External Coatings For Corrosion Protection of Steel Pipes and Components

Eni S.p.A.
Exploration & Production Division
FUNCTIONAL SPECIFICATION
EXTERNAL COATINGS FOR CORROSION

PROTECTION OF STEEL PIPES AND COMPONENTS
20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD
Documento riservato di proprietà di Eni S.p.A. Divisione Agip. Esso non sarà mostrato a Terzi né utilizzato per scopi diversi da quelli per i quali è stato inviato.
This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent.
Eni S.p.A. 20550 PIP.COR.FUN
Page 2 of 20
FOREWORD
Rev 0 Issue
Pages 20
Appendix “A” – Pages 9
Appendix “B” – Pages 10
Appendix “C” – Pages 14
Appendix “D” – Pages 14
Appendix “E” – Pages 9
Appendix “F” – Pages 10
Appendix “G” – Pages 11
Appendix “H” – Pages 11
Appendix “I” – Pages 12
February 2004
This specification replaces the following Company Functional Specifications:
Spray coating of steel pipes external surface with epoxy or

• 20001.PIP.PAI.FUN. Rev.0
polyurethane paint.
External Polyethylene or Polypropylene Coating, Plant Applied on
• 20002.PLI.PAI.FUN. Rev.0
Steel Pipe.
• 20003.PLI.PAI.FUN. Rev.0 External Coating with Plastic Tape for Buried Steel Pipe.
• 20005.PIP.PAI.FUN. Rev.0 External Coal Tar Coating Factory Applied on Steel Pipe.
• 20006.PLI.PAI.FUN. Rev.0 Repair of Damages Found in The Field n Pipe External Coatings.
• 20007.SLI.COR.FUN. Rev.0 External Bitumen Coating, Factory Applied on Steel Pipe.
• 20009.SLI.COR.FUN. Rev.0 External Coating with Epoxy Mastic for Application on Steel Pipes.
• 20012.PLI.PAI.FUN. Rev.0 Supply and Installation of Plastic Tapes.
• 20013.PIP.PAI.FUN. Rev.0 Supply and Installation of Heat Shrinkable Sleeves.
Coated with anticorrosion filler mass of welded joints areas in
• 20014.SLI.NAV.FUN Rev.0
concrete weighthed pipelines.
• 20015.COR.FUN. Rev.0 External coating with epoxy powders factory applied on steel pipes.
Insulation of bonded pipe straight lengths by polyurethane foam
• 20017.SLI.NAV.FUN Rev.0
injection.
Pipe Assembly of Steel Service Pipes, Polyurethane Thermal
• 20018.PLI.COR.FUN Rev.1
Insulation and Outer Casing of High Density Polyethylene.
• 20022.SLI.COR.FUN. Rev.0 External Tar Polyurethane Coating Factory Applied on Steel Pipes.
Assembly of Fittings and Valves for Steel Service Pipes,
• 20023.VAR.PAI.FUN. Rev.0
Polyurethane Thermal Insulation and Outer Casing of Polyethylene.
• 20476.VAR.PAI.FUN Rev.0 Application of Protective Coating on Pipe Welded Joints.
CORM CORM CORM

0 ISSUE 02.2004
M. CORNAGO M. CORNAGO D. CONDANNI
REV. DESCRIPTION PREPARED VERIFIED APPROVED DATE
Page 3 of 20
CONTENTS
1 GENERAL........................................................................................................................... 4
1.1 INTRODUCTION................................................................................................................. 4
1.2 SCOPE................................................................................................................................ 4
1.3 REFERENCE STANDARDS............................................................................................... 4
1.3.1 European standard ............................................................................................................. 6
1.3.2 ISO and National Organisations ......................................................................................... 6
1.3.3 Standards of other Organisations ....................................................................................... 7
1.3.4 Laws and decrees............................................................................................................... 8
1.4 DEFINITIONS ..................................................................................................................... 9
1.5 SYMBOLS AND ABBREVIATIONS .................................................................................... 9
1.6 OPERATING ENVIRONMENT ......................................................................................... 10
2 FUNCTIONAL REQUIREMENTS..................................................................................... 10
2.1 STORAGE AND HANDLING OF BARE PIPES AND RELATED COMPONENTS .......... 10
2.1.1 Storage areas.................................................................................................................... 10
2.1.2 Handling ............................................................................................................................ 10
2.2 COATING MATERIAL STORAGE AND PRESERVATION.............................................. 10
2.3 CRITERIA FOR COATING SYSTEM SELECTION.......................................................... 11
2.4 QUALIFICATION OF THE COATING............................................................................... 11
2.5 SURFACE PREPARATION .............................................................................................. 12
2.5.1 Abrasive materials ............................................................................................................ 14
2.5.2 Steel imperfections ........................................................................................................... 14
2.6 COATING MATERIAL APPLICATION.............................................................................. 14
2.7 ENVIRONMENTAL CONDITIONS ................................................................................... 14
2.8 CUT BACK ........................................................................................................................ 15
2.9 MARKING ......................................................................................................................... 15
2.10 HANDLING, STORAGE AND DELIVERY OF THE COATED PIPES AND RELATED
COMPONENTS ................................................................................................................ 15
2.10.1 Handling ............................................................................................................................ 15
2.10.2 Storage.............................................................................................................................. 15
2.10.3 Delivery ............................................................................................................................. 16
3 SAFETY AND ENVIRONMENTAL PROTECTION.......................................................... 16

3.1 GENERAL SAFETY REQUIREMENTS............................................................................ 16
3.2 SPECIFIC SAFETY REQUIREMENTS ............................................................................ 17
4 REQUIREMENTS FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE ...... 17

4.1 GENERAL ......................................................................................................................... 17
4.2 PRE-JOB MEETING ......................................................................................................... 17
4.3 RECEPTION OF BARE PIPES......................................................................................... 17
4.4 RECEPTION OF COATING MATERIALS ........................................................................ 17
4.5 INSPECTION AND QUALITY CONTROL FUNCTION..................................................... 18
4.5.1 Contractor ......................................................................................................................... 18
4.5.2 Coating Manufacturer ....................................................................................................... 18
4.5.3 Independent Inspection..................................................................................................... 18
4.5.4 Certification of personnel .................................................................................................. 18
4.6 IDENTIFICATION MARKINGS ......................................................................................... 18
4.7 INSPECTION OF PRODUCTION PROCESS .................................................................. 19
4.8 PRELIMINARY TESTS ..................................................................................................... 19
4.9 TESTS DURING THE WORK PROGRESS ..................................................................... 19
4.10 FINAL INSPECTION......................................................................................................... 19
5 DOCUMENTATION AND REPORTING........................................................................... 19

5.1 DOCUMENTS TO PRODUCE AT THE BEGINNING OF WORK .................................... 19
5.2 DOCUMENTS TO PRODUCE DURING WORK PROGRESS......................................... 19
5.3 DOCUMENTS TO PRODUCE AT THE COMPLETION OF WORK................................. 20
Page 4 of 20
1 GENERAL
1.1 INTRODUCTION
This Specification is formed by a general part in which the requirements, common to all
coatings and systems, are described and by 9 Appendixes, identified with letter “A” to “I“. In
each Appendix the requirements for a specific coating or coating system, and for a specific
method of application, are described.
1.2 SCOPE
This Specification defines the minimum functional requirements related to coating works,
including supply, characterisation, inspection and testing of protective coatings intended to be
applied on the exterior surfaces of steel pipes, including sealines, pipelines, and buried pipes,
etc. and related components and fittings as band, valves, etc.
According to the requirements of this specification, a “Project Technical Specification” shall be
prepared, which must include consideration of the following factors:
• The intended service of the pipes (sealine, buried, temperature, etc.);
• The specific needs of the project;
• The coating system selected;
• The application method.
Based on the requirements of Project Technical Specification, the Contractor shall prepare a
“Working Procedure” in which methods concerning each work and activity (e.g. abrasive
blasting, coating application, cleaning, coating systems selected, inspections, etc.) must be
described in detail. Since the performance of the coating can be significantly affected by the
quality of work execution (e.g. surface preparation, application of various coats, procedures
and inspections) the requirements that must be implemented during intermediate steps of
coating operations, should also be described.
Before coming into force, the “Working Procedure” shall be approved by the Company.
As a general rule, recommendations and instruction listed in Product Data Sheets published by
Coating Manufacturers shall be followed. Possible conflicts and/or discrepancies between
Products Data Sheets and this specification shall be submitted to the Company for resolution,
and approval for all changes shall be obtained.
In Figure 1 the general scheme for the development of the coating project is reported for
information only.
1.3 REFERENCE STANDARDS

This Specification refers to the most recent issue of the standards listed below, which become
an integral part of the specification and all related contractual documents.
In the Appendixes of this Specification, reference standards applicable to the specific coating
system, application method and testing are listed.
It is the Contractor’s duty to have copies of the standards applicable to each project and
provide copies of each relevant standard whenever work takes place. Contractor shall provide
evidence of provision of standards to the Company before work begins and make standard
available during each inspection step.
Page 5 of 20
Figure 1 - Scheme for the devolpment of the coating project
Functional Specification
20550 PIP.COR.FUN. List of Company's
Rev.0 qualified systems
Operative Service
Project Technical
Evaluation of the Coating system
PROJECT Temperature Specification
requirements selection
Environment
No Contractor
QCP Company Working Procedure

Construction PQT Yes
approval
Page 6 of 20
1.3.1 European standard

EN 253 District heating pipes – Preinsulated bonded pipe systems for directly buried
hot water networks- Pipe assembly of steel service pipe, polyurethane thermal
insulation and outer casing of polyethylene.
EN 448 District heating pipes – Preinsulated bonded pipe systems for directly buried
hot water networks- Fitting assemblies of steel service pipe, polyurethane
thermal insulation and outer casing of polyethylene.
EN 10288 Steel tubes and fittings for onshore and offshore pipelines – External two layer
extruded polyethylene based coatings.
EN 10289 Steel tubes and fittings for onshore and offshore pipelines – External liquid
applied epoxy and epoxy-modified coatings.
EN 10290 Steel tubes and fittings for onshore and offshore pipelines – External liquid
applied polyurethane and polyurethane-modified coatings.
EN 12068 External organic coating for the corrosion protection of buried or immersed
steel pipelines used in conjunction with cathodic protection: Tapes and
shrinkable materials.
1.3.2 ISO and National Organisations

ISO 62 Plastics – Determination of water absorption.
ISO 527-2 Plastics – Determination of tensile properties – Part 2: Test conditions for
moulding and extrusion plastics.
ISO 868 Plastics and Ebonite – Determination of indentation by means of durometer
(Shore hardness).
ISO 1133 Plastics – Determination of the melt mass-flow rate (MFR) and the melt
volume-flow rate (MVR) of thermoplastic.
ISO 1183 Plastics, Methods for determining the density and relative density of non
cellular plastics.
ISO 1512 Paints and varnishes – Sampling of products in liquid or paste forms.
ISO 1513 Paints and varnishes – Examination and preparation of samples for testing.
ISO 1514 Paints and varnishes – Standard panels for testing.
ISO 1515 Paints and Varnishes – Determination of volatile and non volatile matter.
ISO 1516 Paints and varnishes – Closed cup equilibrium method.
ISO 1517 Paints and Varnishes – Surface drying test – Ballotini method.
ISO 1519 Paints and varnishes – Bend test (cylindrical mandrel).
ISO 1521 Paints and Varnishes – Determination of resistance to water – Water
immersion method.
ISO 1524 Paints and varnishes – Determination of fineness of grind.
ISO 2409 Paints and varnishes – Cross-cut test.
ISO 2431 Paints and varnishes – Determination of flow time by use of flow cups.
ISO 2555 Resins in the liquid state or as emulsions or dispersions. Determination of
Brookfield RV viscosity.
ISO 2811 Paints and varnishes – Determination of density.
ISO 2815 Paint and Varnishes – Buchholz indentation test.
Page 7 of 20
ISO 3001 Plastics and Ebonite – Epoxide compounds – Determination of epoxide

equivalent.
ISO 3231 Paints and varnishes – Determination of resistance to humid atmospheres
containing sulphur dioxide.
ISO 3233 Paints and varnishes – Determination of volume of dry coating (non-volatile
matter) obtained from a given volume of liquid coating.
ISO 3251 Paints and varnishes –Determination of non-volatile matter of paints,
varnishes and binders for paints and varnishes.
ISO 4287 Geometrical Product Specification (GPS) – Surface texture: Profile method –
Terms, definitions and surface texture parameters.
ISO 4624 Paints and varnishes – Pull-off test.
ISO 6270 Paints and varnishes – Determination of resistance to humidity.
ISO 4892-2 Plastics, Methods of exposure to laboratory light sources – Part 2: Xenon-arc
sources.
ISO 7523 Paints and varnishes – Determination of resistance to neutral salt spray.
ISO 8501 Preparation of steel substrates before application of paints and related
Parts 1 ÷ 3 products. - Visual assessment of surface cleanliness.
ISO 8503 Paints and varnishes – Preparation of steel substrates before application of
Parts 1 ÷ 4 paints and related products. Surface roughness characteristics of blast-
cleaned steel substrates.
Parts 1 ÷ 3 paints and related products. Surface preparation methods.
ISO 8502 Preparation of steel substrates before application of paints and related
Parts 1 ÷ 10 products. - Test for the assessment of surface cleanliness.
ISO 9227 Corrosion tests in artificial atmospheres – Salt Spray tests.
Part 1 ÷ 4 paints and related products. Specifications for metallic blast-cleaning
abrasives.
Parts 1 ÷ 7 paints and related products. Test methods for metallic blast-cleaning
abrasives.
Parts 1 ÷ 8 paints and related products. Specifications for non-metallic blast-cleaning
abrasives.
Parts 1 ÷ 7 paints and related products. Test methods for non-metallic blast-cleaning
abrasives.
ISO 11420 Methods for the assessment of the degree of carbon black dispersion in
polyolefin pipes, fittings and compounds.
ISO 12944 Paint and varnishes. Corrosion protection of steel structures by protective
Parts 1 ÷ 8 paint systems.
1.3.3 Standards of other Organisations

ASTM D 570 Standard test method for water absorption of plastics.
ASTM D 638 Standard test method for tensile properties of plastics.
ASTM 746 Standard test method for brittleness temperature of plastics and
elastomers by impact.
Page 8 of 20
ASTM A 780 Specification for repair of damaged hot-dip galvanized coatings.

ASTM D 823 Method of producing films of uniform thickness of paint, varnish, lacquer
and related products on test panels.
ASTM D 1000 Method of testing pressure sensitive adhesive coated tapes used for
electrical insulation.
ASTM D 1141 Specification for substitute ocean water.
ASTM D 1200 Test method for viscosity of paints, varnishes and lacquers by Ford
viscosity cup.
ASTM D 1525 Standard Test Method for Vicat Softening Temperature of Plastics.
ASTM D 1640 Drying, Curing or film formation of organic coatings at room temperature.
ASTM D 2240 Standard Test Method for Rubber Property - Durometer Hardness.
ASTM D 2369 Test method for volatile content of coatings.
ASTM D 2371 Test method for pigment content of solvent-reducible paints.
ASTM D 3359 Method for measuring adhesion by tape test.
ASTM 3418 Standard test method for transition temperatures of polymers by differential
scanning calorimetry.
ASTM D 4060 Standard test method for abrasion resistance of organic coatings by the
Taber abraser.
ASTM D 4285 Test method for indicating oil or water in compressor air.
ASTM D 4541 Test method for pull-off strength of coatings using portable adhesion
testers.
ASTM D 4940 Test method for conductimetric analysis of water-soluble ionic
contamination of blasting abrasives.
ASTM G 8 Test method for cathodic disbonding of pipeline coatings.
ASTM G 53 Recommended practice for operating light – and water – exposure
apparatus (fluorescent UV-condensation type) for exposure of non-metallic
materials.
NACE RP0188 Discontinuity (holiday) testing of protective coatings.
NACE RP0287 Field measurement of surface profile of abrasive blast cleaned steel
surfaces using replica tape.
NACE RP0394 Application, performance, and quality control of plant-applied, fusion-
bonded epoxy external pipe coating.
NACE RP0490 Holiday detection of fusion-bonded epoxy external pipeline coatings of
(0,25 mm to 0,76 mm).
SSPC-PA 2 Measurement of dry coating thickness with magnetic gauges.
SSPC-SP 1 Solvent cleaning.
1.3.4 Laws and decrees

Italian Health Minister Decree No. 50 dated 16th February 1993.
(Ministero della Sanità)
Italian Internal Minister Circular No. 2838/4112 dated 20th May 1996.
(Ministero degli Interni)
Any other local law, decree and regulation where the coating work is performed.
Page 9 of 20
1.4 DEFINITIONS
• Coating Manufacturer: The manufacturer or supplier of the coating material intended to
be applied on the pipes or components.
• Coating material: The liquid, liquefiable, mastic, powder or any other composition
and material intended to be applied on the pipes or
components.
• Coating system: The complete number and type of coats applied to a substrate
in a predetermined order.
• Coating: The liquid, liquefiable, mastic, powder or any other composition
and material that after application to a substrate, is converted
into a solid protective adherent film.
• Cut-back: The pipe surface (dimension) to be left bare (uncoated) at both
ends of each pipe.
• Dry-spray: Phenomenon that may occur during paint application by spray.
Dry particles (dusting) of atomised paint fall over areas already
coated or to be coated, but not yet dried, making surface rough
and matt. If overcoated can cause possible adhesion problem.
• Material Safety Data Document published by Coating Manufacturer.
Sheet:
• Product Data Sheet: Document published by Coating Manufacturer describing
product characteristics, use, application and storage
instructions.
• Stripe–coat: Additional coat of paint applied usually by brush on difficult-to-
reach areas and on weld seams, edges, bolts, nuts, etc, to
provide specified film thickness.
• Substrate: Solid surface intended to be coated or lined with the specified
coating system.
• Thermo-Hygrometric Environmental conditions detected during coating work.
Condition:
1.5 SYMBOLS AND ABBREVIATIONS

• DFT Dry thickness of a coating present on surface after the complete
(Dry Film Thickness) drying of the product.
• WFT Wet thickness of the coating present on surface at the time of
(Wet Film Thickness) its application.
• N.A. Not Applicable.
• ISO International Organization for Standardization.
• ASTM American Society for Testing and Materials.
• SSPC The Society for Protective Coatings.
• NACE NACE International, formerly the National Association of
Corrosion Engineers.
• DIN Deutsches Institute fur Normung.
• EN European Norms.
• UNI Ente Nazionale Italiano di Unificazione.
Page 10 of 20
1.6 OPERATING ENVIRONMENT

Pipes, components and fittings coated according to the requirements of this Specification and
Appendixes, during the service may be located in various geographic locations and in a variety
of environmental and service conditions.
In each Appendix, suitable operating environments and service conditions for the specific
coating or coating system and for the specific method of application are described in detail.
2 FUNCTIONAL REQUIREMENTS
2.1 STORAGE AND HANDLING OF BARE PIPES AND RELATED COMPONENTS
2.1.1 Storage areas

