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SPECIFICATION FOR AUSTENITIC STEEL FORGED

AND BORED PIPE FOR HIGH-TEMPERATURE


SERVICE

SA-430 /SA-430M

(Identical with ASTM Specification A 430 /A 430M-91 except for clarified heat treatment requirements in 5.4.1.)

1. Scope 2. Referenced Documents


1.1 This specification covers heavy-wall, forged and 2.1 ASTM Standards:
bored austenitic steel pipe (Note 1), intended primarily A 262 Practices for Detecting Susceptibility to Intergran-
for high-temperature central station service. Pipe ordered ular Attack in Austenitic Stainless Steels
to this specification shall be suitable for bending and other A 530/A 530M Specification for General Requirements
forming operations and for fusion welding. Selection will for Specialized Carbon and Alloy Steel Pipe
depend on design, service conditions, mechanical proper- E 381 Method of Macroetch Testing, Inspection, and
ties and high-temperature characteristics. The “H” grades Rating Steel Products, Comprising Bars, Billets,
and nitrogen grades (304N and 316N) are specifically Blooms, and Forgings
intended for high-temperature service. 2.2 ANSI Standard:
B46.1 Surface Texture
NOTE 1 — The use of the word “pipe” throughout the several sections
of this specification is used in the broad sense and intended to mean
pipe, headers, or leads.
3. General Requirements
1.2 Eleven grades of austenitic steels are covered. 3.1 Material furnished to this specification shall con-
Their compositions are given in Table 1. form to the applicable requirements of the current edition
of Specification A 530 /A 530M, unless otherwise pro-
1.3 Optional supplementary requirements (S1 through vided herein.
S11) are provided. These sections call for additional tests
to be made, and when desired shall be so stated in the
order, together with the number of such tests required. 4. Ordering Information
4.1 Orders for material to this specification should
1.4 The values stated in either inch-pound units or include the following, as required, to describe the desired
SI units are to be regarded separately as standard. Within material adequately:
the text, the SI units are shown in brackets. The values
4.1.1 Quantity (feet, centimeters, or number of
stated in each system are not exact equivalents; therefore,
lengths),
each system must be used independently of the other.
Combining values from the two systems may result in 4.1.2 Name of material (forged and bored pipe),
nonconformance with the specification. The inch-pound 4.1.3 Grade (Table 1),
units shall apply unless the “M” designation of this speci- 4.1.4 Size (outside diameter and minimum wall
fication is specified in the order. thickness),
NOTE 2 — The dimensionless designator NPS (nominal pipe size) has 4.1.5 Length (specific or random) (Permissible
been substituted in this standard for such traditional terms as “nominal Variations in Length Section of Specification A530/A
diameter,” “size,” and “nominal size.” 530M),

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SA-430 /SA-430M 2004 SECTION II

4.1.6 End finish (Section 10), [980°C]; and all other grades to minimum temperature
4.1.7 Special surface finish (see 5.3), of 1900°F [1040°C], and quenching in water or rapidly
cooling by other means.
4.1.8 Optional requirements (see 5.4.2, Section 7,
and Supplementary Requirements S1 to S11), 5.4.3 Solution annealing temperature above 1950°F
[1065°C] may impair the resistance to intergranular corro-
4.1.9 Test report required (see Certification Section
sion after subsequent exposure to sensitizing conditions
of Specification A 530/A 530M),
in TP321, TP321H, TP347, and TP347H. When specified
4.1.10 Specification designation, and by the purchaser, a lower temperature stabilization or
4.1.11 Special requirements or exceptions to speci- resolution anneal shall be used subsequent to the initial
fication. high temperature solution anneal (See Supplementary
Requirement S10).

5. Materials and Manufacture 5.4.4 The purchaser may specify controlled struc-
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tural or special service characteristics which shall be used


