Katalog Reaktori PDF

N TA IN
S
2014
P G
RI
CIN
S I N C O R
S P
A
O
L
RA
ACE G
TH
TED
A N N I V E R S A R Y
1936 2011
VI USA
NE , N J
LAND
Reactors Catalog
Bench & Kilo Class
General Information 3
Specifications In case of Shortage:

1. Notify ACE immediately.
The products in this catalog represent what we believe to be
2. A replacement will be issued upon confirming
the most advanced design and construction. However, design
inventory d iscrepancy.
improvements are constantly being made, and we reserve the
right to modify specifications where we feel that a change is In case of Loss:
warranted. 1. First, please verify with all your receiving departments
Apparatus fabricated in accordance with ASTM, API, AOAC and that delivery was not made.
other technical organization specifications such as USP, NIST, 2. Notify ACE immediately.
and NIOSH, are subject to modification by these organizations. 3. ACE will contact the carrier for tracking information
All precision-grade ware is warranted to be within the tolerance as a pplicable.
prescribed in ASTM Specifications. All laboratory-grade ware 4. A replacement will be issued upon verification that the
is twice precision-grade tolerances. shipment was not delivered and upon confirmation
that the carrier cannot locate shipment.
Special Apparatus PLEASE NOTE:

Orders or inquiries for special apparatus should be All breakages and shortages must be
accomp anied by prints or drawings, if possible. To prevent
delay, and to enable us to more intelligently quote on your reported within two weeks of receipt.
specials, all necessary dimensions and tolerances should
be noted. For technical information, design assistance
and help please visit www.aceglass.com. Returns and Repairs
The following information should also be furnished where Incoming material (returns or repairs) must be pre-approved
applicable: joint sizes, Ace‑Thred sizes, capacity, whether “to by our Product Return Specialist. Please follow these steps to
contain” or “to deliver,” porosity of filter, and any abnormal ensure our Receiving Department does not refuse your shipment.
operating conditions, such as extremely high pressure or
1
Contact ACE for an RA# (Return Authorization Number).
temperature, to which the apparatus may be subjected.
1-800-223-4524 (Vineland, NJ, USA)
We reserve the right to overrun or under run by 10% on orders E-mail: returns@aceglass.com
for special items and to ship and invoice for amounts within
this variation. 2. Once an RA# is given, properly pack the item(s) in an inner
and outer box/carton and write the RA# on the outside of
NOTE: Special items are not returnable.
the box. All used items are to be thoroughly cleaned and
Our research and drafting departments are always available to defined in the assignment of an RA#.
assist you in designing special apparatus. Your special will be
3. A 20% restocking fee will be assessed for authorized
assigned a permanent drawing number for future reference,
returns. ACE cannot accept responsibility for damage or
duplication or change. You will be sent a drawing of your special
destruction of glassware that occurs in your shipment to
for your approval/sign off before manufacturing begins.
us. We strongly advise you to purchase additional insurance
with your carrier.
Types of Glass 4. For Returns that are the result of your receiving the item(s)
broken, ACE cannot accept responsibility for further
All ACE-manufactured glassware items listed in this catalog damage or destruction of glassware that occurs in the
are, unless otherwise noted, fabricated from 33 expansion return shipment due to improper packing.
borosilicate glass, such as Pyrex® Brand Glass, a product of
5. Repairs will be evaluated by our technicians. You will
Corning Incorporated; KG-33 Glass, a product of Kimble Glass
be advised if any pieces are beyond repair or cannot be
Company; Duran Glass, a product of Schott Glaswerke; Simax,
salvaged economically. ACE cannot accept responsibility
a product of Kavalier Glaswork.
for further damage or destruction of any glassware that is
damaged during return shipment.
Breakage or Loss PLEASE NOTE:
In case of Breakage:
1. Notify ACE immediately.
ACE cannot accept responsibility
2. Please retain all inner and outer cartons and
for material returned without proper
packing material. authorization.
3. ACE will advise you whether the carrier will
report to your location for inspection or if item(s)
are to be returned for inspection.
Specifications are subject to change without prior notice. Although they are represented to be
accurate, it is best to verify product specifications with ACE prior to purchase in the event they have
been changed since publication of this catalog.
Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

4 General Information
Order by Code ACE Glassware Discounts

Each item in this catalog has a two- or three-digit code in All ACE-manufactured glassware, identified with a spade (♠),
addition to the four- or five-digit number. No other ordering listed in this catalog is subject to the following dollar value
information is needed since each individual size, capacity, etc. discounts. Items marked by a star (★) or that have no designation
has its own code. Example: 5000 10/30 top 14/35 bottom whatsoever are not subject to this discount.
would be ordered as 5000-05. .10% on purchases of $500.00 and over
The majority of items listed in this catalog are normally available .12% on purchases of $1000.00 and over
from stock at our plant in Vineland, NJ. .15% on purchases of $1500.00 and over
In the event your entire order cannot be filled immediately, Terms: Net 30 days (Domestic only)
a partial shipment will be sent, with the back-ordered items Minimum Order: $25.00
following shortly. If you should desire the entire order to be sent
All quantities in this catalog are “each”
in one shipment, please so specify on your purchase order.
unless otherwise noted.
Unless otherwise specified on the order, we will ship material
by what we consider the “best way.” Contact ACE for current price list/pricing CD
or visit our website, www.aceglass.com.
Ways to Order
Ace Glass products are also available from our many lab
distribution partners, particularly VWR International and
Sigma Aldrich.
PHONE 856-692-3333
800-223-4524
FAX 856-692-8919
800-543-6752
CREDIT CARD VISA
MasterCard
American Express
MAIL P.O. Box 688
Vineland, NJ 08362
WEB SITE www.aceglass.com
E-MAIL sales@aceglass.com
INTERNATIONAL export@aceglass.com
Shipments are F.O.B. our factory

in Vineland, NJ, USA.
INTERNATIONAL SALES
Ways to Order Methods of Payment
Mail: Ace Glass Incorporated ◾ Wire Transfer
International Sales Dept.
1430 N. West Blvd — P.O. Box 688 ◾ Irrevocable, payable on-sight,
Vineland, NJ 08360-0688 USA and confirmed letter of credit
Phone: 856-692-3333 ◾ Payment in advance by check or
money order, in US Funds only
Fax: 856-692-8919
◾ Credit Card: Amex, Visa, MasterCard, etc.
E-mail: export@aceglass.com

Technical Information 5
Reference Guide to Ace‑Thred Sizes Fraction Conversion

Length,
Accepts Use Bushing Use With Optional Suggested Fractional Inches Millimeters
Size Tube O.D., mm Number O‑Ring No. Ferrule Uses
1/16 1.6
Mini #7 6-7 5029-10 7855-704 11710-07 A, B, I 1/8 3.2
Midi #11 9-10.5 7506-02 7855-708 11710-11 D, E, F, G 3/16 4.8
1/4 6.4
Maxi #15 12.5-14 7506-06 7855-716 11710-15 C, H 5/16 7.9
#18 16-17 7506-08 7855-720 11710-18 H, L 3∕8 9.5
Giant #25 24-25 7506-10 7855-734 11710-25 K, R 7/16 11.1
#36 34-35 7506-12 7855-740 — K, L, R 1/2 12.7
9/16 14.3
Jumbo #50 47-48 7506-14 7855-744 11710-50 K, L, R 5/8 15.9
#80 80 7506-20 7855-782 — R 11/16 17.5
3/4 19.1
A–Thermometers, B–Bleed Tubes, C–Electrodes, D–Sensing Probes, E–Thermowells,
13/16 20.6
F–Gas Dispersion Tubes, G–Vacuum Take-Offs, H–Inlet and Outlet Tubes,
7/8 22.1
I–Miniature Electrodes, K–Manifolds, L–Immersion Wells, R–Reactors
15/16 23.8
1 25.4
Dimensions in Millimeters
Hose Connection Size Guide
3.0 3.5 3.0 4.0 5.0 7.7 7.3
6.5 7.1 6.0 8.9 8.4 12.5
13.8
10.5 10.4
10.0
12.5 11.5 12.9
16.2
Use with Use with Use with Use with Use with Use with Use with
7.9mm (5/16-in.) 7.9mm (5/16-in.) 7.9mm (5/16-in.) 9.5mm (3/8-in.) 9.5mm (3/8-in.) 11.1mm (7/16-in.) 15.9mm (5/8-in.)
I.D. Tubing or 9.5mm (3/8-in.) or 9.5mm (3/8-in.) I.D. Tubing or 11.1mm (7/16-in.) or 12.7mm (1/2-in.) I.D. Tubing
I.D. Tubing I.D. Tubing I.D. Tubing I.D. Tubing
24/40 24/40 35/25 35/25 #25 O‑Ring

Specifications for Joints, Inner Joint Outer Joint Ball Joint Socket Joint Joint
Threads, and Stopcocks

24 24 35 25
mm mm mm mm
40
mm 25
25
Standard Taper 40 mm
mm
mm 35
Symbol used to designate mm
interchangeable joints, stoppers
and stopcocks that comply with
the requirements of Commercial #25 #25 Bushing 0-5 mm Hi-Vac 12/30 Glass
Standard CS-21 published by Ace‑Thred for Stopcock Stopcock Plug 12
Ace‑Thred mm
N.I.S.T. Straight Bore
30
25 mm
JS
Spherical Joint mm
Symbol designates spherical joints 25 16.2/56

mm Glass
that comply with CS-21. Double
16.2
mm
0-5 mm Orifice Oblique

Stopcock Plug 56
Product Standard Maximum Flow mm
Symbol designates stopcock
plugs made of PTFE that meet 2 mm
BORE
requirements of N.I.S.T. Voluntary 1 1:5 Taper
Size 11/25 PTFE 11
Product Standard PS 28-70. Stopcock Plug
mm
25
mm

6 Technical Information
Low Density High Density

Plastic Properties Polyethylene
(LDPE)
Polyethylene
(HDPE)
Polypropylene
(PP) PTFE/FEP
Polycarbonate
(PC)
Polymethylpentene
(PMP)
Temperature Limit, °C 80 120 135 205 135 175
Specific Gravity 0.92 0.95 0.90 2.15 1.20 0.83
Tensile Strength, psi 2000 4000 5000 3000 8000 4000
Brittleness Temperature, °C –100 –100 0 –270 –135 20
Water Absorption, % <0.01 <0.01 <0.02 <0.01 0.35 <0.01
Flexibility excellent rigid rigid excellent rigid rigid
Transparency translucent translucent translucent translucent clear clear
O‑Ring Compatibility Chart

Key: 1=Recommended; 2=Satistfactory; 3=Poor; 4=Marginal; 5=Not Recommended; A=Acceptable; NA=Not Acceptable
Viton Silicone Buna-N EPDM Chemraz 514 Kalrez 4079 FETFE CAPFE
Temperature Range °C –26 to 204 –62 to 204 –37 to 121 –54 to 149 –30 to 220 –15 to 316 –18 to 204 –60 to 204
Compression set 2 2 2 2 2 2 2 3
Durometer 75 70 70 70 70 75 70 70
Steam < 120 °C 3 4 4 4 1 1 1 5
Acetone 4 3 3 2 1 1 5 1
Toluene 2 3 3 3 1 1 2 2
Tetrachloroethane 1 3 3 3 1 1 1 2
THF 4 4 4 4 1 1 5 3
Methyl Ethyl Ketone 5 5 5 2 1 1 5 2
Acetonitrile 5 5 5 5 1 1 5 2
Hydrochloric Acid (conc) 2 5 4 5 1 1 2 4
Ammonia Gas (cold) 4 1 2 2 1 1 4 2
Tetrachloroethylene 3 5 3 3 1 1 3 2
Sulfuric Acid (dilute) 2 5 1 5 2 2 2 2
Nitric Acid (conc) 2 5 4 5 1 1 2 4
Calcium Carbonate 2 5 1 1 1 1 2 2
Xylene 2 4 4 3 1 1 2 2
Mineral Oils 1 2 1 4 1 1 1 1
Sodium Carbonate 1 1 1 1 1 1 1 2
Vacuum 1 4 2 4 4 4 1 2
FDA A A A A NA NA NA A
Chemical compatibility information courtesy of the respective manufacturers of each o-ring type. Ace is not responsible for errors.
Conversion Factors
Length Volume Power

1 millimeter (mm)............. 0.1 centimeter (cm) 1 cubic centimeter..................... 0.001 liter (L) 1 watt...............................0.73756 foot pound
per second
1 centimeter............................0.01 meter (M) 1 cubic centimeter..............0.0610 cubic inch 1 foot pound
1 centimeter.................................. 0.394 inch 1 cubic inch........... 16.3872 cubic centimeter per second................................ 1.3582 watts
1 inch................................. 2.540 centimeters 1 cubic meter..................... 35.314 cubic feet 1 watt.....................0.056884 BTU per minute
1 meter......................................... 3.2808 feet 1 BTU per minute...................... 17.580 watts
1 cubic foot................... 0.02832 cubic meter
1 foot...........................................0.305 meter
1 watt................. 0.001341 horsepower (U.S.)
Capacity
Area 1 horsepower (U.S.)..................... 754.7 watts
1 milliliter (mL)........................ 0.03382 ounce 1 watt.......................0.01433 kilogram-calorie
1 square centimeter (cm).0.1550 square inch (U.S. Liquid) per minute
1 square inch......... 6.452 square centimeters 1 ounce (U.S. Liquid)............ 29.573 milliliters 1 kilogram-calorie
1 square meter (M)........... 10.764 square feet per minute................................. 69.767 watts
1 liter (L)..................................1.05671 quarts
1 square foot...............0.09290 square meter (U.S. Liquid)
1 quart (U.S. Liquid)................... 0.94633 liter
Temperature
Mass °C = (F–32) 5/9
1 liter....................................... 0.26418 gallon
1 gram.............. 0.03527 ounce (Avoirdupois) (U.S. Liquid) °F = 9/5 C +32
1 ounce (Avoirdupois)............. 28.3495 grams 1 gallon (U.S. Liquid)................ 3.78533 liters
1 kilogram.........2.20462 pound (Avoirdupois) 1 lambda.......................0.001 cc / 1 microliter
1 pound (Avoirdupois)........ 0.45359 kilogram

Glass Properties
Unless otherwise specified, ACE GLASS brand glassware
is fabricated from Corning 7740, Kimble KG-33, Kavalier/ Composition (approximate percent)
Simax, or Schott-Duran ® glass and conforms to federal
specifications DD-G-541B and ASTM E-438. Also meets Corning 7740 Duran Kavalier/Simax
the U.S. Pharmacopoeia specs for Type I Borosilicate Si02 80.6% 81% 80.4%
Glass. Glass properties are those represented by the
B203 13.0% 13% 13.0%
aforementioned companies.
Na20/K20 4.1% 4% 4.2%
Al203 2.3% 2% 2.4%
Properties
Corning 7740 Schott-Duran Kavalier/Simax
Coefficient of Expansion 32.5 x 10-7 cm/cm/°C 3.3 x 10-6 cm/cm/°K 3.3.1 x 10-6 cm/cm/°K
Strain Point 510°C 510°C 510°C
Annealing Point 560°C 560°C 560°C
Softening Point 821°C 815°C 820°C
Density 2.53 g/cm3 2.23 g/cm3 2.23 g/cm3
Temperature Limits 230°C (Normal use) 230°C (Normal use) 240°C (Normal use)
400°C (Extreme, short-term use only) 400°C (Extreme, short-term use only) 400°C (Extreme, short-term use only)
Maximum Thermal Shock 160°C 160°C 160°C
Refractive Index 1.4741 1.4741 1.4721
1
At Sodium D Line
Flask Stoppers ACE Glass Fiber Filter Discs

Approximate Length Diameter Porosity
Stopper Diameter at of Ground at Large Maximum Pore Corning, Kimble
Number Small End, mm Zone, mm End, mm Diameter and ChemGlass
ACE Porosity Range Equivalents/
8 7.25 10 ±1.0 8.25 Designation (micron) Porosities Uses
9 8 14 ±1.0 9.40
13 12 14 ±1.0 13.40 A 145-174 EC (170-220) Coarse Filtration
16 15 15 ±1.0 16.50 B 70-100 — Coarse Filtration
19 18 17 ±1.0 19.70 C 25-50 ACE C (40-60) Gas Dispersion
22 20 20.5 ±1.0 22.05 D 10-20 M (10-15) Extraction
27 25 21.5 ±1.0 27.15 E 4-8 F (4-5.5) Extraction
32 30 21.5 ±1.0 32.15
38 35 30 ±1.0 38.00
Pressure Conversions
Absolute Gauge Pressure
Torr
cm or mm Atmo- lb/ ton/ gram/ ft. of in. of in. of
of Hg of Hg Micron sphere in.2 ft.2 cm2 H20 Hg lb. in. Hg
76 760 760000 1 14.7 1.06 1033 33.9 29.9 0.00 0.00

70 700 700000 0.921 13.53 0.975 952 31.2 27.6 1.16 2.36
60 600 600000 0.79 11.6 0.835 816 26.8 23.6 3.10 6.30
50 500 500000 0.659 9.67 0.696 680 22.3 19.7 5.03 10.2
40 400 400000 0.526 7.74 0.557 545 17.8 15.7 6.97 14.2
30 300 300000 0.395 5.8 0.417 408 13.4 11.8 8.90 18.1
20 200 200000 0.263 3.87 0.278 272 8.92 7.87 10.8 22.0
10 100 100000 0.132 1.94 0.139 136 4.46 3.94 12.8 26.0
5 50 50000 0.006 0.967 0.07 68 2.23 1.97 13.7 27.9
1 10 10000 0.013 0.194 0.014 13.6 0.446 0.394 14.5 29.5
0.1 1 1000 0.001 0.019 0.001 1.36 0.045 0.039 14.68 29.88
0 0 0 0 0 0 0 0 0 14.7 29.92

Reference Guide to ACE Boiling Flasks

Capacity, Approx. Approx. Capacity, Approx. Approx. Capacity, Approx. Approx.
mL O.D. mm O.D. Inches mL O.D. mm O.D. Inches mL O.D. mm O.D. Inches
5 25 1.0 200 75 3.0 12000 285 11.22
10 31 1.24 250 82 3.25 22000 350 13.78
15 35 1.4 300 86 3.385 500001 457 18.0
20 38 1.5 500 100 4.0 500002 488 19.3
25 42 1.68 1000 125 5.0 500003 508 20.0
50 50 2.0 2000 160 6.3 72000 508 20.0
100 58 2.25 3000 180 7.0 100000 610 24.0
5000 225 8.86 2000002 750 29.5
2000003 762 30.0
Corning flask; 2 Schott flask; 3 QVF flask.
1
Guide to Flange Styles
Flat Flange
(with or without o-ring groove) I.D. O.D. Thickness
100 mm (4-inch) 138 mm (5.4-inch) 10 mm (0.4-inch)
130 mm (5.1-inch) 168 mm (6.6-inch) 10 mm (0.4-inch)
Uses Clamp: 6508, 6509, 6510 Flat clamp
Conical Flange I.D. O.D. Thickness

102mm (4-inch) 135mm (5.3-inch) 30mm (1.2-inch)
Uses Clamp: 6496 Standard clamp
Schott-Duran Flange
(with or without o-ring groove) I.D. O.D. Thickness
60mm (2.4-inch) 100mm (4-inch) 20mm (0.8-inch)
Uses Clamp: 6517 Quick release clamp
KF Plane Flange I.D. O.D. Thickness

200mm (8-Inch) 230mm (9-Inch) 24mm (0.95-Inch)
300mm (12-Inch) 338mm (13.3-inch) 24mm (0.95-inch)
Uses Clamp: 6525 Coupling
Beaded Process Beaded Process Pipe flanges range 1/2-inch thru 6-inch I.D.
Pipe Flange Example: 2-inch pipe = 2-inch I.D.
2-9/16 inch bead O.D.
Tube O.D. = 2-5/16-inch
See page 270 for dimensions for all sizes of beaded pipe
Uses Clamp: 8856 Coupling

Standard Pipe Thread Fittings
The illustrations are

actual size. If you have
any questions as to
the size of fitting you
require, simply compare
the threads per inch, the
diameter and length of
the threading, and the
taper of the threading of
your existing fittings to
these drawings.
Sterilization Reference Guide

Method Procedure
Autoclave: Cycle is 121ºC, 15 psig (1bar) 20 min
Dry Heat: 170ºC for 60 min
Gas: Ethylene Oxide for formaldehyde
Microwave: Transmission of microwaves
Gamma Irradiation: High energy ionizing gamma radiation from a Cobolt 60 source
Chemical Disinfectants: Quaternay Ammonim Compounds, Iodophors, Formalin, Benzalkonium
Chloride, Ethanol, etc.
Viscosity Conversion Factors

Viscosity is the resistance to flow due to the internal friction within a fluid. This is generally expressed as the Dilatant Liquids — viscosity increases
force required to move one unit area one unit distance. Kinematic and absolute viscosity are related by the as shear rate increases. Mixers can bog
density of the fluid. down and stall after initially mixing such
liquids. Dilatant liquids include slurries,
Kinematic Viscosity Absolute to Kinematic Viscosity clay, and candy compounds.
Multiply ➝ to get Multiply ➝ to get Newtonian Liquids — viscosity
to get Divide to get Divide remains constant regardless of
➝ ➝
ft2/sec 92903.04 centistokes centipoises 1/density (g/cm ) 3
centistokes shear rate or agitation. As mixer
ft2/sec 0.092903 sq. meters/sec centipoises 0.00067197/density (lb/ft3) ft2/sec speed increases, flow increases
sq. meters/sec 10.7639 ft2/sec proportionately. Newtonian liquids
lbf-sec/ft2 32.174/density (lb/ft3) ft2/sec
sq. meters/sec 1000000.0 centistokes include water, mineral oils, and
centistokes 0.000001 sq. meters/sec kg-sec/m2 9.80665/density (kg/m3) sq. meters/sec hydrocarbons.
centistokes 0.0000107639 ft2/sec Pascal-sec 1000/density (g/cm3) centistokes
Pseudoplastic Liquids — viscosity
decreases as shear rate increases, but
Absolute or Dynamic Viscosity Kimematic to Absolute Viscosity initial viscosity may be sufficiently great
Multiply ➝ to get Multiply ➝ to get to prevent mixing. Typical pseudoplastic
to get
➝
Divide to get
➝
Divide liquids are gels, latex paints, and lotions.
lbf-sec/ft2 47880.26 centipoises centistokes density (g/cm )
3
centipoises Thixotropic Liquids — as with
lbf-sec/ft2 47.8803 Pascal-sec sq. meters/sec 0.10197 x density (kg/m3) kg-sec/m2 pseudoplastic liquids, viscosity
centipoises 0.000102 kg-sec/sq. meter ft2/sec 0.03108 x density (lb/ft3) lbf-sec/ft2 decreases as shear rate or agitation
centipoises 0.001 lbf-sec/ft* ft2/sec 1488.16 x density (lb/ft3) centipoises increases. When agitation is stopped or
Pascal-sec 0.0208854 Pascal-sec centistokes 0.001 x density (g/cm3) Pascal-sec reduced, hysteresis occurs and viscosity
Pascal-sec 1000 centipoises sq. meters/sec 1000/density (g/cm3) Pascal-sec increases. Often the viscosity will not
*Sometimes absolute viscosity is given in terms of pounds return to its initial value. Thixotropic
mass. In this case—centipoises x 0.000672 = lbm/ft sec. liquids include soaps, tars, shortening,
glue, inks, and peanut butter.

Chemical Resistance for Plastic Resins @ 20˚C

Classes of Substances
Acids, Hydro- Oxidiz-
dilute Acids, Hydro- Hydro- carbons, ing
or strong Alcohols, Alde- carbons, carbons, haloge agents,
weak & conc. aliphatic hydes Bases Esters aliphatic aromatic nated Ketones strong
ACL ✖ ✖ ▲ ■ ▲ ▲ ● ● ▲ ▲ ✖
ECTFE/ETFE ● ▲ ● ● ● ● ● ● ● ▲ ■
FEP/TFE/PFA ● ● ● ● ● ● ● ● ● ● ●
FLPE ● ● ● ▲ ■ ● ● ● ▲ ● ■
XLPE ● ● ● ▲ ● ▲ ▲ ▲ ■ ▲ ■
HDPE/XLPE ● ● ● ▲ ● ▲ ▲ ▲ ■ ▲ ■
DLPE ● ● ● ▲ ● ▲ ■ ■ ✖ ▲ ■
PC ● ✖ ▲ ■ ✖ ✖ ■ ✖ ✖ ✖ ✖
PCT ● ■ ● ■ ▲ ■ ● ✖ ✖ ■ ✖
PTE ● ✖ ● ✖ ✖ ✖ ● ✖ ✖ ✖ ✖
PMMA ▲ ✖ ✖ ▲ ■ ✖ ▲ ✖ ✖ ✖ ✖
PMP ● ● ● ▲ ● ▲ ■ ■ ✖ ■ ■
PP/PPCO ● ● ● ▲ ● ▲ ▲ ■ ■ ▲ ■
PS ● ■ ● ✖ ● ✖ ✖ ✖ ✖ ✖ ✖
PSF ● ▲ ▲ ■ ● ✖ ▲ ✖ ✖ ✖ ▲
PUR ▲ ■ ■ ▲ ✖ ✖ ● ✖ ✖ ✖ ✖
PVC Bottles ● ● ● ✖ ● ✖ ● ✖ ✖ ✖ ▲
Flexible PVC Tubing ● ■ ▲ ✖ ▲ ✖ ■ ✖ ✖ ✖ ■
PVDF ● ● ● ● ● ▲ ● ● ✖ ✖ ▲
TPE ● ■ ● ✖ ● ✖ ✖ ✖ ✖ ✖ ✖
Resin Codes Chemical Resistance Classifications

ACL Acetal (Polyoxymethylene)
ECTFE Halar® ECTFE (Ethylene-Chlorotrifluoroethylene Copolymer) ● 30 days of constant exposure causes no damage.
ETFE Tefzel® ETFE (Ethylene-Tetrafluoroethylene) Plastic may even tolerate for years.
FEP Teflon® FEP (Fluorinated Ethylene Propylene) ▲ Little or no damage after 30 days of constant
FLPE Fluorinated High-Density Polyethylene exposure to the reagent.
HDPE High-Density Polyethylene
LDPE Low-Density Polyethylene ■ Some effect after seven days of constant exposure
PC Polycarbonate to the reagent. Depending on the plastic, the
PCT Poly (1,4 Cyclohexylene Dimethylene Terephthalate) effect may be crazing, cracking, loss of strength
PET Polyethylene Terephthalate or discoloration. Solvents may cause softening,
PFA Teflon® PFA (Perfluoroalkoxy) swelling and permeation losses with LDPE, HDPE,
PMMA Polymethyl Methacrylate (Acrylic) PP, PPCO and PMP. The solvent effect on these five
PMP Polymethylpentene (“TPX®”) resins are normally reversible; the part will usually
PP Polypropylene return to its normal condition after evaporation.
PPCO Polypropylene Copolymer ✖ Not recommended for continuous use. Immediate
PS Polystyrene damage may occur. Depending on the plastic, the
PSF Polysulfone effect will be a more severe crazing, cracking, loss
PUR Polyurethane of strength, discoloration, deformation, dissolution
PVC Polyvinyl Chloride or permeating loss.
PVDF Polyvinyllidene Fluoride
TFE Teflon®TFE (Tetrafluoroethylene)
TPE Thermoplastic Elastomer
XLPE Cross-Linked High-Density Polyethylene

Bench Reactors/Filter 11
ACE Filter Reactors allow single

or multi-step reactions and
filtrations in the same vessel.
Stirrer Motors
13500 series or
13566 series
Major Design Chuck Typical

Features 8124, 8126
Assembly
Shaft
■■ 100 mL to 6000 mL 8075
standard
Bearing
8050, 8066
■■ Unjacketed or jacketed
■■ All inert materials Head
6527/6528/6529
■■ Reactions at ambient
Clamp
or pressure conditions 6517
■■ Filtering by vacuum
and/or pressure Reactor Body
6384, 6386
Clamp Holder
■■ Removable/changeable 13550-25
PTFE Agitator
filters, poly screen or 8089
glass, wide choice of
Chain Clamp
porosities PTFE Adapter 11079-24
5857, 5838, 5861
■■ Mechanical agitation
Filter Support
5848
■■ Inert bottom drain valve Valve
5839
w/5844 Adapter
■■ Easy assembly/
disassembly for cleaning
Support Stands
12840, 13550, 13586

12 Bench Reactors/Filter
8075
Stirring
Shaft
6384 UNJACKETED FILTER REACTOR «
Rugged heavy wall reactor with 60mm (2.4‑inch), 100mm (4‑inch), or 150mm (6‑inch)
Schott style top flange with o‑ring groove at top, for connection to 6527, 6528 or 6529
heads, with 6517 quick release clamp. Bottom has an Ace‑Thred (internal glass thread)
for installing 5838-83 (size 50) or 5857-86 (size 80) bottom adapter with filter support
8066 and drain valve. Head has three  24/40 joints on 60mm size; four  24/40 joints on
Bearing 100mm and 150mm sizes.
Complete item consists of: reactor body with CAPFE o‑ring, head with  joints, 6517
clamp, PTFE bottom adapter with CAPFE o‑ring (with perforated plate—#80 thread only),
6527/6528/6529 retainer ring, 350 micron polypropylene screen support and 100 micron polyethylene
Head support, 5844 adapter, 5839 shutoff valve (optional larger valve is available), 8066 bearing,
8075 stirring rod, and 8089 multipaddle agitator.
For replacement glass fritted support, polyethylene support or polypropylene screen,
see 5848 or 5814. For condenser and funnel, see 6029 and 7298; stoppers with  24/40
joints, see 8250. For stirring motor, see 13511 or 13566 motor; for chuck, see 8124 or
6517 8126. Use 7855-829 CAPFE o-ring for #50 adapter, 7855-864 for #80 bottom adapter.
Clamp Flange Bottom Body Approx. Top
Cap., I.D., Thread I.D., Height*, CAPFE Order
mL mm (in.) Size mm mm O‑Ring Code Each
150 60 (2.4) #50 60 100 7855-878 6384-115 1240.55
7855 600 60 (2.4) #50 79 205 7855-878 6384-121 1284.35
CAPFE 1000 100 (4) #80 100 180 7855-880 6384-125 1457.18
O‑Ring
2000 100 (4) #80 126 210 7855-880 6384-129 1624.11
3000 150 (6) #80 150 205 7855-881 6384-133 2012.91
6000 150 (6) #80 150 395 7855-881 6384-137 2103.95
6384-15
Reactor *Height measurements are measured from top of flask flange to seal on top thread.
Body Note: 150mL and 600mL heads have angled side necks.
8089
Agitator
Stand (13550), Clamp
(11079) and Clamp Holder
(13550-25) not included.
#50 / 5838 or / #80 5857
Bottom Adapter
w/Filter Support
(with 3/8" FNPT
outlet)
5844/12770 Adapter
3/8" MNTP – 1/4" FNPT/
3/8" MNTP – 3/8" MNTP
5839
Bottom Valve
See page 51 for stands.
(For #80, bottom also available with 1/2" MNPT.)
Ordering & Product Information: 1-800-223-4524 n www.aceglass.com Subject to Ace Discount (Page 4) Net
6384
UNJACKETED FILTER REACTOR, PRESSURE VERSION «
Heavy wall glass reactor available with 60mm (2.4-inch), 100mm (4-inch), or 150mm
(6‑inch) diameter Schott style flange with o-ring groove at top. Connects to #6433
35 PSIG
@100°C
head with a #6517 quick release clamp. Reactor bottom has an Ace‑Thred for installing 8075
a 5838-83 (size 80) or 5857-86 (size 50) adapter with a filter support and bottom drain Stirring
valve. The 60mm reactor head has a #15 Ace‑Thred center neck, (2) #15 and (1) #7 Shaft
Ace‑Thred side necks. The 100mm head has a #15 Ace‑Thred center neck, (3) #15 and
(1) #7 Ace‑Thred side necks. The 150mm head has a #15 Ace‑Thred center neck, (4) 8044
#15 and (1) #7 Ace‑Thred side necks. The Ace‑Threds allow for vacuum or pressure Bearing
applications and for easy draining of material out of the reactor. The main bearing, funnel
and condenser are designed to connect to the threads on the head via compression
bushing connections. The #7 Ace‑Thred is used for connecting a 1/4‑inch O.D. tubing
fitting to allow for a direct connection to a pressure source or a #6448 pressure manifold.
Complete item consists of: reactor body with 60mm CAPFE o-ring, head with
Ace‑Threds, 6517 clamp, PTFE bottom threaded adapter and valve with CAPFE o-ring, 6433
Head
retainer ring, 350 micron polypropylene screen support, 100 micron polyethylene
support, 5844 adapter, 8044 bearing, 8075 stir rod, 8089 paddle agitator, 6024
condenser, 7299 addition funnel and #7 Ace‑Thred bushing. Size 80 bottom adapter
also comes with a perforated glass plate support.
6517
Pressure manifold (page 20), stand and clamps are optional. For replacement glass Clamp
fritted discs and supports see 5848 or 5814. See 13511 or 13566 motor; for chuck,
see 8124 or 8126. Use 7855-829 CAPFE o-ring for #50 adapter, 7855-864 for #80
bottom adapter. 7855
Flange Bottom Body Approx. Top CAPFE
Cap., I.D., Thread I.D., Height*, CAPFE Order O‑Ring
150 60 (2.4) #50 60 100 7855-878 6384-225 1751.53
600 60 (2.4) #50 99 205 7855-878 6384-231 1802.37
1000 100 (4) #80 100 180 7855-880 6384-235 2009.44
2000 100 (4) #80 126 210 7855-880 6384-239 2195.92
3000 150 (6) #80 150 205 7855-881 6384-243 2635.79 6384-19
6000 150 (6) #80 150 395 7855-881 6384-247 2753.61 Reactor
*Height measurements are measured from top of flask flange to seal on top thread. Body
Note: 150mL and 600mL heads have angled side necks.
8089
Agitator
Stand (13586) and Support
Shelf (11173) not included.
#50 / 5838 or / #80 5857
Bottom Adapter
w/Filter Support
(with 3/8" FNPT
outlet)
5844/12770 Adapter
3/8" MNPT – 1/4" FNPT/
3/8" MNPT – 3/8" MNPT
Glass Filter Discs

5839
Bottom
Valve
(For #80, bottom also available with 1/2‑inch MNPT.)

6386 JACKETED FILTER REACTOR «

Rugged heavy wall reactor, jacketed for cooling and/or heating of reaction material. With 60mm
(2.4‑inch), 100mm (4‑inch), or 150mm (6‑inch) Schott style flange with o‑ring groove at top,
for connection to 6527, 6528 or 6529 heads, with 6517 quick release clamp. Bottom has an
Ace‑Thred (internal glass thread) for installing 5838-83 (size 50) or 5857-86 (size 80) bottom
adapter with filter support and drain valve. Body is jacketed with size 28/15 o‑ring ball joints
on inlet/outlet, sealed tangentially for more efficient circulation. Head has three  24/40 joints
on 60mm size; four  24/40 joints on 100mm and 150mm sizes.
8075
Stirring Complete item consists of: reactor body with 60mm CAPFE o‑ring, head with joints, 6517
Shaft clamp, PTFE bottom adapter with CAPFE o‑ring (with perforated plate — #80 thread only),
retainer ring, 350 micron polypropylene screen support and 100 micron polyethylene support,
5844 adapter, 5839 shutoff valve (optional larger valve is available), non-flaking 8066 bearing,
8075 stirring rod, 8089 multipaddle agitator.
For replacement glass fritted support, polyethylene support or polypropylene screen, see 5848
8066 or 5814. For condenser and funnel, see 6029 and 7298; stoppers with  24/40 joints, see 8250.
Bearing For stirring motor, see 13511 or 13566 motor; for chuck, see 8124 or 8126. Use 7855-829
CAPFE o-ring for #50 adapter, 7855-864 for #80 bottom adapter.
Flange Bottom Body Approx. Top
6527/6528/ Cap., I.D., Thread I.D., Height*, CAPFE Order
6529 Head mL mm (in.) Size mm mm O‑Ring Code Each
150 60 (2.4) #50 60 100 7855-878 6386-40 1965.54
600 60 (2.4) #50 79 205 7855-878 6386-45 2232.07
1000 100 (4) #80 100 180 7855-880 6386-50 2731.96
6517 2000 100 (4) #80 126 210 7855-880 6386-55 3072.39
Clamp 3000 150 (6) #80 150 205 7855-881 6386-60 3691.26
6000 150 (6) #80 150 395 7855-881 6386-65 4011.93
*Height measurements are measured from top of flask flange to seal on top thread.
7855 Note: 150mL and 600mL heads have angled side necks.
CAPFE
O‑Ring
6386-16
Jacketed
Reactor Stand (13586) and Support
Body Shelf (11173) not included.
28/15 O‑Ring
Ball Joint
8089 Connectors
Agitator
#50 / 5838 or / #80 5857

Bottom Adapter
w/Filter Support
(with 3/8” FNPT
outlet)
5844/12770
Adapter
3/8" MNPT – 1/4" FNPT/ For a complete catalog of
3/8" MNPT – 3/8" MNPT
recirculating chillers, please
contact Ace Glass.
5839
Bottom
Valve
6386 JACKETED FILTER REACTOR, PRESSURE VERSION «

Heavy wall glass reactor, jacketed version for cooling or heating of reactor. Available with 60mm
(2.4-inch), 100mm (4-inch), or 150mm (6-inch) diameter Schott flange with o-ring grove at top.
35 PSIG
@100°C
Connects to #6433 head with a #6517 quick release clamp. Reactor bottom has an Ace‑Thred
for installing a 5838-83 (size 50) or 5857-86 (size 80) adapter with a filter support and bottom
drain valve. Jacket inlet/outlet are size 28/15 o-ring ball joint connections, sealed tangentially for
more efficient circulation. The 60mm reactor head has a #15 Ace‑Thred center neck, (2) #15 and 8075
(1) #7 Ace‑Thred side necks. The 100mm head has a #15 Ace‑Thred center neck, (3) #15 and Stirring
(1) #7 Ace‑Thred side necks. The 150mm head has a #15 Ace‑Thred center neck, (4) #15 and Shaft
(1) #7 Ace‑Thred side necks. The Ace‑Threds allow for vacuum or pressure applications and
for draining material out of the reactor. The main bearing, funnel and condenser are designed to
connect to the threds on the head via compression bushing connections. The #7 Ace‑Thred is 8044
used for connecting a 1/4-inch O.D. tubing fitting to allow for a direct connection to a pressure Bearing
source or a #6448 pressure manifold.
Complete item consists of: reactor body with 60mm CAPFE o-ring, head with
Ace‑Threds, 6517 clamp, PTFE bottom threaded adapter and valve with CAPFE
o-ring, retainer ring, 350 micron polypropylene screen support, 100 micron
polyethylene support, 5844 adapter , 8044 bearing, 8075 stir rod, 8089 paddle 6433
agitator, 6024 condenser, 7299 addition funnel and #7 Ace‑Thred bushing. Head
Size 80 bottom adapter also comes with a perforated glass plate support.
Pressure manifold (page 20), stand and clamps are optional. For replacement
glass fritted discs and supports see 5848 or 5814. For motor, see 13511 or 6517
13566; for chucks see 8124 or 8126. Use 7855-829 CAPFE o-ring for #50 Clamp
adapter, 7855-864 for #80 bottom adapter
7855
Flange Bottom Body Approx. Top CAPFE
Cap., I.D., Thread I.D., Height*, CAPFE Order O‑Ring
150 60 (2.4) #50 60 100 7855-878 6386-107 2476.52
6386-16
600 60 (2.4) #50 79 205 7855-878 6386-110 2750.09
Jacketed
1000 100 (4) #80 100 180 7855-880 6386-115 3284.22 Reactor
2000 100 (4) #80 126 210 7855-880 6386-120 3644.20 Body
3000 150 (6) #80 150 205 7855-881 6386-124 4314.14
6000 150 (6) #80 150 395 7855-881 6386-128 4661.59
*Height measurements are measured from top of flask flange to seal on top thread. 28/15 O‑Ring
Ball Joint
Note: 150mL and 600mL heads have angled side necks. Connectors
8089
Agitator
Stand (13586) and Support #50 / 5838 or / #80 5857

Shelf (11173) not included. Bottom Adapter
w/Filter Support 5844/12770
(with 3/8” FNPT outlet) Adapter
3/8" MNPT – 1/4"
FNPT/3/8" MNPT –
3/8" MNPT
E-SA
AC
FE
ON
OR

C
N ECT
5839
Bottom
Valve

Small
Volume 6381 UNJACKETED FILTER REACTOR «
Small-volume filter reactor with  45/50 joint at top and #50 Ace‑Thred (internal glass thread)
at bottom that accepts a 5838-83 (size 50) PTFE bottom adapter with filter support and drain
valve. Head has a  19/38 center neck and three  14/20 side necks. Complete item consists
of: reactor body, head with joints, clamp, #50 PTFE bottom adapter with size –136 CAPFE
o‑ring, 350 micron polypropylene screen support, 100 micron polyethylene support, 5844
adapter, 5839-42 shutoff valve, 8066-120 non-flaking bearing, 9534-40 stirring rod, 9542-20
blade. For glass fritted support replacements for polypropylene screen and polyethylene sup-
9534 port, see 5848 or 5814; for condensers see 6024; for addition funnel see 7299. For stirring
Stirring
Shaft
motor, see 13523; for chuck, see 8124 or 8126.
Complete:
Bottom Thread Body I.D., Approx. Use
Cap., mL Top Joint Size mm Height, mm Joint Clamp
100 45/50 #50 51 65 7598-45
150 45/50 #50 51 125 7598-45
Head, only Body, only Complete

8066 Cap., mL Order Code Each Order Code Each Order Code Each
Bearing 100 9443-10 188.78 6381-05 114.95 6381-25 836.60
150 9443-10 188.78 6381-10 119.18 6381-30 840.83
Components:
Order Order
Description Code Each Description Code Each
Adapter, PTFE, Stirring Shaft, 6mm x 318mm
5844-120 88.91 9534-40 42.71
3
∕8" mpt–¼" FNPT, only long, with button
Bottom Adapter, Stirring Blade, PTFE 9542-20 9.45
5838-83 232.72
#50–3∕8" FNPT, only Order
Bottom Shutoff Valve, Optional Accessories Code
9443 5839-42 110.20
Head ¼" MNPT–¼" Tube, PTFE PTFE Sleeves 14/20/Pkg. 3 7642-07 10.00
Clamp, Plastic, 45/50 7598-45 50.48 PTFE Sleeves 19/38/Pkg. 3 7643-06 5.73
Bearing, 19/22, 6mm 8066-120 111.21 PTFE Sleeves 45/50/Pkg. 3 7642-23 27.14
Stopper, 14/20 9543-04 14.30 Thermometer Adpt., 14/20 5028-26 27.55
6381-05
CAPFE o-ring 7855-829 23.39
Body
9542
Blade
Stand (13550), Clamp
(11079) and Clamp Holder
#50 / 5838 (13550-25) not included.
Bottom Adapter
w/Filter Support
(3/8" FNPT outlet)
5844-120
Adapter
3/8" MNPT– 1/4" FNPT
5839
Valve
Bench Reactor Accessories 17
Filter Reactor Accessories and Replacement Parts
Instatherm Heated Filter Reactor ®
Use with either regular or pressure version head and accessories.

6388 FILTER REACTOR, UNJACKETED Instatherm, Body only
Same rugged, heavy-wall reactor flask as 6384, except Instatherm® coated for
safer, rapid heating. Instatherm is an integral noble metal alloy fused permanently
to the glass and covered with a tough silicone rubber-treated glass cloth insulation
which serves as a thermal barrier as well as protection against physical shock. Heat
response is rapid and thermal lag low — typical heating rates are approximately 5° per
minute. Instatherm can be operated at 120v or 40v with ACE or J-Kem temperature
controllers. Flange at top is Schott-Duran style 60mm (2.4‑inch), 100mm (4‑inch),
or 150mm (6‑inch) with shallow o‑ring groove, for connection to 6527, 6528, 6529
or 6533 head, with 6517 quick release clamp. Bottom has a #50 or #80 Ace‑Thred
(internal glass thread) for installing 5838, 5857, or 5861 bottom adapter with filter
support and drain valve. For head, bottom adapter, and other accessory items,
order separately. Supplied with cord and CAPFE o-ring. Maximum temperature
(with no vacuum or pressure) is 200°C.
Flange Bottom Body Approx. Top

Cap., I.D., Thread I.D., Height, CAPFE Order
mL mm (in.) Size mm mm O‑Ring Volts Amps Watts Code Each
150 60 (2.4) #50 50 100 7855-878 40 6 240 6388-15 988.47
600 60 (2.4) #50 50 205 7855-878 40 8 320 6388-20 1052.27
1000 100 (4) #80 96 180 7855-880 120 5 600 6388-25 1139.96
2000 100 (4) #80 126 210 7855-880 120 8 960 6388-30 1331.27 6388
3000 150 (6) #80 150 205 7855-881 120 9 1080 6388-35 1674.05
6000 150 (6) #80 150 395 7855-881 120 10 1200 6388-40 1785.64
ACE Custom Glass

Design Service
www.aceglass.com
ACE Scientific Glass Repair Service
www.aceglass.com
1-800-223-4524
18 Bench Reactor Accessories
6384 FILTER REACTOR Unjacketed, Body only

Reactor body, only, with Schott-style flange with o‑ring groove at top and ACE #50 or
#80 internal thread at bottom. Pressure rating is 35 psi. Supplied with CAPFE o‑ring.
Flange Bottom Body Body Approx. Top
6384 Cap., I.D., Thread O.D., I.D., Height, CAPFE Order
mL mm (in.) Size mm mm mm O‑Ring Code Each
150 60 (2.4) #50 70 60 100 7855-878 6384-05 257.21
600 60 (2.4) #50 89 79 205 7855-878 6384-11 301.01
1000 100 (4) #80 110 100 180 7855-880 6384-15 369.42
2000 100 (4) #80 140 126 210 7855-880 6384-19 536.35
3000 150 (6) #80 165 150 205 7855-881 6384-23 827.76
6000 150 (6) #80 165 150 395 7855-881 6384-27 913.96
6386 FILTER REACTOR Jacketed, Body only

6386 Reactor body, only, with Schott-style flange with o‑ring groove at top and ACE #50 or
#80 internal thread at bottom. Body is jacketed for heating/cooling. Inlet/outlet of jacket
are 28/15 o‑ring ball joints, sealed tangentially, for more efficient circulation. Pressure
rating is 35 psi. Supplied with CAPFE o‑ring.
Flange Bottom Body Body Approx. Top
Cap., I.D., Thread O.D., I.D., Height, CAPFE Order
mL mm (in.) Size mm mm mm O‑Ring Code Each
150 60 (2.4) #50 100 60 100 7855-878 6386-06 982.20
600 60 (2.4) #50 120 79 205 7855-878 6386-12 1248.73
1000 100 (4) #80 140 100 180 7855-880 6386-16 1644.20
2000 100 (4) #80 180 126 210 7855-880 6386-20 1984.63
3000 150 (6) #80 190 150 205 7855-881 6386-24 2506.11
6000 150 (6) #80 190 150 395 7855-881 6386-28 2821.94
5839 VALVE PTFE, Bottom Shut Off

PTFE valve for bottom of 5838, 5857, or 5861 bottom adapter to control flow from reactor.
Code -42 has an male NPT thread at one end for attaching to 5844 adapter, other end is
a 1/4-inch O.D. tubing compression fitting; codes -47 and -55 have female NPT threads
on both ends, for connecting to 5844 adapter using 12770 nipple. Must use 5844-120
adapter (3/8-inch male NPT – 1/4-inch female NPT) when connecting 5839-42; 12770-54
(3/8-inch male NPT – 3/8-inch male NPT) when connecting 5839-47.
For Bottom
Adapter Size NPT Size Order Code Each
50 1/4" Male NPT–1/4" Tube 5839-42 110.20
5839-42 80 3/8" Female NPT–3/8" Female NPT 5839-47 505.36
5839-47, -55
80 1/2" Female NPT–1/2" Female NPT 5839-55 532.33
Barb (for use with 5839-47) 3/8" Male NPT–3/8" I.D. Tube 12770-38 24.21
Reactor Bottom 12770 ADAPTER PTFE

Combinations PTFE adapter used to connect 5839-47 or -55 valve to 5838 or 5857 bottom adapter.
5838-80 5857-68 5857-85
Order Order
NPT Size Code Each NPT Size Code Each
5844-120 12770-59 5844-120
3/8" MNPT–3/8" MNPT 12770-54 19.40 1/2" MNPT–1/2" MNPT 12770-59 29.49
5839-42 5839-55 5839-42 12770
5857-85 5838-80 5844 ADAPTER PTFE
Used to connect 5839 valve to 5838 or 5857 bottom adapter.
12770-54 12770-54
Order Order
5839-47 5839-47 NPT Size Code Each NPT Size Code Each
5844 3/8" MNPT–1/4" FNPT 5844-120 88.91 1/2" MNPT–1/2" FNPT 5844-125 107.15
12770-38 12770-38
5848 PLATE Glass 5848-60

Perforated glass plate for #80 thread size 5857 or 5861 adapters.
Order Code Each

5848-60 86.83
5838/5857 ADAPTER PTFE, Bottom Outlet

Bottom adapter for use with 6384, 6386 or 6388 reactor bodies and 6390 PTFE reactor.
Fabricated from PTFE, #50 and #80 have a 3/8-inch female NPT for connecting bottom
valve. Both have a CAPFE o‑ring to seal adapter in Ace‑Thred. #50 size supplied with 100
micron polyethylene support disc (see 5848, above, for replacement or glass substitute).
Can also be replaced with screen support using retainer ring. #80 size supplied with
dual filter supports; a 100 micron polyethylene filter (see 5848, above) and/or perforated
support plate with retainer ring for use with 350 micron polypropylene screen (for other
screen sizes, see 5814).
5838
For Thread Size Bottom Opening Order Code Each (Size 50)
50 3/8-inch FNPT 5838-83 232.72 5857-86, -89
80 3/8-inch FNPT 5857-86 326.41 (Size 80)
(Optional) 80 1/2-inch FNPT 5857-89 326.41
CAPFE o‑ring, replacement for #50, Pkg/1 — 7855-829 23.39
CAPFE o‑ring, replacement for #80, Pkg/1 — 7855-864 28.62
5857 RETAINER RING PTFE

5857-38
PTFE rings for size #50 & #80 adapters. Slide in to hold screens, filter paper, etc.
Dimensions
Adapter Size Thickness, mm O.D., mm I.D., mm Order Code Each
#50 0.125 1.955 1.750 5857-38 13.39
#80 0.127 2.950 2.656 5857-52 15.30
5814 SCREEN SUPPORT Polypropylene

For use with 5838, 5857, or 5861 bottom adapters. It is necessary to use a PTFE retainer
ring (above) to hold support in adapter. See page 265 for additional sizes.
Thread Size Micron Pkg. Quantity Order Code Each

50 350 12 5814-348 35.76
80 350 12 5814-350 46.80
50 295 12 5814-358 35.76
80 295 6 5814-60 54.39
50 210 12 5814-368 35.76
80 210 6 5814-70 54.39 5814
50 105 12 5814-88 36.45
80 105 6 5814-90 54.39
50 74 12 5814-378 35.76
5861 ADAPTER PTFE, with Side Outlet 5861

Same adapter as 5838/5857 except with 3/8-inch NPT side discharge port. Fits 6384,
6386, 6388 reactor flask bodies. Comes with 7855-800 series CAPFE o-rings. See 5814
screen support and 5857 retainer ring (above).
For Thread Size Order Code Each

50 5861-03 234.71
80 5861-07 323.51
CAPFE o‑ring, replacement for #50, Pkg/1 7855-829 23.39

13385-44
8767-20
6448 MANIFOLD Pressure, Epoxy Coated
5844-176 Complete glass manifold, fitted with a pressure gauge, primary
adjustable pressure relief valve, and secondary rupture disc to allow
5844-62 5844-74 for safer operation of pressure and filter reactors.
5844-74
13385 Pressure Gauge is a 0-60 psi stainless steel internal, with
12517-14 5844-74 1-1/2‑inch face and 1/8-inch npt male connection for use with
5844-74 adapter in #15 Ace‑Thred.
8767 Pressure Relief Valve is adjustable from 3-50 psig by adjusting
set screws to desired cracking pressure. Ends are 1/4-inch npt for
6448-24 6445-12
connecting to #15 Ace‑Thred on manifold with 5844-74 adapter.
To 5844-58 #7 Ace‑Thred and 12517-08, -40
6445 Rupture Disc is a secondary safety device that, in the event of an overpressure (one that cannot be handled by the 8767
relief valve) will rupture at a predetermined burst rating; 55 psig (±3 psig) for -12 version, 65 psig (±3 psig) for -41 version. Disc is
manufactured from high-purity carbon with a PTFE coating on the underside. No springs or moving parts, disc is secured directly
in #25 Ace‑Thred of manifold with 5844‑176 adapter.
Manifold is connected to #7 Ace‑Thred on 6433 head using 5844‑58 adapter (must be ordered separately) and 12517 tubing
connectors with 1/4‑inch tubing.
For Two-Piece For One-Piece

