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International Journal of Multiphase Flow 69 (2015) 18–30

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International Journal of Multiphase Flow


j o u r n a l h o m e p a g e : w w w . e l s e v i e r . c o m / l o c a t e / i j m u l fl o w

Bubble characterization in horizontal air–water intermittent flow


W.R. de Oliveira, I.B. de Paula, F.J.W.A. Martins, P.S.C. Farias, L.F.A. Azevedo ⇑
Departamento de Engenharia Mecânica, Pontifícia Universidade Católica do Rio de Janeiro – PUC-Rio, Rio de Janeiro, Brazil

a r t i c l e i n f o a b s t r a c t

Article history: Elongated bubbles were characterized experimentally for air–water flow in a horizontal pipe at nearly
Received 26 December 2013 atmospheric conditions. The range of flow rates employed covered regimes at the transition from
Received in revised form 2 October 2014 elongated bubble to slug. Ensemble-averaged digital image processing techniques were applied for detec-
Accepted 21 October 2014
tion of the liquid–gas interface with aid of a set of photo gates to synchronize bubble passage with image
Available online 29 October 2014
acquisition. Quantitative data of front and tail parts of the bubbles were analysed for different mixture
velocities and the results confirmed visual observations frequently reported in the literature. Close to
Keywords:
transition, a linear tendency of the bubble nose to move towards the pipe centerline position, for increas-
Slug flow
Elongated bubble
ingly higher values of the Froude numbers, was observed and quantified. Bubble tail shapes were
Air–water flow quantified and the hydraulic jumps were shown to be dependent of Froude number, while the liquid film
Image processing thicknesses were governed by the liquid volume fraction. Changes on the bubbles characteristics are
apparently linked to variations in the bubble velocities and seem to reflect a competition between viscous
and inertia effects.
Ó 2014 Elsevier Ltd. All rights reserved.

Introduction separated from one another by gas bubbles, travelling near the
centre of the pipe. In this last regime, the frequency of flow inter-
The transport of gas and liquid simultaneously in horizontal mittence is higher when compared to plug flow. Also, the typical
pipelines is present in many engineering applications. During the lengths of liquid slugs and bubbles are much shorter when com-
last decades, an intense effort has been devoted to the study and pared to plug flow.
modelling of the flow characteristics in order to increase safety In the oil and gas industry, significant capital losses can occur
and profit margins in pipeline operations (see Havre et al., 2000, when long liquid slugs are present due to the elevated pressure
for a review). levels generated by their passage that can, for safety reasons,
An important characteristic of two phase flows is the existence require production shut down. Also, intermittent flows can induce
of a variety of flow regimes, depending, among other variables, on severe transient loads on the structures with potentially cata-
the flow rates of each phase. These regimes are defined based on strophic consequences. Although the slug and the plug flow
the geometrical distribution of phases in the pipe cross section regimes are both considered intermittent, the typical loads, lengths
(see Mandhane et al., 1974; Taitel and Dukler, 1976). The present of slugs and bubbles and frequencies associated with each regime
work is devoted to investigating the horizontal intermittent flow can be remarkably different (see Nydal et al., 1992; Hurlburt and
regime that is characterized by the passage of a succession of liquid Hanratty, 2002; Kadri et al., 2009). Thus, it is very important to dis-
slugs followed by elongated bubbles travelling above a thin liquid tinguish between these regimes for a proper design of pipelines
film. Intermittent flows can be subdivided into two sub-regimes: and damping devices, such as the slug catchers.
(i) plug or elongated bubble flow and (ii) slug flow. The plug flow According to the flow maps of Mandhane et al. (1974), Taitel
regime is found at low flow rates. It is usually composed of liquid and Dukler (1976), Barnea (1987), Lin and Hanratty (1987a),
slugs with a low concentration of dispersed gas bubbles followed among others, for a given liquid superficial velocity, the transition
by elongated bubbles that move along the top of the pipe. Accord- from plug to slug regime is expected to occur above a threshold of
ing to Kadri et al. (2009), in this regime the liquid slugs can extend gas velocities. However, at transition, these two regimes are not
for more than 100 pipe diameters. The slug flow regime is charac- clearly distinguishable, especially for the case of horizontal pipes.
terized by the intermittent appearance of aerated liquid slugs, The absence of dispersed gas bubbles was suggested by Barnea
et al. (1980), as a criterion to distinguish plug from slug regime.
Lin and Hanratty (1987b), used pressure measurements to define
⇑ Corresponding author. the transition threshold. Based on a photographic study, Ruder

http://dx.doi.org/10.1016/j.ijmultiphaseflow.2014.10.014
0301-9322/Ó 2014 Elsevier Ltd. All rights reserved.
W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30 19