5.1 Discard — A sufficient discard shall be made from
as a guide for the most suitable heat treatment. If the
each ingot to secure freedom from injurious defects and
final heat treatment is at a temperature other than that
undue segregation.
given in 5.4.2, each pipe shall be stenciled with the final
5.2 Manufacturing Practice: heat treatment temperature in degrees Fahrenheit or
5.2.1 Material for forgings shall consist of ingots, degrees Celsius after the suffix “HT”. For “H-Grade”
or of blooms, slabs, or bars either forged or rolled from Code materials, this heat treatment, if at a lower tempera-
an ingot, and cut to the required length by a process that ture than specified in 5.4.2, shall be applied following
will not produce injurious defects in the forging. the heat treatment in 5.4.2.
5.2.2 The material shall be forged by hammering,
pressing, rolling, or extruding, and shall be brought as
nearly as practicable to the finished shape and size by 6. Chemical Composition
hot working. The material shall be adequately worked 6.1 The steel shall conform to the requirements as to
under a tool of sufficient capacity to refine the structure chemical composition prescribed in Table 1.
in the wall of the finished pipe.
5.3 Machining:
5.3.1 All forgings shall have both the inner and 7. Product Analysis
outer surfaces machined. 7.1 At the request of the purchaser, a product analysis
5.3.2 After heat treatment, the pipe shall be of each heat or of two pipes from each lot (Note 3) shall
machined to a finish with a roughness value no greater be made by the manufacturer. A lot of pipe shall consist
than 250 ␮in. [6.4 ␮m] arithmetical average deviation of the following:
(AA), terms as defined in ANSI B46.1, unless otherwise NPS Number of
Designator Lengths of Pipe in Lot
specified.
Under NPS 2 400 or fraction thereof
5.4 Heat Treatment: NPS 2 to NPS 5, incl 200 or fraction thereof
5.4.1 All pipe shall be furnished in the solution- NPS 5 and over 100 or fraction thereof
treated condition unless the order specifically states that
no final heat treatment shall be applied. For H grades, NOTE 3—A lot shall consist of the number of lengths specified in 7.1,
separate solution heat treatments are required for solution of the same size and wall thickness from any one heat of steel.
annealing; in-process heat treatments are not permitted as
a substitute for the separate solution annealing treatments. 7.2 The results of these analyses shall be reported to
When the order is furnished without final heat treatment, the purchaser or his representative, and shall not vary
each pipe shall be stenciled “HT-O”. The purchaser shall from the requirements specified in Table 1 by more than
have the responsibility for completing the heat-treatment the amounts prescribed in Table 2.
requirement. 7.3 If the analysis of any of the tests specified in this
5.4.2 Unless otherwise stated in the order, heat section does not conform to the requirements specified,
treatment shall consist of heating Types FP 321H and FP an analysis of each pipe from the same heat or lot may
347H to a minimum temperature of 1925°F [1050°C]; be made, and all pipe conforming to the requirements
Type FP 16-8-2H to a minimum temperature of 1800°F shall be accepted.

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PART A — FERROUS MATERIAL SPECIFICATIONS SA-430 /SA-430M

8. Tensile Requirements in accordance with 11.1 to be deeper than 5% of the


8.1 The material shall conform to the requirements nominal wall thickness.
as to tensile properties prescribed in Table 3. 11.4 At the purchaser’s discretion, pipe shall be sub-
8.2 Tests for acceptance shall be made after final heat ject to rejection if surface imperfections acceptable under
treatment of the pipe. 11.2 are not scattered, but appear over a large area in
excess of what is considered a workmanlike finish. Dispo-
sition of such pipe shall be a matter of agreement between
9. Workmanship the manufacturer and the purchaser.
9.1 The pipe shall conform to the sizes and shapes 11.5 When imperfections or defects are removed by
specified by the purchaser. grinding, a smooth curved surface shall be maintained,
and the wall thickness shall not be decreased below that
permitted by this specification. The outside diameter at
10. Ends the point of grinding may be reduced by the amount so
10.1 Pipe ends shall be machined as specified in the removed.
purchase order. 11.5.1 Wall thickness measurements shall be made
with a mechanical caliper or with a properly calibrated
nondestructive testing device of appropriate accuracy. In
11. Finish case of dispute, the measurement determined by use of
11.1 The pipe manufacturer shall explore a sufficient the mechanical caliper shall govern.
number of visual surface imperfections to provide reason-
11.6 Weld repair shall be permitted only subject to
able assurance that they have been properly evaluated
the approval of the purchaser and in accordance with
with respect to depth. Exploration of all surface imperfec-
Specification A 530/A 530M.
tions is not required but may be necessary to assure
compliance with 11.2. 11.7 The finished pipe shall be reasonably straight.
11.2 Surface imperfections that penetrate more than
121⁄2% of the nominal wall thickness or encroach on the 12. Mechanical Tests Required
minimum wall thickness shall be considered defects. Pipe
12.1 Transverse of Longitudinal Tension Test —One
with such defects shall be given one of the following
test shall be made on a specimen from one end of one
dispositions:
length of pipe representing each heat in each heat-treat-
11.2.1 The defect may be removed by grinding ment lot.
provided that the remaining wall thickness is within speci-
fied limits. 12.2 Flattening Test —A test shall be made on speci-
mens from one end of each length of pipe.
11.2.2 Repaired in accordance with the repair weld-
ing provisions of 11.6.
11.2.3 The section of pipe containing the defect 13. Product Marking
may be cut off within the limits of requirements on length. 13.1 In addition to the marking prescribed in Specifi-
11.2.4 Rejected. cation A 530/A 530M, the marking shall include the
length, hydrostatic test pressure (when so tested), the
11.3 To provide a workmanlike finish and basis for marking requirements of 5.4, and an additional symbol
evaluating conformance with 11.2, the pipe manufacturer “S” if the pipe conforms to the supplementary require-
shall remove by grinding the following: ments specified in S1 to S10, the heat number or manufac-
11.3.1 Mechanical marks, abrasions, and pits, any turer’s number by which the heat can be identified. On
of which imperfections are deeper than 1⁄16 in. [1.6 mm]. pipe sizes larger than NPS 4, the weight shall be given.
11.3.2 Visual imperfections commonly referred to 13.2 No steel indentation stamping shall be done with-
as scabs, seams, laps, tears or slivers found by exploration out the consent of the purchaser.

