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Water Research 36 (2002) 1585–1595

The influence of contact zone configuration on the flow


structure in a dissolved air flotation pilot plant
Ma( ns Lundha,*, Lennart Jonsson
. b
, Jan Dahlquistc
a
Department of Water and Environmental Engineering, Lund University, P.O. Box 118, 221 00 Lund, Sweden
b
Department of Water Resources Engineering, Lund University, P.O. Box 118, 221 00 Lund, Sweden
c
PURAC Sweden, P.O. Box 1146, 221 05 Lund, Sweden
Received 22 December 2000; received in revised form 3 July 2001; accepted 20 July 2001

Abstract

The dissolved air flotation process is used in water and wastewater treatment. Among many parameters the fluid
dynamics determine the capacity of the process. The contact zone is assumed to be important for the removal function,
as it is believed to be the location for the aggregation of bubbles and flocs. This paper presents an experimental study on
the flow structure in a contact zone of a DAF pilot tank and the influence of contact zone configuration. The flow
structure in the contact zone was examined for different horizontal lengths of the zone and for different heights and
inclinations of the shaft wall. The hydraulic surface loading was 11 m/h over the total tank surface area and the recycle
rate was constant at 10% of the main flow. The examined hydraulic surface loading over the contact zone ranged from
40 to 98 m/h. Water velocities in the longitudinal, central section of the tank were measured with an acoustical Doppler
velocimeter in a grid net for the different contact zone configurations, giving an insight into the flow structure. The
result showed that the flow structure in the contact zone was characterised by a turbulent lower region and a plug-flow
higher region. The hydraulic surface loading, a function of the length of the contact zone, seemingly determined the
extension of the turbulent region. A higher hydraulic surface loading decreased the turbulent region while the lower
loading increased it. A hydraulic surface loading of 65 m/h was suggested for design. It was not possible to determine
the turbulent intensity quantitatively due to the measurement method. The height and inclination of the shaft wall did
not seem to have a significant influence on the turbulent region. However, an increased height of the contact zone
enhanced the higher, plug flow region and a recommended height of 0.81 m or higher for the recommended hydraulic
surface loading was suggested when both mixing and plug-flow are desired. The separation zone was characterised by a
stratified flow structure, mainly influenced by the cross-flow velocity that is a function of the distance between the shaft
wall top and the water surface. A cross-flow velocity of 37 m/h or higher resulted in a clearly defined stratification,
believed to be crucial for an efficient separation of flocs. Finally, the extension of the lower, denser plug-flow region in
the separation zone increased when the shaft wall height increased. r 2002 Elsevier Science Ltd. All rights reserved.

Keywords: Dissolved air flotation; Fluid dynamics; Flow profiles; Contact zone; Separation zone; Acoustical Doppler velocimeter

1. Introduction based on removing suspended solids from water by


utilising the lifting force induced when bubble-floc
Dissolved air flotation is a process used in the aggregates of low density are produced.
treatment of water and wastewater. The technique is The process takes place in two separated zones, each
with a different mechanism. The contact zone provides
*Corresponding author. Tel.: +46-31-7722133; fax: +46-31- for the contact and attachment of bubbles and floc
7722128. (aggregation) while the separation zone separates the
E-mail address: mans.lundh@wet.chalmers.se generated aggregates from the water phase. Previous
(M. Lundh). research has established that the contact zone config-

0043-1354/02/$ - see front matter r 2002 Elsevier Science Ltd. All rights reserved.
PII: S 0 0 4 3 - 1 3 5 4 ( 0 1 ) 0 0 3 5 7 - 8
1586 M. Lundh et al. / Water Research 36 (2002) 1585–1595

