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SECTION TOC
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 1 of 3
PROCESS MANUAL
TABLE OF CONTENTS DATE 07-95
1.0 INTRODUCTION
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PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 2
PROCESS MANUAL
TABLE OF CONTENTS 07-95
1.0 INTRODUCTION
This manual, which deals mainly with flow of fluids through circular pipe, is divided into two
books. This first book provides design methods and guidelines for sizing and specifying piping
systems. Included are sections on single-phase flow, two and three-phase flow, non-Newtonian
flow, liquid-solid slurries and pneumatic conveying. In addition, general hydraulic charts are
provided along with sample calculations and a listing of Fluor Daniel's hydraulic computer
programs.
The second book provides background information and includes sections on fluid flow
parameters and the development of equations and correlations for single-phase and two-phase
flow.
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PROCESS MANUAL PIPE SIZING AND SPECIFICATION
GUIDELINES DATE 07-95
1.0
1.0
It is the responsibility of the Process Engineer to specify the diameter of all pipes in a
process unit. Consideration must be given to pressure drop, to maximum permissible
velocity from the standpoint of erosion and noise, and to economics (when a fluid is
compressed or pumped). The pipe must be sized to ensure that the total system
pressure drop (including pressure drop due to control valves, equipment, etc.) does not
exceed the available pressure drop.
In most instances the Process Engineer will summarize pipe sizing information on a Line
Sizing Calculation Sheet (Form E-701), which is provided as Figures 2-1(a) and 2-1(b)
(metric form).
The frictional pressure drop for single-phase and two-phase systems should be
calculated using the methods described in this manual. It is recommended that
the computer programs described in Section 9 be used for this purpose. For
preliminary line sizing with single phase flow, the Darcy equation in Section 3 or
the generalized charts may be used. There are many instances where hand
calculations or the generalized charts are adequate, such as for study work.
However, for detail design engineering, or for systems that have high velocities
and/or large pressure drops with compressible fluids, these charts should not be
used. Table 2-1 presents recommended pressure drop limits for various liquid
and gas systems. These limits are somewhat arbitrary and are intended as
guidelines only.
Every calculated line size must be checked to ensure the resulting velocity is
reasonable. If a line size is not governed by pressure drop availability or
economics, then velocity limits are usually the deciding factor. Table 2-1
contains recommended velocity limits for various liquid and gas systems. The
velocity limits presented can be quite arbitrary and are intended as guidelines
only. In addition to these guidelines, other velocity limitations -- erosional
velocity, sonic velocity, entrainment velocity and noise -- must be considered
when sizing lines.
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Table 2-1
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a. Erosional Velocity
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b. Sonic Velocity
Sonic flow can also occur in liquids, but is less common because of the
higher sonic velocity in liquids. In addition, sonic velocity can occur in
any constricted area in a piping system. For example, if the
cross-sectional area of a fitting within a system is appreciably less than
that of the line, sonic velocity may occur at that constriction.
c. Noise
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PROCESS MANUAL PIPE SIZING AND SPECIFICATION
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Long lines that transport fluids which are pumped or compressed should be sized
on an economic basis. Perry's Chemical Engineer's Handbook (6th Edition, pp.
5-34) provides an excellent discussion, with several references, on this topic. An
economic study is usually not worthwhile for pipes of short length (e.g., pipes
within a unit boundary), since there is no sharp optimum in the selection of pipe
diameter for these systems.
Long pipelines
Cooling water headers
Alloy pipe
Special pipe (e.g., refractory-lined pipe)
The minimum acceptable line size is 3/4" unless the client allows a smaller size.
Line sizes of 1¼", 3½", 5", 7", and 9" shall not be used. Many clients want a
minimum size of 2" on pipe racks. Also, some clients do not allow the use of 2½"
or 14" piping.
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PROCESS MANUAL PIPE SIZING AND SPECIFICATION
GUIDELINES DATE 07-95
Early in project execution after sales award numerous project specific topics are
addressed and formally documented in the form of a Design Criteria. Other
details unforeseen at this time are developed as the project progresses.
Contributions are made by clients, licensors, equipment suppliers and Fluor
Daniel. Sufficient detail is developed to be built into the design to assure stable
operation of process units over the full range of anticipated operating conditions.
Such conditions include, but are not limited to, SOR, EOR, turn-down, feed and
product composition variations, utilities and other emergency operations, catalyst
conditioning/regeneration, heat exchanger cleaning, etc. Conflict of interest must
be addressed to assure a reasonable compromise between operating flexibility
and capital/operating costs.
Tables 2-2 and 2-3 provide pipe dimensions for the various schedule pipes,
Figure 2-21,2 provides friction factors as a function of Reynolds Number and
relative roughness of the pipe. Figure 2-3 and Table 2-4 contain relative
roughness factors and absolute roughness (rugosity) for various pipe materials.
1
See Cameron Hydraulic Data for large diameter pipes.
2
Figure 2-2 is Figure IIIA-3 in Hydraulic Institute Engineering Data Book, 2nd Edition 1990.
Figures IIIA-1 and -2 are for Asphalt-Dipped Cast Iron Pipe and Steel or Wrought Iron Pipe, respectively.
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Figure 2-3
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Table 2-2
PIPE DIMENSIONS
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Table 2-3
PIPE DIMENSIONS
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PIPE DIMENSIONS
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PIPE DIMENSIONS
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Table 2-4
CONCRETE PIPE
ε, ft
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PROCESS MANUAL PIPE SIZING AND SPECIFICATION
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Special care must be taken when sizing relief valve inlet and outlet
piping. Refer to the Fluor Daniel Relief and Flare, Process Offsites
Manual, Volume No. 48 for a detailed discussion on this subject.
b. Vessel Drawoff
The vortex that is formed when liquid is drawn out of the bottom of a
vessel that contains liquid and vapor in equilibrium or a two-phase liquid
mixture can cause entrapment of the vapor or the lighter liquid in the
liquid draw. In general, vortexing occurs when the static head above a
liquid drawoff nozzle is less than two velocity heads. For example, if a
column drawoff line has a velocity of 8 ft/sec (2.4 m/sec), vortexing will
usually occur when the liquid-gas or liquid-liquid interface is 2 ft or less
from the bottom of the drawoff nozzle.
The nozzle and line used to withdraw a stream from the side of a
fractionating column should be sized for a maximum velocity according
to Table 2-5.
Table 2-5
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This limitation is set to prevent trapped vapors from getting into the
pump. From a point 10 ft (3 m) below the drawoff nozzle, the line can be
reduced to its regular size.
Table 2-6 provides recommended line sizes for various steam flow rates
to exhaust heads.
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Table 2-6(a)
Notes:
(a) Swartout's basis for sizing
f. Boiler Blowdown
The information presented in the previous section is used as a guide for completing the
line sizing part of the Line Sizing Calculation Sheet (refer to Figure 2-1 in the previous
section). This section presents information required to complete the line specification
design data portion of Figure 2-1. This data includes the operating and design pressure,
operating and design temperature, insulation requirements, and a description of
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the flowing fluid. This information is used by the Piping Design Group to accomplish the
following:
Select the proper material and flange and valve rating (after a first pass by
process/metallurgist in materials review).
Select the proper pipe schedule, either from the piping material specifications or
by computation.
Calculate the necessary flexibility required in the piping layout to handle thermal
expansion.
Fluor Daniel's Piping Engineering Master Specifications are listed in Table 2-7. These
standards conform to the Chemical Plant and Petroleum Refining Piping Code
(ASME B31.3). Client specifications or supplements to this design criteria, when
submitted to Fluor Daniel, shall take precedence over this information.
The operating scenario which requires the highest design temperature may not
coincide with the one that requires the highest design pressure. For example, a
unit may operate normally at low temperature and high pressure but, during
regeneration, may operate at high temperature and low pressure. It would be
incorrect to design for the highest temperature and pressure as these two
conditions will not coincide. These two individual operating scenarios must be
considered separately and must be listed on the Line Sizing Calculation Sheet,
since either or both may govern the piping design. In addition, the scenario that
includes the highest design temperature should always be listed, even if it does
not include the highest design pressure, because it may determine the thermal
expansion stresses on the piping.
