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Insoluble impurities"
DEFINITION
This method determines dirt, meal and other foreign substances insoluble in kerosene and petroleum
ether.
SCOPE
Applicable to all normal fats and oils.
APPARATUS 3. Filter through the prepared Gooch crucible with the aid
1. Gooch crucible--prepared with a glass-fiber filter with- of a vacuum. Wash with five 10-mL portions of hot
out organic filler (Reeve Angel 934 AH or WhatmanJ kerosene, allowing each portion to drain before adding
GF/C). Wash the filter with y , ~ x , all;l2b& and e h s the next.
Dry to constant weight at I0 I k 1"C Cool in a desicca- 4. Wash thoroughly with petroleum ether to remove all of
tor to room temperature and weigh. J the kerosene. Dry the crucible and contents to a
2. Filter flask of convenient size ahd Gooch crucible constant weight at 101 k 1°C. cool to room temperature
v in a desiccator and weigh.
(
adapter.
F
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