Pressure Reactors (55 Pressure R eactors
psig) and Filter Reactors (65 psig)
Order Code Each Order Code Each
Adapter, PTFE, #15–1/8-inch NPT 5844-62 67.75 5844-62 67.75
Adapter, PTFE, #15–1/4-inch NPT (3) 5844-74 67.75 5844-74 67.75
Adapter, PTFE, #25–1/4-inch NPT, w/o o‑ring 5844-176 88.93 5844-176 88.93
Rupture Disc, Graphite, 55 psig 6445-12 133.39
Rupture Disc, Graphite, 65 psig (for pressure version only) 6445-41 133.39
Manifold, Glass, (4) #15, (1) #25, Epoxy Coated 6448-24 197.03 6448-24 197.03
Valve, Pressure Relief, 1/4-inch NPT, 3–50 psig 8767-20 86.02 8767-20 86.02
Coupling Body, 1/8-inch MPT 12517-08 11.42 12517-08 11.42
Coupling Insert, for 1/4-inch O.D. tubing (2) 12517-40 12.25 12517-40 12.25
Tubing, PP, 1/4-inch O.D. x .170-inch I.D., 10 feet 12681-110 13.22 12681-110 13.22
Gauge, Pressure, 0–60 psi, 1/8-inch MPT 13385-44 171.92 13385-44 171.92
Complete 6448-54* 989.82 6448-68** 989.82
Replacement o-rings
Size –110 for #15 adapters (shelf-pack of 12) 7855-716 19.78 7855-716 19.78
Additional Items
*6448-54 is for use with two-piece pressure and filter style reactors.
**6448-68 is for use with one-piece pressure reactors only.
Bench Reactors 21
A complete, general purpose

benchtop cylindrical reactor.
All-in-One Self-supported and portable,
with a small footprint.
Benchtop Reactor • Electric heating mantle with digital
temperature controller and Type
“J” PTFE-covered thermoprobe for
1 or 2 liter Cylindrical operation from room temperature
to 200°C
• Large 4-in. diameter flange on flask and head with • 125 mL pressure equalizing addition
CAPFE (PTFE encapsulated silicone rubber) o‑ring and funnel
Quick Release clamp facilitate assembly/disassembly
and removal of contents. • Reflux condenser
• All glass and PTFE wetted components. • Support stand, clamps, clamp
holders and joint clips
• PTFE joint sleeves and valves and FETFE o‑rings for
high-purity, grease-free system with high chemical
resistance. Note: This re
ac
• Suitable for high-vacuum situations. available with tor is
bo
outlet on flask ttom
• Overhead mechanical stirring with 10 mm diameter glass ; call or
e-mail for pric
stirring shaft, PTFE multi-paddle agitator, flexible shaft e.
and variable speed motor with controller.
1 LITER 2 LITER
Order Order
Code Each Code Each
FLASK, 1-liter, Cylindrical, 4-inch (100mm) Grooved FLASK, 2-liter, Cylindrical, 4-in. (100mm) Grooved Flange
6521-10 152.00 6521-12 161.73
Flange with CAPFE o‑ring with CAPFE o‑ring
HEAD, 4-inch (100mm) 24/40 Center Neck, HEAD, 4-in. (100mm) 24/40 Center Neck,
6528-31 281.42 6528-31 281.42
(3) 24/40 Side Necks (3) 24/40 Side Necks
CLAMP, Quick Release, 4-inch 6517-25 98.23 CLAMP, Quick Release, 4-inch 6517-25 98.23
CONDENSER, 24/40, 300mm Jacket Length with CONDENSER, 24/40, 300mm Jacket Length with
5946-118 152.29 5946-118 152.29
Ace-Safe Connectors Ace-Safe Connectors
FUNNEL, Addition, 125mL, Pressure Equalizing, FUNNEL, Addition, 125mL, Pressure Equalizing,
7298-05 231.90 7298-05 231.90
24/40 Joints 24/40 Joints
STIRRING SHAFT, 10mm, Polished with Ring, 44cm 8075-32 57.11 STIRRING SHAFT, 10mm, Polished with Ring, 58 cm 8075-34 60.33
AGITATOR, PTFE, 4-Blade Multipaddle, 64 mm dia. 8089-06 111.43 AGITATOR, PTFE, 4-Blade Multipaddle, 64mm dia. 8089-06 111.43
BEARING, 10mm, PTFE, 24/40, Complete 8066-43 111.75 BEARING, 10mm, PTFE, 24/40, Complete 8066-43 111.75
CHUCK, Flex-Grip, for 10mm Rod, 5/16-in. Motor Shaft 8124-10 43.92 CHUCK, Flex-Grip, for 10mm Rod, 5/16-in. Motor Shaft 8124-10 43.92
STIRRING MOTOR & CONTROLLER, Reversible, Variable STIRRING MOTOR & CONTROLLER, Reversible, Variable
13649-19 1265.18 13649-19 1265.18
Speed, Complete Speed, Complete
FLEXIBLE SHAFT, 91.4cm (36-inch) 8081-30 187.03 FLEXIBLE SHAFT, 91.4cm (36") 8081-30 187.03
HEATING MANTLE, Aluminum Housed, 335w, 115v 12058-12 325.00 HEATING MANTLE, Aluminum Housed, 450w, 115v 6478-51 356.00
TEMP. CONTROLLER, Digital, Type “J,” 120 volts 12125-14 797.11 TEMP. CONTROLLER, Digital, Type “J,” 120 volts 12125-14 797.11
THERMOPROBE, Type “J,” 1/4-in. O.D. x 12 in. long, THERMOPROBE, Type “J,” 1/4-in. O.D. x 12" long,
12141-25 118.70 12141-25 118.70
PTFE covered PTFE covered
THERMOPROBE, Lead Only, Detachable, Type “J” 12141-80 69.68 THERMOPROBE, Lead Only, Detachable, Type “J” 12141-80 69.68
ADAPTER, Offset, 24/40–#7, Complete 5032-22 34.31 ADAPTER, Offset, 24/40–#7, Complete 5032-22 34.31
ADAPTER, 24/40, 2mm Bore PTFE Stopcock 5202-12 80.01 ADAPTER, 24/40, 2mm Bore PTFE Stopcock 5202-12 80.01
ADAPTER, Offset, 24/40– 24/40 5268-10 36.56 ADAPTER, Offset, 24/40– 24/40 5268-10 36.56
STOPPER, Glass 24/40 (3) 8250-12 19.79 STOPPER, Glass 24/40 (3) 8250-12 19.79
SLEEVES, PTFE 24/40, Pkg/3 (2) 7642-11 10.70 SLEEVES, PTFE 24/40, Pkg/3 (2) 7642-11 10.70
JOINT CLIPS, Plastic 24/40, Pkg/10 7598-24 39.32 JOINT CLIPS, Plastic 24/40, Pkg/10 7598-24 39.32
SUPPORT STAND, 29 in. High x 5/8-in. Dia. Rod, “U” Base 13586-10 274.82 SUPPORT STAND, 36 in. High x 5/8-in. Dia. Rod, “U” Base 13586-13 313.93
CLAMP, Three-jaw, Medium 11067-14 39.73 CLAMP, Three-jaw, Medium 11067-14 39.73
CLAMP HOLDER, Regular (3) 11080-19 18.82 CLAMP HOLDER, Regular (3) 11080-19 18.82
COMPLETE 6542-12 3953.86 COMPLETE 6542-25 4120.32

22 Bench Reactors
A complete, general purpose

All-in-One Jacketed benchtop cylindrical reactor.
Self-supported and portable,
Benchtop Reactor with a small footprint.
• Temperature controller and Type
1 or 2 liter Cylindrical “J” PTFE-covered thermoprobe for
operation from room temperature
to 200°C
• Large 4-in. diameter flange on jacketed flask and
• 125 mL pressure equalizing addition
head with CAPFE (PTFE encapsulated silicone rubber)
funnel
o‑ring and Quick Release clamp facilitate assembly/
disassembly and removal of contents. • Reflux condenser
• All glass and PTFE wetted components. • Support stand, clamps, clamp
holders and joint clips
• PTFE joint sleeves and valves and FETFE o‑rings for
high-purity, grease-free system with high chemical • Pressure manifold optional
resistance.
• Mechanical stirring with 10 mm diameter glass stirring
shaft, PTFE multi-paddle agitator, flexible shaft and
variable speed motor with controller.
• Includes temperature controller and probe
1 LITER 2 LITER
Order Order
Code Each Code Each
FLASK, Jacketed, 1-liter, Cylindrical, 4-inch (100mm) FLASK, Jacketed, 2-liter, Cylindrical, 4-in. (100mm)
6524-13 883.96 6524-15 995.14
Grooved Flange with CAPFE o‑ring, Bottom Outlet Grooved Flange with CAPFE o‑ring, Bottom Outlet
HEAD, 4-inch (100mm) 24/40 Center Neck, HEAD, 4-in. (100mm) 24/40 Center Neck,
6528-31 281.42 6528-31 281.42
(3) 24/40 Side Necks (3) 24/40 Side Necks
CLAMP, Quick Release, 4-inch 6517-25 98.23 CLAMP, Quick Release, 4-inch 6517-25 98.23
CONDENSER, 24/40, 300mm Jacket Length with CONDENSER, 24/40, 300mm Jacket Length with
5946-118 152.29 5946-118 152.29
Ace-Safe Connectors Ace-Safe Connectors
FUNNEL, Addition, 125mL, Pressure Equalizing, FUNNEL, Addition, 125mL, Pressure Equalizing,
7298-05 231.90 7298-05 231.90
24/40 Joints 24/40 Joints
STIRRING SHAFT, 10mm, Polished with Ring, 44cm 8075-32 57.11 STIRRING SHAFT, 10mm, Polished with Ring, 58 cm 8075-34 60.33
AGITATOR, PTFE, 4-Blade Multipaddle, 64 mm dia. 8089-06 111.43 AGITATOR, PTFE, 4-Blade Multipaddle, 64mm dia. 8089-06 111.43
BEARING, 10mm, PTFE, 24/40, Complete 8066-43 111.75 BEARING, 10mm, PTFE, 24/40, Complete 8066-43 111.75
CHUCK, Flex-Grip, for 10mm Rod, 5/16-in. Motor Shaft 8124-10 43.92 CHUCK, Flex-Grip, for 10mm Rod, 5/16-in. Motor Shaft 8124-10 43.92
STIRRING MOTOR & CONTROLLER, Reversible, Variable STIRRING MOTOR & CONTROLLER, Reversible, Variable
13649-19 1265.18 13649-19 1265.18
Speed, Complete Speed, Complete
FLEXIBLE SHAFT, 91.4cm (36-inch) 8081-30 187.03 FLEXIBLE SHAFT, 91.4cm (36") 8081-30 187.03
ADAPTER, Offset, 24/40–#7, Complete 5032-22 34.31 ADAPTER, Offset, 24/40–#7, Complete 5032-22 34.31
ADAPTER, 24/40, 2mm Bore PTFE Stopcock 5202-12 80.01 ADAPTER, 24/40, 2mm Bore PTFE Stopcock 5202-12 80.01
ADAPTER, Offset, 24/40– 24/40 5268-10 36.56 ADAPTER, Offset, 24/40– 24/40 5268-10 36.56
STOPPER, Glass 24/40 (3) 8250-12 19.79 STOPPER, Glass 24/40 (3) 8250-12 19.79
SLEEVES, PTFE 24/40, Pkg/3 (2) 7642-11 10.70 SLEEVES, PTFE 24/40, Pkg/3 (2) 7642-11 10.70
JOINT CLIPS, Plastic 24/40, Pkg/10 7598-24 39.32 JOINT CLIPS, Plastic 24/40, Pkg/10 7598-24 39.32
SUPPORT STAND, 29 in. High x 5/8-in. Dia. Rod, “U” Base 13586-10 274.82 SUPPORT STAND, 36 in. High x 5/8-in. Dia. Rod, “U” Base 13586-13 313.93
CLAMP, Three-jaw, Medium 11067-14 39.73 CLAMP, Three-jaw, Medium 11067-14 39.73
CLAMP HOLDER, Regular (4) 11080-19 18.82 CLAMP HOLDER, Regular (4) 11080-19 18.82
CLAMP, Chain Clamp 11079-24 51.23 CLAMP, Chain Clamp 11079-24 51.23
PLATE SUPPORT SHELF, w/102mm center hole 11173-17 111.28 PLATE SUPPORT SHELF, w/102mm center hole 11173-17 111.28
STAINLESS STEEL SUPPORT ROD, 28 inches high 13586-25 104.64 STAINLESS STEEL SUPPORT ROD, 28 inches high 13586-25 104.64
COMPLETE 6539-05 4203.00 COMPLETE 6539-10 4355.59
Bench Reactors/Pressure 23
Pressure Reactors
T he following ACE heavy wall borosilicate glass Pressure
Reactors have been designed and tested to provide the
chemist with a system to perform low to moderate positive
pressure reactions, synthesis, and catalysis, or simply to
run reactions under inert gas conditions. Reactor capacities
range from 500 mL to 5000mL, and use Ace‑Threds to
achieve a leak-tight system.
Typical
Two types of Pressure Reactors are available:
Assembly
1— Two-Piece System, with a maximum
pressure limit of 35 psig @ 100°C.
2— One-Piece System, with a maximum
pressure limit of 45 psig @ 100°C
The Two-Piece System consists of a flanged flask and
head with a shallow o‑ring groove, o‑ring and quick release
clamp. Flange sizes range from 60mm to 150mm inside
diameter, allowing the use of large a
gitators and facilitating
product removal and clean-out.
The One-Piece System provides a 25mm center opening,
with smaller openings as side necks, and has a higher
allowable operating pressure. Safety is the foremost concern when operating
Both systems offer vessels with or without bottom outlet pressurized glass reactors. With this in mind, ACE
valves and with or without heating/cooling jackets. These offers a separate manifold, 6448 (see photo), which
jackets are heat sealed. MUST be used in conjunction with all pressure systems
listed in this catalog. It consists of a glass manifold
Complete systems and their components are listed on the with Ace‑Threds, PTFE adapters, a pressure gauge,
following pages. Systems are available with: a primary adjustable pressure release valve, and a
■■ Mechanical Stirring, using stirring shaft with secondary fixed pressure rupture disc. In addition,
agitator, and a unique bearing designed with internal approved safety shields, eye and body protection
o‑ring seals. should be used to avoid personal injury.
For all complete systems the following accessories have

Due to varying conditions, ACE cannot been included:
guarantee glassware against breakage
■■ Liquid addition funnel
caused by pressure or vacuum.
■■ Stirring motor, controller and flexible shaft
■■ Heating mantle and temperature control system
■■ Thermowell
■■ Temperature controller with thermocouple
■■ Pressure relief manifold
IMPORTANT— General Warnings for Pressurized Glassware

Due to varying conditions, ACE cannot guarantee glass vessels from breakage under pressure.
ALL LABORATORY SAFETY PROCEDURES SHOULD BE OBSERVED. ALWAYS WORK BEHIND A SHIELD.
■■Do not use with materials ■■Before applying pressure, ■■Questions regarding the safe ■■Safety coatings: epoxy and
which solidify on standing examine glassware carefully operating conditions of a plastic coating help prevent
and create excessive stress for surface scratches which particular glass vessel under scratching and shattering and
on glass. may weaken its strength. pressure may be directed to reduce spills; however, they
ACE GLASS INCORPORATED. do not prevent breakage

24 Bench Reactors/Pressure
Complete ACE
Two-Piece Unjacketed
Pressure Reactors
6423
SERIES ONE
8081
Pressure Reactor
Manifold, Complete, 6448
(See page 20 for a complete
listing of parts in this assembly)
5846
Tubing
12681
8075
8124
6024 7299
13530
8044
12110
7506
6433
6471
6423 6517
12111
13649
12058
8082-04 8116
8648-19 14120
Does NOT include stand, base or clamps.
6423
Complete Unjacketed Two-Piece Pressure Reactor
Two-piece systems with a maximum pressure limit of 35 psig @ 100ºC.
SERIES ONE
6423-200 Complete System Order Code Each 6423-215 Complete System Order Code Each
(contains all items listed below) 6423-200 5962.58 (contains all items listed below) 6423-215 6145.75
500mL, 60mm Flange Order Code Each 2000mL, 100mm Flange Order Code Each
#15 PTFE Plug (Complete contains TWO) 5846-48 38.41 #15 PTFE Plug (Complete contains TWO) 5846-48 38.41
West Condenser w/Ace‑Threds 6024-20 129.75 West Condenser w/Ace‑Threds 6024-20 129.75
Flask, 500 mL, 60mm flange top 6423-05 170.98 Flask, 2000 mL, 100mm flange top 6423-20 497.34
Head, 60mm, #15 center neck, three side necks 6433-23 295.48 Head, 100mm, #15 center neck, four side necks 6433-35 396.77
Pressure Reactor Manifold, complete 6448-54 989.82 Pressure Reactor Manifold, complete 6448-54 989.82
Thermowell 6471-04 36.76 Thermowell 6471-14 37.64
Clamp, 60mm, Quick Release 6517-22 87.08 Clamp, 100mm, Quick Release 6517-25 98.23
Addition Funnel, 60mL 7299-06 305.29 Addition Funnel, 250mL 7299-25 336.29
#15 PTFE Bushing (Complete contains TWO) 7506-27 40.65 #15 PTFE Bushing (Complete contains TWO) 7506-27 40.65
Bearing, complete, with Ace‑Threds 8044-24 233.08 Bearing, complete, with Ace‑Threds 8044-24 233.08
Stir Shaft, 10mm 8075-12 55.65 Stir Shaft, 10mm 8075-12 55.65
Flexible Shaft, complete, 91.4cm 8081-30 187.03 Flexible Shaft, complete, 91.4cm 8081-30 187.03
Stirrer Blade, PTFE, 19mm 8082-02 8.39 Stirrer Blade, PTFE, 19mm 8082-04 10.03
Krytox® High Vacuum Grease 8116-10 105.04 Krytox® High Vacuum Grease 8116-10 105.04
Flex-Grip Chuck 8124-10 43.92 Flex-Grip Chuck 8124-10 43.92
Bushing, PTFE, #15 with o‑ring 8648-19 31.37 Bushing, PTFE, #15 with o‑ring 8648-19 31.37
Aluminum Heating Mantle 12058-03 622.85 Aluminum Heating Mantle 12058-16 335.00
Type “J” Thermocouple Sensor, PTFE-clad 12110-25 50.88 Type “J” Thermocouple Sensor, PTFE-clad 12110-25 50.88
Digital Temperature Controller, “J” output 12111-15 1424.21 Digital Temperature Controller, “J” output 12111-15 1424.21
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID 12681-110 13.22 Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID 12681-110 13.22
Stirrer Motor Controller, Solid State 13530-10 523.17 Stirrer Motor Controller, Solid State 13530-10 523.17
Stirrer Motor with Mounting Rod, Solid State 13649-09 742.01 Stirrer Motor with Mounting Rod, Solid State 13649-09 742.01
PTFE Sealing Tape, 1/2-inch Width 14120-18 11.91 PTFE Sealing Tape, 1/2-inch Width 14120-18 11.91
#15 PTFE Plug (Complete contains TWO) 5846-48 38.41 #15 PTFE Plug (Complete contains THREE) 5846-48 38.41
Head, 100mm, #15 center neck, four side necks 6433-35 396.77 Head, 150mm, #15 center neck, five side necks 6433-44 544.04

Complete ACE
Two-Piece Unjacketed
Pressure Reactors
6425
SERIES TWO
Bottom Outlet
8081
5846 Pressure Reactor

7299
12681
8124
8044
6024
8075
13530
12110
7506
6433
6517 6471
6425
12111
12058
13649
8082-04 8116
8648-19 14120
Does NOT include stand, base or clamps
6425
Complete Unjacketed Two-Piece Pressure Reactor
Two-piece systems with a maximum pressure limit of 35 psig @ 100ºC. Flask has bottom outlet.
SERIES TWO
Flask, 500mL, 60mm flange top w/bottom outlet 6425-04 300.71 Flask, 2000mL, 100mm flange top w/bottom outlet 6425-15 651.79
Stirrer Blade, PTFE, 19mm wide 8082-02 8.39 Stirrer Blade, PTFE, 19mm wide 8082-04 10.03

Complete ACE
Two-Piece Jacketed
Pressure Reactors
6427
SERIES ONE
8081
5846 Pressure Reactor

7299
12681
8124 6024
8075
8044
13530
7506
6433
6517
6471
6427
13649
8082-04 8116
8648-19 14120 Does NOT include stand, base or clamps.
Shown without clamps for better visibility.
6427
Complete Jacketed Two-Piece Pressure Reactor
Two-piece systems with a maximum pressure limit of 35 psig @ 100ºC.
SERIES ONE
500mL, 60mm Flange Order Code Each 2000mL, 100 Flange Order Code Each
Flask, 500mL, 60mm flange top 6427-09 797.82 Flask, 2000mL, 100mm flange top 6427-18 1250.49
6427-223 Complete System Order Code Each

(contains all items listed below) 6427-223 6944.97
3000mL, 150mm Flange Order Code Each
500mL, 100mm Flange Order Code Each #15 PTFE Plug (Complete contains THREE) 5846-48 38.41
#15 PTFE Plug (Complete contains TWO) 5846-48 38.41 West Condenser w/Ace‑Threds 6024-20 129.75
West Condenser w/Ace‑Threds 6024-20 129.75 Flask, 3000mL, 150mm flange top 6427-23 3435.42
Flask, 500mL, 100mm flange top 6427-13 783.11 Head, 150mm, #15 center neck, five side necks 6433-44 544.04
Head, 100mm, #15 center neck, four side necks 6433-35 396.77 Pressure Reactor Manifold, complete 6448-54 989.82
Pressure Reactor Manifold, complete 6448-54 989.82 Thermowell 6471-22 38.07
Thermowell 6471-10 36.76 Clamp, 150mm, Quick Release 6517-27 117.67
Clamp, 100mm, Quick Release 6517-25 98.23 Addition Funnel, 150mL 7299-25 336.29
Addition Funnel, 60mL 7299-06 305.29 #15 PTFE Bushing (Complete contains TWO) 7506-27 40.65
#15 PTFE Bushing (Complete contains TWO) 7506-27 40.65 Bearing, complete, with Ace‑Threds 8044-24 233.08
Bearing, complete, with Ace‑Threds 8044-24 233.08 Stir Shaft, 10mm 8075-12 55.65
Stir Shaft, 10mm 8075-12 55.65 Flexible Shaft, complete, 91.4cm 8081-30 187.03
Flexible Shaft, complete, 91.4cm 8081-30 187.03 Stirrer Blade, PTFE, 24mm wide 8082-06 12.60
Stirrer Blade, PTFE, 19mm wide 8082-04 10.03 Krytox® High Vacuum Grease 8116-10 105.04
Krytox® High Vacuum Grease 8116-10 105.04 Flex-Grip Chuck 8124-10 43.92
Flex-Grip Chuck 8124-10 43.92 Bushing, PTFE, #15 with o‑ring 8648-19 31.37
Bushing, PTFE, #15 with o‑ring 8648-19 31.37 Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID 12681-110 13.22
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID 12681-110 13.22 Stirrer Motor Controller, Solid State 13530-10 523.17
Stirrer Motor Controller, Solid State 13530-10 523.17 Stirrer Motor with Mounting Rod, Solid State 13649-09 742.01
Stirrer Motor with Mounting Rod, Solid State 13649-09 742.01 PTFE Sealing Tape, 1/2-inch Width 14120-18 11.91
PTFE Sealing Tape, 1/2-inch Width 14120-18 11.91
5000mL, 150mm Flange Order Code Each
1000mL, 100mm Flange Order Code Each #15 PTFE Plug (Complete contains THREE) 5846-48 38.41
#15 PTFE Plug (Complete contains TWO) 5846-48 38.41 West Condenser w/Ace‑Threds 6024-20 129.75
West Condenser w/Ace‑Threds 6024-20 129.75 Flask, 5000mL, 150mm flange top 6427-26 3539.72
Flask, 1000mL, 100mm flange top 6427-16 801.21 Head, 150mm, #15 center neck, five side necks 6433-44 544.04
Head, 100mm, #15 center neck, four side necks 6433-35 396.77 Pressure Reactor Manifold, complete 6448-54 989.82
Pressure Reactor Manifold, complete 6448-54 989.82 Thermowell 6471-24 38.51
Thermowell 6471-14 37.64 Clamp, 150mm, Quick Release 6517-27 117.67
Clamp, 100mm, Quick Release 6517-25 98.23 Addition Funnel, 500mL 7299-34 367.99
Addition Funnel, 125mL 7299-12 313.29 #15 PTFE Bushing (Complete contains TWO) 7506-27 40.65
#15 PTFE Bushing (Complete contains TWO) 7506-27 40.65 Bearing, complete, with Ace‑Threds 8044-24 233.08
Bearing, complete, with Ace‑Threds 8044-24 233.08 Stir Shaft, 10mm 8075-14 57.59
Stir Shaft, 10mm 8075-12 55.65 Flexible Shaft, complete, 91.4cm 8081-30 187.03
Flexible Shaft, complete, 91.4cm 8081-30 187.03 Stirrer Blade, PTFE, 24mm wide 8082-06 12.60
Stirrer Blade, PTFE, 19mm wide 8082-04 10.03 Krytox® High Vacuum Grease 8116-10 105.04
Krytox® High Vacuum Grease 8116-10 105.04 Flex-Grip Chuck 8124-10 43.92
Flex-Grip Chuck 8124-10 43.92 Bushing, PTFE, #15 with o‑ring 8648-19 31.37
Bushing, PTFE, #15 with o‑ring 8648-19 31.37 Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID 12681-110 13.22
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID 12681-110 13.22 Stirrer Motor Controller, Solid State 13530-10 523.17
Stirrer Motor Controller, Solid State 13530-10 523.17 Stirrer Motor with Mounting Rod, Solid State 13649-09 742.01
Stirrer Motor with Mounting Rod, Solid State 13649-09 742.01 PTFE Sealing Tape, 1/2-inch Width 14120-18 11.91

Complete ACE
Two-Piece Jacketed
Pressure Reactors
6429
SERIES TWO
Bottom Outlet
8081
5846
Pressure Reactor
7299
8124
8075
12681
8044
6024 13530
7506
6433
6471
6517
6429
13649
8082-04 8116
8648-19 14120
Does NOT include stand, base or clamps.
6429
Complete Jacketed Two-Piece Pressure Reactor
Two-piece systems with a maximum pressure limit of 35 psig @ 100ºC. Flask has bottom outlet.
SERIES TWO
Flask, 500mL, 60mm flange top, bottom outlet 6429-09 877.65 Flask, 2000mL, 100mm flange top, bottom outlet 6429-24 1425.01

Complete ACE
One-Piece Unjacketed
Pressure Reactors
6436
SERIES FOUR
8081
Pressure Reactor
8124
5846
Tubing
12681
8075
7299 13530
8044
6024
12110
7506
6436
12111 6471
13649
12058
8082-04
8116 14120
8648-19
6436
Complete Unjacketed One-Piece Pressure Reactor
One-piece systems with a maximum pressure limit of 45 psig @ 100ºC.
SERIES FOUR
500mL Order Code Each 3000mL Order Code Each
Flask, 500mL 6436-06 458.51 Flask, 3000mL 6436-31 598.78
Flask, 1000mL 6436-09 495.44 Flask, 5000mL 6436-37 647.28

2000mL Order Code Each
#15 PTFE Plug (Complete contains TWO) 5846-48 38.41
West Condenser w/Ace‑Threds 6024-20 129.75
Flask, 2000mL 6436-22 555.89
Pressure Reactor Manifold, complete 6448-68 989.82
Thermowell 6471-43 36.76
Addition Funnel, 150mL 7299-25 336.29
#15 PTFE Bushing (Complete contains TWO) 7506-27 40.65
Bearing, complete, with Ace‑Threds 8044-55 247.66
Stir Shaft, 10mm 8075-12 55.65
Flexible Shaft, complete, 91.4cm 8081-30 187.03
Stirrer Blade, PTFE, 19mm 8082-04 10.03
Krytox® High Vacuum Grease 8116-10 105.04
Flex-Grip Chuck 8124-10 43.92
Bushing, PTFE, #15 with o‑ring 8648-19 31.37
Aluminum Heating Mantle 12058-16 335.00
Type “J” Thermocouple Sensor, PTFE-clad 12110-25 50.88
Digital Temperature Controller, “J” output 12111-15 1424.21
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID 12681-110 13.22
Stirrer Motor Controller, Solid State 13530-10 523.17
Stirrer Motor with Mounting Rod, Solid State 13649-09 742.01

Complete ACE
One-Piece Unjacketed
Pressure Reactors
8081
6437
SERIES SIX
with Bottom Outlet
Pressure Reactor
5846 listing of parts in this assembly)
7299 8124
8075
8044
12681
6024
7506
13530
6437 6471
12110
12058
12111
13649
8082-04
8116 14120
8648-19
6437
Complete Unjacketed One-Piece Pressure Reactor
One-piece systems with a maximum pressure limit of 45 psig @ 100ºC. Flask has bottom outlet.
SERIES SIX
Flask, 500mL 6437-07 589.48 Flask, 3000mL 6437-20 760.35
Stirrer Blade, 19mm 8082-04 10.03 Stirrer Blade, 19mm 8082-04 10.03
Flask, 1000mL 6437-13 615.91 Flask, 5000mL 6437-24 700.32
Stirrer Blade, 19mm 8082-04 10.03 Stirrer Blade, 19mm 8082-04 10.03

Flask, 2000mL 6437-16 700.32
Stir Shaft, 10mm 8075-12 55.65
Stirrer Blade, 19mm 8082-04 10.03
Aluminum Heating Mantle 12058-51 561.86
Type “J” Thermocouple Sensor, PTFE-clad 12110-25 50.88
Digital Temperature Controller, “J” output 12111-15 1424.21

Complete ACE
One-Piece Jacketed
Pressure Reactors 8081
6438
SERIES FOUR
Pressure Reactor
5846
8124
7299
12681
8075
8044 13530
6024
7506
6471
6438
13649
8082-04
8116 14120
8648-19 Does NOT include stand, base or clamps.
6438
Complete Jacketed One-Piece Pressure Reactor
One-piece systems with a maximum pressure limit of 45 psig @ 100ºC.
SERIES FOUR
Flask, 500mL 6438-14 1106.92 Flask, 3000mL 6438-24 3090.02
Flask, 1000mL 6438-17 1152.67 Flask, 5000mL 6438-29 3266.12

Flask, 2000mL 6438-19 1259.39
Stir Shaft, 10mm 8075-12 55.65

Complete ACE
One-Piece Jacketed
Pressure Reactors
6439
SERIES SIX
with Bottom Outlet
8081
Pressure Reactor
5846 listing of parts in this assembly)
12681
7299 8124
8075
6024
8081
7506
13530
6471
6439
13649
8082-04
8116 14120
8648-19 Does NOT include stand, base or clamps.
6439
Complete Jacketed One-Piece Pressure Reactor
One-piece systems with a maximum pressure limit of 45 psig @ 100ºC. Flask has bottom outlet.
SERIES SIX
Flask, 500mL with bottom outlet 6439-15 1198.32 Flask, 3000mL with bottom outlet 6439-29 3243.02
Flask, 1000mL with bottom outlet 6439-21 1251.81 Flask, 5000mL with bottom outlet 6439-34 3583.92

Flask, 2000mL with bottom outlet 6439-25 1375.16
Stir Shaft, 10mm 8075-12 55.65

6423 FLASK Pressure Reaction, Unjacketed

Heavy wall unjacketed reaction flask, part of the two-piece pressure reactor, for use at
elevated pressures*. Schott-Duran type top flange supplied with o‑ring groove for use
with heads 6433, 6527, 6528 or 6529. Supplied with CAPFE o‑ring (silicone optional).
For heating mantle, see 12058. Uses 6517 quick release clamp.
A Capacity, O.D., I.D., Height, Flange Size, Top Order

mL mm mm mm (A) mm (In.) O‑Ring Code Each
500 70 60 210 60 (2.4) 7855-878 6423-05 170.98
6423 500 110 100 100 100 (4) 7855-880 6423-07 218.67
1000 110 100 180 100 (4) 7855-880 6423-10 242.49
2000 140 130 230 100 (4) 7855-880 6423-20 497.34
3000 165 155 210 150 (6) 7855-881 6423-30 745.21
5000 165 155 310 150 (6) 7855-881 6423-35 847.86
6425 FLASK Pressure Reaction, Unjacketed, with Bottom Outlet

Heavy wall reaction flask with threaded bottom outlet, part of the two-piece pressure
reactor, for use at elevated pressures*. Schott-Duran type top flange supplied with o‑ring
groove for use with heads 6433, 6527, 6528 or 6529. Supplied with CAPFE o‑ring (silicone
A optional). For heating mantle, see 12058. Bottom outlet tube has 28/15 o‑ring ball joint
connection with size –116 FETFE o-rings. Uses 6517 quick release clamp.
Capacity, O.D., I.D., Height, Flange Size, Bottom Top Order
mL mm mm mm (A) mm (In.) Outlet, mm O‑Ring Code Each
500 70 60 210 60 (2.4) 0-8 7855-878 6425-04 300.71
6425 500 110 100 100 100 (4) 0-8 7855-880 6425-06 354.34
1000 110 100 180 100 (4) 0-8 7855-880 6425-12 376.20
2000 140 130 230 100 (4) 0-8 7855-880 6425-15 651.79
3000 165 155 210 150 (6) 0-10 7855-881 6425-19 890.27
5000 165 155 310 150 (6) 0-10 7855-881 6425-23 990.44
6427 FLASK Pressure Reaction, J acketed

Heavy wall reaction flask with jacket, part of the two-piece pressure reactor, for use at
elevated pressures*. Schott-Duran type top flange supplied with o‑ring groove for use
with heads 6433, 6527, 6528 or 6529. Supplied with CAPFE o‑ring (silicone optional).
Cooling/heating jacket is heat sealed. Inlet/outlet on jacket has size 28/15 o‑ring ball
joints with size –116 FETFE o-rings. Uses 6517 quick release clamp.
A Capacity, O.D., I.D., Height, Flange Size, Top Order
6427 mL mm mm mm (A) mm (In.) O‑Ring Code Each
500 110 60 210 60 (2.4) 7855-878 6427-09 797.82
500 130 96 100 100 (4) 7855-880 6427-13 783.11
1000 150 96 180 100 (4) 7855-880 6427-16 801.21
2000 180 126 230 100 (4) 7855-880 6427-18 1250.49
3000 215 151 210 150 (6) 7855-881 6427-23 3435.42
5000 215 151 310 150 (6) 7855-881 6427-26 3539.72
6429 FLASK Pressure Reaction, Jacketed, with Bottom Outlet

Heavy wall reaction flask with jacket and threaded bottom outlet, part of the two-piece
pressure reactor, for use at elevated pressures. Schott-Duran type top flange supplied
with a shallow o‑ring groove for use with heads 6433, 6527, 6528 or 6529. Supplied
with CAPFE o‑ring (silicone optional). Cooling/heating jacket is heat sealed. Inlet/outlet
A on jacket and bottom valve have size 28/15 o‑ring ball joint connections with size –116
FETFE o-rings. Uses 6517 quick release clamp.
Capacity, O.D., I.D., Height, Flange Size, Bottom Top Order
mL mm mm mm (A) mm (In.) Outlet, mm O‑Ring Code Each
500 110 60 210 60 (2.4) 0-8 7855-878 6429-09 877.65
6429 500 130 96 100 100 (4) 0-8 7855-880 6429-14 953.89
1000 150 96 180 100 (4) 0-8 7855-880 6429-20 963.17
2000 180 126 230 100 (4) 0-8 7855-880 6429-24 1425.01
3000 215 151 210 150 (6) 0-10 7855-881 6429-28 3568.78
5000 214 151 310 150 (6) 0-10 7855-881 6429-33 3765.86
*One-piece systems have maximum pressure limit of 45 psig @ 100°C;

Two-piece systems have maximum pressure limit of 35 psig @ 100°C.
6518 FLASK Reaction, Cylindrical, with ZDS™ Valve

Cylindrical, heavy wall flask with round bottom. Flask has Schott-Duran top type flange
supplied with o‑ring groove for use with heads 6433, 6527, 6528 or 6529. Comes with
one CAPFE o‑ring (silicone optional). Bottom outlet is ZDS™ (Zero Dead Space) PTFE
valve with Chemraz o-rings. Uses 6517 quick release clamp.
A
Capacity, O.D., I.D., Height, Flange Size. Bottom Top Order
mL mm mm mm (A) mm (in.) Outlet, mm O‑Ring Code Each
1000 110 100 180 100 (4) 0-10 7855-880 6518-10 538.44
2000 110 100 265 100 (4) 0-10 7855-880 6518-12 622.60
2000 155 145 200 150 (6) 0-20 7855-881 6518-14 627.86
3000 110 100 400 100 (4) 0-10 7855-880 6518-16 644.69
3000 150 140 250 150 (6) 0-20 7855-881 6518-18 651.37 6518
4000 155 145 300 150 (6) 0-20 7855-881 6518-20 758.94
6436 FLASK Pressure Reaction, Unjacketed

Heavy wall unjacketed reaction flask, part of the one-piece pressure reactor system, for
use at elevated pressures*. With vertical† Ace‑Thred necks for positive connection of 6436
stirrer, funnel, thermowell, condenser, etc.
Capacity, O.D., I.D., Height, Center Order
mL mm mm mm (A) Neck Side Necks Code Each
500 110 96 100 #25 (1) #7; (3) #15 6436-06 458.51
1000 110 96 180 #25 (1) #7; (3) #15 6436-09 495.44 A
2000 140 126 180 #25 (1) #7; (3) #15 6436-22 555.89
3000 165 151 195 #25 (1) #7; (4) #15 6436-31 598.78
5000 165 151 310 #25 (1) #7; (4) #15 6436-37 647.28
500mL and 1000mL sizes have necks angled at 5°.
†
6433 HEAD For Pressure or Filter Reactors, Ace‑Threds 6433-23

Reactor head, only, with Schott-Duran style flange and Ace‑Threds for use with 6384,
6386, 6388, or 6518 reactor bodies. Also fits 6423, 6425, 6427, and 6429 flasks. Pressure
rating is 35 psi. 6433-23 (only) has angled side joints. Uses 6517 quick release clamp.
For Flask Flange I.D., Center
Cap., mL mm (in.) Neck Side Necks Order Code Each
150- 600 60 (2.4) #15 (2)#15-(1)#7 6433-23 295.48
1000-2000 100 (4) #15 (3)#15-(1)#7 6433-35 396.77
3000-6000 150 (6) #15 (4)#15-(1)#7 6433-44 544.04
6433-35


6527-26 6527/6528/6529 HEAD For Filter Reactors, Joints

Reactor head, only, with Schott-Duran style flange and  joints for use with 6384, 6386
or 6388 reactor bodies. 6527-26 has three  24/40 joints (two side joints are angled);
6528-31 and 6529-32 have four  24/40 joints.
For Flask # of  24/40
Cap., mL Flange I.D., mm (in.) Joints Order Code Each
150- 600 60 (2.4) 3 6527-26 278.81
1000-2000 100 (4) 4 6528-31 281.42
3000-6000 150 (6) 4 6529-32 387.69
6528-31 / 6529-32
6471 THERMOWELL
For use with two-piece pressure reactors in #15 Ace‑Thred. Well has a shoulder that rides
against bottom of bushing to prevent “blowout.” o‑ring groove makes thermowell suitable
for full vacuum as well as pressure use. Inner diameter of well at top is approximately
6471 5mm. Order thermowell and bushing separately.
For Reactor
Cap., mL Length, mm Order Code Each
500 205 6471-04 36.76
500 170 6471-10 36.76
1000-2000 220 6471-14 37.64
3000 235 6471-22 38.07
5000 360 6471-24 38.51
8648-19
500 115 6471-41 36.76
1000-2000 180 6471-43 36.76
3000 210 6471-47 37.64
5000 290 6471-49 38.51
Bushing with FETFE o‑ring, only 8648-19 31.37
6437 FLASK Pressure Reaction, with Bottom Outlet

Heavy wall reaction flask with threaded bottom outlet valve, part of the one-piece pressure
reactor, for use at elevated pressures*. With vertical† Ace‑Thred necks for positive connection
of stirrer, funnel, thermowell, condenser, etc. Bottom outlet is a 28/15 o‑ring ball joint (with
size –116 FETFE o-rings, 7855-726) and a threaded valve for retrieving contents of flask.
Capacity, O.D., I.D., Height, Bottom Center Order
mL mm mm mm (A) Outlet, mm Neck Side Necks Code Each A
500 110 96 100 0-8 #25 (1) #7; (3) #15 6437-07 589.48
1000 110 96 180 0-8 #25 (1) #7; (3) #15 6437-13 615.91
2000 140 126 180 0-8 #25 (1) #7; (3) #15 6437-16 700.32
3000 165 151 185 0-10 #25 (1) #7; (4) #15 6437-20 760.35
5000 165 151 310 0-10 #25 (1) #7; (4) #15 6437-24 843.32
6437
†
6438 FLASK Pressure Reaction, J acketed 6438

Heavy wall reaction flask with jacket, part of the one-piece pressure reactor, for use at
elevated pressures*. With vertical† Ace‑Thred necks for positive connection of stirrer,
funnel, thermowell, condenser, etc. Cooling/heating jacket is heat sealed. Inlet/outlet on
jacket has easy connect/disconnect size 28/15 o‑ring ball joints with size –116 FETFE
o-rings, 7855-726.
Capacity, O.D., I.D., Height, Center Order
mL mm mm mm (A) Neck Side Necks Code Each
500 140 96 108 #25 (1) #7; (3) #15 6438-14 1106.92
1000 150 96 195 #25 (1) #7; (3) #15 6438-17 1152.67
2000 180 126 195 #25 (1) #7; (3) #15 6438-19 1259.39 A
3000 215 151 205 #25 (1) #7; (4) #15 6438-24 3090.02
5000 215 151 325 #25 (1) #7; (4) #15 6438-29 3266.12
†
6439 FLASK Pressure Reaction, Jacketed, with Bottom Outlet

Heavy wall reaction flask with jacket, part of the one-piece pressure reactor, for use at
elevated pressures*. With vertical† Ace‑Thred necks for positive connection of stirrer,
funnel, thermowell, condenser, etc. Cooling/heating jacket is heat sealed. Inlet/outlet
on jacket has easy connect/disconnect size 28/15 o‑ring ball joints. Bottom outlet is a
28/15 o‑ring ball joint (with size –116 FETFE o-rings, 7855-726) and a threaded valve for
retrieving contents of flask.
Capacity, O.D., I.D., Height, Center Bottom Order A
mL mm mm mm (A) Neck Side Necks Outlet, mm Code Each
500 130 96 108 #25 (1) #7; (3) #15 0-8 6439-15 1198.32
1000 150 96 195 #25 (1) #7; (3) #15 0-8 6439-21 1251.81
2000 180 126 195 #25 (1) #7; (3) #15 0-8 6439-25 1375.16
3000 215 151 205 #25 (1) #7; (4) #15 0-10 6439-29 3243.02
6439
5000 215 151 325 #25 (1) #7; (4) #15 0-10 6439-34 3583.92
†


7701 MOISTURE TEST RECEIVER Pressure

Used to determine heavier-than-water, co-distilling solvent component content of reaction
mixture. For use with ACE pressure reactors with #15 Ace‑Thred. Side arm is connected to
#15 Ace‑Thred on pressure reactor head with 7506 bushing and size –110 FETFE o‑ring,
7855-716. The 6024-20 pressure condenser, with #15 top plug, is attached to #15 thread
at top of receiver with bushing and o‑ring. Receiver capacity is 60mL, graduated in 1mL
subdivisions. Bottom outlet stopcock is a 0-3mm with FETFE o‑rings. Pressure rating,
45 psig @100°C. Complete consists of receiver and bushing with o‑ring. Condenser and
#15 Plug NOT supplied — order separately.
7701-20
Order Code Each
Receiver, only, 60 mL, #15 7701-04 585.23
Bushing, Nylon, #15, w/FETFE o‑ring (2) 7506-06 12.35
Complete 7701-20 609.93
7506 BUSHING Nylon or PTFE

B Used with o‑ring and Ace‑Thred to make a compression seal between thread and glass
like 6024 condenser or 7299 funnel. Supplied with one 7855-716 size –110 FETFE o‑ring.
7506 NYLON PTFE
Ace‑Thred I.D.
Size (B), mm Order Code Each Order Code Each
15 14 7506-06 12.35 7506-27 40.65
5844 ADAPTER Swagelok, PTFE

PTFE adapter with male Ace‑Thred to NPT female for connecting pressure gauge,
pressure relief valve or connection from pressure tank to Ace‑Thred on head of pressure
reactor Supplied with one FETFE o‑ring (see size and Order Code below) except -176.
NPT Thread O-Ring Size/
Ace‑Thred Size Size (In.) Order Code Order Code Each
7 1/8 –009 / 7855-707 5844-58 40.02
15 1/8 –110 / 7855-716 5844-62 67.75
5844 15 1/4 –110 / 7855-716 5844-74 67.75
25 (w/o o‑ring) 1/4 — 5844-176 88.93
5846 PLUG Nylon or PTFE

Solid plug for sealing top of 6024 condenser or Ace‑Threds on 6433 head. Supplied with
one FETFE o‑ring (see size and Order Code below).
NYLON PTFE
Ace‑Thred O-Ring Size/
Size Order Code Order Code Each Order Code Each
7 –009 / 7855-707 5846-04 9.21 5846-44 22.15
15 –110 / 7855-716 5846-12 21.56 5846-48 38.41
5846 25 –212 / 7855-734 5846-16 36.14 5846-50 59.54
12681 TUBING Polypropylene
Polypropylene tubing used to make connection between pressure source and 12517
quick disconnect on side of pressure manifold and between other side of manifold the 12681
pressure reactor.
Size (Inches) Quanity Order Code Each

1/4 O.D. x 0.170 I.D. 100-foot box 12681-10 45.20
1/4 O.D. x 0.170 I.D. 10-foot length 12861-110 13.22
3/8 O.D. x 75mm length Pkg. of 12 lengths 12861-812 28.38
8767 VALVE Pressure Relief, Adjustable

The primary protection to personnel and equipment involved with static and dynamic
pressurized systems. This one-piece pressure relief valve is adjustable from 3 to 50
psig (for use with ACE pressure reactors) by simply adjusting set screws to desired
8767
cracking pressure. When pressure exceeds set cracking pressure, valve bleeds; when
safe lower pressure is realized, valve will reseal. Fabricated from 316 stainless steel
with a Viton o‑ring. Ends are 1/4-inch MPT for connecting to Ace‑Thred with a 5844
adapter. Combining this valve with the 6445 rupture disc in the same pressure manifold
offers fail-safe protection against runaway pressure situations.
Order Code Each

8767-20 86.02
6444 SPARGER TUBE for Pressure Reactor, PTFE

Sparger tube for use in #15 Ace‑Thred with either one- or two-piece reactors. Consists
of a closed bottom, 1/2-inch O.D. tube with a 1/8-inch I.D. bore. Bottom of tube has two
3/64‑inch holes, 90° apart; top has a 5/16-inch male thread for connecting to bottom
of #15 adapter. Adapter has a female thread in handle for tubing connection. Simply
thread tube into bottom of #15 adapter. Thread into #15 Ace‑Thred on reactor. Attach 6444
appropriate size tubing to top of adapter. Adapter and tube are fabricated from PTFE.
o‑ring on adapter is FETFE. For replacement FETFE o‑rings, order 7855-716. Order tube
and adapter separately.
TUBE ONLY ADAPTER ONLY

Tube Length, Thread Size,
mm (in.) Order Code Each Top of Adapter Order Code Each
140 (5.5) 6444-04 156.95 1/4-in.-28 UNF 6444-30 56.19
190 (7.5) 6444-09 156.95 1/4-in. NPT 6444-38 56.19
343 (13.5) 6444-16 156.95
6445 RUPTURE DISC Pressure, Graphite Installation

Direction
For use in 6448 pressure manifold, these rupture discs provide extra protection to
personnel and equipment involved with static and dynamic pressurized systems. In
the event of an overpressure — one that cannot be handled by the 8767-20 pressure
relief valve — this disc will rupture at a predetermined burst rating; 55 psig (±3 psig)
for two-piece units, 65 psig (±3 psig) for one-piece units. Manufactured from a single
Disc
piece of a high-purity carbon, these discs have a PTFE coating on underside, are
tamper-proof, have no springs or moving parts and mount directly in a #25 Ace‑Thred.
Simply place the FETFE o‑ring (7855-734) supplied with disc, on the underside to make O‑Ring
6445
the seal, drop into the #25 Ace‑Thred and hold in place using a 5844-176 adapter.
Disc Burst Pressure Use With Order Code Each

55 psig TWO-PIECE Reactor 6445-12 133.39 Flow
Direction
65 psig ONE-PIECE Reactor 6445-41 133.39

13385-44
5844-176
8767-20 6448 MANIFOLD Pressure, Epoxy Coated
Complete glass manifold, fitted with a pressure gauge, primary
adjustable pressure relief valve, and secondary rupture disc to allow
5844-62 5844-74
for safer operation of pressure and filter reactors.
12517-14 5844-74 13385 Pressure Gauge is a 0-60 psi stainless steel internal, with
5844-74
1-1/2‑inch face and 1/8-inch npt male connection for use with
5844-74 adapter in #15 Ace‑Thred.
8767 Pressure Relief Valve is adjustable from 3-50 psig by adjusting
6448-24 6445-12 set screws to desired cracking pressure. Ends are 1/4-inch npt for
connecting to #15 Ace‑Thred on manifold with 5844-74 adapter.
To 5844-58 #7 Ace‑Thred and 12517-08, -40
6445 Rupture Disc is a secondary safety device that, in the event of an overpressure (one that cannot be handled by the 8767
relief valve) will rupture at a predetermined burst rating; 55 psig (±3 psig) for -12 version, 65 psig (±3 psig) for -41 version. Disc is
manufactured from high-purity carbon with a PTFE coating on the underside. No springs or moving parts, disc is secured directly
in #25 Ace‑Thred of manifold with 5844‑176 adapter.
Manifold is connected to #7 Ace‑Thred on 6433 head using 5844‑58 adapter and 12517 tubing connectors with 1/4‑inch tubing.
For Two-Piece For One-Piece

Pressure Reactors (55 Pressure R eactors
psig) and Filter Reactors (65 psig)
Adapter, PTFE, #15–1/4-inch NPT (3) 5844-74 67.75 5844-74 67.75
Adapter, PTFE, #25–1/4-inch NPT, w/o o‑ring 5844-176 88.93 5844-176 88.93
Rupture Disc, Graphite, 55 psig 6445-12 133.39
Rupture Disc, Graphite, 65 psig (for pressure version only) 6445-41 133.39
Manifold, Glass, (4) #15, (1) #25, Epoxy Coated 6448-24 197.03 6448-24 197.03
Valve, Pressure Relief, 1/4-inch NPT, 3–50 psig 8767-20 86.02 8767-20 86.02
Coupling Insert, for 1/4-inch O.D. tubing (2) 12517-40 12.25 12517-40 12.25
Tubing, PP, 1/4-inch O.D. x .170-inch I.D., 10 feet 12681-110 13.22 12681-110 13.22
Gauge, Pressure, 0–60 psi, 1/8-inch MPT 13385-44 171.92 13385-44 171.92
Complete 6448-54* 989.82 6448-68** 989.82
Replacement o-rings
*6448-54 is for use with two-piece pressure and filter style reactors.
**6448-68 is for use with one-piece pressure reactors only.
12517 TUBING CONNECTOR Quick Connect/Disconnect

Tubing
Connection 12517 Two-piece tubing connector, used to connect tubing from a pressure source to the
manifold of the ACE pressure reactor. Offers the convenience of a quick connect/
Coupling
disconnect coupling. Body has MPT thread for connecting to a 5844 adapter at end of
Insert ACE pressure manifold. Coupling insert is connected to tubing from pressure source.
Push coupling insert into coupling body for leak-tight connection; press thumb latch
to quick disconnect. Fabricated of polypropylene. Order body and insert separately.
Order Code Each

Coupling
Body
Coupling Body, 1/8-inch MPT 12517-08 11.42
Coupling Body, 1/4-inch MPT 12517-14 12.07
Coupling Insert, for 1/4-inch OD x 0.170 ID Tubing 12517-40 12.25
13270 SAFETY SHIELD Self Supporting

Weighted, all-transparent safety shield for laboratory worker protection. Polycarbonate
shield is 4.7mm (3/16-inch) thick. Three-sided construction provides stability and
protects personnel from front and sides. Heavy steel perimeter base is 25mm x 48mm 13270
(1-inch x 1-1/2-inch), coated with green epoxy. Outside width is 50cm (19-1/2-inch),
17cm (6‑1/2-inch) front to back.
Height, cm Weight, Kg Order Code Each

76 8.4 (18.5 lbs) 13270-07 430.20
91 8.9 (19.6 lbs) 13270-10 476.70
9655 REACTION FLASK Instatherm® Heated, Schott-Duran Flange

Rugged cylindrical reaction flask with Schott-Duran, flat, ground 4-inch flange with
o‑ring groove for use with 6517-25 quick release clamp and integral heating element
that eliminates the local superheating commonly associated with more conventional
heating methods and eliminates cumbersome oil baths. The heating response is rapid
and accurate. Supplied with silicone coating for insulation and protection. O-Ring
(supplied with flask) is CAPFE (PTFE encapsulated silicone). Flask is coated to within
approximately 38mm of the flange for 250°C operation. Interchangeable with ACE A
4-inch reactor heads with Schott-Duran flange. Three-pronged plug for insertion into
ACE temperature controllers. Integral six-foot controller cord.
Capacity, O.D., I.D., Height, Volt/Amp Order
Liters mm mm mm (A) Rating Watts Code Each
1 110 100 180 40/8 400 9655-17 766.76
2 110 100 200 120/5 600 9655-22 869.89 9655
9656 REACTION FLASK Instatherm® Heated, Conical, 4-Inch Flange

Same flask as listed under 6476, except with Instatherm coating. Has flat-ground, 4-inch
conical flange. This integral heating element eliminates the local super-heating commonly
associated with more conventional heating methods. Eliminates cumbersome and
dangerous oil baths. The heating response is rapid and accurate. Supplied with 9698-
20 cord for connection to variable voltage or termperature controller. Flask is coated
to within 38mm of the flange for 200ºC operation, 360°C maximum on special order.
Interchangeable with ACE 4-inch reactor heads with Schott-Duran flange. For controllers, A
see ACE or J-Kem temperature controllers with voltage limiting output, such as 12125,
12324. Use 6496 clamp for securing head to flask.
1 110 100 180 40/8 400 9656-08 758.58
2 114 104 260 120/5 500 9656-12 864.03 9656
6526 FLASK Reaction, Cylindrical, Indented Style

Rugged cylindrical reaction flask with Schott-Duran flat flange with o‑ring groove, for
use with 6517 quick release clamp but with indents for greater agitation. Each flask
is supplied with one CAPFE o‑ring (PTFE encapsulated silicone o‑ring). Plain silicone
o‑rings are also available. For reaction heads, see 6528. For cooling/heating coils, see
12067. NOT suitable for vacuum or pressure operation. Uses 6517 quick release clamp. 6526
Capacity, O.D., I.D., Height, Flange Size. Top Order
Liters mm mm mm (A) mm (in.) O‑Ring Code Each A
1 110 100 180 100 (4) 7855-880 6526-10 200.17
2 110 100 265 100 (4) 7855-880 6526-12 223.10
ted
Inden
New