Area(s) intended for the storage of pipes, components and fittings shall meet the following
requirements:
a) They shall be at least 30 m away from any type of electric power cable. The distance shall
be measured along the ground from the vertical projection to the ground of the nearest
cable;
b) Shall be free from any kind of vegetation (e.g. grass, weed, shrubs, etc). A surrounding
area of sufficient width to prevent fire spreading to the pipe stacks shall also be free of
vegetation;
c) Shall be free of prominent stones and other foreign matter that may damage the pipe or
components;
d) Shall be levelled, in order to allow uniform loading of the supports and ensure stack
stability;
e) Shall have sufficient load bearing capacity to prevent pipe sinking into contact with the
ground;
f) Shall never be directly exposed to salt water spray.
2.1.2 Handling
All stacking operations shall be performed using suitable lifting equipment (such as cranes,
overhead or other lift trucks) with adequate slings and hooks. Hooks for lifting pipes from their
ends shall be equipped with a rubber or copper sheathing in order to avoid damages to pipe
and end bevels.
Suspended pipes shall be provided with appropriate side guide ropes to the lifting equipment,
to prevent the traverse of the pipes.
During handling operation the pipes shall not knock or bump against other obstacles or pipes.
The positioning of the pipes on those already stacked shall be performed with greatest care.
Slings and hooks shall also neither strike nor scrape the pipes.
Suitable flat wooden supports shall be positioned on the ground. The first and last wooden
supports shall be positioned at least at 0,5 m from the pipe end.
2.2 COATING MATERIAL STORAGE AND PRESERVATION

All coating materials must be properly stored in the Contractor’s facility.
The following minimum requirements must be satisfied:
a) The store shall be appropriately ventilated and comply with provisions law in force
concerning safety and fire prevention;
b) Coating materials (liquid, solid or packaged) shall be kept in their original sealed and
labelled containers or package;
Page 11 of 20
c) Coating materials shall be protected from direct sun, frost and rain, stored in a thermally
controlled store with constant temperature in the range of +15 to +25°C;
d) The coating materials store shall be located at a proper distance from any significant heat
source and from any area where free flames, welding works, and tools causing sparks are
used;
e) Containers and packages shall not be placed nor stored on wet or damp surfaces, nor in
areas where flood can occur;
f) All products that become altered for any reason or show the container and/or package
partially or totally destroyed and/or damaged shall be removed from the store, not used for
the coating work and properly disposed of;
g) Coating materials shall be stored and used in a manner that assures that products are
used within their storage limits (shelf-life), and those stored first are the first used.
2.3 CRITERIA FOR COATING SYSTEM SELECTION

Performance criteria for specific coating systems are defined in the appropriate Appendix. To
select the most suitable system for a project the following basic criteria have to be considered:
a) Project needs and requirements;
b) Environmental service exposure (seawater, soil, other);
c) Service temperature.
2.4 QUALIFICATION OF THE COATING

Only coating materials qualified and approved by the Company shall be selected and applied.
The coating materials shall be purchased directly from a Coating Manufacturer qualified by the
Company.
Qualification requirements shall apply to all coating materials and systems described in the
Appendixes of this Specification, as well as to the repair products. In each Appendix the
requirements for the qualification of the specific coating material and system are described.
As a general rules, two test levels are requested, divided as follows:
a) Tests for the characterisation of the coating material;
b) Tests for the characterisation of the coating system to verify its suitability and
performance in the intended environment and service.
All tests and analysis required by this Specification and by related Appendixes shall be
performed and suitably reported by independent laboratories qualified and approved by the
Company.
The qualification of a coating material or coating system is not binding for the Company, which
shall select, at its sole discretion, coatings that are added to the qualified coatings list.
The Company’s qualification is given for an open-ended term. However the Company reserve
the right to require at any time the repetition of one or more of the qualification tests in order to
verify the quality of the coating or as consequence of possible coating failure. If the result of
one or more tests is negative, the qualification will be cancelled.
Any modification to the formulation or components of a coating material or system, even if
considered minor, made by the producer after the qualification, shall be notified in writing to
the Company. The Company reserves the right to require the performance of part or all of the
test procedure, or to accept or reject the modified product, without further tests. The modified
coating material or system - when qualified - may be used in place of the previous one or as
an alternative.
The Contractor is obliged to select the specific coating material(s) from the list of products
qualified by the Company for the specific use.
Page 12 of 20
Under no circumstance the Company approval of a coating system shall be considered a

guarantee from the Company related to the coating materials and repair products and they
performance, but just an approval to use it.
The process steps for the pre-qualification and qualification of coating materials and coating
systems are shown in Figure 2, which is provided for information and clarification only.
2.5 SURFACE PREPARATION

Surface preparation method shall be selected in accordance with standard ISO 8504-1 and in
conformance with the recommendations of standard ISO 12944-4.
As general rule, all surfaces to be coated shall be cleaned to the specified preparation grade to
obtain a surface that meets the requirements defined the appropriate Appendix.
Before any surface preparation (abrasive blasting, power tooling, etc.) oil, grease and other
visible contaminants, shall be removed with suitable detergents according to SSPC-SP1
standard. Petroleum, kerosene, naphtha or other greasy solvent shall not be used.
At completion of surface preparation, and in any case before application of coating materials,
the amount of water-soluble salts (chlorides) on surfaces shall not be more than 5 µg/cm²
(micrograms per square centimetre). Extraction of contaminants from surface shall be done
according to standard ISO 8502-6. Quantitative determination of water-soluble salts shall be
performed according to standard ISO 8502-9.
No surface preparation shall be performed on surfaces that are moist or may become moist
before application of the coating.
Blast cleaned surfaces may not be washed with acids, detergents or solvent solutions, nor
treated with rust inhibitors, unless otherwise specified.
Surface preparation, shall be always carried out by abrasive blasting according to the
recommendation of standard ISO 8504-2.
Page 13 of 20
Figure 2
Schematic process for the pre-qualification and qualification of coating materials and coating system
ENI Data
evaluation
Document for pre-
qualification of each
coating material and
system
Comments
Negative (Positive or
Negative)
Coating
Manufacturer
Data, information and

sample for testing Positive
ENI
Independent Testing schedule
Laboratory
Steel samples
Inspection
preparation
Lab test
execution
Report of the tests Data

evaluation
Comments
Negative (Positive or
Negative)
Coating materials
Positive
and coating systems
qualified
Page 14 of 20
Preparation grade will conform to the specified requirements of specific coating materials listed
in the Appendixes and in any case according to standard ISO 8501-1.
Profile of abrasive blasted surface shall conform to the specified requirement listed in the
Appendix for the specific coating system and measured according to standard ISO 8503 or to
NACE RP 0287.
2.5.1 Abrasive materials

All abrasive material used for blasting shall be dry and clean and shall be tested for soluble
salts content. Conductivity measured according to standard ASTM D-4940, shall not exceed
150 µS/cm (microSiemens per centimetres) and chloride content, shall be less than 25 ppm.
Non-metallic abrasives shall meet the requirements of standard ISO 11126 Parts 1÷8. Tests
and controls shall be done according to standard ISO 11127 Part 1÷7.
Metallic abrasives shall meet the requirements of standard ISO 11124 Parts 1÷4. Tests and
controls shall be done according to standard ISO 11125 Part 1÷7.
Abrasive type and size shall be selected in order to assure the required profile and roughness
of substrate.
In no circumstance will use of silica abrasive be allowed.
2.5.2 Steel imperfections

All surface imperfections of substrate detected before or during surface preparation shall be
removed with suitable power tools according to the requirement of standard ISO 8501-3 as
follows:
• Grade P3 for all pipes, components and fitting projected for immersion service (permanent
or intermittent) or buried;
• Grade P2 for all pipes, components and fitting that will be used in marine and industrial
environments.
Welding shots, drops and spatters, pores in welding seams, lamination defects, edges, flame
cuts, fragments and dents or any other foreign material not removed during construction are
considered to be imperfections, and shall be removed.
Spot and discontinuous welds are not permitted on these surfaces.
2.6 COATING MATERIAL APPLICATION

In general before the application of any coating material, all surfaces shall be dry and free of
rust, grease, oil, dust and dirtiness, soluble salts and any other foreign material. Coating
materials must be applied to the blast cleaned pipes before any oxidation appears. Surfaces
that show visible oxidation or deterioration shall be re-prepared.
In particular all coating materials application shall be performed according to Coating
Manufacturer’s recommendations reported in the product data sheet of each material and
according to the specified requirements listed in the appropriate Appendix.
Any conflict between product data sheets and Company requirements listed in the Appendixes
shall be submitted to the Company for approval.
2.7 ENVIRONMENTAL CONDITIONS

Surface preparation shall not be carried out when the steel temperature is less than 3°C above
dew point or when the relative humidity of the air is greater than 85%.
No coatings shall be applied when the steel temperature is less than 3°C above dew point,
when the relative humidity of the air is greater than 85%, or when the air temperature is less
than 10°C, excluding those products which are suitable for application at low temperature.
Environmental conditions shall be measured according to standard ISO 8502-4.
Page 15 of 20
In outdoor application, no coating materials shall be applied when there is a likelihood of a

detrimental weather change within two hours after application.
The contractor shall supply all necessary weather protection and any other equipment to
ensure that the coating works are carried out according to this specification and agreed
production programme.
Where preheating is required the specific requirements defined in the appropriate Appendix
must be carefully followed.
2.8 CUT BACK

Cut back dimension are specific to each coating. The requirements related to the cut back are
detailed in the relevant Appendix.
As general rule, before coating application the Contractor shall properly protect the end areas
and the pipe bevel that must remain perfectly clean and free from any traces of coating.
Once the coating operations are completed these bare ends shall be temporarily protected
from corrosion, using only products that are easily removable by brushing.
If not specified in the order or other contractual documents, the Company shall approve the
materials used for temporary protection.
2.9 MARKING
All pipes shall be identified with specific and unique markings.
The Contractor shall restore any original markings that may have been removed by the coating
process, according to Company instructions.
Markings shall be applied using indelible paint.
2.10 HANDLING, STORAGE AND DELIVERY OF THE COATED PIPES AND RELATED
COMPONENTS
2.10.1 Handling
Handling shall be carried out using suitable equipment, provided with the proper protective
sheathing, in order to avoid damages to the pipes and/or to the coating. Use of steel ropes or
slings or any equipment, which could damage the coating and the ends, shall be prohibited.
All personnel involved in the handling operations shall be of proven experience and adequately
trained.
Handling operations and equipment shall strictly comply with the applicable safety rules and
laws.
At completion of coating work the minimum time before handling, storage and loading of
coated pipes shall be fully in accordance with the instructions reported in Product Data Sheet
published by the Coating Manufacturer, to the specific requirements mentioned in the relevant
Appendix and any particular instruction provided by the Company.
2.10.2 Storage
Area(s) intended for the storage of the pipes and components shall meet the following
requirements:
a) They shall be at least 30 m away from any type of electric power cable. The distance shall
be measured along the ground from the vertical projection to the ground of the nearest
cable;
b) Shall be free from any kind of vegetation (e.g. grass, weed, shrubs, etc). A surrounding
area of sufficient width to prevent fire spreading to the pipe stacks shall also be free of
vegetation;
Page 16 of 20
c) Shall be free of prominent stones and other foreign matter that may damage the coatings;
d) Shall be levelled, in order to allow uniform loading of the supports and ensure stack
stability;
e) Shall have sufficient load bearing capacity to prevent pipe sinking into contact with the
ground;
f) Shall never be directly exposed to salt water spray.
Stacks of coated pipes and components intended to be stored for a long period shall be
protected from the action of ultraviolet radiation and direct heat.
Stacks shall have a maximum height of 3 m, excluded the dimensions of bottom and
intermediate supports. In consideration of the type of the ground (cement slab, compressed
rock, soil, etc) the support shall provide sufficient distance from the ground and shall be
sufficient in size and number to avoid permanent deformation and to provide proper load
distribution.
As a general rule, the maximum allowable number of rows is as follows:
• For pipes of diameter up to 12" (323 mm): No. 6;
• For pipes with diameter between 14" (355 mm.) and 20" (508 mm.): No. 4;
• For pipes with diameter over 36" (915 mm.): No. 1.
2.10.3 Delivery
Coated pipes and components shall be visually inspected before delivery, and any damage
shall be repaired according to the requirements reported in the Appendix for the specific
coating.
Handling of coated pipes for loading shall be done fully in accordance with the requirement of
previous item 2.9.1.
Loading of pipes and components in the factory or in the field shall be done with particular care
to avoid damages to the pipes, components and to the coating during transportation.
Pipes having a diameter under 80 mm (3 in) shall be shipped in bundles strapped in at least 4
or 5 points using strong, possibly non metallic, straps at least 25 mm wide.
Careful visual inspections shall be performed after transportation, and all pipes and
components showing damages and/or surface defects shall be properly repaired according to
the requirements of the Appendix for the specific coating.
Coating flattened due to stacking on wooden bearing pieces shall retain at least 67% of their
former thickness, or repairs shall be made.
3 SAFETY AND ENVIRONMENTAL PROTECTION
3.1 GENERAL SAFETY REQUIREMENTS

The Company, in consideration of its policy for Safety and Environmental protection, forbids
the use of any coating material containing tar and any abrasive material considered hazardous
to health for the operators.
The Contractor shall observe the rules, laws and regulations on health, safety and
environmental protection applicable to his premises, or in the country where the works are
performed.
Page 17 of 20
All coating materials, solvents, curing agents, etc. shall report on their containers, data
required by local laws and rules, and shall be accompanied by the related Material Safety Data
Sheets.
3.2 SPECIFIC SAFETY REQUIREMENTS

Safety requirements must be carefully observed during handling and application of each
coating according to Material Safety Data Sheets and Product Data Sheets published by
Coating Manufacturers.
Special attention is to be given to the following items:
• Mixing and handling of coating material shall be performed in areas that are not judged to
be dangerous and where air can circulate freely;
• Blast cleaning abrasives shall not be harmful to operators' health;
• Storage of coating material shall be done as reported in item 2.2 of this Specification;
• Disposal of residual materials (spent abrasives, coating materials, solvent, etc.) shall be
performed fully in accordance with rules, regulations and laws in force in the country
where the coating work is performed.
4 REQUIREMENTS FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE
4.1 GENERAL
Contractor must comply with all Requirements for Quality Management and/or Quality
Assurance that are defined in the applicable “Quality and Execution Requirements
Specification” attached to the invitation to bid.
Before starting any coating work the Contractor shall submit for approval to the Company the
procedures relevant to the qualification tests and to the proposed methods of execution of the
works, applicable for the specific coating process.
4.2 PRE-JOB MEETING

Before the beginning of the works a pre-job meeting shall be held with attendance of the
representatives of all involved parties (Company, Contractor, Coating Manufacturer,
Subcontractors and Third-Party Inspector) The purpose of the meeting is to clarify and agree
the production procedures, qualification tests, checks and inspections program, report forms
and any other necessary requirements to achieve the correct job execution.
4.3 RECEPTION OF BARE PIPES

Upon receiving the pipes to be coated, the Contractor shall first verify that the pipes are not
damaged and are free of any visible defect.
Damages and defects, including but not limited to, dents, cuts or scratches on the bevel, shall
be immediately recorded on the shipping documents, reporting the serial number of the pipe(s)
concerned.
Damaged or non-conforming pipes and components shall be set aside. A detailed report of the
damage must be prepared and submitted to the Company, which shall provide instructions for
repair or disposal of the damaged pipes and components.
4.4 RECEPTION OF COATING MATERIALS

The Contractor shall ensure that coating materials purchased and supplied comply with the
specified requirements.
The Contractor shall file and retain for at least 3 years all the technical and administrative
documents related to the purchase, both those issued by himself and by the Coating
Manufacturer.
Page 18 of 20
All coating materials shall be delivered to the job site in their original containers with intact
labels and seals. The containers shall be provided with identifying documents clearly stating
their content and shelf life.
4.5 INSPECTION AND QUALITY CONTROL FUNCTION
4.5.1 Contractor
The Contractor shall nominate the inspector responsible for performing quality control
functions according to the Quality Control Plan (QCP). The inspector shall have adequate
experience of the specific coating process. A statement of the inspector’s name and a listing of
appropriate experience shall be included with the QCP when submitted for approval, and shall
be subject to the approval of the Company.
The Contractor’s inspector shall perform all necessary QC checks and tests to ensure that
work complies with the requirements of the approved QCP and with the Company’s
specification.
4.5.2 Coating Manufacturer

The Coating Manufacturer shall provide technical support whenever work is performed.
The Coating Manufacturer shall verify that the coating process meets written technical
requirements, and shall, through visits and inspections as necessary, confirm that completed
work complies with the specified requirements.
4.5.3 Independent Inspection

In addition to the in-house inspector defined in item 4.5.1 above, the Contractor shall appoint
an independent, third-party inspector, who shall verify and confirm that the execution of every
working step, from storage of bare pipes to the final inspection and delivery, complies with the
requirements of this specification and the appropriate Appendix(s). The appointment of the
third-party inspector shall be subject to approval by the Company.
The independent inspector shall verify the Contractor’s QC testing, and provide written reports
that are submitted to both the Contractor and the Company, and to the Coating Manufacturer
when requested.
4.5.4 Certification of personnel

All personnel involved in the inspection process and defined in items 4.5.1, 4.5.2 and 4.5.3
shall be NACE International or FROSIO Certified, and shall have adequate experience of the
specific coating process.
4.6 IDENTIFICATION MARKINGS

Before starting any work, the Contractor shall have the Packing List of the pipes and
components to be coated. If the Packing List is not yet available, the Contractor shall request
and obtain it before starting the work.
The serial numbers shall be compared and reconciled with those reported in the Packing List,
identifying any inconsistencies and discrepancies. In case the anomaly noticed cannot be
resolved (e.g. lack of serial number) a report shall be submitted to the Company in writing.
Before starting the work the serial numbers shall be marked in such way that the identification
can be maintained thorough the coating process (e.g. with indelible paint on the inside surface
of pipe).
This serial number shall follow the pipe or components in all production steps and is an
integral part of the final marking procedure. It shall be recorded on all production documents
and on the quality control certificates.
Page 19 of 20
If no original serial number can be found or traced for any pipe or component, the Contractor
shall assign a special serial number or sequence of serial numbers to such items.
4.7 INSPECTION OF PRODUCTION PROCESS

Contractor shall provide a suitable organisation, able to perform the following tasks:
• Prepare a work procedure describing in detail the various activities to be performed,
including the proper equipment to be used, an adequate work environment, compliance
with reference standard and rules and with specific Company requirements;
• Monitor and check specific characteristics of any production process.
4.8 PRELIMINARY TESTS

The following tests/inspections shall be performed before start the coating work. Verify:
• Storage of the pipes;
• Storage of coating material;
• Containers and packaging integrity;
• Shelf life validity of coating materials;
• Compliance of all documents (shipping, packing list identification, marking etc.).
4.9 TESTS DURING THE WORK PROGRESS