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Table 2-7
DESIGN AND
FABRICATION
SPECIFICATIONS
PIPING
MATERIAL
SPECIFICATIONS
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000.250.86210: Painting
000.250.86310: Coating and Wrapping of Steel Piping
000.250.50200: Piping Flexibility
000.250.50201: Piping Support Elements
000.250.50202: Metallic Expansion Joints
000.250.50203: Elastomer Expansion Joints
000.250.50204: Shock Arrestors
RELATED
INTERDISCIPLINE
SPECIFICATIONS
If the system does not contain a relief valve, or if the system can
be isolated from the relief valve, the maximum pressure that
upstream equipment can generate (e.g., the shut-in discharge
pressure of a centrifugal pump, the stalling pressure of a
reciprocating pump, etc.).
The design pressure of a line must be carried through to the last valve
which can be used to shut-in the system.
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The design pressure of the line and equipment on the discharge side of a
centrifugal pump should be selected from one of the following two cases,
on the basis that either the suction is subject to excess pressure or the
discharge is shut-in, but not both:
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d. Pulsating Service
e. Thermal Expansion
For piping systems that can experience vacuum conditions, the external
design pressure is set as the maximum difference in pressure between
the atmosphere and the inside of piping. The cooling of a gas or vapor
in a piping system that is normally pressurized may reduce the pressure
sufficiently to create an internal vacuum. In such a case, the piping shall
be capable of withstanding the external pressure at the lower
temperature, or a vacuum-breaking device must be installed. Large
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For lines that are subject to steam-out, use 250 oF (121 oC) as
the maximum design temperature minimum.
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Flashing liquids across valves: The MDT for the valve and
downstream piping must be adequate for the resulting low
temperature.
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Once the MDT has been defined the Piping Materials Group shall be
responsible to select the proper materials for the specified MDT.
Process Engineers shall assist in this effort because a balance must be
made between capital costs, engineering design efforts and possible
start-up and shutdown operating limitations.
c. Economics
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d. Internal Insulation
a. Short-Term Conditions
ASME B31.3 allows a design pressure that is higher than that normally
permitted for a specific piping component to be used if it only occurs for
a limited period. According to Section F of B31.3, when the increased
operating conditions do not exceed 10 hours at any one time and occur
no more than 100 hours per year, the pressure rating or the
pressure/stress value for piping may be increased by no more than 33 %
at the temperature of the increased condition. This condition is identified
on the Line Sizing Calculation Sheet (Figures 2-1(a) and 2-1(b)) as
Case II.
B31.3 also states that when the variation lasts no more than 50 hours at
any one time and no more than 500 hours per year, the pressure rating
or the pressure/stress value for piping may be increased by no more
than 20 % at the temperature of the increased condition. This is
identified as Case III on the Line Sizing Calculation Sheet.
In order to rate piping valves using Case II or III, written permission must
be obtained from the valve manufacturer. Also, be aware that these
cases are not allowed in some countries. Application of these short-term
condition cases may yield cost savings due to the use of flanged
equipment having a lower rating. In reality, however, their application is
somewhat limited. With equipment setting the design conditions in a
large number of instances for piping, even for short-term conditions, a
conservative pipe design temperature and pressure is usually
considered. Examples of Case II and III conditions were provided in
abandoned Fluor Daniel Engineering Standard ST-1-5002. ASME B31.3
is primary reference.
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with the result that the temperature of this valve would be lower than the
more severe service condition, then this valve may be rated for the most
severe coexistent temperature/pressure condition to which it will be
actually subjected in normal operation. This temperature will lie
somewhere between the more severe service temperature and the less
severe temperature of the joining line.
When completing the Line Sizing Calculation Sheet (Figures 2-1(a) and
2-1(b)), the Process Engineer must designate the type of insulation or
heat tracing which is required. This designation is usually made by using
one of the following symbols:
The Insulation Group will select the insulation type and thickness from
the specified operating temperature. Design temperatures are not used
for selecting insulation, except where they dictate the mechanical
characteristics of the insulation.
The Piping Stress Group is responsible for ensuring that the design of
piping systems has sufficient flexibility to prevent thermal expansion from
causing either failure of piping or anchors, leakage at joints, or excessive
thrusts and moments on connected equipment, such as pumps or
turbines. The thermal expansion values used in computing piping stress
are based on the maximum and minimum metal temperatures normally
expected during operation or shutdown. For the maximum metal
temperature, the Piping Stress Group uses the operating temperature at
flowing conditions. Therefore, it is important that all of the various
operating condition cases be listed on the Line Sizing Calculation Sheet,
particularly those where the operating temperature may be greater than
the normal operating case. The minimum metal temperature that is used
for stress calculations is 250 oF (121 oC) for onsite or on-plot refinery
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piping that is subject to steam out operations. For all other lines,
including those in a tank farm, the minimum metal temperature is 180 oF
(82 oC) for evaluating piping clearances and 150 oF (65 oC) for analyzing
piping flexibility.
The flowing fluid specific gravity, as listed on the Line Sizing Calculation
Sheet, is also used by the Piping Group to design pipe hangers and
supports.
a. Pipe Classification
Identifier 1 Identifier 2
Business Sectors Pressure Rating
B-Biotech
C-Process Identifier 3
D-Pharmaceuticals Material
F-Food
G-Government Identifier 4
H-Hydrocarbons Modifiers
I-Industrial
P-Power Note that Commodity Code is part of
S-Steel Mills Line Numbering System.
U-Utilities
W-Pulp and Paper
b. Line Identification3
All process and utility lines are numbered on the P&ID's and utility flow
diagrams by the Piping Materials Group, primarily to aid in spooling pipe
runs. The Fluor Daniel line identification normally consists of the
following five parts:
3
Piping Engineering, Material Engineering - Line Identification and Line Numbering,
Practice 000 250 3705.
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All lines in a plant are itemized on a Pipe Line List prepared by the Piping
Materials Group. The lines are listed in numerical order with the
following information given for each line:
The line list is a key document for other groups, including Piping
Materials, Piping Layout, Piping Stress, and Construction. The line list
facilitates working between the P&ID's and the pipe spool drawings.
The Piping Design Group is responsible for the layout of all equipment and
piping. The piping and equipment layout must satisfy requirements of:
Economics
Thermal stress
Accessibility (both for operating and maintenance)
Safety
Process
Special layout requirements (e.g., do not pocket)5
The Process Engineer should work closely with the piping designers, especially
in the early stages of layout work, to ensure mutual understanding of process
and layout requirements and limitations.
4
Piping Engineering, Material Engineering - Control and Issue of Line Lists,
Practice 000 250 0822.
5
See superseded Process Manual Volume V Flow of Fluids, Section A General Discussion,
page 25 for other special conditions.
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GPSA Engineering Data Book, Volume II, Section 17 - Fluid Flow and
Piping, Figure 17-26 - Design Properties and Allowable Working
Pressure for Piping.
A conference should be held at the start of the job between the lead Control Systems
engineer and all Process Engineers involved in sizing valves or in providing data, to
confirm the guidelines presented here or to explain any departures therefrom that may be
requested by the client.
Pressure drop allowance for control valves is specified by the process engineer. If the
allowance does not meet the requirements outlined here, check with the Control Systems
Engineer.
Sufficient pressure drop must be allowed for control valves to obtain good regulation,
maintain flow characteristics, and obtain desired maximum capacity. It is important that
a valve pressure drop allowance be made in specifying pumps, blowers, compressors
and reboilers. The following minimum control valve pressure drops are for normal
applications and standard types of valves. A check should be made for hydrostatic head.
It should not be included in the variable system pressure drop unless it varies (which may
occur in storage tanks), keeping in mind the relative rate of response of the valve to the
rate of head change in the tank.
At normal design rate (which is the normal flow rate or the rate required at nominal plant
throughput, or the material balance flow rate), allow a pressure drop across the valve
equal to one-half of the variable system pressure drop exclusive of the control valve; in
other words, one-third of the total variable system drop including the control valve.
On light hydrocarbon products to storage that are stored under product vapor pressure,
use a valve pressure drop based on downstream vapor pressure at maximum ambient
temperature of, say, 120 oF (49 oC).
For control valves at the discharge of reflux, charge and recycle pumps, use whichever of
the following four pressure drops is greater:
a. At normal design rate, one-third of the total variable system pressure drop.
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c. At maximum design rate (the rated flow on the pump data sheet, which is
10-25 % more than the normal flow rate), 20 % of the total variable system drop.
Limitations c. and d. are required to make sure there is enough pressure drop built into
the pump head for the control valve to operate at the maximum design rate.