et al. (1989), described plug flows as being an unaerated liquid slug Fluorinated Ethylene Propylene (FEP) pipes, in order to reduce
followed by a gas bubble with characteristics similar to a ‘‘Benja- optical distortions during image acquisition. This material was pre-
min bubble’’ (Benjamin, 1968). Later, this definition was extended viously used in the work of Hewitt et al. (1990), and it proved to
by Ruder and Hanratty (1990), with the aid of pressure pulsation reduce light scattering at the wall due to the matching of its refrac-
and void fraction measurements, and photographic visualization, tive index with that of water.
to include qualitative characteristics of the front and rear part of Air and water were injected into the section by a ‘‘Y’’ junction
the bubbles. They suggested that the transition from plug to slug located at the inlet of the test pipe. A split plate was mounted
regimes occurs when the tail of the bubble approximates the form inside the junction to reduce the level of flow fluctuations at the
of a single-stage hydraulic jump. Although they have measured dif- inlet. Water was pumped in closed loop at superficial liquid veloc-
ferent parameters of the flow, the major contribution to define ities up to 0.5 m/s. A centrifugal compressor provided air to the test
plug flows was derived from qualitative analysis of a restricted section with velocities up to 40 m/s. The flow rates of air and water
number of images. Based on observations of different behaviours were measured using calibrated turbines, CONTECHÒ models SVTG
for the two regimes, Fagundes Netto et al. (1999) also suggested G19 and SVTL L19, with experimental uncertainties estimated to
the use of the characteristic shapes of the front and rear of elon- be within 1% and 0.5%, respectively. At the end of the line, the
gated bubbles as a means of accessing transition. They suggested air–water mixture was separated into two vessels from where
the angle of the hydraulic jump at the rear of the bubble as a the water was returned to the pump inlet, while the air was vented
possible criterion to define this threshold. out of the laboratory space.
The goal of the present study is to apply quantitative visualiza- The measurement section was located at a distance of approxi-
tion techniques to investigate the shape of the rear and front parts mately 400 pipe diameters from the inlet. It was composed of three
of the bubbles in the transition from plug to slug regimes. This infrared gate sensors, PASCOÒ model ME-9204B, a CMOS high
work was motivated by the recent availability of high frame rate frame rate camera (Motion Pro X3TM with 1.3MPixels), an illumi-
cameras that, combined with techniques for image analysis, added nating panel of LEDs, and a visualization box. As will be described
new possibilities to address the problem. The combination of these shortly, the infrared gates had a dual role in the experiments. They
techniques have been used to investigate two-phase flows in were used to measure slug statistics, such as slug length, velocity
several works, such as (Polonsky et al., 1999; Nogueira et al., 2003; and frequency, as well as to provide a trigger signal for the image
Ursenbacher, 2004; Shemer et al., 2007; Mayor et al., 2007; Guo acquisition system. Downstream of the photo gates, the FEP tube
et al., 2010). The non-intrusive nature of these techniques make was encased in a visualization box filled with water in order to
them suitable for studying flow regimes sensitive to disturbances, reduce refractive indexes mismatches. On the opposite side of
such as plug, slug and annular flows. The main drawback of the the camera, the panel of high power white LEDs was installed to
technique is the requirement of optical access to the flow. provide background illumination for image acquisition with proper
In the present work, procedures based on back-illuminated contrast.
bubble images were combined with a high frame rate digital
camera to enable the extraction of the bubble-slug interfaces at Measurement of bubble and slug statistics
the transition from plug to slug flow. Back-illuminated bubble
images have been widely used in the literature as a two-phase flow The three infrared photo gate sensors mentioned before are pre-
visualization technique (e.g. Bendiksen, 1984; Ruder and Hanratty, sented in more detail in Fig. 2. They were employed to measure the
1990). Also, the acquisition of images triggered by the passage bubble and slug statistics of interest, namely, bubble front and rear
of bubbles has been extensively applied to investigate bubble velocities, slug length and slug frequency. These parameters were
behaviour in two-phase pipe flow (e.g. Gopal and Jepson, 1998; estimated as suggested in the work of Polonsky et al. (1999). The
Polonsky et al., 1999; van Hout et al., 2002; Nogueira et al., three infrared gates were installed orthogonally to the pipe, and
2003; Ursenbacher, 2004; Mayor et al., 2007; Guo et al., 2010; spaced 0.3 m from each other (Ddgates). According to preliminary
Shemer et al., 2007). In the works of Polonsky et al. (1999), Pinto experiments, a sensible noise reduction in the signals from the
et al. (2001), Shemer et al. (2007), Mayor et al. (2007), the photo gates was observed when the sensors were placed close to
techniques for extraction of instantaneous and averaged bubble the centerline of the pipe. The reason for this behaviour is the high
contours, as well as for quantitative measurements of the velocity concentration of dispersed bubbles travelling close to the top of the
field around the bubbles, were developed and validated. pipe. However, for low Froude numbers the elongated bubbles also
An improvement introduced here is the estimation of individual travel close to the top of the pipe. Therefore, the sensor is not sen-
bubble velocity in real time, what allows for the utilization of an sitive to their passage when positioned at the centerline of the
automatic adaptive adjustment of time delays used to synchronize pipe. Thus, a good compromise between the detection of elongated
each bubble passage with image acquisitions. By this technique, bubbles and the noise reduction was found when the sensor was
bubbles travelling at different velocities could still be captured positioned at a height of 2/3 of the pipe diameter, as shown in
within the field of view of the camera. This feature can aid in the Fig. 2.
study of plug and slug flows in horizontal pipes, since in these The first two photo gates were used to measure the front and
flows instantaneous bubbles can display variations in their veloci- rear velocities of the bubbles, while a third gate provided a trigger
ties under the same nominal flow conditions. By the procedure signal to start a quartz based clock, properly adjusted according to
used in the present work, hundreds of bubble contours could be measured front or rear velocity. The clock was used to output sig-
ensemble averaged with increased efficiency, providing useful nals for synchronization for image acquisitions. For fast measure-
statistical information about the bubble characteristics. ments of the bubble front and rear velocities the output signals
of gates 1 and 2 were fed to an external XOR logic circuit, which
produced a single pulse of finite duration. The circuit provided a
Experiments high state logical level during the passage of the front or the rear
of the bubble through photo gates 1 and 2. This pulse width could
The experiments were performed in a horizontal pipe with be quickly and accurately measured at a rate of 20 MHz, using a
internal diameter (D) of 0.0508 m and length (L) of 23 m, yielding built-in function of a multifunction D/A board model AT-
a length-to-diameter ratio of approximately 450. A schematic view MIO-16X and Labview™ routines. The bubble front or rear velocity
of the apparatus is shown in Fig. 1. The test rig was built from was then calculated as the ratio of the distance between the photo
20 W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30

Fig. 1. Schematic diagram of the test section.

