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GRAVIMETRIC ANALYSIS

A. Constant Weighing of empty Crucible 1 Crucible 2


crucible
Weight after 1st heating 20.5974 22.9602
2nd heating 20.5970 22.9598
3rd heating 20.5978 22.9608
4th heating 20.5981 22.9605
Constant weight(g) (wt±0.0003g) 0.0003 0.0003
Trial 1 Trial 2
B. Weight of Unknown Soluble 0.6310 0.5063
Sulfate (g)

C. Weight of BaCl2, 2H2O (g) 1.3193 1.2870

D. Constant Weighing of unknown Crucible 1 Crucible 2


BaSO4 ppt in crucible
Weight after 1st heating 21.3824 23.6396
2nd heating 21.3822 23.6206
3rd heating 21.3826 23.6206
4th heating 21.3824
Constant weight(g) (wt±0.0003g) 0.0002 0.000
Trial 1 Trial 2
E. Weight if BaSO4 ppt (g) 0.7843 0.6601

F. %SO3 42.64% 44.72%

Mean % SO3 43.68%


Standard deviation (s) %SO3 1.471%
Relative Standard Deviation rsd 3.367%