For control valves in the steam line to reboilers, allow a pressure drop of 5 % to 10 % of
the initial absolute steam pressure or, when operating with low pressure steam of 30 psig
(2.0 barg) or less, use a minimum drop of 5 psi (0.34 bar). (Note that this drop must also
be considered when specifying the reboiler.)
The same criteria apply to vapors and gases other than steam.
If 5 psi is not available (which may be the case in low pressure gaseous systems),
consult with the Control Systems Engineer to determine mutually satisfactory conditions.
Gas streams can be controlled properly with less valve pressure drop than is required for
liquids. However, a limit may exist below which proper control cannot be realized with
commonly used control valve types.
For large variable system pressure drops of 150 psi (10.3 bar) or more, such as may be
encountered with heaters or furnaces, allow 15 % of the variable system pressure drop
exclusive of the control valve.
For automatic pump start-up where the control valve is in the steam line to the pump
driver, the control valve shall be line size. The resulting pressure drop generally should
be 5 psi (0.34 bar) or less.
Despite these guidelines, expensive loops may warrant a separate economic study of
capital and operating costs for pump and driver, piping, control valve and control valve
manifold.
Block and bypass valves shall normally be sized by a Control Systems Engineer.
Formerly sized by abandoned Engineering Standard ST-4-5084A Control Manifold
Arrangement and Layout Guide. Client may stipulate design basis. Most current
standard is Instrument Piping - Control Manifold Arrangement and Layout Guide -
Practice 000 250 2701.
When filling out control valve data sheets, the value for "P Sizing" is the drop across the
control valve only. The drop across the remainder of the control manifold (block valves,
swages, elbows, etc.) should be included in line losses. Also, remember start-up
conditions, especially for the "Pressure Maximum In".
Note that at times there is insufficient straight run pipe upstream of control valve orifices
and that installation of straightening vanes may be used to alleviate this situation in lieu
of repiping for a suitable straight run. See Control Systems for more detail.
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PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 1 of 11
PROCESS MANUAL
SINGLE-PHASE FLOW DATE 07-95
1.0
1.0
2.0
The hydraulic programs used at Fluor Daniel compute pressure drop from the Bernoulli
equation. For quick calculations of frictional pressure drop in liquid systems, the Darcy
equation may be used:
fρv 2 L
∆P = .001294 (English)
d
fρv 2 L
∆P = .0001967 (Metric)
d
where:
This formula does not include a safety margin and the calculated pressure drop should
be multiplied by 1.2 when determining line sizes.
The Darcy equation is valid for laminar or turbulent flow of any liquid in a pipe. However,
when extreme velocities occur in a pipe and cause the downstream pressure to fall to the
vapor pressure of the liquid, cavitation occurs and the results will not be accurate. The
Crane Technical Paper No. 410 presents several versions of the Darcy formula using
different flow rate parameters (gpm, lb/hr, ft3/sec, etc.).
A sample calculation using the above equation is provided in Section 11. The hydraulic
charts shown in Figures 3-1, 3-2 and 3-3 are also available and are very useful for
estimating frictional pressure drop and line sizes in liquid systems for Schedule 40 pipe.
Examples are provided with the charts. These liquid flow charts include a 20 % safety
margin. Additional charts providing correction factors for friction losses of different
schedule pipes and for various pipe materials are shown in Figures 3-4 and 3-5.
In Book 2 of this manual, friction factor and velocity of flow are discussed in Section 2
and the derivation of the Darcy equation from Bernoulli's equation is presented in
Section 3. Also discussed in Section 3 are pressure drop calculations that involve pipe
fittings and elevation changes.
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1.0
For incompressible fluids, the changes in fluid density and kinetic energy are negligible
and pressure drop is easily and accurately solved using the Darcy equation.
Compressible flow, however, is often accompanied by changes in kinetic energy and fluid
density. The hydraulic programs at Fluor Daniel compute pressure drop for gas flow
from the isothermal equation (discussed in Section 3 in Book 2).
For hand calculations, the Darcy equation can be extended to gases under limited
conditions. If the calculated pressure drop is less than 10 % of the inlet pressure,
reasonable accuracy is obtained if the gas density used in the formula is based upon
either the upstream or downstream conditions. If the calculated pressure drop is greater
than 10 %, but less than 40 % of the inlet pressure, the Darcy equation may be used with
reasonable accuracy by using a gas density based on the average of upstream and
downstream conditions. For pressure drops greater than 40 % of the inlet pressure,
break the line up into segments or use the isothermal flow equation.
A sample calculation using the Darcy formula for gas flow is provided in Section 11. As
mentioned previously for liquid flow, the Darcy equation in Section 3.1 does not include a
safety margin and the calculated pressure drop should be multiplied by 1.2 when
determining line sizes (except for steam). The hydraulic charts in Figures 3-6 and 3-7
are also available for estimating frictional pressure drop and line sizes for gas flow for
Schedule 40 pipe. Examples are provided with the charts. These gas flow charts
include a 20 % safety margin (except for steam). The correction factors for pipe
schedule and material are provided in Figures 3-4 and 3-5.
Section 3 in Book 2 of this manual presents equations for compressible isothermal flow
and sonic velocity. In addition, the Crane Technical Paper No. 410 provides a thorough
write-up on the principles of compressible flow.
Special charts for sizing steam lines are provided in Figures 3-8 and 3-9 for Schedule 40,
80 and 160 pipes. These charts permit rapid determination of frictional pressure loss and
linear velocity. Examples are provided with the charts.
The frictional pressure drop for steam systems is calculated in accordance with the
Standards of the Hydraulic Institute, on the basis of clean commercial pipe. Therefore,
no safety margin is provided in the charts for steam flow. Correction factors for pipe
schedule and material are provided in Figures 3-4 and 3-5.
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SECTION 4.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 1 of 6
PROCESS MANUAL
TWO-PHASE (GAS-LIQUID) FLOW DATE 07-95
1.0
1.0
2.0
3.0
4.1 INTRODUCTION
Two-phase (gas-liquid) flow has been the subject of a great deal of experimentation, and
is a very important consideration in the design of process plant piping. It is most often
encountered in vacuum transfer lines, reboiler return lines, and condenser outlet lines,
and may occur in relief and flare lines.
If two-phase flow is not considered during design, pressure drop will be underestimated.
Higher than expected pressure drops can reduce plant capacity and, in the case of relief
valves, lead to increased back-pressure that can restrict relief valve capacity. Ignoring
two-phase flow may also lead to poor process control. Two-phase flow to a control valve
is difficult to regulate smoothly and reproducibly. Slug or intermittent flow destabilizes
separation operations and can affect product purity or recovery. Continued operation in
slug flow can lead to increased maintenance costs, reduced equipment service life, and
catastrophic piping and equipment failure.
It is important to note that the prediction of two-phase flow regimes and pressure drops is
not very accurate. For example, one of the better horizontal flow regime maps was
shown to predict the correct regime only 67.2 % of the time. In addition, errors as high
as ± 50 % in pressure drop calculations are not uncommon. It is essential that
engineering judgement be used when designing for two-phase flow. The potential impact
on the system design and operation must be evaluated for scenarios where pressure
drop is under- or over-predicted and/or where the flow regime is incorrectly identified.
This section of the Hydraulics Manual describes two-phase (gas-liquid) flow and presents
guidelines for sizing both general and specific systems. In addition, detailed background
is provided in Section 4 of Book 2 on two-phase flow design criteria, including flow
regimes, liquid hold-up and pressure drop correlations, and velocity considerations.
Two-phase flow regimes are broadly categorized according to the continuity of the
flowing gas and liquid phases. The three most commonly identified types include:
Segregated Flow
Each phase is continuous. Stratified, wavy, and annular flow regimes are
examples of segregated flow.
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Intermittent Flow
Distributed Flow
One phase is continuous and the other is discontinuous, such as in bubble flow
(liquid phase is continuous) and mist flow (gas phase is continuous). This type of
flow regime most closely resembles homogeneous single phase flow.
For a given system, flow regimes can vary depending on the orientation of the
pipe (horizontal, vertical, or inclined). Each type of flow regime is described in
Section 4 of Book 2 according to pipe orientation.
The recommended design methods for two-phase flow applications are summarized in
this section. Several methods were evaluated in the course of preparing this manual.