Fig. 2. Schematic assembly of photo gates.

gates 1 and 2 and the measured pulse duration. In order to identify pulses to the CMOS camera ordering it to capture 4 consecutive
the pulses related to each part of the bubbles it was necessary to images of bubble front or rear. The time interval between the
perform a logic AND operation using the XOR gate and the sensors acquisitions was adjusted in the synchronizer according to the flow
output signals. This logic operation with the signal from photo gate mixture velocities being studied. Intervals of 20 ms were set for
Sensor 1 enabled the identification of pulses related to the rear part cases with low mixture velocities (jm < 1.5 m/s), while 10–15 ms
of the bubble, while the pulses associated with the front could be were used for other cases. Also, the camera exposition had to be
identified by using the signal from Sensor 2. A high amount of adjusted according to the bubble speed in order to avoid image
dispersed bubbles close to the front part of the elongated bubble blurring. Downstream from the infrared gates, at the position of
was observed for high mixture velocities, causing high frequency the visualization box, an array of 176 white light LEDs was
oscillation in the output of the photo gates. In order to avoid such installed to provide back illumination for the images. The intensity
oscillations, the signals from the sensors were low-pass filtered of the light was controlled by an adjustable power supply. To
using a cut-off frequency of 250 Hz. achieve uniform illumination in the background of the images,
The length of a liquid slug was estimated by the product of mea- the light emitted by the LEDs was diffused by a sheet of white
sured bubble velocity (uB) and the time delay between two consec- paper.
utive pulses. Similarly, the length of unit cells could be estimated The synchronization process developed guaranteed that the
by multiplying uB and the time delay between two consecutive front or tail parts of the bubbles were exactly at the camera field
passages of the bubble rear part (Dt). The inverse of the delay Dt of view at the moment of image capture, even though each individ-
provided information about the frequency of the slugs. A detailed ual bubble travelled at different velocities. This feature allowed for
description of these equations can be found in the literature the capture of hundreds of bubble images that were later post-
(e.g. Polonsky et al., 1999). processed to produce an ensemble-averaged bubble image, as will
Due to the simplicity of the calculations performed, all param- be described shortly. Ensemble-averaged bubble images are useful
eters could be estimated in real time. Velocity information experimental information that can contribute to clarify the bubble
extracted from the infrared photo gate sensors was used in real behaviour.
time to provide a proper delay for synchronization of image The main characteristic of the present study is the analysis of
acquisitions with bubble passage. Thus, a proper delay for image the bubble features based on ensemble-averaged interfaces con-
acquisition could be estimated and set to the hardware counter structed from hundreds of instantaneous bubbles images. This
of the quartz based clock (20 MHz), before the bubble reached technique presents a significant advantage when compared to
the third photo gate. The signal generated by the bubble passage the widely used method of imaging a continuous interval of the
through the third photo gate was used to start the counter and, fluid flow employing high frame rate digital cameras. The continu-
immediately after finish counting, a high logic level signal was ous imaging of only a few seconds of the bubble and slug passage
set to a digital gate of the D/A board. This procedure provided an at high frame rates and reasonable spatial resolution rapidly fills
accurate and adaptive time delay for the image acquisitions, which the camera memory space of currently available cameras. Most
automatically compensated for slight variations in bubble veloci- of the images acquired in this operating mode are related to the
ties, thereby allowing that bubble front or rear images from differ- body of the bubbles, with only a few frames displaying the desired
ent bubbles were properly captured at the same position in front of bubble nose or tail images. For instance, in the present experi-
the camera field of view. ments the highest shedding frequency of slugs was slightly below
The delayed trigger was used to start the camera synchronizer. 0.5 Hz, while the lowest was close to 0.1 Hz. If one considers a typ-
At each trigger pulse, the synchronizer (model BNC-575) sent ical frequency of 0.25 Hz for a rough estimate, it can be concluded
W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30 21