During the works progress, Contractor shall perform all inspections and tests detailed in each
Appendix related to the coating and application method.
All data concerning each inspection step shall be permanently recorded in reports or a
logbook.
4.10 FINAL INSPECTION

When coating work is finished, the Contractor shall perform all final inspections and tests
detailed in each Appendix related to the coating and application method.
All data concerning each inspection step shall be permanently recorded in reports or a
logbook.
5 DOCUMENTATION AND REPORTING
5.1 DOCUMENTS TO PRODUCE AT THE BEGINNING OF WORK

Prior to start the activity the Contractor shall submit to the Company documents that describe
the following:
• Working method(s);
• Plan and schedule of operations for surface preparation and coating;
• Characteristics of storage area and location where the coating materials will be stored;
• Plan of inspection and administrative controls to be performed before, during and after
operations;
• Type of coating materials that will be used.
5.2 DOCUMENTS TO PRODUCE DURING WORK PROGRESS

During work progress, the Contractor must keep a working Data Log, which shall be available
any time to the Company, as well as reports and information required by item 4. of this
specification and by the specific requirements of the relevant Appendix.
Page 20 of 20
Furthermore, the product and material safety data sheets for each product used shall be
available.
5.3 DOCUMENTS TO PRODUCE AT THE COMPLETION OF WORK

When work is completed the Contractor shall prepare a final report including following data:
• Surface preparation characteristics;
• Trade name and characteristics of the coating used;
• Test certificates of the coating materials, divided by batch numbers;
• Sequence of coating application;
• Atmospheric and thermo-hygrometric conditions;
• Inspections and tests performed and the relevant results, including final acceptance
reports;
• Repairs (if any).
Eni S.p.A.
APPENDIX “A”
FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF
LIQUID EPOXY AND EPOXY-MODIFIED COATINGS ON EXTERNAL SURFACES OF
STEEL PIPES AND COMPONENTS
20550 PIP.COR.FUN
Rev. 0 February 2004
Appendix “A” - Page 2 of 9
CONTENTS
APPENDIX “A” ....................................................................................................................................... 1
1 GENERAL........................................................................................................................... 3
1.1 INTRODUCTION................................................................................................................. 3
1.2 SCOPE................................................................................................................................ 3
2 GENERAL COATING CHARACTERISTICS ..................................................................... 3
3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM .......................... 3

3.1 GENERAL CRITERIA ......................................................................................................... 3
3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING ......................... 4
3.3 COATING MATERIALS CHARACTERISATION TEST ...................................................... 4
3.3.1 Labelling.............................................................................................................................. 4
3.3.2 Required product information.............................................................................................. 4
3.4 COATING SYSTEM CHARACTERISATION TESTS ......................................................... 5
3.4.1 Preparation of steel samples .............................................................................................. 5
3.4.2 Qualification tests................................................................................................................ 6
3.5 FINAL REPORTING OF LAB.............................................................................................. 7
4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 7
5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................... 8

5.1 PREHEAT ........................................................................................................................... 8
5.2 SURFACE PREPARATION ................................................................................................ 8
5.3 COATING APPLICATION................................................................................................... 8
5.3.1 Wet Film Thickness (WFT) and Dry Film Thickness (DFT) ................................................ 8
5.4 CUT BACK .......................................................................................................................... 8
5.5 REPAIR OF DEFECTS....................................................................................................... 9
6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE........... 9

6.1 GENERAL ........................................................................................................................... 9
6.2 QUALITY CONTROL PLAN................................................................................................ 9
6.3 TESTS DURING THE WORKS PROGRESS AND FINAL INSPECTION.......................... 9
7 DOCUMENTATION AND REPORTING............................................................................. 9

1 GENERAL
1.1 INTRODUCTION
This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0
and for no reason can be used separately. All requirements, standards and articles reported in
the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix.
It refers to European Standard EN 10289 (Steel tubes and fittings for onshore and offshore
pipelines – External liquid applied epoxy and epoxy-modified coatings), the content of which
must be considered an integral part of this Appendix.
Moreover, the Company’s additional functional requirements for pre-qualification and
application of the coating are defined.
1.2 SCOPE
This Appendix defines the minimum functional requirements for qualification, supply and
application of liquid epoxy and epoxy-modified tar-free coating to external surfaces of steel
pipes and components for onshore and offshore services as defined in Item 1 of standard EN
10289.
The coating system assumed by this Appendix is the Type 3: -20°C to +80°C, thickness class
“C” (1.500 µm) of standard EN 10289.

This Appendix refers to the most recent version of the standards listed in the Functional
Specification 20550 PIP.COR.FUN Rev. 0.
All listed standards become an integral part of this Appendix and all related contractual
documents.
It is Contractor’s duty to have copies of the standards applicable to each project and provide
copies of each relevant standard whenever work takes place. Contractor shall provide
evidence of provision of standards to the Company before work begins and during each
inspections step.
2 GENERAL COATING CHARACTERISTICS

The coating systems considered in this Appendix are two-pack liquid products, solvent free,
and composed of a base (epoxy resin) and curing agent that can be applied by brush or
spatula, airless spray or plural-components spray equipment in high thickness and that harden
rapidly in air.
The coating materials can be applied at ambient temperature over + 5°C with a Dry Film
Thickness (DFT) of 1.500 µm when applied by brush or spray showing a continuous and
uniform film free of sags, runs or any other visible defect.
3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM
3.1 GENERAL CRITERIA

All requirements provided in Item 2.4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0
must be fully followed.
Qualification requirements shall apply to all coating materials and coating systems, including
those provided for repair, subject of this Appendix.
The Coating Manufacturer shall arrange, at its own expenses, all tests required by this
Appendix. The tests shall be performed and suitably reported by independent laboratory,
qualified and approved by the Company. The Company reserve the right to attend and inspect
the tests execution.
If the formulation of one or all coating materials forming a coating system is changed after the
qualification test, the new coating material and coating system shall be re-qualified.
Two levels of tests are requested:
a) Coating materials characterisation tests;
b) Coating system characterisation tests.
3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING

Any Coating Manufacturer that intends to qualify one or more of its coating systems shall
inform the Company in writing.
The application documentation shall include all data listed in Table 1 of standard EN 10289. In
addition the following data must be provided:
a) Material Safety Data Sheet of each component;
b) Application method, i.e. brush, spatula, airless spray, plural-component (bi-mixer) spray;
c) Coating system description;
d) Finger printing – Infrared scans of each component of a coating material with and without
pigment. Coating Manufacturer’s Product Quality Manager shall certify the finger printing;
e) Name and address of the laboratory where the tests will be performed;
f) Reference list of the major projects reporting at least the following information: name of
the project, name of the customer, name of the applicator, year in which the work was
performed, length and dimension of the pipeline coated.
3.3 COATING MATERIALS CHARACTERISATION TEST
3.3.1 Labelling
Each coating material, solvent or thinner to be tested shall be delivered and stored in original
containers bearing the Coating Manufacturer’s label, clearly showing following information:
a) Name of the coating material (Part A);
b) Name of the curing agent (Part B);
c) Coating Manufacturer name;
d) Colour of the coating material;
e) Batch number of each component (Part A, Part B);
f) Manufacturing date.
3.3.2 Required product information

For each coating material submitted to qualification testing, Coating Manufacturer shall provide
to the selected laboratory the information listed in the Table 1 of standard EN 10289. In
addition, the following data shall be provided:
b) Viscosity of the base and curing agent according to standard ISO 2555 at temperature of
5, 15, 25, 35 and 40°C;
c) Finger printing – Infrared scans of each component of a coating material with and without
pigment and of coating fully cured. Coating Manufacturer’s Product Quality Manager shall
certify the finger printing, reporting the method and resolution used;
d) Thermal analysis, reporting the method used:
• Curve of curing reaction with temperature scan from ambient temperature to the end
of reaction;
• Glass Transition (Tg) temperature;
• Scan speed (°C/min);
• Temperature at the beginning of the reaction, max temperature at the end of the
reaction and heat content;
e) Shore “D” according to standard ISO 868 in consideration of the time in isothermal
condition at 5, 15, 25, 35 and 40°C.
For all data provided, the Coating Manufacturer must report the method and standard used,
the figure assured and related acceptable deviations.
All data and documentation provided by Coating Manufacturer shall be included as part of the
final test report prepared by the laboratory.
For each Batch Number three samples shall be drawn: one will be used for the analysis, while
the other two will be kept, for a time not exceeding the shelf life reported on the product data
sheet, for possible further checks.
For two-pack products, the tests shall be performed both for the base and the curing agents.
The selected laboratory must test the coating material in order to verify the accuracy and
consistency of the data for physical properties provided by the Coating Manufacturer,
including, but not limited to:
• Viscosity;
• Density;
• Solids by Volume;
• Solids by Weight;
• Infra-Red Scans (Finger printing).
3.4 COATING SYSTEM CHARACTERISATION TESTS

The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating
material forming the coating systems, together with detailed mixing and application
instructions. The Coating Manufacturer shall also supply a sufficient number of test samples
(e.g. pipe and steel panels) as defined in the next paragraph. The laboratory shall perform the
necessary coating work on the samples (surface preparation, application, inspection and
reporting) fully in accordance with the requirements of Functional Specification 20550
PIP.COR.FUN. Rev. 0 and this Appendix.
If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturer’s
duty to perform the work in another suitable location provided that the Company is informed
and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this
Appendix are carefully followed. The selected laboratory shall supervise, record and report all
coating work steps. The Company reserve the right to attend during preparation of samples.
3.4.1 Preparation of steel samples

As general rule the tests shall be performed on carbon steel samples having following
dimension:
a) Pipe sections: Length 700 mm, Diameter 150-300 mm (6-12”), Wall Thickness 4 mm
minimum;
b) Panels: 300 x 300 mm, Thickness 5 mm.
For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while
one shall be identified and kept for possible checks and controls.
Where dimensions of steel samples reported in this item differ from those reported in the
standard EN 10289, the requirements laid in the standard EN 10289 shall apply.
Samples shall be cleaned and coated with the complete coating system listed in this Appendix,
according to all requirements provided by items 5 and 6 of this Appendix and Functional
Specification 20550 PIP.COR.FUN. Rev. 0 including but not limited to inspections, controls
and testing reports of each working step.
The coating application shall be performed using the same method (brush, spatula, airless
spray, etc.) for which the qualification is required and to the same application parameters (e.g.
DFT).
The coated samples may be tested immediately after complete curing or suitably stored.
However the tests must be executed within 3 months from the preparation of the samples.
3.4.2 Qualification tests

Two coated samples shall be used for the execution of each required test. The result of the
test performed on the two samples shall not be in conflict or different. The results will be
considered acceptable if all results conform to the requirements and acceptance criteria of this
Appendix.
The tests to be performed and the acceptance criteria are reported in Table 1.
TABLE 1
Test to be performed on coated steel samples
Test Type Standard/Method Acceptance criteria
Dry Film Thickness EN 10289 Annex A Min 1.500 µm (Class “C”) – Max 1.800 µm
Appearance and continuity EN 10289 Item 7.4 Free of defects as per standard EN 10289
• At –5°C, 4,5 J
Impact test EN 10289 Annex C
• At +23°C, 10 J
Hardness Shore “D” ISO 868 As per Coating Manufacturer data
EN 10289 Annex B
Holiday detection Free from holidays
NACE RP0188
Adhesion test – • Rating 2 at (23 ±2)°C
EN 10289 Annex D
Resistance to removal • Rating 4 at max service temp. ±2°C
EN 24624 Not less than 10 MPa at (23 ±2)°C, using
Adhesion test Pull-off method
ISO 4624 pneumatic instrument
• 8 mm max at (23 ±2)°C per 28 days
Cathodic Disbonding EN 10289 Annex E
Specific electrical insulation EN 10289 Item 7.11 • Rs = 107 at (23 ±2)°C per 100 days
resistance and Annex F • Rs = 104 at Tmax service ±2°C per 30 days
Adhesion test after immersion
EN 10289 Annex G Rating 2 at (23 ±2)°C per 100 hours
in tap water
• 0,2 mm at (23 ±2)°C
Indentation resistance EN 10289 Annex H • 30% of initial measured thickness at max
service temp ±2°C
10 MPa after cooling using pneumatic
Thermal ageing EN 10289 Annex J
instrument
No variations of the values demonstrated by
Infrared scan
the Coating Manufacturer.
ISO 62
Water absorption 1% max
ASTM D 570
≤195 mg weight loss after 1000 cycles with
ASTM D4060
Abrasion resistance abrasive wheels CS-17 and 1000 g applied
Taber Test
load as average of at least 3 test specimens.
3.5 FINAL REPORTING OF LAB

At completion of all tests a detailed report shall be provided to the Company, describing the
preparation of the samples, the description and the results of the tests performed on coating
materials, the description and the results of the tests performed on the steel samples.
4 PRACTICAL APPLICATION TEST IN THE SHOP

At completion of qualification tests of coating materials and coating systems in the laboratory a
practical application test shall be performed in the shop in order to ascertain:
a) The applicability of the coating material;
b) The correctness and suitability of the instructions provided by Coating Manufacturer;
c) The need, where applicable, for special application equipment.

The test shall be performed on a significant length and number of pipes and/or components,
which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if
any, faced during the application.
At completion of the application test the following checks shall be performed:
• Dry Film Thickness according to standard EN 10289 Annex A;
• Appearance and continuity according to standard EN 10289 Item 7.4;
• Hardness Shore “D” According to standard ISO 868;
• Holiday detection according to standard EN 10289 Annex B or NACE RP0188;
• Adhesion test Resistance to removal according to standard EN 10289 Annex D.
5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION
5.1 PREHEAT
The equipment used for preheating the pipes shall be approved by the Company.
If the Contractor uses for preheating purposes free open flames in direct contact with the pipe
surface, the surface shall be kept in motion in respect to the flame at a minimum rate of 10
mm/s, along a helically winding path. The flame shall also be adjusted in its combustion ratio
so that soot or other combustion products are not deposited on the metal.
All measures shall be taken and developed by the Contractor in order to avoid possible
stoppages of the line resulting in the steel being brought to uselessly or damagingly high
temperatures.
The preheat temperature shall be kept between 35°C and 50°C; it shall be checked at least
three times for every work shift (at start, middle, and end) and whenever stoppages occur in
the production line.
The preheat temperature can be checked using either temperature indicating crayons or
contact thermometers. All temperature measurements shall be recorded on the production
certificate.

Surface preparation shall be performed fully in accordance with item 6.1 of standard EN 10289
and to the specific requirements reported in item 2.5 of Functional Specification 20550
PIP.COR.FUN Rev.0.
5.3 COATING APPLICATION

Coatings shall be mixed and applied fully in accordance with item 6.2 of standard EN 10289
PIP.COR.FUN Rev. 0.
5.3.1 Wet Film Thickness (WFT) and Dry Film Thickness (DFT)
Wet film thickness shall be measured in accordance with standard ISO 2808.
Calibration of DFT gauges and measurement method shall be carried out according to
standard SSPC-PA2.
5.4 CUT BACK

The pipe surface shall be left bare (uncoated) at both ends of the pipe for (150 ± 20) mm
distance from the ends. For fittings and components cut back shall be specified and approved
by the Company’s Representative.
The Contractor shall properly protect these end areas and the pipe bevel, that must remain
perfectly clean and free from any traces of paint.
Once the coating operations are completed cut-back areas shall be protected from corrosion
by applying a temporary protection, easily removable by brushing.
The type of this temporary protection, if not specified in the order or other contract documents,
must be approved by the Company’s Representative.
5.5 REPAIR OF DEFECTS

The Contractor shall repair all coating defects and damages that may occur during or after
construction or shipping.
Coating used for repair of defects and damages shall be supplied by the same Coating
Manufacturer of the original coating system.
Any repair shall be performed according to item 9 of standard EN 10289.
6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE
6.1 GENERAL
Additional requirements for Quality Management and/or Quality Assurance are contained in
the applicable “Quality and Execution Requirements Specification” attached to the Invitation to
Bid.
The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN Rev. 0 must
be carefully followed.
6.2 QUALITY CONTROL PLAN

Before the pre-job meeting and the beginning of the work the Contractor shall prepare and
submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all
the Production Quality Tests (PQT) necessary to fully meet the requirements of Functional
Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but
not limited to, must be listed:
a) Description of the activity,
b) Description of the test;
c) Applicable reference documents;
d) Applicable check procedures and methods;
e) Acceptability criteria;
f) Frequency of the checks;
g) Persons required to be present at the inspections.
6.3 TESTS DURING THE WORKS PROGRESS AND FINAL INSPECTION

Contractor shall perform during the works progress and at completion of the work all
inspections and tests reported in the Table 5 of standard EN 10289.

At completion of the work the Contractor shall produce all documentation and reporting
required in item 5 of Functional Specification 20550 PIP.COR.FUN Rev. 0.
Eni S.p.A.
APPENDIX “B”
LIQUID POLYURETHANE AND POLYURETHANE MODIFIED COATINGS ON
EXTERNAL SURFACES OF STEEL PIPES AND COMPONENTS
20550 PIP.COR.FUN
Appendix “B” - Page 2 of 10
CONTENTS
APPENDIX “B” ....................................................................................................................................... 1
1 GENERAL........................................................................................................................... 3
1.1 INTRODUCTION................................................................................................................. 3
1.2 SCOPE................................................................................................................................ 3

3.3.1 Labelling.............................................................................................................................. 4

5.1 PREHEAT ........................................................................................................................... 8
5.4 CUT BACK .......................................................................................................................... 9

6.1 GENERAL ........................................................................................................................... 9
6.2.1 Tests during the works progress and final inspection......................................................... 9

1 GENERAL
1.1 INTRODUCTION
It refers to the European Standard EN 10290 (Steel tubes and fittings for onshore and offshore
pipelines – External liquid applied polyurethane and polyurethane-modified coatings), the
content of which must be considered an integral part of this Appendix.
1.2 SCOPE
application of liquid polyurethane and polyurethane-modified tar-free coating to external
surface of steel pipes and components for onshore and offshore services as defined in Item 1
of standard EN 10290.
The coating system assumed by this Appendix is the Type 3: -20°C to +80°C, thickness class
“B” (1.500 µm) of standard EN 10290.

Specification 20550 PIP.COR.FUN. Rev. 0.
documents.
inspections step.

The coating systems considered in this Appendix are multi-component liquid products and
composed of a polyol and an isocyanate that can be applied by brush or spatula, or airless
spray or plural-components spray equipment in high thickness and that harden rapidly in air.
The coating materials can be applied at ambient temperature over + 5°C with a Dry Film
Thickness (DFT) of 1.500 µm when applied by brush or spray showing a continuous and
uniform film free of sags, runs or any other visible defect.

