements.
Begin logging or manual recording of the outlet and recycle loop temperatures as the heater is switched on.
If using manual recording, record the values at five-second intervals until the outlet temperature reaches a
constant or near-constant value.
Start a new results table, and begin logging or manual recording of the same parameters, this time as the
heater is switched off. Record or log at five-second intervals until the outlet temperature stabilises again.
Through flow:
Keeping all other system parameters constant, change the system through flow by adjusting the inlet valve.
Perform response rate measurements for a range of through flow rates.
Recycle flow:
Keeping all other system parameters constant, change the recycle flow rate by adjusting the recycle loop
valve. Perform response rate measurements for a range of recycle rates.
Loop volume:
Keeping all other system parameters constant, change the recycle flow volume by replacing the Perspex
reservoir with the short length of flexible pipe provided. Perform the response rate measurement at this new
recycle loop volume. If desired, further changes in volume may be generated by using different lengths of
pipe (not supplied).
Results
Tabulate your results under the following headings:
Conclusion
Describe the effect that changing each parameter had on the response rate observed. Include observations
on both the direction and the magnitude of any change.
Compare the responses of the recycle loop temperature and the outlet temperature. Which parameter
changes produce the greatest lag between the two responses?
Compare the results from the different parameters. Which parameter produced the greatest change in
response? Which had the least effect?
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Armfield Ltd Instruction Manual TH4
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