that 1 Gbyte of data is necessary to record the passage of only 5 the bubble shapes. In cases with a high concentration of dispersed
slugs, when a camera of 1Mpixels is operated in continuous acqui- bubbles near the nose of the main bubble, an initial guess for the
sition, at a rate of 50 Hz. Using the triggered image acquisition pro- position of the nose tip was given by visual identification employ-
cedure employed in the present study, only images of bubble noses ing guided user interface (GUI) routines. This initial estimation of
or tails are stored in the camera memory, what makes it possible to the nose tip was used to crop the images. It facilitated the auto-
store hundreds of such images allowing for the computation of matic detection of the contour, which was performed afterwards.
ensemble-averaged contours and other flow statistics. By using Other efforts in the literature have faced the same difficulty in
the proposed acquisition procedure, only 40 Mbytes are required identifying bubble interfaces in highly aerated flows, (e.g. van
to record the information of 5 consecutive slugs. Thus, a clear Hout et al., 2002).
advantage of the method developed is the optimization of the cam- Standard pre-processing techniques, such as contrast enhance-
era memory and the reduced number of images used in the data ment, background subtraction and grey intensity normalization,
processing. The main drawback of the method is the lack of contin- were applied to each individual instantaneous cropped image, in
uous imaging of the flow, what does not allow for a complete order to remove any bias that could have been introduced by dif-
reconstruction of the slugs. ferences in illumination intensity (see Gonzales et al., 2009 for a
review of the standard image processing routines). The standard
Image processing of bubble nose and tail techniques for image processing are capable to precisely detect
the bubble interface in images having a low concentration of
The identification of bubble characteristics was performed dispersed bubbles, such as the one of Fig. 3(a). For the detection
using back-illuminated images, in a similar way as done previously of interfaces in images with a high concentration of dispersed
in the work of Polonsky et al. (1999), Mayor et al. (2007), and bubbles, such as the one exemplified in Fig. 3(b), a low-pass digital
Shemer et al. (2007). This is a simple, non-intrusive, optical tech- filter was applied to the images before the processing. Thereby, it
nique suitable for measuring liquid and gas interfaces. It relies on was possible to detect interfaces in the instantaneous images,
the acquisition of images with an intense and uniform background even in the presence of dispersed bubbles. For each flow rate, a
illumination that passes through the flow. At the interface, the set of approximately 400 instantaneous interfaces was determined,
light transmission is attenuated, creating a shadow on the acquired producing statistic features about bubble nose shape and position.
image. The ensemble-averaged interface shape was one of these features,
Prior to analysis of the images, a calibration procedure was per- and it was employed to yield all the results presented in the
formed in order to convert from pixels to actual flow dimensions. present study.
To this end, a semi-cylindrical target marked with an array of
spaced dots, was introduced into the pipe filled with water. After Uncertainty estimation of bubble interface determination
adjustment of the camera focus to the plane of the target, an image The image processing procedures just described for detecting
was acquired and the calibration factor extracted. The FEP pipes the instantaneous bubble interfaces are associated with uncer-
reduced the optical distortions induced by differences in the tainty levels that need to be estimated. The uncertainty on the
refraction indexes of water and the pipe. Thus a single calibration binary operations employed to detect the interface position at a
factor could be used for the complete area imaged by the camera. certain axial coordinate involve binarization of the original image
With the magnification selected for the measurements, a calibra- and open and close binary operations. Tests on samples of the com-
tion factor of 11 pixels/mm was obtained. Although the refractions plete acquired image sets indicate that open and close operations
indexes of the pipe and the fluid were similar, their light absorp- with an average of 10 iterations were necessary to properly iden-
tion coefficients were not the same. Therefore, the light was signif- tify the bubble interface. An uncertainty of 1 pixel was associated
icantly attenuated at locations very close to the top and the bottom with each of these iterations, totalling an uncertainty of 10 pixels
of the pipe, hence reducing the region of measurements in 10% of for the interface detection. The uncertainty level associated with
the diameter. This effect is expected to occur also for different the image binarization procedure was found to be typically of 1
materials and can be reduced by using transparent pipes with pixel, which can be considered negligible in face of the uncertainty
reduced wall thickness. Due to the inaccuracy of the results at such levels on the interface detection. For the detection of the ensem-
locations, the bubble contours presented in the present study are ble-averaged interfaces, a second source of uncertainty should be
shown within the limits of 5–95% of the pipe diameter. This is a considered. It originates from the random nature of the bubble
conservative limit and it was chosen to ensure that no influence shapes that constitutes the set of images employed in the determi-
of the illumination intensity at the bottom and top of the pipe nation of the ensemble-averaged interfaces. This uncertainty con-
would be present in the obtained results. tribution was estimated by the standard error, which is given by
The procedures developed for analysis of bubble nose and tail the standard deviation of the interface position at a particular axial
images differed due to the nature of these images, but shared the location, divided by the square root of the number of bubble image
same basic steps that will be outlined in the next subsections. All samples used. The final uncertainty level was estimated by the
the image processing routines and bubble feature extraction square root of the sum of the squares of the two uncertainty con-
routines were implemented using a Matlab platform. tributions (JCGM, 2008). The estimated uncertainty levels for the
results obtained in the present study are indicated in the figures
Bubble nose interface detection from instantaneous images as vertical bars.
The procedure used to extract the interfaces of individual
instantaneous bubble images was applied to hundreds of images Bubble nose velocity from image analysis
in order to allow the determination of statistically relevant infor- The velocity of the bubble nose was obtained using the dis-
mation about the bubble contours. Each image of the bubble nose placement of the bubble nose between two consecutive captured
was cropped into a size of approximately one-by-one pipe diame- images. Following the expressions given in the work of Polonsky
ter after the identification of the nose tip. The position of the bub- et al. (1999), the velocity could be estimated by Eq. (1), since the
ble nose tip was used to align all the instantaneous images. time interval between the images was known.
Although the image triggering guaranteed that all bubbles were
inside the camera field of view nearly at the same position, small 1 Ddimages
uB ¼ ð1Þ
shifts could be observed from image to image due to changes in c Dt images
22 W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30

Fig. 3. Example of images of bubble fronts for liquid superficial velocity jL = 0.2 m/s and gas superficial velocity jG = 0.7 m/s and jL = 0.2 m/s and jG = 1.9 m/s.

where c denotes the calibration factor (for the present work obtained from the ensemble-averaged image (dotted line). Cases
c = 11 pixels/mm), Ddimages and Dtimages denote, respectively, the with the same gas and liquid velocities as those from Fig. 3(a)
horizontal image displacement extracted from two consecutive and (b) are respectively analysed in Fig. 5(a) and (b). The bubble
images and the time interval between the images. interfaces were shifted by the nose tip position (xB) in order to
Fig. 4 presents a comparison of bubble velocities obtained from have all curves initiated at the same location. As can be seen,
image analysis against those measured with the aid of photo gates. the resulting contours obtained from both methods can be consid-
As can be seen in the figure, both techniques provided the same ered coincident, within the levels of experimental uncertainties
results within the expected experimental uncertainty levels. This expected and indicated by the vertical bars. It is conceivable that
good agreement suggests that no bias in the velocities was intro- under different flow conditions the two methodologies may pres-
duced by the measurement techniques employed. ent different results. However, it is important to emphasize that
no significant differences were observed for all cases investigated
Bubble interface detection from ensemble-averaged image in the present work. Bubble contours extracted from ensemble-
The processing of ensemble-averaged images for estimation of averaged images are shown only in this section, for a comparative
averaged liquid–gas interfaces can be an alternative to the method analysis against the ensemble-averaged contours obtained from
based on the processing of instantaneous images, just described. In instantaneous images descried before. As already mentioned, the
the averaged bubble image, the most frequent positions of the latter technique was employed to obtain the results that are
interfaces are reinforced and seen as black shadows. Due to the presented in the next sections of the present work.
random location of dispersed bubbles in the instantaneous images,
the averaging procedure was capable of effectively removing noise Bubble tail image analysis
induced by the presence of small bubbles, making the image The methodology used to process the images of the bubble tail
processing simpler. The binarization of the averaged image was shares similar steps with the processing adopted for the detection
performed using a fixed threshold criterion determined by the of interfaces in the bubble nose images. However, due to the
minimum value of grey intensity in the column of the image different characteristics of the images, specific steps had to be
corresponding to the nose position, which was detected during employed and the main differences are highlighted in this para-
pre-processing. Standard, close, open and fill operations were used graph. The images were cropped into a length of 1.4D, as illustrated
to smooth and close the main bubble interface. The processing was in Fig. 6. The cropping length was chosen according to the work of
extremely fast, and most of the computational time was spent in Fagundes Netto et al. (1999), where the hydraulic jumps presented
reading the images. The main drawback of this procedure is the lengths from 0.7D to 1.3D. The region upstream from the vertexes
great number of images necessary to remove noise when the of the hydraulic jump typically displays a quiet liquid layer. There-
slugs are highly aerated, and the loss of other valuable statistical fore this region was selected for the detection of the liquid film
features. Fig. 5(a) and (b) present a comparison of mean bubble thickness (hL), as depicted in Fig. 6.
nose interfaces obtained from the ensemble average of 400 instan- The vertexes detected in instantaneous interfaces were shifted
taneous bubble interfaces (dashed lines) with the interfaces to the image origin and a least-squares linear fit procedure through
all points of the interface was employed to determine the angle of
the hydraulic jump. The shifting of the interfaces was implemented
in order to reduce the influence of variations in the instantaneous
film thickness on the estimation of the angle of the hydraulic jump.
As demonstrated for the case of the bubble nose contours, the
detection of the bubble tail characteristics from ensemble-aver-
aged images provided similar results to those obtained from the
methodology based on the ensemble-averaged interface from
instantaneous images described in the above paragraph. However,
results from ensemble-averaged images were not used in the pres-
ent work since they do not yield statistical information about the
interfaces.