All requirements provided in the Item 2.4 of Functional Specification 20550 PIP.COR.FUN.
Rev. 0 must be fully followed.
a) Coating materials characterisation tests
b) Coating system characterisation tests

The application documentation shall include all data listed in Table 1 of standard EN 10290. In
b) Application method, i.e. brush, spatula, airless spray, plural-component (bi-mixer) spray;
performed, length and dimension of the pipeline coated;
3.3.1 Labelling
a) Name of the coating material (Part A);
b) Name of the curing agent (Part B);
c) Coating Manufacturer name;
e) Batch number of each component (Part A, Part B);

the selected laboratory whit the information listed in the Table 1 of standard EN 10290. In
addition, the following data shall be provided:
b) Viscosity of the base and curing agent according to standard ISO 2555 at temperature of
5, 15, 25, 35 and 40°C;
c) Finger printing – Infrared scans of each component of a coating material with and without
d) Thermal analysis, reporting the method used:
• Curve of curing reaction with temperature scan from ambient temperature to the end
of reaction;

• Scan speed (°C/min);
• Temperature at the beginning of the reaction, max temperature at the end of the
reaction and heat content.
e) Shore “D” according to standard ISO 868 in consideration of the time in isothermal
condition at 5, 15, 25, 35 and 40°C.
consistency of the data for physical properties provided by the Coating Manufacturer,
including, but not limited to:
• Viscosity;
• Density;
• Solids by Volume;
• Solids by Weight;
• Infra-Red Scans (Finger printing).

(e.g. pipe and steel panels) as defined in the next paragraph.
The laboratory shall perform the necessary coating work on the samples (surface preparation,
application, inspection and reporting) fully in accordance with the requirements of Functional
Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to
perform the coating work, it shall be the Coating Manufacturer’s duty to perform the work in
another suitable location provided that the Company is informed and the requirements of
Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix are carefully
followed.
The selected laboratory shall supervise, record and report all coating work steps. The
Company reserve the right to attend during preparation of samples.

dimension:
a) Pipe sections: Length 700 mm, Diameter 150-300 mm (6-12”), Wall Thickness 4 mm
minimum;
according to all requirements provided by items 5, and 6 of this Appendix and Functional
spray, etc.) for which the qualification is required and to the same application parameters (e.g.
DFT).

Appendix. The tests to be performed and the acceptance criteria are reported in Table 1.
TABLE 1
Dry Film Thickness EN 10290 Annex A Min. 1.500 (Class “B”) – Max. 1.800 µm
Impact test EN 10290 Annex C • At –5°C, 4,5 J At +23°C, 10 J
Hardness Shore “D” ISO 868 As per Coating Manufacturer data
EN 10290 Annex B
Holiday detection Free from holiday
NACE RP0188
Adhesion test – • Rating 3 at (23 ±2)°C
EN 10290 Annex D
Resistance to removal • Rating 4 at max service temp. ±2°C
Not less than 10 MPa at (23 ±2)°C, using
Adhesion test: Pull-off EN 24624-ISO 4624
pneumatic instrument.
Cathodic Disbonding EN 10290 Annex E
Specific electrical insulation EN 10290 Item 7.11 • Rs = 107 at (23 ±2)°C per 100 days
resistance and Annex F • Rs = 104 at max service temp ±2°C per 30 days
Adhesion test after
EN 10290 Annex G Rating 2 at (23 ±2)°C per 100 hours
immersion in tap water
• 0,2 mm at (23 ±2)°C
Indentation resistance EN 10290 Annex H • 30% of initial measured thickness at max
service temp ±2°C
Thermal ageing EN 10290 Annex J 10 MPa after cooling using pneumatic instrument
No variations of the values demonstrated by the
Infrared scan
Coating Manufacturer.
ISO 62
Water absorption 1% max
ASTM D 570
1. Pipes:
• S = 0,020 at 0 ± 2°C
EN 10290 Item 7.15 • S = 0.030 at 23 ± 2°C
Flexibility
and Annex K 2. Fitting:
• S = 0,005 at 0 ± 2°C
• S = 0.010 at 23 ± 2°C
Elongation EN 10290 Item 7.17 10%
≤ 195 mg weight loss after 1000 cycles with
ASTM D4060
Abrasion resistance abrasive wheels CS-17 and 1000 g applied load
Taber Test
as average of at least 3 test specimens.

At completion of all tests a detailed report shall be provided to the Company describing the

practical test shall be perform in the shop in order to ascertain:
c) The need, where applicable, for special application equipment;
• Dry film Thickness according to standard EN 10290 Annex A;
• Hardness Shore “D” according to standard ISO 868;
• Holiday detection according to standard EN 10290 Annex B or NACE RP0188;
• Adhesion test Resistance to removal according to standard EN 10290 Annex D.
5.1 PREHEAT
temperatures.
The preheat temperature can be checked using either temperature indicating crayons or
contact thermometers. All temperature measurements shall be recorded on the production
certificate.

PIP.COR.FUN Rev.0.

Coatings shall be mixed and applied fully in accordance with item 6.2 of standard EN 10290
PIP.COR.FUN. Rev. 0.
Wet film thickness shall be measured in accordance with standard ISO 2808.
Calibration of DFT gauges and measurement method shall be carried out according to
standard SSPC-PA2.
5.4 CUT BACK


Any repair shall be performed according to item 9 of standard EN 10290.
6.1 GENERAL
Bid.
The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0

a) Description of the activity;
6.2.1 Tests during the works progress and final inspection

inspections and tests reported in the Table 5 of standard EN 10290.

required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
Eni S.p.A.
APPENDIX “C”
THREE LAYERS EXTRUDED POLYETHYLENE COATINGS ON EXTERNAL
SURFACES OF STEEL PIPES AND COMPONENTS
20550 PIP.COR.FUN
Appendix “C” - Page 2 of 14
CONTENTS
APPENDIX “C” ....................................................................................................................................... 1
1 GENERAL........................................................................................................................... 3
1.1 INTRODUCTION................................................................................................................. 3
1.2 SCOPE................................................................................................................................ 3
1.3 OPERATIVE ENVIRONMENT............................................................................................ 3

2.1 CHARACTERISTICS OF THE PRIMER............................................................................. 3
2.2 CHARACTERISTICS OF THE ADHESIVE ........................................................................ 4
2.3 EXTRUDED POLYETHYLENE........................................................................................... 4
2.4 COATING THICKNESS ...................................................................................................... 5

3.2 REQUIREMENTS FOR PRE-QUALIFICATION OF THE COATING ................................. 6
3.3.1 Labelling.............................................................................................................................. 6
3.3.2 Product information............................................................................................................. 6
3.5 QUALIFICATION TESTS.................................................................................................... 8
5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................. 10

5.1 PREHEAT ......................................................................................................................... 10
5.3 COATING APPLICATION................................................................................................. 10
5.3.1 Application of Powder Epoxy Primer ................................................................................ 10
5.3.2 Application of the Adhesive............................................................................................... 10
5.3.3 Application of Extruded Polyethylene ............................................................................... 10
5.3.4 Cooling .............................................................................................................................. 10
5.3.5 Thickness of the coating system....................................................................................... 11
5.4 CUT BACK ........................................................................................................................ 11
5.5 REPAIR OF DEFECTS..................................................................................................... 11
5.5.1 Max number of repair........................................................................................................ 11
5.5.2 Inspection.......................................................................................................................... 11
6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE......... 11

6.1 GENERAL ......................................................................................................................... 11
6.2 QUALITY CONTROL PLAN.............................................................................................. 11

1 GENERAL
1.1 INTRODUCTION
It refers to the European Standard EN 10288 (Steel tubes and fittings for onshore and offshore
pipelines - External two layers extruded polyethylene based coatings), the content of which
must be considered an integral part of this Appendix.
1.2 SCOPE
This Appendix defines the minimum functional requirements for the qualification, supply and
application of factory applied external three layers extruded polyethylene based coatings for
the external surfaces of steel pipes and components for onshore and offshore services as
defined in Item 1 of standard EN 10288.
1.3 OPERATIVE ENVIRONMENT

External extruded polyethylene coating can be used for the protection of buried or submerged
tubes service and suitable for the following maximum service temperature:
From –20° to +80°C for offshore application;
From –20° to +70°C for onshore buried pipelines.

documents.
evidence of provisions of standards to the Company before work begins and during each
inspections step.

The coating systems considered in this Appendix consist of three layers as follows:
1st layer - Powder Epoxy Primer (DFT 80 – 150 µm);
2nd layer - Extruded Adhesive (DFT 150 – 250 µm);
3rd layer - Extruded Polyethylene outer sheath.
2.1 CHARACTERISTICS OF THE PRIMER

The 1st layer (Primer) shall be formed by a powder epoxy primer completely compatible with
the adhesive that shall maintain perfect adhesion to the substrate and to the adhesive and
shall meet the characteristics specified in the Table 1:
Table 1
Characteristic Method Acceptance Criteria
Gel time @ 180°C Heating plate (DIN 55990 T8) 80 + 10 s Max
Specific gravity Standard method 1,20 – 1,60
Powder: 20 g
Moisture content Temperature: 105°C 0,5% (max.)
Time: 30 minutes
Glass Transition (Tg) Differential heat analysis
∆ Tg < -5°C
temperature
2,5° per diameter
Bend test DIN 53452
No holiday
2.2 CHARACTERISTICS OF THE ADHESIVE

The 2nd layer (Adhesive) shall be formed by a polymer intended to provide adhesion between
the primer and 3rd layer (extruded polyethylene)
The extruded adhesive shall meet the requirements listed in the Table 2:
Table 2
Characteristic Standard Acceptance Criteria
Melt flow rate ISO 1133 1 to 6 g/10 min
Density ISO 1183 0,93 to 0,95
Breaking strength ≥ 12 MPa
ASTM D 638
Elongation at break ≥ 600 %
Shore D hardness ASTM 2240 ≥ 35
Brittle point ASTM 746 - 60°C
VICAT Softening point (9,8 N) ASTM 1525 > 90°C
Melting point ASTM 3418 > 120°C
2.3 EXTRUDED POLYETHYLENE

The 3rd layer (Extruded Polyethylene) shall be formed by the polyethylene outer sheath.
The extruded polyethylene shall meet the requirements of Table 3:
Table 3
Melt flow rate ISO 1133 0,25 to 3 g/10 min
Carbon Black content ASTM D 1603 ≥ 2.0%
Tensile strength at yield at 23°C ASTM D 638 ≥ 17 MPa
Elongation at break at 23°C ASTM D 638 > 600%
Shore D hardness ASTM D 2240 ≥ 50
Water Absorption ASTM D 570 ≤ 0,05% 24 h
VICAT Softening point (9,8 N) ASTM D 1525 > 110°C
Melting point ASTM D 3418 > 110°C
Brittle point MA 17238 < -20°C
Specific resistance DIN 30670 ≥ 108 Ω at (23±2)°C per 100 days
2.4 COATING THICKNESS

The minimum thickness of the coating system at any point shall correspond to the value given
in Table 2 of the standard EN 10288 depending on the specified Class (1, 2, 3). Coating
thickness shall be measured in accordance with the method defined in Annex A of the
standard EN 10288.
The coating thickness is also given in the following Table 4 where for Classes 1, 2 and 3 the
following definition shall be assumed:
Class 1 “Normal Thickness”: buried condition with low mechanical aggressiveness or on
lines with extra anti-rock protection;
Class 2 “Reinforced Thickness”: buried condition with mechanical aggressiveness (rock or
clay) and for submerged pipeline with service temperature below 80°C;
Class 3 “Extra-reinforced Thickness”: submerged pipeline for deep sea or with concrete
coating and/or when the temperature is higher than 80°C.
Table 4
Line pipe diameter Minimum thickness (mm)

(mm) “Class 1” “Class 2” “Class 3”
D ≤ 114,3 1,5 1,8 2,5
114,3 < D ≤ 273 1,8 2 2,7
273 < D ≤ 508 2 2,2 2,9
508 < D ≤ 762 2,2 2,5 3,2
762 < D 2,5 3 3,7

All requirements provided by the Item 2.4 of Functional Specification 20550 PIP.COR.FUN.
3.2 REQUIREMENTS FOR PRE-QUALIFICATION OF THE COATING

The documentation forwarded to the Company shall include all data listed in Table 1 of
standard EN 10288. In addition the following data must be provided:
b) Application method;
d) Name and address of the laboratory where the tests will be performed;
e) Reference list of the major projects reporting at least the following information: name of
3.3.1 Labelling
a) Name of the coatings material (primer, adhesive and extruded polyethylene);
b) Coating Manufacturer name;
c) Colour of the coating material;
d) Batch number of each component (primer, adhesive and extruded polyethylene);
e) Manufacturing date.
3.3.2 Product information

For each coating material submitted to qualification testing, the Coating Manufacturer shall
provide the selected laboratory whit the information listed in the following Table 5.
Table 5 - Information and data to be provided by Coating Manufacturer

Item Primer Adhesive Polyethylene
Product Data Sheet (PDS) Yes Yes Yes
Material Safety Data Sheet (MSDS) Yes Yes Yes
Date of issue of PDS Yes Yes Yes
Date of issue of MSDS Yes Yes Yes
Name of Manufacturer Yes Yes Yes
Name and type of the product Yes Yes Yes
Factory of origin Yes Yes Yes
Batch number Yes Yes Yes
Shelf life Yes Yes Yes
Physical state of delivered product Yes Yes Yes
Packaging Yes Yes Yes
Storage condition Yes Yes Yes
Sieve analysis Yes No No
Gel time Yes No No
Specific gravity Yes No No
Moisture content Yes No No
Glass Transition (Tg) temperature Yes No No
Bend test Yes No No
Density No Yes Yes
Melting point No Yes Yes
Melt flow rate No Yes Yes
Braking strength No Yes Yes
Elongation at break @ 23°C No Yes Yes
Shore D hardness No Yes Yes
Brittle point No Yes Yes
VICAT Softening point (9,8N) No Yes Yes
Carbon black content No No Yes
Tensile strength at yield at 23°C No No Yes
Water absorption No No Yes
Thermal ageing No No Yes
UV ageing No No Yes
Stress cracking resistance No No Yes
Specific resistance No No Yes
Content of pigment No No Yes
Dispersion of pigment No No Yes
consistency of the data for physical properties provided by the Coating Manufacturer.

material forming the coating systems, together with detailed mixing and application instruction.
The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe) as
defined in the next paragraph. The laboratory shall perform the necessary coating work on the
samples (surface preparation, application, inspection and reporting) fully in accordance with
the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix.
and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this
Appendix are carefully followed.
The selected laboratory shall supervise, record and report all the steps of the coating work.
The Company reserve the right to attend during preparation of samples.

dimension:
• Pipe sections: Length 700 mm, Diameter 150-300 mm (6-12”), Wall Thickness 4 mm
minimum.
Specification 20550 PIP.COR.FUN. Rev. 0, including but not limited to inspections, controls
The coating application shall be performed using the same method for which the qualification
is required and according to the same application parameters (e.g. thickness).
3.5 QUALIFICATION TESTS

Appendix.

At completion of all tests a complete report shall be provided to the Company describing the
Table 6
Dry Film Thickness EN 10288 Annex A As per standard EN 10288 Table 2.
EN 10288
Impact resistance 5 J per mm coating thickness
Annex C
EN 10288 Annex B
NACE RP0274
30 mm max at (23 ±2)°C per 28 days
Cathodic Disbonding EN 10288 Annex J 30 mm max at (60 ±2)°C per 2 days
30 mm max at (40±2)°C per 7 days
Specific electrical insulation
EN 10288 Annex F Rs = 108 at (23 ±2)°C per 100 days
resistance
0,3 mm at (23 ±2)°C
Indentation resistance EN 10288 Annex E
0,5 mm at (60 ±2)°C
EN 10288 At (23 ±2)°C Min Average 60, Average 80
Peel Force (N/10 mm)
Annex D At (80 ±2)°C Min Average 15, Average 20
EN 10288
Elongation at break ≥ 350 % at (23 ±2)°C
Annex G
Resistance to ultraviolet EN 10288 A ≥ 50%
irradiation Annex H.1 0,65 ≤ ∆ MFR ≤ 1,35
EN 10288 0,65 ≤ ∆ MFR ≤1,35 at (100 ±2)°C per 2400
Thermal stability
Annex H.2 hours
EN 10288
Flexibility ≥3% at (23 ±2)°C
Item 8.14
Hardness Shore “D” ASTM D 2240 ≥ 50

At completion of qualification tests of coating materials and coating systems in the laboratory,
a practical test shall be performed in the shop in order to ascertain:
• Dry Film Thickness according to standard EN 10288 Annex A;

• Holiday detection according to standard EN 10288 Annex B or NACE RP0274.
5.1 PREHEAT
temperatures.
All temperature measurements shall be recorded on the production certificate.

PIP.COR.FUN Rev.0.

Coatings shall be mixed and applied, in a continuous coating line, fully in accordance with item
7.2 of standard EN 10288 and to the specific functional requirements reported in item 2.6 of
Functional Specification 20550 PIP.COR.FUN. Rev. 0.
5.3.1 Application of Powder Epoxy Primer

The pipes shall be heated in an induction oven in accordance with the temperature
recommended by the Coating Manufacturer.
Application shall be made by electrostatic spray equipment at DFT of 80 – 150 µm in
consideration of the powder and intended service operation.
5.3.2 Application of the Adhesive

The adhesive shall be applied by extrusion prior the complete polymerisation of the Powder
Epoxy Primer. The temperature shall be fully in accordance with Coating Manufacturer
recommendations.
5.3.3 Application of Extruded Polyethylene

The application of Extruded Polyethylene outer sheath shall be performed by lateral or axial
extrusion and than the coating shall be smoothed by pressure rollers.
During the production the temperature shall be always in accordance with Coating
Manufacturer recommendations.
5.3.4 Cooling
When the coating process is completed, the pipe shall be sprayed with fresh water in order to
cool it to a temperature of 60°C (±10°C).
5.3.5 Thickness of the coating system

Coating thickness shall be measured in accordance with the method defined in Annex A of the
standard EN 10288.
in Table 4 of this Appendix depending on the specified class (1, 2 or 3).
5.4 CUT BACK
The pipe surface shall be left bare (uncoated) at both ends of the pipe for 150 (± 20) mm
distance from the ends and the coating shall be beveled at the cut back forming a bevel angle
of ≤ 30° unless otherwise specified. For fittings and components cut back shall be specified
and approved by the Company’s Representative.
The type of this temporary protection, if not specified in the order or other contractual
documents, must be approved by the Company’s Representative.
Coating used to repair the defects and damages shall be supplied by the same Coating
Any repair shall be performed according to item 10 of standard EN 10288 and method
submitted to the Company for approval before the beginning of the production.
5.5.1 Max number of repair

Contractor shall repair all defects detected by holiday detection and/or any kind of damaged
area less than 50 cm2.
In case any individual damaged area is greater than 50 cm2, the pipe shall be completely re-
coated. A maximum of 3 (three) repairs per pipe is allowed, but in no case the total repaired
areas shall exceed 150 cm2.
5.5.2 Inspection
The repaired area shall be 100% inspected with a holiday detector set to 10 kV per mm of
coating thickness according to the methods defined in Appendix B of standard EN 10288.
6.1 GENERAL
Bid.

the Production Quality Tests (PQT) necessary to fully meet the provisions of Functional
According to Table 8 of standard EN 10288 and the requirements of this Appendix, the
Contractor shall perform during the works progress and at completion of the coating works all
inspections and tests reported in the following Table 7.

