STD-ASTM ALS3/AL93M REV A-ENGL 1997 MM O7S9S10 Ob07b57 823 a afl Designation: A 193/A 193M - 97a /AUERICAN SOCIETY FOR TESTING AND MATENALS noeraod ty Mantacurers Standen Soc ‘ta Valve aa Pings raat) ‘Use in USNAC ADT standards ‘eptember Soe AST Sana Copah AST Standard Specification for Alloy-Steel and Stainless Steel Bolting Materials for High- Temperature Service’ ‘his tandad is ssl under the ised designation A 13/4 193M: the number mmedately following the designation nice the ese ‘of eiinal adoption rn the ease of revision, he per of revision. A nurber i parethsss acts the year of la epprval A supesrpt epsilon ( indeates n eal charge since the ast revision oe rppoval ‘This standard has Been epproved frase by agencies of the Deparment of Defense. 1, Scope 1.1 This specification? covers alloy and stainless stee! bolt- ing material for pressure vessels, valves, flanges, and fittings for high-temperature service. The term “bolting material” as used in this specification covers bars, bolts, screws, studs, stud bolts and wire. Bars and wire shall be hot-wrought. The ‘material may be further processed by centerless grinding or by cold drawing. Austenitic stainless stee! may be carbide solution treated or carbide solution treated and strain-hardened, 1.2 Several grades are covered, including ferritic steels und austenitic stainless steels designated B 5, B 8, etc. Selection will depend upon design, service conditions, mechanical prop- cnties, and high-temperature characteristics, Nore I—The commince formulating this specification has included fifteen stel types that have been rather extensively used for the present purpose. Other compositions will be considered for inclusion by the ‘committee from time to time as the need becomes apparent. [Nore 2—For grades of alloystel bolting material suitable for use at the lower range of high-temperature applications, reference should be ‘made 19 Specification A 354, [Note 3—For grades ofalloy-stee! bolting material suitable for use in low-temperature applications, reference should be made to Specifation ‘A 320/4 320M. 1.3 Nuts for use with this bolting material are covered in Section 14, 1.4 Supplementary Requirements $1 through $8 are pro- vided for use when additional tests or inspection are desired, These shall apply only when specified in the purchase order. 1.5 This specification is expressed in both inch-pound units and in SI units. However, unless the order specifies the applicable “M” specification designation (SI units), the mate- rial shall be furnished to inch-pound units. "This speciation is under the json of ASTM Commitee AI on Stel ‘Stainless Ste. und Relat Alloysand isthe det responsibly of Subsommites| ‘A0122 on Valves, Fitings, Bolg, and Fangs for High and Sebatmosphene iret edition approved Mach 10, and June 10, 1997. Publied December 1997. Originally published as A 199-367 Late previous edition A 193) 1930456 *'For ASME Boiler and Presse Vessel Code applictons see reed Spel ation SA-193 in Seaton Il of that Code 1.6 The values stated in either inch-pound units or SI units, are to be regarded separately as standard. Within the text, the ‘SI units are shown in brackets. The values stated in each system are not exact equivalents; therefore, each system must 'be used independently of the other. Combining values from the ‘two systems may result in nonconformance with the specifi- cation, 2. Referenced Documents 21 ASTM Standards: ‘A28/A 29M_ Specification for General Requirements for Steel Bars, Carbon and Alloy, Hot-Wrought and Cold Finished? A I94/A 194M. Specification for Carbon and Alloy Steel Nuts for Bolts for High-Pressure and High-Temperature Service® A320/A 320M. Specification for Alloy Stee! Bolting Me- terials for Low-Temperature Service® ‘A354 Specification for Quenched and ‘Tempered Alloy Steel