8044 BEARING Pressure, with Ace‑Threds, 1 0mm

8044-24 8044-55 Glass bearing with #15 Ace‑Thred at each end and glass tubing between for use
with 10mm O.D. 8075 stirring shafts. PTFE coupling, with internal FETFE o‑ring seal,
connects bottom of bearing to either #15 or #25 Ace‑Thred on vessels such as 6433
pressure reactor head or one-piece pressure reactors. Top bushing also has an internal
o‑ring seal for additional seal on shaft to allow pressure reactions. Maximum operating
speed 600 rpm. Coupling and bushing supplied with o‑rings. For replacement o‑rings
(the bearings take two o-rings, one internal and one external): for #15–#15 coupling,
7855‑730 external, 7855-716 internal; for #15–#25 coupling, 7855-730 and 7855-742
external, 7855-716 internal; for #15 bushing, 7855-730 external, 7855-716 internal.
For Coupling to #15 Ace‑Thred For Coupling to #25 Ace‑Thred
Order Order
Code Each Code Each
Glass Bearing, only, #15-#15 8044-07 39.14 Glass Bearing, only, #15-#15 8044-07 39.14
Coupling, PTFE, #15-#15 5840-60 113.73 Coupling, PTFE, #15-#25 5843-62 128.31
Bushing, PTFE, #15 8044-13 80.21 Bushing, PTFE, #15 8044-13 80.21
Complete 8044-24 233.08 Complete 8044-55 247.66
5848 FILTER DISC

5848
Filter disc for use with 5837 and 5838 adapters. Available in polyethylene (100 micron
pore size), and borosilicate glass — Porosity A (145-174 microns), B (70-100 microns),
C (25-50 microns) and D (10-20 microns). Sold in packages. (Caution: These discs are
intended to be removable. However, because of the tight fit, the glass disc may break
when being removed.)
Polyethylene Borosilicate Glass

Porosity A Porosity B Porosity C Porosity D
100 microns 145-174 microns 70-100 microns 25-50 microns 10-20 microns
For
Adapter Pkg. Order Per. Order Per Order Per Order Per Order Per
Size,mm Qty. Code Pkg. Code Pkg. Code Pkg. Code Pkg. Code Pkg.
11 6 5848-07 14.44 5848-43 58.53 5848-52 58.53 5848-21 58.53 5848-31 58.53
15 6 5848-10 14.44 5848-44 58.53 5848-54 58.53 5848-23 58.53 5848-33 58.53
25 6 5848-14 16.58 5848-47 66.12 5848-56 66.12 5848-25 66.12 5848-35 66.12
50 6 5848-17 34.99 5848-49 130.80 5848-58 130.80 5848-28 130.80 5848-38 130.80
80 1 5848-19 9.03 5848-100 126.50 5848-120 129.55 5848-122 147.23 5848-124 161.95
5021 ADAPTER Bushing, Thermometer

For thermometers having a  10/30 joint.
Inner Outer Order Code Each

10/30 14/35 5021-05 36.10
5021 10/30 24/40 5021-09 41.53
10/30 29/42 5021-12 45.16
5028 ADAPTER Thermometer, “Mini” #7 Ace‑Thred

With ground joint at bottom and threaded bushing at top which tightens into #7 Ace‑Thred
to form an o‑ring compression seal with thermometers, bleed tubes, etc. Nylon bushing
comes complete with FETFE o‑ring.  10/18 size will accommodate thermometers up
to 6.5mm diameter, all others will accommodate 7mm diameters. Suitable for vacuum
work. Supplied complete with 5029-10 nylon bushing. For extra o‑rings, see 7855-704.
Joint Order Code Each Joint Order Code Each

10/18 5028-24 27.51 24/20 5028-30 27.61
14/20 5028-26 27.55 29/42 5028-32 32.61
19/22 5028-28 27.38 18/9 5028-38 33.42
24/40 5028-30 27.61 35/25 5028-42 35.95
5028
5269 ADAPTER Offset, with Ace‑Thred

Offset adapter with #15 Ace‑Thred offset to a 14mm OD tube with o‑ring groove. For use
with ACE pressure reactors to locate condenser, etc., away from stirrer. NOT supplied
with bushing or o‑ring. Order 7506-06 for bushing and FETFE o‑ring.
Order Code Each

5269-12 39.20
5269
6024/6029 CONDENSER West
6029
West style condenser for use with 6433 threaded or 6527, 6528 or 6529 jointed heads.
6024-20 supplied with #15 Ace‑Thred at top for 5846 plug (not supplied) and drip stem
with groove, and long enough to be secured in #15 Ace‑Thred with 7506-06 bushing
and FETFE o‑ring (not supplied) to restrict blowout. With #7 Ace‑Thred on inlet/outlet
for use with “Ace-Safe” 5853 tubing connectors. Supplied with bushing and connectors
for 1/4‑inch I.D. tubing.
6029-13 supplied with  24/40 joint at top and bottom and D size (see page 5 for sizing)
barbed hose connection on inlet/outlet for ¼‑inch I.D. tubing.
Use with Head No. Jacket Length, mm Order Code Each

6433 200 6024-20 129.75 6024
6527,6528,6529 250 6029-13 105.87
7234 FUNNEL Powder Dispensing

Side operated screw feed funnel for addition of powders and solids, up to 25 mesh, to
reactions without problems of seizing or binding.
Features a flexible PTFE screw thread wrapped on a precision PTFE-ceramic shaft and
contained within a precision bore housing. This offers a unique flexibility in that the thread
can move aside temporarily; as one spacing increases, the adjacent spacing decreases,
thereby maintaining an average feed rate.
Completely inert materials allow flushing with solvents without fear of contamination.
#15 Ace‑Thred offers easy disassembly for cleaning. Large 1¼‑inch knob makes turning
smooth and easy. Top outer and bottom inner joints are S
T 24/40. S
T 14/20 outer joint atop
inner joint is for easier flushing.
Capacity, mL Order Code Each 7234

100 7234-25 331.84
250 7234-35 358.50

7298/7299 FUNNEL Addition, Pressure Equalizing

Funnel for use with 6433 threaded or 6527, 6528 or 6529 jointed heads.
7298 7298 (use with 6527,6528, or 6529 head) supplied  24/40 joint at top and bottom, with
threaded PTFE stopcock shutoff.
7299 (use with 6433 head) supplied with #15 Ace‑Thred at top for 5846 plug (not
supplied) and drip stem with groove and long enough to be secured in a #15 Ace‑Thred
with 7506-06 bushing and FETFE o‑ring (not supplied) to restrict blowout. With threaded
PTFE stopcock shutoff.
Replacement Plugs
Stopcock
Cap., Orifice, Order Order Order
mL mm Code Each Code Each For 7298 Code Each
7299 60 0-3 — 7299-06 305.29 0-3 mm 8192-261 37.87
125 0-3 7298-05 231.90 7299-12 313.29 0-5 mm 8192-263 52.16
250 0-3 7298-10 249.35 7299-25 336.29
500 0-3 7298-15 278.92 7299-34 367.99 For 7299
1000 0-5 7298-24 326.09 — 0-3 mm 8189-43 38.16
7233 FUNNEL Powder Dispensing, Vertical

A vertical, compact, screw feed funnel for addition of powders and solids, up to 25
mesh, into reactions without seizing or binding. Features a flexible PTFE screw thread
wrapped on a precision PTFE-ceramic shaft and contained within a precision bore
housing. This offers a unique flexibility in that the thread can move aside temporarily;
as one spacing increases, the adjacent spacing decreases, thereby maintaining an
average feed rate. Completely inert materials allow flushing with solvents without fear
of contamination. #15 Ace‑Thred at top offers easy disassembly for cleaning. Large
7233 1¼‑inch knob makes turning smooth and easy. Top side port is S T 14/20 outer joint,
bottom inner joint is S
T 24/40. Overall height, 9½ inches.
Capacity, mL Order Code Each

50 7233-20 250.88
100 7233-30 282.08

A vertical, compact, screw feed funnel for addition of powders and solids, up to 25 mesh,
into reactions without seizing or binding. Features a flexible PTFE screw thread wrapped
on a precision PTFE-ceramic shaft and contained within a precision bore housing. This
offers a unique flexibility in that the thread can move aside temporarily; as one spacing
increases, the adjacent spacing decreases, thereby maintaining an average feed rate.
Completely inert materials allow flushing with solvents without fear of contamination. #7
Ace‑Thred offers easy disassembly for cleaning. Top outer and bottom inner joints are S
T 14/20.
Approximate capacity, 15mL.
Order Code Each

9485-15 238.41
9485
6517 CLAMP Quick Release

Stainless steel quick release clamp for use with two-piece pressure reaction flasks
and heads with Schott-Duran flanges. Available with or without extension rod for
clamping to support frame. Note: Welded extension rod is 5/8‑inch O.D. x 12 inches
long for stabilizing reactor only. Reactors should be supported from below in usual
manner, namely cork rings, mantle, etc.
6517-22, -25, -27
WITHOUT EXTENSION WITH EXTENSION
For Flange
Size, mm (in.) Order Code Each Order Code Each
60 (2.5) 6517-22 87.08 —
100 (4) 6517-25 98.23 6517-54 158.10
150 (6) 6517-27 117.67 6517-56 172.33
6517-54, -56
7669 CLAMP Pinch Type, Stainless Steel

Spherical joint clamps made of stainless steel. With strong spring-closed, forked jaws.
Size For Order Size For Order
No. Joint Code Each No. Joint Code Each
12 12/5 7669-03 7.79 40 7669-16 41.45 7669
18/9 7669-05 8.64 50 50/30 7669-18 32.03
12/5 7669-08 14.30 65 65/40 7669-20 35.90
18 18/9 7669-10 14.33 75 75/50 7669-22 72.92
28 28/15 7669-12 16.57 100 102/75 7669-26 246.61
35 35/25 7669-14 18.51
13550 SUPPORT STAND/CLAMP HOLDER

Stand: Rugged, with “H” shaped base for use with filter reaction flasks. Stainless steel
vertical rod available 25mm O.D. x 70cm (27 inches) long; 25mm O.D. x 92cm (36 inches);
or 25mm O.D. x 122cm (48 inches). Base is 17 inches wide x 16 inches deep. Clamp
Holder: For connecting up to 13mm O.D. mounting rod to 25mm O.D. support rod.
Order Order 13550
Code Each Code Each
Stand, only, 25mm O.D. x 70cm 13550-21 305.91 Clamp Holder, only 13550-25 139.05
Stand, only, 25mm O.D. x 92cm 13550-23 314.96
Stand, only, 25mm O.D. x 122cm 13550-24 314.96
11079 CHAIN CLAMP

Use code -24, for connecting up to 170mm O.D. vessels. Code -38 & -40, for connecting
up to 280mm O.D. vessels. Code -40 has extended 12-inch (305mm) arm.
For Vessel O.D. Order Code Each

Up to 170 mm 11079-24 51.23
Up to 280 mm 11079-38 75.28
11079
Up to 280 mm (with 12-inch extension arm) 11079-40 79.46
11080 CLAMP HOLDER Regular 11080

Normally used to hold the Nos. 11065 through 11072 clamps to rods and lab frame
supports. Made of heavily nickel-plated zinc. Will grip rods up to and including 19mm
diameter. Attaches clamp at right angle.
Order Code Each

11080-19 18.82

12840 BENCH REACTOR STAND
Ace Glass is pleased to introduce a new bench

reactor stand assembly to accommodate all types
of glass bench filter and pressure reactors. The
stand is compatible with reactors from 1-Liter up to
6-Liters having overhead drive motors, and in both
jacketed and non-jacketed flask versions. The bottom
plate, motor mount and middle flask supports are all
adjustable to fit any small reactor, and the stand will
New fit into most laboratory hoods. It comes completely
assembled, but it is very easy to take apart for
cleaning. The open bottom accommodates round-
bottom and flat-bottom flasks, and even flasks with
bottom valves. Will accept either IKA or Heidolph
overhead stir motors. All stand components are
either anodized or powder coated aluminum. The
flasks sit on an attached rubber base plate.
12840
Dimensions, Inches Order Code Each

43 H x 24 W x 24 D 12840-10 2665.13
13586 SUPPORT STAND

All-stainless-steel support stand. Heavy base, six pounds, can accommodate vessels
up to 18 inches in diameter within its “U” shape. Support rod is 5/8-inch diameter,
approximately 29 or 36 inches high, fastened to base with stainless steel lock nuts. Two
additional threaded holes in base legs to accommodate extra support rods. Complete
item consists of one base and one rod. For extra rods, order 29 inch, 13586-25; 36 inch,
13586-27. Base is 19 inches wide by 11 inches deep.
13586
Rod Height, in Order Code Each
29 13586-10 274.82
36 13586-13 313.93
Additional Support Rods:
28 13586-25 104.64
36 13586-27 133.18
60 13586-15 181.78
11086 New 11086 CLAMP HOLDER 13mm Grip, Stainless Steel

Lab frame hook connector allow one-handed assembly of two components with one
adjustment screw.
Order Code Each

11086-01 27.18
11173 PLATE SUPPORT SHELF

Adjustable cast alloy, black epoxy coated support shelf. With knob, measures 7 inches
x 10 inches. Fits up to 5/8-inch O.D. rod. Plain or with 4‑inch diameter hole and with
1‑inch rubber around perimeter.
Style/Size Order Code Each

Solid, No Hole 11173-08 111.57
11173-17
4-inch Hole 11173-17 111.28
11057 CLAMP Stainless Steel, Three-Prong 11057

Multi-purpose, three-prong clamps manufactured from electropolished stainless steel
for improved corrosion resistance and autoclave sterilization. Features include dual
screw adjustments and vinyl sleeved prongs. See our 11074 product family for vinyl
or fiberglass (high temperature) replacement sleeves. See our 11083 & 11086 product
families for stainless clamp holders.
Maximum
Size Grip Size (cm) Arm Length (in.) Order Code Each
Small 4.8 4 11057-01 70.05
Medium 6.9 5 11057-03 80.51
Large 10.2 5 11057-05 89.91
11065/11067/11069 CLAMP Versatile, Vinylized Jaws

Three-prong grip clamp. Because both jaws are adjustable, with double screws that
operate independently, large or small objects can be held easily. Comes with an extra
set of fiberglass prong covers for temperatures above 100°C.
Clamp Overall Will Hold Objects
Size Length, cm up to mm diameter Order Code Each
Large 27 89 11065-16 41.82 11065/67/69
Large 30 89 11065-17 51.23
Medium 22 57 11067-14 39.73
Small 17 25 11069-18 37.64
11066 CLAMP Versatile, Vinylized Jaws New

Three-prong grip clamp. Because both jaws are adjustable, with double screws that
operate independently, large or small objects can be held easily. Comes with an extra
set of fiberglass prong covers for temperatures above 100°C. Has 12-inch (305mm)
extended arm.
Clamp Overall Will Hold Objects
Size Length, cm up to mm diameter Order Code Each 11066
Medium 40.6 69 11066-10 Call
Large 45.1 105 11066-12 Call
11081 CLAMP HOLDER Pilot Plant

11081
Used with 11065 versatile jaw-type clamp to secure condenser, etc., on 6472 pilot plant
reactor support frame. Holder clamps to 1-inch bar on frame of reactor; 11065 clamp
is held in clamp holder with thumb screw. Fabricated of aluminum, painted black. For
clamps, see 11065.
Order Code Each

11081-21 84.80

54 Bench Reactor — ROBO
ROBO
INTRODUCING…
ROMASZEWSKI OIL BENCH OXIDATION

Reactor and Components for ASTM D7528-09 procedure for
simulation and test of auto engine oils
A
ll new components and reactor for testing
and simulation of automobile engine oil
aging as per ASTM D7320 sequence
IIIG method.
T h i s p ro c e d u re w a s d e v e l o p e d b y R .
omaszewski, B. Kinker and P. Palmer of
R
Evonik (RohMax) USA.
Before auto engine oils are made available for
the global market for use in auto engines, they
must pass rigorous testing and meet tough
specifications for performance. ASTM and the
International Lubricant Standardization and
Approval Committee, (ILSAC) set the standards
for US and Japanese auto manufacturers. This
revised, updated method is part of D7320 IIIG
engine oil test method. The new revised method
reduces the costs and test times substantially
from the old method.
Ace Glass is pleased to be part of this effort and
this new protocol. Our proprietary Instatherm ®
coating on the flask body allows for very
precise control of the heating in one complete
vessel. ACE offers all the glass and stainless
steel components, as well as accessories for
the reactor system with the appropriate part
numbers from the ASTM D7528-09 document.
Components: Order Code Each

1000mL Instatherm® flask D120676 Call
Dual chamber trap/condenser D127507 Call
Inner condenser (two required) D127590 Call
12mL “V” bottom tube with side tab D120677 Call
New
Stainless steel head RMI-1002-DH Call
Bearing RMI-1004-DH Call
Squash cap RMI-1005-DH Call
Stainless steel shaft, 8mm RMI-1003-DH Call
Stainless steel turbine blade RMI-1001-DH Call
ACE clamp D124780 Call
Accessories:
PTFE ring seal RMI-1007-DH Call
Head gasket 6495-43 19.53 Stainless steel extension arms for head
Rack assembly 11162-08 500.80 (two required, not needed if using D124780 RMI-1006-DH Call
Gas drying tube 10165-10 106.81 clamp)
Heidolph RZR motor 13507-51 2363.71 Water flow monitor (J-Kem) 12168-120 354.20
Stainless steel fittings, tubing 6650-10 Call Valve for WFM (J-Kem) 12168-03 240.00
Stainless steel valves 6650-20 Call Temperature controller with “J” thermo-
12324-25 823.40
Stainless steel vacuum/pressure gauge 6650-30 Call couple Model 410 (J-Kem)
Flow Meter 6650-40 Call Vacuum regulator (J-Kem) 14061-08 1127.00
Complete 6650-01 Call Vacuum regulator valve 14066-01 485.00
Bench Reactor — PTFE 55
6390 REACTOR PTFE, Filter, Complete

All PTFE filter reactor. An extension of the famous ACE borosilicate glass filter reactor
product line. The head, head joints, body, stir-bearing, bottom filter assembly with valve,
and stir shaft with agitator are all PTFE. Even the o-rings are PTFE encapsulated. The filter
New
supports are polypropylene. The bottom filter assembly is either #50 or #80 Ace‑Thred
and threads in/out for easy capture of filtrate, or for cleaning. Unit is excellent for fluorine
chemistry work as well as any work using strong alkalis where glass can’t be used. Halar
coated stainless steel internal coil can be used for heating or cooling the contents. Three
sizes are available as standard. Other sizes are available on request. Support stand
(13586 or 13550-21) and chain clamp (11079) not included. We recommend Caframo
BDC2010 stir‑motor (13566-05). Recommend Julabo circulator (12254-33) for heating/
cooling and Ace/J‑Kem 260T temperature controller (12318-05) with a 12-inch PTFE 6390
coated “T” temperature sensor (12318‑25).
250mL Reactor
Component Order Code Each
Reactor Body (A = 5.8 in.; O.D. = 3.5 in.) 6391-02 1184.49
PTFE Head (60mm, 4 openings, 24/40) 12858-15 193.24
CAPFE o-ring (60mm) 7855-878 28.10
Quick Release Clamp (60mm) 6517-22 87.08
Bottom Filter Assembly (#50) 5838-83 232.72
Bottom Valve (1/4-inch/3/8-inch) 5839-42 110.20
Adapter 5844-120 88.91
Polypropylene Filter Supports (#50) (Pkg. of 12) 5814-348 35.76
Stirrer Bearing (10mm) 13443-12 428.93
PTFE Coated Stainless Steel Shaft
13852-10 335.81
with Agitator (10mm)
Complete 6390-02 2874.94
500mL Reactor
PTFE Head (60mm, 4 openings, 24/40) 12858-15 193.24
CAPFE o-ring (60mm) 7855-878 28.10
Adapter 5844-120 88.91
13852-10 335.81 A
Complete 6390-05 3133.48
1,000mL Reactor
PTFE Head (100mm, 7 openings, 5x24/40, 2x#7) 12860-12 348.95
CAPFE o-ring (100mm) 7855-880 28.63
Adapter 5844-120 88.91
13852-15 335.81
Halar Coated Heating Coil 12069-06 835.14
Complete 6390-10 4809.74

56 Reactors/Large-Scale Pilot Plants
ACE Pilot Plant Reactors

ACE cylindrical and spherical pilot plant reactors have been field tested and improved to
provide a portable, self-contained reaction system for research and production purposes.
Standard Design Specifications:

■■ Complete listing of domed as well as flat head reactor assemblies.
■■ Cylindrical, jacketed, and spherical type flasks.
■■ Various bottom outlet valve versions available.
■■ Stainless steel support frame with reactor support platform/ring, and stirring m
otor
mount.
■■ Three-point adjustable top bracing system that provides greater stability
of flask and head on four-post stands.
■■ Large, locking wheels on support frame for easier movement and greater stability.
■■ Unique design for securing bottom and upper agitators on shaft.
■■ New pinned valve/agitator assemblies for reduced vibration/flexing.
■■ Digital temperature control systems for added safety.
■■ Numerous stirring motor types
■■ Clear safety shields for support frame available, call or email for details.
LIMITATIONS MAXIMUM ALLOWABLE MAXIMUM PRESSURE

AND PRECAUTIONS TEMPERATURES Maximum pressure for reactors is 5 psi
The strength of glass is primarily The standard reactors have a maximum with standard taper joints (domed head)
determined by its surface condition, operating temperature of 160°C. The using clips. Flat head NOT recommended
thickness, and uniformity. Mechanical maximum allowable temperature difference for use with pressure.
stress applied to glass contributes to (∆T) across the glass wall for units with
strain, which results in breakage when the domed head is 80°C; 30°C for flat head. MAXIMUM VACUUM
total strain exceeds its allowable limit (i.e., Also, these values limit the rate at
tensile strength). Thus, careful handling which a reactor may heat up or cool Maximum permissible operating vacuum
and use of glassware are important to down. ACE recommends continuous for spherical and cylindrical vessels with
avoid scratching and mechanical shock monitoring of internal and external 50°C max. ∆T:
to outside and inside surfaces. temperatures to avoid exceeding 10 liter = “Full” Vacuum (i.e., 5 mm Hg)
Thermal stress may produce the allowable temperature differences.
same result — catastrophic breakage.
It is important to avoid rapid or uneven
Caution must be used when heating a
reactor vessel with mantles since they
30 & 50 liter Cylindrical
}
50, 72 & 100 liter Spherical
50mm Hg
}
temperature changes across any glass produce local temperatures in excess 100 & 200 liter Cylindrical
wall. This refers to temperature increases of 350°C. When using variable voltage 200mm Hg
200 liter Spherical
from externally applied heat (mantles) controllers, we suggest 3/4 voltage
or internally generated heat (exothermic (i.e., half power) during warm-up and Flat head NOT recommended
reactions), as well as temperature gradually increasing voltage until for use under vacuum.
decreases such as rapidly introducing large desired internal temperature is reached,
quantities of cold liquids to hot reactants, never exceeding the maximum ∆T.
etc. Remember: Mechanical and Thermal
Stresses are additive.
Reactors/Large-Scale Pilot Plants 57
A Guide to Ordering Custom Pilot Plants

It’s easy to customize one of our standard listings with a Pilot Plant Reactor
design that will meet your specific application needs. Here are some key points
to consider when specifying a Pilot Plant that will work for you:
Overall Height Limit

3- or 4-Post Stand Door or Hood Clearance
Motor Size & Type

• Air-Driven
Accessories • Electric
• Condensers • Digital
• Powder Funnel • Analog
• Liquid Addition Funnel
• Sample Ports Coupling
• Temperature Sensors
Temperature • Baffles
Bearing Type/Size
Controller
Needed? Addition or Sample Port
Head
Flat or Domed; number
of ports, sizes
Flask Type & Size
• Spherical
• Cylindrical
• Jacketed
• Unjacketed
Heating/Cooling Coil
Safety Shields
Heating/Cooling Circulator
needed?
If so, what capacity? Total Capacity
& Reaction
Heating Girdle/Mantle Volume
Bottom
Heating
Mantle
Jacketed or
Unjacketed
Flask
Agitators
Number & Type
Bottom Valve Type Pin or no pin
• Easy Action • Piston Type
Bottom • Sink Type • Beaded
Clearance • ZDS Valve • Flush Seal
Required

➧➧Complete 12 & 22 liter

➧➧Elevated mantle support
➧➧Temperature controlled heating mantle
➧➧Bottom outlet
6469 REACTION ASSEMBLY Complete, 12 and 22 Liter
Complete self-supporting pilot plant assembly. Needs only to be located near
electrical outlet. When not in use, entire assembly can be moved, intact, without
breakdown.
Features
• Flask with 4 inch (10.2 cm) center opening, • Flat-sided powder funnel offers easier
two   45/50 side necks, one #7 Ace‑Thred additions.
thermometer opening and one  28/15 • Rugged steel-reinforced PTFE stirring rod
ball joint take-off at bottom. needs no lubrication. Turns in a precision
• Electric stirring motor, Cat. No. 13649-07, Trubore® economy bearing. The PTFE
is self-standing on flask-mounted motor paddle agitator is removable for cleaning.
mount (air motor also available). • Mantle supports raise the mantle about
• With PID Digital readout temperature 91.4 cm (36 inches) to allow easy access
controller and PFA coated “J” thermo to bottom of flask.
probe for better temperature control. • Approximate overall height: 12 L and 22L,
• Bottom heating mantle 71 inches; Base width: 28 inches
12 Liter 22 Liter
FLASK, Center Neck 10.2cm
Flange, Two 45/50 Side Necks,
One #7 Ace‑Thred and One
28/15 Ball Outlet At Bottom 6469-16 763.28 6469-18 1062.02
6469 HEAD, 45/50 6469-26 199.64 6469-26 199.64

GASKET, PTFE 6495-10 11.28 6495-10 11.28
CHUCK, Flex-Grip 8124-10 43.92 8124-15 152.25
ROD, PTFE with Stainless Steel
Core 8071-07 264.62 8079-03 477.57
Flask with
or Zero D Sink Valve AGITATOR, PTFE Paddle 8089-08 112.73 8091-10 226.34
ead Spac
available e Va MOTOR, only 13649-07 509.07 13649-07 509.07
upon requ lve MOTOR MOUNT 6469-30 487.00 6469-32 487.00
est.
MOTOR CONTROLLER, only 13530-10 523.17 13530-10 523.17
BEARING, Economy, 45/50 8042-121 105.74 8065-64 169.59
CLAMP, Head, Aluminum 6468-13 503.79 6468-13 503.79
ADAPTER, Stopcock, 28/15,
Temperature range: PTFE, 6mm Bore
TEMPERATURE CONTROLLER
6469-40
12126-24
173.03
874.72
6469-40
12126-24
173.03
874.72
Ambient +5° to 200°C SENSOR, PFA Coated, 12 inch
x 1/4 inch 12141-25 118.70 12141-25 118.70
SENSOR LEAD, only, Type “J” 12141-80 69.68 12141-80 69.68
FUNNEL, Powder, 45/50 6469-52 228.81 6469-52 228.81
STOPPER, 45/50 8250-20 44.68 8250-20 44.68
ACE Reaction Assemblies are CLAMP, 28/15 7666-15 40.04 7666-15 40.04
available as listed. If you require a CLAMP Holder, Regular 11080-19 18.82 11080-19 18.82
design change or just a modification, MANTLE, Heating, with Hole 12044-28 1091.72 12044-30 1207.35
we’ll fabricate to order. MANTLE, Support 12097-45 467.00 12097-47 492.00
COMPLETE 6469-62 6358.09 6469-67 7248.21
Email, phone or fax for a quotation.
➧➧Full range of pilot size flasks

➧➧Rugged, steel-reinforced PTFE stirring rod
➧➧Heavy duty mechanical lab stirrer
➧➧Temperature controlled heating mantle
6470 REACTION ASSEMBLY 12 thru 72 Liter

Complete reaction assembly using standard ACE reaction equipment.
The 12 thru 72 liter flasks have three  65/40 in-line spherical joints
and two 29/42 standard taper joints.
Features
• Full range of pilot-size flasks from 12 liter to 72 liter with spherical
and standard taper joints.
• Rugged 19mm diameter, steel-reinforced PTFE stirring rod needs no
lubrication. Runs in a precision Trubore® bearing. The PTFE paddle is
removable and other interchangeable agitators, available from ACE,
may be substituted.
• The 12 liter assembly has a 10 mm diameter, steel-reinforced PTFE
rod as well as a 10 mm bearing, chuck, and paddle.
• Highly efficient 6016 condenser is attached directly to 65/40 side joint.
• Thermowell depth is completely adjustable via an Ace‑Thred adapter.
• Unit as supplied has a heavy-duty mechanical lab stirrer; for situations
that call for non-electric motors, ACE can supply a compact air-driven
motor and support. Call or email for a quotation.
• Heavy-duty bottom heating mantle.
• Approximate overall height: 12 L and 22L – 59 inches; 50 L and 6470
72L – 63 inches.
12 Liter 22 Liter 50 Liter 72 Liter
Order Order Order Order
Code Each Code Each Code Each Code Each
FLASK, Center and Two Side
65/40, Two 29/42 6470-20 892.05 6470-24 1034.76 6470-26 1673.33 6470-28 2162.67
CONDENSER, Pilot Plant 6016-75 972.51 6016-77 1048.01 6016-79 1328.76 6016-79 1328.76
BEARING, 65/40, Water-
Cooled 8040-55 217.99 8060-10 299.67 8060-10 299.67 8060-10 299.67
ROD, PTFE with SSteel Core 8071-10 267.94 8079-05 484.69 8079-10 528.19 8079-10 528.19
AGITATOR, PTFE, Single Blade 8088-10 222.39 8092-10 256.36 8092-10 256.36 8092-10 256.36
CHUCK, Flex-Grip 8124-10 43.92 8124-15 152.25 8124-15 152.25 8124-15 152.25
FUNNEL, Pressure Equalizing,
24/40, 1000 mL 7297-37 332.65 7297-37 332.65 7297-37 332.65 7297-37 332.65
STOPPER, 24/40 8250-12 19.79 8250-12 19.79 8250-12 19.79 8250-12 19.79
ADAPTER, 24/40 - 65/40 5025-24 118.29 5025-24 118.29 5025-24 118.29 5025-24 118.29
ADAPTER, Maxi 29/42 5030-42 45.73 5030-42 45.73 5030-42 45.73 5030-42 45.73
ADAPTER, Midi 29/42 5030-24 44.98 5030-24 44.98 5030-24 44.98 5030-24 44.98
THERMOWELL, 10 mm O.D. 6470-42 16.99 6470-44 16.99 6470-46 18.53 6470-46 18.53
STIRRER MOTOR & CONTROLLER 13649-19 1265.18 13647-35 1269.00 13647-35 1269.00 13647-35 1269.00
CLAMPS, 65/40 Union Type (3) 7666-30 170.88 7666-30 170.88 7666-30 170.88 7666-30 170.88
HEATING MANTLE, Alum.
Housing 12043-27 871.00 12043-29 984.00 12043-31 1624.37 12043-33 1784.00
MANTLE SUPPORT 12097-08 139.00 12097-10 186.00 12097-12 201.00 12097-14 233.00
VOLTAGE CONTROLLER (2) 12087-10 621.30 12087-10 621.30 — — 12082-10 1119.76
VOLTAGE CONTROLLER (3) — — — — 12087-10 621.30 — —
COMPLETE 6470-60 6841.45 6470-64 7649.40 6470-68 10041.59 6470-72 11098.18

6472 Cylindrical Pilot Plants

10 & 20 Liter Reactors
Domed Head
Unjacketed
With Stainless Steel Support
➧➧10 & 20 liter flasks with

bottom outlet
➧➧Large side
port on head 6472-284
for material
addition
➧➧Internal heat
exchange coil* 6472-282
➧➧Rugged stainless steel

support frame on casters for
mobility
➧➧Adjustable height flask
support
➧➧Available with Lexan™ safety
shields
*Supplied with PTFE-coated copper
tubing; also available in Hastalloy C-276
or 316 stainless steel.
Order
Each
Code
10-Liter COMPLETE, Unjacketed Flask, with Electric DIGITAL Motor 6465-405 13549.56
10-Liter COMPLETE, Unjacketed Flask, with Electric ANALOG Motor 6465-401 12480.33 6472-280
10-Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor 6472-47 11835.62
20-Liter COMPLETE, Unjacketed Flask, with Electric DIGITAL Motor 6472-280 16526.01
20-Liter COMPLETE, Unjacketed Flask, with Electric ANALOG Motor 6472-282 15143.18
20L shown above
20-Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor 6472-284 15206.51
6472 PILOT PLANT REACTOR Cylindrical, 10 & 20 Liter Unjacketed Flask, D

omed Head
Complete cylindrical pilot plant reactor Head is traditional domed style, with paddle PTFE agitator at bottom and a
on one‑inch stainless steel tubing mobile seven openings. One  45/50 center “pinned” turbine blade PTFE agitator
support frame: measures 60 inches high, neck, one  45/50, two  29/42 and higher on shaft for grease-free operation
15 inches wide, 15 inches deep. Note: two  24/40 openings plus a 60 mm I.D. with 8067 PTFE bearing. Note: Steel
Frame shipped assembled. side port. Motor is secured on an epoxy reinforced PTFE shafts or ground glass
Flask opening is 200 mm (8 inches), coated mounting plate over center  45/50 shafts can be supplied along with other
Schott style flange with o‑ring groove. opening; other openings are for condenser, bearings.
Bottom outlet is 0-14 mm Easy Action thermop robe, cooling coil, etc. Head is Cooling coil is copper tubing
adjustable threaded valve opening or flush secured to flask with a quick release clamp. encapsulated with PTFE; also available
seal valve. O‑Rings supplied on valves Stirring motor can be air-driven or in 316 stainless steel or Hastalloy C-276.
are Chemraz (PTFE elastomeric material) electric, either digital or analog. A digital temperature control system is
f o r e x c e l l e n t c h e m i c a l re s i s t a n c e . Stirring rod is a 19 mm (3/4 inch) O.D., supplied to control heating mantles. This
Flasks with other bottom outlet types precision ground and polished glass prevents overheating, overshoot and
are available. stirring shaft with a “pinned” multi- gives an instant readout of temperature.
10 LITER 20 LITER
STIRRING MOTOR, Air Driven, 1-1/2 HP with 1/2 inch Motor Shaft 13370-10 411.74 13370-10 411.74
SUPPORT ASSEMBLY, Complete 6472-27 2563.97 6472-364 3265.22
CHUCK, Flex-Grip, 12.7mm — 19mm 8124-20 152.25 8124-20 152.25
FILTER/REGULATOR/LUBRICATOR for Air Motor 13372-45 237.98 13372-45 237.98
COMPLETE AIR DRIVEN MOTOR SYSTEM 6472-47 11835.62 6472-284 15206.51
STIRRING MOTOR, Analog 13544-20 582.32 13544-20 582.32
CHUCK, Flex-Grip, 9.5mm — 19mm 8124-17 152.25 8124-17 152.25
COMPLETE ANALOG MOTOR SYSTEM 6465-401 12480.33 6472-282 15143.18
STIRRING MOTOR, Digital 13504-41 1948.46 13504-41 1948.46
CHUCK, Flex-Grip, 13mm — 19mm 8124-22 152.25 8124-22 152.25
COMPLETE DIGITAL MOTOR SYSTEM 6465-405 13549.56 6472-280 16526.01
All the above COMPLETE items contain these components: Order Code Each Order Code Each
FLASK, with CAPFE O‑Ring and 0-14 E-Z Action Bottom Valve 6522-21 1131.71 — —
FLASK, with 200mm Flange, O‑Ring groove — — 6472-02 2242.57
HEAD, Domed, with seven (7) openings 6530-37 1095.60 6530-37 1095.60
GLASS CAP, Side Port 15312-30 60.05 15312-30 60.05
CAPFE O‑Ring, Side Port 7855-878 28.10 7855-878 28.10
CLAMP, Side Port, Quick Release 6517-22 87.08 6517-22 87.08
CLAMP, Head, 200mm, Quick Release 6517-31 145.09 6517-31 145.09
DRAIN VALVE, only, Flush Seal — — 6472-245 1010.52
CLAMP, Drain Valve, 1 inch — — 8856-07 112.13
SWEEP ELBOW, 60º, 1 inch Beaded Pipe — — 8830-207 65.97
MANTLE, Bottom, Aluminum, with hole, 1–180w115v 12053-50 676.91 — —
MANTLE, Bottom, Aluminum, with hole, 1–250w115v — — 12053-64 874.66
MANTLE, #2 & #3, Fabric, Removable 1–495w115v 12041-10 860.65 — —
MANTLE, #2 & #3, Fabric, Removable 1–770w115v (2) — — 12041-12 777.15
HEAT EXCHANGE COIL, Cooling, Copper/PTFE 12067-39 547.05 12067-48 600.74
TEMPERATURE CONTROL SYSTEM, Complete 6472-67 1745.08 6472-67 1745.08
AGITATOR, Lower, PTFE, Multipaddle 8091-10 226.34 8091-10 226.34
AGITATOR, Upper, PTFE, Turbine, 102mm 8093-12 186.56 8093-12 186.56
STIRRING SHAFT, 19mm Polished Glass 8076-40 248.02 8076-40 248.02
BEARING, PTFE, 45/50 8067-30 269.05 8067-30 269.05
COLLAR, with PTFE Gasket 8127-20 36.68 8127-20 36.68
ADAPTER, #7 – 24/40 (2) 5028-30 27.61 5028-30 27.61
ADAPTER, #7 – 29/42 5028-32 32.61 5028-32 32.61
ADAPTER, #11 – 29/42 5030-24 44.98 5030-24 44.98
ADAPTER, #11 – 24/40 — — 5030-06 28.65
ADAPTER, Offset – 24/40 — — 5268-10 36.56
ADAPTER, Offset – 29/42 — 5268-15 40.74
ADAPTER, with 2mm bore PTFE stopcock — — 5202-12 80.01
CONDENSER, 300mm, 29/42 5945-24 137.68 — —
CONDENSER, 300mm, 24/40 — — 5946-18 125.23
STOPPER, 24/40 (2) 8250-12 19.79 8250-12 19.79
STOPPER, 29/42 (2) 8250-14 25.05 8250-14 25.05
CLAMP HOLDER, Large Scale 11081-21 84.80 11081-21 84.80
ROD, 6 inch x 1/2 inch for Temperature Controller 11166-22 8.36 11166-22 8.36
GREASE, Krytox GPL 8115-08 59.40 8115-08 59.40


Domed Head
Unjacketed
➧➧30 & 50 liter reactors with bottom

outlet
➧➧Domed glass head with large side
port opening
➧➧Internal heat exchange coil*
➧➧Rugged stainless steel pipe
mobility
➧➧Adjustable height flask support
shields

6472-56
Order Code Each

30 Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor 6472-56 19978.81
6472 PILOT PLANT REACTOR Cylindrical, 30 & 50 Liter Unjacketed Flask, D

omed Head
Complete cylindrical pilot plant reactor to allow room under flask for various ACE also o ffers electric stirrer motors
on one‑inch pipe, self-supporting, stainless outlet configurations. (see 13554, page 216).
steel mobile support frame: 30 liter size Head is traditional domed style, with Stirring rod is a 28mm (1-1/8 inch)
measures 76 inches high, 26 inches wide, eight openings. One  45/50 center neck, O.D., precision ground and polished
26 inches deep; 50 liter size measures 84 four  45/50 and two  29/42 openings plus glass stirring shaft with a “pinned” multi-
inches high, 26 inches wide, 26 inches a 100 mm I.D. side port. Motor is secured paddle PTFE agitator at bottom and a
deep. Note: Frame shipped assembled. on an epoxy coated mounting plate over turbine blade PTFE agitator higher on
Flask opening is 300 mm (12 inch), center  45/50 opening; other openings are shaft for grease-free operation with 8067
flat-ground plane flange. Bottom outlet is for condenser, thermop robe, cooling coil, PTFE bearing. Note: Steel reinforced
0-20mm Easy Action adjustable threaded etc. Head is secured to flask with a PTFE PTFE shafts or ground glass shafts can be
valve opening with o‑ring ball joint outlet gasket and two-piece polymer coupling. supplied along with other bearing types.
tube. O‑Rings supplied on valves are Maximum bolt-tightening torque for plastic Cooling coil is copper tubing
Chemraz (PTFE elastomeric material) coupling (cold state) is 30 in-lbs. In place encapsulated with PTFE; available in
f o r e x c e l l e n t c h e m i c a l re s i s t a n c e . of domed head, ACE also offers a flat glass 316 stainless steel or Hastalloy C-276.
Flasks with other bottom outlet types or flat stainless steel head (see page 113). A digital temperature control system is
are available. Stirring motor is a compact, air supplied to control heating mantles. This
Black epoxy coated aluminum flask driven motor that develops 1.5 HP at 90 prevents overheating, overshoot and
support plate is adjustable, vertically, lbs. air pressure. As an optional item, gives an instant readout of temperature.
30 LITER 50 LITER
FLASK, with 300mm Plane Flange and Bottom Valve 6472-03 2583.56 6472-05 3046.63
HEAD, Domed, with eight (8) openings 6530-45 2562.18 6530-45 2562.18
GASKET, Head, PTFE 6525-51 326.26 6525-51 326.26
COUPLING, Head, with Inserts and Hardware 6525-30 1056.54 6525-30 1056.54
WRENCH, Torque, 30 in-lbs. 6525-60 144.09 6525-60 144.09
SOCKET, 1/4 inch 6525-61 10.69 6525-61 10.69
MANTLE, Bottom, Aluminum, with hole, 1–370w115v 12053-54 697.89 12053-54 697.89
MANTLE, #2, Fabric, Removable 2–880w115v 12041-16 1201.84 12041-18 1090.99
MANTLE, #3, Fabric, Removable 2-725w115v — — 12041-35 1236.96
HEAT EXCHANGE COIL, Cooling, Copper/PTFE 12067-40 1134.78 12067-44 1692.90
AIR MOTOR, 1-1/2 Hp with 1/2 inch Motor Shaft 13370-10 411.74 13370-10 411.74
AGITATOR, Upper, PTFE, with four Pitched Blades, 152mm 8093-35 628.06 8093-35 628.06
STIRRING SHAFT, Polished Glass 8080-14 402.64 8080-18 446.02
BEARING, PTFE, 45/50 8067-105 320.08 8067-105 320.08
CONNECTOR, Beam Connects 1/2 inch Motor Shaft to Chuck 6472-155 55.71 6472-155 55.71
CHUCK, 28mm Connects Beam Connection to Stirring Shaft 6472-157 89.89 6472-157 89.89
ADAPTER, #7 – 24/40 5028-30 27.61 5028-30 27.61
ADAPTER, #15 – 29/42, (2) 5030-42 45.73 5030-42 45.73
ADAPTER, #11 – 45/50 5030-60 51.58 5030-60 51.58
ADAPTER, #15 – 45/50 8042-17 33.38 8042-21 33.38
ADAPTER, #15 – 45/50, with 4mm PTFE Stopcock 5274-22 117.64 5274-22 117.64
ADAPTER, #11 and #15 – 45/50 5031-86 119.50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30 5075-45 123.30
BUSHING, Nylon, #11 7506-02 11.39 7506-02 11.39
BUSHING, Nylon, #15, (4) 7506-06 12.35 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96 5945-76 382.96
CONDENSER, Cold Finger, 14mm O.D., 625mm 5958-99 92.87 5958-99 92.87
STOPPER, 45/50, (4) 8250-20 12.35 8250-20 12.35
COMPLETE 6472-56 19978.81 6472-60 22534.06
Custom variations and other stirring motors are available via

special order. Contact ACE Engineering and Technical Staff.


Flat Head
Unjacketed
➧➧30 & 50 liter reactors with bottom

outlet
➧➧Stainless steel flat head
➧➧Rugged stainless steel pipe support
frame on casters for mobility
➧➧Adjustable height top and
bottom flask supports
➧➧Available with Lexan™ safety shields
*Supplied with PTFE-coated

copper tubing; also available
in Hastalloy C-276 or 316
stainless steel.
6472-51
Order Code Each

6472 PILOT PLANT REACTOR Cylindrical, 30 & 50 Liter Unjacketed Flask, F lat Head
Complete cylindrical pilot plant reactor on allow room under flask for various outlet Stirring motor is a compact, air driven m
otor
self-supporting, mobile support frame: 30 configurations. that develops 1.5 HP at 90 lbs. air pressure.
liter size on one‑inch stainless steel pipe, Unique flat 316 stainless steel head is As an optional item, ACE also offers electric
measures 70 inches high, 26 inches wide, 0.250 inches (6.4mm) thick, with seven stirrer motors: see 13554.
26 inches deep; 50 liter size on one‑inch openings. Head has  45/50 PTFE center Stirring rod is a 28 mm (1-1/8 inch),
stainless steel pipe, measures 78 inches joint insert, four  45/50 PTFE joint inserts, precision ground and polished glass stirring
high, 26 inches wide, 26 inches deep. Note: and two   29/42 PTFE joint inserts. Stainless shaft with a “pinned” multi-paddle PTFE
Frame shipped assembled. steel head has a PTFE cover. Maximum agitator at bottom and a turbine blade PTFE
Flask opening on 30 and 50 liter is 300 mm bolt-tightening torque of head clamp (cold agitator higher on shaft for grease-free
(12 inch) flat-ground plane flange. Bottom state) is 30 in-lbs. Motor is secured on an operation with 8067 PTFE bearing.
outlet on 30 and 50 liter is 0-20 mm valve. epoxy coated mounting plate over center Cooling coil is copper tubing encapsulated
O‑Rings supplied on valves are Chemraz  45/50 PTFE insert; other openings are for with PTFE; available in 316 stainless steel
(PTFE elastomeric material) for excellent condenser, thermoprobe, cooling coil, etc. or Hastalloy C-276.
chemical resistance. Flasks with other bottom Head is secured to flask with PTFE gasket A digital temperature control system is
outlet valves are available. and two-piece polymer coupling. In place of supplied to control heating mantles. This
Black epoxy coated aluminum flask flat head, ACE offers a domed glass head with prevents overheating, overshoot and gives
support plate is adjustable, vertically, to traditional raised joints. an instant readout of temperature.
30 LITER 50 LITER
FLASK, with 300mm Plane Flange and Bottom Valve 6472-03 2583.56 6472-05 3046.63
HEAD, Flat, Stainless Steel, with 7 openings 6472-26 835.47 6472-26 835.47
HEAD COVER, 300mm, PTFE 6472-30 219.16 6472-30 219.16
JOINT INSERTS, PTFE – 29/42 (2) 6413-07 90.78 6413-07 90.78

GASKET, Head, PTFE 6525-51 326.26 6525-51 326.26
WRENCH, TORQUE, 30 in-lbs. 6525-60 144.09 6525-60 144.09
SOCKET, 1/4 inch 6525-61 10.69 6525-61 10.69
MANTLE, Bottom, Aluminum, with hole, 1–370w-115v 12053-54 697.89 12053-54 697.89
MANTLE, #2, Fabric, Removable 2–880w-115v 12041-16 1201.84 12041-18 1090.99
MANTLE, #3, Fabric, Removable 2–725-w115v — — 12041-35 1236.96
COIL, Cooling, Copper/PTFE, 1/2 inch 12067-40 1134.78 12067-44 1692.90
AIR MOTOR, 1-1/2 HP with 1/2 inch Motor Shaft 13370-10 411.74 13370-10 411.74
AGITATOR, Lower, PTFE, Multipaddle, 178mm 8091-36 613.84 8091-36 613.84
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm 8093-35 628.06 8093-35 628.06
BEARING, PTFE, 45/50 8067-105 320.08 8067-105 320.08

CONNECTOR, Beam, Connects 1/2 inch Motor Shaft to Chuck 6472-155 55.71 6472-155 55.71
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft 6472-157 89.89 6472-157 89.89
ADAPTER, #15 – 29/42 (2) 5030-42 45.73 5030-42 45.73
ADAPTER, #11 – 45/50 5030-60 51.58 5030-60 51.58
ADAPTER, #15 – 45/50 8042-21 50.57 8042-21 50.57
ADAPTER, #11 & #15 – 45/50 5031-86 119.50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30 5075-45 123.30

BUSHING, Nylon, #11 7506-02 11.39 7506-02 11.39
BUSHING, Nylon, #15 (4) 7506-06 12.35 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96 5945-76 382.96

STOPPER, 45/50 (4) 8250-20 44.68 8250-20 44.68

COMPLETE 6472-51 18892.72 6472-54 21447.97


Jacketed or Unjacketed Flask 30 Liter Reactors
3-Post Stand
➧➧New 3-post support stand
with open top offers easier
access to head and/or
placement of condensers,
probes, etc.
➧➧Portable 30 liter reactor
with bottom outlet
➧➧Internal heat exchange
coil (unjacketed flask)*
➧➧Rugged user-friendly
support frame has
flanges with captive
hardware
➧➧PTFE-covered bottom
flask support shelf
For heating/cooling
circulators, see
listing starting on
page 240.
*Supplied with PTFE-coated

6473-150 copper tubing; also available 6473-275
in Hastalloy C-276 or 316
stainless steel.
Adapter and side drive motors are available.
6473 PILOT PLANT REACTOR Cylindrical, 30 Liter Jacketed or Unjacketed Flask, D

omed Head
Complete cylindrical pilot plant Jacket on flask is direct sealed to inner Stirring rod is a 28mm (1-1/8 inch)
reactor on self-supporting 3-post, mobile vessel at top and silicone rubber sealed O.D. precision ground and polished
support frame. Frame is fabricated at bottom. Jacket inlet/outlet 35/25 solid glass stirring shaft with a “pinned”
from stainless steel and powder coated O‑Ring ball joints sealed tangentially multi-paddle PTFE agitator at bottom
aluminum: measures 74 inches high, 24 Flask support is adjustable, vertically, and a turbine blade PTFE agitator higher
inches wide, 20 inches deep. Note: Frame to allow room under flask for various on shaft for grease-free operation with
shipped assembled. outlet configurations. 8067 PTFE bearing.
Flask can be jacketed or unjacketed Head is traditional domed style, with Heat exchange coil for unjacketed
with 300mm (12 inch) opening, flat eight openings:  45/50 center neck, reactor is a 1/2 inch O.D. copper tubing
ground plane flange. Bottom outlet four  45/50 and two  29/42 side necks, encapsulated with PTFE; available in
is a 0-20mm Easy Action adjustable plus a 100mm (4 inch) I.D. side port 316 stainless steel or Hastalloy C-276.
opening threaded valve with C hemraz with grooved flange. Head is secured A digital temperature control system
(PTFE elastomeric material) o‑rings to flask with a new “swing open” front is supplied with unjacketed reactor
for excellent chemical resistance on flange clamp, torqued to 30 in-lbs (tools consisting of a type “J” digital controller
unjacketed flask; a flush seal drain with supplied). with a PFA covered thermoprobe to
one‑inch beaded drain discharge with Stirring motor is a 1/2 HP, 120v, control heating mantles.
CAPFE and Kalrez o‑rings on jacketed 50/60Hz electric motor, for hazardous A type “J” temperature monitoring
flask. Flasks with other bottom valves locations, mounted over center of system is supplied with the jacketed
are available.  45/50 center neck. flask version.
30 LITER UNJACKETED 30 LITER JACKETED

(12 inch Flange; 12 inch Body) (12 inch Flange; 12 inch Body)
FLASK, with 300mm Plane Flange and Valve or Valve Opening 6472-03 2583.56 6472-030 6038.75
HEAD, Domed, with Eight Openings 6530-45 2562.18 6530-45 2562.18
GLASS CAP, 100mm 15312-33 107.78 15312-33 107.78
CAPFE O‑Ring, 100mm 7855-880 28.63 7855-880 28.63
CLAMP, Quick Release, 100mm 6517-25 98.23 6517-25 98.23
GASKET, PTFE 6525-51 326.26 6525-51 326.26
SOCKET, 1/2-inch, 1/4-inch 6525-61 10.69 6525-61 10.69
DRAIN VALVE, Flush Seal (Jacketed only) — — 6472-245 1010.52
SWEEP ELBOW, 60°, 1 inch BP — — 8830-207 65.97
MANTLE, Bottom, Aluminum, with hole, 1-370w-115v 12053-54 697.89 — —
MANTLE, #2, Fabric, Removable, 2-880w-115v 12041-16 1201.84 — —
COIL, Cooling, Copper/PTFE, 1/2 inch 12067-40 1134.78 — —
SUPPORT ASSEMBLY, 3-Post Complete 6473-47 5188.31 6473-51 5531.62
TEMPERATURE CONTROL SYSTEM, Complete 6472-77 2937.00 — —
TEMPERATURE MONITORING SYSTEM, Complete — — 8318-207 1028.28
STIRRER MOTOR AND CONTROLLER, 1/2 HP 13554-55 3369.54 13554-55 3369.54
AGITATOR, Lower, PTFE, Multipaddle, 178mm 8091-36 613.84 8091-36 613.84
STIRRING SHAFT, Polished Glass, 28mm 8080-14 402.64 8080-14 402.64
BEARING, PTFE, 45/50 8067-105 320.08 8067-105 320.08
CONNECTOR, Beam Coupling, 5/8 inch Motor Shaft to Chuck 6472-156 54.09 6472-156 54.09
ADAPTER, #7 – 24/40 5028-30 27.61 5028-30 27.61
ADAPTER, #15 – 29/42 (2) 5030-42 45.73 5030-42 45.73
ADAPTER, #11 – 45/50 5030-60 51.58 5030-60 51.58
ADAPTER, #15 – 45/50 8042-21 50.57 8042-21 50.57
ADAPTER, #11 and #15 – 45/50 5031-86 119.50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 45/50 5040-96 169.62 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30 5075-45 123.30
ADAPTER, Offset, 45/50 – 45/50 5268-21 109.58 5268-21 109.58
BUSHING, Nylon, #11 7506-02 11.39 7506-02 11.39
BUSHING, Nylon, #15 (4) 7506-06 12.35 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96 5945-76 382.96
CONDENSER, Cold Finger, 14mm O.D., 625m 5958-99 92.87 5958-99 92.87
STOPPER, 45/50 (4) 8250-20 44.68 8250-20 44.68
COMPLETE 6473-150 23975.32 6473-275 24274.92