Table 7 - Nature and frequency of testing and control

Properties Test method Acceptance Criteria Frequency
Surface condition before blasting - Every pipe
Steel imperfection ISO 8501-3 Grade P3 Every pipe
Dimensions, shape and properties of abrasive blasting Conductivity ≤150 µS/cm
ASTM D-4940 Twice per shift
material Chloride content < 25 ppm
Cleaning before abrasive blasting SSPC-SP1 Free of oil, grease, etc. Every pipe
Degree of abrasive blasting ISO 8501-1 Sa 2,5 Every pipe
Degree of cleanliness (dust level) ISO 8502-3 < Class 2 First 10 pipes and 4 time per shift
Roughness of the blast cleaned surface - 60 ≤Rz ≤ 80 µm Once per shift
Relative Humidity and Dew Point ISO 8502-4 RH < 85% 4 time per shift
Steel temperature 3°C above dew point 4 time per shift
Temperature of heating before coating IR camera recording As per Coating Manufacturer Every pipe
Appearance and continuity Visual Free of defects Every pipe
Thickness of the primer EN 10288 Annex A As per requirement First 10 pipes and 1 per hour
Thickness of the coating system EN 10288 Annex A As per requirement First 10 pipes and 1 per hour
Cut back Visual As per requirement Every pipe
Holiday detection EN 10288 Annex B As per requirement Every pipe
Impact resistance EN 10288 Annex C As per requirement Once per week
2 Tests once per shift at 23°C
Peel force EN 10288 Annex D As per requirement
2 Tests once per week at 60°C
Indentation resistance EN 10288 Annex E As per requirement Once per week
Electrical insulation resistance EN 10288 Annex F As per requirement To be agreed at pre-job meeting
Elongation at break EN 10288 Annex G As per requirement To be agreed at pre-job meeting
Table 7 - Nature and frequency of testing and control

Resistance to ultraviolet irradiation EN 10288 Annex H.1 As per requirement To be agreed at pre-job meeting
Thermal stability EN 10288 Annex H2 As per requirement To be agreed at pre-job meeting
Cathodic disbonding EN 10288 Annex J As per requirement To be agreed at pre-job meeting
Eni S.p.A.
APPENDIX “D”
THREE LAYERS EXTRUDED POLYPROPYLENE COATINGS ON EXTERNAL
SURFACES OF STEEL PIPES AND COMPONENTS
20550 PIP.COR.FUN
Appendix “D” - Page 2 of 14
CONTENTS
APPENDIX “D” ....................................................................................................................................... 1
1 GENERAL........................................................................................................................... 3
1.1 INTRODUCTION................................................................................................................. 3
1.2 SCOPE................................................................................................................................ 3

2.1 CHARACTERISTIC OF THE PRIMER ............................................................................... 3
2.2 ADHESIVE .......................................................................................................................... 4
2.3 EXTRUDED POLYPROPYLENE........................................................................................ 4
2.4 COATING THICKNESS ...................................................................................................... 5

3.2 REQUIREMENTS FOR PRE-QUALIFICATION OF THE COATING ................................. 6
3.3.1 Labelling.............................................................................................................................. 6
3.3.2 Product information............................................................................................................. 6
5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................. 10

5.1 PREHEAT ......................................................................................................................... 10
5.3 COATING APPLICATION................................................................................................. 10
5.3.1 Application of Powder Epoxy Primer ................................................................................ 10
5.3.2 Application of the Adhesive............................................................................................... 10
5.3.3 Application of Extruded Polypropylene ............................................................................. 10
5.3.4 Cooling .............................................................................................................................. 10
5.4 CUT BACK ........................................................................................................................ 11
5.5 REPAIR OF DEFECTS..................................................................................................... 11
5.5.1 Max number of repair........................................................................................................ 11
5.5.2 Inspection.......................................................................................................................... 11

6.1 GENERAL ......................................................................................................................... 11

1 GENERAL
1.1 INTRODUCTION
For testing and acceptance criteria only, this Appendix refers to the European Standard EN
10288 (Steel tubes and fittings for onshore and offshore pipelines – External two layers
extruded polyethylene based coatings).
1.2 SCOPE
application of factory applied external three layers extruded polypropylene based coatings for
the external surface of steel pipes and components for onshore and offshore pipelines
transporting oil, gas or water.

External extruded polypropylene coating can be used for the protection of buried or
submerged tubes service and suitable for the following maximum service temperature:
• From –20° to +80°C for applications at ambient temperature or medium temperatures
(standard coating);
• From –20° to +120°C for high temperatures offshore application (thermal stabilised
coating);
• From –20° to +110°C for high temperatures onshore buried pipelines (thermal stabilised
coating).

documents.
inspections step.

The coating systems considered in this Appendix consist of three layers as follows:.
• 1st layer - Powder Epoxy Primer (DFT 80 – 150 µm);
• 2nd layer - Extruded Adhesive (DFT 250 – 300 µm);
• 3rd layer - Extruded Polypropylene outer sheath.
2.1 CHARACTERISTIC OF THE PRIMER

The 1st layer (Primer) shall be formed by a powder epoxy primer completely compatible with
the adhesive that shall maintain perfect adhesion to the substrate and to the adhesive. The
thickness of The Company requirements of the primer are given in the Table 1:
Table 1
Characteristic Method Acceptance Criteria
Gel time @ 180°C Heating plate (DIN 55990 T8) 80 + 10 s Max
Specific gravity Standard method 1.20 – 1.60
Powder: 20 g
Moisture content Temperature: 105°C 0.5% (max.)
Time: 30 minutes
Glass Transition (Tg)
Differential heat analysis ∆ Tg < -5°C
temperature
2,5° per diameter
Bend test DIN 53452
No holiday
2.2 ADHESIVE
The 2nd layer (Adhesive) shall be formed by a polymer intended to provide adhesion between
the primer and 3rd layer (extruded polypropylene)
The extruded adhesive shall meet the requirements listed in the Table 2:
Table 2
Melt flow rate ISO 1133 1 to 12 g/10 min
Breaking strength ≥ 20 MPa
ASTM D 638
Elongation at break ≥ 400%
Shore D hardness ASTM 2240 ≥ 57
Brittle point ASTM 746 - 20°C
VICAT Softening point (9,8 N) ASTM 1525 > 120°C
Melting point ASTM 3418 > 130°C
2.3 EXTRUDED POLYPROPYLENE

The 3rd layer (extruded polypropylene) shall be formed by the polypropylene outer sheath.
The extruded polypropylene shall meet the requirements of Table 3:
Table 3
Melt flow rate ISO 1133 0,6 to 4 g/10 min.
Carbon Black content ASTM D 1603 0%
Tensile strength at yield at 23°C ASTM D 638 ≥ 20 MPa
Elongation at break at 23°C ASTM D 638 > 400%
Shore D hardness ASTM D 2240 ≥ 60
Water Absorption ASTM D 570 ≤ 0,05% 24 h
VICAT Softening point (9,8 N) ASTM D 1525 > 135°C
Melting point ASTM D 3418 > 150°C
Brittle point MA 17238 < -20°C
Specific resistance DIN 30670 ≥ 108 Ω at (23±2)°C per 100 days
2.4 COATING THICKNESS

in the Table 4 where for Classes 1, 2 and 3 the following definition shall be assumed:
• Class 1 “Normal Thickness”: buried condition with low mechanical aggressiveness or on
lines with extra anti-rock protection;
• Class 2 “Reinforced Thickness”: buried condition with mechanical aggressiveness (rock or
clay) and for submerged pipeline with service temperature below 80°C;
• Class 3 “Extra-reinforced Thickness”: submerged pipeline for deep sea or with concrete
coating and/or when the temperature is higher than 80°C.
Table 4
Line pipe diameter Minimum thickness (mm)

(mm) “Class 1” “Class 2” “Class 3”
D ≤ 114,3 1,5 1,8 2,5
114,3 < D ≤ 273 1,8 2 2,7
273 < D ≤ 508 2 2,2 2,9
508 < D ≤ 762 2,2 2,5 3,2
762 < D 2,5 3 3,7

All requirements provided item 2.4 of Functional Specification. 20550 PIP.COR.FUN. Rev. 0
3.2 REQUIREMENTS FOR PRE-QUALIFICATION OF THE COATING

The documentation forwarded to the Company shall include all data listed in Table 1 of
standard EN 10288. In addition the following data must be provided:
a) Material Safety Data Sheet of each component,
3.3.1 Labelling
a) Name of the coatings material (primer, adhesive and extruded polypropylene);
b) Coating manufacturer name;
d) Batch number of each component (primer, adhesive and extruded polypropylene);

provide the selected laboratory with the information listed in the following Table 5.
Table 5 - Information and data to be provided by Coating Manufacturer

Item Primer Adhesive Polyethylene
Sieve analysis Yes No No
Gel time Yes No No
Specific gravity Yes No No
Moisture content Yes No No
Glass Transition (Tg) temperature Yes No No
Bend test Yes No No
Density No Yes Yes
Melting point No Yes Yes
Melt flow rate No Yes Yes
Braking strength No Yes Yes
Elongation at break @ 23°C No Yes Yes
Shore D hardness No Yes Yes
Brittle point No Yes Yes
VICAT Softening point (9,8N) No Yes Yes
Carbon black content No No Yes
Tensile strength at yield at 23°C No No Yes
Water absorption No No Yes
Thermal ageing No No Yes
UV ageing No No Yes
Stress cracking resistance No No Yes
Specific resistance No No Yes
Content of pigment No No Yes
Dispersion of pigment No No Yes

(e.g. pipe) as defined in the next paragraph.
perform the coating work, it shall be the Coating Manufacturer ’s duty to perform the work in
Functional Specification 20550 PIP.COR.FUN. Rev. 0 and Appendix are carefully followed.
The selected laboratory shall supervise, record and report all steps of the coating work. The

dimension:
• Pipe sections: Length 700 mm, Diameter 150-300 mm (6-12”), Wall Thickness 4 mm
minimum.
For each test, 2 series of 3 samples shall be prepared. One series shall be used for the test,
while one shall be identified and kept for possible checks and controls.
according to all requirements provided by items 5 and 6 of this Appendix and Functional
is required and to the same application parameters (e.g. thickness).

Appendix.

TABLE 6
Dry Film Thickness EN 10288 Annex A As per value of Table 4 of this Appendix
Appearance and
EN 10288 Item 8.2 Free of defects
continuity
Impact resistance EN 10288 Annex C 7 J per mm coating thickness
EN 10288 Annex B
NACE RP0274
• 30 mm max at 23 (±2)°C per 28 days
• 30 mm max at 60 (±2)°C per 2 days
Cathodic Disbonding EN 10288 Annex J
• 40 mm max at max service temperature per
28 days
Specific electrical
EN 10288 Annex F Rs = 108 at (23 ±2)°C per 100 days
insulation resistance
• 0,2 mm at (23 ±2)°C
Indentation resistance EN 10288 Annex E
• 0,4 mm at (60 ±2)°C
• At (23 ±2)°C Min Average 80, Average 100
Peel Force (N/10 mm) EN 10288 Annex D • At (100 ±2)°C Min Average 30, Average 40
• At (120 ±2)°C Min Average 15, Average 20
Elongation at break EN 10288 Annex G ≥ 400% at (23 ±2)°C
Resistance to ultraviolet EN 10288 A ≥ 50%
irradiation Annex H.1 0,65 ≤ ∆ MFR ≤ 1,35
EN 10288 0,65 ≤ ∆ MFR ≤1,35 at (100 ±2)°C per 2400
Thermal stability
Annex H.2 hours
Flexibility EN 10288 Item 8.14 ≥3% at (23 ±2)°C
Hardness Shore “D” ASTM D 2240 ≥ 60

• Dry film Thickness according to standard EN 10288 Annex A

• Appearance and continuity according to standard EN 10288 Item 8.2.
• Holiday detection according to standard NACE RP0274.
5.1 PREHEAT
temperatures.

Surface preparation shall be performed fully in accordance with the specific requirements
reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.

Coatings shall be mixed and applied, in a continuous coating line, fully in accordance to the
specific functional requirements reported in item 2.6 of Functional Specification 20550
PIP.COR.FUN. Rev. 0.
5.3.1 Application of Powder Epoxy Primer

The pipes shall be heated in an induction oven in accordance with the temperature
recommended by the Coating Manufacturer.
Application shall be made by electrostatic spray equipment at DFT of 80 – 150 µm in
consideration of the powder and intended service operation.
5.3.2 Application of the Adhesive

The adhesive shall be applied by extrusion prior the complete polymerisation of the Powder
Epoxy Primer. The temperature shall be fully in accordance with Coating Manufacturer
recommendations.
5.3.3 Application of Extruded Polypropylene

The application of Extruded Polypropylene outer sheath shall be performed by lateral or axial
extrusion and than the coating shall be smoothed by pressure rollers.
During the production the temperature shall be always in accordance with Coating
Manufacturer recommendations.
5.3.4 Cooling
When the coating process is completed, the pipe shall be sprayed with fresh water in order to
cool it to a temperature of 60°C (±10°C).

Coating thickness shall be measured in accordance with the method defined in Annex A of the
standard EN 10288.
in Table 4 of this Appendix depending on the specified class (1, 2 or 3).
5.4 CUT BACK
The pipe surface shall be left bare (uncoated) at both ends of the pipe for 150 (±20) mm
distance from the ends and the coating shall be beveled at the cut back forming a bevel angle
of ≤ 30° unless otherwise specified. For fittings and components cut back shall be specified
and approved by the Company’s Representative.
Any repair shall be performed according to item 10 of standard EN 10288 and method
submitted to the Company for approval before the beginning of the production.
5.5.1 Max number of repair

Contractor shall repair all defects detected by holiday detection and/or any kind of damaged
area less than 50 cm2.
In case any individual damaged area is greater than 50 cm2, the pipe shall be completely re-
coated.
A maximum of 3 (three) repairs per pipe is allowed, but in no case the total repaired areas
shall exceed 150 cm2.
5.5.2 Inspection
The repaired area shall be 100% inspected with a holiday detector set to 10 kV per mm of
coating thickness according to the methods defined in Appendix B of standard EN 10288.
6.1 GENERAL
Bid.

the Production Quality Tests (PQT) necessary to fully meet the provisions of Functional
b) Description of the test,
c) Applicable reference documents,
d) Applicable check procedures and methods,
e) Acceptability criteria
f) Frequency of the checks
According to the requirements of this Appendix, the Contractor shall perform during the works
progress and at completion of the coating works all inspections and tests reported in the the
following Table 7

Table 7
Nature and frequency of testing and control
Surface condition before blasting - Every pipe
Steel imperfection ISO 8501-3 Grade P3 Every pipe
Dimensions, shape and properties of abrasive blasting 150 µS/cm
ASTM D-4940- Twice per shift
Cleaning before abrasive blasting SSPC-SP1 Free of oil, grease, etc. Every pipe
Degree of cleanliness (dust level) ISO 8502-3 < Class 2 First 10 pipes and 4 time per shift
As per Coating
Temperature of heating before coating IR camera recording Every pipe
Manufacturer
Appearance and continuity Visual Free of defects Every pipe
Thickness of the primer EN 10288 Annex A As per requirement First 10 pipes and 1 per hour
Thickness of the coating system EN 10288 Annex A As per requirement First 10 pipes and 1 per hour
Cut back Visual As per requirement Every pipe
Holiday detection EN 10288 Annex B As per requirement Every pipe
Impact resistance EN 10288 Annex C As per requirement Once per week
2 Tests once per shift at 23°C
Peel force EN 10288 Annex D As per requirement
2 Tests once per week at 60°C
Indentation resistance EN 10288 Annex E As per requirement Once per week
Electrical insulation resistance EN 10288 Annex F As per requirement To be agreed at pre-job meeting
Table 7
Elongation at break EN 10288 Annex G As per requirement To be agreed at pre-job meeting
Resistance to ultraviolet irradiation EN 10288 Annex H.1 As per requirement To be agreed at pre-job meeting
Thermal stability EN 10288 Annex H2 As per requirement To be agreed at pre-job meeting
Cathodic disbonding EN 10288 Annex J As per requirement To be agreed at pre-job meeting
Eni S.p.A.
APPENDIX “E”
PLASTIC TAPE OR SHRINKABLE SLEEVES COATINGS ON EXTERNAL SURFACES
OF STEEL PIPES AND COMPONENTS
20550 PIP.COR.FUN
Appendix “E” - Page 2 of 9
CONTENTS
APPENDIX “E” ............................................................................................................................................ 1
1 GENERAL................................................................................................................................ 3
1.1 INTRODUCTION...................................................................................................................... 3
1.2 SCOPE..................................................................................................................................... 3
1.3 OPERATIVE ENVIRONMENT................................................................................................. 3
1.4 REFERENCE STANDARDS.................................................................................................... 3
2 GENERAL COATING CHARACTERISTICS .......................................................................... 3
3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM ............................... 3

3.1 GENERAL CRITERIA .............................................................................................................. 3
3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING .............................. 4
3.3 COATING MATERIALS CHARACTERISATION TEST ........................................................... 4
3.3.1 Labelling................................................................................................................................... 4
3.3.2 Product information.................................................................................................................. 4
3.4 COATING SYSTEM CHARACTERISATION TESTS .............................................................. 4
3.4.1 Preparation of steel samples ................................................................................................... 5
3.5 QUALIFICATION TESTS......................................................................................................... 5
3.6 FINAL REPORTING OF LAB................................................................................................... 5
4 PRACTICAL APPLICATION TEST IN THE SHOP ................................................................ 7
5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION........................................ 7

5.1 PREHEAT ................................................................................................................................ 7
5.2 SURFACE PREPARATION ..................................................................................................... 7
5.3 COATING APPLICATION........................................................................................................ 8
5.3.1 Thickness of the coating system.............................................................................................. 8
5.4 CUT BACK ............................................................................................................................... 8
5.5 REPAIR OF DEFECTS............................................................................................................ 8
6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE................ 8

6.1 GENERAL ................................................................................................................................ 8
6.2 QUALITY CONTROL PLAN..................................................................................................... 8
6.2.1 Tests during the works progress and final inspection.............................................................. 9
7 DOCUMENTATION AND REPORTING.................................................................................. 9

1 GENERAL
1.1 INTRODUCTION
This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and
for no reason can be used separately. All requirements, standards and articles reported in the
Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix.
It refers to the European Standard EN 12068 (External organic coating for the corrosion protection
of buried or immersed steel pipelines used in conjunction with cathodic protection: Tapes and
Shrinkable materials) the content of which must be considered an integral part of this Appendix.
Moreover, the Company’s additional functional requirements for pre-qualification and application
of the coatings are defined.
1.2 SCOPE
application of Plastic Tape or Shrinkable sleeves coating to external surfaces of steel pipes and
components for buried or immersed services as defined in Item 1 of standard EN 12068.