Section 4.3.1 provides an overview of the recommended flow regime maps and
correlations. In Section 4.3.2, recommended evaluation procedures are described for
new and rerate designs. Section 4.3.3 provides a discussion of some special cases:
vacuum unit transfer lines, reboiler return lines, and condenser outlet lines. A sample
calculation illustrating some of the recommended design methods can be found in
Section 10.
1
Piping Design Handbook, McKetta, Two-Phase Flow, Pressure Drop and Holdup Equations,
pages 647-658.
2
Two Phase (Gas-Liquid) Flow Articles, Volumes I and II, Irvine Process Library.
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Flow regime maps and details of these recommended methods are provided in
Section 4.2 of Book 2.
To obtain the most accurate pressure drop estimation, the piping system
should be evaluated in small segments. In addition, because the
methods presented in this manual are flow regime and pipe orientation
dependent, each segment should only have one pipe diameter, one pipe
orientation and flow direction, and one flow regime. Pipe fittings should
be treated as their own segments.
The pressure drop for each segment should be limited to less than 10 %
of either the upstream or downstream pressure. This reduces the
compressibility induced errors to less than one percent. Significant
changes in the gas/liquid ratio due to flashing may necessitate further
subdivision to update the phase volumes and physical properties.
Caution must be used to ensure that a flow regime transition has not
occurred due to flashing.
b. Flow Regimes
When designing for two-phase flow, all turndown and alternate operating
conditions must be evaluated. The flow may be annular at normal or
design conditions, but may transition to slug flow at turndown conditions.
The intermittent flow regimes, slug and plug flow, should be avoided if at
all possible. Use more than one map, if possible, to determine the
system flow regime. Each map must be checked for generally
unacceptable flow regimes. If one of the maps shows an intermittent
flow regime, the basis and implications must be understood before the
map is disregarded or the flow conditions are changed.
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It must be emphasized that flow regime maps are not very accurate. In
fact, one of the recommended maps was found to correctly predict flow
regime only 67.2 % of the time. These maps are only an approximation.
Thought must be given to what is occurring in the system under
evaluation.
Changes from horizontal flow to inclined upward flow can greatly alter
the flow regime. Horizontal stratified flow will transition to slug flow when
the piping is rotated toward vertical. Unfortunately, the inclined flow
maps are the least well developed and are probably less reliable than
either the vertical or horizontal flow maps.
The flow regime may also be affected by weld penetration into the pipe.
Weld penetration may prevent the establishment of a uniform flow
regime. However, in most cases, this effect should be minor.
c. Slug Flow
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Engineering Data Book, Volume II, Section 17 Fluid Flow and Piping,
17-21 Liquid Slugging for one slug catcher design.
d. Erosional Velocity
The first step in designing or rating a transfer line is to determine the flow
regime. At design conditions, mist flow is almost always present. At
turndown, the flow regime may transition to annular flow. Due to the
high flowing velocities at design and turndown conditions, all of the
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At design conditions where mist flow is present, the liquid holdup should
closely approximate the feed liquid volume fraction (no-slip liquid
holdup). Both Dukler's method using the Hughmark liquid holdup
correlation and Dukler's no-slip correlation should give reliable pressure
drop estimates. Beggs & Brill's pressure drop method should also
perform well. At turndown, the liquid hold-up should be considered.
When designing reboiler return lines use the recommended flow regime
maps and pressure drop correlations listed previously in Section 4.3.1.
When the reboiler is rated by Mechanical Engineering, the HTRI program
will select the line size and predict the pressure drop for the return line.
The HTRI result should be reviewed and any significant discrepancies in
line sizing resolved.
Also see Houston Design Manual for Reboiler and Condenser - Kern
method, etc. A new writeup titled "Thermosyphon Reboiler" Calculation
Method is in preparation.
4.4 REFERENCES
Two-phase flow references are located in Section 4.3 Book 2 of this manual.
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PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 1 of 4
PROCESS MANUAL
THREE-PHASE (GAS-LIQUID-SOLID) FLOW DATE 07-95
1.0
1.0
2.0
3.0
4.0
5.1 INTRODUCTION
There are two similar vacuum resid hydrogenation processes that contain three-phase
flow systems that have been studied recently by Fluor Daniel: the Intevep HDH process
and the Veba Combi-Cracking process. In each of these processes the vacuum resid is
mixed with a solid catalyst to form a slurry, which is then mixed with a hydrogen-rich gas
to form a three-phase stream. This stream is fed through preheat exchangers and then
to a hydrogenation reactor. The resulting three-phase effluent stream is separated into
liquid, gas and solid streams via several processing stages. Both of these processes
have been successfully operated in small-capacity (150 to 3,500 BPD throughput) plants.
In a typical vacuum resid hydrogenation process the feed slurry has a solids content of
approximately 2 to 3 wt%, and a particle size under 300 µ (can be as low as 10-20 µ).
These solids may be either a non-reactive inorganic material or an organic type material
which reacts as the three phase system is heated. Due to the low solids content and
relatively small particle sizes, the three-phase lines have been treated as two-phase
(gas-liquid) lines, using the homogeneous slurry mixture rates and properties as the
"liquid" rates and properties. Line sizes are selected to give a velocity that is below the
erosional velocity and above the solids particle "settling" velocity, while still maintaining
an acceptable two-phase flow regime.
Segev and Golan found that for the EDS heater, the slurry could be regarded as a
homogeneous fluid (they did not present any data on particle size or shape). Therefore,
they concluded that the actual gas-liquid-solid flow in the heater could be represented as
a gas-liquid flow, and a suitable two-phase model could be used to predict pressure drop.
The "liquid" density was taken as the weighted average slurry density, while the viscosity
was estimated taking into account solid volume fraction and stream temperature. The
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authors used the Chisholm two-phase flow correlation, which is a modification of the
Lockhart-Martinelli correlation. For most of the reported test runs the predicted pressure
drop was within ± 10 % of the measured pressure drop. At the maximum, the calculated
pressure drop was 40 % below the measured value, which the authors thought may have
been due to experimental procedure difficulties, such as plugging in a pressure tap line.
a. Simplify Problem
For systems where the particle size is 40 µ or less, the combined liquid-solid
phase can be assumed to be homogeneous (refer to Slurry (Liquid-Solid) Flow,
Section 7.0 of this manual). If this assumption can be made for the system
under consideration, then the three-phase system can be reduced to a
two-phase system by treating the liquid and solid as a single "liquid" phase.
Even if some of the particle sizes are greater than 40 µ, as is the case with the
vacuum resid hydrogenation processes discussed earlier, the liquid-solid mixture
can most likely be treated as a single phase if the particle concentration is low.
With these simplifying assumptions, the appropriate two-phase methods for flow
regime and pressure drop can be used (refer to the Two-Phase (Gas-Liquid)
Flow, Section 4.0 of this manual). If the particle size is larger than 40 but under
300, the same procedure may be applied but special attention to be given to
settling velocities. In case of larger than 300 particles test data must be obtained
for any design. Refer to Section 7.0 for further details.
The slurry density is calculated as the weighted average of the liquid and solid
densities, using the following formula:
where:
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c. Size Line
Choose an initial line size and calculate its pressure drop using an appropriate
method for the system under consideration as recommended in the two-phase
flow section of this manual. Avoid problem flow regimes (e.g., slug flow).
If the initial line size does not meet all of the pressure drop and velocity
guidelines, select a new line size and repeat the procedure described above. If
other operating conditions apply to this line (e.g., turndown, alternate operating
cases, etc.), the selected line size must be further evaluated. It may prove
difficult to stay within the settling and erosional velocity limitations at all operating
conditions. If this is the case, it may be necessary to increase the margin above
the minimum settling velocity at the design throughput. Alternately, a
recirculation system can be used to maintain an adequate liquid-phase velocity at
reduced throughput conditions. Increasing the vapor volume fraction will also
have the same effect.
Long radius ells, pipe bends, and dead leg tees are generally used to minimize the
erosive effects of slurries.
For ease in maintenance, flushing connections, cleanout tees, swing ells, and drop-out
spools should be provided to access all piping components. Alternatively, piping sections
may be removable for inspection and cleaning at grade.
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5.5 REFERENCES
1. Segev, A., and Golan, L.P., Multiphase Flow and Heat Transfer in the EDS
Slurry Preheat Furnace, AIChE Symposium Series, No. 255, Vol. 79, 1983.