100 Liter Reactor
Domed Head
Unjacketed
➧➧100 liter reactor with bottom outlet

port opening
➧➧Adjustable height top and bottom
flask supports

6473-60
Order Code Each

100 Liter COMPLETE, Unjacketed Flask, with Motor 6473-60 29452.59
6473 PILOT PLANT REACTOR Cylindrical, 100 Liter Unjacketed Flask, D

omed Head
Complete cylindrical pilot plant reactor supplied to stabilize flask. 5/8 inch O.D. Controller operates on 120
on self-supporting, mobile support frame Head is traditional domed style, with volts 50/60 Hz (air motor available — call
on one‑inch stainless steel pipe, measures eight openings; five  45/50 and two for quotation).
88 inches high, 28 inches wide, 28 inches  29/42 plus one 100 mm I.D. side port. Features a 28 mm (1-1/8 inch) O.D.
deep. Note: Frame shipped assembled. Motor is secured on black epoxy coated precision ground and polished glass stirring
Flask opening is 300 mm (12 inch) flat- mounting plate over center  45/50 opening shaft with a “pinned” multi-paddle PTFE
ground plane flange. Flask body is 18 inch on head; other openings are for condenser, agitator at bottom and a turbine blade PTFE
outside diameter. Bottom outlet is 0-20 thermoprobe, cooling coil, etc. Head is agitator higher on shaft for grease-free
mm adjustable opening threaded valve secured to flask with PTFE gasket and
operation with 8067 PTFE bearing.
with Chemraz (PTFE elastomeric material) two-piece polymer coupling. Maximum bolt Cooling coil is 1/2 inch O.D. copper tubing
O‑Rings for excellent chemical resistance. tightening torque for coupling (cold state) encapsulated with PTFE; also available in
Other bottom valve types are available. is 30 in-lbs. In place of domed head, ACE 316 stainless steel or Hastalloy C-276.
Black epoxy coated aluminum flask offers a flat glass or flat stainless steel head. A digital temperature control system is
support plate is adjustable, vertically, to Stirring motor is heavy duty, 1/2 HP supplied to control heating mantles. This
allow room under flask for various outlet electronic motor for hazardous area duty, prevents overheating, overshoot and gives
receptacles. Upper support brackets complete with controller. Motor shaft is an instant readout of temperature.
100 LITER (12 inch Flange; 18 inch Body) Order Code Each
FLASK, with 300mm Plane Flange and Valve 6473-02 5531.62
HEAD, Domed, with 8 Openings 6530-45 2562.18
GLASS CAP, 100mm 15312-33 107.78
CAPFE O‑Ring, 100mm 7855-880 28.63
CLAMP, Quick Release, 100mm 6517-25 98.23
GASKET, PTFE 6525-51 326.26
COUPLING, with Inserts and Hardware 6525-30 1056.54
WRENCH, TORQUE, 30 in-lbs. 6525-60 144.09
SOCKET 6525-61 10.69
MANTLE, Bottom, Aluminum, with hole, 1-775w-115v 12053-74 1462.92
MANTLE, #2, Fabric, Removable, 4-1100w-115v 12041-52 2228.41
COIL, Cooling, Copper/PTFE, 1/2 inch 12067-79 1773.43
SUPPORT ASSEMBLY, Complete 6473-34 3855.28
TEMPERATURE CONTROL SYSTEM, Complete 6472-79 2988.82
STIRRER MOTOR AND CONTROLLER, 1/2 HP 13554-55 3369.54
AGITATOR, Lower, PTFE, Multipaddle, 178mm 8091-36 613.84
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm 8093-35 628.06
STIRRING SHAFT, Polished Glass, 28mm 8080-22 472.33
BEARING, PTFE, 45/50 8067-105 320.08
CONNECTOR, Beam, Connects 5/8 inch Motor Shaft to Chuck 6472-156 54.09
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft 6472-157 89.89
COLLAR, with PTFE Gasket 8127-28 73.09
ADAPTER, #7 – 24/40 5028-30 27.61
ADAPTER, #15 – 29/42 (2) 5030-42 45.73
ADAPTER, #11 – 45/50 5030-19 62.97
ADAPTER, #15 – 45/50 8042-21 50.57
ADAPTER, #15 – 45/50, with 4mm PTFE Stopcock 5274-22 117.64
ADAPTER, #11 and #15 – 45/50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30
ADAPTER, Offset, 45/50 – 45/50 5268-21 109.58
BUSHING, Nylon, #11 7506-02 11.39
BUSHING, Nylon, #15 (4) 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96
CONDENSER, Cold Finger, 14mm O.D., 625mm 5958-99 92.87
STOPPER, 45/50 (4) 8250-20 44.68
CLAMP, Chain 11079-24 51.23
CLAMP HOLDER, Pilot Plant (2) 11081-21 84.80
SUPPORT ROD, 1/2 inch diameter, 12 inches long 11166-37 13.60
END-TO-END ROD CONNECTOR 11175-23 19.87
ROD, 6 inch x 1/2 inch for Temperature Controller 11166-22 8.36
GREASE, Krytox GPL 8115-08 59.40
COMPLETE 6473-60 29452.59


200 Liter Reactor
Domed Head
Unjacketed
➧➧200 liter reactor with bottom outlet

port opening
➧➧Adjustable height top and bottom
flask supports

Order Code Each 6473-72

200 Liter COMPLETE, Unjacketed Flask, with Motor 6473-72 39583.21
6473 PILOT PLANT REACTOR Cylindrical, 200 Liter Unjacketed Flask, D

omed Head
Complete cylindrical pilot plant reactor place. Upper support brackets supplied Motor shaft is 5/8 inch O.D. Controller
on self-supporting, mobile support frame to stabilize flask. operates on 120 volts 50/60 Hz. (Air motor
on one‑inch stainless steel pipe, measures Head is traditional domed style, with available, call for quotation).
118 inches high, 32 inches wide, 32 inches eight openings; five  45/50, two  29/42, 28 mm (1-1/8 inch) O.D. precision
deep. Note: Frame shipped assembled. plus one 100 mm I.D. side port. ground and polished glass stirring shaft
Flask opening is 300 mm (12 inch) flat- Motor is secured on black epoxy coated with a “pinned” multi-paddle PTFE agitator
ground plane flange. Flask body is 18 inch mounting plate over center  45/50 opening at bottom and two turbine blade PTFE
outside diameter. Bottom outlet is a flush on head; other openings are for condenser, agitators higher on shaft for grease-free
seal drain valve with a one‑inch beaded thermoprobe, cooling coil, etc. Head is operation with 8067 PTFE bearing.
drain discharge. O‑Ring supplied on valve is s ecured to flask with PTFE gasket and
Cooling coil is 1/2 inch O.D. copper
a CAPFE (silicone encapsulated with PTFE), two-piece plastic coupling. Maximum bolt tubing encapsulated with PTFE; also
and Kalrez for excellent chemical resistance. tightening torque for coupling (cold state) available in 316 stainless steel or Hastalloy
Black epoxy coated aluminum flask is 30 in-lbs. In place of domed head, ACE C-276.
support plate is adjustable, vertically, offers a flat glass or flat stainless steel head A digital temperature control system
to allow room under flask for various that use PTFE joint inserts. is supplied to control heating mantles. This
outlet receptacles. Plate is supplied with Stirring motor is heavy duty, 1/2 HP prevents over-heating and overshoot, and
three adjustable braces to hold mantle in electronic motor for hazardous area duty. gives an instant readout of temperature.
200 LITER (12 inch Flange; 18 inch Body) Order Code Each
FLASK with 300mm Plane Flange, 200L 6473-11 10958.02
HEAD, Domed, with 8 Openings 6530-45 2562.18
GLASS CAP, 100mm 15312-33 107.78
CAPFE O‑Ring, 100mm 7855-880 28.63
GASKET, PTFE 6525-51 326.26
SOCKET 1/4 inch 6525-61 10.69
DRAIN VALVE, Flush Seal 6472-245 1010.52
CLAMP, Drain Seal 1 inch 8856-07 112.13
CLAMP, Drain Seal 2 inch 8856-11 150.55
SWEEP ELBOW, 60º, 1 inch BP 8830-207 65.97
MANTLE, Bottom, Aluminum, with hole, 1-775w-115v 12053-74 1462.92
MANTLE, #2, Fabric, Removable, 4-1100w-115v (2) 12041-52 2228.41
COIL, Cooling, Copper/PTFE, 1/2 inch 12067-80 2123.00
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm (2) 8093-35 628.06
BEARING, PTFE, 45/50 8067-105 320.08
CONNECTOR, Beam, Conn. 5/8 inch Motor Shaft to Chuck 6472-156 54.09
CHUCK, 28mm, Connects Beam Conn. to Stirring Shaft 6472-157 89.89
ADAPTER, #7 – 24/40 5028-30 27.61
ADAPTER, #11 – 45/50 5030-19 62.97
ADAPTER, #15 – 29/42 5030-42 45.73
ADAPTER, #15 – 45/50 8042-21 50.57
ADAPTER, #15 – 45/50, with 4mm PTFE stopcock 5274-22 117.64
ADAPTER, #11 and #15 – 45/50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30
ADAPTER, Offset, 45/50 – 45/50 5268-21 109.58
BUSHING, Nylon, #11 7506-02 11.39
BUSHING, Nylon, #15 (4) 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96
STOPPER, 45/50 (4) 8250-20 44.68
CLAMP, Chain 11079-24 51.23
SUPPORT ROD, 1/2 inch diameter, 12 inches long (2) 11166-37 13.60
COMPLETE 6473-72 39583.21

6472/6465 C ylindrical Pilot Plants

Domed Head
Jacketed
➧➧10 & 20 liter jacketed

reactors with bottom
outlet
➧➧Domed glass head
with large side 6472-367
port
opening
➧➧Internal heat
exchange coil 6472-365
available, not
supplied
support frame on casters
for mobility
shields
For heating/cooling circulators,

see listing starting on page 240.
Order Code Each

10-Liter COMPLETE, Jacketed Flask, with Electric ANALOG Motor 6465-501 10591.42
10-Liter COMPLETE, Jacketed Flask, with Electric DIGITAL Motor 6465-505 11977.03
10-Liter COMPLETE, Jacketed Flask, with AIR DRIVEN Motor 6472-147 9933.34
6472-363
20-Liter COMPLETE, Jacketed Flask, with Electric DIGITAL Motor 6472-363 14738.20
20-Liter COMPLETE, Jacketed Flask, with Electric ANALOG Motor 6472-365 13344.23
20-Liter COMPLETE, Jacketed Flask, with AIR DRIVEN Motor 6472-367 13417.02
6472/6465 PILOT PLANT REACTOR Cylindrical, 10 & 20 Liter Jacketed Flask, D

omed Head
Complete cylindrical pilot plant reactor on flask is direct sealed at the top and Stirring rod is a 19 mm (3/4 inch) O.D.,
on 1-inch stainless steel tubing mobile silicone rubber sealed at bottom. 28/15 or precision ground and polished glass
support frame: measures 60 inches high, 35/25 o-ring ball joint on inlet/outlet sealed stirring shafts with a “pinned” multi-paddle
15 inches wide, 15 inches deep. Note: tangentially. PTFE agitator at bottom and a turbine
Frame shipped assembled. Head is traditional domed style, with blade PTFE agitator higher on shaft for
Jacketed flask opening is 200 mm seven openings. One  45/50 center neck, grease-free operation with 8067 PTFE
(8 inch), Schott style flange with o‑ring one  45/50 , two  29/42 and two  24/40 bearing. Note: Steel reinforced PTFE
groove. Bottom outlet on 10L flask is openings, plus a 60 mm I.D. side port. Motor shafts or ground glass shafts can be
0-14 mm Easy Action adjustable threaded is secured on an epoxy coated mounting supplied along with other bearings.
valve opening; bottom outlet on 20L plate over center  45/50 opening; other A temperature monitoring system, with
flask is low dead space, flush seal valve. openings are for condenser, thermop robe, PTFE-covered Type “J” Thermocouple,
O‑Rings supplied on valves are Chemraz cooling coil, etc. Head is secured to flask is supplied to give an instant readout of
(PTFE elastomeric material) for excellent with a quick release clamp. temperature.
chemical resistance. Flasks with other Stirring motor can be air-driven or Jacket volume for 10L flask is six liters.
bottom outlet types are available. Jacket electric, either digital or analog. Jacket volume for 20L flask is 13.4 liters.
10 LITER 20 LITER
STIRRING MOTOR, Air Driven, 1-1/2 HP with 1/2 inch Motor Shaft 13370-10 411.74 13370-10 411.74
SUPPORT ASSEMBLY, Stainless Steel, Complete 6472-328 2601.49 6472-337 3294.38
CHUCK, “Flex-Grip”, 12.7mm — 19mm 8124-20 152.25 8124-20 152.25
COMPLETE AIR DRIVEN MOTOR SYSTEM 6472-147 9933.34 6472-367 13417.02
STIRRING MOTOR, Analog 13544-20 582.32 13544-20 582.32
CHUCK, “Flex-Grip”, 9.5mm — 19mm 8124-17 152.25 8124-17 152.25
COMPLETE ANALOG MOTOR SYSTEM 6465-501 10591.42 6472-365 13344.23
STIRRING MOTOR, Digital 13504-41 1948.46 13504-41 1948.46
CHUCK, “Flex-Grip”, 13mm — 19mm 8124-22 152.25 8124-22 152.25
COMPLETE DIGITAL MOTOR SYSTEM 6465-505 11977.03 6472-363 14738.20
All the above COMPLETE items contain these components: Order Code Each Order Code Each
FLASK, Jacketed with O‑Ring Groove and 0-14mm Bottom Valve, 10L 6524-23 3002.10 — —
FLASK, Jacketed with 200mm Flange, O‑Ring groove, 20L — — 6472-16 4361.31
HEAD, Domed, with seven (7) openings 6530-37 1095.60 6530-37 1095.60
DRAIN VALVE, only Flush Seal — — 6472-245 1010.52
SWEEP ELBOW, 60º, 1 inch Beaded Pipe — — 8830-207 65.97
TEMPERATURE MONITORING SYSTEM, Complete 8318-204 865.12 8318-204 865.12
AGITATOR, Upper, PTFE, Turbine, 102mm 8093-12 186.56 8093-12 186.56
STIRRING SHAFT, 19mm Polished Glass 8076-40 248.02 8076-40 248.02
BEARING, PTFE, 45/50 8067-30 269.05 8067-30 269.05
ADAPTER, #7 – 29/42 5028-32 32.61 5028-32 32.61
ADAPTER, #11 – 29/42 5030-24 44.98 — —
ADAPTER, #11 – 24/40 — — 5030-22 40.04
ADAPTER, Offset – 24/40 — — 5268-10 36.56
ADAPTER, Offset – 29/42 5268-15 40.74 — —
ADAPTER, with 2mm bore PTFE stopcock — — 5202-12 80.01
CONDENSER, 300mm, 29/42 5945-24 137.68 — —
CONDENSER, 300mm, 24/40 — — 5946-18 125.23
STOPPER, 24/40 (2) 8250-12 19.79 8250-12 19.79
STOPPER, 29/42 (2) 8250-14 25.05 8250-14 25.05
ROD, 6 inch x 1/2 inch for Temperature Monitor 11166-22 8.36 11166-22 8.36

7885 Pilot Plant Reactor

Photochemical
Jacketed
New
➧➧10 & 20 liter jacketed reactors
with bottom outlet
➧➧Domed glass head with large
side port opening
for mobility
➧➧ Adjustable height flask support
➧➧Large-scale photochemical
quartz immersion well
➧➧Large-scale photochemical U.V.
lamp & 1200 watt power supply
shields
6530-85
Head 7830-71
Order Code Each

7885
10 Liter COMPLETE, Unjacketed Flask, with DIGITAL Motor 7885-10 23009.90
20 Liter COMPLETE, Unjacketed Flask, with DIGITAL Motor 7885-20 24480.30
7885 PHOTOCHEMICAL REACTOR Pilot Plant, 10 & 20 Liter Jacketed Flask

Complete cylindrical pilot plant reactor Head is traditional domed style, stirring shaft with a “pinned” multi-
on 1-inch stainless steel tubing mobile with six openings. One  45/50 center paddle PTFE agitator at bottom of shaft
support frame: measures 60 inches high, neck, one  45/50, one  29/42 and one with 8050 PTFE mechanical seal bearing.
15 inches wide, 15 inches deep. Note:  24/40 side necks, a #50 Ace‑Thred Note: Steel reinforced PTFE shafts or
Frame shipped assembled. neck for immersion well, and a 60 mm ground glass shafts can be supplied
Jacketed flask opening is 200 mm I.D. side port. Motor is secured on an along with other bearings.
(8 inch), Schott style flange with O‑Ring epoxy coated mounting plate over center A temperature monitoring system, with
groove. Bottom outlet is low dead  45/50 opening; other openings are for PTFE-covered type “J” thermocouple,
space “flush seal” valve. O‑Rings condenser, thermoprobe, immersion well, is supplied to give an instant readout
supplied on valves are Chemraz (PTFE etc. Head is secured to flask with a quick of temperature. Also includes a 230V
elastomeric material) for excellent release clamp. power supply and a 120-watt U.V. lamp.
chemical resistance. Flasks with other Stirring motor is 120V Heidolph Includes Pyrex absorption sleeve for well.
bottom outlet types are available. Jacket electric, digital. Other types are available Jacket volume for 10L flask is six liters.
on flask is direct sealed at the top and via special order. Jacket volume for 20L flask is 13.4 liters.
bottom. 35/25 o-ring ball joint on inlet/ Stirring rod is a 19 mm (3/4 inch) O.D.,
outlet sealed tangentially. precision ground and polished glass
10 LITER 20 LITER
STIRRING MOTOR, Digital, Heidolph 13504-41 1948.46 13504-41 1948.46
SUPPORT ASSEMBLY, Stainless Steel 6472-329 3336.90 6472-329 3336.90
CHUCK, 19mm 8126-19 113.26 8126-19 113.26
RZR Stainless Steel Shaft and Coupling 8126-22 276.11 8126-22 276.11
FLASK, 10L Jacketed, 200mm Opening with O‑Ring Groove 6524-73 2890.91 — —
FLASK, 20L Jacketed, 200mm Opening with O‑Ring Groove — — 6472-16 4361.31
Bottom Flush Seal Valve Assembly with Pin 6482-20 1032.42 6482-20 1032.42
HEAD, Domed, with six (6) openings 6530-85 1213.52 6530-85 1213.52
GLASS CAP, 60mm Side Port 15312-30 60.05 15312-30 60.05
CLAMP, 60mm, Side Port, Quick Release 6517-22 87.08 6517-22 87.08
CLAMP, Drain Valve, 1 inch 8856-07 112.13 8856-07 112.13
SWEEP ELBOW, 60º x 1 inch Beaded Pipe 8830-207 65.97 8830-207 65.97
TEMPERATURE MONITORING SYSTEM, J-Kem, with “J” Thermocouple 12327-05 391.00 12327-05 391.00
24-in. PFA “J” Thermocouple 12141-26 171.58 12141-26 171.58
AGITATOR, Lower, PTFE, with Receptacle 8100-19 854.95 8100-19 854.95
STIRRING SHAFT, 19mm Polished Glass, 37 in. length 8076-39 249.51 8076-39 249.51
BEARING, PTFE, 45/50, Mechanical Seal 8050-06 601.93 8050-06 601.93
Stopcock Adapter for Condenser 5202-114 63.72 5202-114 63.72
ADAPTER, #7 – 24/40 5028-30 27.61 5028-30 27.61
ADAPTER, Offset – 29/42 5268-15 40.74 5268-15 40.74
CONDENSER, 400mm, 29/42 5945-25 141.24 5945-25 141.24
STOPPER, 45/50 (1) 8250-20 44.68 8250-20 44.68
CLAMP HOLDER, for Temperature Monitor 11081-21 84.80 11081-21 84.80
GREASE, Krytox 8115-08 59.40 8115-08 59.40
Immersion Well, Quartz, 48mm O.D. x 840mm Long 7874-48 1100.65 7874-48 1100.65
U.V. Lamp 1200w 7825-40 897.10 7825-40 897.10
#50 Bushing 7506-14 854.52 7506-14 854.52
Pyrex Absorption Sleeve, 30mm O.D. x 762mm Long 7835-45 56.98 7835-45 56.98
U.V. Power Supply 230v, 60hz 7830-71 3901.10 7830-71 3901.10
Pressure Relief Manifold 10015-10 2741.31 10015-10 2741.31
Circulator Hose Adapters (1) 12187-35 135.20 12187-35 135.20
Hose Clamps (1) 13010-01 112.28 13010-01 112.28
COMPLETE 7885-10 23009.90 7885-20 24480.30
For safety, either aluminum, stainless steel, or black

plastic shields should be added to the stand, or it should
be used in an enclosed hood.


Domed Head
Jacketed

with bottom outlet
➧➧Domed glass head with
large side port opening
for mobility
shields
For heating/cooling
circulators, see
listing starting on
page 240.
Contact ACE for full circulator catalog.
Order Code Each

30-Liter COMPLETE, Jacketed Flask,
6472-153 19633.14
with AIR DRIVEN Motor

6472-160 20820.72
6472-153
6472 PILOT PLANT REACTOR Cylindrical, 30 & 50 Liter Jacketed Flask, D

omed Head
Complete cylindrical pilot plant reactor a padded metal alloy (coated) ring secured Stirring rod is a 28mm (1-1/8 inch) O.D.,
on one‑inch self-supporting, stainless steel directly to the one‑inch pipe frame. precision ground and polished glass stirring
pipe mobile support frame: 30 liter frame size Head is traditional domed style, with shaft with a “pinned” multi-paddle PTFE
measures 76 inches high, 26 inches wide, 26 eight openings. Five  45/50 and two  29/42 agitator at bottom and a turbine blade PTFE
inches deep; 50 liter size measures 84 inches openings plus a 100 mm I.D. side port with agitator higher on shaft for grease-free
high, 26 inches wide, 26 inches deep. Note: cap, CAPFE O‑Ring and clamp. operation with 8067 PTFE bearing. Note:
Frame shipped assembled. Motor is secured on an epoxy coated Steel reinforced PTFE shafts or ground
Flask opening is 300 mm (12 inch), flat- mounting plate over center  45/50 opening; glass shafts can be supplied along with
ground plane flange. Bottom outlet is a flush other openings are for condenser, thermo other bearings.
seal drain valve with one‑inch beaded pipe probe, etc. Head is secured to flask with a Cooling coil is NOT supplied, but
outlet. O‑Rings supplied on valves are CAPFE PTFE gasket and two-piece plastic coupling. available in copper tubing encapsulated
(silicone encapsulated with PTFE) & Kalrez, Maximum bolt-tightening torque for plastic with PTFE; also available in 316 Stainless
for excellent chemical resistance. Flasks coupling (cold state) is 30 in-lbs. In place of Steel or Hastalloy C-276.
with other bottom outlet types are available. domed head, ACE offers a flat glass head A temperature monitoring system, with
Jacket on flask is direct sealed at the top and with ground-in joints, or a stainless steel PTFE-covered type “J” thermocouple,
silicone rubber sealed at bottom. 35/25 o-ring flat head that uses PTFE joint inserts. is supplied to give an instant readout of
ball joint on inlet/outlet sealed tangentially. Standard stirring motor is a compact, temperature.
Flask support is adjustable, vertically, to air driven motor that develops 1.5 HP at 90 Jacket volume for 30L flask is 6.5 liters.
allow room under flask for various outlet lbs. air pressure. As an optional item, ACE Jacket volume for 50L flask is 9.7 liters.
configurations. 30L and 50L flasks sit on also offers electric stirring: see No. 13554.
30 LITER 50 LITER
FLASK, Jacketed, with 300mm Plane Flange 6472-030 6038.75 6472-050 6821.55
HEAD, Domed, with eight (8) openings 6530-45 2562.18 6530-45 2562.18
GASKET, Head, PTFE 6525-51 326.26 6525-51 326.26
WRENCH, Torque, 30 in-lbs. 6525-60 144.09 6525-60 144.09
SOCKET, 1/4 inch 6525-61 10.69 6525-61 10.69
DRAIN VALVE, Flush Seal 6472-245 1010.52 6472-245 1010.52
SWEEP ELBOW, 60º, 1 inch Beaded Pipe 8830-207 65.97 8830-207 65.97
AIR MOTOR, 1-1/2 Hp with 1/2 inch Motor Shaft 13370-10 411.74 13370-10 411.74
AGITATOR, Upper, PTFE, with four Pitched Blades, 152mm 8093-35 628.06 8093-35 628.06
BEARING, PTFE, 45/50 8067-105 320.08 8067-105 320.08
CONNECTOR, Beam Connects 1/2 inch Motor Shaft to Chuck 6472-155 55.71 6472-155 55.71
CHUCK, 28mm Connects Beam Connector to Stirring Shaft 6472-157 89.89 6472-157 89.89
ADAPTER, #7 – 29/42 5028-32 32.61 5028-32 32.61
ADAPTER, #11 – 45/50 5030-60 51.58 5030-60 51.58
ADAPTER, #15 – 45/50 8042-21 50.57 8042-21 50.57
ADAPTER, #11 and #15 – 45/50 5031-86 119.50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30 5075-45 123.30
BUSHING, Nylon, #11 7506-02 11.39 7506-02 11.39
BUSHING, Nylon, #15, (4) 7506-06 12.35 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96 5945-76 382.96
STOPPER, 45/50, (4) 8250-20 44.68 8250-20 44.68
CLAMP HOLDER 11081-21 84.80 11081-21 84.80
COMPLETE 6472-153 19633.14 6472-160 20820.72


Flat Head
Jacketed

with b
ottom outlet
➧➧Stainless steel flat head
➧➧Rugged pipe support frame
on casters for mobility
➧➧Adjustable height top flask
support
shields
For heating/cooling
circulators, see
listing starting on
page 240.
Order Code Each

6472-151 18664.29

6472-154 19811.28
6472-151
6472 PILOT PLANT REACTOR Cylindrical, 30 & 50 Liter Jacketed Flask, F lat Head
Complete cylindrical pilot plant reactor Flask support is adjustable, vertically, Stirring motor is a compact, air driven
on one-inch, self-supporting, stainless to allow room under flask for various outlet motor that develops 1.5 HP at 90 lbs. air
steel pipe mobile support frame: 30 configurations. 30L and 50L flasks sit on pressure. As an optional item, ACE also
liter size, measures 70 inches high, 26 a padded metal alloy (coated) ring secured offers electronic stirring; see 13554.
inches wide, 26 inches deep; 50 liter size directly to the one‑inch pipe frame. Stirring rod on 30 L and 50 L size is a
measures 78 inches high, 26 inches wide, Unique flat 316 stainless steel head is 28 mm (1-1/8 inch) O.D. precision ground
26 inches deep. Note: Frame shipped 0.250 inches (6.4mm) thick, with seven and polished glass stirring shaft with a
assembled. openings. Head has  45/50 PTFE center “pinned” multi-paddle PTFE agitator at
Jacketed flask opening on 30 and 50 joint insert, four   45/50 PTFE joint inserts, bottom and a turbine blade PTFE agitator
liter is 300 mm (12 inch), flat ground plane and two  29/42 PTFE joint inserts. higher on shaft for grease-free operation
flange. Bottom outlet on 30 and 50 liter Stainless steel head has a PTFE cover. with 8067 PTFE bearing.
is a Flush Seal drain valve with one‑inch Maximum bolt-tightening torque of head Optional cooling coil is available in
b e a d e d p i p e d r a i n o u t l e t . O ‑ R i n g s clamp (cold state) is 30 in-lbs. Motor is copper tubing encapsulated with PTFE;
supplied on valve are CAPFE (silicone secured on an epoxy coated mounting also available in 316 Stainless Steel or
encapsulated with PTFE) & Kalrez, for plate over center  45/50 PTFE insert; Hastalloy C-276.
excellent chemical resistance. Flasks with o t h e r o p e n i n g s a re f o r c o n d e n s e r, A temperature monitoring system, with
other bottom outlet valves are available. thermoprobe, cooling coil, etc. Head is PTFE-covered type “J” thermocouple,
Jacket on flask is direct sealed at top secured to flask with PTFE gasket and is supplied to give an instant readout of
and silicone rubber sealed at bottom. two-piece polymer coupling. In place of temperature.
35/25 O‑Ring ball joint on inlet/outlet flat head, ACE offers a domed glass head Jacket volume for 30L flask is 6.5 liters.
sealed tangentially. with traditional raised joints. Jacket volume for 50L flask is 9.7 liters.
30 LITER 50 LITER
FLASK, Jacketed, with 300mm Plane Flange 6472-030 6038.75 6472-050 6821.55
HEAD, Flat, Stainless Steel, with 7 openings 6472-26 835.47 6472-26 835.47
HEAD COVER, 300mm, PTFE 6472-30 219.16 6472-30 219.16

DRAIN VALVE, Flush Seal 6472-245 1010.52 6472-245 1010.52
SWEEP ELBOW, 60°, 1 inch Beaded Pipe 8830-207 65.97 8830-207 65.97
GASKET, PTFE 6525-51 326.26 6525-51 326.26
COUPLING, with Inserts and Hardware 6525-30 1056.54 6525-30 1056.54
SOCKET, 1/4 inch 6525-61 10.69 6525-61 10.69
AIR MOTOR, 1-1/2 HP with 1/2 inch Motor Shaft 13370-10 411.74 13370-10 411.74
AGITATOR, Lower, PTFE, Multipaddle (178mm) 8091-36 613.84 8091-36 613.84
STIRRING SHAFT, Polished Glass, 28mm 8080-14 402.64 8080-18 446.02
BEARING, PTFE, 45/50 8067-105 320.08 8067-105 320.08

CONNECTOR, Beam, Connects 1/2 inch Motor Shaft to Chuck 6472-155 55.71 6472-155 55.71
COLLAR, w/PTFE Gasket 8127-28 73.09 8127-28 73.09
ADAPTER, #7 – 29/42 5028-32 32.61 5028-32 32.61
ADAPTER, #11 – 45/50 5030-60 51.58 5030-60 51.58
ADAPTER, #15 – 45/50 8042-21 66.87 8042-21 66.87
ADAPTER, #15 – 45/50, w/4mm PTFE Stopcock 5274-22 117.64 5274-22 117.64
ADAPTER, #11 and #15 – 45/50 5031-86 119.50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30 5075-45 123.30

BUSHING, Nylon, #11 7506-02 11.39 7506-02 11.39
BUSHING, Nylon, #15 (4) 7506-06 12.35 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96 5945-76 382.96

STOPPER, 45/50 (4) 8250-20 44.68 8250-20 44.68

CLAMP HOLDER 11081-21 84.80 11081-21 84.80
GREASE, Krytox, GPL 8115-08 59.40 8115-08 59.40
COMPLETE 6472-151 18664.29 6472-154 19811.28


100 Liter Reactor
Domed Head
Jacketed
➧➧100 Liter Reactor with bottom

outlet
➧➧Domed glass head with large
side port opening
mobility
shields
For heating/cooling
circulators, see
listing starting on
page 240.
Order Code Each

6473-66
100 Liter COMPLETE, Jacketed Flask, with Motor 6473-66 32441.89
6473 PILOT PLANT REACTOR Cylindrical, 100 Liter Jacketed Flask (12 inch Flange), D
omed Head
Complete cylindrical pilot plant secured directly to one‑inch pipe, and is Motor shaft is 5/8 inch O.D. Controller
reactor on self-supporting, mobile adjustable, vertically, to allow room for operates on 120 volts 50/60 Hz. (Air
support frame on one‑inch stainless various outlet configurations. motor available, call for details).
steel pipe, measures 94 inches high, Head is traditionally domed style, with 28mm (1-1/8 inch) O.D. precision
28 inches wide, 28 inches deep. Note: eight openings: five   45/50, two  29/42 ground and polished glass stirring shaft
Frame shipped assembled. plus one 100 mm I.D. side port. with a “pinned” multi-paddle PTFE
Flask opening is 300mm (12 inch) Motor is secured on black epoxy agitator at bottom and a turbine blade
flat-ground plane flange. Bottom outlet coated mounting plate over center PTFE agitator higher on shaft for grease-
is a flush seal drain valve with one‑inch   45/50 opening on head; other openings free operation with 8067 PTFE bearing.
beaded drain discharge. O‑Rings are for condenser, thermoprobe, cooling Optional cooling coil is 1/2 inch O.D.
supplied on valve are CAPFE (silicone coil, etc. Head is secured to flask with copper tubing encapsulated with PTFE;
encapsulated with PTFE) & Kalrez, for PTFE gasket and two-piece plastic also available in 316 stainless steel or
excellent chemical resistance. coupling. Maximum bolt tightening Hastalloy C-276.
Jacket on flask is direct sealed at torque for coupling (cold state) is 30 in- A temperature monitoring system, with
top and silicone sealed at bottom. lbs. In place of domed head, ACE offers PTFE-covered type “J” thermocouple,
35/25 o‑ring ball joints on inlet/outlet a flat glass or flat stainless steel head. is supplied to give an instant readout of
ports sealed tangentially. Flask sits Stirring motor is heavy duty, 1/2 HP temperature.
on a padded metal alloy (coated) ring electric motor for hazardous area duty. Jacket volume of flask is 26 liters.
100 LITER (12 inch Flange) Order Code Each

FLASK with 300mm Plane Flange, 100L 6473-09 14341.21
HEAD, Domed, with Eight Openings 6530-45 2562.18
GLASS CAP, 100mm 15312-33 107.78
CAPFE O‑Ring, 100mm 7855-880 28.63
GASKET, PTFE 6525-51 326.26
SOCKET 1/2 inch 6525-61 10.69
CLAMP, Drain Seal, 1 inch 8856-07 112.13
CLAMP, Drain Seal, 2 inch 8856-11 150.55
SWEEP ELBOW, 60º, 1 inch BP 8830-207 65.97
TEMPERATURE MONITORING SYSTEM, Complete 8318-209 1080.10
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm (1) 8093-35 628.06
BEARING, PTFE, 45/50 8067-105 320.08
ADAPTER, #7 – 24/40 5028-30 27.61
ADAPTER, #11 – 45/50 5030-19 62.97
ADAPTER, #15 – 29/42 (2) 5030-42 45.73
ADAPTER, #15 – 45/50 8042-21 50.57
ADAPTER, #11 and #15 – 45/50 5040-96 169.62
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5031-86 119.50
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30
ADAPTER, Offset, 45/50 – 45/50 5268-21 109.58
BUSHING, Nylon, #11 7506-02 11.39
BUSHING, Nylon, #15 (3) 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96
STOPPER, 29/42 (2) 8250-14 25.05
STOPPER, 45/50 (4) 8250-20 44.68
CLAMP, Chain 11079-24 51.23
SUPPORT ROD, 1/2 inch diameter, 12 inch long (2) 11166-37 13.60
COMPLETE 6473-66 32441.89

6559 Low-Profile Pilot Plant

50 Liter Reactor
Flat Head
Jacketed
➧➧Portable 50 liter jacketed

reactor with bottom outlet
➧➧Low profile for walk-in hoods
➧➧Rugged pipe support frame
on casters for mobility
➧➧Also available with domed
head
➧➧Also available with three-
post stand
shields
➧➧Stainless steel flat heads
For heating/cooling
circulators, see
listing starting on
page 240.
6559-10
Order Code Each

50 Liter COMPLETE, Jacketed Flask, with ELECTRIC Motor 6559-10 24683.76
6559 PILOT PLANT REACTOR Low-Profile, 50 Liter Jacketed Flask, F lat Head
Complete cylindrical pilot plant reactor on available. Jacket on flask is direct sealed at top cooling coil, etc. Head is secured to flask with
1‑inch stainless steel pipe, self supporting, and silicone rubber sealed at bottom. 35/25 PTFE gasket and two-piece polymer coupling.
mobile support frame; measures 22 inches O‑Ring ball joint inlet/outletconnections ae In place of flat head, ACE offers a domed glass
wide by 22 inches deep x 68 inches high. Note: sealed tangentially. head with traditional raised joints.
Frame shipped assembled. Bottom padded flask support is adjustable Stirring motor is high powered, 1/2HP
This system has the new low-profile 50L to allow room under flask for various outlet explosion proof motor complete with controller
jacketed flask which has a reduced height vs. configurations. box and with a side drive gear box to save even
the standard 50L flask by 25%. The reactor Unique flat 316 stainless steel head is 0.250 more head space. Stir rod is 28mm (1‑1/8‑inch)
has the same capacity as the standard 50L inches (6.4mm) thick, with seven openings. O.D. precision ground and polished glass shaft
but the shorter frame and flask enable it to fit Head has   45/50 PTFE center joint insert, four with a “pinned” multi-paddle PTFE agitator at
into hoods easier. Jacketed flask has a 300mm  45/50 PTFE joint inserts, and two  29/42 the bottom and a turbine blade PTFE agitator
(12‑inch) opening, flat ground plane flange top. PTFE joint inserts. Stainless steel head has a in the middle of the shaft running through an
Bottom outlet is a flush seal drain valve with PTFE cover. Maximum bolt-tightening torque ACE Tru-Bore bearing.
one-inch beaded pipe outlet. O‑Rings provided of head clamp (cold state) is 30 in-lbs. Motor A J-Kem temperature monitor and 36‑inch
for valve are CAPFE, (silicone encapsulated is secured on an epoxy coated mounting “T” thermocouple is included to give an instant
with PTFE) for excellent chemical resistance. plate over center  45/50 PTFE insert; other readout of vessel temperature. Jacket volume
Flasks with other bottom outlet valves are openings are for condenser, thermoprobe, of flask is 14.25 liters.
50 LITER Order Code Each

FLASK, Jacketed, with 300mm Plane Flange and 2 inch BP Bottom Opening 6543-30 8228.25
HEAD, Flat, Stainless Steel, with 7 openings 6472-26 835.47
FLAT HEAD COVER, 300mm, PTFE 6472-30 219.16
JOINT INSERTS, PTFE – 29/42 (2) 6412-07 90.78
JOINT INSERTS, PTFE – 45/50 (5) 6412-09 111.18
CLAMP, Drain Valve, 1 inch 8856-07 112.13
SWEEP ELBOW, 60°, 1 inch Beaded Pipe 8830-207 65.97
GASKET, PTFE 6525-51 326.26
SOCKET, 1/4 inch 6525-61 10.69
J-KEM TEMPERATURE MONITORING SYSTEM, Complete 12327-03 391.00
PROBE T 36 inch 12180-11 62.00
EXTENSION CORD, 11-foot 12190-11 38.80
1/2 HP ELECTRIC MOTOR 13554-50 2276.62
CONTROLLER 13554-26 1092.92
SIDE DRIVE GEAR BOX 13557-10 651.97
AGITATOR, Lower, PTFE, Multipaddle (178mm) 8091-36 613.84
STIRRING SHAFT, Polished Glass, 28mm, 40 inch Length 8080-12 378.55
BEARING, PTFE, Inner Body, 45/50 8067-55 114.72
GLASS FILLED PTFE BUSHING 8067-58 75.44
GLASS FILLED PTFE LOCK-NUT 8067-60 21.59
SADDLE O-RING 8067-65 30.45
GLASS BODY ONLY, 45/50-36 5030-78 77.88
CONNECTOR, Beam, Connects 5/8-inch Motor Shaft to Chuck 6472-156 54.09
COLLAR, w/PTFE Gasket 8127-28 73.09
ADAPTER, #7 – 29/42 5028-32 32.61
ADAPTER, #11 – 45/50 5030-60 51.58
ADAPTER, #15 – 45/50 8042-21 50.57
ADAPTER, #15 – 45/50, w/4mm PTFE Stopcock 5274-22 117.64
ADAPTER, #11 and #15 – 45/50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30
BUSHING, Nylon, #11 7506-02 11.39
BUSHING, Nylon, #15 (4) 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96
STOPPER, 45/50 (4) 8250-20 44.68
ADAPTER, Offset, 45/50 – 45/50 5268-21 109.58
CLAMP, Chain 11079-24 51.23
CLAMP HOLDER (2) 11081-21 84.80
ROD, 6 inch x 1/2 inch for Temperature Monitor (2) 11166-22 8.36
GREASE, Krytox, GPL 8115-08 59.40
COMPLETE 6559-10 24683.76

6474 Spherical Pilot Plants

50/72/100 Liter Reactors
Domed Head
Unjacketed
➧➧50, 72 & 100 liter reactors with

bottom outlet
mobility
➧➧Adjustable height flask supports
shields

Order Code Each

50-Liter COMPLETE, Unjacketed Flask, with Motor 6474-60 17615.70
72-Liter COMPLETE, Unjacketed Flask, with Motor 6474-64 19224.40 6474-60
100-Liter COMPLETE, Unjacketed Flask, with Motor 6474-68 24262.69
6474 PILOT PLANT REACTOR Spherical, 50/72/100 Liter Unjacketed Flask (8 inch Flange), D
omed Head
Complete spherical pilot plant reactor on Black epoxy coated aluminum flask support and 100 L have 28 mm (1-1/8 inch) O.D. rods,
self-supporting, mobile one‑inch stainless steel plate is adjustable, vertically, to allow room with a “pinned” multi-paddle PTFE agitator
pipe support frame: 50 liter size measures 72 under flask for various outlet configurations. at bottom and a turbine blade PTFE agitator
inches high, 26 inches wide, 26 inches deep; Domed style head has one  45/50 center higher on shaft for grease-free operation with
72 liter size measures 85 inches high, 32 inches joint, two  29/42 side joints and connects 8067 PTFE bearing.
wide, 32 inches deep; 100 liter size measures to flask head with 6517 quick release clamp. Cooling coil is 3/8-inch O.D. copper tubing
85 inches high, 40 inches wide, 40 inches deep. Motor is secured on black epoxy coated encapsulated with PTFE; also available in 316
Note: Frame shipped assembled. mounting plate over center  45/50 opening stainless steel or Hastalloy C-276.
Flask opening is 200 mm (8 inches); Schott- on head; other openings are for condenser, A digital temperature control system is
style flange with O‑Ring groove as center neck thermoprobe, cooling coil, etc. supplied to control heating mantles. This prevents
(supplied with 7855-884 CAPFE O‑Ring); three Stirring motor is a heavy duty, 1/4 HP (50 L over-heating and overshoot, and gives an
 45/50 side necks on all capacities. Bottom and 72 L), 1/2 HP (100 L) electric motor for instant readout of temperature.
outlet is a 0-20 mm adjustable opening threaded hazardous area duty. Motor shaft is 5/8 inch
valve on all sizes. O‑Rings supplied on valves O.D. Controller operates on 120 volts, 50/60 Hz.
are Chemraz (PTFE elastomeric material) for (Air motor available, call for quotation).
excellent chemical resistance. Other bottom Precision ground and polished glass stirring
outlet valves available, contact Ace for options. shaft: 50 L Reactor has a 19 mm O.D. rod; 72 L
50 LITER 72 LITER 100 LITER

(8 inch I.D. Flange) (8 inch I.D. Flange) (8 inch I.D. Flange)
Order Code Each Order Code Each Order Code Each
FLASK, with Side Necks and Bottom Valve 6530-10 2917.90 6530-17 2883.44 6530-23 5066.97
HEAD, 45/50 Center Neck, 29/42 Side Necks 6530-33 594.98 6530-33 594.98 6530-33 594.98
CLAMP, Quick Release 6517-31 145.09 6517-31 145.09 6517-31 145.09
MANTLE, Bottom, Low Profile, w/Twist-Lock Connector 12050-41 813.52 12050-43 1121.28 12050-45 1586.14
(Wattage-Voltage) (370w-115v) (1300w-230v) (1600w-230v)
MANTLE, Girdle, Low Profile, w/Twist-Lock Connector 12041-40 1394.13 12041-42 1771.47 12041-44 2335.70
(Wattage-Voltage) (1-1200w-115v) (2-1800w-230v) (3-1400w-230v)
SUPPORT ASSEMBLY, Complete 6474-370 2793.00 6474-371 3021.00 6474-372 3534.01
TEMPERATURE CONTROL SYSTEM, Complete 6472-73 2908.50 6472-75 2908.50 6472-75 2908.50
STIRRING MOTOR AND CONTROLLER, 1/4 HP 13554-45 2670.40 13554-45 2670.40 — —
STIRRING MOTOR AND CONTROLLER, 1/2 HP — — — — 13554-55 3369.54
AGITATOR, Lower, PTFE, Multipaddle, 140mm 8091-26 318.61 — — — —
AGITATOR, Lower, PTFE, Multipaddle, 140mm — — 8091-34 616.11 8091-34 616.11
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 140mm — — — — 8093-25 583.27
STIRRING SHAFT, Polished Glass, 19mm 8076-45 290.38 — — — —
STIRRING SHAFT, Polished Glass, 28mm — — 8080-14 402.64 8080-14 402.64
BEARING, PTFE, 45/50 8067-30 269.05 8067-105 320.08 8067-105 320.08
CHUCK, “Flex-Grip,” 19mm 8124-23 152.25 — — — —
CONNECTOR, Beam, Connects 5/8 inch Motor Shaft to Chuck — — 6472-156 54.09 6472-156 54.09
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft — — 6472-157 89.89 6472-157 89.89
COLLAR, with PTFE Gasket 8127-20 36.68 8127-28 73.09 8127-28 73.09
COIL, Cooling/Heating, Copper/PTFE, 3/8 inch 12067-61 892.76 12067-63 995.02 12067-65 1045.32
ADAPTER, #11 – 29/42 (2) 5030-24 44.98 5030-24 44.98 5030-24 44.98
ADAPTER, #15 – 45/50 8042-21 50.57 8042-21 50.57 8042-21 50.57
ADAPTER, #15 – 45/50, with 4mm PTFE Stopcock 5274-22 117.64 5274-22 117.64 5274-22 117.64
ADAPTER, #11 and #15 – 45/50 5031-86 119.50 5031-86 119.50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62 5040-96 169.62 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30 5075-45 123.30 5075-45 123.30
ADAPTER, Offset, 45/50 – 45/50 5268-21 109.58 5268-21 109.58 5268-21 109.58
BUSHING, Nylon, #11 7506-02 11.39 7506-02 11.39 7506-02 11.39
BUSHING, Nylon, #15 (4) 7506-06 12.35 7506-06 12.35 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96 5945-76 382.96 5945-76 382.96
CONDENSER, Cold Finger, 14mm O.D., 625mm 5958-99 92.87 5958-99 92.87 5958-99 92.87
STOPPER, 45/50 (3) 8250-20 44.68 8250-20 44.68 8250-20 44.68
CLAMP, Chain 11079-24 51.23 11079-24 51.23 11079-24 51.23
CLAMP HOLDER, Pilot Plant (2) 11081-21 84.80 11081-21 84.80 11081-21 84.80
SUPPORT ROD, 1/2 inch diameter, 12 inch long (2) 11166-37 11.66 — — — —
SUPPORT ROD, 1/2 inch diameter, 18 inch long (2) — — 11166-25 14.69 11166-25 14.69
END-TO-END CONNECTOR 11175-23 19.87 11175-23 19.87 11175-23 19.87
GREASE, Krytox GPL 8115-08 59.40 8115-08 59.40 8115-08 59.40
COMPLETE 6474-60 17615.70 6474-64 19224.40 6474-68 24262.69

6474 Spherical Pilot Plants

200 Liter Reactor
Domed Head
Unjacketed
➧➧200 liter reactor with bottom

outlet
mobility
shields

or 316 stainless steel. 6474-75
Order Code Each

200 Liter COMPLETE, Unjacketed Flask, with ELECTRIC Motor 6474-75 35282.07
6474 PILOT PLANT REACTOR Spherical, 200 Liter Unjacketed Flask (12 inch Flange), D
omed Head
Complete cylindrical pilot plant reactor on configurations. Upper support brackets Features a 28 mm (1-1/8 inch) O.D.
self-supporting, mobile support frame with supplied to stabilize flask. precision ground and polished glass stirring
one‑inch stainless steel pipe. Measures 90 Head is traditional domed style, with shaft with a “pinned” multi-paddle PTFE
inches high, 42 inches wide, 42 inches deep. seven openings; five  45/50, two  29/42. agitator at bottom and a turbine blade PTFE
Note: Frame shipped assembled. Motor is secured on black epoxy coated agitator higher on shaft for grease-free
Flask opening is 300 mm (12 inch) flat- mounting plate over center   45/50 opening operation with 8067 PTFE bearing.
ground flange. Bottom outlet is a flush seal on head; other openings are for condenser, Cooling coil is 1/2 inch O.D. copper tubing
drain valve with one‑inch beaded drain thermoprobe, cooling coil, etc. Head is encapsulated with PTFE; also available in
discharge. O‑Ring supplied on valve is a secured to flask with PTFE gasket and 316 stainless steel or Hastalloy C-276.
CAPFE (silicone encapsulated with PTFE), plastic coupling. Maximum bolt tightening A digital temperature control system
and Kalrez for excellent chemical resistance. torque for coupling (cold state) is 30 in-lbs. is supplied to control heating mantles. This
Flask has 100mm I.D. side port, angled 45 Stirring motor is heavy duty, 1/2 HP prevents over-heating and overshoot, and gives
degrees. electric motor for hazardous area duty. an instant readout of temperature.
Black epoxy coated aluminum flask Motor shaft is 5/8 inch O.D. Controller
support plate is adjustable, vertically, to operates on 120 volts 50/60 Hz. (Air motor
allow room under flask for various outlet available, call for details.)
200 LITER
(12 inch I.D. Flange)
Order Code Each
FLASK, with Side Necks and 2 inch Beaded Pipe Bottom Opening 6474-29 8410.93
HEAD, Domed, with Seven Openings 6472-23 2379.08
GASKET, PTFE 6525-51 326.26
COUPLING, with inserts and hardware 6525-30 1056.54
WRENCH, Torque, 30 in-lbs 6525-60 144.09
SOCKET, 1/4 inch 6525-61 10.69
SWEEP ELBOW, 60°, 1 inch BP 8830-207 65.97
CAP, 4 inch 15312-33 107.78
O‑Ring, CAPFE, for 4 inch Flange 7855-880 28.63
CLAMP, Quick Release 6517-25 98.23
MANTLE, Bottom, Aluminum, w/hole, 4-2000x-230v, wired w/plugs 12053-78 4360.53
STIRRING MOTOR AND CONTROLLER, 1/2 HP 13554-55 3369.54
BEARING, PTFE, 45/50 8067-105 320.08
COLLAR, w/PTFE Gasket 8127-28 73.09
COIL, Cooling/Heating, Copper/PTFE, 1/2 inch 12067-68 2011.00
ADAPTER, #15 – 29/42 (2) 5030-42 45.73
ADAPTER, #15 – 45/50 8042-21 50.57
ADAPTER, #11 and #15 – 45/50 5031-86 119.50
ADAPTER, Side Arm, 45/50 – 45/50 – 24/40 5040-96 169.62
ADAPTER, Angle, 45/50 – 45/50 5075-45 123.30
ADAPTER, Offset, 45/50 – 45/50 5268-21 109.58
BUSHING, Nylon, #11 7506-02 11.39
BUSHING, Nylon, #15 (4) 7506-06 12.35
CONDENSER, 500mm, 45/50 5945-76 382.96
STOPPER, 45/50 (3) 8250-20 44.68
CLAMP, Chain 11079-24 51.23
SUPPORT ROD,1/2 inch diameter, 18 inch long 11166-25 14.69
END-TO-END CONNECTOR 11175-23 19.87
COMPLETE 6474-75 35282.07

The
Impresario I
Reactor
Controller
New
SPECIFICATIONS (Base Configuration)
6458-10 Impresario I SYSTEM • PC running Windows XP, Windows 7 or higher
REQUIREMENTS: • 250 MB of disk space
• Minimum 1 GB RAM
Reactor Control System
DRIVERS INCLUDED FOR: • Julabo recirculators
Introducing the Impresario I, Ace Glass’s new, • Heidolph and IKA digital stirring motors
expandable reactor control system. The Impresario I SOFTWARE FEATURES: • Configurable emergency stop
controls and monitors various reaction parameters via • Configurable safety alarm actions
an expandable hardware unit and highly configurable • Graph single parameter over time for each
Windows-based software (XP and Windows 7). monitored parameter
The base configuration includes the ability to control • Creates CSV (comma-delimited file) data file
hardware from equipment manufacturers such as PARAMETERS • pH via probe
J‑Kem, Heidolph, IKA, and Julabo. MONITORED: • Stirrer speed
Users also have the option of creating reaction recipes • Stirrer torque
via an easy-to-use graphical interface. • Vacuum/pressure via onboard transducer
(35 psi maximum)
Call Ace today to discuss a quotation for a new • Temperature of circulator oil
reaction system, or for an Impresario I configuration to • Temperature of reaction via probe
work with your existing equipment.
PARAMETERS • Temperature via chiller
CONTROLLED: • Stirring speed
• Pressure and vacuum via proportioning valve
(not included — call for details)
ITEMS • Impresario controller
INCLUDED: • USB cable for connection to PC
• Impresario software
ITEMS • PC not sold by Ace; Netbook is available,
NOT however only the Impresario software is sup-
INCLUDED: ported
• Cables for connection to peripherals
Base system includes Impresario I • Proportioning valve (see Ace 14066 family)
controller, USB cable, and all software • Recirculator, stir motor, vacuum pump, liquid
pump, syringe pump, etc.
and standard drivers. Reactor, • Drivers for equipment other than those listed
recirculator, computer, cables and other above (can be supplied as custom orders)
peripherals must be ordered separately.
10/20L Pilot Plant Packages

A
ce Glass combines our expertise in tion and package. Ace’s glass reactors and
Pilot Plant-Kilo Scale Reactors with Julabo’s Presto series chillers are a perfect
Julabo’s expertise in recirculating combination for your large scale, pilot or
chillers to provide a total, convenient solu- production process needs.
Key Components for Key Components for

10L Pilot Plant System 20L Pilot Plant System
Item Description Order Code Item Description Order Code
10L Jacketed Flask 6524-73 20L Jacketed Flask 6472-16
Domed Head, 7 ports 6530-37 Domed Head, 7 ports 6530-37
Stainless Steel Stand 6472-329 Bottom Drain Valve 6472-245
Digital Stirring Motor 13504-41 Drain Valve Clamp 1-inch 8856-07
PTFE Agitator (Lower) 8091-10 Drain Valve Clamp 2-inch 8856-11
PTFE Agitator (Upper) 8093-12 Stainless Steel Stand 6472-329
Stirring Shaft, 19mm 8076-43 Digital Stirring Motor 13504-41
Condenser, 300mm, 29/42 5945-24 PTFE Agitator (Lower) 8091-10
Julabo LH85 Circulator 12262-38 PTFE Agitator (Upper) 8093-12
Hose Clamps (2) 13010-01 Stirring Shaft, 19mm 8076-40
Julabo Hoses (2) 12677-15 Condenser, 300mm, 24/40 5946-18
Julabo PT100 Sensor 12307-44 Julabo LH85 Circulator 12262-38
Julabo 2L Expansion Tank 12497-02 Hose Clamps (2) 13010-01
Julabo Hoses (2) 12677-15
Julabo PT100 Sensor 12307-48
Julabo 2L Expansion Tank 12497-02
$
47578.28
Complete 10L System
Order Code: 10000-10
$
50807.50
Complete 20L System
Order Code: 10000-20

30/50L Pilot Plant Packages

Key Components for
$
66708. 99 30L Pilot Plant System
Complete 30L System Item Description
30L Jacketed Flask
Order Code
6472-030
Order Code: 10000-30 Domed Head, 8 ports 6530-45
PTFE Head Gasket, 300mm 6525-51
$
68328.91 Bottom Drain Valve
Drain Valve Clamp 1-inch
Drain Valve Clamp 2-inch
6472-245
8856-07
8856-11
Complete 50L System Three-Post Stand 6473-51
Order Code: 10000-50 Stirring Motor, 1/2-HP XP 13554-50
Motor Controller 13554-26
PTFE Agitator (Lower) 8091-36
PTFE Agitator (Upper) 8093-35
Stirring Shaft, 28mm 8080-14
Connect Beam Coupling 6472-156
Chuck, 28mm 6472-157
Condenser, 500mm 5945-76
Condenser, Cold Finger 5958-99
Julabo LH50 Circulator 12262-40
Hose Clamps (2) 13010-01
Key Components for

50L Pilot Plant System
Item Description Order Code
50L Jacketed Flask 6472-050
Domed Head, 8 ports 6530-45
PTFE Head Gasket, 300mm 6525-51
Bottom Drain Valve 6472-245
Drain Valve Clamp 1-inch 8856-07
Drain Valve Clamp 2-inch 8856-11
Three-Post Stand 6473-51
Stirring Motor, 1/2-HP XP 13554-50
Motor Controller 13554-26
PTFE Agitator (Lower) 8091-36
PTFE Agitator (Upper) 8093-35
Stirring Shaft, 28mm 8080-18
Connect Beam Coupling 6472-156
Chuck, 28mm 6472-157
Condenser, 500mm 5945-76
Condenser, Cold Finger 5958-99
Julabo LH50 Circulator 12262-40
Hose Clamps (2) 13010-01
Reactors/Large-Scale Filter Reactors 91
Process Scale
Filtration Apparatus
and Filter Reactors
Ace Glass fabricates bench scale filtration
apparatus and reactors as standard products.
ACE also fabricates kilo scale filter reactors such
as the one pictured here.
ACE has produced units from 150mL up to as

large as 200L custom units. ACE has typically
produced 20L, 30L and 50L filter apparatus as
well for various applications such as Nutsche
filters, etc. All filter reactors are built on corrosion
resistant stainless steel stands with locking, rolling
casters for portability. All borosilicate heavy-wall
glass bodies with either glass or PTFE bottom
units. Many bottom and side outlet valve styles
are available such as our flush seal or ZDS valves.
Various agitator styles exist in either stainless steel
or PTFE and custom fabrication is possible. Glass
vessels can be standard single wall or jacketed
double wall. Heads can be stainless steel or glass
domed or flat head style.
Filter apparatus stands can be fabricated from

anodized aluminum or stainless steel with
powder coated components. Various sizes and
types of stir motors are available, including UL
classified Hazardous duty motors that meet
either; Class I, Div 1, Group D and Class II, Div
I, Group F&G atmospheres.