Item 4 of standard EN 12068 defines the classification of Plastic Tape or Shrinkable coating on
the basis of their mechanical loss resistance, maximum service temperature and of special
condition of use.
For the mechanical resistance the coating combination considered by this Appendix shall be
Class “C” of standard EN 12068, High mechanical resistance coating.
For the maximum service temperature and special condition of use, the Classes considered by
this Appendix are all those defined in the Items 4.1.3 and 4.1.4 of standard EN 12068.

documents.
copies of each relevant standard whenever work takes place. Contractor shall provide evidence of
provision of standards to the Company before work begins and during each inspections step.

The different type of coatings that are considered by this Appendix are listed in Item 3.2 of
standard EN 12068 “Qualification of coating material and coating system”.

All requirements provided by Item 2.4 of Functional Specification. 20550 PIP.COR.FUN. Rev. 0
Qualification requirements shall apply to all coating materials and coating systems subject of this
Appendix.
The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix.
The tests shall be performed and suitably reported by independent laboratory, qualified and
approved by the Company. The Company reserve the right to attend and inspect the tests
execution.

Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform
the Company in writing.
The application documentation shall include all data listed in Tables 3 to 7 of standard EN 12068.
In addition the following data must be provided:
e) Reference list of the major projects reporting at least the following information: name of the
project, name of the customer, name of the applicator, year in which the work was performed,
length and dimension of the pipeline coated.
3.3.1 Labelling
containers bearing the coating manufacturer’s label, clearly showing following information:
a) Name of the coatings material;
b) Coating manufacturer name;
d) Batch number of each component;

the selected laboratory with the information listed in the Tables 3 to 7 of standard EN 12068.
For all data provided, the Coating Manufacturer must report the method and standard used, the
figure assured and related acceptable deviations.
For each Batch Number three samples shall be drawn: one will be used for the analysis, while the
other two will be kept, for a time not exceeding the shelf life reported on the product data sheet,
for possible further checks.

material forming the coating systems, together with detailed mixing and application instructions.
The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe) as
defined in the next paragraph.
Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix are carefully followed.
The selected laboratory shall supervise, record and report all coating work steps. The Company
reserve the right to attend during preparation of samples.

Test sample shall be representative for the production and shall be prepared according to the
provisions of standard EN 12068.
If not otherwise specified as general rule the pipe sections shall have the following dimension:
• Length 700 mm, Diameter 150-300 mm (6-12”), Wall Thickness 4 mm minimum.

For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one
shall be identified and kept for possible checks and controls.
Specification 20550 PIP.COR.FUN. Rev. 0, including but not limited to inspections, controls and
testing reports of each working step.
The coating application shall be performed using the same method for which the qualification is
required and to the same application parameters (e.g. thickness).
The coated samples may be tested immediately after complete curing or suitably stored. However
the tests must be executed within 3 months from the preparation of the samples.

Two coated samples shall be used for the execution of each required test. The result of the test
performed on the two samples shall not be in conflict or different. The results will be considered
acceptable if all results conform to the requirements and acceptance criteria of this Appendix.
The tests to be performed and the acceptance criteria are reported in Tables 1 and 2.

TABLE 1
Standard Method Acceptance criteria
Test Type Max Temp
EN 12068 Cathodic Disbonding Peeling tape on tape Peeling from pipe
Impact Resistance, At 23°C 30/50/HT Appendix H ≥ 15 J ≥ 15 J ≥ 15 J
Indentation Resistance
2 2 2
At 23°C 30 10,0 N/mm 10,0 N/mm 10,0 N/mm
Appendix G 2 2 2
At operating Tmax 50/HT 10,0 N/mm 10,0 N/mm 10,0 N/mm
residual thickness ≥0,6 mm ≥0,6 mm ≥0,6 mm
Specific electrical insulation resistance
8 2 8 2 8 2
Rs 100 30/50/HT Appendix J ≥ 10 Ωm ≥ 10 Ωm ≥ 10 Ωm
2 2 2
Rs 100/ Rs 70 ≥ 0,8 Ωm ≥ 0,8 Ωm ≥ 0,8 Ωm
Cathodic Disbonding
At 23°C 30/50/HT Appendix K ≤ 10 mm ≤ 10 mm ≤ 10 mm
At operating Tmax 50/HT ≤ 25 mm ≤ 25 mm ≤ 25 mm
Peel resistance tape on tape
Internal tape on internal tape and external tape on internal
tape
At 23°C 30/50/HT ≥1,0 N/mm ≥1,5 N/mm ≥1,5 N/mm
Appendix B
At operating Tmax 50/HT ≥ 0,2 N/mm ≥ 0,2 N/mm ≥ 0,2 N/mm
External tape on external tape
At 23°C 30/50/H ≥ 0,2 N/mm ≥ 0,2 N/mm ≥ 0,2 N/mm
Peeling resistance of the tape
From steel pipe
At 23°C 30/50/HT ≥0,5 N/mm ≥0,75 N/mm ≥1,0 N/mm
At operating Tmax 50/HT Appendix C ≥ 0,05 N/mm ≥ 0,075 N/mm ≥ 0,1 N/mm
From coating applied on shop
At 23°C 30/50/HT ≥ 0,4 N/mm ≥ 0,4 N/mm ≥ 0,4 N/mm
Lap shear strength
At 23°C 30/50/HT Appendix D ≥ 0,05 N/mm
2
≥ 0,05 N/mm
2
≥ 0,05 N/mm
2
2 2 2
.
TABLE 2
Standard Method
Test Type Classes Acceptance criteria
EN 12068
Thermal ageing, relation between
125 ≥ B100/B0 ≥ 0,75
• Resistance to scratch
B100/B70 ≥ 0,8
125 ≥ E100/E70 ≥ 0,75
• Elongation to break
All classes Appendix E E100/E70 ≥ 0,8
P100/PT ≥ 0,75
• Resistance to peeling tape on tape
P100/P70 ≥ 0,8
A100/AT ≥ 0,75
• Resistance to peeling on steel pipe
A100/A70 ≥ 0,8
UV radiation resistance, relation between
Class UV
• Elongation to break Appendix F 125 ≥ EX/E0 ≥ 0,75
only
• Resistance to scratch 125 ≥ BX/B0 ≥ 0,75
Low- temperature flexibility
Class L No delamination
At –20°C Appendix N
Class VL No cracking or scratch
Below –20°C
No variation compared to the
Microbiologic resistance All classes Appendix M
not buried samples

b) The correctness and suitability of the instructions provided by coating manufacturer;
5.1 PREHEAT
The pipe or component shall be preheated to at least 5°C above the dew point to remove the
presence of moisture prior to surface cleaning.

Surface preparation shall be performed according to the recommendations of the Coating
Manufacturer reported in the product data sheet of each material, as required in Table 7 of
standard EN 12068 and to the specific functional requirements reported in item 2.5 of

Coatings material application shall be performed in accordance with Coating Manufacturer’s
recommendation reported in the product data sheet of each material, as required in Table 7 of
standard EN 12068 and to the specific functional requirements reported in item 2.6 of

The minimum thickness of the coating system at any point shall correspond to the value
reported in the product data sheet of each material, as required in Table 7 of standard EN
12068 depending on the type and class of the coating specified.
5.4 CUT BACK

Where applicable the pipe surface shall be left bare (uncoated) at both ends of the pipe for
(150 ± 20) mm distance from the ends and the coating shall be beveled at the cut back forming
a bevel angle of ≤30° unless otherwise specified. For fittings and components cut back shall
be specified and approved by the Company’s Representative.
perfectly clean and free from any traces of coating.

The Contractor shall repair all coating defects and damages that may occur during or after the
Coating and any other material used for the repair of defects and damages shall be supplied
by the same Coating Manufacturer of the original Coating system.
Any repair shall be performed according to specific Coating Manufacture’s recommendation as
required in Table 7 of standard EN 12068.
The acceptability of coating repair and the repair procedure is subject to agreement between
the Company and Contractor.
6.1 GENERAL
Bid.
The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.



inspections and tests required by Functional Specification 20550 PIP.COR.FUN. Rev. 0 and
by this Appendix, including, but not limited to:
• Surface condition of the pipes or component;
• Steel imperfection;
• Dimension and properties of the abrasive material, if applicable;
• Degree of surface preparation;
• Degree of cleanliness;
• Relative humidity, dew point, steel temperature;
• Appearance and continuity of the coating;
• Coating thickness;
• Cut back, if applicable;
• Holyday detection;
• Peel force;
• Etc.

Eni S.p.A.
APPENDIX “F”
EPOXY POWDER COATING ON EXTERNAL SURFACES OF STEEL PIPES AND
COMPONENTS
20550 PIP.COR.FUN
Appendix “F” - Page 2 of 10
CONTENTS
APPENDIX “F” ....................................................................................................................................... 1
1 GENERAL........................................................................................................................... 3
1.1 INTRODUCTION................................................................................................................. 3
1.2 SCOPE................................................................................................................................ 3

3.2 DOCUMENTATION FOR THE PRE-QUALIFICATION OF THE COATING ...................... 4
3.3.1 Labelling.............................................................................................................................. 4

5.1 PREHEAT ........................................................................................................................... 8
5.3.1 Coating Thickness .............................................................................................................. 9
5.4 CUT BACK .......................................................................................................................... 9

6.1 GENERAL ........................................................................................................................... 9
6.2.1 Tests during the works progress and final inspection....................................................... 10

1 GENERAL
1.1 INTRODUCTION
It refers to the NACE Standard RP 0394 “Application, Performance, and Quality Control of
Plant-Applied, Fusion-Bonded Epoxy External Pipe Coating”, the content of which must be
considered an integral part of this Appendix.
1.2 SCOPE
This Appendix defines the minimum requirements for qualification, supply and application of
fusion-bonded epoxy (FBE) coatings to the external surfaces of steel pipes and components
for onshore and offshore service as defined in Section 1 of NACE standard RP0394.

documents.
inspections step.

The coating system considered by this Appendix is the epoxy resin powders applied by fusion.
To meet the minimum requirements listed in Table 2 of this appendix the coating thickness
shall be 360 ± 50 microns (µm).
The Company, taking in consideration the specific requirements of the Project Technical
Specification, shall specify the minimum and maximum thickness.
However the differential between minimum and maximum thickness shall not be less than 100
µm.

Qualification requirements shall apply to all coating materials and coating systems subject of
this Appendix.
If the formulation of one or all coatings materials forming a coating system is changed after the
3.2 DOCUMENTATION FOR THE PRE-QUALIFICATION OF THE COATING

The documentation forwarded to the Company shall include all data listed in Table 1 of this
Appendix. In addition the following data must be provided:
a) Material Safety Data Sheet of each product;
3.3.1 Labelling
Each coating material, to be tested shall be delivered and stored in original containers bearing
the Coating Manufacturer’s label, clearly showing following information:
a) Name of the coating material;
d) Batch number of each product;

the selected laboratory with the following information:
• Product Data Sheet (PDS);
• Material Safety Data Sheet (MSDS);
• Date of issue of PDS;
• Date of issue of MSDS;
• Name of Coating Manufacturer;
• Name and type of the product;
• Factory of origin;
• Batch number;
• Shelf life;
• Physical state of delivered product;

• Packaging;
• Storage condition;
• Sieve analysis;
• Gel time;
• Specific gravity;
• Moisture content;
• Bend test;
• Finger printing – Infrared scans of each component of a coating material with and without
certify the finger printing, reporting the method and resolution used.
consistency of the data for physical properties provided by the Coating Manufacturer, including
and listed in Table 1.
The epoxy powder shall meet the value limits for the properties listed in following table:
Table 1
Epoxy Powder Properties
Property Test Method Acceptance criteria
NACE RP0394
Density As per Coating Manufacturer’s specification ± 3,5%
Appendix B
Particle Size 2% max retained on 150 µm (100 mesh) sieve;

0,1 % max retained on 250 µm (60 mesh) sieve;
NACE RP0394
Shelf life As per Coating Manufacturer’s recommendation
Appendix C
NACE RP0394
Gel Time As per Coating Manufacturer’s specification ± 20%
Appendix D
As per Coating Capable of cure at temperatures below 275°C; time:
Cure Cycle
Manufacturer as per Coating Manufacturer recommendation.
Glass Transition (Tg) NACE RP0394
As per Coating Manufacturer’s recommendation
Temperatures Appendix E
NACE RP0394
Heat of reaction As per Coating Manufacturer’s s recommendation
Appendix E
NACE RP0394
Moisture content 0,5 % max
Appendix F
NACE RP0394
Total volatile Content 0,6 % max
Appendix G

(e.g. pipe and steel panels) as defined in the next paragraph.
Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix.
and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and Appendix
are carefully followed. The selected laboratory shall supervise, record and report all coating
work steps.

dimension:
a) Pipe section: Length 700 mm, Diameter 150-300 mm (6-12”), Wall Thickness 4 mm
minimum;
standard NACE RP0394, the requirements laid in the standard NACE RP0394 shall apply.
is required and to the same application parameters (e.g. DFT).

Appendix.

Table 2
Standard/Method
Test Type Acceptance criteria
NACE RP0394
Cathodic Disbonding (24 h) Appendix H Max. radius: 8 mm
Cathodic Disbonding (28 d) Appendix H Max. radius: 10 mm
Chemical Resistance Appendix I No blistering
Cross-Section Porosity Appendix J Rating of 1 to 3
Interface Porosity Appendix K Rating of 1 to 4
Flexibility Appendix K No cracks, tears or delamination
Impact Resistance Appendix L 1,5 J min
Strain Polarization Appendix M No cracking
Thermal Analysis (Differential Scanning As per Coating Manufacturer’s
Appendix E
Calorimetry) recommendations
Hot Water Soak Appendix N A rating of 1 to 3, inclusive
Abrasion Appendix O Max. 300 mg
Penetration ASTM G 17 at 93°C Less than 10%

practical test shall be performed in the shop in order to ascertain:
any, faced during the application;
At completion of the application test, all the checks listed in Table 4 shall be performed;
Table 3
Production test Requirements
Test Method
Test Acceptance Criteria
NACERP0394
Cathodic Disbonding (24 h) Appendix H Max radius: 12mm(1)
Flexibility Appendix K No cracks, tears, or delamination(1)
Hot water Soak Appendix N Rating of 1 to 3, inclusive (1)
Interface Contamination Appendix P Max 30%(2)
Cross-Section Porosity Appendix J Rating of 1 to 3, inclusive (2)
Thermal Characteristics Appendix E Tg of 5°C, max or 95% conversion H minimum (3)
Impact Resistance Appendix L 1,5 J minimum (3)
(1) The failure of this tests shall be grounds for rejection of all pipe coated after the previous acceptable test and prior to
the next acceptable test result.
(2) The failure of this test shall be grounds for requiring changes to the application process parameters.
(3) This test is required only when specified by the Company.
5.1 PREHEAT
temperatures.

Surface preparation shall be performed fully in accordance with the specific functional
requirements reported in Item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.

Coatings shall be applied in accordance with the functional requirements reported in item 2.6
of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and with the Coating Manufacturer’s
recommendations as defined in Section 7 of standard NACE RP0394.
Powder recycling shall be allowed up to a proportion of 10%, suitable mixed with fresh powder.
The recycled powder shall be clean and passed through a magnetic filter to remove metallic
particles and through a 120 mm sieve to remove all aggregates.
5.3.1 Coating Thickness

The Dry film thickness (DFT) shall be 360 (±50) µm and the absolute minimum thickness shall
not be less 310 µm.
Coating thickness shall be measured fully in accordance with the requirements of Item 5.3.3.2
of standard NACE RP0394.
5.4 CUT BACK

Once the coating operations are completed, cut-back areas shall be protected from corrosion

Any repair shall be performed according to Section 9 of standard NACE RP0394 and method
submitted to the Company for approval beginning of the production.
6.1 GENERAL
Bid.


inspections and tests reported in Table 4:
Table 4
Inspection during work progress
Test Test method Frequency
Surface Preparation ISO 8501-1 Continuously
Surface Profile ISO 8503-1 Once per four hour
Surface Inspection - Each pipe
Application Temperature - Each pipe
Application criteria - Systematically during any application
3 location on each pipe
(The acceptance criteria of the test shall be in
Coating Thickness -
accordance with the provisions of item 8.3.3.7
of standard NACE RP0394)
Each pipe
(The acceptance criteria of the test shall be in
Holiday inspection NACE RP0490
accordance with the provisions of item 8.3.3.8
of standard NACE RP0394)
At minimum one sample for each of the lots
Production Test Rings - defined in paragraph 8.3.4 of standard NACE
RP0394

Eni S.p.A.
APPENDIX “G”
ANTICORROSIVE FILLER MASS ON WELDED JOINTS AREAS OF STEEL PIPES
AND COMPONENTS
20550 PIP.COR.FUN
Appendix “G” - Page 2 of 11
CONTENTS
APPENDIX “G”....................................................................................................................................... 1
1 GENERAL........................................................................................................................... 3
1.1 INTRODUCTION................................................................................................................. 3
1.2 SCOPE................................................................................................................................ 3

3.2 DOCUMENTATION FOR THE PRE-QUALIFICATION OF THE COATING ...................... 4
3.3.1 Labelling.............................................................................................................................. 4

5.1 PREHEAT ........................................................................................................................... 8
5.3.1 General ............................................................................................................................... 8
5.3.2 Application method ............................................................................................................. 8
5.3.3 Coating thickness................................................................................................................ 9

6.1 GENERAL ........................................................................................................................... 9
6.2.1 Tests during the works progress and final inspection......................................................... 9

1 GENERAL
1.1 INTRODUCTION
Moreover, the Company’s additional functional requirements for qualification and application of
the coating are defined reported.
1.2 SCOPE
This Appendix defines the minimum functional requirements for pre-qualification, supply and
application of anticorrosion filling mass of polyurethane base, that shall be applied immediately
before pipe laying for refilling and protection of the weld of the steel pipes and component.

External polyurethane mass coating can be used for the protection of buried or submerged
tubes service and suitable for the following maximum service temperature:
• From –20° to +80°C for applications at ambient temperature or medium temperatures
(standard coating);
• From –20° to +120°C for high temperatures offshore application (thermal stabilised
coating);
• From –20° to +110°C for high temperatures onshore buried pipelines (thermal stabilised
coating).

Specification 20550 PIP.COR.FUN. Rev. 0
documents.
inspections step.

The coating systems considered by this Appendix are based on polyurethane resins and
special fillers with regulating density. The product may be formed by a base component, a
hardening agent, filler and an accelerator (if applicable).
As general guide, the coating shall be applied with a Dry Film Thickness (DFT) in the range of
10 to 500 mm. Application can be made by extrusion or by gravity casting, into a metal mould
positioned around the welded joint pneumatically or by hand. The final coating shall have a
continuous and uniform film free of sags, runs or any other visible defect.
The Dry Film Thickness shall be selected in consideration of the product and intended service
operation.