Bolts, Studs, and Other Externally Threaded Fasten- ‘A370 Test Methods and Definitions for Mechanical Testing of Steel Products! * AATSIA4T9M Specification for Stainless and Heat- Resisting Bars and Shapes for Use in Boilers and Other Pressure Vessels® A 484/A. 484M Specification for General Requirements for Stainless and Heat-Resisting Bars, Billets, and Forgings? A7SI Test Methods, Practices, and ‘Terminology for Chemical Analysis of Steel Products® A788 Specification for Steel Forgings, General Require- ments? E 18 Test Methods for Rockwell Hardness. and Rockwell Superficial Hardness of Metallic Materials” E21 Practice for Elevated Temperature Tension ‘Tests of Metallic Materials? 3 mut Book af AST Stondards, ol OLS ‘Annual Rook ef ASTM Standards, YOON * Annual Book of ASTM Stondaris. Vo 15.08 “ Annual Book of ASTM Standards, Vl 0103 annual Book of ASTM Stondans, VoL O30.STD-ASTM ALQ3/AL93M REV A-ENGL 1997 MM 0759520 Ob07658 767 ml (ih) A 193/8 193M E 139 Practice for Conducting Creep, Creep-Rupture, and Stress-Rupture Tests of Metallic Materials? E150 Practice for Conducting Creep and Creep-Rupture Tension Tests of Metallic Materials Under Conditions of Rapid Heating and Short Times® E151 Practice for Tension Tests of Metallic Materials at Elevated Temperatures with Rapid Heating and Conven- tional or Rapid Strain Rates* E292 Practice for Conducting Time-for-Rupture Notch ‘Tension Tests of Materials? E328 Methods for Stress-Relaxation Tests for Materials and Structures” E 381 Method of Macroetch Testing, Inspection, and Rating ‘Steel Products, Comprising Bars, Billets, Blooms and Forgings” E 566 Practice for Electromagnetic (Eddy-Current) Sorting, of Ferrous Metals” E709 Guide for Magnetic Particle Examination” F 606 Test Methods for Determining the Mechanical Prop- erties of Externally and Internally Threaded Fasteners, Washers, and Rivets'® 22. ANSI Standards:"' BL.1 Screw Threads B 18.2.1 Square and Hex Bolts and Screws B 18.3 Hexagon Socket and Spline Socket Screws 2.3 AIAG Standard: AIAG B-5 02.00 Primary Metals Identification Tag Appli- cation Standard”? 3. Ordering Information 3.1 The inquiry and order for material under this specifica tion shall include the following as required to describe the ‘material adequately: 3.1.1 Specification, designation, year date, and grade. 3.1.2 Heat-treated condition (that is, normalized and tem- peted, or quenched and tempered, for the ferritic materials, and carbide solution treated (Class 1), carbide solution treated after finishing (Class 1A), and carbide solution treated and strain hardened (Classes 2, 2B and 2C), for the austenitic stainless steels; Classes 1B and IC apply to the carbide solution-treated nitrogen-bearing stainless steels; Class ID applies to material carbide solution treated by cooling rapidly from the rolling temperature) 3.1.3 Quantity (that is, number of pieces or weight), 3.1.4 Description of items required (that is, bars, bolts, serews, o studs), 3.1.5 Dimensions (that is, diameter, length of point, overall length, finish, shape, and threads), ® Discontined, see 1983 Antal Book of ASTM Standards, Vl 030 “Anal Book of ASTM Stndrds, ol 0303. dual Book of ASTM Sandan, Nol 13.08. "Ava fom Amica National Standards Ie, 11 West 208 St, 13th Flos, New York, NY 10036 "grail from Avtomive Industry Acton Croup, 26200 Laser, Suite 200, Sout, 448034, 3.1.6 Nuts, 14.1, 3.1.7 Supplementary requirements, if any, and 3.1.8 Special requirements, in accordance with 6:3, 6.6, 113, 15.1, 16.1, 18.1, and 17.1 4, Manufacture (Process) 4.1 The steel shall be produced by any of the following processes: open-hearth, basic-oxygen, electric-furnace or vacuum-induction melting (VIM). The primary melting method may incorporate separate degassing of refining. The molten steel may be vacuum-treated priot to or during pouring of the ingot or strand casting, The basic-oxygen process shall be limited to steels containing not over 6 % chromium. 