Results

Modelling of intermittent two phase flow has been investigated


by many research groups, as can be seen in the review paper of
Fabre and Liné (1992). Valuable databases about the statistics of
plug and slug flows are available in the literature for model valida-
Fig. 4. Comparison of bubble nose velocities measured by the photo gates and by tion, (e.g. Barnea, 1987; Nydal et al., 1992; Spedding and Spence,
the image processing techniques developed. 1993; Fossa et al., 2003; Woods et al., 2006). However, the results
W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30 23

Fig. 5. Comparison of bubble front contours obtained from ensemble-averaged images and from ensemble-averaged interfaces of instantaneous images for: (a) jL = 0.2 m/s
and jG = 0.7 m/s; (b) jL = 0.2 m/s and jG = 1.9 m/s.

environmental conditions. The validation of the test rig, including


the measurement techniques, was done by comparing the results
obtained with those from the literature.
The range of phase velocities investigated is illustrated in the
map of flow patterns shown in Fig. 7. The reference map was
extracted from the work of Mandhane et al. (1974), which is based
on several experimental results obtained under conditions similar
to those of the present investigation. The same symbol is used to
represent cases that share the same superficial liquid velocity.
The range studied covers the transition from elongated bubble to
slug regime, and it is located between cases of very long slugs,
Fig. 6. Example of image of bubble tail for liquid superficial velocity jL = 0.2 m/s and studied in the work of Kadri et al. (2009), and hydrodynamic slugs,
gas superficial velocity jG = 0.7 m/s.
investigated in Nydal et al. (1992). Although the range covers a gap
existing between these two works, it still enables a comparison
from different research groups are not always in close agreement. with those results.
According to Bendiksen and Malne (1987), the slug initiation can Following the concept of unit cell given by Dukler and Hubbard
be significantly affected by inlet and outlet configurations of test (1976), the slug flow can be seen as a sequence of similar slug
rigs and hence have influence on slug statistics. This effect is more units. At regions close to the onset of slugging, the slug units are
pronounced for short pipes. Therefore, long test rigs are often used
to enable the development of slugs. For instance, the works of
Wang et al. (2007) and Kadri et al. (2009) describe apparatus hav-
ing lengths longer than 2500 pipe diameters. Indeed, long lines
reduce significantly the influence of inlet conditions but, on the
other hand, are associated with higher costs, being their real need
justified only for the investigation of very long slugs. According to
Kadri et al. (2009), this regime occurs for very low gas velocities
that are lower than those covered by the present measurements.
For higher mixture velocities, lines with lengths ranging from
350 to 500D have been used with success. For instance, the work
of Nydal et al. (1992) provided statistical data about developed
slugs using a test rig with a length of 360D.

Preliminary assessment of the test section

In view of the sensitivity of slug development to the inlet con-


ditions, a series of preliminary tests was conducted to assess the
quality of the results obtained from the test rig constructed and
the experimental procedures developed. In particular, these preli-
minary tests were aimed at verifying that no bias was introduced
into the results due to inlet and outlet configurations, and also Fig. 7. Flow regime map indicating the experimental conditions tested. The base
map is extracted from Mandhane et al. (1974). The phase velocities covered in the
due to the curves installed along the test pipe. These curves present work are shown as symbols:: – jL = 0.2 m/s; – jL = 0.3 m/s; –
were installed to extend the pipe length while keeping the whole jL = 0.4 m/s; – jL = 0.5 m/s. Shaded areas correspond to ranges covered in the
set-up inside the available laboratory space with controlled works of Nydal et al. (1992) and Kadri et al. (2009).
24 W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30