Qualification requirements shall apply to all coating materials and coating systems subject of
this Appendix.
If the formulation of one or all coatings materials forming a coating system is changed after the
3.2 DOCUMENTATION FOR THE PRE-QUALIFICATION OF THE COATING

The documentation forwarded to the Company shall include all data listed in Table 1 In
e) Name and address full style of the laboratory where the tests will be performed;
3.3.1 Labelling
container bearing the Coating Manufacturer’s label, clearly showing following information:
a) Name of the coating material (Base, Hardener, Filler, Accelerator);
d) Batch number of each component (Base, Hardener, Accelerator);

the selected laboratory with the following information:
• Product Data Sheet (PDS);

• Material Safety Data Sheet (MSDS);
• Date of issue of PDS;
• Date of issue of MSDS;
• Name of Coating Manufacturer;
• Name and type of the products;
• Date of manufacture;
• Factory of origin;
• Batch number;
• Shelf life;
• Colour of the mixed product;
• Method of application;
• Physical state of delivered product;
• Method of application;
• Solids content;
• Packaging;
• Storage condition;
• Pot life;
• Shelf life;
• Surface preparation;
• Mixing ratio (by weight);
• Mixing instructions;
• Recommended cleaning solvent(s);
• Recommended instruction for application;
• Range of application temperature (ambient, pipe and product) and humidity;
• Range of service temperature;
• Recommended minimum and maximum DFT;
• Specific curing requirements;
• Time to complete curing;
• De-moulding time;
• Viscosity of the base and curing agent according to standard ISO 2555 at temperature of
5, 15, 25, 35 and 40°C;
• Finger printing – Infrared scans of each component of a coating material with and without
• Thermal analysis, reporting the method used:
Curve of curing reaction with temperature scan from ambient temperature to the end
of reaction;
Glass Transition (Tg) temperature;
Scan speed (°C/min);
Temperature at the beginning of the reaction, max temperature at the end of the
reaction and heat content.
The tests shall be performed both for the base and the curing agents.

(e.g. pipe) as defined in the next paragraph.
other suitable location provided that the Company is informed and the requirements of
Functional Specification 20550 PIP.COR.FUN. Rev. 0 and Appendix are carefully followed.
The selected laboratory shall supervise, record and report all coating work steps. The

The tests shall be performed on carbon steel samples as described in the following items.
3.4.1.1 Steel pipes samples
Since one of the main scope of the qualification tests of weld field joint coating is to ascertain
its compatibility with shop applied coating, steel pipes samples must be coated with one or
more system listed in Table 1 and for which the Coating Manufacturer of weld field joint
coating requires the qualification.
The length of the coated steel pipe shall be such as to assure that the length of the test zones
is equivalent to the field joint coating plus the overlap areas. The minimum acceptable
dimension of coated steel pipe sections is: Length 1000 mm, Diameter 150 mm (6”), and Wall
thickness 5 mm.
The test zone shall be free of any coating and a girth cap weld shall be added at the centre of
it in order to mimic the field weld.
The time for coating application on a test zone shall not exceed the estimated field joint
coating time on shop, yard, on the barge, etc.
3.4.1.2 Steel panels

Where applicable, the dimension of steel panels sample shall be: 300 x 300 mm, Thickness 5
mm.
3.4.1.3 General
according to all requirements provided by items 5, and 6 of this Appendix and the Functional
is required and to the same application parameters (e.g. DFT).

Appendix.
TABLE 1
Compression strength ASTM D 695 45 Mpa
3
25 cm specimen immerged in sea
No loss in properties. No
Sea water resistance water for 1000 hours at temperatures
significant water absorption
varying from 18°C to 40°C
Cylindrical specimen, 60 mm.
Impact resistance diameter 60 mm. high, under a 5 kg No breaks – No cracks
sphere falling from 1,5 m
Cubic specimen, 60 mm side,
exposed to 10 cycles as follows No variation in any one
Resistance to temperature
dimension, no loss in
changes 1 hour in 90°C
properties
1 hour in 0° C refrigerator
Thermal resistance Cubic specimen, 60 mm side, No variation in any one
dimensional stability exposed 4 hours at 135°C dimension
Apparent density ASTM D 1622 1500 Kg/m3 ± 1,5 %
Cathodic disbonding ASTM G8 Max 9 mm
Tensile strength ASTM D 638 Average 11 MPa
Resistance to bacterial No variation compared to
attack the not buried samples
De-moulding time ≤ 5 min.


At completion of qualification tests of coating materials and coating systems, a practical test
shall be performed in the shop in order to ascertain:
b) The correctness and suitability of the instruction provided by Coating Manufacturer;
Company can required additional specific tests if consider necessary for a particular project.
5.1 PREHEAT
temperatures.
The pipe shall be preheated to at least 5° C above the dew point to remove the presence of
moisture prior to surface cleaning; it shall be checked at least three times for every work shift
(at start, middle, and end) and whenever stoppages occur in the production line.

Surface preparation shall be performed fully in accordance with specific functional
requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
5.3.1 General
Coatings shall be applied fully in accordance with the Coating Manufacture’s
recommendations and to the specific functional requirements reported in item 2.6 of Functional
5.3.2 Application method

As general requirements the coating mass shall be applied either by extrusion or by gravity
casting, into a metal mould positioned around the weld joint pneumatically or by hand.
The filling mass shall be introduced in the mould by extrusion equipment that automatically
doses and mixes the components, or by direct casting from a container of the previously dosed
and thoroughly stirred component mix.
The extrusion equipment shall include all the component suitable to perform a correct
application according to the Coating Manufacturer recommendation
5.3.3 Coating thickness

The minimum and maximum coating thickness shall be in accordance with the characteristic of
the product and intended service operation.
The minimum and maximum coating thickness shall be in accordance with Coating
Manufacturer’s recommendation.

The Contractor shall repair all coating defects and damages that may occur during or after the
application.
Coating used to repair of defects and damages shall be supplied by the same Coating
Manufacturer of the original Coating system.
Any repair shall be performed according to Coating Manufacturer recommendations and the
method submitted to the Company for approval before the beginning of the production.
6.1 GENERAL
Bid.
The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.


inspections and tests reported in the Table 2.

Table 2
Surface condition before blasting - Every weld joint
Steel imperfection ISO 8501-3 Grade P3 Every weld joint
Dimensions, shape and properties of abrasive blasting 150 µS/cm
ASTM D-4940- Twice per shift
Cleaning before abrasive blasting SSPC-SP1 Free of oil, grease, etc. Every weld joint
Degree of cleanliness (dust level) ISO 8502-3 < Class 2 First 10 weld joint and 4 time per shift
As per Coating
Temperature of heating before coating IR camera recording Every weld joint
Manufacturer
Appearance and continuity Visual Free of defects Every weld joint
Thickness of the coating system - As per requirement First 10 pipes and 1 per hour
Eni S.p.A.
APPENDIX “H”
FUNCTIONAL REQUIREMENTS FOR THE QUALIFICATION AND APPLICATION OF
PROTECTIVE COATING ON EXTERNAL WELD JOINTS OF ONSHORE AND
OFFSHORE PIPELINES
20550 PIP.COR.FUN
Appendix “H” - Page 2 of 11
CONTENTS
APPENDIX “H” ....................................................................................................................................... 1
1 GENERAL........................................................................................................................... 3
1.1 INTRODUCTION................................................................................................................. 3
1.2 SCOPE................................................................................................................................ 3

2.1 TYPES OF FIELD JOINT COATINGS................................................................................ 3
2.2 CRITERIA FOR COATING SELECTION............................................................................ 4

3.3.1 Labelling.............................................................................................................................. 5
3.6 PRACTICAL APPLICATION TEST IN THE SHOP............................................................. 7

4.1.1 General ............................................................................................................................... 7
4.1.2 Power tool cleaning............................................................................................................. 7
4.1.3 Abrasive blasting tool cleaning ........................................................................................... 7
4.1.4 Overlapping areas............................................................................................................... 8
5 SPECIFIC REQUIREMENTS FOR COATING APPLICATION ......................................... 9

5.1 HEAT-SHRINKABLE MATERIALS APPLICATION ............................................................ 9
5.2 POLYMERIC PLASTIC TAPES .......................................................................................... 9
5.3 FUSION-BONDED EPOXY POWDER ............................................................................... 9
5.4 INJECTION APPLIED POLYPROPYLENE ........................................................................ 9
5.5 INJECTION APPLIED POLYURETHANE ........................................................................ 10
5.6 LIQUID EPOXY RESIN (TAR FREE) ............................................................................... 10
5.7 LIQUID POLYURETHANE (TAR FREE) .......................................................................... 10

6.1 GENERAL ......................................................................................................................... 10
6.2 CHECKS INSPECTION AND TESTING........................................................................... 10
6.2.1 Tests during the works progress and final inspection....................................................... 10

1 GENERAL
1.1 INTRODUCTION
application of the coatings are defined.
1.2 SCOPE
This Appendix defines the minimum functional requirements for qualification, selection, supply
and application of the external weld field joint coatings.
The coatings for weld field joint coatings shall ensure the suitable corrosion protection and
coating continuity to the steel pipes surface left bare (uncoated) during coating application on
shop. They are applied when pipes are joined by welding to form pipelines used for onshore or
offshore oil, gas or water transportation.

Specification 20550 PIP.COR.FUN. Rev. 0
documents.
inspections step.

Weld field joints shall be protected with a coating system compatible with the coating already
applied on the pipes and allow suitable application under the conditions expected to be faced
on the field.
2.1 TYPES OF FIELD JOINT COATINGS

The coatings for weld joints considered in this Appendix are listed in Table 1.
TABLE 1
TYPE OF FIELD JOINT COATINGS
Heat-shrinkable materials
Polymeric plastic tapes
Fusion-bonded epoxy powder
Injection applied polypropylene
Injection applied polyurethane
Liquid epoxy resin (tar free)
Liquid polyurethane (tar free)
2.2 CRITERIA FOR COATING SELECTION

The external coatings for the corrosion protection of steel pipes and components provided by
Functional Specification 20550.PIP.COR.FUN. Rev.0 are defined in the various appendixes as
follows:
• Appendix “A”: Liquid epoxy and epoxy-modified coating;
• Appendix “B”: Liquid polyurethane and polyurethane-modified coating;
• Appendix “C”: Three layers extruded polyethylene (PE) coating;
• Appendix “D”: Three layers extruded polypropylene (PP) coating;
• Appendix “F”: Epoxy Powder (FBE) coating.

The field joint coatings has to satisfied the following requirements:
a) It must be compatible with one or more coating provided by the above Appendixes;
b) It must be resistant to the service temperature of the pipeline;
c) It must be suitable for the application condition and process provided on the various fields.

Qualification requirements shall apply to all coating materials and coating systems, included
If the formulation of one or all coating materials forming a coating system shall be changed
after the qualification test, the new coating material and coating system shall be re-qualified.

The application documentation shall include all data concerning each weld field joint coating
for which the pre-qualification is required, including, but not limited to:
a) Name of the coating system;
b) Product Data Sheet;
c) Code of the coating as listed in Table 1 of this Appendix;
d) Compatibility of the proposed coating with the coating system provided in the Appendixes
of Functional Specification 20550 PIP.COR.FUN. Rev.0;
e) Finger printing (where applicable) – Infrared scans of each component of a coating
material with and without pigment. Coating Manufacturer’s Product Quality Manager shall
certify the finger printing;
f) Application procedures;
g) Material Safety Data Sheet of each component;
h) Name and address of the laboratory where the tests will be performed;
i) Reference list of the major projects reporting at least the following information: name of
performed, length and dimension of the pipeline coated, coating type applied on the
pipeline.

The characterisation test of the coating materials and coating systems for weld joint have to
satisfy the requirements reported in Table 2.
TABLE 2
Characterisation tests
TYPE OF COATING CHARACTERISATION
Heat-shrinkable materials As per Appendix “E” requirements
Polymeric plastic tapes As per Appendix “E” requirements
Fusion-bonded epoxy powder As per Appendix “F” requirements
Injection applied polypropylene As per Appendix “D” requirements
Injection applied polyurethane As per Appendix “G” requirements
Liquid epoxy resin (tar free) As per Appendix “A” requirements
Liquid polyurethane (tar free) As per Appendix “B” requirements
3.3.1 Labelling
Each coating material, solvents and thinners to be tested shall be delivered and stored in
original container bearing the Coating Manufacturer’s label, clearly showing following
information:
a) Coating manufacturer name;
b) Name and complete identification of product including factory origin;
c) Reference to applicable coating standards;
e) Batch number of each component;

For each coating material submitted to qualification testing, Coating Manufacturer shall
provide the selected laboratory with the information detailed in each relevant Appendix and
related to the different field joint coating system.
consistency of the data for physical properties provided by the Coating Manufacturer for each
coating as required in Table 2.

material forming the coating systems, together with detailed mixing, where applicable, and
application instruction. The Coating Manufacturer shall also supply a sufficient number of test
samples (e.g. pipe and/or steel panels) as defined in the next paragraph.
Specification 20550 PIP.COR.FUN. Rev. 0 and relevant Appendix.
and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and relevant
Appendix are carefully followed. The selected laboratory shall supervise, record and report all
coating work steps. The Company reserve the right to attend during preparation of samples.

The tests shall be performed on carbon steel samples as described in the following items.
3.4.1.1 Steel pipes samples
Since one of the main scope of the qualification tests of weld field joint coating is to ascertain
its compatibility with shop applied coating, steel pipes samples must be coated with one or
more system listed in Table 1 and for which the Coating Manufacturer of weld field joint
coating requires the qualification.
The length of the coated steel pipe shall be such as to assure that the length of the test zones
is equivalent to the field joint coating plus the overlap areas. The minimum acceptable
dimension of coated steel pipe sections is: Length 1000 mm, Diameter 150 mm (6”), and Wall
thickness 5 mm.
The test zone shall be free of any coating and a girth cap weld shall be added at the centre of
it in order to mimic the field weld.
The time for coating application on a test zone shall not exceed the estimated field joint
coating time on shop, yard, on the barge, etc.
3.4.1.2 Steel panels
Where applicable, the dimension of steel panels sample shall be: 300 x 300 mm, Thickness 5
mm.
3.4.1.3 General
Samples shall be cleaned and coated with the complete weld field joint coating, according to
all requirements provided by this Appendix and Functional Specification 20550 PIP.COR.FUN.
Rev. 0 including, but not limited, to inspections, controls and testing reports of each working
step.
spray, etc.) for which the qualification is required and to the same application parameters.

Appendix.
The tests to be performed and the acceptance criteria are detailed in the items related to the
different field joint coating system.

3.6 PRACTICAL APPLICATION TEST IN THE SHOP

which has to be agreed with the Coating Manufacturer, to enable the evaluation of problem, if

The requirements listed in the following items are common to all field joint coatings.
4.1.1 General
Surface preparation shall be performed in accordance with Coating Manufacturer
recommendations and with the requirements of Functional Specification 20550 PIP.COR.FUN.
Rev.0 and related applicable Appendix.
At the time of coating application, the surface to be coated shall be dry, clean and free of any
foreign material and contaminants.
Any steel and welding imperfection shall be removed to comply with the grade P2 of standard
ISO 8501-3. After removal of the steel imperfections, the thickness of the steel pipe shall
comply with the minimum tolerance requirements of the pipe standard.
4.1.2 Power tool cleaning

Power tool cleaning shall be performed according to standard ISO 8504-2 in order to comply
with grade Sa 2,5 of standard ISO 8501-1. The roughness of the cleaned surface shall be in
accordance with Coating Manufacturer recommendations.
4.1.3 Abrasive blasting tool cleaning

Abrasive blasting shall be performed according to standard ISO 8504-3 in order to comply with
grade St3 of standard ISO 8501-1. The roughness of the cleaned surface shall be in
accordance with Coating Manufacturer recommendations.
4.1.4 Overlapping areas

The shop-applied coating close to the field joint to be coated shall be prepared and abraded to
assure the suitable adhesion of the field joint coating. The method shall be in accordance with
Coating Manufacturer recommendations.
In consideration of the type of shop-applied coating and the field joint coating the dimension
overlap area shall be according to the figure listed in Table 3.
TABLE 3
Overlapping
FIELD JOINT COATING OVERLAP DIMENSION
Heat-shrinkable materials ≥ 100 mm
Polymeric plastic tapes ≥ 70 mm
Fusion-bonded epoxy powder ≥ 50 mm
Injection applied polypropylene ≥ 70 mm
Injection applied polyurethane ≥ 70 mm
Liquid epoxy resin (tar free) ≥ 50 mm
Liquid polyurethane (tar free) ≥ 50 mm

The steel temperature of field joint shall be 3°C above the dew point and within the range of
Coating Manufacturer recommendations.
Field joint temperature must be checked with suitable instrument in order to meet the
application conditions (steel temperature and shop-applied coating) recommended by Coating
Manufacturer.
As general rule coating application shall be done according to the general requirements
reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and related
Appendixes. In particular Coating Manufacturer’s recommendation reported in the product
data sheet shall be followed.
In case an additional mechanical resistance is required, the provisions of Appendix “I” of
Functional Specification 20550 PIP.COR.FUN Rev. 0 shall apply.
Where applicable, Wet Film Thickness and Dry Film Thickness for each type of coating
provided by this appendix shall be in accordance with Coating Manufacturer
recommendations.