4.2 Quality—To ensure soundness, ferrtic steel bars and wire shall be tested in accordance with Method E 381, or other suitable method as agreed upon between the purchaser and the producer. When bar or wire is supplied, the bar or wire producer shall perform the test. When fasteners are supplied, either the bar or wire producer or the fastener producer, as agreed upon between them, shall perform the test. Quality control procedures shall be sufficient to demonstrate that the testing was performed and that the results were acceptable. A bar lot consisting of one heat or 10 000 Ibs whichever is smaller, shall be represented by a minimum of one macroetch. Visual ‘examination of transverse sections shall show no imperfections worse than the macrographs of Method E 381 S4-R4-C4 or equivalent as agreed upon. Distinct zones of solidification shall not be present, 5, Discard 5.1 A sufficient discard shall be made to secure freedom from injurious piping and undue segregation. if required by purchaser, in accordance with 6, Heat Treatment 6.1 Ferrtic steels shall be properly heat treated as best suits, the high-temperature characteristics of each grade, Immedi ately after rolling or forging, the bolting material shall be allowed to cool to a temperature below the cooling transfor mation range, The materials which are to be furnished in the Tiquid-quenched condition shall then be uniformly reheated to the proper temperature to refine the grain (a group thus reheated being known as a “quenching charge") and quenched in a liquid medium under substantially uniform conditions for each quenching charge. Use of water quenching is prohibited for any ferritic grade when heat treatment is part of the fastener ‘manufacturing process. This prohibition does not apply to heat treated bar or to fasteners machined therefrom. Material Grade B16 shall be heated to a temperature range of 1700° to 1750°F [925° to 954°C] and oil quenched. The materials that are (0 be furnished in the normalized or air-quenched condition shall be reheated to the proper temperature to refine the grain and cooled uniformly in air to a temperature below the transfor- ‘mation temperature range. The material, whether liquid- ‘quenched or normalized, shall then be uniformly reheated for tempering. The minimum tempering temperature shall be as specified in Table 2.STD-ASTM ALS3/AL93M REV A-ENGL 2997 Ml 0759530 Ob07659 LTL mm 4) A 19978 193M TABLE 1 Chemical Requirements (Composition, percent)* Tne Fonte Stele iderfeaton Sto! os a ana Bax rece {3 Corum (ASI Tpe 501) 12% Chromium (IS! Type 470) ‘Si Type 40) Range Product Vara, Range Product Vaan (ver or Under? Over or Under Caton tioma ‘Or under 075 max 001 over Manganese, max 400 0.08 over 100 0.03 over Phosphorus, max oto (2.008 over 000 2.008 over Sut max ooa0 0.006 over 003 91008 over Sco | 4100 max 005 over 11.00 max 05 over Chromium 4060 030 5495 O18 Moyasnum ooo 0.05 Tipe Forte tsa lontfeaon Symbol oem Be Gree ‘Ghromiam-Achbdenun (AIS 4140, 4742, 416, CGiomiumavederum-vanacian “SOM, 42H, and 41461), Pred Varaton, Produ Varaion Range Over or Under ange (ver or Unde ‘arson oarawe 002 036047 002 Manganese reer O08 045070 03 Phosphor, max Boas 9.005 over as 1.006 over Sulu, max 080 2.008 over ou 1008 over Sticon ors03s 02 015095 bo (Crim oret20 005 080115 05 Mo}jodenum otso2s 002 soos 03 Vonadium 25038 003 ‘Aim, a Bors. De Austenitic Stele Clases 1, 18, 10, and 2 i sentation Symbol Bs, oa BRO, BCA BEM, BBA, BAND, BONS Ba BaP Grace ‘Urstanized 16 Crema Suablzed 18 Chorin ® 16 Chromiun10 Naket2 Untailized 18 Conia ckel (AIS Type 304) Nika 1 Typ9 247), oon (AISI Tyee 318) Ne (ASI Type 205 with, eatieled earbon) ProduetVaaten, Produc