Beruflich Dokumente
Kultur Dokumente
Powder Technology
j o u r n a l h o m e p a g e : w w w. e l s ev i e r. c o m / l o c a t e / p ow t e c
a r t i c l e i n f o a b s t r a c t
Article history: The particle size distribution of cylinder-shaped solid particles was measured using a buoyancy weighing-bar
Received 17 September 2009 method where the liquid phase density was adjusted to settle or float the particles. The particle size
Received in revised form 13 April 2010 distribution obtained in our experiment agrees with the particle size measured by other method. The present
Accepted 13 April 2010
study demonstrates that a buoyancy weighing-bar method, a novel method for measuring the particle size
Available online 18 April 2010
distribution, is suitable for measuring the particle size distribution of a floating solid. The precision of the
Keywords:
resulting particle size distribution is comparable to that of a laser diffraction/scattering method as well as a
Floating particle direct measurement with a micrometer. Moreover, this buoyancy weighing-bar method can measure the
Particle size distribution particle size distribution even in a mixture of two particles with different sizes.
Buoyant mass © 2010 Elsevier B.V. All rights reserved.
Solid particle
Stokes diameter
C0
⁎ Corresponding author. Tel.: + 81 143 46 5768; fax: + 81 143 46 5701. ρS0 = ρL + ðρ −ρL Þ; ð1Þ
E-mail address: ohira@mmm.muroran-it.ac.jp (Y. Ohira). ρP P
0032-5910/$ – see front matter © 2010 Elsevier B.V. All rights reserved.
doi:10.1016/j.powtec.2010.04.015
284 T. Motoi et al. / Powder Technology 201 (2010) 283–288
ρS∞ = ρL ; ð7Þ
WB∞ = VB ρL ; ð8Þ
Table 1
Sample particles.
dGBt dWBt
=− : ð14Þ
dt dt
Table 2
Liquid properties.
Fig. 9. Particle size distributions of a nylon particle mixture. Solid line: calculated line of
Fig. 8. Particle size distributions of nylon particles (cylinder-shaped particles). nylon particles A and C.
288 T. Motoi et al. / Powder Technology 201 (2010) 283–288
in the particle mixture. In addition, we calculated the particle size x particle size, m
distribution of the particle mixture, which consisted of nylon particles ε voidage, −
A and C, from independent data obtained using nylon particle A and ϕ shape factor, −
nylon particle C. The results are shown in Fig. 9 (solid line). There is a μL liquid viscosity, Pa s
slight difference between the calculated results and the results ρL liquid density, kg/m3
obtained in the experiment, but they are close. ρB density of weighing tool, kg/m3
Thus, we conclude that the particle size distribution of particles, ρP particle density, kg/m3
which consists of two different sized particles, can be measured using ρS density of suspension, kg/m3
the BWM if the particle density is the same. Taken together, the BWM
is reliable for measuring a particle size distribution. Subscripts
max maximum
5. Conclusions min minimum
0 initial t = 0
Using the BWM, we measured the particle size distribution of the ∞ infinity t = ∞
floating solid particles in the liquid phases where the density was
adjusted with the concentration of sodium chloride. The following
results were determined:
Acknowledgements
(1) Using the BWM, the particle size distributions of floating solid
particles can be measured, suggesting the theory established in A part of this work has been supported by the Japan Science and
particle size distribution of settling particle measurements can Technology Agency (JST). The authors would like to thank our
be applied to floating particles. students for experimental assistance: Mr. Y. Koikeda and K. Nakano.
(2) The particle size distribution for a particle mixture consisting of
two different size particles can be measured using the BWM.
References
(3) The precision of the particle size distribution is comparable to
that obtained by the laser diffraction/scattering method, a [1] T. Allen, Particle Size Measurement, Fourth edition, Chapman and Hall, London,
representative high precision method used to measure particle 1990, pp. 345–355.
[2] Society of Chemical Engineering of Japan, Chemical Engineering Handbook, 5th
size. edition, Maruzen, Tokyo, Japan, 1988, pp. 224–231.
[3] K. Fukui, H. Yoshida, M. Shiba, Y. Tokunaga, Investigation about data reduction
Nomenclature and sedimentation distance of sedimentation balance method, J. Chem. Eng. Japan
33 (2000) 393–399.
C solid concentration of suspension, kg/m3 [4] M. Arakawa, G. Shimomura, A. Imamura, N. Yazawa, T. Yokoyama, N. Kaya, A new
D(x) mass percentage undersize of particle size x, % apparatus for measuring particle size distribution based on centrifugal sedimen-
f(x) mass frequency of the particle size x, − tation, Journal of the Society of Materials Science Japan 33 (1984) 1141–1145.
[5] M. Kuriyama, H. Tokanai, E. Harada, Maximum stable drop size of pseudoplastic
F(ε) voidage function, − dispersed-phase in agitation dispersion, Kagaku Kogaku Ronbunshu 26 (2000)
g gravitational acceleration, m/s2 745–748.
GBt mass of weighing tool at t = t, kg [6] H. Minoshima, K. Matsushima, K. Shinohara, Experimental study on size
distribution of granules prepared by spray drying: the case of a dispersed slurry
GRt VB ρ B − WRt, kg containing binder, Kagaku Kogaku Ronbunshu 31 (2005) 102–107.
h submerged length of weighing tool, m [7] Y. Ohira, H. Takahashi, M. Takahashi, K. Ando, Wall heat transfer in a double-tube
R(x) mass percentage oversize of particle size x, % coal–slurry bubble column, Kagaku Kogaku Ronbunshu 30 (2004) 360–367.
[8] E. Obata, Y. Ohira, M. Ohta, New measurement of particle size distribution by
t time, s
buoyancy weighing-bar method, Powder Technology 196 (2009) 163–168.
v(x) floating velocity of particle size x, m/s [9] J.F. Richardson, W.N. Zaki, Sedimentation and fluidization: Part I, Trans. Inst.
VB submerged volume of weighing tool, m3 Chem. Engrs. 32 (1954) 35–52.
WB buoyant mass of the submerged weighing tool in the [10] T. Allen, Particle Size Measurement, Fourth edition, Chapman and Hall, London,
1990, pp. 258–261.
suspension, kg [11] T. Allen, Particle Size Measurement, Fourth edition, Chapman and Hall, London,
WRt W0 −ðW0 −W∞ Þ∫xxmax
i
f ðxÞdx, kg 1990, pp. 128–140.