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PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 1 of 1
PROCESS MANUAL
NON-NEWTONIAN FLUID FLOW DATE 07-95
1.0
1.0
2.0
3.0
4.0
5.0
[ LATER ]
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SLURRY (LIQUID-SOLID) FLOW DATE 07-95
1.0
1.0
2.0
3.0
4.0
5.0
6.0
7.1 INTRODUCTION
This manual section is intended to give the user a guide to designing an in-plant slurry
transport system. Transporting solids in a pipe using a liquid carrier is becoming
increasingly more common, especially in the area of coal transport through pipelines.
Much of the theory and published literature on the design of pipelines can be used in the
design of in-plant slurry systems, and has, in fact, been used here.
Solid particles immersed in a stagnant fluid tend to rise or sink according to the
relative densities of the two phases. Stokes law, based on the assumption that
the fluid is infinite with respect to the particles (i.e. the volume fraction of solids is
less than 10 % and the nearest wall is 20 particle diameters away), can be used
to explain why small particles do not settle and instead are carried along with the
fluid. In the Stokes regime the drag coefficient is related to the particle Reynolds
number by the following equation:
With this relationship, we can find the terminal velocity for particles with NReP < 1.
gd 2 (ρ p − ρ)
VP =
18µ
When the liquid is flowing, lift forces become significant which tend to keep the
slurry mixed. Obviously, a well designed slurry piping system will keep the solids
from settling and building up deposits which could inhibit or stop flow.
7.1.3 Erosion
Turbulent eddies can cause severe erosion of pipes, pumps and fittings when
solid particles are present. Abrasion can be lessened by ensuring that wetted
surfaces are smooth. Easily replaceable pipe linings are often used. Long radius
elbows spread out erosion effects.
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Particle properties may change as the particles rub against each other and erode.
This will have a significant effect only in long distance pipelines.
7.1.4 Slippage
This condition occurs when the solid and liquid phases are traveling at different
rates. The extent of slippage between phases is a function of pipe angle, particle
size, relative phase densities and average velocity.
The slurry density, usually taken to be the weighted average of the solid and
liquid phases, is not constant when slippage occurs. The density will be a
function of the amount of slippage expressed as a concentration gradient.
7.2.1 Viscosity
Viscosity correlations for slurries are many and varied. Our recommendation is
that the viscosity be measured. Viscometers used to measure slurry properties
must keep the slurry in suspension. A Brookfield viscometer is especially
inaccurate for slurries. A viscometer that is recommended is the Haake-Roto
viscometer made in Germany. (1) The Stormer viscometer is frequently used for
drilling mud. Shear stress vs. shear rate data should be obtained over the entire
range of anticipated velocities. This data will be essential for calculating pressure
drops.
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Figure 7-1
DESIGN PROCEDURE
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Solids in category 2 tend to settle because gravity forces dominate. The larger
particles and the liquid phase tend to retain their own identities, not interacting
chemically or physically. These slurries are known as heterogeneous slurries.
a. How to Measure
It is also important that the scaled-down particles settle in the same flow
regime (laminar, transition, turbulent) as the particles on the full scale.
1. Non-settling fluids
Laminar Flow
Turbulent Flow
Dx τ = kVw (1)
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2. Settling fluids
Table 7-1
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7.2.3 Erosion/Corrosion
The corrosion rate in slurry pipelines could be accelerated over that of the carrier
fluid by the presence of solids. Solids can also abrade the pipe. In addition,
solids can erode away the corrosion products which form a protective film and
further increase the corrosion rate.
The corrosion rate can be measured in a reaction kettle with a mixer by means of
a corrosometer probe. The corrosion rate, dissolved oxygen concentration, and
pH of the slurry should be measured. Instead of a corrosometer, steel "coupons"
can be dropped into the reaction kettle. The weight loss of the coupons will be a
measure of the corrosion rate. Electrochemical measuring techniques can also
be used, the electrochemical method will give instantaneous corrosion rates.
7.2.4 Restart
Restarting a slurry system after the slurry has been stagnant in the pipe over a
period of time may prove to be difficult if not impossible. Some solid particles
may tend to interact physically and essentially create a solid mass which may not
be pumpable.
Therefore, it is recommended that all lines be equipped with purges unless there
is unequivocal evidence that restart will be easy. Then in the event of a
shutdown of lasting duration the lines can be purged. In the event of a
slowdown, water may be recycled to maintain the minimum transport velocity.
If it is possible, when testing is done on the other properties, the slurry should be
allowed to set for specified lengths of time (e.g., 4 hrs, 8 hrs, 16 hrs., 24 hrs, 2
days etc.) and the restart ability observed at the end of each time segment. This
will give the operators an idea of how soon after shutdown they should consider
purging the lines.
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Most sources recommend, as a rule of thumb, that the design velocity be 1 ft/sec greater
than the minimum transport velocity. However, the design velocity should not exceed
this amount by very much due to the erosive nature of slurries.
Check to see that the design velocity meets the criterion discussed above; if it
does not, go to step one and repeat the procedure.
If it does, more work may need to be done to determine the economic optimal
pipe diameter. If data on the erosion rate vs. slurry velocity is available, it should
be considered here also. In the economic analysis pipe material and linings
should be considered as well.
a. Non-Settling/Homogeneous
τ = τ y + K nγ (3)
where:
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Figure 7-2
FLUID CLASSIFICATION
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τw = D ∆P (4)
4 L
where:
Q =
πD 3 4n τ w 1/h 1 − τ y
32 3n + 1 K τw
τ y /τ w 2n ( τ y ) (1 + n τ y ) }
{1 − 1 + τ w (5)
2n + 1 n + 1 τw
Dodge & Metzner (4) derived the modified von Karman equation
to describe turbulent flow characteristics:
ρs VD 3n + 1 n 8V n−1
N Re = (7)
K 4n D
a 1 = 1 − n2 (10)
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E2 = 4.0/n (11)
F2 = - 0.4/n (12)
a2 = 1 − n
2
(13)
C f 2 ρs V 2 1lb f /ft 2
= ∆P (14)
gc D L ft
In one, Cf becomes:
C f = 16/N Re 1 − 2He2 {1 − 1 2He }
C f Re
N 2n − 1 C 2
f N Re
1 + 2n 2He (1 + n 2He )
(15)
n + 1 C fN2
Re C f N 2Re
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where:
ρVD
NRe = µ (16)
and
τ y N Re 2
He = (17)
ρV 2
For fluids which have an n < 0.28 the turbulent flow curve
intercepts the laminar flow curve at a point higher than NRe2.
This means that such fluids have no transitional flow regime. If a
transitional flow regime does not exist the procedure for turbulent
flow should be used (3).
b. Settling/Heterogeneous Slurries
1. Horizontal Pipes
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V 2 C 0.5
Nl = D
N (18)*
C v Dg (S − 1) l
J − Jw
∅ = (21)
Cv Jw
where:
V 2 C 0.5
Ψ = D
(22)*
gD (S − 1)
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2. Vertical Pipes
According to Wasp et. al. (6) the friction losses in vertical pipes
differ from the friction losses in horizontal pipes for
heterogeneous slurries only.
2f p V 2 L
∆P = (ft) (23)
gD
c. Hetero-Homogeneous Flow
∆ PT = ∆ Pv + ∆ PH (24)
where:
To actually calculate the pressure losses, the friction factor must first be
calculated. For hetero-homogeneous slurries the following empirical
correlation may be applied:
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Govier and Aziz (8) suggest that K' = 150 be used and Hanks (7) asserts
that data exist which back Govier and Aziz.
a. Laminar Flow
For Laminar flow conditions, the fitting losses depend on the fluid
properties. Cheng (3) suggests that the losses, when expressed as a
ratio to corresponding Newtonian losses, increases as the Reynolds
number decreases and can be on the order of ten when NRe is low.
Cheng has a method from which the ratio may be determined for various
Reynolds numbers and pipe diameters. See Appendix 1 of Section 7.10.
From the ratio read from the graph, the non-Newtonian fittings losses
may be calculated using the tabulated Newtonian losses.
b. Turbulent Flow
Cheng (3) suggests that for suspensions in turbulent flow, the fittings
losses do not depend on fluid properties and the pressure losses can be
assumed to be the same as for a Newtonian fluid.
For slurries in which the solids thermal conductivity is greater than that of the
suspending medium, the controlling resistance to heat transfer is in the liquid and
the thermal conductivity of the solid does not appreciably affect heat transfer (9).