92 Components / Flasks
ZDS™ Valve Easy Action

Bottom Valve
Flush Seal Beaded
Valve Types
for
Reaction Flasks
Sink Type Piston Type
Easy Action Bottom Valve Piston Type Valve

Flask has Easy Action Plug bottom outlet with Chemraz® o‑rings Flask has 35/25 or 28/15 o‑ring ball joint on outlet and utilizes a sealed‑in
for draining contents. Bottom outlet has size 35/25 o‑ring ball joint threaded stopcock assembly that rotates CLOSED into the bottom of
connection. Supplied with one 7855‑884 CAPFE o‑ring (PTFE the flask thereby offering nearly zero dead space. Turn stopcock handle
encapsulated silicone o‑ring). Plain silicone o‑rings also available. counterclockwise and piston plunger retracts to allow contents to
drain. Drain opening is approximately 15mm. Piston plunger supplied
Sink Type Valve with FETFE o‑rings (two 7855‑726, one 7855‑721); Chemraz® o‑rings
Flask is fabricated with a #36 Ace‑Thred on bottom. The all‑PTFE valve can be offered as replacements.
is inserted into the Ace‑Thred. A stainless steel handle is then secured
to the drain tube. By rotating the handle, plug rises into the flask and Beaded
contents drain through three (3) 1/2 inch wide x 1-1/2 inch long slit Flask is supplied with a one-inch beaded pipe‑type flange extension off
openings. Rotate handle in opposite direction and plug seals at bottom bottom for connection to a 0–20 mm threaded PTFE stopcock as the
of flask, with NO dead space. Supplied with two Chemraz® o‑rings: one outlet. Stopcock assembly has a mating one-inch beaded flange that
7859‑540, to secure valve in #36 Ace‑Thred; the other, 7859‑542, on connects to extension off bottom via a Viton lined coupling. Takeoff on
bottom of plug to make seal at bottom of flask. stopcock is one-inch O.D. tubing. Drain assembly plug supplied with
FETFE o‑rings; Chemraz® o‑rings can be offered as replacements. ACE
ZDS™ Valve can supply the takeoff with beaded flange, Ace‑Thred, hose connection,
Flask has new Zero Dead Space (ZDS™) valve. When in the full open etc.; call or email for quotation.
position, the ZDS™ valve allows for complete product drainage, and has
no “hang-up” where material can be trapped or suspended. The product Flush Seal Valve
drains through openings in the valve stem, and will completely empty — Flask is fabricated with a two-inch beaded valve seat, for 30L and 50L.
including dissolved and small, solid particles. When closed, the valve The plug, with a CAPFE o‑ring, is inserted into valve seat and s ecures
plug seals flush to the bottom of the flask. The valve is available in two within a coupling. By rotating the handle, plug rises into the flask and
standard sizes. All wetted parts are borosilicate glass or inert PTFE. seals to afford zero dead space. Back thread out to drain through
The PTFE plug stem o‑rings are made from Chemraz®, so the valve can one‑inch beaded pipe angled side port. Supplied with CAPFE o‑ring for
handle almost any type of material or chemical. seal at flask, two Kalrez o‑rings supplied on valve stem. Other o‑ring
materials available.
Components / Flasks 93
6472 FLASK Reaction, Pilot Plant, Cylindrical, with Piston Type Drain
Similar to flask supplied with 6472 pilot plant reactor systems except this flask has a
bottom outlet with o‑ring ball joint and utilizes a sealed-in threaded PTFE stopcock
assembly that rotates CLOSED into the bottom of the flask thereby offering nearly zero
dead space. Turn stopcock handle counterclockwise and piston plunger retracts to
allow contents to drain. Drain opening is approximately 15mm. Piston plunger supplied
with FETFE o‑rings (two 7855-726, one 7855-721); Chemraz® o‑rings can be offered as
replacements. Offered as flask only with drain assembly. Can also be substituted for
outlets on 6473 or 6474 assemblies, call for details.
FLASK with Drain Assembly, ONLY
Capacity, Liters O‑Ring Ball Joint Size Order Code Each
10 28/15 6472-39 2236.22
20 28/15 6472-45 Call 6472-41
30 35/25 6472-40 2483.33
50 35/25 6472-41 2694.33
6472 FLASK Reaction, Pilot Plant, Cylindrical, with Sink Type Drain
sink type drain assembly as a bottom outlet. Flask is fabricated with a #36 Ace‑Thred
on bottom. The all-PTFE valve is inserted into the Ace‑Thred. A stainless steel handle
is then secured to the drain tube. By rotating the handle, plug rises into the flask and
contents drain through three (3) 1/2-inch wide x 1-1/2-inch long slit openings. Rotate
handle in opposite direction and plug seals at bottom of flask, with NO dead space.
Supplied with two Chemraz® o‑rings: one 7859-540, to secure valve in #36 Ace‑Thred; the
other, 7859‑542, on bottom of plug to make seal at bottom of flask. Offered as flask with
thread only, drain assembly only, or flask with drain assembly. Can also be substituted
for outlets on 6473 or 6474 assemblies, call for details.
FLASK, with SINK DRAIN FLASK COMPLETE

Thread, only ASSEMBLY, only w/SINK DRAIN ASSY.
Cap., Order Cap., Order Cap., Order
Liters Code Each Liters Code Each Liters Code Each
10 6472-64 2079.57 10 6472-69 845.27 10 6472-164 2924.84 6472-66
20 6472-68 Call 20 6472-69 845.27 20 6472-163 Call
30 6472-65 2396.10 30 6472-69 845.27 30 6472-165 3241.37
50 6472-66 2861.39 50 6472-69 845.27 50 6472-166 3706.66
6472 FLASK Reaction, Pilot Plant, Cylindrical,

with Beaded Drain Assembly
Similar to flask supplied with 6472 pilot plant reactor systems except this flask is
supplied with a 1-inch beaded pipe-type flange extension off bottom for connection to
a 0–20 mm threaded PTFE stopcock as the outlet. Stopcock assembly has a mating
1-inch beaded flange that connects to extension off bottom via a Viton lined coupling.
Takeoff on stopcock is 1-inch O.D. tubing. Drain assembly plug supplied with FETFE
o‑rings; Chemraz® o‑rings can be offered as replacements. ACE can supply the takeoff
with beaded flange, Ace‑Thred, hose connection, etc.; phone for quotation. Listed as
flask with beaded pipe extension only, drain assembly only (includes 0–20 plug plus glass 6472-98
thread with mating beaded pipe) or flask with drain assembly. Order coupling separately.
Can also be substituted for outlets on 6473 or 6474 assemblies, call for details.
FLASK, with BEADED VALVE FLASK COMPLETE 8856-07

Bead, only ASSEMBLY, only w/BEADED VALVE ASSEM. 6472-99
Cap., Order Cap., Order Cap., Order
Liters Code Each Liters Code Each Liters Code Each
10 6472-96 2061.34 10 6472-99 418.62 10 6472-196 2592.09
20 6472-94 Call 20 6472-99 418.62 20 6472-195 Call
30 6472-97 2352.39 30 6472-99 418.62 30 6472-197 2883.14
50 6472-98 2799.44 50 6472-99 418.62 50 6472-198 3330.19
Coupling, only 8856-07 112.13

6472 FLASK Reaction, Pilot Plant, Cylindrical, with

Flush Seal Drain Assembly
Martin-style flush seal drain assembly as a bottom outlet. Flask is fabricated with a 2-inch
beaded valve seat, for 30L and 50L. The plug with a CAPFE o‑ring is inserted into valve
seat and secures within a coupling. By rotating the handle, plug rises into the flask and
seals to afford zero dead space. Back thread out to drain through 1-inch beaded pipe
angled side port. Supplied with CAPFE o‑ring for seal at flask, two Kalrez o‑rings supplied
on valve stem. Other o‑ring materials are available. Offered as flask with valve seat only,
drain assembly only, or flask with drain assembly. Can also be substituted for outlets on
8856-11 6473 or 6474 assemblies, call for details.
FLASK, with FLUSH SEAL DRAIN FLASK COMPLETE

Bead, only ASSEMBLY, only w/FLUSH SEAL DRAIN ASSEM.
Cap., Order Cap., Order Cap.,
6472-242 Liters Code Each Liters Code Each Liters Order Code Each
20 6472-02 2242.57 20 6472-245 1010.52 20 6472-247 2,250.00
30 6472-241 2325.19 30 6472-245 1010.52 30 6472-248 3486.26
50 6472-242 2772.68 50 6472-245 1010.52 50 6472-249 3933.75
Coupling, only 8856-11 150.55
6482 VALVE ASSEMBLY PTFE, Flush Seal, with Top Pin

New Redesigned flush-seal type valve similar to 6472-245 except that the top of the valve has
a 1-1/2-inch x 3/8-inch O.D. pin that extends upward. The pin fits into the receptacle on
the bottom of the 8100 and 8101 bottom agitators. This assembly is designed to reduce
shaft wobble or “flexing” on the larger reactors. Top opening is 2-inch beaded pipe and
the side drain port is 1-inch beaded pipe. Uses 8856-11 clamp.
Order Code Each
Complete Valve Assembly 6482-20 1032.42
6482
S INN O Necks, Heavy Wall, with ZDS™ Valve

6483 AS Three
6483 LFLASK V
Heavy wall, round-bottom flask with three  24/40 vertical necks and ZDS™ valve
G
AT
attached. Other  neck

TH joint sizes are available as special orders. Bottom outlet is Zero
ACE
Dead Space (ZDS) valve.

ON
Neck
Capacity,
A N N Nominal
I V E R S Nominal
A R Y Height, Height, Center Side Bottom Order
A Liters O.D., mm I.D., mm
1936 2011 mm (A) mm Neck Necks Outlet, mm Code Each
1 125 115 180 100 24/40 24/40 0-10 6483-110 306.44
J
2I 160 150 250 100 24/40 24/40 0-10 6483-112 364.07

V
3 N E 180
N
LAN D166, 270 100 24/40 24/40 0-10 6483-120 421.27
6475 FLASK Reaction, Jacketed, Conical 4-Inch Flange

Jacketed cylindrical flask with conical neck opening of four inches (100mm). Inlet and
outlet connections are size 28/15 o‑ring ball joints, both sealed tangentially, one at top 6475
and one at bottom of jacketed section. See 6495 for gaskets, 6496 for clamp.
Capacity, O.D., I.D., Height, Top PTFE Order
mL mm mm mm (A) Gasket Code Each
1000 150 104 235 6495-10 6475-10 476.88 A
1500 150 104 245 6495-10 6475-15 499.04
2000 150 104 335 6495-10 6475-20 544.80
3000 150 104 415 6495-10 6475-25 648.09
6476 FLASK Reaction, Conical 4-Inch Flange

Rugged cylindrical flask with conical neck opening of four inches (100mm). Uses 6496 clamp
for securing flask head to flask. See 6495 for gaskets.
Capacity, O.D., I.D., Height, Top PTFE Order 6476
mL mm mm mm (A) Gasket Code Each A
500 114 104 120 6495-10 6476-05 128.36
1000 114 104 180 6495-10 6476-10 137.05
1500 114 104 220 6495-10 6476-15 154.46
2000 114 104 260 6495-10 6476-20 155.51
3000 114 104 340 6495-10 6476-25 159.36
6477 FLASK Reaction, with Indents, Conical 4-Inch Flange

Same as 6476, except with side indents for improved stirring characteristics. Not suitable
for vacuum operation. Uses 6496 clamp for securing conical flask head to flask. See
6495 for gaskets.
6477
Capacity, O.D., I.D., Height, Top PTFE
mL mm mm mm (A) Gasket Order Code Each
500 114 104 120 6495-10 6477-05 156.51 A
1000 114 104 180 6495-10 6477-10 173.24
ted
Inden
1500 114 104 220 6495-10 6477-15 181.90
2000 114 104 260 6495-10 6477-20 196.99
3000 114 104 340 6495-10 6477-25 222.36
New
6479 FLASK Reaction, Conical 4-Inch Flange
Rugged spherical flask with conical neck opening of 4-inches (100mm). Standard size
flasks use regular Glas-Col heating mantles of equivalent capacity. Length of straight
section including flange, approximately 95mm (3-3/4 inches). Uses 6496 clamp for 6479
securing flask head to flask. See 6495 for gaskets.
Neck A
Capacity, Nominal Nominal Height, Height, Order
Liters O.D., mm I.D., mm mm (A) mm Code Each
3 180 166 270 100 6479-05 181.94
5 225 212 320 100 6479-10 210.00
12 285 270 380 100 6479-15 334.21
22 350 336 450 100 6479-20 557.04
50 457 461 550 100 6479-25 1682.00
72 508 496 570 100 6479-30 1555.59

6540 FLASK Reaction, Spherical, with ZDS™ Valve

Heavy wall spherical reaction flask with Schott-Duran style flat grooved flange opening.
Flask uses 6517 quick release clamp. Takes all Schott-Duran style heads. Flask comes
with one CAPFE o‑ring. Bottom outlet is Zero Dead Space (ZDS) valve.
A Neck Flange Bottom
Capacity, Nominal Nominal Height, Height, I.D., Outlet, Top CAPFE Order
Liters O.D., mm I.D., mm mm (A) mm mm (In.) mm O‑Ring Code Each
2 160 150 250 100 100 (4) 0-10 7855-880 6540-104 548.09
3 180 166 270 100 100 (4) 0-20 7855-880 6540-106 604.15
5 226 212 320 100 100 (4) 0-20 7855-880 6540-108 616.61
5 226 212 320 100 150 (6) 0-20 7855-881 6540-110 819.38
12 285 270 380 100 150 (6) 0-20 7855-881 6540-115 1107.41
22 350 336 450 100 150 (6) 0-20 7855-881 6540-120 1538.40
6540
6469 FLASK Reaction, 4-Neck, Spherical, with Bottom Outlet,

Conical 4-inch Flange
Spherical reaction flask with flat, ground conical style flange with o‑ring groove and
bottom outlet. Supplied with capacity reference gradations. Nominal flange I.D. is 100mm
(4 inches). With three side ports: one #7 Ace‑Thred and two  45/50 outer joints. Bottom
outlet is  28/15 spherical ball joint. Each flask is supplied with one 7855-880 CAPFE
(PTFE encapsulated silicone) o‑ring.
Neck Flange
A Capacity, Nominal Nominal Height, Height, I.D., Order
Liters O.D., mm I.D., mm mm (A) mm mm (In.) Code Each
12 285 270 380 100 100 (4) 6469-16 763.28
22 350 336 450 100 100 (4) 6469-18 1062.02
6469-16
6474 FLASK Reaction, Spherical, 100mm Side Port, with Bottom Outlet
Spherical reaction flask with flat, ground KF flange and bottom outlet. Supplied with
capacity reference gradations. Nominal flange I.D. is 300mm (12 inches). Side sample port
A is angled at 45° (Schott-Duran style flange 2.5 inches in diameter). Main flange opening
uses 6525-30 clamp and 6525-51 gasket. Each flask is supplied with one 7855-880
CAPFE (PTFE encapsulated silicone) o‑ring for side port.
Neck Flange Bottom
Capacity, Nominal Nominal Height, Height, Nominal Outlet
Liters O.D., mm I.D., mm mm (A) mm I.D., mm Style Order Code Each
200 750 736 960 210 300 0-20mm 6474-16 8521.67
200 750 736 960 210 300 Piston 6474-18 8521.67
200 750 736 960 210 300 Sink 6474-23 8521.67
200 750 736 960 210 300 Beaded 6474-25 8399.85
200 750 736 960 210 300 Flush 6474-29 8410.93
Glass Cap for Side Port, 100mm 15312-33 107.78
CAPFE O‑Ring for Side Port, 100mm 7855-880 28.63
Gasket for Main Flange, 300mm 6525-51 326.26
6474-29
Clamp for Main Flange, 300mm 6525-30 1056.54
Clamp for Side Port, 60mm, quick release 6517-22 87.08
6480 FLASK Reaction, Jacketed, Conical 4-Inch Flange

Spherical flask with conical neck opening of 4 inches (100mm). Inlet and outlet
connections are size 28/15 o‑ring ball joints, both sealed tangentially, on jacketed 6480
section. Uses 6496 clamp for securing flask head to flask. See 6495 for gaskets.
Capacity, Nominal Nominal Height, Neck Height, Order
A
3 220 170 370 95 6480-05 703.82
5 285 211 450 95 6480-10 1055.60
6481 FLASK Reaction, with Indents, Conical 4-Inch Flange

Same as 6479, except with side indents for improved stirring characteristics. Not suitable New
for vacuum operation. Uses 6496 clamp for securing conical flask head to flask. See
6495 for gaskets.
Capacity, Nominal Nominal Height, Neck Height, Order
3 180 166 270 100 6481-05 249.01
5 226 212 320 100 6481-10 292.80 A 6481
12 285 270 380 100 6481-15 490.01
ted
Inden
6491 REACTION FLASK Conical 4-Inch Flange

With 4mm bore stopcock for rapid removal of contents without disturbing the general
arrangement of the apparatus. Conical neck opening is 100mm (4-inches). Use 6496
clamp for securing head to flask. See 6495 for gaskets.
Capacity, O.D., I.D., Height, Top PTFE A
Liters mm mm mm (A) Gasket Order Code Each
1 114 104 180 6495-10 6491-10 266.46
2 114 104 260 6495-10 6491-20 279.54
6491

6492 REACTION FLASK Conical 4-Inch Flange

With 4mm bore stopcock. Stopcock is separated from lower section by  28/15 joint.
Otherwise, identical to 6491. For bottom joint clamp, order 7669-12. Use 6496 Clamp
A for securing head to flask. See 6495 for gaskets.
Flask, only Stopcock, only Complete

Capacity, O.D., I.D., Height, Order Order Order
Liters mm mm mm (A) Code Each Code Each Code Each
6492 1 114 104 220 6492-02 173.95 6492-10 117.28 6492-15 291.23
2 114 104 300 6492-06 194.10 6492-10 117.28 6492-25 311.38
6511 FLASK Reaction, Flat Flange

Cylindrical, heavy-wall reaction flask, round bottom, with flat, ground flange. Without
constriction at top to facilitate introduction/removal of material and allow for ease of
cleaning. For reaction heads, see 6512, 6513 and 6515. For clamp, see 6508 or 6510.
Capacity, O.D., I.D., Height, Flange Top FETFE Order
A Liters mm mm mm (A) O.D., mm Gasket Code Each
1 110 100 165 137 6495-21 6511-06 156.21
2 140 130 185 168 6495-23 6511-08 188.86
3 140 130 260 168 6495-23 6511-10 207.26
4 140 130 335 168 6495-23 6511-12 233.67
6511-06
6511 FLASK Reaction, Flat Flange, with O‑Ring Groove

Cylindrical, heavy-wall reaction flask, round bottom. Top has flat flange with an o‑ring
groove for use with CAPFE® (PTFE encapsulated silicone rubber) o‑ring instead of gasket.
Without constriction at top to facilitate introduction/removal of material and allow for
ease of cleaning. For reaction heads, see 6512, 6513 and 6515. Flask is supplied with
one CAPFE o‑ring. For clamp, see 6508 or 6510.
A
Capacity, O.D., I.D., Height, Flange Top CAPFE Order
Liters mm mm mm (A) O.D., mm O‑Ring Code Each
1 110 100 165 137 7855-887 6511-42 183.81
2 140 130 185 168 7855-889 6511-45 224.38
6511-42 3 140 130 260 168 7855-889 6511-47 236.37
4 140 130 335 168 7855-889 6511-49 269.10
6511 FLASK Reaction, Flat Flange

Cylindrical heavy wall reaction flask, with flat bottom rounded into side wall, and flat,
ground flange top. Without constriction at top to facilitate introduction/removal of material
6511-24 and allow for ease of cleaning. For reaction heads, see 6512, 6513 and 6515. For clamp,
see 6508 or 6510.
Capacity, O.D., I.D., Height, Flange Top PTFE Order
A Liters mm mm mm (A) O.D., mm Gasket Code Each
1 110 100 165 137 6495-21 6511-24 158.45
2 140 130 185 168 6495-23 6511-27 188.31
3 140 130 260 168 6495-23 6511-29 208.78
4 140 130 335 168 6495-23 6511-31 233.67
6511 FLASK Reaction, Flat Flange, with O‑Ring Groove

Cylindrical heavy-wall reaction flask, with flat bottom rounded inside wall, and flat flange.
Flange has an o‑ring groove for use with CAPFE® (PTFE encapsulated silicone rubber)
o‑ring instead of gasket. Without constriction at top to facilitate introduction/removal of 6511-53
material and allow for ease of cleaning. For reaction heads, see 6512, 6513 and 6515.
Flask is supplied with one CAPFE o‑ring. For clamp, see 6508 or 6510. A
Capacity, O.D., I.D., Height, Flange Top CAPFE
Liters mm mm mm (A) O.D., mm O‑Ring Order Code Each
1 110 100 165 137 7855-887 6511-53 187.54
2 140 130 185 168 7855-889 6511-56 223.88
3 140 130 260 168 7855-889 6511-58 245.25
4 140 130 335 168 7855-889 6511-60 273.13
6516 FLASK Reaction, with Indents, Flat Flange

Cylindrical heavy wall reaction flask, with flat bottom rounded into side wall, and flat,
ground flat flange. Without constriction at top to facilitate introduction/removal of material
and allow for ease of cleaning. Indented sides for better mixing. For reaction heads, see
6512, 6513 and 6515. For clamp, see 6508 or 6510. 6516
Capacity, O.D., I.D., Height, Flange Top PTFE Order

Liters mm mm mm (A) O.D., mm Gasket Code Each A
1 110 100 165 137 6495-21 6516-01 190.13
ted
Inden
2 140 130 185 168 6495-23 6516-03 225.99
3 140 130 260 168 6495-23 6516-05 246.85
4 140 130 335 168 6495-23 6516-07 280.21
New
6518 FLASK Reaction, Cylindrical, with ZDS™ Valve
Cylindrical, heavy wall flask with round bottom. Flask has Schott-Duran style top flange
supplied with o‑ring groove for use with heads 6433, 6527, 6528 or 6529. Comes with
one CAPFE o‑ring (silicone optional). Bottom outlet is ZDS™ (Zero Dead Space) PTFE
valve with Chemraz o‑rings. Uses 6517 quick release clamp.
A
Capacity, O.D., I.D., Height, Flange Size. Bottom Top Order
mL mm mm mm (A) mm (in.) Outlet, mm O‑Ring Code Each
1000 110 100 180 100 (4) 0-10 7855-880 6518-10 538.44
2000 110 100 265 100 (4) 0-10 7855-880 6518-12 622.60
2000 155 145 200 150 (6) 0-20 7855-881 6518-14 627.86
3000 110 100 400 100 (4) 0-10 7855-880 6518-16 644.69
3000 150 140 250 150 (6) 0-20 7855-881 6518-18 651.37 6518
4000 155 145 300 150 (6) 0-20 7855-881 6518-20 758.94

6519 FLASK Reaction, Jacketed, Flat Flange, with O‑Ring Groove

Cylindrical, heavy-wall reaction flask, except flat flange has an o‑ring groove for use
with CAPFE® (PTFE encapsulated silicone rubber) o‑ring instead of gasket. Without
6519 constriction at top to facilitate introduction/removal of material and allow for ease of
cleaning. Flat bottom rounded into side wall. For reaction heads, see 6512, 6513 and
6515. Flask is supplied with one CAPFE o‑ring. For clamp, see 6510. For replacement
o‑rings, see 7855. With 28/15 o‑ring ball joints for easy connect/disconnect from hoses.
A
Capacity, O.D., I.D., Height, Flange Top CAPFE Order
Liters mm mm mm (A) O.D., mm O‑Ring Code Each
1 140 100 165 137 7855-887 6519-01 605.60
2 170 130 185 168 7855-889 6519-02 633.13
3 170 130 260 168 7855-889 6519-03 660.66
4 170 130 335 168 7855-889 6519-04 770.76
6521 FLASK Reaction, Cylindrical, Schott-Duran Flange

Rugged cylindrical reaction flask with Schott-Duran style ground flange with o‑ring groove,
for use with 6517 quick release clamp. Ten liter and larger are supplied with capacity
reference graduations. Each flask is supplied with one CAPFE (PTFE encapsulated silicone)
o‑ring. Plain silicone o‑rings are also available. For reaction heads, see 6528 or 6530. For
cooling/heating coils, see 12067. Thirty (30) liter and above have reduced area to flange.
Capacity, O.D., I.D., Height, Flange I.D., Use Top CAPFE
Liters mm mm mm (A) mm (In.) Clamp O‑Ring Order Code Each
A 1 110 100 180 100 (4) 6517-25 7855-880 6521-10 152.00
2 110 100 265 100 (4) 6517-25 7855-880 6521-12 161.73
3 110 100 400 100 (4) 6517-25 7855-880 6521-14 180.95
6 215 205 280 200 (8) 6517-31 7855-884 6521-16 846.55
10 215 205 470 200 (8) 6517-31 7855-884 6521-20 1189.70
15 250 236 470 200 (8) 6517-31 7855-884 6521-25 1463.07
20 250 236 570 200 (8) 6517-31 7855-884 6521-27 1636.17
30 315 300 540 200 (8) 6517-31 7855-884 6521-30 1736.55
50 315 300 890 200 (8) 6517-31 7855-884 6521-35 2194.61
100 457 443 940 200 (8) 6517-31 7855-884 6521-40 Priced
6521 200 450 436 1575 200 (8) 6517-31 7855-884 6521-44 upon request
6526 FLASK Reaction, Cylindrical, Indented Style

Rugged cylindrical reaction flask with Schott-Duran style flat flange with o‑ring groove,
for use with 6517 quick release clamp but with indents for greater agitation. Each flask
is supplied with one CAPFE o‑ring (PTFE encapsulated silicone o‑ring). Plain silicone
6526 12067. NOT suitable for vacuum or pressure operation. Uses 6517-25 quick release clamp.
Capacity, O.D., I.D., Height, Flange Size. Top Order
A Liters mm mm mm (A) mm (in.) O‑Ring Code Each
1 110 100 180 100 (4) 7855-880 6526-10 200.17
2 110 100 265 100 (4) 7855-880 6526-12 223.10
ted
Inden
New
6630 REACTION ASSEMBLY Spherical, 8-inch Schott-Duran Flange

Spherical reaction flask with 200mm (8-inch) Schott-Duran style flange with o‑ring groove
as center neck and three (3)  45/50 side necks. Large center neck affords easy clean-out
and allows insertion of a heat exchange coil, 12067. Use 6530 head on center neck and
secure head to flask with 6517 quick release clamp. Flask is supplied with one 7855-288
silicone rubber o‑ring. For replacement, use silicone o‑ring or CAPFE o‑ring. Also listed
are a low-profile, aluminum-housed heating mantle for bottom and a removable fabric
(girdle) mantle for the sides.
50 Liter 72 Liter 100 Liter
Order Order Order
Code Each Code Each Code Each
Flask, 200mm Flange,
8-inch Center Neck and
(3) 45/50 Side Necks 6530-08 2807.79 6530-15 2643.93 6530-20 4893.78
Head, only, 45/50 6530-32 425.01 6530-32 425.01 6530-32 425.01
Clamp, only 6517-31 145.09 6517-31 145.09 6517-31 145.09
Coil, Cooling,
Copper/PTFE, 1/2-inch 12067-71 1110.49 12067-71 1110.49 12067-84 1446.60
Mantle, Bottom,
Low-Profile 12050-34 909.03 12050-36 1530.57 12050-38 2044.00
(Wattage) (1000w-115v) (1300w-230v) (1600w-230v)
Mantle, Girdle 12041-40 1394.13 12041-42 1771.47 12041-44 2335.70
(Wattage) (2-1200w-115v) (2-1800w-230v) (2-2200w-230v) 6630
Complete 6630-10 Call 6630-20 Call 6630-30 Call
6495 GASKET PTFE
PTFE gaskets, white in color, for mating ground flange surfaces on reactor flasks and
matching heads. Can be used with all conical style and flat flange style flask and heads.
PTFE makes a leak-free seal with slight clamp pressure. They also provide the added 6495-10
chemical resistance and purity of PTFE.
Thickness, O.D., Inches Fits Flask Order
inches/mm (mm) Size, mL Grooved Code Each
6495-21
0.03/0.8 5.250 (133.4) 500-3000mL No 6495-10 11.28
0.03/0.8 5.375 (136.7) 500-1000mL Yes 6495-21 60.28
0.03/0.8 6.625 (168.4) 2000-4000mL Yes 6495-23 64.15
6495 GASKET FETFE
ACE FETFE gaskets, black in color, for mating ground flange surfaces on reactor flasks
and matching heads. Can be used with all conical style and flat flange style flask and
heads. FETFE makes a leak-free seal with clamp pressure. FETFE is an exclusive
ACE product made from TFE impregnated fluoroelastomers with good chemical and 6495-43
temperature resistance.
0.02/0.5 5.375 (136.7) 500-1000mL Yes 6495-43 19.53
0.02/0.5 6.625 (168.4) 2000-1000mL Yes 6495-47 20.12

6530 FLASK Reaction, Spherical, 3-Neck, Side Port, Flange Top

Rugged, spherical reaction flask with Schott-Duran style o‑ring grooved side port, angled
45° for ease in adding material to flask. In addition to the side port, flask has three  45/50
side necks, all vertical. Center is a Schott-Duran style o‑ring grooved flange supplied
with a CAPFE (PTFE encapsulated silicone) o‑ring for use with 6517 quick release clamp.
Supplied with capacity reference gradations. Order cap, clamps, and extra o‑rings (listed
Cap, clamp, and below) separately.
O‑Ring for Side Port Neck Center
(not included) Capacity, Nominal Nominal Height, Height, Neck, mm Side Port
Liters O.D., mm I.D., mm mm (A) mm (Inches) Size (mm) Order Code Each
50 457 443 550 75 100 (4) 60 6530-42 2012.46
50 457 443 550 75 150 (6) 60 6530-43 2111.69
50 457 443 550 75 200 (8) 60 6530-44 2182.55
50 457 443 550 75 100 (4) 100 6530-47 2047.89
50 457 443 550 75 150 (6) 100 6530-48 2154.20
50 457 443 550 75 200 (8) 100 6530-49 2239.22
72 508 496 570 75 100 (4) 100 6530-52 2402.22
72 508 496 570 75 150 (6) 100 6530-54 2501.43
72 508 496 570 75 200 (8) 100 6530-56 2636.06
100 610 596 680 75 100 (4) 100 6530-64 4917.80
100 610 596 680 75 150 (6) 100 6530-65 4974.49
100 610 596 680 75 200 (8) 100 6530-66 5073.69
Glass Cap, 60mm 15312-30 60.05
Glass Cap, 100mm 15312-33 107.78
CAPFE O‑Ring, 60mm 7855-878 28.10
CAPFE O‑Ring, 100mm 7855-880 28.63
CAPFE O‑Ring, 150mm 7855-881 59.65
A CAPFE O‑Ring, 200mm 7855-884 75.27
Clamp, 60mm, quick release 6517-22 87.08
6530-47
6530 FLASK Reaction, Spherical, 3-Neck, Flange Top

Rugged, spherical reaction flask with three  45/50 side necks, all vertical. Center is a
Schott-Duran style o‑ring grooved flange supplied with a CAPFE (PTFE encapsulated
silicone) o‑ring for use with 6517 quick release clamp. Supplied with capacity reference
gradations. Order clamp and extra o‑rings (listed below) separately.
Capacity, Nominal Nominal Height, Neck Height, Center Neck,

Liters O.D., mm I.D., mm mm (A) mm mm (Inches) Order Code Each
22 350 336 450 100 100 (4) 6530-06 1046.04
50 457 443 550 75 200 (8) 6530-08 2807.79
72 508 496 570 75 200 (8) 6530-15 2643.93
100 610 596 680 75 200 (8) 6530-20 4893.78
CAPFE O‑Ring, 100mm 7855-880 28.63
CAPFE O‑Ring, 200mm 7855-884 75.27
6530-08
6530 FLASK Reaction, Spherical, 4-Neck, 8-in. Flange, with Bottom Outlet
Spherical reaction flask with Schott-Duran style flat, ground flange and bottom valve
assembly. Supplied with capacity reference gradations. Nominal flange I.D. is 200mm
(8 inches). Uses 6517-31 clamp and 7855-884 CAPFE o‑ring. Flask has three  45/50
side joints. 35/25 o‑ring/ball joint connection off 0-20 and piston-style valve. Each flask
is supplied with one CAPFE (PTFE encapsulated silicone) o‑ring.
Capacity, Nominal Nominal Height, Neck Height, Bottom Outlet Order
Liters O.D., mm I.D., mm mm (A) mm Style Code Each A
50 457 443 550 75 0-20 mm 6530-10 2917.90
50 457 443 550 75 Piston 6530-11 2229.72
50 457 443 550 75 Sink 6530-12 2196.69
50 457 443 550 75 Beaded 6530-13 2196.69
50 457 443 550 75 Flush 6530-14 2196.69
72 508 496 570 75 0-20 mm 6530-17 2883.44
72 508 496 570 75 Piston 6530-18 2669.82
72 508 496 570 75 Sink 6530-19 2623.40
72 508 496 570 75 Beaded 6530-22 2,385.00
72 508 496 570 75 Flush 6530-21 2626.12
100 610 596 680 75 0-20 mm 6530-23 5066.97 6530-11
100 610 596 680 75 Piston 6530-24 5006.93
100 610 596 680 75 Sink 6530-25 4952.73
100 610 596 680 75 Beaded 6530-26 4934.18
100 610 596 680 75 Flush 6530-27 4831.04
6957 FLASK Reaction, Spherical, 4-Neck, Side Port

Rugged, spherical reaction flask with Schott-Duran style 60mm (2.4 inch) I.D. o‑ring
grooved side port, angled 45° for ease in adding material to flask. In addition to the
60mm side port, flask has a  45/50 center neck and three  side necks, all vertical.
Supplied with capacity reference gradations. For 60mm side port, order cap, o‑ring and
clamp separately.
Neck
Capacity, Nominal Nominal Height, Height, Center Side
Liters O.D., mm I.D., mm mm (A) mm Neck Necks Order Code Each
22 350 336 450 100 45/50 45/50 6957-28 1026.50
22 350 336 450 100 45/50 29/42 6957-26 907.56
22 350 336 450 100 45/50 24/40 6957-24 896.76
50 457 443 550 75 45/50 45/50 6957-65 Call
Glass Cap, 60mm 15312-30 60.05
CAPFE O‑Ring, 60mm 7855-878 28.10
Cap, clamp, and A

O‑Ring for side port
(not included)
6957-65
For a full listing of round-bottom reaction flasks in smaller

sizes, see our Laboratory Glassware & Equipment Catalog

6522/6472 FLASK Reaction, Cylindrical, with Bottom Outlet

Similar to 6521 but with bottom outlet for draining contents. Easy Action and Piston style
bottom outlets have 28/15 o‑ring ball joint connection. Flasks have capacity reference
graduations, and each flask is supplied with one CAPFE (PTFE encapsulated silicone)
o‑ring. Plain silicone o‑rings are also available.
Nominal Top Valve
Cap., O.D., I.D., Height, Flange I.D. Use CAPFE Size Bottom Order
Liters mm mm mm (A) mm (in.) Clamp O‑Ring mm Outlet Style Code Each
1 110 100 180 100 (4) 6517-25 7855-880 0-8 Easy Action 6522-11 538.78
2 110 100 265 100 (4) 6517-25 7855-880 0-8 Easy Action 6522-13 549.56
3 110 100 400 100 (4) 6517-25 7855-880 0-8 Easy Action 6522-15 561.92
6 205 215 280 200 (8) 6517-31 7855-884 0-8 Easy Action 6522-17 1359.86
10 205 215 470 200 (8) 6517-31 7855-884 0-14 Easy Action 6522-21 1131.71
15 240 250 470 200 (8) 6517-31 7855-884 0-20 Easy Action 6522-26 1471.89
20 236 250 570 200 (8) 6517-31 7855-884 0-20 Easy Action 6472-167 2481.48
30 301 315 540 200 (8) 6517-31 7855-884 0-20 Easy Action 6522-31 2013.47
50 301 315 890 200 (8) 6517-31 7855-884 0-20 Easy Action 6522-36 2568.90
100 443 457 940 200 (8) 6517-31 7855-884 0-20 Easy Action 6522-41 4619.10
200 436 450 1575 200 (8) 6517-31 7855-884 0-20 Easy Action 6522-45 10955.90
10 205 215 470 200 (8) 6517-31 7855-884 0-20 Piston 6522-51 1512.39
15 205 215 470 200 (8) 6517-31 7855-884 0-20 Piston 6522-52 1571.04
A 20 236 250 570 200 (8) 6517-31 7855-884 0-20 Piston 6472-168 2383.33
30 301 315 540 200 (8) 6517-31 7855-884 0-20 Piston 6522-53 2093.14
50 301 315 890 200 (8) 6517-31 7855-884 0-20 Piston 6522-54 2901.33
100 443 457 940 200 (8) 6517-31 7855-884 0-20 Piston 6522-55 5027.94
200 436 450 1575 200 (8) 6517-31 7855-884 0-20 Piston 6522-56 10873.32
10 205 215 470 200 (8) 6517-31 7855-884 — Sink 6522-61 1361.17
15 205 215 470 200 (8) 6517-31 7855-884 — Sink 6522-62 1435.21
20 236 250 570 200 (8) 6517-31 7855-884 — Sink 6472-169 2180.03
30 301 315 540 200 (8) 6517-31 7855-884 — Sink 6522-63 1990.82
50 301 315 890 200 (8) 6517-31 7855-884 — Sink 6522-64 2824.17
100 443 457 940 200 (8) 6517-31 7855-884 — Sink 6522-65 4933.81
200 436 450 1575 200 (8) 6517-31 7855-884 — Sink 6522-66 12387.33
10 205 215 470 200 (8) 6517-31 7855-884 — Beaded 6522-71 1327.19
15 205 215 470 200 (8) 6517-31 7855-884 — Beaded 6522-72 1404.35
20 236 250 570 200 (8) 6517-31 7855-884 — Beaded 6472-170 2166.02
30 301 315 540 200 (8) 6517-31 7855-884 — Beaded 6522-73 1963.03
6522-31
50 301 315 890 200 (8) 6517-31 7855-884 — Beaded 6522-74 2793.30
100 443 457 940 200 (8) 6517-31 7855-884 — Beaded 6522-75 4904.48
200 436 450 1575 200 (8) 6517-31 7855-884 — Beaded 6522-76 12084.53
10 205 215 470 200 (8) 6517-31 7855-884 — Flush Valve 6522-81 1365.80
15 205 215 470 200 (8) 6517-31 7855-884 — Flush Valve 6522-82 1447.56
20 236 250 570 200 (8) 6517-31 7855-884 — Flush Valve 6472-02 2242.57
30 301 315 540 200 (8) 6517-31 7855-884 — Flush Valve 6522-83 2006.24
50 301 315 890 200 (8) 6517-31 7855-884 — Flush Valve 6522-84 2833.42
100 443 457 940 200 (8) 6517-31 7855-884 — Flush Valve 6522-85 4953.87
200 436 450 1575 200 (8) 6517-31 7855-884 — Flush Valve 6522-86 12084.53
6473 FLASK Reaction, Cylindrical, with Bottom Outlet, KF Plane Flange

Cylindrical reaction flask with top KF plane flange and bottom outlet for draining contents.
Easy Action bottom outlet has 28/15 o‑ring ball joint connection. Sink bottom outlet has
#36 Ace‑Thred connection. Flasks have capacity reference graduations. Gasket and
coupling must be purchased separately.
Nominal Top Valve
Cap., O.D., I.D., Height, Flange I.D. Use PTFE Size Bottom Order
Liters mm mm mm (A) mm (in.) Coupling Gasket mm Outlet Style Code Each
100 457 443 940 300 (12) 6525-30 6525-51 0-20 Easy Action 6473-02 5531.62
100 457 443 940 300 (12) 6525-30 6525-51 — Flush Valve 6473-05 4977.90 A
200 450 436 1575 300 (12) 6525-30 6525-51 — Flush Valve 6473-11 10958.02
100 457 443 940 300 (12) 6525-30 6525-51 — Sink 6473-22 5371.03
200 450 436 1575 300 (12) 6525-30 6525-51 — Sink 6473-26 12176.20
100 457 443 940 300 (12) 6525-30 6525-51 — Beaded 6473-40 4983.43
200 450 436 1575 300 (12) 6525-30 6525-51 — Beaded 6473-44 10880.50
6473-02
6523 FLASK Reaction, Cylindrical, Jacketed 6523

Rugged cylindrical reaction flask with Schott-Duran style flat flange with o‑ring groove,
for use with 6517 quick release clamp. Inlet and outlet connections on jacket, sealed
tangentially, are o‑ring size 35/25 ball joints. Ten (10) liter and larger are supplied with
capacity reference graduations. Each flask is supplied with one CAPFE (PTFE encapsulated
silicone) o‑ring for flange. Plain silicone o‑rings are also available. For reaction heads,
see 6528 or 6530. Jacket is direct sealed to inner flask.
Nominal Top
Capacity, O.D., I.D., Height, Flange I.D. APFE
C Order
Liters mm mm mm (A) mm (In.) Use Clamp O‑Ring Code Each
1 160 100 230 100 (4) 6517-25 7855-880 6523-12 574.48 A
2 160 100 395 100 (4) 6517-25 7855-880 6523-14 655.16
3 160 100 425 100 (4) 6517-25 7855-880 6523-16 725.63
6 270 205 315 200 (8) 6517-31 7855-884 6523-19 2164.47
10 270 205 525 200 (8) 6517-31 7855-884 6523-22 2287.00
15 315 240 575 200 (8) 6517-31 7855-884 6523-27 2967.46
20 315 236 675 200 (8) 6517-31 7855-884 6523-30 3077.56
30 350 301 540 200 (8) 6517-31 7855-884 6523-32 3297.79
50 350 301 925 200 (8) 6517-31 7855-884 6523-37 3958.44

6524/6472 FLASK Reaction, Cylindrical, with Bottom Outlet, Jacketed

Rugged cylindrical reaction flask with Schott-Duran style flat flange with o‑ring groove, for
use with quick release clamp. Inlet and outlet connections on jacket, sealed tangentially, are
o‑ring ball joints. Ten (10) liter and larger are supplied with capacity reference graduations.
Each flask is supplied with one CAPFE (PTFE encapsulated silicone) o‑ring. Plain silicone
o‑rings are also available. For reaction heads, see 6528 or 6530. Bottom Easy Action and
Piston outlets on 15L and larger flasks have size 35/25 o‑ring ball joint; below 15L, o‑ring
ball joints are size 28/15.
Hgt, Nominal Top Valve Inlet/ Bottom

Cap., O.D., I.D., mm Flange I.D. Use CAPFE Size, Outlet Outlet Bottom Order
Liters mm mm (A) mm (In.) Clamp O‑Ring mm Size Size Outlet Style Code Each
1 160 100 205 100 (4) 6517-25 7855-880 0- 8 28/15 28/15 Easy Action 6524-13 883.96
2 160 100 240 100 (4) 6517-25 7855-880 0- 8 28/15 28/15 Easy Action 6524-15 995.14
3 160 100 425 100 (4) 6517-25 7855-880 0- 8 28/15 28/15 Easy Action 6524-17 1106.33
6 270 205 340 200 (8) 6517-31 7855-884 0- 8 28/15 28/15 Easy Action 6524-20 2885.36
10 270 205 530 200 (8) 6517-31 7855-884 0-14 35/25 28/15 Easy Action 6524-23 3002.10
15 315 240 545 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Easy Action 6524-28 3218.92
20 315 236 700 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Easy Action 6472-175 5722.92
A 30* 350 301 550 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Easy Action 6524-33 3502.45
50* 350 301 900 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Easy Action 6524-38 7044.57
10 270 205 530 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Piston 6524-43 2946.51
15 315 240 545 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Piston 6524-44 3057.70
20 315 236 700 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Piston 6472-176 6112.53
30* 350 301 550 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Piston 6524-45 3280.08
50* 350 301 900 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Piston 6524-46 7116.10
10 270 205 530 200 (8) 6517-31 7855-884 — — — Sink 6524-53 2946.51
15 315 240 545 200 (8) 6517-31 7855-884 — — — Sink 6524-54 3057.70
20 315 236 700 200 (8) 6517-31 7855-884 — — — Sink 6472-177 5705.98
30* 350 301 550 200 (8) 6517-31 7855-884 — — — Sink 6524-55 3280.08
50* 350 301 900 200 (8) 6517-31 7855-884 — — — Sink 6524-56 7116.10
10 270 205 530 200 (8) 6517-31 7855-884 — — — Beaded 6524-63 2946.51
6524-33
15 315 240 545 200 (8) 6517-31 7855-884 — — — Beaded 6524-64 3057.70
20 315 236 700 200 (8) 6517-31 7855-884 — — — Beaded 6472-178 5666.74
30* 350 301 550 200 (8) 6517-31 7855-884 — — — Beaded 6524-65 3280.08
50* 350 301 900 200 (8) 6517-31 7855-884 — — — Beaded 6524-66 7116.10
10 270 205 530 200 (8) 6517-31 7855-884 — — — Flush Seal 6524-73 2890.91
15 315 240 545 200 (8) 6517-31 7855-884 — — — Flush Seal 6524-74 3330.11
20 315 236 700 200 (8) 6517-31 7855-884 — — — Flush Seal 6472-16 4361.31
30* 350 301 550 200 (8) 6517-31 7855-884 — — — Flush Seal 6524-75 3363.47
50* 350 301 900 200 (8) 6517-31 7855-884 — — — Flush Seal 6524-76 7116.10
*Jackets on 30 and 50 Liter capacities are silicone rubber sealed at bottom only.
6473 FLASK Reaction, Jacketed, Cylindrical, with Bottom Outlet,

KF Plane Flange,
Cylindrical, jacketed reaction flask with top KF plane flange and bottom flush style outlet
for draining contents. Inlet and outlet connections on jacket, sealed tangentially, are 35/25
o‑ring ball joints. Flasks has capacity reference graduations. Gasket and coupling must
be purchased separately.
Nominal Top
Cap., O.D., I.D., Height, Flange I.D. Use PTFE Bottom Order
Liters mm mm mm (A) mm (in.) Coupling Gasket Outlet Style Code Each
100 460 443 940 300 (12) 6525-30 6525-51 Flush 6473-09 14341.21
A
6473-09
6533 FLASK Reaction, Spherical, Plain, 4, 6, or 8 in. Flange

Rugged spherical reaction flask with Schott-Duran style flat flange with o‑ring groove,
for use with 6517 quick release clamp. Each flask is supplied with one CAPFE (PTFE
encapsulated silicone) o‑ring. Flasks (12L and above) are supplied with capacity reference
graduations. Plain silicone o‑rings are also available. For reaction heads, see 6529 or A
6530. For cooling/heating coils, see 12067. For mantles, see 12043.
Nominal Top
Capacity, O.D., I.D., Height, Flange I.D., Use CAPFE Order
Liters mm mm mm (A) mm (In.) Clamp O‑Ring Code Each
3 180 166 270 100 (4) 6517-25 7855-880 6533-03 247.75
5 226 212 320 100 (4) 6517-25 7855-880 6533-05 302.81
5 226 212 320 150 (6) 6517-27 7855-881 6533-07 338.67
12 285 270 380 150 (6) 6517-27 7855-881 6533-12 453.98
22 350 336 450 150 (6) 6517-27 7855-881 6533-15 649.78
50 457 443 550 200 (8) 6517-31 7855-884 6533-25 1596.59 6533
72 508 496 570 200 (8) 6517-31 7855-884 6533-28 1789.29

6534 FLASK Reaction, Spherical, Flange Top, with Bottom Outlet

Rugged spherical reaction flask with Schott-Duran style flat flange with o‑ring groove, for
use with 6517 quick release clamp. Flasks have capacity reference gradations, and can
be configured with one of several different bottom outlets (see page 92 for a description
of each outlet style). Each flask is supplied with one CAPFE (PTFE encapsulated silicone)
o‑ring. Plain silicone o‑rings are also available. For reaction heads, see 6529 or 6530.
For cooling/heating coils, see 12067. For mantles, see 12044. Easy Action and Piston
bottom outlets have size 35/25 o‑ring ball joint connection.
Height, Nominal Repl. Outlet Bottom
Cap., O.D., I.D., mm Flange I.D., Use CAPFE Size, Outlet Order
Liters mm mm (A) mm (In.) Clamp O‑Ring mm Style Code Each
3 180 166 270 100 (4) 6517-25 7855-880 0- 8 Easy Action 6534-04 611.88
5 226 212 320 100 (4) 6517-25 7855-880 0- 8 Easy Action 6534-06 634.18
5 226 212 320 150 (6) 6517-27 7855-881 0- 8 Easy Action 6534-09 705.66
A 12 285 270 380 150 (6) 6517-27 7855-881 0-14 Easy Action 6534-13 976.91
22 350 336 450 150 (6) 6517-27 7855-881 0-20 Easy Action 6534-16 1257.47
50 457 443 550 200 (8) 6517-31 7855-884 0-20 Easy Action 6534-26 2604.68
72 508 496 570 200 (8) 6517-31 7855-884 0-20 Easy Action 6534-29 2529.79
12 285 270 380 150 (6) 6517-27 7855-881 0-20 Piston 6534-30 1099.16
22 350 336 450 150 (6) 6517-27 7855-881 0-20 Piston 6534-32 1379.75
50 457 443 550 200 (8) 6517-31 7855-884 0-20 Piston 6534-34 2463.76
72 508 496 570 200 (8) 6517-31 7855-884 0-20 Piston 6534-36 2652.04
6534-13 12 285 270 380 150 (6) 6517-27 7855-881 — Sink 6534-40 976.91
22 350 336 450 150 (6) 6517-27 7855-881 — Sink 6534-42 1257.47
50 457 443 550 200 (8) 6517-31 7855-884 — Sink 6534-44 2341.50
72 508 496 570 200 (8) 6517-31 7855-884 — Sink 6534-46 2529.79
12 285 270 380 150 (6) 6517-27 7855-881 — Beaded 6534-50 928.00
22 350 336 450 150 (6) 6517-27 7855-881 — Beaded 6534-52 1208.58
50 457 443 550 200 (8) 6517-31 7855-884 — Beaded 6534-54 2292.59
72 508 496 570 200 (8) 6517-31 7855-884 — Beaded 6534-56 2480.87
12 285 270 380 150 (6) 6517-27 7855-881 — Flush Seal 6534-60 964.68
22 350 336 450 150 (6) 6517-27 7855-881 — Flush Seal 6534-62 1245.25
50 457 443 550 200 (8) 6517-31 7855-884 — Flush Seal 6534-64 2329.27
72 508 496 570 200 (8) 6517-31 7855-884 — Flush Seal 6534-66 2517.55
6535 FLASK Reaction, Spherical, Jacketed