aration, py ‘Produ Vario, pang, Prt Varian, Farge over ocUnder® "FAP ovorer Under?” FAP Over or Under®™” R89 Gero Under Carbon, max 08 00r over 008 Lo over 008 dor over (008 Ot ver Manganese, max 2.00.04 oer 200 © antever 200 dos over 200 ok over Phosphor, max «OOKS«OGt over Dow apioever 00% —— oo10 over 0.045 O10 vee Sut max 090 0.008 aver Dox cons ever 003 0005 over 0.030 0.005 over Seon, max 100.008 over 100 aasver 100 0.05 over 100 005 ever chrom 390200 0.20 wo10 020 Woo 020 170-190 0.20 Nike! Bo105 015 9010 048 sor 048 105330 015 Moybdenum 200800 040 Coumtium + 10 xcarton 005 under ‘actalum content, Twe Austoniie Stele Classe 1A, 18, 1D, and 2 identiction Sb BN, BNA IN, BaNINA BeULGuN, BOMLCANA Grade ‘AISI Type 204N) (SI Type S16N) peta, 20 Gvomium, 18 Nel, & Moiodenum with rotted aon Fr reduc Varaion, = Product Variation, Range ange vor or Une | Range vero Unde ‘arbor max ‘08 001 over O08 001 over 20 Manganese, max 200 0.4 over 200 04 over 100 Prosphows, max 0s 0.010 over 04s: 0010 over 0.030 ‘Suite max 0.080 0.008 over 0.0% 0.008 over 000 Slicer, ma 100 0.08 over 100 0.06 over 080 CCrvomiom tao200 = 020 180-180 020 195205, Nieket 0705 015 300140 ois vsi85 ‘Moyodenum 200300 010 sos ‘Niogon dino = aot o10016 oot O1e022 Sooper 050-100 3STD-ASTM ALV3/AL93M REV A-ENGL 1997 MM O759510 OLO7b60 318 mm jp A 193/A 193M TABLE 1 Continued Tre “useniie Seas Cases 1. 1A and? icerateaten Synbot B87, 667A Grace ‘aod 18 Gorian-8 Nek (WS! Type 62 = Produ rian Over of Una Gatton max 208 Manganese, mx 200 Phoshons, max cots Sul, max uso Sie, mx +00 Nett soo rem i7oa80 ‘ann Ercarbon cover in Te Aucune Stet Cases 1C and 10 icerteaten Symbol ____ Ban. Bana 255, ESA Grado 7 Ghvemivn13 Rixas Manganese Te Grerion'8 Neko Seon + Nope Prout Varin rat Varaton, erge Over or Ure Penge Over or Unde Carton max 008 001 or ano G0 ever Marganove soso 005 r090 a0, Prosprus max oto 0005 over oo {005 over ‘utr max 080 005 rer 080, «005 over Sicon ‘00 mae Oa ove a545 015 Chromium 2o5235 025 teo180 a0 Nel nes O15 e090 ao Metyosonam 1503.00 610 Nirogon 020040 ae 08018 on Cotambum + aan 10030 005 vara 10030 ae Te ‘Austere Seas, Classes 1, And 10 icertzaton Sbat Bain, BaINA BENIN, BMWA Seace (Si Te 500 win vested career) (ST STON win retied eaten) a rode Varin aS rosa arin ange Over Unde deo rer or Unser” Sarton 2030 0.005 over om00 2005 oer Manganese 200 Cot over 200, Sou ovr Prephors, mac 004s O10 over 046 D010 0" Sutin mae 030 005 over tao 0.095 oe" ‘Steen +00 Cos over ‘00 0.05 or ‘ever aoz00 020 i600 020 Nt sors ors joot40 as Netyosenam 200300 a0 aooen| coors oo orware aot “he intotonladalton of Bi Sa, Te and Pb isnot ported * Product analyie—ndvoual determinations sometimes vary rem the specsled mits on anges as shown inthe tables. The several determinations of any indvidua cement ina nest may na vary both above ans teow tbo spoatod argo ‘Zorba sizes ver Sin (20m, ns, to carbon conn maybe 0.50 %e, max. For the G7M grade, a imum carbon content of 0.28% Is permit provided that he raquiod tenalepropertes are met in tho secon 8265 vue he usec AISI 430 or 40H i lowed ‘Total of soluble and soul Classes 1 and 1D aro solution Veal, Clases 1, 18 and ome 1C (BBR and BES) procclsao made rom sluten ested mate. Class 1A (BBA, BCA, COMA, BPA.BETA BELNA, SEMLNA, BENA and BEMINA) and some Clase TC (BORA and BUSA) produits are sluton Wssed in he inshed conten. Cass 2 products are feluton toad and ean PardoneaSTD-ASTM AL93/AL93N REV A-ENGL 1997 MM 0759510 ObO7bb1 254 mm Gi) A 193/A 193M TABLE 2 Mechanical Requirements Micimum Tense Yall Strength, Elngaton Reducton Haross, Tempeing —Steng, "mn. ntD. olAta, max Grae iameter, in. (re) ‘Temperature, min, ki fst, min, % in, % Perel Patt Pa) Fer Sele 35 410.6% chrorsam up 04 [00 fe ‘100 593) 100,600) en s80} «© 28 19% erromim wp 4100, 1100 593) 04780) as ses} a) bx 