In this case the following correlation for slurries holds:
C p µ
0.4
h jD 0.8
= 0.029 DG
µ k (26)
k
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For Laminar flow the thermal conductivities and specifics of the mixture can be
found by weighted average of the separate component properties.
Table 7-2
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Where grinding is done specifically to prepare a material for pipelining, the step
will normally involve conventional milling equipment. In some cases the
equipment may be a new application to grinding the specific material.
In slurry preparation, two variables are quite important which may have only
minor significance in other crushing processes. These are the slurry density and
the product top size.
Top-size control is extremely important for any slurry transport. Large quantities
of coarse, fast-settling particles can plug the piping.
a. Purpose
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When specifying mixer types and design, the major things the
engineer should consider are:
b. Power Requirements
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a. Type of Pumps
1. Centrifugal Pumps
2. Positive-Displacement Pumps
These are used where pumping pressures above 600 lb/in2 are
required. For very abrasive slurries, the plunger-type pump is
used, with a flushing arrangement injecting clear liquid to keep
solids away from the plunger packing.
3. Diaphragm Pumps
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b. Selection
Size of the solids (What are the largest particles the pump must
handle?)
Nature of the liquid (Will it lubricate the solids and reduce the
abrasion? Corrosive?)
c. Power Requirements
Once the total pressure drop is known, sizing the pumps is a simple
matter. The pump discharge pressure is the sum of the pressure losses
(line friction losses, and fitting friction losses plus hydrostatic head
changes). The power requirement is then:
Q∆P T
Power = e e = pump efficiency
a. Pipe Material
The designer of slurry systems is always faced with the selection of the
most economical pipe that will have an expected life consistent with the
particular application. Pipe choice depends on pressure, temperature,
limitations, corrosiveness, and abrasiveness of the slurry. Available pipe
includes:
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The last four types are more expensive than conventional unlined carbon
steel and would only be used with a very abrasive or corrosive slurry. As
noted, general pipe abrasion becomes a consideration at velocities of
13 ft/sec (4 m/s). Also, pipe wear increases exponentially with velocity
above a certain threshold velocity. This exponential value has been
reported to range from 2.1 to 2.9.
Table 7-3
MATERIAL HARDNESS
Material Miller Number
Detergent 0
Coal A 11
Coal B 28
Fine magnetite 64
Hematite 260
Carborundum 1,000
After selecting the pipe, the designer must specify the pipe minimum
yield strength and the wall thickness required to contain the expected
pressures. This is done using standard formulas.
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b. Piping Layout
When laying out the slurry piping system, the designer must consider:
Valves, like pumps, must be designed for abrasive service and with
consideration to sedimentation and plugging. They preferably provide a
full opening, should not depend on machined-metal surfaces for closure,
and do not have dead pockets that can fill with solids and restrict
operation.
7.7 INSTRUMENTATION
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Blanket level - The height of solids which have "buildup" on the bottom of
the tank and formed a blanket
Pressure Drop
Flow Rate
a. Solids Concentration
Ultrasonic
Photoelectric
Nuclear
While no one system is suitable for all types of slurries, each of the
above measurement systems has strong and weak points. The
ultrasonic system is good for slurries with low to media solids
concentration. The nuclear system is especially good for extremely
heavy, opaque, abrasive slurries. The photoelectric systems are only
suitable for very thin slurries, since their penetration of individual solid
particles is almost nil and they reach saturation quickly. They are best
for measuring a highly aerated liquid media because ultrasonic and
nuclear sensor become confused by the profusion of water bubbles.
b. Flowmeters
Electromagnetic flowmeters
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Ultrasonic Flowmeters
Also obstructionless they are useful in that sense, but they are
more sensitive to process liquid variations. They have difficulty
measuring liquids containing high concentrations of solids and
air (10).
7.8.1 Glossary
Bingham Plastic Slurries - Slurries which behave like a Bingham Plastic and
require a knowledge of the shear stress as a function of shear rate to be properly
treated.
Froude Number - Fr = V2/gD for a given concentration and particle size, the
onset of deposition occurs at a constant Froude number.
τ y (N Re ) 2
Hedstrom Number - He = identifies the boundary between laminar and
V 2ρ
transitional flows.
Newtonian Slurries - Behaves like a Newtonian fluid and can be treated as such.
Non-Settling Slurries - Slurry in which the particles, due to the relative densities
of the solid and liquid phases, do not settle out.
Power Law Fluid - Non-Newtonian fluid with viscosity a function of fluid velocity.
Pseudo Plastic - Slurries or fluids whose behavior is time independent, for which
an infinitesimal shear stress will initiate motion, and for which the rate of increase
in shear stress with velocity gradient decreases with increasing velocity gradient.
Settling Slurries - Slurry in which the particles, due to the relative densities of the
solid and liquid phases, tend to sink.
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Vehicle - In a slurry with a wide range of particle sizes, the fine particles will mix
with the liquid to form a homogeneous mixture known at the vehicle.
Depositing Velocity - The point at which the particles settle out as the velocity is
lowered. The particles may settle as a static bed or as a moving bed. This
velocity is related to the suspension velocity but they are not necessarily equal.
Also known as the minimum transport velocity.
Velocity for Homogeneous Flow - The velocity at which the particles become
evenly distributed throughout the pipe.
Saltating Velocity - Velocity at which particles are transported along the bottom
of a pipe in a series of jumps.
Sliding Bed Velocity - The velocity at which the shearing forces in the liquid are
just sufficient to move the particles lying on the floor of the pipe.
Standard Velocity - This is defined as the velocity above which the pressure
gradient of the suspension is equal to that for an equivalent fluid (that is, a fluid
with the density of the suspension and the viscosity of the suspending fluid).
Suspending Velocity - This is the velocity at which the particles are just picked up
and remain in suspension, and is the velocity which should be used for designing
most pipelines.
7.8.2 Nomenclature
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d = Particle diameter
Fr = Froude Number
G = Mass velocity
He = Hedstrom number
K = Consistency coefficient
K' = 150
k = Thermal conductivity
n = Consistency index
p = Concentration index
∆P = Pressure drop
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S = Specific gravity
V = Slurry velocity
VD = Design velocity
VP = Particle velocity
γ = Shear rate
ν = Kinematic viscosity
µ = Absolute/dynamic viscosity
ρ = Fluid density
ρP = Particle density
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τ = Shear stress
τY = Yield stress
Note: Units should be consistent with applicable formulas, e.g., Eqn. 1-26,
pages 4-14.
7.9 REFERENCES
2) Wasp E.J., J. P. Kenny, R.L. Gandhi, Solid Liquid Flow, Slurry Pipeline
Transportation, Trans - Tech Publications, Glavsthal, Germany 1977.
* 6) Aude, T.C., N.T. Cowper, T.C. Thompson, E.J. Wasp, Slurry Piping
Systems: Trends Design Methods, Guidelines, Chem. Engr. Vol 78,
June 28, pp 47 (1971).
* 8) Govier, G.W., and K. Aziz, The Flow of Complex Mixtures in Pipes, Van
Nostrand Rheinhold Corp, New York, 1972.
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12) Bain, A.G., and S.T. Bonnington, The Hydraulic Transport of Solids by
Pipelines, Pergamon Press, New York, 1970.
* 13) Carleton, A.J. and D. C-H. Cheng Pipeline Design for Industrial Slurries
Chem. Engr., 84, April 25 pg 95 (1977).
+ 14) Carleton, A.J., and D.C-H. Cheng, Design Velocities for Hydraulic
Conveying of Settling Suspensions, Proceedings, 3rd International
Conference on Hydraulic Transport of Solids in Pipes. BHRA, 1974.
15) Morton Denn, Process Fluid Mechanics, Prentice Hall, Englewood Cliffs,
New Jersey. @ 1980.
* 16) Daistad, J.I., Slurry Pump Selection and Application, Chem Engr., Vol
84, April 25, pg 104 (1977).
* 17) N.T. Cowper, T.L. Thompson, T.C. Aude, and E.J. Wasp. Processing
Steps: Key to Successful Slurry - Piping Systems, Chem.
Engr., Vol. 79, Feb. 7, pg 58 (1972).
* 18) R.H. Derammelaere, E.J. Wasp, Slurry Systems and Pipelines, Piping
Design Handbook by J.J. McKetta, p. 89, Dekker Inc. 1992.
* The above items are available in the FDI Process Engineering Library.