uration could be of great importance for the removal the contact zone. The flow structure in the separation
efficiency, although the lack of quantitative guidelines is zone has been modelled [13–17] and measured experi-
striking [1]. Some researchers have presented ideas about mentally in pilot plants [10–12,15], in laboratory set-ups
the performance of the contact zone but few have [18] and in full-scale plants [16,17].
actually carried out a systematic study. This paper will present the result and analysis of an
Kitchener and Gochin [21] suggested that enough experimental study of the flow structure in a tradition-
turbulence must exist in order to provide adequate ally designed rectangular dissolved air flotation (DAF)
collision opportunities between bubbles and flocs but pilot plant and the influence of varying the internal
that regions of high shear should be avoided due to the geometry, meaning the variation in height, length and
risk of breaking the floc and detaching the bubbles. They inclination of the contact zone shaft wall. The flow
also suggested that the flow should be plug-like and that structure in the contact zone and in the separation zone
the contact zone should be separated from the separa- will be discussed and an attempt to quantify design
tion zone. Vrablik [2] emphasised the importance of a criteria will be presented.
sufficient residence time to achieve the required contact
time. Zabel [3] suggested that the air-enriched recycle
stream should be promptly released into the water 2. How do hydraulic characteristics affect the
influent in order to minimise the loss of air due to separation?
coalescence of bubbles.
Bratby [4] concluded that an inadequately designed The study only covers the hydraulic principles and not
inlet arrangement caused significant amounts of larger the removal of suspended solids. As discussed in the
bubbles to break through the accumulated float layer. introduction of this paper, an initial, efficient mixing of
Ettelt [5] tested six different contact zone configurations the water and bubbles in the lower parts of the zone
and showed that small modifications had a significant probably enhances the aggregation process. The mixing
impact on the properties of the float layer. Vrablik [2] should not be too vigorous to avoid the coalescence of
concluded that the velocity of the recycle should be 2–3 bubbles or the disintegrations of flocs and bubble
times larger than the influent to ensure a sufficient aggregates.
mixing. One might expect that turbulence and strong motions
Baeyens et al. [6] reported on an experimental set-up would affect the hydraulic behaviour of the separation
of a pilot coaxial flotation column and presented zone. Finally, the final vertical transport of the water
theories on flow conditions using the plug flow disper- and its horizontal cross flow above the shaft into the
sion model with the P!eclet number. They concluded that separation zone should probably be a distinct forward
the pilot column behaved nearly as a plug-flow system and gentle movement with a low turbulence level.
within a range of hydraulic surface loading of 5–30 m/h,
and that the injection of bubbles increased the P!eclet
number. Liers et al. [7] developed a model for a coaxial 3. Material and method
DAF column and examined the parameters bubble-floc
attachment efficiency and air-to-solids volume ratio in 3.1. General
the aggregates. Shawwa and Smith [8] performed a pulse
tracer response test in the contact zone. Using a The purpose of the measurements was to map the
dimensionless P!eclet number for determining the resi- velocity profiles in the contact zone for different
dence time distribution, the authors showed that the configurations. The measurements were performed in a
flow conditions inside the contact zone deviated from pilot plant. An acoustic Doppler velocimeter [19] was
plug-flow. The mixing time decreased with increasing used for measuring the average water velocities in a grid
hydraulic loading in the contact zone (from 30 to 90 m/ net, which would then give an insight into the flow
h). Park et al. [9] examined the solids removal efficiency structure. The study was carried out with particle-free
versus water velocity in a coaxial cylinder-type flotation water under the assumption that a solids loading up to
column. 90% efficiency was achieved for a contact zone 800 mg SS/l would not significantly influence the flow
velocity of less than 66 m/h and for a separation zone structure [10,12].
velocity of 18 m/h. Moreover, a flow structure was
modelled with the simple-implicit method for pressure- 3.2. Pilot tank
linked equation.
Studies have shown that the air content influences the The pilot flotation tank (Fig. 1) was rectangular in
flow structure mainly in the separation zone [10–12] and shape with a height of 1.35 m, a length of 1.7 m and a
to a lesser extent in the contact zone [10]. The studies width of 0.7 m. The influent descended behind a baffle
did, however, show that the jets, generated from adding and entered the contact zone through a slot at the
the dispersion, have an impact on the flow structure in bottom. In the contact zone, the water was brought
M. Lundh et al. / Water Research 36 (2002) 1585–1595 1587

Valve Sludge Sludge


handle scraper compartment

Level
ADV Probe
weir

Water level
Influent Baffle Transmitter
Shaft
wall
Separation Receiver
Contact zone
zone
Effluent
Measuring
point
5 cm
z
Distribution pipe Needle valve Perforated
for air-saturated outlet pipe
water

Fig. 1. The pilot plant flotation tank.


x

Fig. 2. The ADV.