19 %ehemium upto 4 (109 a Hoo (885) 90620) 70485) 18 5s HRC er Cronidmebderum wp to 26 (65), ne ‘100 9) s25(860) 10520) 1850 sz Hor 3S HC over 241041651 100) cl 1100(590) 5,75) 55) 169M SOHC over 410710010 180) et HoD(SRa}—100(600) 754515) eB HRC ont CCromismmabederum up 2% (61 in 1is0,620] —s00(600) e080) 18 285 HBr one over 210416510 100) nd 19501620) 100,690) 00(550) 10 aN oon ver 4197 10010 180, nel 19501620) 100600) 751518) 18 0 5 BNor oon ars Ctromsimmolederumvanadm yp to 2 65) i 2001850) 125,860) 105,725) 18 6 ator aS HR over 20 465% 100) het 200850) 140 (780) 95 (655 7 ahr SHR ‘over 4107 [10010 1605 el 1200 (860) 100(600) 05 (586 16 45 a7 Bor 20HR serale ‘old Engaon poe stengtn, Mi) Redon anges, (ass and Grado, Diam (o] Heat Toten? Sveng mmo? min of Aa, 2 Nn Sotset nn ca (ural seis ‘lasses 1 ana 10:68, BBN, BOP, BOLN, carbide soon Wea 75 55) wii a) «CRO Bose RB BBMLN, al ametrs (aes 1 8, 8 a abide sluton teated 75,515) so (20s) 050-228 HB or eH ‘arate Css 1A: B2A.BSCA, SOWA. SEPA, carbide soliton Westen the fhished 75 515) so (20s) 050 Te HB or SoH DSTA, BHLNA, BOMLNA. BONA, BBMNA Condon Classes 18 and 10: 69N, BUN, ard carbide sli ested 0 50) ssi] 900 2ea HB or gS RE BOMLCUN, all ators asses 1C and 10: 69R cametore care soliton tested 10 90) 55 (000) 555 ar HmorzaHAC Cass 1: BORA, a ameters arbide soliton Wate inthe Hshed 100 [oso Sis] BS weaB HRC eraon Classes 1C and 10: 865, al ameter carbide soliton Weated 5 [6s 5015) 3555 HworzaHAC Gln 16: 888A, Cate Soliton esl nth shed E55 BOIS) 35S BAB Or 2B HRC ‘i aneion condon Css 2:88, 880, BBP, G6, and BEN. cai sluton eaed and stain 125 860) joole} 2S se Boras HRC 9120) and ee ‘arenes {Wor 1 1, (200 251k 119 705 sols] 55ST Bocas HRC ter 10 1425 32] 105 (725) sliso] 2) SRI HBOS HRC ver 44 4 [92 640 10 90) Solis) 23ST HBOS RE (ls 2: 86M, BAHN, BNKLCUN® cat acluton eted and stan 110700) 96065) 1845 aR HB ors HRC 2) an uncer hardened ‘vero 1 20 t 25) in 100 (600 sols) = 24s set Horas HRC Seer 1% (5 rl 95 (685) 85s) 2545 SRT HBOS HAC ver 41015 8219 nel 90 (620 5O(] 3045 SRI HB Or BS HAC los 89, 202" carte soliton tealed and stain 88 [65] Tis!) 25 REN HB OS HRC ‘arenes 2 (1) ana nger vr 21 (6 62 el 0 (620 esee0) 30 a21 Ho or 9S HRCSTD-ASTM AL93/AL93M REV A-ENGL 1597 MM 0759510 ObO7bb2 190 mm qb A 1939/4 193M. TABLE 2 Continued Yield Elongation aoe Seng nD. RedicIOn—odneas, (ass and Grade, ameter) Hest Treatment? sueraih min02—min% ofiea, arose, neal ose win ssilvPal Testi Sea ‘ver 2 19 863 nel 30 (550 we) 20 HBorgS HAG cies 20: Ban? carte soliion veates and stain 85 (585) 6560) 30). SAT HB OF SS HAG Fardonee 251) ana nde 215i 5 [505 eo (sis 9060 Sat HB or a5 HAC 36 eels requrerers, he Binal hardnoss shal bo over 200 HB (83 HRB). Class {is sailon reain, Clas tA elton ead inthe fished conditon fr carsion esstance: het eaiment is rial due to physical proprty requirement Class 2s colton eated and sain hardened. Ausente sts in he saihardenedcanditon may not show unr properestreughout the ston pariuay in S295 over 318. 20 mm in amt ‘Sor ezoe 20 min ameter and ema For eharotere 1 [38] and over, cet (eae) pop 6.1.1 Quenched and tempered or normalized and tempered ferrtic material that is subsequently cold drawn for dimen- sional control shall be stress-relieved after cold drawing. The minimum stress-relief temperature shall be 100°F [55°C] below the tempering temperature. Tests for mechanical prop- erties shall be performed after stress relieving. 6.2 Both B6 and B6X materials shall be held, at the tempering temperature for a minimum time of 1 h. Identifica- tion Symbol B 6X material may be furnished in the as-rolled- and-tempered condition. Cold working is permitted with the hardness limitation (26 HRC maximum) of Table 2 for the BOX grade. 