+ The above items are available in the FDI Technical Library, Technical
Data Files under Slurries 5.44.6.1 (with Slurry Files Volumes I and II).
7.10 APPENDIX
Since for laminar flow condition losses depend on fluid properties a method for
determining these losses must be established.
Cheng (3) suggests a method for constructing a graph which gives the ratio of
fittings pressure loss in non-Newtonian flow to fittings pressure loss in
non-Newtonian flow. This graph may be constructed when the fluid parameters
K, and n are known. With these parameters and any given pipe diameter, NRe1
may be calculated; for this and larger values of the Reynolds number, the ratio of
non-Newtonian fittings loss to that of Newtonian is unity. If it is assumed that this
ratio increases to 10 when NRe is reduced from NRel by a factor of 1,000, a
straight line may be drawn in the graph so that the ratio may be fixed at
intermediate Reynolds numbers. As NRe1 varies with the pipe diameter, a family
of parallel lines is obtained for different pipe diameters. From the ratio read off
these lines, the non-Newtonian fittings losses may be calculated using the
tabulated Newtonian losses.
Following is a sample graph (Figure 7-3) for a manganese dioxide slurry. (From
Ref. 3).
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Figure 7-3
SUGGESTED RELATION BETWEEN PRESSURE LOSS IN PIPE FITTING AND REYNOLDS NUMBER
FOR NON-NEWTONIAN FLUIDS FOR A MANGANESE DIOXIDE SLURRY
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PIPING HYDRAULICS AND SPECIFICATIONS
BOOK 1 PAGE 1 of 1
PROCESS MANUAL
PNEUMATIC CONVEYING DATE 08-94
1.0
1.0
2.0
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PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 1 of 1
PROCESS MANUAL
COMPUTER PROGRAMS DATE 08-94
1.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
New program, PALS, is in use for single phase flow. Two phase flow section is scheduled for
completion in FY 1995.
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PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
1.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
9.0
Example Problem:
S.A.E. Lube Oil @ 100oF is flowing at the rate of 600 bbls/hr through 200 feet of 8"
Schedule 40 pipe.
a. Reynolds Number
Qρ
NRe = 50.6
dµ
b. Friction Factor
c. Velocity
0.93 ft 3 / sec
v, ft/sec = 2.7 ft/sec
π (0.33 ft) 2
d. Pressure Drop
0.001294 fρv 2 L
∆P =
d
= 2.65 psi
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Example Problem:
600 psig steam at 850 oF flows through 400 feet of horizontal 6-inch Schedule 80 pipe at
a rate of 90,000 lbs/hr.
The system contains three 90 degree standard elbows and one 6-inch Class
600 Y-pattern globe valve. The valve has a seat diameter equal to 0.9 of the inside
diameter of Schedule 80 pipe, disc fully lifted.
a. Reynolds Number
= 3,650,000
f = 0.015
55 f T 0.5(1 − β 2 ) + (1 − β 2 ) 2
K = + β
β4 β4
fT = 0.015
= 1.44
K = 30 fT
= 0.45
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e. Equivalent Length
K = fL/D
(0.48 ft)
∴L overall = 400 ft + [1.44 + (3)(0.45)]]
(0.015)
= 489 ft
f. Density
V = 1.216 ft3/lbm
ρ = 1 = 1 = 0.8223 lb m /ft 3
V 1.216
g. Velocity
h. Pressure Drop
fρv 2 L
∆P = 0.001294
d
= 38.3 psi
With 20 % safety factor for valves and fittings (no safety factor for pipe per
Section 3.0),
(89)(38.3)
∆ P = 38.3 + (0.2) = 38.3 + 1.4 = 39.7
489
Since the pressure drop is less than 10 % of the inlet pressure, it is not
necessary to repeat the calculation using an average gas density based on the
upstream and downstream conditions.
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Example Problem:
Air is discharged from a large reservoir at 150 psig and 70oF through 33 feet of straight
2-inch Sch. 40 standard steel pipe, and three 90-degree standard elbows to the
atmosphere. The pipe intake projects slightly into the reservoir.
From the Moody friction factor chart or from Figure 2-2, for a 2" Sch 40 pipe,
ε /D = 0.0009, and for completely turbulent flow, f = 0.019.
L/D
Assume f = 0.019 Intake K = 0.78 41
Straight Pipe: (33) (12)/(2.067) = 191.6
Three elbows; (3) (30) = 90
322.6
N1/2 = 2.48
To = 530oR
Po = (150 + 14.7) = 164.7 psia
P3 = 14.7 psia
P3/Po = 0.0893
M = 28.9 lbm/lb mole
e = 2.718
1/2
gc M
GCNi = Po (from Section 3.3, Book 2)
e R To
(32.17)(28.9)
1/2
= (164.7)(144)
(2.718)(1, 545)(530)
It is now possible to calculate the discharge by direct use of the Lapple charts
(Section 3.3, Book 2) as shown by the following tabulation.
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This calculated f is so close to the assumed f that it is not necessary to repeat the
calculation.
Although not a part of the example, it is instructive to identify the impact of different γ ’s.
Example Problem:
QL = 775 gpm
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V 22 ρ V 23 ρ KV 22 ρ
+ P2 = + P3 +
9, 270 9, 270 9, 270
DL
= 4 = 0.5
D 8
QL
= 775 = 0.5
Q 1, 550
K = 0.24
Note: From this calculation we see that there is an actual increase in pressure going
across the fitting but a check of the total energy at both points will show a
decrease in total energy to 0.087 psi due to friction loss.
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Z 2ρ V 22 ρ Z4ρ V 24 ρ KV 22 ρ
P2 + + = + + + P4
144 9, 270 144 9, 270 9, 270
Z4
= 0 By Definition
144
V4 = 20 ft/sec calculated
K = 2.65
Note: In going from (2) to (4) 2.02 psi of static pressure was converted to kinetic
energy.
Example Problem:
System Sketch
This system is just a portion of the piping that may exist between 2 process units. It will
be broken up into the horizontal section, the fitting, and the vertical section. The
conditions are as follows:
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Liquid Gas
For two-phase flow correlations, equations and maps used in this sample problem, refer
to Section 4 in Book 2 of this manual.
Ve = C
ρm
where:
Basis: 1 second
2.1 ft 3 / sec
No slip mixture velocity = = 6.02 ft/sec
0.3491 ft 2
Since the mixture velocity is less than the erosional velocity, we can continue.
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b. Determine the flow regime using the recommended horizontal flow regime maps.
WL 4
ULS = = = 0.286 ft/sec
ρ L A 40(0.3491)
WG 6
UGS = = = 5.73 ft/sec
ρ g A 3(0.3491)
U LS D (0.286) 12
8
N Re LS = νL = −6
= 2.3 x 10 4
8.4 x 10
U GS D (5.73) 12
8
N ReGS = ν = = 1.2 x 10 6
G 3.3 x 10 −6
Since the flow of both phases are turbulent and the pipe is rough, use
the Moody friction factor diagram (see Perry's, 6th Ed., 1984, pp. 5-24)
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 10
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
4f LS ρ L U LS
2
dp 4(0.0064) (40)(0.286) 2
= =
dx LS D 2g c 8 (2)(32.2)
12
1b f /ft 2
= 0.00195
ft
4f GS ρ L U GS
2
dp 4(0.0037) (3) (5.73) 2
= =
dx GS D 2g c 8 (2)(32.2)
12
1b/ f /ft 2
= 0.3395
ft
1/2
3 (5.73) 2 (0.286)
K = −6
= 53.1
(40 − 3)(32.2)(8.4 x 10 )
1/2
0.063
T = = 0.007
( 40 − 3)( 32.2)( 1)
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 11
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
Transition C: Given X = 0.240 and K = 53.1, one finds the point lies
above the C curve, making the flow regime stratified wavy.
Based on these superficial velocities, the Mandhane map shows stratified flow is
present.
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 12
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
For this calculation, we choose to use the Dukler -Constant Slip method with the
Hughmark holdup.
W L /ρ L 4/40
λ = = = 0.048
W L /ρ L + W G / ρ G 4/40 + 6/3
µ TP = µ L λ + µ G (1 − λ)
RL, using the Hughmark correlation. This correlation requires a trial and
error calculation. The Reynolds number is first guessed and then it is
recalculated using the liquid holdup. When the assumed (guessed)
number is equal to the calculated number, the final value of RL is
obtained.