Rugged spherical jacketed reaction flask with Schott-Duran style flat flange with o‑ring
groove, for use with 6517 quick release clamp. Each flask is supplied with one CAPFE
(PTFE encapsulated silicone) o‑ring. Plain silicone o‑rings are also available. 12L size
is supplied with capacity reference graduations. Inlet and outlet are size 28/15 o‑ring
ball joints, sealed tangentially. For reaction heads, see 6529. For cooling/heating coils,
see 12076.
Nominal Top
6535-12 Liters mm mm mm (A) mm (In.) Clamp O‑Ring Code Each
3 225 170 370 100 (4) 6517-25 7855-880 6535-03 967.87
5 285 212 435 100 (4) 6517-25 7855-880 6535-05 1190.00
5 285 121 450 150 (6) 6517-27 7855-881 6535-07 1238.87
12 360 270 505 150 (6) 6517-27 7855-881 6535-12 2889.92
A
6536 FLASK Reaction, Spherical, Jacketed, with Bottom Outlet

Rugged spherical reaction flask with Schott-Duran style flat flange with o‑ring groove, for
use with 6517 quick release clamp. See listing below for different bottom outlet styles.
The 0-14 Easy-Action and Piston bottoms have a 28/15 ball joint bottom connector. Each A
flask is supplied with one 7855 CAPFE (PTFE encapsulated silicone) o‑ring. Plain silicone
o‑rings are also available. All capacities have size 28/15 o‑ring ball joints on inlet and outlet,
sealed tangentially. For reaction heads, see 6529. For cooling/heating coils, see 12067.
Nominal Bottom Top
Capacity, O.D., I.D., Height, Flange I.D., Outlet Use CAPFE Order
Liters mm mm mm (A) mm (In.) Style Clamp O‑Ring Code Each
3 225 170 370 100 (4) Easy-Action 6517-25 7855-880 6536-06 1132.26
5 285 212 435 100 (4) Easy-Action 6517-25 7855-880 6536-09 1520.22
5 285 212 450 150 (6) Easy-Action 6517-27 7855-881 6536-11 1573.96
12 360 270 505 150 (6) 0-14mm 6517-27 7855-881 6536-15 3245.52
12 360 270 505 150 (6) Piston 6517-27 7855-881 6536-25 3369.57
12 360 270 505 150 (6) Sink 6517-27 7855-881 6536-35 3245.52 6536-15
12 360 270 505 150 (6) Beaded 6517-27 7855-881 6536-45 3195.17
12 360 270 505 150 (6) Flush 6517-27 7855-881 6536-55 3232.54
6537 FLASK Reaction, Spherical, Indented Style

Rugged spherical reaction flask with Schott-Duran style flat flange with o‑ring groove,
for use with 6517 quick release clamp but with indents for greater agitation. Each flask
is supplied with one 7855-881 CAPFE (PTFE encapsulated silicone) o‑ring. Plain silicone A
12067. NOT suitable for vacuum or high temperature operation.
Nominal Top
ted
Inden
Liters mm mm mm (A) mm (In.) Clamp O‑Ring Code Each
3 180 166 270 100 (4) 6517-25 7855-880 6537-07 320.35
5 226 212 320 100 (4) 6517-25 7855-880 6537-12 363.68
5 226 212 320 150 (6) 6517-27 7855-881 6537-17 428.55
12 285 270 380 150 (6) 6517-27 7855-881 6537-24 534.04 6537
New
6310 FLASK Reaction, Three-Wall, Double-Jacketed
Unique ACE proprietary designed triple-wall, or double-jacketed, flasks. Available with
various bottom outlets. These flasks are designed with an outside, third wall, vacuum
evacuated and sealed for better thermal control and stability of the jacketed reactor.
The first wall is the main reactor body, the second is the thermal fluid compartment with
inlet/outlet o‑ring ball joints and the third is the evacuated compartment. The double
jacket also eliminates “frosting-up” on the outer jacket as seen in low temperature with
traditional jacketed flasks. The jacket I/O are 35/25 o‑ring ball joints for easier recircula‑
tor hose connection. The top has an 8-inch o‑ring groove Schott-Duran style flange. All
sizes have reference graduations. Flask comes with CAPFE (PTFE encapsulated silicone)
o‑ring. Other sizes and bottom valves are available on special request.
Inner Inner
Flask Overall Inner Flask
Cap., Length, Flask ID, Length,
Liters mm mm mm Bottom Outlet Style Order Code Each
10 626 201 490 2-inch Bead/Flush Valve 6310-100
10 626 201 490 No Outlet/Rounded 6310-105
Priced
Upon
15 785 201 645 No Outlet/Rounded 6310-125 Request 6310
20 800 235 665 No Outlet/Rounded 6310-135

6300 FLASK Reaction, with O‑Ring Groove Flange,

Fritted Disc, Heavy Wall
Cylindrical, heavy wall reaction flasks, with integral fritted disc and bottom tube outlet.
Top of flask has Schott-Duran style flange with a groove for use with o‑ring. For reaction
heads, see 6528, 6529 and 6530 series. Can be used with two-piece or 6517 quick
release clamps.
A Bottom Frit
Capacity, O.D., I.D., Height, Flange I.D., Tube O.D. Frit Diameter, Order
Liters mm mm mm (A) mm (In.) (In.) Porosity mm Code Each
1 110 100 210 100 (4) 5/8 A 100 6300-06 419.05
1 110 100 210 100 (4) 5/8 B 100 6300-08 419.05
1 110 100 210 100 (4) 5/8 C 100 6300-10 419.05
4 155 145 330 150 (6) 1-1/4 A 145 6300-18 508.85
4 155 145 330 150 (6) 1-1/4 B 145 6300-20 508.85
4 155 145 330 150 (6) 1-1/4 C 145 6300-22 508.85
6 215 205 275 200 (8) 1-1/4 A 178 6300-30 808.17
6 215 205 275 200 (8) 1-1/4 B 178 6300-32 808.17
6300 6 215 205 275 200 (8) 1-1/4 C 178 6300-34 808.17
GLASS FRIT CHARACTERISTICS

Porosity
ACE Maximum Pore Dia. Corning, Kimble, &
Designation Range (micron) ChemGlass Equivalent Most Frequent Uses
A 145-174 EC (170-220) Coarse filtration. Gas Dispersion
B 70-100 — Coarse filtration. Gas Dispersion
C 25-50 C (40-60 Filtration. Gas Dispersion
D 10-20 M (10-15) Filtration and extraction
E 4-8 F (4-5.5) Filtration and extraction
6497 FLASK Reaction, Stainless Steel, 4-inch Conical Flange

6497 Cylindrical flask fabricated from 18-8, type 316 electro polished, heliarc welded stainless
steel.* Can be used with 6478 Glas-Col mantles. Interchangeable with our glass units.
Nominal Nominal Height,
Capacity, mL O.D., mm I.D., mm mm (A) Order Code
500 4.0 4.5 3.5 6497-07
Priced on
1000 4.1 4.5 6.0 6497-12
Application
2000 4.1 4.5 9.0 6497-17
A *Other metals are available, phone ACE.
6498 6498 FLASK Reaction, Stainless Steel, 4-inch Conical Flange

Spherical flask fabricated from 18-8, type 316 electro-polished, heliarc-welded stainless
steel. Interchangeable with our glass units. Can be used with 12043 or 12053 Glas-Col
mantles.
Nominal Nominal Height,
A Capacity, Liters O.D., mm I.D., mm mm (A) Order Code
3 178 177 254 6498-12
5 216 215 317 6498-17
12 292 291 380 6498-22 Priced on
22 343 342 416 6498-27 Application
50 444 443 546 6498-32
72 508 507 600 6498-37
D120676 FLASK Instatherm Robo Reactorfor ASTM D7528-09

Flask for use with ASTM Protocol D7528-09 Standard Test Method. For bench oxidation
of engine oils by ROBO. Use ONLY 9698-16 controller cord (supplied) for connection to
temperature controllers. Conical style four-inch flange. Uses 6495 gaskets.
D120676
Capacity,
Liters Volts/Amps Order Code Each
1 40/10 D120676 Call
New
9655 REACTION FLASK Instatherm® Heated, Schott-Duran Flange

Rugged cylindrical reaction flask with Schott-Duran, flat, ground 4-inch flange with
o‑ring groove for use with 6517-25 quick release clamp and integral heating element
that eliminates the local superheating commonly associated with more conventional
heating methods and eliminates cumbersome oil baths. The heating response is rapid
and accurate. Supplied with silicone coating for insulation and protection. O-Ring
(supplied with flask) is CAPFE (PTFE encapsulated silicone). Flask is coated to within
approximately 38mm of the flange for 250°C operation. Interchangeable with ACE A
4-inch reactor heads with Schott-Duran flange. Three-pronged plug for insertion into
ACE temperature controllers. Integral six-foot controller cord.
1 110 100 180 40/8 400 9655-17 766.76
2 110 100 200 120/5 600 9655-22 869.89 9655
9656 REACTION FLASK Instatherm® Heated, Conical, 4-Inch Flange

Same flask as listed under 6476, except with Instatherm coating. Has flat-ground,
4-inch conical flange. This integral heating element eliminates the local super-heating
commonly associated with more conventional heating methods. Eliminates cumbersome
and dangerous oil baths. The heating response is rapid and accurate. Supplied with
9698-20 cord for connection to variable voltage or termperature controller. Flask is
coated to within 38mm of the flange for 200ºC operation. Interchangeable with ACE
4-inch reactor heads with Schott-Duran flange. For controllers, see ACE or J-Kem A
temperature controllers with voltage limiting output, such as 12125, 12324. Use 6496
clamp for securing head to flask.
1 110 100 180 40/8 400 9656-08 758.58
2 114 104 260 120/5 500 9656-12 864.03 9656

HEAVY
6945 FLASK Three Necks, Jacketed, Heavy Wall
DUTY Round bottom flask with three in-line reinforced  outer joints. Fabricated with heavy
6945 walls, approximately 30% heavier than standard-wall flasks. Inlet/outlet connections are
28/15 o‑ring ball joints, sealed tangentially.
Cap., Center Side Order Cap., Center Side Order
mL Neck Necks Code Each mL Neck Necks Code Each
500 24/40 24/40 6945-217 530.52 5000 29/42 29/42 6945-266 849.92
500 29/42 24/40 6945-219 539.65 5000 34/45 24/40 6945-268 879.83
1000 24/40 24/40 6945-223 612.62 5000 45/50 24/40 6945-270 901.08
1000 29/42 24/40 6945-225 621.78 6000 24/40 24/40 6945-274 933.60
2000 29/42 24/40 6945-245 661.37 6000 29/42 24/40 6945-276 946.65
3000 29/42 24/40 6945-255 741.98 6000 29/42 29/42 6945-278 953.17
3000 29/42 29/42 6945-257 749.51 6000 45/50 24/40 6945-280 998.89
3000 34/45 24/40 6945-259 779.12 6000 45/50 29/42 6945-282 1005.41
3000 45/50 24/40 6945-261 807.61 6000 45/50 45/50 6945-284 1039.36
5000 29/42 24/40 6945-264 840.76
7127 FLASK Volumetric, Pilot Plant

Large capacity volumetric flask with  outer joint, without graduation mark. Supplied
without stopper.
Flask only Stopper only
7127 Capacity,
mL Joint Order Code Each Order Code Each
5000 34/28 7127-25 202.74 8255-18 30.08
10000 40/35 7127-30 290.74 8255-20 45.82
Guide to Flange Styles
Schott-Duran
Beaded
Flat Flange Flange Process Pipe
(with or without O‑Ring (with or without O‑Ring
groove) groove) Conical Flange KF Plane Flange Flange
Uses Clamp: Uses Clamp: Uses Clamp: Uses Clamp: Uses Clamp:
6508, 6509, 6510 6517 6496 6525 8856
Flat clamp Quick release clamp Standard clamp Coupling Coupling
See page 8 for flange dimensions.
Components / Heads 113
6472 HEAD Glass, Flat, Pilot Plant

Borosilicate glass head with holes drilled to match (included) 6413 PTFE inserts. Head is
1‑1/4‑inch (32mm) thick, designed for use with 300mm (12-inch) flat ground flanges on reaction
flasks. Use 6525 clamp assembly. Requires 6472-161 bolt/nut assembly (not included).
Center Joint Side Joints Order Code Each

45/50 (4) 45/50; (2) 29/42 6472-20 2018.25
45/50 (4) 45/50; (2) 29/32; (1) 71/60 6472-21 2225.25
Accessories Order Code Each
71/60 Stopper 8250-28 161.88
300mm Coupling 6525-30 1056.54
Nuts & Bolts, 8 inch length 6472-161 11.74
6472-21
6472 HEAD Stainless Steel, Pilot Plant

Reaction flask head fabricated from 316 stainless steel. Replaces flat or domed glass 6472-17
heads. This 1/4-inch thick head has the same openings as the flat glass head and accepts
 PTFE joint inserts secured top and bottom of plate with threaded nuts. 10L size uses
one  45/50, three  29/42 and three  24/40 inserts; 30L and 50L sizes use five  45/50
and two  29/42 inserts (6472-17 also requires a  71/60 insert). See 6412 (below) for
inserts. Stainless head is assembled to reaction flask in the same manner as flat glass head
using 6525 coupling (not included) and one spacer. Optional: flat sheet of PTFE covers
entire underside of stainless steel head and is secured by coupling and  joint inserts.
For
Uses Diameter, Reactor Number of Order
Description Coupling mm Size Openings Code Each
Head only 6525-25 200 10L 7 6472-25 822.56
Head only 6525-30 300 30L & 50L 7 6472-26 835.47
Head only 6525-30 300 30L & 50L 8 6472-17 Call
Flat PTFE cover only — 200 10L 7 6472-29 197.90
Flat PTFE cover only — 300 30L & 50L 7 6472-30 219.16 6472-26
Flat PTFE cover only — 300 30L & 50L 8 6472-15 295.00
6412 JOINT INSERTS PTFE, Standard Taper, for Stainless Steel Heads
Solid, virgin PTFE, standard taper joint inserts for 6472 series stainless steel, flat heads
for ACE reactors. Top of insert is machined for outside standard taper joint that matches
glass inner standard taper joints. Bottom is reverse threaded and has a PTFE collar and
FETFE o-ring for attaching to the flat heads. Tops are also machined to accept the 7597
joint clips. 71/60 size fits glass stopper for 71/60 sample port on 6472-17 head.
For Joint Size Order Code Each

24/40 6412-05 76.50
29/42 6412-07 90.78
45/50 6412-09 111.18
71/60 6412-11 162.18 6412
6413 JOINT INSERTS PTFE, Standard Taper, for Flat Glass Heads
Solid, virgin PTFE, standard taper joint inserts for 6472 series flat glass heads. This low
profile insert allows for increased working space above the head. The insert is secured
to the head with a reverse threaded locking nut and sealed using a FETFE o-ring. The
top of the insert is formed to allow the use of 7597 joint clips.

24/40 6413-05 76.50
6413
29/42 6413-07 90.78
45/50 6413-09 111.18
71/60 6413-11 162.18

114 Components / Heads
S IN C O R
A S P
L
OR
ACE G
ATED
VI USA
NE N
J
LAND,

6433 HEAD For Pressure or Filter Reactors, Ace‑Threds 6433-23

Reactor head, only, with Schott-Duran style flange and Ace‑Threds for use with 6384,
6386 or 6388 reactor bodies. Pressure rating is 35 psi. Uses 6517 quick release clamp.
For Flask Flange I.D., Center
Cap., mL mm (in.) Neck Side Necks Order Code Each
150- 600 60 (2.4) #15 (2)#15-(1)#7 6433-23 295.48
1000-2000 100 (4) #15 (3)#15-(1)#7 6433-35 396.77
3000-6000 150 (6) #15 (4)#15-(1)#7 6433-44 544.04
6433-35
6484 HEAD Reaction, Conical Flange, 4 Necks 6484

Standard 4-inch (100mm) head for use with 6475, 6476, 6477, 6479, 6480, 6481, 6491,
and 6492 ACE reaction flasks. Supplied with three  outer joints in line, plus a  10/30
joint for a ground joint thermometer or 8299 thermometer adapter. Use 6496 clamp for
securing to flasks. Uses 6495 gaskets.
Center Side Thermometer
Joint Joints Joint Order Code Each
24/40 24/40 10/30 6484-10 254.31
29/42 24/40 10/30 6484-20 266.40
45/50 24/40 10/30 6484-40 275.48
6485 HEAD Reaction, Ace‑Thred, Conical Flange, 4 Necks 6485

Standard 4-inch (100mm), four-outlet head for use with 6475, 6476, 6477, 6479, 6480,
6481, 6491, and 6492 ACE reaction flasks. Supplied with three  outer joints in line, plus a
thermometer side neck which is internally threaded (with #7 Ace‑Thred) for use with 5029
nylon bushing. Use of the threaded side neck permits easy adjustment of thermometer
depth. Use 6496 clamp for securing to flasks. Supplied complete with 5029 bushing and
FETFE o‑ring. For extra bushings, see 5029-10. For extra FETFE o‑rings, see 7855-704.
Uses 6495 gaskets.

24/40 (2) 24/40; (1) #7 6485-16 268.18
29/42 (2) 24/40; (1) #7 6485-22 270.37
6486 HEAD Reaction, Conical Flange, 3 Necks 6486

Standard 4-inch (100mm), three-outlet head for use with 6475, 6476, 6477, 6479, 6480,
6481, 6491, and 6492 ACE reaction flasks. Supplied with three outer joints. Use 6496
clamp for securing to flasks. Uses 6495 gaskets.

24/40 24/40 6486-10 232.01
29/42 24/40 6486-20 238.00
29/42 29/42 6486-25 240.51
45/50 24/40 6486-40 245.01

6487 6487 HEAD Reaction, Conical Flange, 3 Necks

Standard 4-inch (100mm), three-outlet head for use with 6475, 6476, 6477, 6479, 6480,
6481, 6491, and 6492 ACE reaction flasks. Supplied with three  socket joints. Use 6496
clamp for securing to flasks. Uses 6495 gaskets.

35/25 35/25 6487-25 268.74
6488
6488 HEAD Reaction, Conical Flange, 4 Necks
This standard 4-inch (100mm) head has three  outer joints in line, plus a  14/35 side
joint which takes a 5021, 5028-26 or 8300-07 bushing adapter to be used with ACE 8314
 10/30 thermometer. The 6500 thermometer well can also be used with this head, when
using a standard thermometer. For use with 6475, 6476, 6477, 6479, 6480, 6481, 6491,
and 6492 ACE reaction flasks. Use 6496 clamp for securing head to flask.
Joint Joints Joint Order Code Each
24/40 24/40 14/35 6488-10 252.82
29/42 24/40 14/35 6488-15 261.60
29/42 29/42 14/35 6488-20 267.50
45/50 24/40 14/35 6488-40 276.12

6489 Standard 4-inch (100mm) head with three  socket joints in line, plus a  14/35 side joint
for thermometer. Use 6496 clamp for securing to flasks. For use with 6475, 6476, 6477,
6479, 6480, 6481, 6491, and 6492 ACE reaction flasks.
Joint Joint Joint Order Code Each
35/25 35/25 14/35 6489-20 281.51
6490 HEAD Reaction, Stainless Steel, Conical Flange, 3 Necks

Fabricated from 18-8 type 316 electro-polished, heliarc-welded stainless steel.
Interchangeable with our glass flasks. Fits all ACE four-inch conical neck reaction flasks
such as 6469, 6475, 6476, 6477, 6479, 6480, 6481, 6491, 6492, 6497, 6498 and 9656.
6490-17 Use 6496 clamp for securing head to flask.

24/40 24/40 6490-12
Priced
29/42 24/40 6490-17
Upon
29/42 29/42 6490-22 Request
35/25 35/25 6490-27
6490-27


Conical flange with 4-inch (100mm) opening. One  center joint and three  side necks. 6499
Similar to 6488 series except all the side necks are   24/40. For use with 6475, 6476, 6477,
6479, 6480, 6481, 6491, and 6492 ACE reaction flasks Use 6496 clamp to secure head.
Center Joint (3) Side Joints Order Code Each

24/40 24/40 6499-10 280.59
29/42 24/40 6499-14 285.17
45/50 24/40 6499-18 297.77
6512 HEAD Reaction, Flat Flange, 3 Necks 6512

For use with 6511 ground flat flange flasks. With three in-line  joints. Uses 6508 or 6510
clamps.
For Flask Center (2) Side
Cap., mL Joints Joints Order Code Each
1000 24/40 24/40 6512-16 271.96
2000-4000 24/40 24/40 6512-20 293.65
2000-4000 29/42 24/40 6512-24 309.75
2000-4000 45/50 24/40 6512-28 329.96
6513 HEAD Reaction, Flat Flange, 4 Necks, with #7 Ace‑Thred 6513

For use with 6511 ground flat flange flasks. With three in-line  joints and a #7 Ace‑Thred,
internally threaded side opening for thermometer (#7 accepts 6-7mm O.D.). Thread forms a
compression seal with 5029 nylon bushing and permits vertical adjustment of thermometer.
Supplied complete with bushing and FETFE o‑ring. Uses 6508 or 6510 clamps.
For Flask Center (2) Side
1000 24/40 24/40 6513-26 299.58
2000-4000 24/40 24/40 6513-30 316.60
2000-4000 29/42 24/40 6513-34 330.61
2000-4000 45/50 24/40 6513-38 351.51
6515 HEAD Reaction, Flat Flange, 4 Necks

For use with 6511 ground flat flange flasks. With three in-line  joints and a  10/30 side
joint for thermometer. Uses 6508 or 6510 clamps.
For Flask Center Side 6515
1000 24/40 (2) 24/40; (1) #7 6515-46 294.29
2000-4000 24/40 (2) 24/40; (1) #7 6515-50 312.62
2000-4000 29/42 (2) 24/40; (1) #7 6515-54 327.92
2000-4000 45/50 (2) 24/40; (1) #7 6515-58 356.63
All ACE full-length outer joints are tooled with reinforcement

rings for added strength and stability.

6527-26 6527/6528/6529 HEAD For Filter Reactors

Reactor head, only, with Schott-Duran style flange and  joints for use with 6384, 6386
or 6388 reactor bodies. 6527-26 has three angled  24/40 joints; 6528-31 and 6529-32
have four vertical  24/40 joints. Use 6517 clamp.
For Flask # of
Cap., mL Flange I.D., mm (in.) Necks Order Code Each
150- 600 60 (2.4) 3 6527-26 278.81
1000-2000 100 (4) 4 6528-31 281.42
3000-6000 150 (6) 4 6529-32 387.69
6528-31/6529-32
6528-31 6528 HEAD Reaction, Schott-Duran Flange, 4 Necks

Flat ground Schott-Duran style flange for use with all reaction flasks that have a 100mm
(4-inch) Schott-Duran ground mating flange. Supplied with three in-line ground  joints
and one  side joint. For clamp, order 6517-25.
Flange I.D.,
Center Joint mm (in.) (3) Side Joints Order Code Each
24/40 100 (4) 24/40 6528-31 281.42
29/42 100 (4) 24/40 6528-35 282.28
45/50 100 (4) 24/40 6528-38 296.74
6528 HEAD Reaction, Schott-Duran Flange, 5 Necks

(4-inch) Schott-Duran ground mating flange. Supplied with three in-line ground  joints
and two  side joints, for thermal probe connection, etc. For clamp, order 6517-25.
Flange I.D.,
24/40 100 (4) 24/40 6528-42 308.50
29/42 100 (4) 24/40 6528-44 308.72
29/42 100 (4) 29/42 6528-46 310.39
45/50 100 (4) 24/40 6528-49 324.05
6528-44


6529 HEAD Reaction, Schott-Duran Flange, 4 Necks 6529-39

(6-inch) Schott-Duran ground mating flange. Supplied with four ground  joints. For
clamp, order 6517-27.
Flange I.D.,
24/40 150 (6) 24/40 6529-32 387.69
29/42 150 (6) 24/40 6529-36 391.40
45/50 150 (6) 24/40 6529-39 411.13
6529 HEAD Reaction, Schott-Duran Flange, 5 Necks

(6-inch) Schott-Duran ground mating flange. Supplied with five ground  joints. For
clamp, order 6517-27.
Flange I.D.,
24/40 150 (6) 24/40 6529-23 390.96
29/42 150 (6) 24/40 6529-25 391.19
29/42 150 (6) 29/42 6529-27 392.04
45/50 150 (6) 24/40 6529-29 438.72
6529-25
6529 HEAD Reaction, Schott-Duran Flange, 4 Necks 6529

(6-inch) Schott-Duran ground mating flange. Supplied with two in-line ground  joints
and one side, 10/30  joint, for thermal probe connection, etc. For adapter with #7
Ace‑Thred for connecting thermometer or other type probe and permits easy vertical
depth adjustment, see 5028. For clamp, order 6517-27.
Flange I.D.,
24/40 150 (6) 24/40 6529-03 371.08
29/42 150 (6) 24/40 6529-04 374.60
29/42 150 (6) 29/42 6529-05 333.01
45/50 150 (6) 24/40 6529-06 388.06


6530 HEAD Reaction, Schott-Duran Flange

(8‑inch) Schott-Duran ground mating flange. Supplied with one through seven ground
joints. For clamp, order 6517‑31.
Flange I.D.,
Center Joint mm (in.) Side Joints Order Code Each
45/50 200 (8) — 6530-32 425.01
45/50 200 (8) (3) 24/40 6530-30 626.07
45/50 200 (8) (2) 29/42 6530-33 594.98
45/50 200 (8) (3) 29/42 6530-31 749.14
45/50 200 (8) (3) 45/50 6530-34 938.98
45/50 200 (8) (2) 45/50 – (2) 29/42 6530-35 984.56
45/50 200 (8) (4) 24/40 6530-36 992.36
45/50 200 (8) (3) 45/50 – (3) 29/42 6530-38 1009.37
6530-33
45/50 200 (8) (2) 29/42 – (2) 24/40 6530-39 981.02
45/50 200 (8) (2) 45/50 6530-40 975.35
6530 HEAD Domed, Schott-Duran Flange, 6 Necks, 60mm Side Port

Domed-style glass head with Schott-Duran style 200mm (8-inch) flange for use with
6530-37
matching flanged reactor flasks like 6472-02, 6472-16, 6522-21, etc. Features a
Schott-Duran flange 60mm (2.4-inch) I.D. side port with o‑ring groove, angled 45
degrees, for ease in adding materials to the reactor. In addition to the 60mm port,
head has a  45/50 center neck, (1)  45/50, (2)  29/42, and (2)  24/40 side necks.
Complete item includes head, 60mm glass cap, CAPFE (PTFE encapsulate silicone)
o‑ring, and 60mm quick release clamp. Main head uses 6517-31 quick release clamp
(not included).
Order Code Each

HEAD, only, 200mm (8-inch) flange 6530-37 1095.60
GLASS CAP, 60mm 15312-30 60.05
CAPFE O‑Ring, 60mm 7855-878 28.10
CLAMP, 60mm, Quick Release 6517-22 87.08
COMPLETE 6530-50 1270.83
6530 HEAD Domed, KF Plane Flange, 7 Necks, 100mm Side Port

6530-45
Domed-style glass head with 300mm (12-inch) flat KF plane flange for use with
matching reactor flasks like 6472‑03, 6472‑05, 6472‑030, 6472‑050 etc. Features a
large Schott-Duran flange 100mm (4-inch) I.D. side port with o‑ring groove, angled 30
degrees, for ease in adding materials to the reactor. In addition to the 100mm port,
head has a  45/50 center neck, (4)  45/50, and (2)  29/42 side necks. Complete
item includes head, 100mm glass cap, CAPFE (PTFE encapsulate silicone) o‑ring,
and 100mm quick release clamp. Main head uses 6525-30 clamp (not included).
Order Code Each

HEAD, only, 300mm (12-inch) KF flange 6530-45 2562.18
GLASS CAP, 100mm 15312-33 107.78
CAPFE O‑Ring, 100mm 7855-880 28.63
COMPLETE 6530-60 2796.82

6530 HEAD Domed, Schott-Duran Flange, 5 Necks, 60mm Side Port 6530-85
Domed-style glass photochemical reactor head with Schott-Duran style 200mm (8-inch)
flange for use with matching flanged reactors and flasks like 6472-02, 6472-16, 6522-21,
6524-73, etc. Features a Schott-Duran flange 60mm (2.4‑inch) I.D. side port with o‑ring
groove, angled 45 degrees, for ease in adding materials to the reactor. In addition to the
60mm port, head has a  45/50 center neck, (1)  45/50, (1)  29/42, (1)  24/40, and (1)
#50 Ace‑Thred side necks.
Order Code Each

HEAD, only, 200mm (8-inch) flange 6530-85 1213.52
GLASS CAP, 60mm 15312-30 60.05
CAPFE O‑Ring, 60mm 7855-878 28.10
6472 HEAD Domed, KF Plane Flange, 7 Necks 6472-23

Domed-style glass head with 300mm (12-inch) flat KF plane flange for use with matching
reactor flasks like 6472‑03, 6472‑05, 6472‑030, 6472‑050 etc. Head has a  45/50 center
neck, (4)  45/50, and (2)  29/42 side necks. Uses 6525-30 clamp (not included).
Order Code Each

HEAD, only 6472-23 2379.08
12858 HEAD PTFE, Reaction Flask, 60mm

12858-15
60mm PTFE heads allow for various combinations of jointed and/or compression fitting
openings as well as the ability to plug unused openings. For use with any Schott-Duran
style, o-ring grooved flanged reaction vessels such as ACE codes 6521, 6522, 6523,
6524 and 6526. For fittings, see ACE codes 12866, 12867, 12869 and 12871. Uses 6517
quick release clamps.
A) vertical 1/2-inch center neck for PTFE standard taper adapter
B) 10° x 10° 1/2-inch compound angle side neck
C) vertical 1/4-inch side neck
Number of
Order Code openings Each
12858-10 4 208.12
12858-15 4 193.24
12858-10

See page 121 for PTFE adapters, plugs, and connectors.

PTFE Inserts for PTFE Reaction Vessel Heads

NPT NPT
Size Order Size Order
Description (In.) Code Each Description (In.) Code Each
Joint Inserts Ace‑Thred Compression Fittings

19/38 PTFE PTFE Ace‑Thred
Standard Taper Adapter, 1/2 12866-05 40.48 1/4 12871-03 56.38
#7-NPT
Outer
PTFE Ace‑Thred
19/38 PTFE 1/2 12871-07 58.87
#7-NPT
Standard Taper Adapter, 3/4 12866-08 40.51
Outer PTFE Ace‑Thred
1/2 12871-11 61.38
24/40 PTFE #11-NPT
Standard Taper Adapter, 1/2 12866-14 45.62 PTFE Ace‑Thred
Outer 3/4 12871-14 81.42
#15-NPT
Standard Taper Adapter, 3/4 12866-16 45.59 3/4 12871-18 83.95
#18-NPT
Outer
1 12871-25 86.46
Standard Taper Adapter, 1 12866-18 50.56 #25-NPT
Outer PTFE Ace‑Thred
1-1/2 12871-28 93.96
29/42 PTFE #25-NPT
Outer Supplied with 5029 PTFE Bushing for #7 thread
29/42 PTFE and 7506 PTFE Bushing for all other threads.
Outer
29/42 PTFE
Standard Taper Adapter, 1 12866-25 65.72
Outer
29/42 PTFE
Standard Taper Adapter, 1-1/2 12866-27 88.51
Outer
45/50 PTFE
Outer
45/50 PTFE
Standard Taper Adapter, 1 12866-35 110.59
Outer
45/50 PTFE
Standard Taper Adapter, 1-1/2 12866-37 106.30
Outer
Plugs
PTFE Plug 1/4 12867-04 11.74
PTFE Plug 1/2 12867-12 14.86
PTFE Plug 3/4 12867-18 19.93
PTFE Plug 1 12867-24 24.57

12860 HEAD PTFE, Reaction Flask, 100mm,

12860-25 100mm PTFE heads allow for various combinations of jointed and/or compression fitting
A) vertical 3/4-inch center neck for PTFE standard taper adapter
B) vertical 3/4-inch side neck for PTFE standard taper adapter
C) 10° x 10° 1-inch compound angle side neck
D) vertical 1/4-inch side neck
E) 10° angled 3/4-inch side neck
Number of
12860-12 Order Code Openings Each
12860-12 7 348.95
12860-25 7 402.49
12862 HEAD PTFE, Reaction Flask, 150mm

12862 150mm PTFE heads allow for various combinations of jointed and/or compression fitting
A) vertical 1-inch center neck for PTFE standard taper adapter
B) vertical 1-inch side neck for PTFE standard taper adapter
D) vertical 1/2-inch side neck
Number of
Order Code Openings Each
12862-16 9 561.95
12864 HEAD PTFE, Reaction Flask, 200mm,

12864-20
200mm PTFE heads allow for various combinations of jointed and/or compression fitting
A) vertical 1-inch center neck for PTFE standard taper adapter
B) vertical 1-1/2-inch side neck for PTFE standard taper adapter
D) vertical 1/2-inch side neck for PTFE standard taper adapter
E) 10° x 10° 1-1/2-inch compound angle side neck
F) 10° angled 1-inch side neck
Number of
Order Code Openings Each
12864-20 8 723.33
12864-27 8 866.52
12864-27
Blank heads and custom configurations available. See page 121

for PTFE adapters, plugs, and connectors.

6525 COUPLING, ACCESSORIES For KF Style Flange

Coupling for clamping reaction flask to reaction flask heads like 6530‑45. Complete
6525‑25 or 6525‑30 coupling consists of two plastic, phenolic resin rings, set of three
clamp inserts with clamp insert clips, and appropriate number of stainless steel bolts,
springs, nuts and washers. The 6525‑72 or 6526‑74 inserts are placed inside the coupling
and used with the 6525-80 clamp insert clips to firmly secure the flask to the head. Preset
optional T-handle torque wrench, 30 in-lbs maximum, and 1/4‑inch socket are available
for safe tightening of coupling. Gaskets (required), wrench, and socket are not included
with coupling, and must be ordered separately.
Description Size Order Code Each

Coupling, Complete 200mm 6525-25 840.64
Coupling, Complete 300mm 6525-30 1056.54
6525-25, Accessories
-30 Torque Wrench, only — 6525-60 144.09
1/4-inch Socket, only — 6525-61 10.69
Replacement Parts
Clamp Insert (each insert = 3 arcs) 200mm 6525-72 59.46
Clamp Insert (each insert = 3 arcs) 300mm 6525-74 160.80
Clamp Insert Clips (package of three) — 6525-80 6.21
6525-72,
-74 Note: Flat heads require 6525 coupling, but with 6472-161 (longer) bolts/nuts
6525 GASKET
PTFE crescent ring “L” shaped gaskets for use with 6525 coupling. These gaskets are
placed between the flat ground glass surfaces of the head and flask. Consists of a flat
ring with locating skirt. Temperature limit, 200°C.
Size Order Code Each

6525-51
200mm 6525-46 164.23
300mm 6525-51 326.26
Color Coated Glassware

Ace Glass offers many of our existing
glass vessels in various coated versions.
Flasks, Pressure Bottles, Beakers,
Bottles and many other items listed
in this catalog can be amber or color
coated on request. The coating is a
proprietary process and gives excellent
UV protection characteristics. Contact
ACE for more details and pricing.

Components / Adapters 125
5021/9061 ADAPTER Reducing
Reducing adapter, bushing type, larger outside joint, smaller inside joint.
Top Bottom Order Top Bottom Order Top Bottom Order
Inside Outside Code Each Inside Outside Code Each Inside Outside Code Each
10/18 14/20 9061-05 31.70 14/20 24/40 5021-14 36.21 24/40 29/42 5021-28 42.04
10/30 14/20 9061-10 31.70 14/20 29/42 5021-15 40.10 24/40 34/45 5021-30 54.42 5021
10/30 14/35 5021-05 36.10 14/35 19/38 5021-18 35.53 29/42 34/45 5021-35 66.77 9061
10/30 19/38 5021-07 38.47 14/35 24/40 5021-20 39.53 24/40 45/50 5021-36 88.33
10/30 24/40 5021-09 41.53 14/35 29/42 5021-22 43.11 29/42 45/50 5021-94 88.63
10/30 29/42 5021-12 45.16 19/38 24/40 5021-24 37.41 34/45 45/50 5021-39 88.94
14/20 19/22 9061-16 31.70 19/38 29/42 5021-26 43.06
S IN N O
AS
5028 ADAPTER V“Mini” #7 Ace‑Thred, with PTFE Ferrule
L
G
AT
With inner joint atTH bottom and #7 Ace‑Thred at top. Suitable for most vacuum work.
AC E
Supplied complete with nylon bushing and PTFE ferrule in place of o‑ring. For extra
ON
ferrules, order 11710‑07.

1936 2011
Bottom Joint Order Code Complete
J
14/20 5028-27 27.95

V
N 24/40 , 5028-31 28.05

I
E LAND
5028-27
5028 ADAPTER Electrode, “Mini” #7 Ace‑Thred

With inner joint at bottom and #7 Ace‑Thred at top. For use with any probes up to 8mm
diameter. Suitable for most vacuum work. Supplied complete with 5029-30 nylon bushing
and FETFE o‑ring. For extra o‑rings, order 7855-704.

14/20 5028-117 32.39
24/40 5028-119 34.63 5028-117
6500 THERMOWELL with Joint

For reaction flasks, can be used with either cylindrical or spherical type. With  14/35
joint. Length measurement is distance below joint to bottom of tube.
6500
For Flask Length Order For Flask Length Order
Cap., mL mm, Code Each Cap., mL mm, Code Each
500 190 6500-01 32.32 5000 360 6500-05 35.87
1000 230 6500-02 32.32 12000 400 6500-06 37.90
1500 270 6500-03 32.32 22000 475 6500-08 47.74
2000 310 6500-20 34.10 50000 582 6500-10 54.52
3000 325 6500-04 35.64 72000 600 6500-12 67.07

126 Components / Adapters
5029 BUSHING Nylon or PTFE, #7 Ace‑Thred

Machine threaded nylon or #7 Ace‑Thred PTFE bushing with hole in center or solid. For
If o‑rings are a use with 5027, 5028, 5031, 5032, 5034, 5086, 5092, 5101, 5136, 5261, 5263 and other
problem, see 11710, apparatus with #7 internal threads. Two FETFE o‑rings supplied with bushing. Note: Solid
PTFE ferrules bushing is for drilling different size hole, only. NOT intended for use as a stopper. For
for use with stoppers, see 5803 or 5846. Nylon version has a maximum temperature of 100°C.
Ace‑Threds. PTFE version has a maximum temperature of 160°C.
Nylon PTFE
With 7.5mm hole 5029-10 2.77 5029-35 14.08
With 8mm hole 5029-30 8.65 5029-31 14.08
Solid 5029-20 8.28 5029-40 13.85
With 7.5mm hole, for use
with PTFE Ferrule 5029-12 2.91 5029-45 14.08
5029
Extra FETFE O‑Rings 7855-704 13.68
5030/7506/8042 ADAPTER “Maxi” #15 Ace-Thred

With ground joint at bottom and #15 Ace-Thred at top. Will accept tubes with diameters
of 12.5 to 14mm such as electrodes, inlet and outlet tubes, etc. Suitable for most vacuum
5030-40 work. Supplied complete with nylon bushing and FETFE o‑ring. For extra o‑rings, order
7855-716.
5030-44 Glass Only Nylon Bushing Only Complete
Bottom Order Order Order
Joint Code Each Code Each Code Each
24/40 8042-15 31.22 7506-06 12.35 5030-40 43.57
29/42 8042-17 33.38 7506-06 12.35 5030-42 45.73
45/50 8042-21 50.57 7506-06 12.35 5030-45 62.92
35/25 8042-35 35.92 7506-06 12.35 5030-44 48.27
5030/7506/8067 ADAPTER “Giant” #25 or #36 Ace‑Thred

With ground inner joint at bottom and either a #25 or #36 Ace‑Thred that accepts outside
diameters of 24-25mm and 34-35mm, respectively (Note: Joint size limits size O.D. of
inserted tube). Complete item supplied with nylon bushing and FETFE o‑ring. For o‑ring
replacements, see “Reference Guide to Ace‑Threds” on page 5.
Glass Only Nylon Bushing Only Complete

Bottom Ace‑Thred Order Order Order
5030-70 Joint Size Code Each Code Each Code Each
24/25 #25 5030-52 35.83 7506-10 21.17 5030-70 57.00
24/25 #36 5030-55 60.00 7506-12 50.46 5030-76 110.46
45/50 #36 5030-78 77.88 7506-12 50.46 5030-80 128.34
45/50 #25 8067-18 106.40 7506-10 21.17 5030-84 127.57
50/55 #25 8067-20 102.13 7506-10 21.17 5030-86 123.30
71/60 #25 8067-22 112.06 7506-10 21.17 5030-88 133.23
55/50 #36 8067-24 104.94 7506-12 50.46 5030-90 155.40
5031 ADAPTER “Twin” Ace‑Thred

With inner joint at bottom and two offset Ace‑Thred ports at top. Two threaded openings
enable you to insert two inner tubes, such as a thermometer and bleed tubes, through
the same joint. The  24/25 medium length joint is compatible with  24/40 full length
outer joints. Supplied complete with two nylon bushings and FETFE o‑rings. For extra
o‑rings, order 7855-704 (for #7), 7855-708 (for #11) or 7855-716 ( for #15).
5031 Thread Size Joint Order Code Each
#7 24/25 5031-10 79.08
#7 29/42 5031-12 83.26
#11 45/50 5031-24 99.60
#15 45/50 5031-33 106.17
#11 & #15 45/50 5031-86 119.50
5032 ADAPTER Offset, #7 Ace‑Thred

5032
Thermometer adapter with inner joint at bottom and top threaded piece offset and angled
approximately 10° for use in multiple neck flasks. Threaded nylon bushing tightens into glass
piece to form an o‑ring compression seal with thermometers, bleed tubes, etc. up to 7mm
diameter. Thread at top not only allows for variable vertical positioning of thermometers,
etc. but also, because of the 10° angle, by rotating joint you can position the thermometer in
the bottom of the flask. Supplied complete with nylon bushing and FETFE o‑ring. For extra
o‑rings, order 7855-704. For extra bushings, order 5029-10.

19/22 5032-18 40.00
24/40 5032-22 34.31
29/42 5032-25 37.09
5040/9074 ADAPTER 75° Side Arm

With inner joints at bottom and side, reinforced outer joint at top. 5040
9074
Top Outer Side Inner Bottom Inner Order
Joint Joint Joint Code Each
14/20 14/20 14/20 9074-02 48.70
19/22 19/22 19/22 9074-04 49.16
24/40 24/40 24/40 5040-10 56.65
29/42 29/42 29/42 5040-12 58.67
24/40 45/50 45/50 5040-96 169.62
5050 ADAPTER 105° Side Arm 5050-10

With reinforced outer joints at top and side, inner joint at bottom.
Joints Order Code Each
24/40 5050-10 58.60
29/42 5050-12 60.25
5050 ADAPTER 105° Side Arm, with Ace‑Thred

With reinforced outer joint on side, inner joint at bottom, and Ace‑Thred at top. Not 5050-86
supplied with bushing and FETFE o‑ring, which must be ordered separately.
Ace‑Thred
Joints Size Order Code Each
45/50 #25 5050-86 172.91
45/50 #15 5050-96 169.40
For Size Order Code Each

Bushing w/FETFE O‑Ring, only #15 7506-06 12.35
Bushing w/FETFE O‑Ring, only #25 7506-10 21.17
5090 ADAPTER 75° Angle

With joint at bottom and side. Top thermometer joint is for 76mm immersion.
Top Outer Immersion Side Inner Bottom Inner Order

Joint Depth Joint Joint Code Each
10/30 76mm 24/40 24/40 5090-10 54.70
10/30 76mm 29/42 29/42 5090-15 59.40
5090

5221-20 5221-05 5221-24

5221 ADAPTER Connecting, Outer Socket Joint, Glass
For connecting to comparable o‑ring/ball joints.
Outer Joint Connects to Size Order Code Each

10mm tube 28/15 5221-05 27.40
#11 Ace‑Thred 28/15 5221-09 33.57
#15 Ace‑Thred 28/15 5221-11 39.05
3/4-inch tube 35/25 5221-20 28.77
#15 Ace‑Thred 35/25 5221-24 36.64
#25 Ace‑Thred 35/25 5221-28 39.05
5221-28 5221-11
5221-09
5263 ADAPTER Multineck, “Mini” #7 Ace‑Thred

With  inner joint at bottom, two #7 Ace‑Threds and one side reinforced  outer joint at
top. Ace‑Threds would commonly be used for thermometers and gas inlet tubes thus
leaving joint for condenser, addition funnel, still head, etc.  24/25 medium length bottom
joint is compatible with  24/40 full length joint. Supplied complete with two 5029-10
nylon bushings and FETFE o‑rings. For extra FETFE o‑rings, order 7855-704.
Top Outer Bottom Inner Order Code Each

24/40 24/25 5263-17 126.79
5263
5268/9089 ADAPTER Offset
WITHOUT BOTTOM DRIP TIP WITH BOTTOM DRIP TIP
Joints Order Code Each Joints Order Code Each
14/20 9089-08 25.36 14/20 9089-40 34.88
24/40 5268-10 36.56 24/40 5268-54 37.33
29/42 5268-15 40.74 29/42 5268-56 41.60
45/50 5268-21 109.58 45/50 5268-58 110.94
35/25 5268-35 48.17
5268-54 5268-10 5268-35
9089-40 9089-08
5278 ADAPTER pH Probe, Pilot Plant 5278

Adapter tube, 25mm O.D., with a #15 Ace‑Thred at one end, other end open.
Insert 1/2-inch probe in open end down to and through the Ace‑Thred, leaving
enough exposed to secure with 7506 bushing and size –110 FETFE o‑ring to make
a compression seal. Adapter tube is held in flask  joint with 5030 “maxi” adapter
with nylon bushing and size –212 FETFE o‑ring, again with a compression seal,
thus making the tube vertically adjustable. Complete item consists of glass adapter
tube, 7506 PTFE bushing with size –110 FETFE or Chemraz o‑ring and 5030 “maxi” 5278-14
adapter. Takes any standard size pH probe. Adapter Tube
With FETFE O‑Ring With Chemraz O‑Ring

7506 Bushing
Length,
cm (Inches) Order Code Each Order Code Each
61 (24) 5278-40 146.63 5278-141 194.96
91 (36) 5278-44 147.40 5278-145 195.73
122 (48) 5278-48 5278-149 196.49 Adapter, “Maxi”
148.16 8067-18
Replacement Items:
ADAPTER TUBE, Glass only Bottom BUSHING, PTFE only, with O‑Ring
Length, Order For Thread O‑Ring Order
cm (Inches) Code Each Size Type Code Each
61 (24) 5278-14 22.14 15 FETFE 7506-27 40.65
91 (36) 5278-18 22.91 15 Chemraz 7506-127 88.98
122 (48) 5278-23 23.67
ADAPTER, “Maxi,” #25 Ace‑Thred to 45/50 Joint, only

Complete item includes glass member, nylon bushing and size –212 FETFE o-ring.
Glass Member Nylon Bushing Complete
Bushing, PTFE
Joint Order Code Each Order Code Each Order Code Each
45/50 8067-18 106.40 7506-10 21.17 5030-84 127.57
*pH probe not included.
12990 PROBE pH, Process Pilot Plants

pH probe for process applications consists of three parts; a rugged standard combination
pH probe, 3-ft lead and a 3-ft extension cord, total lead length 6-ft. BNC connector end for
connecting to ACE Impresario controller. Probe is 127mm long and has Ag/AgCl internals
and rugged epoxy body. 80ºC max temperature. Fits easily into Ace 5278 probe adapter.
Order
Code Each
12990-01 300.85

5853 “ACE-SAFE” CONNECTIONS Tubing, Polypropylene

Replacement tubing connector, used with nylon bushing to make easy and safe connect/
disconnect of coolant or steam tubing to jacketed reaction flasks, condensers, or any
vessel utilizing the Ace‑Thred as the connection port. Connector is fitted with a silicone
o‑ring. Bushing compresses connector and o‑ring for leak-tight seal. Once tubing is
5853 attached to serrated end of connector, bushing will not come off. Hose connections are
supplied with silicone o‑ring. For replacement o‑rings, order 7855-207 for Code -03;
7855-206 for codes -09 and -10; 7855-210 for code -18 and -21; 7855-772 for code -31
and -33. Maximum temperature is 110°C.
For #7 Ace‑Thred For #11 Ace‑Thred For #15 Ace‑Thred For #11 Ace‑Thred
to 1/4-inch I.D. Tubing to 1/4-inch I.D. Tubing to 1/4-inch I.D. Tubing to 3/8-inch I.D. Tubing
Order Code Each Order Code Each Order Code Each Order Code Each
Hose Connection, only, w/O‑Ring 5853-03 11.06 5853-09 10.54 5853-18 11.43 5853-10 10.54
Nylon Bushing, only 5029-05 2.50 7506-01 10.83 7506-05 12.20 7506-01 10.83
Complete 5853-06 13.53 5853-12 22.02 5853-20 24.36 5853-15 22.02
to 3/8-inch ID Tubing to 1/2-inch ID Tubing to 3/4-inch ID Tubing to 1-inch ID Tubing
Nylon Bushing, only 7506-05 12.20 7506-05 12.20 7506-09 19.30 7506-09 19.30
Complete 5853-23 24.36 5853-26 25.25 5853-35 47.44 5853-37 48.76
5858 “ACE-SAFE” CONNECTIONS Tubing, PTFE

Same as 5853 above, but manufactured from PTFE instead of polypropylene.
Connectors are supplied with FETFE o‑ring. For replacement o‑rings, order 7855-707
for Code -03; 7855-706 for codes -05 and -10; 7855-710 for code -07, -12, and -14.
Maximum temperature is 200°C.
5858
to 1/4-inch I.D. Tubing to 1/4-inch I.D. Tubing to 1/4-inch I.D. Tubing to 3/8-inch I.D. Tubing
PTFE Bushing, only, w/O-Ring 5029-35 14.08 7506-23 39.80 7506-27 40.65 7506-23 39.80
For #15 Ace‑Thred For #15 Ace‑Thred
to 3/8-inch ID Tubing to 1/2-inch ID Tubing
Hose Connection, only, w/O‑Ring 5858-12 31.11 5858-14 33.49
PTFE Bushing, only, w/O-Ring 7506-27 40.65 7506-27 40.65
5853/5858 Tubing Connector Reference Chart

(Flow Rate @10 lbs. H20)
Fits Connector Nominal
Tubing Connector Ace‑Thred I.D., Flow Rate Use Bushing Use O-Ring For Tubing I.D.,
Catalog No. Size in. (mm) Gal./Min. Number Number In. (mm)
5853-03 / 5858-03 7 .125 (3.18) 1.5 5029-05 / 5029-35 7855-207 / 7855-707 1/4 (6.35)
5853-09 / 5858-05 11 .125 (3.18) 1.5 7506-01 / 7506-23 7855-206 / 7855-706 1/4 (6.35)
5853-10 / 5858-10 11 .187 (4.74) 3.3 7506-01 / 7506-23 7855-206 / 7855-706 3/8 (9.5)
5853-18 / 5858-07 15 .125 (3.18) 1.5 7506-05 / 7506-27 7855-210 / 7855-710 1/4 (6.35)
5853-19 / 5858-12 15 .187 (4.74) 3.3 7506-05 / 7506-27 7855-210 / 7855-710 3/8 (9.5)
5853-21 / 5858-14 15 .375 (9.5) 13.3 7506-05 / 7506-27 7855-210 / 7855-710 1/2 (12.7)
5853-31 25 .500 (12.7) 23.6 7506-09 7855-772 3/4 (19)
5853-33 25 .750 (19) 53.3 7506-09 7855-772 1 (25.4)
6472 ADAPTER Beaded Pipe, for “Flush Valve”, Glass

Attach to 1-inch beaded pipe outlet on 6472-245 “Martin style” flush valve to adapt to
tubing NPT fitting.
Style Order Code Each

1-inch BP x 1/2-inch O.D. Tube 6472-275 50.38
1-inch BP x 1/2-inch I.D. Hose Conn. (Size G) 6472-276 53.03
1-inch BP x #15 Ace‑Thred 6472-277 59.67
1-inch BP x #25 Ace‑Thred 6472-278 64.97
6472-277, -278
12067 ADAPTER Connecting, Heat Exchange Coil

Stainless steel adapter for connecting 12067 heat exchange coil tubing to pipe thread
(NPT). Adapter fits over tubing and makes a compression seal via o‑ring for working
pressure of 25 psig. Complete item includes compression adapter, elbow, and pipe nipple.
Elbow Nipple O‑Ring

Adapter Size (Inches) (FPT) (MPT) (Size) Order Code Each
1/4 O.D. tube x 1/4 1/4-inch 1/4-inch -010 12067-02 39.63
See coils on page 150 12067-02
12187 ADAPTERS Stainless Steel, Circulator Hose

304 Stainless steel adapters designed for use with ACE jacketed glass pilot plant 12187-100
reactors and circulator hoses for popular circulating chillers. One style connects o‑ring
ball joints on jacket inlet/outlet to hoses to/from circulator. The other style connects
“M” style to NPT thread. 12187-05
Order
Connection Description Code Each
Flask to Hose, 28/15 Socket to M16x1 Male 12187-05 88.40
Flask to Hose, 35/25 Socket to M38x1.5 Male 12187-14 93.60
Hose to Circulator, M16x1 Male to 3/4 inch NPT Male 12187-100 93.60
Hose to Circulator, M30x1.5 Male to 3/4 inch NPT Male 12187-101 93.60
Hose to Circulator, M24x1.5 Male to 3/4 inch NPT Male 12187-102 93.60
5299 ADAPTER Distillation

Distillation adapter for use with bench or pilot plant reactors. Moisture is collected in
center vessel and drained off through the bottom stopcock which is ground to accept
a compression style fitting. Stopcock is PTFE plug. Available with either one or two top
standard taper outer joints.
With one top/outer T

joint
S
Stopcock Size, Compression Fitting Order

Joint mm Joint Size, In. Code Complete
24/40 6 1/2 5299-01 198.26
29/42 6 1/2 5299-03 247.40 5299-16
45/50 10 3/4 5299-07 326.01
With two top/outer T
joints
S
24/40 6 1/2 5299-10 231.20

29/42 6 1/2 5299-12 260.69
45/50 10 3/4 5299-16 398.83
5299-07

132 Components / Funnels
12560 FUNNEL Buchner, Table Top

POROUS FILTER PLATE type or PERFORATED PLATE type, fixed or removable,
polyethylene Buchner funnel. Features one-piece, welded construction with welded-in
plate and multiple-ring support grid below plate. A non-porous ring around plate seals
filter paper. Vacuum connection accepts 1/2-inch I.D. tubing. For use below 125°F (52°C).
FILTER PLATE is available in medium (M) or coarse (C) porosity, 1/4-inch (6.4mm) thick.
PERFORATED PLATE is 3/16 inches (4.8mm) thick with 3/16-inch perforations on 7/16-inch
(11mm) centers. Good for coarse filtration or use with cloth or paper filter.
Perforated Plate Porus Plate

Overall Rim to
I.D., Height Plate Order Plate Type/ Order
Inches (cm) (Inches) (Inches) Code Each Porosity ( ) Code Each
10-1/4 (26) 7 5 12560-14 352.50 Fixed/(M) 12560-02 352.50
10-1/4 (26) 7 5 12560-14 352.50 Fixed/(C) 12560-04 347.70
10-1/4 (26) 7 5 12560-50 352.50 Removable/(M) 12560-30 352.50
10-1/4 (26) 7 5 12560-50 352.50 Removable/(C) 12560-32 352.50
18 (45.7) 11-1/2 9 12560-16 745.50 Fixed/(M) 12560-05 862.90
18 (45.7) 11-1/2 9 12560-16 745.50 Fixed/(C) 12560-06 862.90
18 (45.7) 11-1/2 9 12560-57 745.50 Removable/(M) 12560-35 862.90
18 (45.7) 11-1/2 9 12560-57 745.50 Removable/(C) 12560-37 862.90
24 (61) 13 10-1/2 12560-18 1182.60 Fixed/(M) 12560-07 1793.40
24 (61) 13 10-1/2 12560-18 1182.60 Fixed/(C) 12560-08 1793.40
24 (61) 13 10-1/2 12560-59 1182.60 Removable/(M) 12560-38 1793.40
12560
24 (61) 13 10-1/2 12560-59 1182.60 Removable/(C) 12560-39 1793.40
36 (91.4) 14-3/4 12 12560-20 2108.10 Fixed/(M) 12560-09 2818.95
36 (91.4) 14-3/4 12 12560-20 2108.10 Fixed/(C) 12560-10 2818.95
36 (91.4) 14-3/4 12 12560-63 2108.10 Removable/(M) 12560-41 2818.95
36 (91.4) 14-3/4 12 12560-63 2108.10 Removable/(C) 12560-53 2818.95
FILTER PAPER is to fit 12560 funnels. Rough crepe surface, 0.25mm thick, flow rate
235mL / min., retention of 24 microns and wet strength of 25cm of water. Packed 100
per box.
For Funnel Size
(Inches) Order Code Per Box
10-1/4 12560-70 91.05
18 12560-72 169.95
24 12560-74 216.30
36 12560-76 862.15
12563 FUNNEL Buchner, All Stainless Steel

316 stainless steel Buchner funnel for organic or inorganic chemical synthesis. This funnel
incorporates a removable perforated plate that allows thorough manual cleaning and
autoclaving. Since the plate is removable, yield is increased because internal supports
that would trap product are eliminated. Will not chip, crack or break. Offered in 24cm and
50cm sizes that accept commercially available filter sizes. Completely electropolished
for critical applications, i.e., pharmaceuticals. Outlet port is 1/2-inch O.D.
Height Overall
Inside Dia., Above Disc Height Grit Order
cm (In.) (Inches) (Inches) Finish Code Each
12563 24 (9.5) 5 7 240 12563-09 6454.08
50 (20) 10 12 240 12563-27 8153.06
Components / Funnels 133
7233 FUNNEL Powder Dispensing, Vertical

A vertical, compact, screw feed funnel for the addition of powders and solids (up to 25
mesh) into reactions without seizing or binding. Features a flexible PTFE screw thread
average feed rate. Completely inert materials allow flushing with solvents without fear of
contamination. #15 Ace‑Thred at top offers easy disassembly for cleaning. Large 1-1/4-
inch knob makes turning smooth and easy. Top side port is S T  14/20 outer joint, bottom
inner joint is S
T  24/40. Overall height, 9-1/2 inches. 7233
50 7233-20 250.88
100 7233-30 282.08

Side operated screw feed funnel for the addition of powders and solids (up to 25 mesh)
to reactions without problems of seizing or binding.
Features a flexible PTFE screw thread wrapped on a precision PTFE-ceramic shaft and
contained within a precision bore housing. This offers a unique flexibility in that the thread
can move aside temporarily; as one spacing increases, the adjacent spacing decreases,
thereby maintaining an average feed rate.
Completely inert materials allow flushing with solvents without fear of contamination. #15
Ace‑Thred offers easy disassembly for cleaning. Large 1-1/4-inch knob makes turning
smooth and easy. Top outer and bottom inner joints are S T  24/40. S
T  14/20 outer joint atop
inner joint is for easier flushing.
Capacity, mL Order Code Each 7234

100 7234-25 331.84
250 7234-35 358.50

A vertical, compact, screw feed funnel for the addition of powders and solids (up to 25
mesh) into reactions without seizing or binding. Features a flexible PTFE screw thread
average feed rate. Completely inert materials allow flushing with solvents without fear
of contamination. #7 Ace‑Thred offers easy disassembly for cleaning. Top outer and bottom
inner joints are S
T 14/20. Approximate capacity, 15mL.