The Contractor shall repair all coating defects and damages that will occur during the coating
application or at its completion.
Manufacturer of the original Coating system.
Any repair shall be performed according to Coating Manufacturer’s recommendation reported
in the product data sheet.
5 SPECIFIC REQUIREMENTS FOR COATING APPLICATION
5.1 HEAT-SHRINKABLE MATERIALS APPLICATION

Heat-shrinkable materials may be applied without or with a liquid epoxy primer, depending on
the nature of adhesive. If required the application of epoxy primer shall be made according to
the requirement of Table 7 of standard EN 12068 (ref. Appendix “E” of Functional Specification
20550 PIP.COR.FUN. Rev.0).
For the application of heat-shrinkable materials, in addition to the provision of Appendix “E” of
Functional Specification 20550 PIP.COR.FUN. Rev.0, as general guide the following
procedure shall be implemented:
• When the welding joint has been completed the area shall be cleaned as specified;
• Area to be coated shall be heated to 70°C;
• The shrinkable sleeve must be positioned so as to provide a 100 mm overlap on both
sides of the shop-applied coating suitably abraded to assure the good adhesion when
shrinking is completed;
• By external side heat sleeve to a surface temperature adapted to the specific product to
be applied (from 90 to 240°C) with a hot air ring unit or a gas torch. Heat progressively
and regularly, starting from the middle of the sleeve and going towards the ends to avoid
forming air pockets.
5.2 POLYMERIC PLASTIC TAPES

Polymeric plastic tape may be applied without or with a liquid epoxy primer, depending on the
nature of adhesive. If required the application of epoxy primer shall be made according to the
requirement of Table 7 of standard EN 12068 (ref. Appendix “E” of Functional Specification
20550 PIP.COR.FUN. Rev.0).
For the application of polymeric plastic tape, in addition to the provision of Appendix “E” of
Functional Specification 20550 PIP.COR.FUN. Rev.0, as general guide the following
procedure shall be implemented:
• When the welding joint has been completed the area shall be cleaned as specified;
• Apply a thin coat of compatible primer, if any, and allow the primer to dry.
Spirally wrap the area with tapes of a sufficient width, using the right overlap (no less than
50%) and sufficient tension to ensure a complete adhesion of the coating. Suitable hand tools
shall be used to achieve a suitable coating application (e.g. cigarette wrapping may be used in
certain circumstances).
In any case overlapping shall be made according to Coating Manufacturer recommendations.
5.3 FUSION-BONDED EPOXY POWDER

The application of fusion bonded epoxy powder (FBE) on field joints shall be made fully in
accordance with the provisions of Functional Specification 20550 PIP.COR.FUN Rev.0,
Appendix “F”.
5.4 INJECTION APPLIED POLYPROPYLENE

Injection applied polypropylene coating system consists of:
• An epoxy primer coat, which if in form of powder can be applied by dusting or by
electrostatic spray, if liquid it can be applied by spraying. No primer must be applied to
shop-applied coating.
• One coat of modified polypropylene powder applied by spraying. The coating thickness is
obtained injecting polypropylene in a suitable mould.
Suitable heating system and process shall be used to obtain the proper adhesion of the field
joint coating on the shop-applied coating.
5.5 INJECTION APPLIED POLYURETHANE

The application of injection applied polyurethane on field joints shall be made fully in
accordance with the provisions of Functional Specification 20550 PIP.COR.FUN Rev.0,
Appendix “G”.
5.6 LIQUID EPOXY RESIN (TAR FREE)

The application of liquid epoxy resin on field joints shall be made fully in accordance with the
provisions of Functional Specification 20550 PIP.COR.FUN Rev.0, Appendix “A”.
5.7 LIQUID POLYURETHANE (TAR FREE)

The application of liquid polyurethane resin on field joints shall be made fully in accordance
with the provisions of Functional Specification 20550 PIP.COR.FUN Rev.0, Appendix “B”.
6.1 GENERAL
The additional requirements for Quality Management and/or Quality Assurance are contained
in the applicable “Quality and Execution Requirements Specification” attached to the Invitation
to Bid.
6.2 CHECKS INSPECTION AND TESTING

g) Persons required to be present at the inspections;

inspections and tests reported in the items related to the different field joint coating system.
The specific requirements provided in the Appendixes listed in Table 2 and item 4 of
Functional Specification 20550.PIP.COR.FUN Rev. 0 shall be fully followed unless otherwise
specified by the Company.
As general rule, the Contractor shall perform during the work progress and at completion of it
at least the inspection and test reported in Table 4. The feasibility of the test listed in Table 4 is
related to the specific site condition of the project such as production rate, location etc. In any
case all data concerning each inspection step, or the reasons for that it has not been
performed, shall be permanently recorded in report or logbook.

Table 4
Inspection during the work progress
Test Method of test Frequency
Surface preparation ISO 8501-1 Each weld joint
Roughness of the blast cleaned surface of Checks number to be agreed with the
ISO 8503-1
the weld joint Company
Temperature of the surface to be coated - Each weld joint
Three times per shift and any time the
Thermo-hygrometric condition -
condition changed
Application criteria - Systematically during any application
Visual inspection of the coating - Each weld joint
Inspection of the thickness - Once per shift
Holiday detection test NACE RP 0274 Each weld joint
Checks number to be agreed with the
Adhesion test DIN 30671
Company
Checks number to be agreed with the
Cathodic disbonding DIN 30671
Company
Eni S.p.A.
APPENDIX “I”
POLYURETHANE THERMAL INSULATION SYSTEMS TO PIPE AND ASSEMBLY OF
INSULATED PIPES, VALVES AND FITTINGS
20550 PIP.COR.FUN
Appendix “I” - Page 2 of 12
CONTENTS
APPENDIX “I”......................................................................................................................................... 1
1 GENERAL........................................................................................................................... 3
1.1 INTRODUCTION................................................................................................................. 3
1.2 SCOPE................................................................................................................................ 3

2.1 CHARACTERISTIC OF THE PRIMER ............................................................................... 4
2.2 CHARACTERISTIC OF THE POLYURETHANE RIGID FOAM (PUR) .............................. 4
2.3 CHARACTERISTIC OF THE CASING ............................................................................... 4

3.3.1 Labelling.............................................................................................................................. 6

5.1 PIPE ASSEMBLY ............................................................................................................... 9
5.1.1 Surface preparation ............................................................................................................ 9
5.1.2 Coating Application ............................................................................................................. 9
5.1.3 Thickness of the coating system......................................................................................... 9
5.1.4 Centre line deviation ........................................................................................................... 9
5.1.5 Cut back ............................................................................................................................ 10
5.1.6 Repair of defects............................................................................................................... 10
5.2 FITTINGS ASSEMBLIES.................................................................................................. 10
5.2.1 Surface preparation .......................................................................................................... 10
5.2.3 Centre line deviation ......................................................................................................... 10
5.2.4 Cut back ............................................................................................................................ 10
5.2.5 Angular between casing segments of bend and minimum length .................................... 10
5.2.6 Polyethylene welding ........................................................................................................ 11
5.2.7 Increase of the diameter of the casing pipe...................................................................... 11
5.2.8 Minimum insulation thickness in bends ............................................................................ 11
5.2.9 Tolerance of the main fitting dimensions .......................................................................... 11

6.1 GENERAL ......................................................................................................................... 11

1 GENERAL
1.1 INTRODUCTION
It refers to the following European Standards:
• EN 253 (District heating pipes – Preinsulated bonded pipe system for directly buried hot
water networks – Pipe assembly of steel service pipe, polyurethane thermal insulation and
outer casing of polyethylene)
• EN 448 (District heating pipes – Preinsulated bonded pipe system for directly buried hot
water networks – Fitting assemblies of steel service pipe, polyurethane thermal insulation
and outer casing of polyethylene)
1.2 SCOPE
application for straight lengths and fittings assemblies (e.g. bends, T-pieces, reducers and
anchor) of prefabricated thermal insulated pipe-in-pipe assemblies, comprising as steel service
pipe from DN 20 to DN 1200, rigid polyurethane foam insulation and an outer casing of
polyethylene as defined in item 1 of standard EN 253 and item 1 of standard EN 448.

Polyurethane thermal insulation and outer casing of polyethylene coating can be used for the
protection of buried or submerged pipes and fittings for continuous service at various
temperatures up to 120°C and occasionally with a peak temperature up to 140°C as defined in
item 1 of standard EN 253.

documents.
inspections step.

The coating systems considered in this Appendix consist of three layers as follows:
• 1st layer – Liquid Epoxy Primer (DFT not less 250 µm)
• 2nd layer - Polyurethane rigid foam (PUR)
• 3rd layer - Polyethylene outer casing
The characteristics of the coatings materials are applicable to pipe assembly and to fitting
assemblies and shall meet the requirements of standard EN 253.
2.1 CHARACTERISTIC OF THE PRIMER

The 1st layer (Primer) shall be formed by a liquid epoxy or powder epoxy primer completely
compatible with the polyurethane rigid foam and shall meet the characteristics specified in the
Table 1.
Table 1
Requirements of liquid Primer
Characteristic Acceptable Criteria
Dry film Thickness Not less than 150 µm
Solid by weight (for liquid epoxy primer) ≥ 90
Minimum operating temperature 120°C
2.2 CHARACTERISTIC OF THE POLYURETHANE RIGID FOAM (PUR)

The 2nd layer (polyurethane rigid foam) shall be formed by a polymer and shall meet the
requirements listed in Table 2:
Table 2
Requirements of Polyurethane Rigid Foam for pipe assembly and fittings
Characteristic Standard Units Acceptable Criteria
EN 253 item % Closed cells
Cells structure ≥ 88
4.4.2 content
EN 253 item
Foam density Kg/m3 ≥ 60
4.4.3
EN 253 item
Compressive strength MPa ≥ 0,3
4.4.4
Water absorption at EN 253 item
% Volume ≤ 10
elevated temperature 4.4.5
2.3 CHARACTERISTIC OF THE CASING

The 3rd layer (polyethylene outer casing) shall provide complete protection from water moisture
and the suitable strength necessary for handling and laying the insulated pipe.
The polyethylene outer casing shall meet the requirements listed in the Table 3.
Table 3
Requirements of Polyethylene Outer Casing for pipe assembly and fittings
MATERIAL PROPERTIES
Characteristic Standard Acceptable Criteria
Density EN 253 item 4.3.1.1 ≥944 Kg/m3
Black content EN 253 item 4.3.1.1 2,5 % ± 0,5
0,58 g/10 min
Melt flow rate EN 253 item 4.3.1.2
(when tested according to EN 1133)
≥ 20 min
Thermal stability EN 253 item 4.3.1.3
(when tested according to EN 278)
CASING PROPERTIES
Characteristic Standard Acceptable Criteria
In accordance with Table 5 of standard
Thickness EN 253 item 4.3.2.2
EN 253 but never less than 3 mm
Appearance EN 253 item 4.3.2.4 Free of defects
Elongation at break EN 253 item 4.3.2.5 ≥ 350%
Heat reversion EN 253 item 4.3.2.6 ≤ 3%
Long- term mechanical 2000 h with tensile stress of 4,0 MPa at
EN 253 item 4.3.2.7
properties 80°C
Stress crack resistance EN 253 item 4.3.2.8 ≥ 300 h

All requirements provided by the item 2.4 of Functional Specification. 20550 PIP.COR.FUN.
If the formulation of one or all coating materials forming a coating system shall be changed
after the qualification test, the new coating material and coating system shall be re-qualified.
a) Coating materials characterisation tests
b) Coating system characterisation tests

The documentation forwarded to the Company shall include all data listed in following table 4.
In addition the following data must be provided:

a) Material Safety Data Sheet of each component
b) Application method.
c) Coating system description
d) Name and address of the laboratory where the tests will be performed.
3.3.1 Labelling
Each coating material, solvent and thinner to be tested shall be delivered and stored in original
container bearing the Coating Manufacturer’s label, clearly showing following information:
a) Name of the coatings material (primer, polyurethane rigid foam, and polyethylene outer
casing);
c) Batch number of each component (primer, polyurethane rigid foam, and polyethylene
outer casing);
d) Manufacturing date.

provide the selected laboratory with the information listed in the following Table 4.
Table 4
Information and data to be provided by Coating Manufacturer
Polyurethane Polyethylene
Item Primer
Rigid Foam Outer Casing
Viscosity Yes No No
Density Yes No Yes
Solid by volume Yes No No
Finger printing Yes No No
Viscosity Yes No No
Cells structure No Yes No
Foam density No Yes No
Compressive strength No Yes No
Water absorption at elevated temperature No Yes No
Black content No No Yes
Melt flow rate No No Yes
Thermal stability No No Yes
Long- term mechanical properties No Yes Yes
Appearance No No Yes
Elongation at break No No Yes
Heat reversion No No Yes
Stress crack resistance No No Yes

instructions.
The Coating Manufacturer shall also supply a sufficient number of pipe sections and as
defined in the next paragraph. The laboratory shall perform the necessary coating work on the
samples (surface preparation, application, inspection and reporting) fully in accordance with
the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix.
and the requirements of Functional Specification and Appendix are carefully followed. The
selected laboratory shall supervise, record and report all the steps of the coating work.

Test sample shall be representative for the production and shall be prepared as follows:
• For pipe assembly: according to Item 5.1.1 of standard EN 253;
• For fitting assemblies: according to Item 5.2 of standard EN 448.
Where test requirements specified in the standards EN 253 and EN 448 differ from those in
other standards referred to, the requirements laid in the standards EN 253 and EN 448 shall
apply.
according to all requirements provided by items 5 and 6 of this Appendix and by the Functional
is required and to same application parameters.

The method for testing shall comply with the provisions of Item 5 of standard EN 253 for pipe
assembly and Item 5 of standard EN 448 for fitting assemblies.
Appendix.
The acceptance criteria are reported in Tables 2, 3 and 5.

TABLE 5
Requirements of Pipe Assembly and Fitting Assemblies
Increase in diameter of the casing pipe EN 253 item 5.4.1 ≤ 2%
Centre line deviation As per Table 7 of EN 253
Shear strength EN 253 item 5.4.4 As per Table 8 of EN 253
Thermal conductivity EN 253 item 5.4.5 ≤ 0,033 W/(m x K)
Impact resistance EN 253 item 5.4.6 No visible cracks
Creep behavior EN 253 item 5.4.7 Radial displacement ≤ 2,5 mm

a) The applicability of the coating material
b) The correctness and suitability of the instruction provided by Coating Manufacturer.
c) The need, where applicable, for special application equipment
5.1 PIPE ASSEMBLY
5.1.1 Surface preparation

Surface preparation shall be performed fully in accordance with item 4.2.4 of standard EN 253
and to the specific functional requirements reported in item 2.5 of Functional Specification
20550 PIP.COR.FUN. Rev.0.
5.1.2 Coating Application

Coatings shall be applied fully in accordance with the Coating Manufacture’s
recommendations and to the specific requirements reported in item 2.6 of Functional

The minimum thickness of the coating system at any point shall correspond to the
recommended value given in Tables 1 and 5 of standard EN 253.
The tolerance on the outside diameter of the pipe ends shall be in accordance with Table 2 of
EN 253.
5.1.4 Centre line deviation

The distance between the centre line of the service pipe and fittings ends shall correspond to
the values given in Table 7 of standard EN 253.
5.1.5 Cut back

Both ends of the service pipe shall be free from insulation for a minimum of 150 mm. The
tolerance on the declared value shall be ±10mm as defined in item 4.5.1 of standard EN 253.
5.1.6 Repair of defects

construction or shipping
Any repair shall be performed according to the requirements specified in the standard EN 253.
5.2 FITTINGS ASSEMBLIES
5.2.1 Surface preparation

Surface preparation shall be performed fully in accordance with item 4.1.8 of standard EN 448
PIP.COR.FUN. Rev.0.

The minimum thickness of the coating system at any point shall comply with the requirements
of item 4.1.2 of standard EN 448.
The tolerance on the outside diameter of the pipe ends shall be in accordance with Table 2 of
EN 253.
5.2.3 Centre line deviation

The distance between the centre line of the service pipe and the casing at fittings ends shall
correspond to the values given in Table 2 of standard EN 448.
5.2.4 Cut back

Both ends of the service pipe shall be free from insulation for a minimum of 150 mm. The
tolerance on the declared value shall be ±10mm as defined in item 4.4.4.1 of standard EN 448.
5.2.5 Angular between casing segments of bend and minimum length

The maximum angle α (alpha), between two adjacent segments of the casing of a bend shall
not exceed 45° as defined in item 4.4.2 of standard EN 448.
The length, of the casing pipe at the ends of the fittings and valves shall not be less than 200
mm.
5.2.6 Polyethylene welding

The welding process shall be performed in accordance with procedure reported in Annex B of
standard EN 448.
The melt flow rate of the pipes to be welded shall not differ more than 0,5 g/10 min. The
related test shall be performed in accordance with item 4.3.1.2 of EN 253.
The visual appearance of all welds shall be examined in accordance with item 5.6.2 of
standard EN 448 and with the requirements provided in item 4.4.3 of standard EN 448.
5.2.7 Increase of the diameter of the casing pipe

After foaming, the mean outside diameter of the casing pipe shall not have increased by more
than 2%. The measurement shall be performed in accordance with item 5.6.4 of standard EN
448.
5.2.8 Minimum insulation thickness in bends

The insulation thickness of the bends, shall not at any point be less than 50% of the nominal
insulation thickness and nowhere less than 15 mm. The measurement shall be performed in
accordance with item 5.6.5 of standard EN 448.
5.2.9 Tolerance of the main fitting dimensions

The tolerance of the main fitting dimension shall be in accordance with Table 6.
TABLE 6
Tolerances of the main fitting dimensions
DN H L
≤ 300 ± 10 mm ± 20 mm
> 300 ± 25 mm ± 50 mm
6.1 GENERAL
Bid.

b) Description of the test,
c) Applicable reference documents,
d) Applicable check procedures and methods,

e) Acceptability criteria,
f) Frequency of the checks,
The Contractor shall perform during the works progress and at completion of the work all
inspections listed in the Tables D.1, D.2, D.3 and D.4 of Annex D of standard EN 253 and
Table A.2 of standard EN 448.


External Coatings For Corrosion Protection of Steel Pipes and Components

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Eni S.p.A.

Exploration & Production Division

EXTERNAL COATINGS FOR CORROSION

Rev. 0 - February 2004

ENGINEERING COMPANY STANDARD

Spray coating of steel pipes external surface with epoxy or

CORM CORM CORM

3 SAFETY AND ENVIRONMENTAL PROTECTION.......................................................... 16

4 REQUIREMENTS FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE ...... 17

5 DOCUMENTATION AND REPORTING........................................................................... 19

1.3 REFERENCE STANDARDS

Figure 1 - Scheme for the devolpment of the coating project

QCP Company Working Procedure

1.3.1 European standard

1.3.2 ISO and National Organisations

ISO 3001 Plastics and Ebonite – Epoxide compounds – Determination of epoxide

1.3.3 Standards of other Organisations

ASTM A 780 Specification for repair of damaged hot-dip galvanized coatings.

1.3.4 Laws and decrees

1.5 SYMBOLS AND ABBREVIATIONS

1.6 OPERATING ENVIRONMENT

2.1 STORAGE AND HANDLING OF BARE PIPES AND RELATED COMPONENTS

2.1.1 Storage areas

2.2 COATING MATERIAL STORAGE AND PRESERVATION

2.3 CRITERIA FOR COATING SYSTEM SELECTION

2.4 QUALIFICATION OF THE COATING

Under no circumstance the Company approval of a coating system shall be considered a

2.5 SURFACE PREPARATION

Data, information and

Independent Testing schedule

Report of the tests Data

2.5.1 Abrasive materials

2.5.2 Steel imperfections

2.6 COATING MATERIAL APPLICATION

2.7 ENVIRONMENTAL CONDITIONS

In outdoor application, no coating materials shall be applied when there is a likelihood of a

2.8 CUT BACK

3 SAFETY AND ENVIRONMENTAL PROTECTION

3.1 GENERAL SAFETY REQUIREMENTS

3.2 SPECIFIC SAFETY REQUIREMENTS

4 REQUIREMENTS FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE

4.2 PRE-JOB MEETING

4.3 RECEPTION OF BARE PIPES

4.4 RECEPTION OF COATING MATERIALS

4.5 INSPECTION AND QUALITY CONTROL FUNCTION

4.5.2 Coating Manufacturer

4.5.3 Independent Inspection

4.5.4 Certification of personnel

4.6 IDENTIFICATION MARKINGS

4.7 INSPECTION OF PRODUCTION PROCESS

4.8 PRELIMINARY TESTS

4.9 TESTS DURING THE WORK PROGRESS

4.10 FINAL INSPECTION

5 DOCUMENTATION AND REPORTING

5.1 DOCUMENTS TO PRODUCE AT THE BEGINNING OF WORK

5.2 DOCUMENTS TO PRODUCE DURING WORK PROGRESS

5.3 DOCUMENTS TO PRODUCE AT THE COMPLETION OF WORK

Rev. 0 February 2004

ENGINEERING COMPANY STANDARD

APPENDIX “A” ....................................................................................................................................... 1

2 GENERAL COATING CHARACTERISTICS ..................................................................... 3

3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM .......................... 3

4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 7