upward. The water flowed horizontally over the shaft
wall and entered the separation zone. Effluent was
removed at the bottom via two perforated pipes. The about 1 cm. The measurements of this study were hence
tank arrangement was capable of operating at surface assumed to be displaced 4 cm upwards, which is of little
loadings up to 30 m/h. significance to the overall flow structure considering the
The recycle flow was saturated with air in an ejector size of the contact zone.
that brought water and air together. It was continuously
added to the main flow through three, evenly spaced 3.4. Operating conditions
needle valves at the bottom of the contact zone. The
released air bubbles were thus mixed with the main flow. The hydraulic surface loading over the whole tank
The system could produce about 3 m3/h. was set at 11 m/h. Nine different configurations regard-
ing height, length and inclination were measured for the
3.3. Acoustic Doppler velocimeter same operational settings, which are displayed in the
vector plots and defined in Table 1.
The principle of the ADV is based on the Doppler The required hydraulic surface loading in the contact
effect. An acoustical pulse that is scattered on a moving zone determined the configuration of the contact zone.
object, experiences a frequency shift that is related to the The contact zone was arranged to fit loadings of
speed of the object. The ADV is constructed with a approximately 40, 65 and 100 m/h, based on the surface
central transmitter and three receivers located in a circle area above the contact zone. The pilot plant construc-
around the transmitter (Fig. 2). The receivers are slanted tion had some limitations and the actual operational
towards a measuring point approximately 5–6 cm from variables are presented in Table 1.
the transmitter. The ADV makes it possible to determine The shaft wall of the pilot plant consisted of two
more or less continuously (25 samples per second) three wallboards giving the possibility to study different
velocity components in the measuring point. configurations. The dispersion rate was set at 10%,
Lohrmann et al. [20] have reported that the instru- producing an air content of about 4.5–5.5 ml air/l water
ment is capable of measuring velocities down to in the contact zone. The saturator pressure was set at
0.4 mm/s. The maximum was determined at 2.5 m/s. 5 bar. As the air content did not seem to have any
Other measurements [10,11] showed, however, that in immediate influence on the flow structure in the contact
water with a high concentration of micro-bubbles of zone it was not analysed specifically. The air content was
about 40–120 mm, the measured velocity was reduced up taken from Lundh [10] based on the performance of the
to 70%, depending on the air content and probe saturator system.
orientation. Furthermore, there were indications that The turbulence has not been analysed in this study as
the measuring point was not located 5 cm from the such an analysis is based on the standard deviation of
probe transmitter as stated by the manufacturer but only the velocity signals, which in turn requires adequate
1588 M. Lundh et al. / Water Research 36 (2002) 1585–1595

Table 1
General variables in the DAF tank

Measurement Incoming Recycle Hydraulic Air content Retention Retention time Description
flow rate surface loading in c-zone time in tank in s-zone of c-zone
m3/h % m/h ml/l min min

M4c 9.7 10.3 10.7 5.5 8.0 7.0 Half tilted/


half vertical
M48 10 10 11 4.5 7.8 7.3 Vertical
M49 10 10 11 4.5 7.8 7.1 Vertical
M50 10 10 11 4.5 7.8 6.9 Vertical
M51 10 10 11 4.5 7.8 6.8 Vertical
M53 10 10 11 4.5 7.8 7.0 Vertical
M54 10 10 11 4.5 7.8 6.4 Vertical
M55 10 10 11 4.5 7.8 7.3 Vertical
M56 10 10 11 4.5 7.8 7.1 Tilted

Measurement Contact zone Contact zone Shaft wall Hydraulic Retention Distance Cross flow
length height inclinationa surface loading time in c-zone between water velocity
in c-zoneb level and top
of shaft wallf
cm cm 1 M/h s cm m/h
c d
M4 10/25 89 171 61 57 35 44
M48 24 51 F 65 28 73 22
M49 24 81 F 65 45 43 37
M50 24 101 F 65 56 23 68
M51 24 111 F 65 61 13 121
M53 24 91 F 65 50 33 48
M54 39 91 F 40 82 33 48
M55 16 91 F 98 33 33 48
M56 16/39d 88 151 98/40e 43 36 44
a
Inclination in relation to a vertical line.
b
Calculated for the vertical part of the contact zone.
c
Ejector 1.
d
Length from the baffle to the start of inclination at bottom/length from the baffle to the end of inclination.
e
Loading at the start of inclination at tank bottom/loading at the end of inclination.
f
Water surface at 124 cm above tank bottom.