100 9485-15 238.41
9485

Side operated screw feed funnel similar to 7234 except ST 14/20 outer joint atop bottom
inner joint has been eliminated. Bottom ST joint and top S
T outer joints are 24/40. Same
features as 7233.

100 7239-30 267.61
250 7239-40 331.07
7239

7236/9488 FUNNEL Powder

Useful in pouring powders or liquids into ground joint containers. Available with JS or
T  inner
S joint.
Approx. T
S Approx. S
J
Top Dia., Bottom Order Top Dia., Bottom Order
mm Joint Code Each mm Joint Code Each
65 14/20 9488-10 32.15 100 35/25 7236-20 51.37
65 19/38 7236-06 42.84
75 24/40 7236-08 45.15
7236/9488 100 24/40 7236-10 47.70
125 24/40 7236-11 48.44
100 29/42 7236-12 51.13
125 34/45 7236-14 60.00
7238 FUNNEL Powder, 58° Offset, Heavy Wall

Offset funnel with heavy walls for greater durability when pouring powders or liquids into
multi-neck flasks.
Approx. Top
Dia., mm T
S Bottom Joint Order Code Each
75 24/40 7238-06 71.38
7238 100 24/40 7238-08 74.72
7245 FUNNEL Powder, Angled, H eavy Wall

Borosilicate funnel angled to permit use in multi-neck flasks. On angled neck flasks such
as 6948, this funnel will bring the mouth of the funnel back to vertical.
Top Diameter, Height A, T
S Bottom
mm mm Joint Order Code Each
A 75 120 24/40 7245-07 59.51
100 150 24/40 7245-15 69.98
100 195 29/42 7245-21 81.25
7245 200 200 45/50 7245-25 98.28
B 7250/6469 FUNNEL Powder, Flat Side

Powder funnel with S
T  joint and flattened side for easy use with multi-neck flasks.
T
S Bottom Top Opening (B), Height (A),
Joint mm mm Order Code Each
14/20 50 70 7250-01 40.10
24/40 75 90 7250-05 52.51
24/40 100 145 7250-09 60.85
A
29/42 145 145 7250-10 65.68
29/32 145 145 7250-12 65.68
45/50 150 250 6469-52 228.81
7250/ 71/60 255 255 7250-15 280.66
6469
Components / Funnels 135
7252 FUNNEL Powder, Schott-Duran Flange Bottom

Borosilicate glass powder or liquid addition funnels with a Schott-Duran Flange bottom.
Glass funnel fits onto 100mm or 60mm side ports on ACE 6530 glass reactor heads. Funnels
are slightly angled to allow for easy pouring of ingredients into reactors. Use the 6517 quick
release clamp to add to head. B
A
For Port Size Approx.
“C”, mm Volume, mL A, mm B, mm Order Code Each
60 1,800 200 160 7252-06 247.56
100 2,800 200 200 7252-10 296.00
7252
C
7295 FUNNEL Addition, with Offset
Graduated, borosilicate glass, liquid addition funnels with an offset bottom outlet and
T   joint. Bottom outlet has a PTFE stopcock. Top outlet has the same size S
S T  joint as the 7295
bottom. This design is ideal for crowded reactor heads, and allows for a larger addition
funnel to be used.
Approximate
Capacity, mL Length, mm T
S Joint Size Order Code Each
125 125 24/40 7295-03 180.52
250 250 24/40 7295-05 201.64 New
500 500 24/40 7295-07 216.42
1000 1000 24/40 7295-09 248.09
1000 1000 29/42 7295-11 254.42
7297 FUNNEL Graduated, Pressure Equalizing, PTFE Stopcock

Borosilicate glass addition funnel. Cylindrical shape with S
T  joints top and bottom. 7297-45
Funnel has a side pressure equalizing tube and has a PTFE plug stopcock. Inner drip
tube at bottom doesn’t extend below the main joint, to reduce breakage. 5L size has
100mL graduations.
Overall
Capacity, Stopcock Plug T
S Joint O.D., Length, Order
mL Bore, mm Size Graduations mm mm Code Each
125 2 24/40 1mL 38 345 7297-31 220.00
250 2 24/40 5mL 51 390 7297-33 251.93
500 4 24/40 5mL 64 430 7297-35 275.87
1000 4 24/40 100mL 75 500 7297-37 332.65
2000 4 29/42 100mL 85 650 7297-39 373.35
5000 8 45/50 100mL 155 565 7297-45 840.01
All full-length outer standard taper joints are reinforced.

7298 FUNNEL Pressure Equalizing, Graduated,

with PTFE Needle Valve Stopcock
Graduated addition funnel with threaded stopcock with PTFE plug permits smooth needle
valve adjustment down to 0.1mL/min. flow rate. Double PTFE ring seals prevent exposure
of backup o‑ring to corrosive liquids. Angled position makes manipulation of stopcock
easier than conventional style. ST  24/40 joints top and bottom, double scale graduations.
Capacity, Overall Stopcock Order
mL Length, mm Bore, mm Code Each
125 380 0-3 7298-05 231.90
250 385 0-3 7298-10 249.35
500 500 0-3 7298-15 278.92
500 500 0-5 7298-20 346.69
1000 565 0-5 7298-24 326.09
2000 760 0-5 7298-28 529.40
Replacement Stopcock Plugs:
For Size Order Code Each
7298 0-3 mm 8192-261 37.87
9493-40 0-5 mm 8192-263 52.16
7278 FUNNEL Addition, Separatory, Jacketed

Graduated addition funnels like 7268 series, except with outside jacket for cooling or
heating. Jacket extends from just below shoulder of vessel down to the bottom tube just
above the bottom stopcock. Stopcock is 4mm bore PTFE. Bottom drip tube extends to
the bottom edge of the lower, inner standard taper, joint, Top outer stopcock size matches
7278 the bottom joint size. Side hose connections are size D for 3/8-inch (9.5mm) ID tubing.
Capacity, Order
mL Joints Code Each
1000 24/40 7278-15 462.40
1000 29/42 7278-17 462.40
1000 29/32 7278-19 462.40
2000 29/42 7278-23 502.51
2000 29/32 7278-25 502.51
7281 FUNNEL Addition, Pressure Equalizing, Jacketed

Jacketed version of 7297 series addition funnels. Jacket runs from shoulder at top of
vessel to just above the PTFE stopcock with size D hose connections for 3/8-in ID tubing.
Equalizing side arm runs from top of vessel to just below the stopcock. Graduations are
both ascending and descending volume. Top and bottom standard taper joints are the
same size. Bottom drip tip extends to the edge of the bottom inner joint. Top outer joint
is reinforced. PTFE stopcock plug is 4MM bore.
Capacity, mL Joints Order Code Each

1000 24/40 7281-14 484.57
1000 29/42 7281-16 484.57
1000 29/32 7281-18 484.57
2000 29/42 7281-22 626.03
7281 2000 29/32 7281-24 626.03
Components / Condensers 137
S I N C OR
S P
A
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ACE G
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1936 2011
VI USA
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LAND

138 Components / Condensers
5945 CONDENSER Allihn, Pilot Plant

Bulb type, approximately one bulb per every 50mm, with  or  joint at bottom and top.
5945 Use with 3/8‑inch I.D. tubing, size D hose connections. See page 5 for more detailed
hose connection information.
Jacket
Length, mm Joints Order Code Each
500 24/40 5945-16 142.23
600 24/40 5945-17 145.06
500 29/42 5945-26 150.81
600 29/42 5945-27 173.65
5945/5946 CONDENSER Allihn, with Ace‑Thred Connectors

Bulb type, approximately one bulb per 50mm, with  inner and outer joint at bottom and
e top, #7 Ace‑Thred and “Ace-Safe” hose connections on inlet and outlet with barb for
lu 1/4-inch I.D. tubing. For replacement connectors, see 5853.
Va
5946 Jacket
Length, mm Joints Order Code Each
250 24/40 5946-116 143.67
300 24/40 5946-118 152.29
300 29/42 5946-122 152.29
E-SA 500 45/50 5945-76 382.96
AC
FE
ON
OR
C
N ECT
5958 CONDENSER Cold Finger, Pilot Plant Reactors

Jacket length is measured from the lower shoulder of the bulb to the bottom of the
finger. Diameter of tube is 14mm. Used in 6472 pilot plant reactors. Use with 5030-45
#15 Ace‑Thred adapter to fit top  45/50 joint in 5945-76 condenser. Can also be used
with 6015, 6016, and 6020 condensers. Use with 5/16-inch or 3/8-inch I.D. tubing, size
C hose connections. See page 5 for more detailed hose connection information.
Jacket Order
Length, mm Code Each
625 5958-99 92.87
5958
5960 CONDENSER Cold Finger

With  joint. The 5960-12 condenser is used with our 6606, 6609, and 6613 distilling
heads and 5943, 5945 and 5946 condensers. See page 5 for more detailed hose
connection information.
Length Below Tubing Order
Joint, mm Joint Size (Inches) Code Each
110 24/40 3/8 (D) 5960-08 94.16
215 24/40 3/8 (D) 5960-12 88.67
5960
6012 CONDENSER Pilot Plant, Long Path

Turbulent flow created makes this condenser very desirable for use under reduced
pressure. Internal and external cooling surfaces result in high efficiency per unit length.
24/40 inner and outer joints. Use with 7/16-inch or 1/2-inch I.D. tubing, size F hose
connections. See page 5 for more detailed hose connection information.
Jacket
Length, mm Order Code Each
500 6012-16 829.93
600 6012-17 849.88
6012
Custom condensers with various joint or length sizes are

available upon special request.

E-SA 6015 CONDENSER Double Coil, High Capacity, Pilot Plant
AC
FE
High throughput double coil condensers are made for larger systems and large-scale
ON
reactors, to handle larger scale reactions. These are also similar to rotary evaporator
OR
C
N ECT type condensers where a lot of material is being condensed at a higher temperature and
where large amounts of cooling water are needed to generate higher efficiency. The unit
can be ordered with standard taper joints or beaded pipe end connections. The overall
length is approximately 390mm and O.D.is approximately 85-90 mm. Both units have
#15 Ace‑Thred side connections for Ace-Safe hose connections. Supplied with full Ace
Safe connections.
Jacket Length, Condensing
mm Area, cm2 End Finish Order Code Each
315 1480 1-inch bead pipe 6015-12 644.26
290 1400 45/50 6015-17 708.70
6015-17 6015-12
6016 CONDENSER Pilot Plant

Highly efficient. May be used either for thorough condensation or refluxing. Internal
baffling acts as impinging surface for entrained particles and discourages diffusion loss.
Use with 7/16-inch or 1/2-inch I.D. tubing, size F hose connection. Available with either
spherical or standard taper joint.
Joint Size 45/50 Joint Size 71/60 Joint Size 35/25 Joint Size 65/40
Jacket
6016 Length, Order Order Order Order
mm Code Each Code Each Code Each Code Each
500 6016-36 923.04 — — 6016-66 919.15 6016-75 972.51
750 6016-39 1059.31 6016-52 1176.47 — — 6016-77 1048.01
1000 6016-41 1255.92 — — 6016-69 1237.21 6016-79 1328.76
6016 CONDENSER Pilot Plant, with Side Ace‑Thred Connectors

Highly efficient. May be used either for thorough condensation or refluxing. Internal
baffling acts as impinging surface for entrained particles and discourages diffusion loss.
With #11 side Ace‑Thred and “Ace-Safe” hose connections on inlet and outlet with
barb for 1/4-inch I.D. tubing. Available with either spherical or standard taper joints.
Joint Size 45/50 Joint Size 35/25 Joint Size 65/40
E-SA Jacket Order Order Order
AC
Length, mm Code Each Code Each Code Each

FE
500 6016-137 947.33 6016-167 930.09 6016-176 982.69

ON
OR
C
N ECT 750 6016-139 1083.60 — — 6016-178 1057.13

1000 6016-141 1280.21 6016-170 1243.55 6016-180 1333.79
6016
6017 CONDENSER Triple Coil, High Capacity E-SA
AC
FE
With three internal cooling coils, this new design gives even higher throughput than the
double coil or any rotary evaporator condenser. Designed for pilot plants and larger ON 6017
OR
C
reactors where a lot of cooling area is needed for condensing or for higher temperature N ECT
reactions where more throughput is needed. Comes with #15 Ace‑Thred ports with or
without Ace-Safe connections. Top and bottom connections are 2-inch beaded pipe.
Overall length is approximately 460mm and O.D. is approximately 110mm.
Glass only Complete
Coil Condensing
Length, mm Area, cm2 Order Code Each Order Code Each
220 1600 6017-210 822.02 6017-212 870.74
6020 CONDENSER Spiral, Reflux

With spiral condensing tube having both inlet and outlet connections at top, on same
side.With inner and outer joints at bottom and top. Length between joints is approximately
80-90mm longer than coil length.
Coil Length, Tubing Size
mm Joints (Inches) Order Code Each
200 24/40 3/8 (D) 6020-02 213.34
250 24/40 3/8 (D) 6020-04 229.00 6020
300 24/40 3/8 (D) 6020-06 236.11
400 24/40 3/8 (D) 6020-08 260.30
300 29/42 3/8 (D) 6020-10 240.15
400 45/50 3/8 (D) 6020-12 315.13
6021 CONDENSER Modified Keenan, Dual Coil, Horizontal

Highly efficient, double coil condenser with 30 degree horizontal angle vs. typical
vertical style. Great for under hoods or on pilot plant reactors where height may be an
issue and a high level of distillation is required. Condenser has a 45/50 bottom joint
to fit on reactor heads, all other connections are either #7 or #15 Ace-Safe, (supplied).
Comes with either a PTFE or glass stopcock. Overall length is approximately 470mm.
Height from top of bottom joint to highest point at top is 90mm.
Joints Stopcock Type Order Code 6021

45/50 PTFE 6021-20 Priced Upon
45/50 Glass 6021-30 Request
6022 CONDENSER Keenan, Single Tube, Horizontal

Highly efficient, newly designed condenser. Features a horizontal angle for low clearence
but extremely good capacity and throughput. Especially useful when assembling large
reactor in limited height clearance situations. Surface area is 710 cm2. Cooling fluid
volume: 600 mL. Condenser has a  45/50 bottom joint. All other connections are #7 or
#15 Ace‑Thred that accepts a 7mm O.D. tube or 5853 “Ace-Safe” connectors (supplied)
to attach tubing. Overall length: 475mm.
Joints Stopcock Type Order Code 6022

45/50 Glass 6022-22 Priced Upon
45/50 PTFE 6022-30 Request

6810 CONDENSER Pilot Plant, Bulb Type

Pilot plant bulb-type Soxhlet condenser. Use with 7/16-inch or 1/2-inch I.D. tubing, size
F hose connections. See page <OV> for more detailed hose connection information.
Overall Condenser
Length Length Bottom
(mm) (mm) Joint Length, mm Order Code Each
450 340 71/60 340 6810-04 296.18
6810
525 375 103/60 460 6810-14 551.81
930 730 55/50 730 6810-24 702.05
7744 RECEIVER, MOISTURE TEST Barrett Type, Pilot Plant

One liter Barrett type moisture test receiver. 2mm PTFE stopcock on bottom for
draining contents. 45/50 joints at top and on side arm. 60mm distance between
side arm and body for clearance on spherical or cylindrical reactor bodies. Graduated
in 10mL subdivisions.
Order
Code Each
7744-50 1810.83
7744
Custom configurations are available. Call 800-223-4524

or email sales@aceglass.com.
AC E-SA 6024/6029 CONDENSER West

FE
West style condenser for use with 6433 threaded or 6527, 6528 or 6529 jointed heads.
6029
ON OR 6024-20 supplied with #15 Ace‑Thred at top for 5846 plug (not supplied) and drip stem
C
N ECT
with groove, and long enough to be secured in #15 Ace‑Thred with 7506-06 bushing
and o‑ring (not supplied) to restrict blowout. With #7 Ace‑Thred on inlet/outlet for use
with “Ace-Safe” 5853 tubing connectors. Supplied with bushing and connectors for
1/4‑inch I.D. tubing.
6029-13 supplied with   24/40 joint at top and bottom and D size barbed hose connection
on inlet/outlet for 1/4‑inch I.D. tubing.
Use with Head No. Jacket Length, mm Order Code Each

6433 200 6024-20 129.75
6527,6528,6529 250 6029-13 105.87
6024
6042 CONDENSER Reflux, Bulb

New New style, compact, high-output reflux condenser, has an inner double wall, thimble-
shape internal bulb. Overall height is approximately 250mm, but has the output equal
to condensers with twice the length. Unit has outer top joint and drip-tip inner
joint bottom. Top and bottom hose connections size D (see page 5 for sizing),
for 3/8‑inch tubing.
Angled Top Inner Drip-Tip
Joint Bottom Joint Order Code Each
24/40 24/40 6042-04 205.40
29/42 29/42 6042-06 216.06
29/32 29/32 6042-08 200.78
45/50 45/50 6042-10 343.50
6042
6046 CONDENSER Angled

Condenser similar to the 5945 series except with a 45 degree angle on the bottom joint.
When using with ACE reactor heads, this allows for height space savings vs. the standard
New vertical condensers in reactor systems. Has joints at top and bottom. Hose barbs are
glass size D (see page 5 for sizing) for 3/8-inch ID tubing.
Jacket Length, mm Joint Size Order Code Each

300 24/40 6046-03 114.75
300 29/42 6046-05 128.11
6046 400 24/40 6046-09 130.56
400 29/42 6046-11 131.58
400 35/45 6046-13 137.70
500 24/40 6046-17 131.58
500 29/42 6046-19 139.74
600 24/40 6046-23 139.74
600 29/42 6046-25 145.86
600 35/45 6046-27 151.98

3965-10,
-15
3965-05,
-07
3965-26,
3965-19, -28
-22
3965 CONDENSERS Triple Coil

The condensers are available in either poly-coated or plain, non-coated versions. All condensers fit easily into the glass sets listed
below. DN40 inner ball joints include CAPFE (PTFE-encapsulated silicone rubber) o-rings. Black caps (included) are SVL-22 threads;
red cap (included) is GL-14 thread.
Fits Similar Ball/Socket
Glassware to Buchi® Fits DN Joint Uses O-Ring Order
Description Set Coated? Part No. Buchi® Models Sizes Size / Code Code Each
Triple-Coil Condenser R, D2 Yes 41159 R220, 40 –225 / 7855-844 3965-05 3114.32
Triple-Coil Condenser R, D2 No 41399 R200EX, SE 40 –225 / 7855-844 3965-07 3008.75
Triple-Coil Condenser D, D2 Yes 27308 R220 40 –225 / 7855-844 3965-10 3747.74
Triple-Coil Condenser D, D2 No 41333 R200EX, SE 40 –225 / 7855-844 3965-15 3642.17
Glass Condenser (Bullfrog) DB, DB2 Yes 27825 R220 40 –225 / 7855-844 3965-19 5273.22
Glass Condenser (Bullfrog) DB, DB2 No 46516 R220EX, SE 40 –225 / 7855-844 3965-22 5162.37
Glass Condenser (Bullfrog) RB, DB2 Yes 27824 R220 40 –225 / 7855-844 3965-26 5273.75
Glass Condenser (Bullfrog) RB, DB2 No 41458 R220 40 –225 / 7855-844 3965-28 5067.36
Also available with standard taper or process pipe joints
Components / Distillation Columns 145
6565 DISTILLATION COLUMN Perforated Plate

Perforated plate column, without jacket. Holes are 0.032-inch diameter
Plate Plate
No. of Dia., Order No. of Dia., Order 6565
Plates mm Joint Code Each Plates mm Joint Code Each
5 28 29/42 6565-02 801.86 5 50 55/50 6565-32 1453.40
10 28 29/42 6565-04 1324.56 10 50 55/50 6565-34 2421.26
15 28 29/42 6565-06 1840.10 15 50 55/50 6565-36 3263.06
20 28 29/42 6565-08 2368.22 20 50 55/50 6565-38 4167.04
30 28 29/42 6565-10 3789.74 30 50 55/50 6565-40 6349.38
5 33 34/45 6565-12 972.95 5 75 71/60 6565-42 3068.00
10 33 34/45 6565-14 1903.54 10 75 71/60 6565-44 6014.81
15 33 34/45 6565-16 2703.86 15 75 71/60 6565-46 7540.85
20 33 34/45 6565-18 3746.43 20 75 71/60 6565-48 9462.64
30 33 34/45 6565-20 5832.12
5 40 45/50 6565-22 1273.57 5 100 103/60 6565-52 5466.54
10 40 45/50 6565-24 2431.16 10 100 103/60 6565-54 8586.13
15 40 45/50 6565-26 3335.31 15 100 103/60 6565-56 11998.06
20 40 45/50 6565-28 4453.18 20 100 103/60 6565-58 14435.73
30 40 45/50 6565-30 5893.46
Large-scale Chromatography columns, see page 261

146 Components / Distillation Columns
6566 DISTILLATION COLUMN Perforated Plate, Internal Bellows, Silvered

Similar to 6565 except with vacuum-jacketed internal bellows and silvered internally.
Plate Plate
No. of Dia., Order No. of Dia., Order
Plates mm Joint Code Each Plates mm Joint Code Each
5 28 29/42 6566-03 1110.48 5 50 55/50 6566-33 2052.65
10 28 29/42 6566-05 1786.20 10 50 55/50 6566-35 3902.58
15 28 29/42 6566-07 2473.18 15 50 55/50 6566-37 4625.35
20 28 29/42 6566-09 3367.70 20 50 55/50 6566-39 5491.75
30 28 29/42 6566-11 4420.88 30 50 55/50 6566-41 7603.81
5 33 34/45 6566-13 1731.53 5 75 71/60 6566-43 3805.55
10 33 34/45 6566-15 2285.59 10 75 71/60 6566-45 6392.42
15 33 34/45 6566-17 3575.66 15 75 71/60 6566-47 8738.56
20 33 34/45 6566-19 4395.96 20 75 71/60 6566-49 10933.52
30 33 34/45 6566-21 5917.11
5 40 45/50 6566-23 2125.66 5 100 103/60 6566-53 6308.82
10 40 45/50 6566-25 3276.51 10 100 103/60 6566-55 9149.10
15 40 45/50 6566-27 4219.64 15 100 103/60 6566-57 13377.08
20 40 45/50 6566-29 5436.73 20 100 103/60 6566-59 15244.10
30 40 45/50 6566-31 6097.17
Ace Glass offers various types of column packing

material. Please contact Technical Services at
800-223-4524 or visit our website.
6566
6088 SPLITTER Distillation, Reflux

Reflux distillation splitter adapters for all size reactors. Standard taper, inner joint bottom,
6088
standard taper, outer joint top. A slight angle to bottom inner standard taper joint allows
for addition to reactor heads with angled side necks and keeps splitter straight for flow
upward to the condenser. Three standard joint sizes are available. Side valve is 0-10 with
a 1/2-inch precision ground bottom take-off that matches 1/2-inch compression fittings.
Valve replacement FETFE o-rings are size -011 and -111.
Joints Qty. Order Code Each

24/40 1 6088-08 326.40
29/42 1 6088-10 351.90
29/32 1 6088-12 351.90
45/50 1 6088-14 402.90
Components / Distillation Columns 147
6569 DISTILLATION COLUMN Vacuum Jacketed

With internal expansion bellows. Baked out and evacuated to 10-6 Torr. All  top
joints are jacketed. Spherical joints are not jacketed in order to allow for clamping.
All vacuum jacketed distilling columns are furnished with internal type expansion
bellows to compensate for the unequal expansion between the inside tube and the
outer jacket and will withstand a temperature differential of 180°C. All columns,
regardless of length, are supplied with the proper number of bellows to withstand the
above temperature differential at all times. Standard silvered columns are supplied
with an observation stripe running down the entire length of the jacket.
The packing support is a conical tripod in which the free area is at least 90% of the
diametrical area. In addition to the columns listed, we also have facilities for fabricating
a complete line of special vacuum jacketed units to your specifications. This includes
additional bellows to enable you to maintain temperature differentials greater than 180°C.
When ordering a special column, please specify the highest temperatures which may
be reached in the column, so that we can supply the unit with sufficient bellows to take
care of the expansion which may take place during distillation.
Length, cm I.D., mm Joints Order Code Each

61 12.7 24/40 6569-40 1169.98
61 25.4 29/42 6569-50 1187.37
61 25.4 35/25 6569-60 1193.17
91 12.7 24/40 6569-42 1309.28
91 25.4 29/42 6569-52 1326.68
91 25.4 35/25 6569-62 1332.48
122 12.7 24/40 6569-44 1547.10
122 25.4 29/42 6569-54 1564.50
122 25.4 35/25 6569-64 1570.30
6569
6087 SPLITTER Distillation, Reflux

Used to “take off” liquid distillate, splitter is installed between boil-up pot or fractionating
column and condenser. Main body is approximately 4 inches in diameter with #7 Ace‑Thred
and bushing for 1/4-inch diameter thermoprobe to monitor vapor temperature. Upper
alembic chamber has 2-inch diameter domed tube with two 1-1/4-inch diameter holes
for vapor flow upwards to condenser while preventing condensate from returning to pot.
Side 0-20mm PTFE stopcock allows take off when closed and reflux return when open.
Take-off tube terminus is 35/25 o‑ring ball joint. 350mm overall height. All o‑rings are
Kalrez for maximum chemical resistance. Joints are  45/50 inner on bottom,  45/50
outer on top.
Joint Size Side Port Order Code Each

45/50 35/25 o‑ring Ball Joint 6087-10 2122.41
6087
Columns can be custom designed and quoted to meet your

specifications. Non-silvered columns are available via special order.

148 Components / Spargers
6452 SPARGER Easy Action Stopcock and Hose Connection

Sparger tube with ACE frit at bottom, 0-3mm or 0-5mm Easy Action stopcock at top,
and 90° hose barb connecztion side port. See page 5 for more detailed hose connection
information. To connect this sparger to a head, use a 5030 adapter that matches the
Ace‑Thred sizes listed below.
Glass Fits
Overall Tubing Tube Ace‑Thred
Length, Stopcock Connection O.D., Adapter Order
mm Porosity Size Size (Inches) mm Size Code Each
400 A (145-174 micron) 0-3 C (5/16) 10 11 6452-03 188.78
400 B (70-100 micron) 0-3 C (5/16) 10 11 6452-05 188.78
400 C (25-50 micron) 0-3 C (5/16) 10 11 6452-07 188.78
575 A (145-174 micron) 0-5 D (3/8) 14 15 6452-14 217.94
575 B (70-100 micron) 0-5 D (3/8) 14 15 6452-16 217.94
575 C (25-50 micron) 0-5 D (3/8) 14 15 6452-18 217.94
6452-14 775 B (70-100 micron) 0-5 D (3/8) 14 15 6452-33 228.06
915 B (70-100 micron) 0-5 D (3/8) 14 15 6452-44 234.39
6452 SPARGER Easy Action Stopcock and #7 Ace-Safe Connection

Sparger tube with ACE frit at bottom, 0-3mm or 0-5mm Easy Action stopcock at top,
and 90° #7 Ace-Safe Connector side port for use with 7mm O.D. tubing. Supplied with
5853-06 Ace‑Safe Connector (complete item includes nylon bushing and FETFE o-ring).
For replacement nylon bushing only, order 5029-05. For replacement FETFE o‑ring only,
order 7855-706. For replacement Ace-Safe Connector only, order 5853-03. To connect
this sparger to a head, use a 5030 adapter that matches the Ace‑Thred sizes listed below.
E-SA
Glass Fits
AC
FE
Tube Ace‑Thred
ON Overall Stopcock O.D., Adapter
OR
C
N ECT Length, mm Porosity Size mm Size Order Code Each

400 A (145-174 micron) 0-3 10 11 6452-104 234.39
400 B (70-100 micron) 0-3 10 11 6452-106 234.39
400 C (25-50 micron) 0-3 10 11 6452-108 234.39
575 A (145-174 micron) 0-5 14 15 6452-121 239.47
575 B (70-100 micron) 0-5 14 15 6452-123 239.47
575 C (25-50 micron) 0-5 14 15 6452-125 239.47
775 B (70-100 micron) 0-5 14 15 6452-132 252.14
915 B (70-100 micron) 0-5 14 15 6452-145 259.72
6452-121
See page 149 for 5030 adapters.
Components / Spargers 149
6453 SPARGER Straight and #7 Ace‑Thred

Straight sparger tube with ACE frit at bottom and #7 Ace‑Thred connection at top for
7mm O.D. tubing connection. Supplied with 5853-06 Ace‑Safe Connector (complete item Use 5853-06
includes nylon bushing and FETFE o-ring). For replacement nylon bushing only, order Ace-Safe Connector
5029-05. For replacement FETFE o‑ring only, order 7855-706. For replacement Ace-Safe here!
Connector only, order 5853-03. To connect this sparger to a head, use a 5030 adapter
that matches the Ace‑Thred sizes listed below.
E-SA
AC
FE
Fits
Ace‑Thred
ON
OR
C
Overall Tube O.D., Adapter N ECT
Length, mm Porosity mm Size Orde Code Each
400 A (145-174 micron) 10 11 6453-105 144.58
400 B (70-100 micron) 10 11 6453-107 144.58
400 C (25-50 micron) 10 11 6453-109 144.58
575 A (145-174 micron) 14 15 6453-122 147.13
575 B (70-100 micron) 14 15 6453-124 147.13
575 C (25-50 micron) 14 15 6453-126 147.13
775 B (70-100 micron) 14 15 6453-133 147.13
915 B (70-100 micron) 14 15 6453-146 154.82
6453-122
6453 SPARGER Straight with Hose Connection

Straight sparger tube with ACE frit at bottom and size F hose connection at top for 1/2‑inch
I.D. hose. See page 5 for more detailed hose connection information. To connect this
sparger to a head, use a 5030 adapter that matches the Ace‑Thred sizes listed below.
Fits
Ace‑Thred
Overall Tube O.D., Adapter
Length, mm Porosity mm Size Order Code Each
400 A (145-174 micron) 10 11 6453-04 83.17
400 B (70-100 micron) 10 11 6453-06 83.17
400 C (25-50 micron) 10 11 6453-08 83.17
575 A (145-174 micron) 14 15 6453-21 88.27
575 B (70-100 micron) 14 15 6453-23 88.27
575 C (25-50 micron) 14 15 6453-25 88.27
775 B (70-100 micron) 14 15 6453-32 92.12
915 B (70-100 micron) 14 15 6453-45 94.66
6453-21

150 Components / Baffles
12177 BAFFLE PTFE
Fabricated from virgin PTFE (meets USP Class 6 requirements), this fully encapsulated,
seamless baffle with a stainless steel reinforcing core fits through standard taper joint of
reaction flasks to increase agitation and promote mixing. Takes the place of indented or
Morton vessels that can be a problem when using pressure or vacuum. Shaft of baffle
is sized to be secured using 5030 Ace‑Thred adapter with nylon bushing and FETFE
o‑ring. This connection allows vertical and rotational adjustment of the baffle inside the
flask for optimum effect. In place of o‑ring, a PTFE ferrule can be used for maximum
chemical resistance.
Fits
Shaft Shaft Ace‑Thred Baffle Overall
Diameter, Length, Adapter W x L x D, Length, Use Adapter Order
12177 mm mm Size mm mm (sold separately) Code Each
6.4 175 #7 18 x 152 x 10 327 5028-30 12177-145 379.26
10 180 #11 18 x 150 x 10 330 5030-22 12177-148 424.39
13 220 #15 30 x 150 x 12 380 5030-42/-45 12177-152 649.26
13 300 #15 30 x 250 x 12 550 5030-42/-45 12177-154 717.88
25 250 #25 32 x 360 x 14 610 5030-80 12177-157 746.38
12177 BAFFLE Glass
Borosilicate glass baffle fits through standard taper joint of reaction flasks to increase
agitation and promote mixing. Takes the place of indented or Morton vessels that can be
a problem when using pressure or vacuum. Shaft of baffle is sized to be secured using
5030 Ace‑Thred adapter with nylon bushing and FETFE o‑ring. This connection allows
vertical and rotational adjustment of the baffle inside the flask for optimum effect. In place
of o‑ring, a PTFE ferrule can be used for maximum chemical resistance. Order baffle,
adapter and optional ferrule separately. Custom sizes can be made to order.
Fits
12177 Shaft Shaft Ace‑Thred Baffle Overall
mm mm Size mm mm (sold separately) Code Each
10 250 #11 18 x 60 x 6.4 310 5030-22 12177-10 54.90
10 350 #11 18 x 90 x 6.4 440 5030-22 12177-13 61.23
12.7 400 #15 36 x 65 x 9.5 465 5030-42 12177-19 99.24
12.7 500 #15 36 x 100 x 9.5 600 5030-42 12177-23 102.40
12193 BAFFLE PTFE, for Temperature Probe

Similar to 12177 PTFE baffle but with stainless steel inner reinforcing tube and #7 Ace‑Thred
New machined into PTFE at bottom that accepts 1/4-inch diameter thermocouple or tubing.
The Ace‑Thred makes a compression seal with bushing and Kalrez o‑ring. Probe or tubing
can be extended below baffle tip to any desired length. Can be used for subsurface liquid
addition or withdrawl when used with tubing. Thermocouple not included.
Fits
Shaft Shaft Ace‑Thred Baffle Overall
mm mm Size mm mm (sold separately) Code Each
12193 10 180 #11 18 x 150 x 10 330 5030-22 12193-03 459.23
13 220 #15 30 x 250 x 12 380 5030-42/-45 12193-07 770.66
25 250 #25 32 x 360 x 14 610 5030-80 12193-09 809.72
E-SA
AC
FE
ON
OR
C
N ECT
5030/7506 ADAPTER “Midi” #11 Ace‑Thred

With ground joint at bottom and #11 Ace‑Thred at top. Will accept inner tubes with
diameters of 9mm to 10.5mm such as thermowells, gas dispersion tubes, vacuum
take-offs, etc. Suitable for most vacuum work. Supplied complete with nylon bushing 5030-28 5030-20
and FETFE o‑ring. For extra o‑rings, order 7855-708. See 6470 for thermowell.

Joint Code Each Code Each Code Each
19/22 5030-04 27.92 7506-02 11.39 5030-20 39.31
24/40 5030-06 28.65 7506-02 11.39 5030-22 40.04
29/42 5030-08 33.59 7506-02 11.39 5030-24 44.98
45/50 5030-60 51.58 7506-02 11.39 5030-19 62.97 E-SA
AC
FE
35/25 5030-16 40.00 7506-02 11.39 5030-28 51.39
ON
OR
C
N ECT
5030/7506/8042 ADAPTER “Maxi” #15 Ace‑Thred E-SA
AC
FE
With ground joint at bottom and #15 Ace‑Thred at top. Will accept tubes with diameters
of 12.5 to 14mm such as electrodes, inlet and outlet tubes, etc. Suitable for most vacuum ON
OR
C
work. Supplied complete with nylon bushing and FETFE o‑ring. For extra o‑rings, order N ECT
7855-716.
Glass Only Nylon Bushing Only Complete 5030-40

Joint Code Each Code Each Code Each 5030-44
24/40 8042-15 31.22 7506-06 12.35 5030-40 43.57
29/42 8042-17 33.38 7506-06 12.35 5030-42 45.73
45/50 8042-21 50.57 7506-06 12.35 5030-45 62.92
35/25 8042-35 35.92 7506-06 12.35 5030-44 48.27
5030/7506/8067 ADAPTER “Giant” #25 or #36 Ace‑Thred

With ground inner joint at bottom and either a #25 or #36 Ace‑Thred that accepts
outside diameters of 24-25mm and 34-35mm, respectively (Note: Joint size limits size
O.D. of inserted tube). This item can be used with ultrasonics equipment. 5030‑70 will E-SA
accept 9852‑41 slide adapter; 5030‑76 will accept 9852‑45 slide adapter and/or 9814
AC
FE
ultrasonic horn with extenders. (Note: When using horn with extenders, depth distances
ON
OR
must be determined for proper operation.) Complete item supplied with nylon bushing
C
N ECT
and FETFE o‑ring.

Bottom Ace‑Thred Order Order Order 5030-70
Joint Size Code Each Code Each Code Each
24/25 #25 5030-52 35.83 7506-10 21.17 5030-70 57.00
24/25 #36 5030-55 60.00 7506-12 50.46 5030-76 110.46
45/50 #36 5030-78 77.88 7506-12 50.46 5030-80 128.34
45/50 #25 8067-18 106.40 7506-10 21.17 5030-84 127.57
50/55 #25 8067-20 102.13 7506-10 21.17 5030-86 123.30
71/60 #25 8067-22 112.06 7506-10 21.17 5030-88 133.23
55/50 #36 8067-24 104.94 7506-12 50.46 5030-90 155.40

152 Components / Temperature Control
6472 TEMPERATURE CONTROL SYSTEM Pilot Plant

A complete package to enable the user to control the temperature of pilot plant reactors.
Consists of:
1) 12111-15, Type “J” auto-tune PID temperature controller with
fuzzy logic featuring digital display of reactor temperature.
hi and lo alarm set points, 120 volt/3 amp alarm outlet, a
16-segment ramp and soak program, and an auto rate circuit to
control temperature rise time.
2) 7832, auxiliary relay control unit allowing simultaneous
control of heating mantles. Relay unit is activated by
temperature controller and requires a 230 volt, 30A with
neutral and ground 4-wire, 50/60 Hz power source.
3) 12141, PFA-covered Type “J” temperature sensor,
with detachable lead, for use with 12111 temperature
controller to measure temperature inside reactor. 24-inch
for 10L & 20L cylindrical, 50L, 72L and 100L spherical;
36-inch for 36L cylindrical; 48-inch for 50L and 100L
cylindrical/200L spherical; 60-inch for 150L; 72-inch
6472-77 for 200L cylindrical.
4) 7482-33 or 5028-30, glass and PTFE adapter, #25–#7
5) 8067-18, adapters to secure temperature sensor in
head of reactor.
6) 5029-10, nylon bushing.
FOR 10L & 20L FOR 30L FOR 50L FOR 72L & 100L
CYLINDRICAL CYLINDRICAL SPHERICAL SPHERICAL
Item Each Each Each Each
Code Code Code Code
Temperature Controller 12111-15 1424.21 12111-15 1424.21 12111-15 1424.21 12111-15 1424.21
Power Strip, Four Outlets 12195-20 47.00 — — — — — —
Adapter, #7— 29/42 5028-32 32.61 — — — — — —
Auxiliary Relay Control — — 7832-14 1080.76 7832-14 1080.76 7832-19 1080.76
Adapter, Glass, 45/50-#25 — — 8067-18 106.40 8067-18 106.40 8067-18 106.40
Adapter, PTFE, #25-#7 — — 7482-33 53.10 7482-33 53.10 7482-33 53.10
Bushing, Nylon, #7 — — 5029-10 2.77 5029-10 2.77 5029-10 2.77
“J” Thermocouple Sensor,
12141-26 171.58 12141-28 200.08 12141-26 171.58 12141-26 171.58
PFA Covered, Detachable
Sensor Lead, only 12141-80 69.68 12141-80 69.68 12141-80 69.68 12141-80 69.68
Complete 6472-67 1745.08 6472-77 2937.00 6472-73 2908.50 6472-75 2908.50
FOR 50L & 100L FOR 200L FOR 200L

CYLINDRICAL SPHERICAL CYLINDRICAL
Order Order Order
Item Each Each Each
Code Code Code
Temperature Controller 12111-15 1424.21 12111-15 1424.21 12111-15 1424.21
Auxiliary Relay Control 7832-14 1080.76 7832-17* 1606.29 7832-19 1080.76
Adapter, Glass, 45/50-#25 8067-18 106.40 8067-18 106.40 8067-18 106.40
Adapter, PTFE, #25-#7 7482-33 53.10 7482-33 53.10 7482-33 53.10
Bushing, Nylon, #7 5029-10 2.77 5029-10 2.77 5029-10 2.77
“J” Thermocouple Sensor,
12141-29 251.90 12141-29 251.90 12141-30 280.65
PFA Covered, Detachable
Sensor Lead, only 12141-80 69.68 12141-80 69.68 12141-80 69.68
Complete 6472-79 2988.82 6472-83 3514.35 6472-87 3017.57
*7832-17 is 230v, 50A with ground wire.
Components / Temperature Control 153
8318 THERMOMETER Digital Display, Electronic, with Recorder Output

A complete package to enable the user to monitor the temperature of cylindrical jacketed
pilot plant reactors.
Consists of:
■■ 8318-35, Type “J” input digital temperature inside reactor. 24
thermometer with 5/8 inch LED inch for 10L cylindrical, 36 inch
display for reading across the for 30L cylindrical, 48 inch for 50L
room. 120v 50/60 Hz operation, 1°C cylindrical.
resolution, –20°C to 390°C range, ■■ 7482-33 or 5028-30, PTFE adapter,
±2% accuracy reading, ±1°C with #25–#7
recorder output, fused with clamp
for mounting to 1/2 inch bars. ■■ 8067-18, adapters to secure
temperature sensor in head of
■■ 12141 PFA covered type “J” reactor
t h e r m o c o u p l e s e n s o r, w i t h 8318
detachable cord, to measure ■■ 5029-10, #7 nylon bushing
For Use with For Use with For Use with

10L & 20L Cylindrical 30L Cylindrical 50L & 100L Cylindrical
Item Order Code Each Order Code Each Order Code Each
Thermometer, Digital 8318-35 596.25 8318-35 596.25 8318-35 596.25
Adapter, Glass 45/50 — #25 — — 8067-18 106.40 8067-18 106.40
Adapter, PTFE, #25 — #7 — — 7482-33 53.10 7482-33 53.10
Bushing, Nylon, #7 — — 5029-10 2.77 5029-10 2.77
Adapter, #7 — 24/40 5028-30 27.61 — — — —
“J” Thermocouple Sensor, PFA Covered, Detachable 12141-26 171.58 12141-28 200.08 12141-29 251.90
Sensor Cord, only 12141-80 69.68 12141-80 69.68 12141-80 69.68
Complete 8318-204 865.12 8318-207 1028.28 8318-209 1080.10
12327 DIGITAL TEMPERATURE MONITOR J-Kem

Monitors and displays the temperature of an attached piece of equipment on a bright
LED display. Built-in USB port and free data logging software allows remote temperature
monitoring, and provides a GMP, GLP compliant temperature history. Audible digital alarm
available as an option. 230vac versions are CE marked.
2.5 x 4.75 x 5.5 (Inches, HxWxD) / 50 watts, 120VAC, USB 2.0
Temperature Thermocouple
J-Kem Model Range (ºC) Type Order Code Each
DM120-T –200 to 250 T 12327-03 391.00
DM120-J 0 to 800 J 12327-05 391.00
DM120-K –50 to 1200 K 12327-07 391.00
12327 DIGITAL TEMPERATURE MONITOR J-Kem

230VAC, CE-marked version of digital temperature monitor, above. 12327
Temperature Thermocouple
J-Kem Model Range (ºC) Type Order Code Each
DM230-T –200 to 250 T 12327-33 391.00
DM230-J 0 to 800 J 12327-35 391.00
DM230-K –50 to 1200 K 12327-37 391.00
6470 THERMOWELL without Joint

For use with 5030 “Midi” Ace‑Thred adapter. The completely adjustable depth feature
of this combination means the well is less expensive and more versatile than the jointed
style. Outside diameter, 10mm. 6470
For Flask Cap., mL Length, mm Order Code Each
250-3000 300 6470-38 16.99
3000-5000 350 6470-40 16.49
12000 400 6470-42 16.99
22000 465 6470-44 16.99
50000-72000 570 6470-46 18.53

12067 COIL Cooling/Heating, Cylindrical Flasks

For use with pilot plant reactors with cylindrical flasks, with 200mm (8-inch) or 300mm
(12‑inch) size flanges. Coils are ideal for steam heating or water cooling of reactor contents.
See chart below for tubing size and materials selection; PTFE coated copper, Hastelloy
or stainless steel. Available in 1/4-inch or 1/2-inch O.D. sizes.
Flask Neck Tubing Copper/PTFE 316 Stainless Steel Hastalloy C-276

Size, Size, Size Order Order Order
L In. (In.) Code Each Code Each Code Each
10 8 1/4 12067-39 547.05 12067-239 636.09 12067-439
10 8 1/2 12067-71 1110.49
15 8 1/2 12067-71 1110.49
20 8 1/4 12067-48 600.74 12067-248 686.14 12067-448 Call
20 8 1/2 12067-71 1110.49 for
30 8 1/2 12067-40 1134.78 12067-240 1001.74 12067-440 Pricing
50 8 1/2 12067-44 1692.90 12067-244 1310.98 12067-444
100 12 1/2 12067-79 1773.43 12067-279 1584.81 12067-479
12067 200 12 1/2 12067-80 2123.00 12067-280 1826.24 12067-480
12067 COIL Cooling/Heating, Spherical Flasks

For use with pilot plant reactors with spherical flasks, with 200mm (8-inch) or 300mm
(12‑inch) size flanges. Coils are ideal for steam heating or water cooling of reactor contents.
See chart below for tubing size and materials selection; PTFE coated copper, Hastelloy
or stainless steel. Available in 1/4-inch, 1/2-inch and 3/8-inch O.D. sizes.
Flask Neck Tubing Copper/PTFE 316 Stainless Steel Hastalloy C-276

Size, Size, Size Order Order Order
L In. (Inches) Code Each Code Each Code Each
12 6 3/8 12067-58 803.64
22 6 3/8 12067-58 803.64
50 8 3/8 12067-61 892.76 12067-261 827.92 12067-461
50 8 1/4 12067-52 598.00
Call
72 8 3/8 12067-63 995.02 12067-263 876.97 12067-463
for
72 8 1/4 12067-54 Call Pricing
100 8 3/8 12067-65 1045.32 12067-265 1482.00 12067-465
100 8 1/2 12067-84 1446.60
12067 100 8 1/4 12067-56 Call
200 12 1/2 12067-68 2011.00 12067-268 1620.67 12067-468
12069 COIL Cooling/Heating, Halar Coated

Halar coated 1/4-inch O.D. stainless steel coil for heating and cooling. Designed for small
New reactors like the ACE 1000mL PTFE reactor (page <?>) or 1L filter reactors. Fits PTFE
threaded adapters for PTFE heads.
Order
Code Each
12069-06 835.14
12069
12067 HEAT EXCHANGER TUBING Fluorocarbon Covered

Copper tubing encapsulated with Fluorocarbon for use as a make-your-own heat ex-
changer coil.* Can be used in corrosive solutions or strong solvents like ammonia, fuming
sulfuric acid, potassium hydroxide concentrate, sodium sulfate, etc. Eliminates need for
costly metals like Tantalum. Highly temperature resistant, electrically insulated and will
not stain, corrode or contaminate. Does not support bacteria, and anti-stick property of
Fluorocarbon rinses easily of sticky or clinging materials.
Easy to custom make your own exchanger for heat or cooling by wrapping around
simple mandrel or form to desired size.* Tubing ends can be connected to most any
compression type fitting.
*Shipped in 2-3 foot diameter coils for forming to desired shape, 50 foot max. continu-
ous run. ACE can supply coiled exchanger to suit your needs. For a quotation, please 12067
send us specifications.
Fluoro- Approx.
Nominal carbon Copper Approx. Sq. Ft. of
Copper Wall Wall Min. Bend Surface Per Order
O.D., in. (Inches) (Inches) Dia., in. Linear Ft. Code Each
1/4 .015 .030 2 .0733 12067-15 20.62
3/8 .015 .030 4 .106 12067-20 25.21
1/2 .020 .030 8 .141 12067-25 31.22
12111 TEMPERATURE CONTROLLER Time Proportional, Digital

Microprocessor based, compact, temperature controller, with bright LED display. Tem-
perature range is -70° to 870º C with 0.1° C resolution. Temperature readout in farenheit or
centigrade is field selectable. Designed to use Type “J” thermocouple sensors. The code
-15 and -33 units have two, 120V front outlets. The -47 and -58 units have 2-120 volt rear
outlets and one selectable, 20V or 40V front outlet. Both models have 16 segment ramp
and soak selectable profile. This model has an over-temp cutoff and alarm output for added
safety. Output circuitry utilizes zero-crossing fired solid state relay for proportional control
that provides interference free power (RFI) to electric heater type resistive loads. 120volt,
15Amp, 60Hz input. Unit is 6-inch x 6.5-inch x 5.5-inch (HxDxW); weight = 4 lbs. Three-year 12111-15
conditional warranty. Complete unit comes with type “J” thermocouple.
Order
With Two Front 120v Outlets Code Each
Controller, only 12111-15 1424.21
Sensor, Type “J” Thermocouple, 318mm, 1/4-inch O.D. 12110-15 103.65
Complete (above two components) 12111-33 1527.86
OPTIONAL COMPONENTS:
Sensor, Type “J” Thermocouple, 102mm, 3/16-inch 12110-17 89.63
Sensor, Type “J” Thermocouple, 305cm, fiberglass insulated, w/ot sheath 12110-24 50.88
Sensor, Type “J” Thermocouple, 305cm, double PTFE insulated, w/o sheath 12110-25 50.88
Sensor Extension, 2.4M (8-inch) w/mating connectors, double PTFE insulated 12110-26 59.97
Contact ACE to get a copy of our Laboratory Glassware

and Equipment catalog!