6.3 All austenitic stainless steels shall receive a carbide solution treatment. Classes 1, 1B, IC (Grades B8R and B8S only), 2, 2B, and 2C can apply to bar, wire, and finished fasteners. Class 1A (all grades) and Class 1C (grades B8RA and BBSA only) can apply to finished fasteners. Class 1D applies only to bar and wire and finished fasteners that are machined directly from Class ID bar or wire without any subsequent hot or cold working. 63.1 Classes 1 and 1B, and Class 1C Grades B&R and B8S—Atter rolling of the bar, forging, or heading, whether done hot or cold, the material shall be heated from ambient temperature and held a sufficient time at a temperature at which the chromium carbide will go into solution and then shall be cooled at a rate sufficient to prevent the precipitation of the carbide. 6.3.2 Class ID—Rolled or forged Grades B8, B8M, BSP, BSLN, BEMLN, BSN, B8MN, BSR, and B8S bar shall be cooled rapidly immediately following hot working while the temperature is above 1750°F [955°C], so that grain boundary carbides are in solutioin, (See A479-88) and subsequent revisions). Class ID shall be restricted to applications at temperatures less than 850°F [455°C]. 6.33 Class IA and Class 1C Grades BSRA and B8SA— Finished fasteners shall be carbide solution treated after all rolling, forging, heading, and threading operations are com- plete. This designation does not apply to starting material such a bar. Fasteners shall be heated from ambient temperature and held a sufficient time at @ temperature at which the chromium, carbide will go into solution and then shall be cooled at a rate sufficient to prevent the precipitation ofthe carbide. mum harass ct 241 H (100 HAS) Is pamitod 2 may be lower han Indicated ty tet repos which are based on valves datermine at ¥ aus 634 Classes 2, 2B, and 2C—Matertial shall be carbide solution treated by heating from ambient temperature and holding a sufficient time at a temperature at which the chromium carbide will go into solution and then cooling at a rate sufficient to prevent the precipitation of the carbide. Following this treatment the material shall then be strain hardened to achieve the required properties. Nore 4—Heat weatmont following operation performed ona limited portion ofthe product, sich as heading, may result n now-aniform pain Size and mechanical properies though Ue Seton aete 64 If scale-free bright finish is required, this shall be specified in the purchase order. 65 B7 and B7M bolting material shall be heat treated by quenching in a liquid medium and tempering. For BTM bolting, the final heat treatment, which may be the tempering operation if conducted at 1150°F [620°C] minimum, shall be done afer all machining and forming operations, including thread rolling, are complete 65.1 Unless otherwise specified, material for Grade B7 may be heat treated by the Furnace, the Induction or the Electrical Resistance method, ors $—It should be taken into consideration that stress-tlaxtion properties may vary fom heat lot heat ot oe these properties may vary from one heat eating method 0 another The purchaser may specify Requirement S8, fstese-rlaxation testing is dese. 7. Chemical Composition 7.1 Each alloy shall conform to the chemical composition requirements prescribed in Table 1. Steels with added lead shall not be used. 7.2 The steel shall not contain an unspecified element for the ordered grade to the extent that the stel conforms to the requirements of another grade for which that element is a specified element. Furthermore, elements present in concentra- tions greater than 0.75 weight/% shall be reported. Chemical analysis shall be performed in accordance with Test Methods ATI 8. Heat Analysis 8.1 An analysis of each heat of steel shall be made by the manufacturer to determine the percentages of the elements specified in Section 7. This analysis shall be made from a test