The measured mean lengths of the liquid slugs (LS) are depicted
in Fig. 9(a). According to Nydal et al. (1992) and to Kadri et al.
(2009), both liquid and gas superficial velocities can affect the
length of the liquid slugs. Therefore, the mixture velocity was
chosen to scale the data in Fig. 9(a), because it includes both
velocities. For the range of flow velocities covered in the present
experiments, the scaling was fairly good. However, for larger range
of mixture velocities a scattering of the data can occur when using
the mixture velocity to scale the slug lengths. The data indicate a
change from long to short slug lengths for increasingly higher
mixture velocities (jm). For high mixture velocities, experimental
results asymptotically approach the lengths observed in Nydal
et al. (1992). On the other end, for low mixture velocities the mean
slug lengths were closer to those from the work of Kadri et al.
(2009). For slugs under development, the measured lengths would
be considerably shorter than those reported in the literature,
which is not the case here. A comparison between the regimes
measured in the present work with those reported in the work of
Kadri et al. (2009) is shown in Fig. 9(b). The symbols used in
Fig. 8. Comparison of translational velocities measured at the nose and tail of the
bubble. Fig. 9(a) and (b) represent the same cases. A reasonable agreement
is observed with the map given in the work of Kadri et al.
(2009). This suggests that the typical slugs lengths observed at
under development and may exhibit a different statistical behav- the measurement station location were of the order of those
iour from fully developed ones. According to Nydal et al. (1992) reported in the literature. Moreover, for mixture velocities lower
the existence of fully developed slug flow in pipes is a matter of than 1.5 m/s, the results show that small reductions in velocity
definition, as gas expansion due to pressure losses along the pipe may result in a remarkable increase in the length of the liquid
will cause an increase in the mixture velocity. However, they also slugs.
mention that after an initial stage of development, the slug units The shedding frequency of the slugs is a relevant parameter to
change slowly along the pipe and mostly depend on the local value characterize the intermittent flow regime. According to Nydal
of the gas velocity and gas expansion rather than on the previous et al. (1992), the frequency of non-developed slugs displays a prob-
history of the flow. At this stage, the translational velocities of ability density distribution with two peaks, with one of them hav-
the front and rear part of the bubble would be similar, as suggested ing a high frequency, which is not typical for slugs at a given flow
by Ruder et al. (1989). Therefore, the translational velocities of the rate. This can shift the mean shedding frequency toward higher
front and the rear parts of the bubble were compared to each other frequencies. The present results, depicted in Fig. 10, were com-
prior to the statistical analysis of the slug units. The results pre- pared against an empirical correlation proposed in the work of
sented in Fig. 8 shows that, within the experimental uncertainty Fossa et al. (2003) which was based on several different databases
levels, estimated according to the ISO guide for expression of reported in the literature. The correlation relates the dimensionless
uncertainties (JCGM, 2008), both velocities were close for most of slug frequency, given in terms of a Strouhal number (St = fsD/jG),
the collected points. However, a small systematic difference is with the ratio of superficial liquid to mixture velocities
verified in the velocities of the rear part of the bubble that are (kL = jL/jm). Experimental results extracted from the work of Wang
slightly lower than the front. This might be related either to the et al. (2007) for a pipe with approximately 2600D were also
gas expansion caused by pressure loss along the pipe or to the included in the figure as a second reference. The good agreement
growth of the liquid slugs. In order to have a clearer picture about of the present results with those from literature is an indication
this behaviour it is necessary to analyse other statistics of the flow. of the presence of developed slugs at the region of measurement,

Fig. 9. Comparison of measured slug length with literature results for long and hydrodynamic slugs. (a) Length of the liquid slugs against the mixture velocity, (b) map of
regimes extracted from the work of Kadri et al. (2009).
W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30 25

and suggests that the curves installed in the test section had no
influence on the slug statistics.
As already noted, the measured translational velocities of the
front and rear part of the slugs, shown in Fig. 8, displayed small
differences, suggesting that the slugs were still under develop-
ment at the streamwise location where the measurements were
carried out. However, the fact that the length and the intermit-
tency of slugs, depicted in Figs. 9 and 10, are in agreement with
those reported in the literature for well-developed slugs, is an
indication that the slugs are developed or nearly close to this
condition.
The preliminary tests conducted were considered satisfactory,
validating the test section constructed and the experimental proce-
dures developed. Results for slug velocity and bubble characteris-
tics will now be presented.

Bubble nose translation velocities

Fig. 10. Comparison of measured non-dimensional slug shedding frequencies with Bubble front translation velocity is an important parameter
data from the literature. for modelling intermittent two-phase flow. It is generally
accepted that the bubble velocity (uB) is a function of the mixture
velocity, jm, and drift velocity, ud (Bendiksen, 1984), as indicated
by Eq. (2),
uB ¼ Cjm þ ud ð2Þ
The coefficient C is, in general, a function of the Reynolds,
Froude, and Etvös numbers (Fabre and Liné, 1992). Several correla-
tions are found in the literature for the bubble velocity in horizon-
tal flows, and there is still not complete agreement with regard to
the contribution of the drift
pffiffiffiffiffiffivelocity for low values of the mixture
velocity, i.e., for jm < 3:5 gD, where g is the gravitational acceler-
ation. Bendiksen (1984) and Woods and Hanratty (1996) recog-
nized the importance of the drift velocity in predicting bubble
velocity, while other authors, as Cook and Behnia (1997) and van
Hout et al. (2002), do not recommend its utilization, proposing that
uB and jm be directly related by uB = 1.2jm Bendiksen (1984),
discusses the change in the coefficient C in Eq. (2), indicating that
its value reflects the competition between inertia and gravitational
forces which determines the radial position of the bubble nose and,
consequently, its velocity. For low values of the Froude number,
gravitational forces dominate and the bubble travels at a position
Fig. 11. Comparison of measured and predicted bubble nose velocity as a function closer to the upper part of the pipe. For higher values of Froude,
of mixture Froude numbers.
inertia forces dominate and the bubble is pushed toward the pipe