807
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SA-430 /SA-430M 2004 SECTION II

TABLE 1
CHEMICAL REQUIREMENTS
FP304 or FP316 or FP321 or FP347 or
Grade FP304H FP304N FP316H FP316N FP321H FP347H FP16-8-2H

Element Composition, %

Carbon 0.04–0.10 0.04–0.10 0.04–0.10 0.04–0.10 0.04–0.10 0.04–0.10 0.05–0.10


Manganese, max 2.00 2.00 2.00 2.00 2.00 2.00 2.00
Phosphorus, max 0.040 0.040 0.040 0.040 0.040 0.040 0.040
Sulfur, max 0.030 0.030 0.030 0.030 0.030 0.030 0.030
Silicon, max 0.75 0.75 0.75 0.75 0.75 0.75 0.75
Nickel 8.00–11.0 8.00–11.0 11.00–14.0 11.00–14.0 9.00–13.0 9.00–13.0 7.50–9.50
Chromium 18.0–20.0 18.0–20.0 16.0–18.0 16.0–18.0 17.0–20.0 17.0–20.0 14.5–16.5
Molybdenum ... ... 2.00–3.00 2.00–3.00 ... ... 1.5–2.0
A
Titanium ... ... ... ... ... ...
B
Columbium ... ... ... ... ... ...
NitrogenC ... 0.10–0.16 ... 0.10–0.16 ... ... ...
A
The titanium content shall be not less than four times the carbon content and not more than 0.60%.
B
The columbium content shall be not less than eight times the carbon content and not more than 1.00%.
C
The method of analysis for nitrogen shall be a matter of agreement between the purchaser and manufacturer.

TABLE 2 TABLE 3
PERMISSIBLE VARIATIONS IN PRODUCT TENSILE REQUIREMENTSA
ANALYSIS
All Grades
Limit, or Permissible Variations,
ksi MPa
Maximum of Over the Maximum Limit
Specified or Under the Minimum Tensile strength, min 70 485
Elements Element, % Limit, % Yield strength, min 30 205
Carbon ... 0.0 Longitudinal Transverse
Manganese ... 0.04
Phosphorus ... 0.005 Elongation in 2 in. or 50 mm, min, % 45 20
Sulfur ... 0.005 Reduction of area, min, % 50 30
Silicon ... 0.05
A
Nickel Over 5.00 to 0.10 For grades FP304N and FP316N the minimum tensile
10.00 incl strength shall be 75 000 psi [550 MPa] and the minimum yield
Over 10.00 to 0.15 strength shall be 35 000 psi [240 MPa].
20.00 incl
Chromium ... 0.20
Molybdenum ... 0.10
Titanium ... 0.0
Columbium ... 0.0

808
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PART A — FERROUS MATERIAL SPECIFICATIONS SA-430 /SA-430M

SUPPLEMENTARY REQUIREMENTS FOR PIPE REQUIRING


SPECIAL CONSIDERATION

One or more of the following supplementary requirements shall apply only when specified
in the purchase order. The purchaser may specify a different frequency of test or analysis
than is provided in the supplementary requirement. Subject to agreement between the
purchaser and manufacturer, retest and retreatment provisions of these supplementary
requirements may also be modified.