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 13
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
Z = (210,000)1/6(1.69)1/8(0.048)-1/4 = 17.59
If Z <8
If Z ≥ 8
⇒K = 0.8206
RL = 1 - (1 - 0.048)(0.8206) = 0.2188
ρ ns V M D
NRe =
R Lµ L + RG µG
where:
ρ ns = No-slip density = ρ L λ + ρ G (1 - λ )
= 40(0.048) + 3 (1 - 0.048)
= 4.776 lb/ft3
(4.776)(6.02) 12
8
NRe =
0.2188(0.000336) + (1 − 0.2188)(0.00001)
NRe = 235,000
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 14
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
⇒Z = 17.92
⇒K = 0.822
RL = 1 - (1 - 0.048)(0.822) = 0.2175
Calculate NRe
(4.776)(6.02) 12
8
NRe =
0.2175(0.000336) + (1 − 0.2175)(0.00001)
= 236,911
Guess NRe = 237,000 (guess is slightly higher since calculated values are
increasing).
⇒Z = 17.95
⇒K = 0.8221
⇒ RL = 0.2174
(4.776)(6.02) 12
8
NRe =
0.2174(0.000336) + (1 − 0.2174)(0.00001)
= 237,011 ≈ 237,000
Since the guessed and calculated NRe #'s are similar, we continue, using
the final RL value of 0.2174.
= 3.898 lb/ft3
DV m ρ TP
NReTP = µ TP
8 (6.02)(3.898)
12
= = 611,093
2.56 x 10 −5
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 15
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
fTP = fα
where:
α = 1+ − Inλ
1.281 − 0.478( − Inλ) + 0.444( − Inλ) 2 − 0.094( − Inλ) 3 − 0.00843( − Inλ) 4
and:
α = 1 + 3.0366
2.008
= 1 + 1.512 = 2.512
fTP = fα = (0.0032)(2.512)
= 0.008
∆P = 2f TP ρTP V 2m
∆Z f gcD
2(0.008)(3.898)(6.02) 2
=
32.2 12
8
1b f /ft 2
= 0.1053 = 0.073 psi per 100 ft
ft
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 16
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
∆ Ps = ρ TP V NS V SG /g c P
∆P [∆P/∆Z]
=
∆Z total 1 − ∆P s
= 0.073
1 − 0.000135
The horizontal pipe in the first part of the system is connected to the
vertical pipe section by means of a 90o elbow.
We must determine the pressure loss due to the fitting and will use the Chisholm
method.
1/2
W L 1/8 ρ V µ L 0.2
For smooth tubes, X = ρL µ G , however our pipe
WG
is rough so we use the X we calculated earlier in this example.
X = 0.240
2. Calculate C2
307.2 lb 1 sec
C2 = x x 0.3491 ft 2
sec ft 2 10 lb
= 10.7
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 17
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
WG 6 0.6
X = =
W G + WL 6 + 4
4. Calculate parameter Tc
2− n/2 µ
X L ρG
n/2 1/2
Tc = 1 − X µ G ρL
= 0.411
5. Calculate parameter C1
ρL ρ 0.5
0.5
C1 = ρG + ρG
L
0.5 0.5
= 40 + 3 = 3.925
3 40
6. Calculate parameter C3
ρ g 0.5
C3 = λ + (C 2 − λ) ρFG C 1
where:
ρ FG = ρ F - ρG
3 3.925
0.5
C3 = 1 + (10.7 − 1)
40 − 3
= 14.77
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 18
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
C3
1 + Tc
+ 1
2
Tc
ψ = C1
1 + Tc
+ 1
T 2c
2
1 + 14.77
0.411
+ 0.411
1
= 2
= 2.6
1+ 3.925
0.411
+ 0.411
1
8. Calculate φf2
C1
φf 2 = 1 + + 12 Ψ
X X
3.925 + 1 x 2.6
= 1 +
0.24 0.24 2
= 90.26
KG 2T φ2f
∆P =
2g c ρL
where:
= 28.645 lb
sec ft 2
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 19
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
For the pressure drop, we will use the recommended correlation, Beggs
& Brill.
e. Determine the flow regime using the recommended vehicle flow regime maps
First the Beggs & Brill map will be used and then the other vertical maps.
The Beggs and Brill flow regimes can be determined with or without the map
present.
where:
NFR, the Froude number, = 1.69 (previously calculated). The flow pattern can be
determined as follows:
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 20
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
Since Rule 1 (NFR < L1) applies here, the flow pattern is segregated. This is
confirmed by looking at the Beggs & Brill map.
This point occurs in the bubble region of the map, however, its flow regime areas
are very broad and don't include stratified or wavy.
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 21
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
For Govier et. al's map, the modified superficial liquid velocity:
ρ L 72.4 V
1/4
y = YVSL= σ
62.4 SL
1/4
40 72.4 (0.286) = 0.33 ft
=
62.4 25 sec
= 22.3 ft/sec
These values, plotted on the Govier map, indicate froth flow is present.
All three maps indicate suitable flow regimes, so the calculations are continued.
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` FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 22
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
Since we determined the flow regime to be segregated on the Beggs & Brill map,
we use the recommended correlation, Beggs & Brill to calculate holdup.
1. Calculate Holdup
0.98(0.48) 0.486
R L (0) = 0.98λ0.868 =
0.846
= 0.215
N FR 1.69 0.0868
(This is the horizontal holdup which will be corrected for the angle of
inclination, 90o).
2. Calculate C
0.011N LV3.539
C = (1 − λ) In
λ 3.768 N 1.614
Fr
where:
1/4
= 1.938(0.286) 40 = 0.6234
25
C = 4.2
3. Calculate φ and Ψ
ρ TP = ρ LRL + ρ G (1 - RL)
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D FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 23
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 03-99
6. Calculate fTP/fns
f TP In y
= exp
f ns −0.0523 + 3.182 (In y) − 0.8725 (In y) − 0.01853 (In y)
2 4
where:
y = λ = 0.048 2 = 0.20322
[R L (θ)] 2 0.4859
f TP
ln y = -1.59 ⇒ = 1.247
f ns
−2
N Re ns
= 2 log
fns
4.5223 log N Re − 3.8215
where:
[ρ L λ + ρ G (1 − λ)] V m D
NRe ns =
µ L λ + µ G (1 − λ)
= 747,336
−2
2 log 747, 336
fns = 4.5223 log (747, 336) − 3.8215
= 0.01225
∆P = f TP G T V m
∆Z f 2g c D
0.015(28.645)(6.02)
=
8
2(32.2) 12
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D FLUOR DANIEL
SECTION 10.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 24
PROCESS MANUAL
SAMPLE HAND CALCULATIONS DATE 08-94
lb f ft 2
= 0.0602 = 0.042 psi per 100 ft
ft
∆P = g sin θ[ρ L R L + ρ G (1 − R L )] g
= g sin θ ρ TP
∆Z el gc c
lb m lb f lb f /ft 2
= 20.98 = 20.98
ft 3 lb m ft
But, when designing for uphill flow, the elevation term should be
evaluated as liquid-full and, therefore, the liquid density would be used
instead of the 2 phase density.
2
∆P = 20.98 40 = 40 lb f /ft = 27.8 psi per 100 ft
∆P e1 20.98 ft
2 1 ft 2
= 0.1047 in2 x = 0.00073
ft 144 in 2
∆P + ∆P
∆P = ∆Z el ∆Z f
∆Z T 1 − ACC
40 lb f ft 3 + 0.0602 lb f /ft 3
=
1 − 0.00073
lb f /ft 2
= 40.09 = 27.84 psi per 100 ft in vertical line
ft
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` FLUOR DANIEL
SECTION 11.0
PIPING HYDRAULICS AND SPECIFICATION
BOOK 1 PAGE 1 of 1
PROCESS MANUAL
GENERAL BIBLIOGRAPHY DATE 11-94
1.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
9.0
10.0
11.1 Piping Design Handbook, John J. McKetta, Marcel Dekker, Inc., 1992.
11.3 Flow of Fluids Through Valves, Fittings and Pipe, Crane Technical Paper No. 410, latest
edition.
11.5 GPSA Engineering Data Book, Volume II, Section 17 - Fluid Flow and Piping, latest
edition.
11.6 Two-Phase (Gas-Liquid) Flow Articles, Volumes I and II, compiled by A.R. Smith, Irvine
Process Library.
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