Fig. 12. Change in bubble nose shape and position with mixture Froude number.
26 W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30

uB ¼ 1:2jm ; for Frm > 3:5


pffiffiffiffiffiffi
where Frm ¼ jm = gD Woods and Hanratty (1996) introduced an
intermediate Froude number regime where inertia and gravita-
tional forces are comparable, proposing the following correlations
for bubble velocity,
pffiffiffiffiffiffi
uB ¼ 1:0jm þ 0:542 gD; for Fr m < 2
pffiffiffiffiffiffi
uB ¼ 1:1jm þ 0:542 gD; for 2 < Fr m < 3:5 ð4Þ
uB ¼ 1:2jm ; for Fr m > 3:5
Fig. 11 presents a comparison of bubble velocities measured in
the present study employing the optical techniques implemented,
with the predictions of the correlations presented in Eqs. (3) and
(4). Fig. 11 displays the comparisons of bubble velocities with
the mixture Froude number. For the range of mixture velocities
investigated in the present study, the results of Fig. 11 show that
both correlations approximate reasonably well the bubble velocity
Fig. 13. Measured bubble nose radial positions as a function of the mixture Froude data, with a better agreement observed for Woods and Hanratty
number. (1996). This correlation considers a change in the coefficient C
for an intermediate range of Froude numbers, or mixture velocities.
Also plotted in Fig. 11 is the correlation that does not consider
centerline. Based on these arguments, Bendiksen proposed a the effect of the drift velocity. As can be seen, comparison with
correlation that considers the low and high mixture Froude (Frm) experiments indicates that, for low values of the mixture velocity,
number ranges, the contribution of the drift velocity should not be neglected. In
pffiffiffiffiffiffi addition, the results clearly show the shift in bubble velocity at
uB ¼ 1:05jm þ 0:542 gD; for Frm < 3:5 ð3Þ Froude number equal to 2, as proposed by Woods & Hanratty.

Fig. 14. Measured ensemble-averaged bubble shapes for different mixture velocities.
W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30 27

Fig. 15. Comparison between measured bubble shapes and prediction by Benjamin’s (1968) inviscid theory for jL = 0.2 m/s and jG = 0.18 m/s (a). Images (b) and (c) are
examples of instantaneous bubbles used to compute the ensemble averaged contour.

Bubble nose radial position number, for the range of parameters investigated. The results of
Fig. 13 confirm quantitatively, seemingly for the first time, the
The change in the radial position of the bubble nose tip reflects qualitative observations of Bendiksen (1984) and Ruder and
the relative importance of gravitational and inertia effects. As the Hanratty (1990).
Froude number increases, inertia effects dominate and the bubble
nose position tends to move to the pipe centerline. Also, the shapes
of the bubbles tend to become narrower as Froude increases, with Bubble nose shape
an impact on bubble velocity.
Fig. 12 was prepared to demonstrate quantitatively the qualita- Ensemble-averaged bubble nose shapes obtained in the present
tive observations of the previous paragraph, and that were first work, as those presented in Fig. 12, allows for an analysis of
mentioned in Bendiksen’s work. Fig. 12(a) is a reproduction of the influence of liquid and gas superficial velocities on the bub-
Fig. 11 without some of the experimental data in order to avoid ble shapes. Fig. 14 was prepared to facilitate the analysis. Each
overcrowding the figure. Fig. 12(b) presents bubble nose shapes figure corresponds to nose shapes measured for a fixed value of
corresponding to the same mixture Froude number as those repre- the mixture velocity. For the lowest value of mixture velocity
sented in Fig. 12(a). The symbols plotted on the bubble shapes of studied, jm = 1.2 m/s, the results of Fig. 14(a) indicate that the
Fig. 12(b) are related to those in Fig. 12(a). The bubble shapes bubble shapes are quite similar, having a nose position located at
presented in Fig. 12(b) were obtained by the optical techniques y=D ffi 0:75. As shown in Fig. 14(b)–(d), for increasingly higher
described previously, with each bubble contour representing an velocities the bubbles display different shapes for different mixture
average of 400 instantaneous bubble contours. A careful observa- velocities, becoming narrower. Narrowest shapes are found in
tion on the results displayed in Fig. 12 demonstrate quantitatively Fig. 14(d). However, for the same mixture velocity the shapes are
the radial motion of the bubble nose tip toward the centre of the nearly the same in all cases analysed. This observation can be ver-
pipe for increasing values of the mixture Froude number. For the ified by comparing bubble shapes represented by dashed and dot-
lowest values of Froude investigated, Frm = 1.28, the bubble nose ted lines. As indicated in the figure, similar shapes are observed for
tip is located at y ffi 0:75D, while for Froude equal to 2.98, this the same mixture velocity, although these mixture velocities were
position moves downward to y ffi 0:6D. In the reference frame obtained from different combinations of gas and liquid superficial
employed, y = 0D is at the lower wall of the horizontal pipe. Thus, velocities.
y = 0.5D is at the pipe centerline. It is interesting to relate the bubble shapes presented in Fig. 14
Fig. 13 displays the bubble nose position (yB) versus mixture with the corresponding points in the flow map of Mandhane
Froude number measured for all tests conducted in the present shown in Fig. 7. The fat bubbles of Fig. 14(a) fall in the elongated
work. The ordinate indicates the vertical bubble nose position bubble regime, while the thinner shapes of (b), (c) and (d) fall in
measured from the lower pipe surface and made dimensionless the slug regime. According to the experimental findings, the nose
by the pipe diameter. This figure indicates a nearly perfect linear shapes are linked to the translational velocities, which are basically
relationship between bubble nose position and mixture Froude a function of the mixture Froude number (see Eqs. (3) and (4)).
28 W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30

of ensemble-averaged bubble noses that allow for a better compar-


ison with Benjamin’s potential theory. Fig. 15 presents this
comparison, where 300 instantaneous images of elongated bubbles
were ensemble averaged for a liquid superficial velocity of 0.2 m/s
and a gas superficial velocity of 0.18 m/s. The bubble shapes pre-
dicted by Benjamin’s theory are overlaid on the average contour
in Fig. 15(a). A low level of agreement can be verified, indicating
that the potential theory does not predict accurately the behaviour
of the bubble, even for this case where the Froude number is equal
to 0.45, which is certainly lower than the Froude numbers where
slug flow regime is expected to prevail. Major differences are found
around the tip of the bubble nose. Fig. 15(b) and (c) represent dif-
ferent samples of instantaneous images obtained under this exper-
imental condition. It can be seen that one of the instantaneous
bubbles is well represented by the shape given by Benjamin’s the-
ory, as depicted in Fig. 15(b). However, shapes like this are a minor
part of the total set of acquired images. Most images are similar to
that of Fig. 15(c), in which bubble contours are rather different
Fig. 16. Variation of the liquid film thickness with the liquid volume fraction (kL). from the theoretical predictions. These results suggest that Benja-
min’s solution might be valid for extremely low mixture velocities,
which in practice do not correspond to slug regimes. Tests at even
Ruder and Hanratty (1990) and Woods and Hanratty (1996), lower mixture velocities could not be performed in the present
observed good agreement between their experiments and the study since the required flow rates were below the values where
potential theory of Benjamin (1968), for the elongated bubble stable conditions could be sustained in the test section available.
regime. Their conclusions on the agreement between experiments
and theory were based not on full images of the bubble nose, but Bubble tail shape
on measurements of average liquid film by conductive probes
and on the visual observation of the bubble nose position near The work of Fagundes Netto et al. (1999), pointed out for
the pipe top surface. The present work provides complete images changes in the bubble tail during transition from the elongated