S1. Product Analysis shall also be specified. If a specimen from any length
S1.1 Product analysis shall be made on each length of shows objectionable defects, the length shall be rejected,
pipe. Individual lengths failing to conform to the chemical subject to removal of the defective end and subsequent
composition requirements shall be rejected. retests indicating the remainder of the length to be sound
and reasonably uniform material.
S2. Transverse Tension Tests
S2.1 A transverse tension test shall be made on a S5. Photomicrographs
specimen from one end or both ends of each pipe NPS S5.1 Photomicrographs at 100 diameters may be made
8 and over. If this supplementary requirement is specified, from one end of each piece of pipe furnished in sizes 6
the number of tests per pipe shall also be specified. If a in. [152 mm] and larger in the as-furnished condition.
specimen from any length fails to meet the required tensile Such photomicrographs shall be suitably identified as to
properties (tensile, yield, and elongation), that length shall pipe size, wall thickness, piece number, and heat. Such
be rejected subject to retreatment in accordance with photomicrographs are for information only, and shall
Specification A 530/A 530M and satisfactory retest. show the actual metal structure of the pipe as finished.

S3. Flattening Test


S6. Ultrasonic Testing
S3.1 The flattening test of Specification
A 530/A 530M shall be made on a specimen from one S6.1 Each piece of pipe may be ultrasonically tested
end or both ends of each pipe. Crop ends may be used. to determine its soundness throughout the entire length
If this supplementary requirement is specified, the number of the pipe. Each pipe shall be ultrasonically tested in a
of tests per pipe shall also be specified. If a specimen circumferential direction in such a manner that the entire
from any length fails because of lack of ductility prior piece is scanned by the ultrasonic beam. The calibration
to satisfactory completion of the first step of the flattening standard shall be prepared from a section of pipe which
test requirement that pipe shall be rejected subject to has two notches, one in the inside surface and one in the
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retreatment in accordance with Specification outside surface. The notches shall be at least 11⁄2 in. [38
A 530/A 530M and satisfactory retest. If a specimen from mm] long and have a depth of 3% of the wall thickness,
any length of pipe fails because of a lack of soundness or 0.004 in. [0.1 mm], whichever is greater. Any pipe
that length shall be rejected, unless subsequent retesting showing an ultrasonic indication of greater amplitude
indicates that the remaining length is sound. than the amplitude of the indication from the calibration
standard shall be subject to rejection.

S4. Etching Tests


S4.1 The steel shall be homogeneous as shown by S7. Hot Ductility Tests (Weldability Tests)
etching tests conducted in accordance with the appro- S7.1 A high-temperature ductility test may be made
priate portions of Method E 381. Etching tests shall be upon each heat of material supplied in heavy-wall pipe
made on a cross section from one end or both ends of sections. An appropriate specimen shall be heated to an
each pipe and shall show sound and reasonably uniform initial temperature, cooled 100°F [50°C], then subjected
material free from injurious laminations, cracks, and simi- to a tensile test, and shall show a minimum reduction of
lar objectionable defects. If this supplementary require- area of 60%. The initial temperature is that temperature
ment is specified, the number of tests per pipe required 50°F [30°C] below the temperature at which material

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SA-430 /SA-430M 2004 SECTION II

exhibits zero ductility. Rejection of material shall not be lower than that used for the initial solution annealing heat
based upon this test. treatment. The temperature of stabilization heat treatment
shall be at a temperature as agreed upon between the
purchaser and vendor.
S8. Hydrostatic Test
S8.1 A hydrostatic test shall be applied as agreed
upon by the manufacturer and purchaser.
S11. Intergranular Corrosion Test
S11.1 When specified, material shall pass intergranu-
S9. Retests lar corrosion tests conducted by the manufacturer in
S9.1 Upon the purchaser’s request, retests shall be accordance with Practices A 262, Practice E.
made from sections of material removed from any part
NOTE 3—Practice E requires testing on the sensitized condition for
of the pipe. Failure to meet the requirements stated in
low carbon or stabilized grades, and on the as-shipped condition for
the body of this specification shall be cause for rejection. other grades.

S11.2 A stabilization heat treatment in accordance


S10. Stabilization Heat Treatment with Supplementary Requirement S10 may be necessary
S10.1 Subsequent to the solution anneal required is and is permitted in order to meet this requirement for the
5.4, Grades TP321, TP321H, TP347, and TP347H shall grades containing titanium or columbium, particularly in
be given a stabilization heat treatment at a temperature their H versions.

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