measurements of the magnitude of the velocity, which is calculated as the difference between the retention time
not possible with the ADV in bubbly water [10]. in the contact zone and the retention time of the whole
The water surface was located about 124 cm from the tank. The cross-flow velocity was calculated as the
tank bottom. The hydraulic surface loading of the hydraulic loading divided by the area defined by the
flotation tank was calculated as the incoming flow water level, the top of the shaft wall and the tank width.
divided by the tank surface area, which was about 1 m2
excluding the area behind the baffle. In reality it was 3.5. Method of measurement and the references of
measured to be about 1.07 m2, which would reduce the direction
surface loading of Table 1 by approximately 6%. The
difference was considered insignificant as the parameter As illustrated in Fig. 3, the tank was defined in an xyz-
works only as a label and is irrelevant to the flow coordinate system to give reference points as to where
structure inside the tank. the measuring point was located. Co-ordinate z gives the
The retention time in the tank was calculated as the height over the tank bottom, x gives the length starting
water volume divided by the hydraulic loading of the from the influent side, and y gives the width, starting
tank, which is the sum of influent and recycle flow. The from the right side going to the left. The velocities also
retention time in the contact zone (c-zone) was follow the coordinate system, meaning that the velocity
calculated as the volume, defined by the baffle and shaft vx refers to the x-direction, etc.
wall, divided with the hydraulic loading in the tank. The Since it was difficult to determine an actual magnitude
retention time in the separation zone (s-zone) was of the water velocity with the ADV in bubbly water,
M. Lundh et al. / Water Research 36 (2002) 1585–1595 1589

Influent c-z s-z Effluent

longitudinal extension
upward
backward forward
c-z s-z
leftward
lateral
extension backward forward downward

y rightward z

x x
Horizontal cross-section Vertical cross-section
Fig. 3. The co-ordinate system of the measurements and the directions referred to in the study.

emphasis has been placed on the flow structure rather the cases, while the height of the shaft wall was increased
than on the exact value of the velocity. The direction from 51 to 81, 91, 101 and 111 cm. Other variables are
was, however, believed to be correct [10]. The conse- presented in Table 1.
quence of this approach is that the scale of the vectors is There was a well-mixed zone in the lower parts of the
the same in a plot but could differ between the plots. contact zone in all cases, more or less independent of the
Each velocity measurement took approx. 80–120 s height of the shaft wall (Fig. 4). The region was located
with a sample frequency of 25 Hz. After processing the in the back of the zone. Three-dimensional movements,
data for different parameters, the average velocities were defined as horizontal movements in the plane (Fig. 5,
plotted on a vector plot or on a surface plot showing the right), also contributed to mixing of the water. As the
overall flow situation. At the bottom of each vector plot height of the shaft was increased (Fig. 4, left to right) the
there is a reference vector defining, by length, the mixing zone seems to have been relocated higher up. The
maximum velocity shown in the plot. mixing does not seem to have been restricted to the
The concept of three-dimensional flows is discussed in lower region of the zone as vertical water transports
the analysis. The basis is the two-dimensional, vertical, from the top of the zone also occurred. A large part of
longitudinal section through the tank. Three-dimen- the water transport through the contact zone, however,
sional flows move in the y-direction according to the seems to have occurred up along the shaft wall and
applied coordinate system. directly out into the separation zone. This is shown as
large velocity vectors along the shaft wall in Fig. 4 or as
an elevated ridge close to and across the shaft wall in the
4. Flow structures in the contact zone surface plot of Fig. 5, left.
A more plug-like flow seems to evolve when the height
4.1. General of the contact zone is increased. The case with a 111 cm
shaft (Fig. 4, M51), giving the retention time of 61 s,
The evaluation of the mixing properties of the zone generated a more or less evenly distributed velocity
has been restricted to the visual observation of the profile in almost 50% of the zone. If the requirements
velocity profiles. The zone was considered mixed if the were an initial mixing phase with a subsequent homo-
pattern indicated strong turbulence and recirculation of genised flow, a high shaft would be better than a lower
water. It was not possible to quantify the mixing one.
intensity by e.g. measurements of the turbulence. The A distinct unidirectional cross flow was generated for
concept of a plug flow was based on evenly distributed an induced cross-flow velocity of 48 m/h or higher.
velocities across the section and directed perpendicular Lower velocities generated more complex and uncon-
to the cross section. trolled flow patterns above the contact zone.