Fig. 17. Measured ensemble-averaged hydraulic jumps for different mixture velocities.
W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30 29

Fig. 18. Comparison of ensemble-averaged hydraulic jumps with the model proposed by Fagundes Netto et al. (1999).

bubble to the slug flow regime. According to their work, a measure predictions given by the model are compared against the results
of the bubble tail shape could be used as a criterion for the transi- of the present study, and are presented in Fig. 18. Due to constrains
tion between those regimes. In the present work, ensemble- in the model, which is not valid for both low liquid velocities and
averaged bubble tail shapes were obtained and measured accord- very high mixture velocities, only cases having liquid velocities
ing to the procedures described previously in Section ‘Image above 0.5 m/s are analyzed. Moreover, the length of the hydraulic
processing of bubble nose and tail’. There, the bubble tail shape jump in the model is fixed and assumed to be equal to 1D.
was characterized by the angle of the hydraulic jump and the Fig. 18(a) and (b) shows good agreement for the angle of the
liquid film thickness, hL. hydraulic jump and an excellent match for the liquid film thick-
The analysis of the liquid film thickness has been performed ness. These results suggest that the model proposed by Fagundes
separately from the analysis of the hydraulic jump, because they Netto et al. (1999), is potentially capable of predicting the behav-
seem to be governed by different parameters of the flow. iour of the bubble tail. However, a more detailed investigation
The variation in the liquid film thickness with the ratio of the for a wider range of liquid velocities is necessary.
superficial liquid velocity to the mixture velocity (kL) is presented
in Fig. 16. A linear relationship of the film thickness with kL is
observed. A least squares fit to the data is also plotted in the figure Conclusions
as a reference. The results suggest that, indeed, the film thickness is
governed by the contribution of the liquid velocity to the total mix- In the present work digital processing of back-illuminated
ture velocity. bubble images in an intermittent flow regime of air and water in
Fig. 17 presents shapes of hydraulic jumps for fixed values of a horizontal pipe were employed to study the transition from elon-
mixture velocities, obtained using the procedures described in gated bubble to slug flow regimes. Original quantitative informa-
Section ‘Image processing of bubble nose and tail’. The lengths of tion about shapes of the bubble nose and tail could be obtained
the bubbles associated with the hydraulic jumps were not the by using a set of procedures for image acquisition and processing.
same for the various cases shown in this figure. Therefore, the For image acquisition, a set of photo gates was used to measure in
horizontal positions of the curves representing the tails were real time the velocity and the properties of the slugs. Based on the
shifted by the vertex position (xR) in order to have all hydraulic measured velocities, an adaptive delay could be adjusted in real
jumps initiated at the same location. Also, the liquid film thickness time to trigger image acquisition with the passage of each bubble.
was subtracted from the curves in order to facilitate the compari- Thus, hundreds of images from the bubble nose and tail could
son among the angles. As can be seen in Fig. 17, for the range of be captured and ensemble averaged. The detection of the bubble
mixture velocities investigated, the angles of the hydraulic jumps shape was performed on the instantaneous images and then
for cases with different gas and liquid velocities, but with the same ensemble averaged. An alternative methodology to process the
mixture velocity, are in excellent agreement. In all cases, the small images, based on ensemble averaged images, was also proposed.
deviations observed are well within the experimental uncertainty The results were validated against the ensemble averaged inter-
levels expected for the experiments, giving support to the idea of faces. It was observed that within the experimental uncertainty
the dependency of the shape of hydraulic jumps on the flow mix- both results are equivalent. However, the method based on the
ture velocity. It is interesting also to note a steepening of the angles ensemble averaged image does not provide statistical information
for higher mixture velocities. According to Mandhane’s map, the about the bubble interfaces and therefore it was not used to obtain
case with the lowest velocity shown in Fig. 17 falls within the plug the results presented in this work.
flow regime, while the others fall in the slug flow regime. Fagundes The results have shown that bubble translational velocities are
Netto et al. (1999), suggested that a steepening of the angle of the dependent on the mixture Froude number, with rates close to
hydraulic jump could be associated with a transition from plug to those suggested by Woods and Hanratty (1996). This has evi-
slug flow regimes. This angle variation was indeed observed in the denced the importance of the contribution of the drift velocity
experiments but, the differences were within the estimated uncer- to the bubble translational velocity for low mixture velocities, as
tainty levels, what did not allow the confirmation of their proposi- suggested in Bendiksen (1984).
tion. Further investigation is necessary to clarify this possibility. The radial movement of the bubble nose toward the pipe
In the work of Fagundes Netto et al. (1999), a one-dimensional centerline as function of the mixture velocity was measured quan-
model was proposed for predicting bubble characteristics. The titatively, seemingly for the first time. The results indicated a linear
30 W.R. de Oliveira et al. / International Journal of Multiphase Flow 69 (2015) 18–30

dependence between bubble nose position and the mixture Froude Gonzales, R.C., Woods, R.E., Eddins, S.L., 2009. Digital Image Processing Using
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extended to the Brazilian Government agencies CAPES and CNPq Pinto, A.M.F.R., Pinheiro, M.N.C., Campos, J.B.L.M., 2001. On the interaction of Taylor
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