4.2. Height 4.3. Length

The length of the contact zone was held constant at The examined lengths of the contact zone were 16, 24
24 cm giving a hydraulic surface loading of 65 m/h for all and 39 cm, resulting in hydraulic surface loadings of 40–
1590 M. Lundh et al. / Water Research 36 (2002) 1585–1595

Fig. 4. The velocity profiles in the central longitudinal and vertical section of the contact zone for an increasing shaft wall height. The
heights are from left to right: 51, 81, 91, 101 and 111 cm.

98 m/h in the contact zone, while the height was held the perpendicular to the tank bottom, reaching about
constant at 91 cm above the tank bottom. The retention 48 cm above the bottom. On top of the inclined board
time varied from 33 to 82 s depending on the zone was a vertical board with a length of 40 cm. The
length. hydraulic surface loading was 98 m/h at the bottom and
A mixing zone was observed in the case with the 39- 65 m/h in the vertical part of the shaft. The retention
cm long contact zone (Fig. 6, M54). Water from above time varied between 33 and 57 s depending on the
did not seem to mix with the lower parts. There was a design.
higher region where the water was moved horizontally The half-inclined, half-vertical shaft wall generated a
but firmly upwards, developing into a relatively homo- strong flow of water upwards along the shaft wall
genised flow. The cross flow was horizontally orientated, (Fig. 7, M4), like in the case when the entire wall was
indicating a steady and stable flow structure. inclined (Fig. 7, M56). There was a downward move-
There was also a mixing zone in the case of the 24-cm ment along the baffle in the lower, back regions,
long contact zone (Fig. 6, M53) with a hydraulic surface identical for both cases, although more distinct in the
loading of 65 m/h. At 50 cm above the tank bottom, the case with the entire shaft wall inclined.
flow was uniform and of a plug-flow nature. The A joint hinge arrangement connected the two wall-
velocities were directed upwards and forwards above boards constituting the shaft wall, with a possible
the contact zone. influence on the flow structure in the contact zone. This
In the case with the narrow shaft of 16 cm (Fig. 6, impact was, however, considered to be small, not
M55), there seemed to be less mixing. The velocity affecting the overall flow characteristics in the contact
profile was concentrated distinctly upwards and the zone [10].
water transport above the contact zone was concen- Above the contact zone, the half-inclined, half-vertical
trated into a well-defined flow, entering the separation case (Fig. 7, M4) resulted in a more distinct forward-
zone horizontally. moving flow into the separation zone, encompassing the
The flow structure above the contact zone was whole section part above the contact zone. This was
horizontally orientated for the cases 16 and 39 cm but probably due to the higher hydraulic surface loading at
also vertically for the 24-cm case. the top of the zone.
The inclination itself did not seem to significantly alter
4.4. Inclination the flow structure when compared to the flow structure
found in the vertical shafts.
The first of two designs was a contact zone where the
entire wall was inclined 151 from the vertical. The height
of the wall was 88 cm in total and the hydraulic surface 5. Flow structures in the separation zone
loading was 98 m/h at the bottom and 40 m/h at the top
of the contact zone. The second inclined design was a The outflow from the contact zone for the 51-cm high
contact zone with the lower wallboard inclined 171 from shaft was not distinct and regular (Fig. 8, M48). There
M. Lundh et al. / Water Research 36 (2002) 1585–1595 1591

Fig. 5. The water velocities in horizontal sections of a 91-cm high and vertical contact zone. The figures to the left are the vertical
velocities (Vz ) and the vector plots to the right are the horizontal velocities (Vx;y ) in the corresponding surface plot. The z-value is the
level above tank bottom.

was a flow transporting the water from the contact zone strong return flow from the outlet wall towards the shaft
towards the outlet wall and slightly upwards. There were wall, which seems to have entered into the contact zone
three large high-velocity arrows just above the shaft just above the shaft wall. Underneath the return flow, at
wall, indicating a strong return flow from the separation about 70 cm above the tank bottom, the transport of
zone into the contact zone. The water transport has water has developed into plug-flow.
become more plug-like just above the bottom of the The flow patterns for the next two cases, with the
separation zone. shaft wall heights 91 and 101 cm, respectively (Fig. 8,
For the case with a vertical shaft wall of 81 cm (Fig. 8, M53 and M50), were similar to the previous one. The
M49) the flow pattern, compared to (Fig. 8, M48), seems last case (Fig. 8, M51) did, however, show significant
to have been brought up closer to the water surface, changes of flow structure. The upper flow, just under-
forming a stratified profile from the contact zone to the neath the water surface, was now located higher up in
outlet wall. There was an indication of a relatively the tank, at z ¼ 105 cm. There was no observable return
1592 M. Lundh et al. / Water Research 36 (2002) 1585–1595

Fig. 6. A comparison between contact zones with varying lengths. Velocity profiles in the central longitudinal and vertical section in
the contact zone. From left to right the lengths are 16, 24 and 39 cm, corresponding to hydraulic surface loads of 98, 65 and 40 m/h over
the contact zone.

wall, the water has returned towards the shaft wall,


generating a return flow. A longer contact zone of 39 cm
(Fig. 8, M54) generated less return flow and a more
concentrated flow underneath the water surface, other-
wise the flow resembles the case with a shaft wall height
of 91 cm and a length 24 cm (Fig. 8, M53).
The cases with inclined wall (Fig. 8, M4 and M56) had
profiles very similar to the case with a 91 cm shaft wall
and a contact zone length of 24 cm.

6. Discussion and conclusion

6.1. Contact zone

The general flow structure in a vertical shaft was


characterised as follows:

The water enters the contact zone through the inlet


slot, follows the tank bottom towards the shaft wall
where it is forced upwards. The vertical velocity
Fig. 7. The velocity profile in the central, longitudinal and profile along a longitudinal extension has a max-
vertical section in a tilted contact zone. The plot to the left is the imum at the shaft wall and a minimum at the baffle.
contact zone with the tilted shaft wall and the plot to the right
The flow is transformed higher up where a more
(less measurements done) is the contact zone with the half-tilted
plug-like pattern is developed. Concentrated partial
and half-vertical shaft wall.
flows are traced as local elevations in a horizontal
velocity profile. Horizontal movements transport the
water towards the back of the zone, where the water
flow and the water flow underneath the horizontal flow is further transported down. The velocities above the
developed immediately into a plug-flow. zone are low but distinctly directed upwards and
The plot with a narrow shaft with a length of 16 cm forwards into the separation zone.
(Fig. 8, M55) indicates an outflow that makes a small
dip just after leaving the contact zone before continuing Mixing in the contact zone was found in the lower
towards the outlet wall. After encountering the outlet regions in all the cases, except maybe when using a
M. Lundh et al. / Water Research 36 (2002) 1585–1595 1593

Fig. 8. Water velocity profiles in the central, longitudinal and vertical section of the separation zone for the increase of shaft wall
height, the shaft length and the inclination of the shaft wall. The positions of the shaft wall, baffle and water level are approximated.

narrow, vertical shaft. If good mixing is required the A cross-flow velocity higher than 37 m/h generated a
hydraulic surface loading should be less than 98 m/h. distinct flow pattern into the separation zone. If the
A plug-like flow seems to have been enhanced with distance from the water surface to the top of the shaft
increasing height of the contact zone. The case with a wall was increased, the flow structure became irregular,
111-cm shaft seems to have generated an evenly possibly inducing a risk for accumulation of bubbles just
distributed velocity profile in almost 50% of the zone. above the contact zone thus enhancing the probability
For the requirements where an initial mixing phase with for return flows down into the contact zone. It is thus
a subsequent homogenised flow, a high shaft would be important to have a firm movement forwards from
preferred to a lower one, meaning a shaft higher than above the contact zone into the separation zone.
81 cm giving a retention time of at least 45 s at a The inclination of the shaft wall that related to the
hydraulic surface loading of 65 m/h. range of hydraulic surface loading (40–98 m/h), did not
1594 M. Lundh et al. / Water Research 36 (2002) 1585–1595

Table 2 P.O. Box 824. Pretoria. 001. Republic of South Africa,


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