ACE Economy Model Temperature Controller

for general laboratory use
■■Economy model
■■Ultra compact (2 inches high)
■■New digital technology
■■16 segment ramp and soak function
■■Fuzzy logic auto tune PID
■■Temp. Range Field Selectable
Features & Specifications

■■Bar mountable or benchtop operation.
■■Single loop type, downsized and lightweight.
■■Temperature range: –50 to 800°C, adjustable.
■■0.1°C* or 0.1°F temperature resolution, selectable.
■■Absolute accuracy: ±0.25% of range, max. ±2°C.
■■Control accuracy: ±0.1°C typical.
■■Microprocessor-based 1/32 DIN model for digital accuracy and
reliability.
Valu
12125-32 e ■■Dual four-digit LED display for instant recognition of process
temperature and setpoint 1 value.
■■Auto tune PID control can maintain ±0.1° under normal
conditions.
■■Ramp and soak, field selectable, 16 segment with hold or
shut-off.
■■Field selectable output % power limit when heating smaller
vessels or when using very low setpoints. See OEM manual
(SIOH) secure menu, affects all heaters.
■■Output circuitry utilizes zero crossing fired solid state relay
proportional control that provides interference free power (RFI)
to electrical heater type resistive loads.
■■Rear heater outlet provides time proportional control, meaning
overshoot is minimized. Percent output decreases as set
temperature is approached.
■■Input power: 120 volts, 50/60 Hz, 15 amps maximum
■■Unit measures: 2 inches high x 5-1/4 inches wide x 5-1/4 inches
deep; weight: 2 lbs, 2 oz.
■■Operating instruction label on top for quick reference.
■■Three-year warranty
12125 TEMPERATURE CONTROLLER
Economy Model
For use in
Order Code Each
all
controlling es
Controller, only (“J” type) 12125-14 797.11
Controller, only (“T” type) 12125-16 797.11
antl
Controller, only (“K” type) 12125-18 797.11
Glas-Col M olts
v
rated at 115
Sensor, Type J Thermocouple,
12110-15 103.65
318 mm, 1/4 inch
Complete (“J” Type only) 12125-32 900.76
Improved ACE Temperature Controller

for General Laboratory Use...
Including mantles up to 22 Liters
Features & Specifications:
■
■Two front-mounted 120v outlets
■■ Two front-mounted outlets.
■■ Bar mountable or benchtop operation. ■
■Compact (3.5 inches high)
■■ Single loop type, downsized and lightweight.
■
■New digital technology
■■ Temperature range: –70 to 870°C, adjustable.
■■ 0.1°C/0.1°F temperature resolution, field selectable. ■ segment ramp and soak function
■16
■■ Absolute accuracy: ±0.25% of range, max. ±2°C.
■■ Control accuracy: ±0.1°C typical.
■
■Fuzzy logic auto tune PID
■■ Microprocessor-based 1/32 DIN model for digital
accuracy and reliability.
■■ Dual four-digit LED display for instant recognition of
process temperature and setpoint 1 value.
■■ Auto tune PID control can maintain ±0.1° under
normal conditions.
■■ Ramp and soak, field selectable, 16 segment with
hold or shut-off.
■■ Field selectable output % power limit when heating
smaller vessels or when using very low setpoints.
(factory set at 60% for safety). See OEM Manual
(S1OH) secure menu.
■■ Output circuity utilizes zero crossing fired solid state
relay proportional control that provides interference
free power (RFI) to electrical heater type resistive
loads.
■■ Heater outlets provide time proportional control,
meaning overshoot is minimized. Percent output
decreases as set temperature is approached.
■■ Universal TC input jack for “mini” or “standard”
plugs.
■■ Input power: 120 volts, 50/60 Hz, 15 amps maximum,
fused.
■■ Unit measures: 3.5 inches high x 6-3/16 inches wide x
6-5/16 inches deep; weight: 2.5 lbs.
■■ Operating instruction label on top for quick reference
12126 TEMPERATURE CONTROLLER Improved Model

For use in Order Code Each
all
controlling tles Controller, only 12126-24 874.72
an
Glas-Col M volts
Sensor, Type J Thermocouple, 318mm, 1/4 in. 12110-15 103.65
Complete 12126-45 978.37
rated at 115
Digital interface available. Call for details.

12127 TEMPERATURE CONTROLLER Instatherm® Model

Bar mountable or benchtop operation. Single loop type, downsized and lightweight.
Temperature range: –70 to 870°C, field settable to °F. FIeld selectable 0.1°C/0.1°F temperature
resolution. Absolute accuracy: ±0.25% of range, maximum ±2°C. Control accuracy: ±0.1°C
12127 typical. Supplied with two 120v controlled rear outlets for up to 22L mantles or 120v
ACE oil baths. Supplied with single 20v or 40v controlled limit front outlet for low voltage
Instatherm® or small mantles. Ramp and soak, field selectable, 16 segment with hold or
shut-off. Field adjustable rear sensitivity control to “tweek” the speed of response to setpoint,
if necessary, this eliminates overshoot. Universal TC input jack for “mini” or “standard”
plugs. Input power: 120 volts, 50/60 Hz, 15 amps maximum, fused. Unit measures: 3.5
high x 6-3/8 wide x 8 deep inches; weight: 3.4 lbs. Operating instruction label on top for
quick reference. Three-year warranty.
Order Code Each
Sensor, Type J Thermocouple, 318 mm, 1/4-inch OD 12110-15 103.65
Complete (above components) 12127-40 1453.81

Sensor, Type J Thermocouple, 102 mm, 3/16-inch OD 12110-17 89.63
Complete (above components) 12127-52 1439.79
12312 TEMPERATURE CONTROLLER J-Kem Apollo Series, Dual Channel

Has all the features of the Gemini series, above, but also has an independent 100-hour
digital timer on each controller channel.
4 x 8 x 9 (Inches, HxWxD) / 120vac, 15 amps, 1800 watts total / 1200 watts maximum
per channel
With Sensor, Cord Temperature Thermocouple Order
J-Kem Model and Adapter Range (ºC) Type Code Each
Apollo-T No –200 to 250 T 12312-03 1393.80
Apollo-J No 0 to 800 J 12312-05 1393.80
Apollo-K No –50 to 1200 K 12312-07 1393.80
12312 Apollo-Pt No –200 to 400 RTD 12312-09 1393.80
The Apollo Series units noted above require two
thermocouple sensors, two cords and two adapters.
12314 TEMPERATURE CONTROLLER J-Kem Quad Series, Four Channel

The Quad is your solution when bench space is at a premium — the Quad packs four
independent temperature controllers into a single unit! Each of the four controller channels
has 1200 watts of power, an independent display, and an over-temperature protection circuit.
5.25 x 7 x 7.5 (Inches, HxWxD) / 120vac, 15 amps, 1800 watts total / 1200 watts max.
per channel
With Sensor, Cord Temperature Thermocouple Order
Quad-T No –200 to 250 T 12314-05 2295.40
Quad-J No 0 to 800 J 12314-07 2295.40
Quad-K No –50 to 1200 K 12314-09 2295.40
Quad-Pt No –200 to 400 RTD 12314-11 2295.40
12314
The Quad Series units noted above require four
thermocouple sensors, four cords and four adapters.
12167 LAB SAFETY CONTROLLER J-Kem Model LS-120

Lab safety controller by J-Kem combines all the features of the digital temperature monitor
and the water-flow monitor into a single versatile instrument. Plug any piece of equipment
into the monitor, then if the water flow rate falls below the set level, or if the reaction tem-
perature goes above or below the user set limits, the outlet power turns off automatically.
The unit will also cut off power if the main power is interrupted. The controller then has to
be reset. See ACE 12168 product family for flow sensors.
With Sensor Cord Temperature Thermocouple Order
LS-120-T No –200 to 250 T 12167-01 772.80
LS-120-J No 0 to 800 J 12167-03 772.80
LS-120-K No –50 to 1200 K 12167-05 772.80
J-Kem Model Description Flow Rate, LPM Order Code Each

WFM-01 Flow Sensor 0.1 to 2.5 12168-01 240.00 12167
WFM-02 Flow Sensor 1 to 10 12168-02 240.00
— Shut-Off Valve — 12168-10 172.50
12160 WATER FILTER

Installs ahead of sensing head. 50 micron screen prevents failure of sensing head due
to dirt or rust coming from the water supply. Supplied with replaceable filter cartridge.
Has 3/8-inch O.D. hose connections. Labeled inlet and outlet.
Order Code Each

12160-35 32.40 12160-35
12162 WATER-FLO POWER CUT-OFF 15 amps, with Timer

Supplied with front panel mounted timer. In the event of water flow failure and subsequent
power shut-off at the outlets, timer indicates accumulated elapsed time. Timer runs for
up to 10,000 hours before starting at zero again, smallest reading is 0.1 hour. Cannot
be reset. Note: a reset-able timer is available, at slightly higher cost. Call for quotation.
Order Code Each

Sensing Head, w/Water Filter 12160-06 235.19
Power Pack, only 12162-07 823.95 12162-14
Complete 12162-14 1059.14
12164 WATER-FLO POWER CUT-OFF 20 amps (230 volts)

Will control one or two apparatus at 4.6 kilowatts AC power, 208-250 volts, 50/60
Hz. (up to 20 amps), fused. Two rear outlets allow use with our 7830-71 power
12164
supply and 12165 shut-off water valve (230v).
Order Code Each

Sensing Head, w/Water Filter 12160-06 235.19
Power Pack, only 12164-20 962.41
Complete 12164-30 1197.60

12165 “ELECTRO-FLO” SHUT-OFF VALVE

A water or air* shut-off solenoid valve for use with 12160, 12162 or 12164 water-flo power
cut-off or as a general laboratory shut-off valve. Operates from 0.35Kg/cm2 to 10.5Kg/
cm2 (5 to 150 psi) for water or 0.35Kg/cm2 for air and up to 91°C. Internal design of pilot-
operated, piston-type, valve assures exceptional flow performance. Constructed of cast
bronze with waterproof cast-coil that has a lifetime warranty. Valve must be installed in
horizontal piping with solenoid in vertical position. Supplied with 1.8 meter grounded
cord and female pipe thread. Codes -14, -20 and -26 for use with 12160 and 12162.
Codes -48, -54 and -57 for use with 12164. Note: a pre-filter is recommended when this
product is used with water or air (15 micron or less).
(For 120v) (For 230v)

Pipe Sizes, mm Order Code Each Order Code Each
12165 9.5 (3/8 in.) 12165-14 243.47 12165-48 246.19
12.7 (1/2 in.) 12165-20 259.87 12165-54 260.33
19.1 (3/4 in.) 12165-26 307.21 12165-57 307.11
*When used as air shut-off valve, a strainer is recommended.
12168 WATER FLOW MONITOR J-Kem Model WFM-120

J-Kem monitor precisely measures the flow of water through a condenser, bath or a
12168 photochemical reactor. Upon interruption or if the flow drops below an operator set
rate, power to the monitored equipment is cutoff. Manual power reset. Inclusion of
a 12168‑10 shut-off valve and either a 12169‑01 audible alarm or a 12169‑05 digital
alarm is recommended.
J-Kem Model Description Flow Rate, LPM Order Code Each

WFM-01 Flow Sensor 0.1 to 2.5 12168-01 240.00
— Shut-Off Valve — 12168-10 172.50
WFM-120 Water Flow Monitor — 12168-120 354.20
12169 ALARM J-Kem
Digital alarm outlet and audible alarm accessories for J-Kem safety controller and water-
flow monitors. Allows 12167 and 12168 units to be set up for alarm warnings when in
unsafe conditions. The audible alarm sounds during low or no water conditions for the
12168 monitor and the digital alarm activates on either the water flow monitor or the safety
controller when conditions are out of set ranges.
J-Kem Model Alarm Type For Controllers Order Code Each

WFM-AA Digital 12167 & 12168 12169-01 65.00
WFM-OC Audible 12168 12169-05 35.00
Components / Sensors 161
TYPE: Thermocouple Sensor Probes (continued)

Length of Max. Lead
Inconel Sheath, Sheath Sheath Sheath Lgth., Lead Order
Type mm (In.) O.D. mm/In. Coating Temp. Ft. Attachment Code Each
“K” 305 (12) 6.35/0.25 Plain 550°C 3-15 Detachable* 12141-43 76.26
“K” 305 (12) 6.35/0.25 PFA 260°C 3-15 Detachable* 12141-52 125.41
*Lead only, for TYPE “J” Sensor (Black) 12141-80 69.68
*Lead only, for TYPE “K” Sensor (Yellow) 12141-83 77.70
PFA: (Tetrafluoroethylene-perfluoro(propyl•vinyl ether) copolymer), colored

black, less permeable than either FEP or TFE. Maximum temperature
260°C. 12141-80, -83
12141
3' coiled PVC

patch cord
stretchable to 15';
detachable
from sheath via
color-coded
universal
connectors with
mini-male plug

162 Components / Sensors
TYPE: Thermocouple Sensor Probes

Length of Max. Lead
Thermocouple Inconel Sheath, Sheath Sheath Sheath Lgth., Lead Order
Subminiature
Type mm (In.) O.D. mm/In. Coating Temp. Ft. Attachment Code Each
flat blade male
connectors “J” 102 (4) 4.76/0.19 Plain 550°C 6 Permanent 12110-17 89.63
“J” 305 (12) 1.59/0.06 Plain 550°C 12 Permanent 12140-04 180.56
12140 “J” 305 (12) 3.17/0.12 Plain 550°C 12 Permanent 12140-05 178.30
PTFE covered “J” 305 (12) 6.35/0.25 Plain 550°C 6 Permanent 12110-15 103.65
with stainless
steel overbraid “J” 305 (12) 6.35/0.25 Plain 550°C 12 Permanent 12140-06 179.64
“J” 305 (12) 1.59/0.06 PFA 260°C 12 Permanent 12140-17 228.66
Permanently “J” 305 (12) 3.17/0.12 PFA 260°C 12 Permanent 12140-19 230.76
attached lead “J” 305 (12) 6.35/0.25 PFA 260°C 12 Permanent 12140-20 232.59
with spring
transition for “J” 600 (24) 6.35/0.25 PFA 260°C 12 Permanent 12140-21 237.17
strain relief “J” 900 (36) 6.35/0.25 PFA 260°C 12 Permanent 12140-25 267.68
“J” 1200 (48) 6.35/0.25 PFA 260°C 12 Permanent 12140-26 302.55
“J” 1800 (72) 6.35/0.25 PFA 260°C 12 Permanent 12140-28 335.48
“J” 305 (12) 6.35/0.25 Plain 550°C 3-15 Detachable* 12141-11 77.05
Plain Inconel or “J” 1800 (72) 6.35/0.25 Plain 550°C 3-15 Detachable* 12141-20 160.06
PFA covered “J” 305 (12) 6.35/0.25 PFA 260°C 3-15 Detachable* 12141-25 118.70
“J” 600 (24) 6.35/0.25 PFA 260°C 3-15 Detachable* 12141-26 171.58
“K” 102 (4) 4.76/0.19 Plain 550°C 6 Permanent 12113-22 88.14
12110
12140 “K” 600 (24) 6.35/0.25 Plain 550°C 12 Permanent 12140-41 191.48
“K” 305 (12) 1.59/0.06 PFA 260°C 12 Permanent 12140-37 228.87
“K” 305 (12) 3.17/0.12 PFA 260°C 12 Permanent 12140-62 228.87
“K” 305 (12) 6.35/0.25 PFA 260°C 12 Permanent 12140-51 226.79
“K” 600 (24) 6.35/0.25 PFA 260°C 12 Permanent 12140-53 236.39
“K” 900 (36) 6.35/0.25 PFA 260°C 12 Permanent 12140-57 270.30
“K” 1200 (48) 6.35/0.25 PFA 260°C 12 Permanent 12140-58 302.55
“K” 1800 (72) 6.35/0.25 PFA 260°C 12 Permanent 12140-59 335.48
Components / Sensors 163
Thermocouple Sensors for

J-Kem Temperature Controllers
12180 T-TYPE SENSORS 12182 K-TYPE SENSORS
Type “T” thermocouple temperature sensors for use with Type “K” thermocouple temperature sensors for use with
all J-Kem “T” type model temperature controllers. Either all J-Kem “K” type model temperature controllers. Either
1/4- or 1/8-inch O.D. Available in 304 stainless steel or 1/4- or 1/8-inch O.D. Available in 304 stainless steel or
PTFE coated stainless steel sheaths of various lengths. PTFE coated stainless steel sheaths of various lengths.
See ACE 12190 series extension cords. See ACE 12190 series extension cords.
O.D. Lgth. PTFE Order O.D. Lgth. PTFE Order
(in.) (in.) Coated? Code Each (in.) (in.) Coated? Code Each
1/8 6 No 12180-03 34.00 1/8 6 No 12182-01 34.00
1/8 12 No 12180-05 34.00 1/8 12 No 12182-03 34.00
1/8 18 No 12180-07 45.00 1/8 18 No 12182-05 45.00
1/8 24 No 12180-09 49.00 1/8 24 No 12182-07 49.00
1/8 36 No 12180-11 62.00 1/8 36 No 12182-09 62.00
1/8 6 Yes 12180-20 64.00 1/8 6 Yes 12182-20 64.00
1/8 12 Yes 12180-22 64.00 1/8 12 Yes 12182-22 64.00
1/8 18 Yes 12180-24 75.00 1/8 18 Yes 12182-24 75.00
1/8 24 Yes 12180-26 79.00 1/8 24 Yes 12182-26 79.00
1/8 36 Yes 12180-28 92.00 1/8 36 Yes 12182-28 92.00
1/4 6 No 12180-31 38.00 1/4 6 No 12182-32 38.00
1/4 12 No 12180-33 38.00 1/4 12 No 12182-34 38.00
1/4 18 No 12180-35 49.00 1/4 18 No 12182-36 49.00
1/4 24 No 12180-37 53.00 1/4 24 No 12182-38 53.00
1/4 36 No 12180-39 66.00 1/4 36 No 12182-40 66.00
1/4 6 Yes 12180-40 68.00 1/4 6 Yes 12182-41 68.00
1/4 12 Yes 12180-42 68.00 1/4 12 Yes 12182-43 68.00
1/4 18 Yes 12180-44 79.00 1/4 18 Yes 12182-45 79.00
1/4 24 Yes 12180-46 83.00 1/4 24 Yes 12182-47 83.00
1/4 36 Yes 12180-48 96.00 1/4 36 Yes 12182-49 96.00
12181 J-TYPE SENSORS 12183 RTD TYPE SENSORS

Type “J” thermocouple temperature sensors for use with “RTD” (Pt/100) type thermocouple temperature sensors
all J-Kem “J” type model temperature controllers. Either for use with J-Kem model “RTD” temperature controllers.
1/4- or 1/8-inch O.D. Available in 304 stainless steel or Either 1/4- or 1/8-inch O.D. All PTFE coated stainless steel
PTFE coated stainless steel sheaths of various lengths. sheaths of various lengths. Uncoated available via special
See ACE 12190 series extension cords. order. See ACE 12190 series extension cords.
O.D. Lgth. PTFE Order O.D. Lgth. PTFE Order
(in.) (in.) Coated? Code Each (in.) (in.) Coated? Code Each
1/8 6 No 12181-02 34.00 1/8 6 Yes 12183-02 129.00
1/8 12 No 12181-04 34.00 1/8 12 Yes 12183-04 129.00
1/8 18 No 12181-06 45.00 1/8 18 Yes 12183-06 140.00
1/8 24 No 12181-08 49.00 1/8 24 Yes 12183-08 144.00
1/8 6 Yes 12181-21 64.00 1/8 36 Yes 12183-10 157.00
1/8 12 Yes 12181-23 64.00 1/4 6 Yes 12183-40 132.00
1/8 18 Yes 12181-25 75.00 1/4 12 Yes 12183-42 132.00
1/8 24 Yes 12181-27 79.00 1/4 18 Yes 12183-44 144.00
1/8 36 Yes 12181-29 92.00 1/4 24 Yes 12183-46 148.00
1/4 6 No 12181-32 38.00 1/4 36 Yes 12183-48 161.00
1/4 12 No 12181-34 38.00
1/4 18 No 12181-36 49.00
1/4 24 No 12181-38 53.00
1/4 36 No 12181-39 72.00
For extension cords, see ACE
1/4 6 Yes 12181-41 68.00 12190 straight and coiled cords,
1/4 12 Yes 12181-43 68.00 on the following page.
1/4 18 Yes 12181-45 79.00
1/4 24 Yes 12181-47 83.00
1/4 36 Yes 12181-49 96.00

164 Components / Sensors
Sensor extension cords for use with all J-Kem thermocouple probes. Cords match color of probe type: blue, black, yellow
or white. Available in either 10- or 20-foot coiled or straight styles. Select length, type, and connector, SMP (flat plug) or
OST (round plug).
12190 12190
(Coiled) (Straight)
Probe Lgth. Connector Order

12190 SENSOR CORDS Coiled Style (ft.) Type Code Each
Probe Lgth. Connector Order
Style (ft.) Type Code Each
J
K
10
10
SMP
SMP
12190-40
12190-41
26.25
26.25
SMP
J 10 SMP 12190-01 33.80 T 10 SMP 12190-42 26.25
K 10 SMP 12190-02 33.80 J 10 OST 12190-44 26.25
T 10 SMP 12190-03 33.80 K 10 OST 12190-45 26.25
RTD 10 SMP 12190-04 56.20 T 10 OST 12190-46 26.25
J 10 OST 12190-08 38.80 J 20 SMP 12190-50 36.30
K 10 OST 12190-10 38.80 K 20 SMP 12190-51 36.30
T 10 OST 12190-11 38.80 T 20 SMP 12190-52 36.30
J 20 SMP 12190-20 67.00 J 20 OST 12190-56 36.30
K 20 SMP 12190-21 67.00 K 20 OST 12190-57 36.30
T 20 SMP 12190-22 67.00 T 20 OST 12190-58 36.30
J 20 OST 12190-26 67.00
K 20 OST 12190-27 67.00 OST
T 20 OST 12190-28 67.00
12190 SENSOR CORDS Straight

12184 DUAL SENSORS PTFE Coated 12191 DUAL SENSOR CORDS
Dual coupling temperature thermocouple sensors for use Dual element extension cords for use with dual element
with Model HCC and 270 J-Kem temperature controllers. 12184 sensors for J-Kem models HCC and 270
Available in “J”, “T” or “K” types. Probes are PTFE coated temperature controllers. Available in “T”, “K”, and “J”
stainless steel in various lengths and O.D. Probes require types in 10‑ or 25-ft. lengths.
12191 extension cords.
Probe Lgth. Order
O.D. Lgth. Sensor Order Style (ft.) Code Each
(in.) (in.) Type Code Each
T 10 12191-02 59.50
1/8 12 T 12184-02 103.00 J 10 12191-06 59.50
1/4 12 T 12184-04 115.00 K 10 12191-08 59.50
1/4 24 T 12184-06 137.00 T 25 12191-20 94.25
1/4 36 T 12184-08 151.00 J 25 12191-22 94.25
1/8 12 J 12184-12 103.00 K 25 12191-24 94.25
1/4 12 J 12184-14 115.00
1/4 24 J 12184-16 137.00
1/4 36 J 12184-18 151.00
1/8 12 K 12184-20 103.00
1/4 12 K 12184-22 115.00
1/4 24 K 12184-24 137.00
1/4 36 K 12184-26 151.00
12184
S I N C OR
S P
A
O
L
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ACE G
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TED
1936 2011
VI USA
N
J
NE ,
LAND

166 Components / Heating Mantles
6478 MANTLE Fabric/Cloth
For use with 6476 and 6477 reaction flasks. Upper temperature limit, 450ºC. Must be
operated through a temperature controller. CSA approved. Detachable 4-foot cord and
6478-05
locking connector.
For Flask Order
Size, mL I.D. x Depth, inches/mm Watts/Volts Code Each
500 4.63/117.4 x 2.5/63.5 250w-115v 6478-05 346.55
1000 4.63/117.4 x 5.63/142.8 300w-115v 6478-10 322.54
1500 4.63/117.4 x 6.63/168.2 380w-115v 6478-15 350.06
2000 4.63/117.4 x 8. 89/225.4 450w-115v 6478-20 374.61
3000 4.63/117.4 x 10/254 600w-115v 6478-25 381.58
6478
6478 MANTLE Aluminum Housing, For Cylindrical Flasks
Cylindrical type for use with 6476 and 6477 reaction flasks. With hard aluminum housing.
CSA approved, 115 volt c omplete with 4-foot detachable cord with locking connector.
Temperature range is Ambient +10°C to 450°C. Must be operated through a temperature
controller. 230V versions available.
For Flask Maximum Flask Order
Size, mL Dia., in. / mm I.D. x Depth, inches/mm Watts/Volts Code Each
500 4.63/117.4 4.63/117.4 x 2.5/63.5 250w-115v 6478-45 320.00
1000 4.63/117.4 4.63/117.4 x 5.63/142.8 300w-115v 6478-47 334.00
1500 4.63/117.4 4.63/117.4 x 6.63/168.2 380w-115v 6478-49 347.00
2000 4.63/117.4 4.63/117.4 x 8. 89/225.4 450w-115v 6478-51 356.00
3000 4.63/117.4 4.63/117.4 x 10/254 600w-115v 6478-53 382.41
12031 MANTLE Spherical, Fabric/Cloth

Covers both top and bottom of 1-, 2-, or 3-neck flasks. Temperature range is Ambient
+10°C to 450°C. The circumferential zipper holds the halves snugly together to prevent
heat loss, and the side split in the top section allows for easy flask removal. CSA certified.
Each half has a four-foot cord and locking connector. 230v CE-approved versions are
available.
For Flask Distribution
Size, mL Lower Half Upper Half Order Code Each
Silicone 1000 380w-115v 140w-115v 12031-19 588.00
Impregnated ➤ 2000 500w-115v 200w-115v 12031-21 616.00
Glass 3000 500w-115v 200w-115v 12031-23 647.00
12031 Fabric 5000 600w-115v 300w-115v 12031-25 768.00
12035 MANTLE Hemispherical, Fabric/Cloth

12035 Adaptable to unusual shapes and sizes. Temperature to 450°C. Detachable 4-foot cord,
2-wire cord and locking connector. CSA certified. Requires 12095 or 12096 supports.
Must be operated through a temperature controller.
For Flask Size mL Watts/Volts Order Code Each

1000 380w-115v 12035-19 219.00
Silicone 2000 500w-115v 12035-21 239.00
Impregnated ➤
3000 500w-115v 12035-23 266.00
Glass
Fabric 5000 600w-115v 12035-25 324.00
12000 (2) 650w-115v 12035-27 657.00
Components / Heating Mantles 167
12036 MANTLES Fabric/Cloth
For use with 6504 or 6511 reaction flasks. Upper temperature limit, 450°C. Four-foot cord
and locking connector. Must be operated through a temperature controller. CSA approved.
For Flask Order
Size, mL I.D. x Depth, inches/mm Watts/Volts Code Each
500 3.75/95.2 x 4.5/114.3 270w-115v 12036-17 334.00
1000 4.25/107.9 x 5.2/132 335w-115v 12036-19 350.00
2000 5.5/139.7 x 6.0/152.3 470w-115v 12036-21 361.00
3000 5.5/139.7 x 9.0/228.6 550w-115v 12036-23 387.00
4000 5.5/139.7 x 11.0/279.4 750w-115v 12036-24 393.00
12036
12041 MANTLE Cylindrical Reaction Flasks, Fabric/Cloth

Girdle style mantles for ACE large size cylindrical and spherical flasks and pilot plant
assemblies. Codes -10 through -37 fit 6521, 6522 and 6472 flasks. -40, -42, -44 fit 6530
and 6533 spherical flasks. Fit easily into our four-post stands for large reactor assemblies.
Flask Size, Liter Flask Type Watts/Volts Order Code Each

6/10 Cylindrical 495w–115v 12041-10 860.65
15 Cylindrical 700w–115v 12041-12 777.15
30 Cylindrical (2) 880w–115v 12041-16 1201.84
50 Cylindrical (2) 880w–115v 12041-18 1090.99
30 Cylindrical (2) 825w–115v 12041-32 979.40
50 Cylindrical (2) 725w–115v 12041-35 1236.96
50 Cylindrical (3) 1100w–115v 12041-37 1617.65
50 Spherical 1200w–115v 12041-40 1394.13
72 Spherical (2) 1800w–230v 12041-42 1771.47
12041
100 Spherical (3) 1400w–230v 12041-44 2335.70
100 Cylindrical (4) 1200w–115v 12041-48 2222.22
200 Cylindrical (4) 1100w–115v 12041-52 2228.41
12043 MANTLE Aluminum Housing

Offers the benefit of grounding through aluminum housing. The heating element is em-
bedded in layers of glass fabric to protect the flask wall from thermal strain, and is thor-
oughly covered with glass insulation to prevent heat from being radiated outward. Glass
fabric affords operating temperatures to 450°C. With detachable 4-foot, 3-wire cord and 12043
locking connector. Requires 12094 support. CSA certified. Must be operated through a
temperature controller. 230v version is also available for 250mL and larger mantles.
Max. Flask
For Flask Size, mL Dia., in. / mm I.D. x Depth, inches/mm Watts/Volts Order Code Each
1000 5.1/130 5.1/130 x 2.5/65 380w-115v 12043-19 295.00
2000 6.6/170 6.6/170 x 3.3/85 500w-115v 12043-21 312.00
3000 7.2/183 7.2/184 x 3.6/91.5 500w-115v 12043-23 375.00
5000 8.6/220 8.7/222 x 4.3/110 600w-115v 12043-25 470.00
12000 11.5/293 11.5/294 x 5.8/147.6 (2) 650w-115v 12043-27 871.00
22000 13.6/347 13.7/350 x 6.8/173.5 (2) 770w-115v 12043-29 984.00
50000 17.9/456 18.0/458 x 8.9/228 (3) 1000w-115v 12043-31 1624.37
50000 (For Schott) 19.9/506 19.9/506 x 8.9/228 (3) 1000w-115v 12043-32 1942.40
72000 20.5/522 20.6/525 x 10.1/258.9 (2) 2000w-230v 12043-33 1784.00
12044 MANTLE Aluminum Housing, with Bottom Opening

Same as 12043, above, but with bottom opening to accommodate flasks such as 6450, 12044
6469, 6534, and 6536.
For Flask Max. Flask Bottom Opening Order
Size, mL Dia., in. / mm I.D. x Depth, inches/mm Watts/Volts Dia., In./mm Code Each
3000 7.2/183 7.2/184 x 3.6/91.5 500w-115v 2.5/63.5 12044-24 579.43
5000 8.6/220 8.7/222 x 4.3/110 600w-115v 2.5/63.5 12044-26 655.20
12000 11.5/293 11.5/294 x 5.8/147.6 (2) 650w-115v 2.5/63.5 12044-28 1091.72
12000 11.5/293 11.5/294 x 5.8/147.6 (2) 650w-115v 5.0/127 12044-29 1085.97
22000 13.6/347 13.7/350 x 6.8/173.5 (2) 770w-115v 2.5/63.5 12044-30 1207.35
22000 13.6/347 13.7/350 x 6.8/173.5 (2) 770w-115v 5.0/127 12044-31 1144.15
50000 17.9/456 18.0/458 x 8.9/228 (3) 1000w-115v 5.0/127 12044-34 1730.49
72000 20.5/522 20.6/525 x 10.1/258.9 (2) 2000w-230v 5.0/127 12044-37 1935.06

12045 STIRMANTLE Aluminum Housing

Mantle with magnetic stirrer built-in, able to handle up to 72L spherical flask. Ideal
for continuous distillations. The variable speed control (included) offers total mixing
management. DC filtering allows the 1/50 hp motor to run cooler, thus extending motor
life. With four bottom, 4-inch high feet to allow bench clearance and air flow. Stir
motor control is detachable and allows speeds of 100–1850 rpm. Heaters are supplied
with a detachable four-foot cord on codes -12, -22; codes -50,-55 and -72 must be
hard wired. Temperature range is Ambient +10°C to 450°C. Supplied with .75-inch
diameter x 3-inch long magnetic stirring bar. CSA certified. Must be operated through
a temperature controller.
Maximum Flask
For Flask Size, mL Dia., in. / mm I.D. x Depth, inches/mm Watts/Volts Order Code Each
12000 11.5/293 11.6/295 x 5.7/147 (2) 650w–115v 12045-12 1452.00
22000 13.6/347 13.7/348 x 6.8/173.5 (2) 770w–115v 12045-22 1551.00
50000 17.9/456 18.1/460 x 8.9/228 (3) 1000w–230v* 12045-50 2086.00
12045 50000 (For Schott) 19.9/506 20/508 x 10.1/258.8 (3) 1000w–230v* 12045-55 2163.00
72000 20.5/522 20.6/525 x 10.1/258.8 (2) 2000w–230v* 12045-72 2160.00
*Codes -50, -55 and -72 must be hard wired. 115v units are also available in 230v versions.
12047 HEATING TOPS Fabric/Cloth

For use with 1-, 2- and 3-neck flasks. Top can be put on flask without disturbing
permanently attached equipment. mperature range is Ambient +10°C to 450°C.For
use with 12043, 12045, 12053 and 12058 mantles. With detachable 4-foot, 2-wire
cord and locking connector. 115v units are CSA certified. Must be operated through
12047 a temperature controller.
For Flask Size, mL Watts/Volts Order Code Each

1000 140w–115v 12047-19 268.00
2000 200w–115v 12047-21 277.00
3000 200w–115v 12047-23 306.00
5000 300w–115v 12047-25 387.00
12000 590w–115v 12047-27 646.00
22000 650w–115v 12047-29 697.00
50000 1000w–115v 12047-31 1082.00
72000 1000w–230v 12047-33 1248.00
All 115v units are also available in 230v versions.
12050 MANTLE Aluminum Housing, Low Profile

12050 For use with ACE 6530 and 6474 reaction assemblies. CSA certified. Easily fits into ACE
4-post reactor stands. Temperature range is Ambient +10°C to 450°C. Must be operated
through a temperature controller. With detachable 4-foot cord and locking connector.
For 6530 Assembly For 6474 Assemby

(Without Bottom Opening) (With Bottom Opening)
For Flask Order For Flask Order
Size, Liter Watts/Volts Code Each Size, Liter Watts/Volts Code Each
50 1000w–115v 12050-34 909.03 50 1000w–115v 12050-41 813.52
72 1300w–230v 12050-36 1530.57 72 1300w–230v 12050-43 1121.28
100 1600w–230v 12050-38 2044.00 100 1600w–230v 12050-45 1586.14
12053 MANTLE Aluminum Housing, Standard Height, Solid Bottom,

for Spherical Flasks
Solid, aluminum housed, heating mantles can be used on benches for smaller sizes
and can be used on floor or reactor stands for large flasks. Temperature range ambient
+10ºC to 450ºC. Must be operated through a temperature controller. Smaller sizes have
4-foot detachable cord with interlocking connector. Larger sizes, codes -31 through -37, 12053
are supplied with a terminal box for hard wiring. CSA approved.
For Flask Maximum Flask I.D. x Depth, Order
Size, mL Dia., in. / mm inches/mm Watts/Volts Code Each
1000 5.1/130 5.1/130 x 2.5/65 380w–115v 12053-19 271.00
2000 6.6/170 6.6/170 x 3.3/86 500w–115v 12053-21 282.00
3000 7.2/183 7.2/183 x 3.6/91.5 500w–115v 12053-23 336.00
5000 8.6/220 8.6/220 x 4.3/109.5 600w–115v 12053-25 417.00
6000 9.25/235 9.25/235 x 4.7/120.6 700w–115v 12053-26 906.51
12000 11.5/293 11.5/293 x 5.7/146.6 (2) 650w–115v 12053-27 779.00
10000 Schott 3.9/100 x 5.7/146.6 (2) 650w–115v 12053-28 786.76
22000 13.6/347 13.6/347 x 6.8/173 (2) 770w–115v 12053-29 898.00
20000 Schott 13.7/350 x 6.8/173 (2) 770w–115v 12053-30 904.49
50000 17.9/456 17.9/457x 8.9/228 (3) 1000w–115v 12053-31 1424.00
50000 Schott 18.3/465 x 8.9/228 (3) 1000w–230v 12053-32 1635.80
72000 20.5/522 20.5/522 x 10.1/258.9 (2) 2000w–230v 12053-33 1623.00
100000 Schott (2) 2000w–230v 12053-35 3226.29
200000 Schott (2) 2000w–230v 12053-37 3903.47
12053 MANTLE Aluminum Housing, Low Form, Solid Bottom,

for Cylindrical Flasks 12053
Solid, aluminum housed, heating mantles can be used on benches for smaller sizes and
can be used on floor or reactor stands for large flasks. Temperature range ambient +10ºC
to 450ºC. Must be operated through a temperature controller. Smaller sizes have 4-foot
detachable cord with interlocking connector. Larger size, code -45, is supplied with a
terminal box for hard wiring. CSA approved.
6000 8.7/222.2 7.73/194 x 2.22/56.4 180w–115v 12053-40 585.95
10000 8.7/222.2 7.73/194 x 2.22/56.4 180w–115v 12053-40 585.95
15000 9.9/251 9.9/251.5 x 5/127 250w–115v 12053-43 1047.62
30000 12.5/317.5 10.9/276.9 x 3.12/79.3 370w–115v 12053-45 744.73
50000 12.5/317.5 10.9/276.9 x 3.12/79.3 370w–115v 12053-45 744.73
12053 MANTLE Aluminum Housing, Standard Height, Bottom Opening

Aluminum housed, heating mantles with a bottom opening to accommodate flasks with
bottom valves. Can be used on benches for smaller sizes and can be used on floor or 12053
reactor stands for large flasks. Fits cylindrical and spherical flasks with bottom valves.
Temperature range ambient +10ºC to 450ºC. Must be operated through a temperature
controller. Smaller sizes have 4-foot detachable cord with interlocking connector. Larger
sizes are supplied with a terminal box for hard wiring. CSA approved.
For Flask Maximum Flask I.D. x Depth, For Flask Order
Size, mL Dia., in. / mm inches/mm Type Watts/Volts Code Each
600 7.63/193.8 7.63/193.8 x 2.22/56.4 Cylindrical 180w–115v 12053-61 717.37
6000 9.25/235 9.25/235 x 5/127 Spherical 700w–115v 12053-162 944.83
10000 7.63/193.8 7.63/193.8 x 2.2256.4 Cylindrical 180w–115v 12053-50 676.91
15000 9.06/230 9.06/230 x 2.75/69.9 Cylindrical 250w–115v 12053-64 874.66
30000 10.9/276.9 10.9/276.9 x 3.12/79.2 Cylindrical 370w–115v 12053-54 697.89
100000 14.38/365.3 14.38/365.3 x 4.12/104.7 Cylindrical 625w–115v 12053-70 936.71
200000 18.5/470 18.5/470 x 9.25/235 Cylindrical 775w–115v 12053-74 1462.92
200000 29.53/750 29.53/750 x 15/381.1 Cyl./Schott (4) 2000w–230v 12053-78 4360.53

12058
12058 MANTLE Aluminum Housing, Cylindrical Flasks
Resin and reaction flask mantle mainly used for ACE pressure reactors, but fit many other
cylindrical reaction flasks such as 6476, 6511-06 series, 6521, Aluminum housed with
solid bottom. The code -03 is for a flask with a flat bottom with rounded corners such
as the 6511-24 series. CSA approved. 4-foot detachable cord with locking connector.
Temperature range is ambient +10ºC to 450ºC. Must be operated through a temperature
controller.
For Flask Max. Flask I.D. x Depth, Order
500 (tall) 2.75/69.9 2.76/70 x 6.25/158.8 280w–115v 12058-03 622.85
500 (short) 4.38/111.3 4.5/114.3 x 3.0/76.2 250w–115v 12058-07 825.72
3000 6.38/162 6.4/162.6 x 6.0/152.4 600w–115v 12058-30 652.46
5000 6.38/162 6.4/162.6 x 10.9/276.9 1000w–115v 12058-33 864.71
12058
12058 MANTLES Aluminum Housing
Resin and reaction flask mantle. Bench top size with small footprint, aluminum housing.
For use with ONLY the following ACE flasks: 6521‑12, 6521‑14, 6472‑15, 6472‑20
and 6472‑25. CSA approved, 115 volt. Complete with 4-foot detachable cord with locking
connector. Must be operated through a temperature controller.
500 3.75/95.2 3.75/95.2 x 4.5/114.3 270w-115v 12058-08 312.00
1000 4.25/107.9 4.25/107.9 x 5.25/133.3 335w-115v 12058-12 325.00
2000 5.5/139.7 5.5/139.7 x 6.0/152.3 470w-115v 12058-16 335.00
3000 5.5/139.7 5.5/139.7 x 9.0/228.6 550w-115v 12058-22 376.00
4000 5.5/139.7 5.5/139.7 x 11.0/279.4 750w-115v 12058-28 410.00
12058 MANTLES Aluminum Housing, Cylindrical Flasks, Bottom Opening

12058 Resin and reaction flask mantle mainly used for ACE pressure reactors with a bottom
valve or outlet, but fit many other cylindrical reaction flasks such as 6518, 6522, 6521,
6300. The code -44 is for a flask with a flat bottom with rounded corners such as 6437
series. Aluminum housed with bottom opening. CSA approved. 4-foot detachable cord
with locking connector. Temperature range is ambient +10ºC to 450ºC. Must be operated
through a temperature controller.
For Flask Max. Flask I.D. x Depth, Order
500 (tall) 2.75/69.9 2.8/70 x 6.25/158.8 280w–115v 12058-44 676.56
500 (short) 4.38/111.3 4.4/111.8 x 3.0/76.2 250w–115v 12058-47 594.66
1000 4.25/107.9 4.28/109 x 5.25/133.4 335w–115v 12058-49 603.06
2000 5.5/139.7 5.7/144.8 x 6.0/152.4 470w–115v 12058-51 561.86
3000 6.38/162.1 6.4/162.6 x 6.0/152.4 600w–115v 12058-53 750.88
5000 6.38/162.1 6.4/162.6 x 10.8/276.4 1000w–115v 12058-55 884.42
12075 MANTLE Aluminum Housing, For Cylindrical Flasks

Resin and reaction flask mantle. Bench top size with small footprint. Aluminum housing 12075
for 6423, 6436, 6526, 6476, 6477, 9526, 6516-01, 6521-10,-12,-14, 6511-06,-42,-24,-53
ACE flasks. CSA approved, 115 volt complete with 4-foot detachable cord with locking
connector. Temperature range is Ambient +10°C to 450°C. Must be operated through a
temperature controller. 230V versions available.
1000 4.5 / 114.3 4.5/114.3 x 4.5/114.3 270w-115v 12075-08 334.00
2000 4.5 / 114.3 4.5/114.3 x 7.5/190.5 400w-115v 12075-10 348.00
3000 4.5 / 114.3 4.5/114.3 x 11/279.4 600w-115v 12075-12 386.00
6494 FLASK HEATER Fabric/Cloth

Specially designed glass/fiber cloth mantle with bottom opening and zipper for use
with 6491, 6492, 6518, and 6522 flasks to allow valve to protrude below heater. Upper
temperature limit, 450ºC. Must be operated through a temperature controller. CSA ap-
proved. Complete with 4-foot cord and locking connector.
For Flask I.D. x Depth, Order
6494
Size, mL inches/mm Watts/Volts Code Each
1000 4.625/117.4 x 5.625/142.8 300w-115v 6494-10 412.26
1500 4.625/117.4 x 6.625/168.2 380w-115v 6494-15 435.16
2000 4.625/117.4 x 8.875/225.4 450w-115v 6494-20 461.47
3000 4.625/117.4 x 10/254 600w-115v 6494-25 491.58
12032 BLANKETS Flask Insulating

Insulating blankets for jacketed reactor flasks. Over 1-inch thick blanket has a grey PTFE
material outside for chemical resistance and 1-inch (25.4mm) fiberglass insulator internal
for excellent insulating of jacketed reactor flasks. Blanket fits in between the Inlet/Outlet
ports on the flask. Each has an overlapping front flap with grommets and lace closure for
easy off/on. Non-electric nor heat. There are six different sizes to fit from 1L up to 100L
jacketed flasks.
Height, Width, Folded
mm mm I.D., mm For Flask Size, L Order Code Each
292 270 270 10 12032-03 457.19
457 315 315 20 12032-05 822.42
310 350 350 30 12032-07 587.29
310 562 460 50 (Low Profile) 12032-09 625.96
560 350 350 50 12032-11 1078.44 12032
510 510 510 100 12032-13 1703.35

12085 VOLTAGE CONTROLLER Mantle Minder II ™

For controlling all Glas-Col mantles. Time proportioning, 1/16 DIN, automatic control for
use with mantles, tapes, cords, small ovens, and other resistive heating loads up to 1800
watts at 120 volts. Features a detachable iron-constantan “J” thermocouple with 6-inch
stainless steel probe, lighted ON/OFF power switch with auxiliary indication, load and
thermocouple receptacles located on front panel for easy accessibility, and set point dial
calibrated in °C in 20 degree increments. Fused to protect small loads. Operates on 120
VAC, 50/60 Hz input. Range 0–750°C. Ambient temperature range 30–130°F. Accuracy
±1.5% of full scale. Supplied with three-wire load receptacle, three-wire line cord with
molded plug. Power consumption four watts plus load. Thermocouple included. Measures
12085 8 wide x 6 deep x 3-3/8 (inches) high.
Order Code Each

12085-20 569.00
12087 VOLTAGE CONTROLLER 0–120v at 10 Amps, Solid State

Variable control from zero output to 95% line voltage. A voltage-limit, rear-mounted center-
off switch is used to select a 40v or 120v maximum output with the control knob full on.
With 0–10 ammeter. 5% accuracy. (Since this is a solid state transformerless line voltage
controller, it is NOT recommended for heaters rated less than 120 volts.) Warning glow
light, mounted next to correcting switch, will illuminate when dangerous reversed wiring
condition exists. Simply flip the switch to extinguish the light and correct the condition.
Easy-access 10 amp fuse type 3 AG (rear mounted). Line voltage pilot light. Standard
1.8 meter heavy duty neoprene three-wire power cord (grounded to case) with NEMA
plug. Dimensions: 17.8cm (7 inches) x 10.2cm (4 inches) x 8.9cm (3-1/2 inches). Weight:
12087 794 grams. Input 120 volts, 60 cycles.
Order Code Each

12087-10 621.30
S IN C O R
P
AS Contact Ace Glass at
O
L
RA
ACE G
TH
800-223-4524
TED
A N N I V E R S A R Y and ask for a copy of our
1936 2011
IN U S A 75th Anniversary Laboratory

J
V
E L A N D, Glassware and Equipment

Catalog
Laboratory Glassware You can also view or download a
digital copy at our website
& Equipment Catalog
www.aceglass.com

Mantle Guide
Heating Mantles for 6521 and 6522 Cylindrical Reaction Flasks
The corresponding 12053 aluminum mantles have a 2-inch bottom opening to match the bottom outlets on the 6522 series flasks.
The 12053 mantles for the 6521 flask have a solid bottom.
Aluminum Hard Mantles Fiber/Soft Girdle Mantles

For Flask For
Size, Liters Flask No. Watts/Volts Order Code Each Watts/Volts Order Code Each
1 6521-10 — — 300w-115v 6478-10 322.54
1 6522-11 — — 300w-115v 6494-10 412.26
2 6521-12 — — 450w-115v 6478-20 374.61

2 6522-13 — — 450w-115v 6494-20 461.47
3 6521-14 — — 600w-115v 6478-25 381.58

3 6522-15 — — 600w-115v 6494-25 491.58
6 6521-16 180w-115v 12053-40 585.95 495w-115v 12041-10 860.65

6 6522-17 180w-115v 12053-61 717.37 495w-115v 12041-10 860.65
10 6521-20 180w-115v 12053-40 585.95 495w-115v 12041-10 (2) 860.65

10 6522-21 180w-115v 12053-50 676.91 495w-115v 12041-10 (2) 860.65
15 6521-25 250w-115v 12053-43 1047.62 2-880w-115v 12041-12 777.15

15 6522-26 250w-115v 12053-64 874.66 2-880w-115v 12041-12 777.15
30 6521-30 370w-115v 12053-45 744.73 2-825w-115v 12041-32 979.40

30 6522-31 370w-115v 12053-54 697.89 2-825w-115v 12041-32 979.40
50 6521-35 370w-115v 12053-45 744.73 3-1100w-115v 12041-37 1617.65

50 6522-36 370w-115v 12053-54 697.89 3-1100w-115v 12041-37 1617.65
100 6521-40 625w-115v 12053-56 Call 4-1200w-115v 12041-48 2222.22

100 6522-41 625w-115v 12053-70 936.71 4-1200w-115v 12041-48 2222.22
200 6521-44 775w-115v 12053-58 Call 4-1100w-115v 12041-52 2228.41

200 6522-45 775w-115v 12053-74 1462.92 4-1100w-115v 12041-52 2228.41
Stirrers, Trubore® 175
S I N C O R
S P
A
O
L
RA
ACE G
TH
TED
1936 2011
VI USA
N
J
NE ,
LAND

176 Stirrers, Trubore®
General Stirring Information LA

SS INN OV
AT
TH
ACE
Bearings: Glass, Polished: use only in
I ON
8044 glass, pressure bearings or
Trubore®, glass bearings are for use with precision-ground glass Trubore® bearings with a PTFE
shafts or PTFE-covered, stainless steel (8071) shafts. They are inner component (8066) or our A N N I V E R S A R Y
not recommended for use with polished glass or plain, stainless 13443 PTFE collet type, 8050 1936 2011
steel shafts. PTFE mechanical seal and 13445
J
PTFE debris-free bearings. IN
N
Trubore® bearings with a PTFE Inner component are for use with
E ,
polished glass shafts and plain, stainless steel shafts. They are Glass, Precision-Ground: use LAND
not recommended for precision-ground glass shafts or PTFE- only Trubore glass bearings
®
covered, stainless steel shafts. such as our 8059, 8060, 8061,

Glass pressure bearings (8044) are for use with 8074 plain stainless 8065, etc. series, or our 13443 PTFE collet seal type and 8050
steel or 8075 polished glass shafts. PTFE mechanical seal bearings.
8050 Mechanical Seal Bearing may be used with polished or Stainless Steel, Plain: use only in 8044 glass, pressure bearings
precision-ground glass and plain stainless steel shafts (10, 19 or Trubore® bearings with a PTFE inner component (8066) or our
& 28mm). Not recommended for use with PTFE-covered shafts. 13443 PTFE collet type, 8050 PTFE mechanical seal and 13445
debris-free bearings.
13443 PTFE Collet Bearing may be used with any type shaft
(6, 8 & 10mm). Stainless Steel, PTFE-Covered: use with Trubore® glass bearings
such as our 8059, 8060, 8061, 8065, etc. series, or our 13443
13445 Debris-free PTFE Bearing should be used with polished PTFE collet type bearings. Not recommended for use with our
glass shafts or plain, stainless steel shafts. They are not PTFE debris-free 13445 bearing.
recommended for precision-ground glass shafts or PTFE-covered,
stainless steel shafts (6, 10 & 19mm).
Stirring Shafts:
Trubore Stirring Equipment — Precision Fit and Performance

®
Bearings and shafts guaranteed 1mm absolute with unlubricated introduced into a solvent system
interchangeable surfaces at speeds less than 100 reaction, they will not react with
Trubore® stirrers, pioneered and rpm. It also means that plastic your product, but will be removed
developed by Ace, are the most shafts, including Fluorocarbon with the solvent. Under no
widely used precision glass coated glass shafts, may be used circumstances should glycerin
stirrers in research today. with bearings — a practice not be used; it acts as a grinding
If both shaft and bearing of a feasible with ground bearings. medium rather than a lubricant.
given size are manufactured by Note that only a small lubricant
Operation well is provided at the top of
Ace, we guarantee them to be
If the components have been some ACE bearings; this is
interchangeable.
p ro p e r l y c l e a n e d p r i o r t o because only a slight amount of
Precision fit and performance operatition, a Trubore® stirring Stir-Lube® is needed for many
Every shaft and bearing is unit can be run unlubricated for a hours of stirring.
individually inspected to insure limited time at a maximum speed
clearance fit of less than .025 mm of 500 rpm. Care and cleaning
(0.001-inch). For continuous operation, or Because of the very close fit
ACE bearings are smooth operation at speeds greater than between shaft and bearing, a
and transparent. This feature 500 rpm, proper lubrication is slight amount of dust or grit
automatically reduces leak required. We recommend ACE will quickly scratch the smooth
path for a given fit clearance 8117 Stir‑Lube® be used as a surface of the bearing. To prevent
and surface roughness; it also proper all-purpose lubricant up this, both shaft and bearing
prolongs bearing life. to 2000 rpm (water cooled) or should be washed with a good
Special “plateau” grinding 1500 rpm (non-cooled). detergent and dried with acetone
is employed on shafts. This For high-speed stirring over — instead of with a wiping cloth
provides maximum smoothness 2000 rpm, we recommend — prior to use.
consistent with optimum a thin base of 8229 grease ACE lubricants may be
retention of lubricant. In terms with application of 8119 Hi- completely removed with
of performance, this texture Lube heavy-duty liquid stirrer acetone or most other ketones.
means a low leak rate, which lubricant. Both materials are also
permits attainment of at least chemically inert. If accidentally
Matching ACE Stir Bearings to the Appropriate Shafts

Use with ACE Code Stirring Shafts
Bearing Type Size ACE Stir Bearing Codes Listed Below
Trubore®, Glass 5mm 9524‑04, 9527‑08 9534‑04, 9535‑06, 9541‑04, 9541‑15
Trubore®, Glass 6mm 9524‑06, 9524‑08, 9527‑12, 9527‑14, 9529 9534‑06
Vacuum 9mm 8098, 8099, 8133, 9528 8134, 9530
8036, 8038, 8039, 8040, 8042, 8043, 8047,
Trubore®, Glass 10mm 8068, 8070, 8071, 8073, 9532, 9533
8051, 8053, 8055
Trubore®, Glass 10mm 8041 Complete Assemblies
Trubore®, Glass 19mm 8059, 8060, 8061, 8065 8076*, 8077, 8078, 8079
Glass, Pressure 10mm 8044 8074, 8075
Trubore , PTFE/Glass
®
10mm 8066 (Plain), 8066 (Debris Trap) 8074, 8075
Trubore®, PTFE/Glass 19mm 8067 (Trubore®), 8067 (Debris Trap) 8076
Trubore , PTFE/Glass
®
28mm 8067 (Trubore ), 8067 (Debris Trap)
®
8080
Mechanical Seal/PTFE 10mm 8050 8068, 8073, 8074, 8075, 9532, 9533
Mechanical Seal/PTFE 19mm 8050 8076, 8077, 8078
Mechanical Seal/PTFE 28mm 8050 8080
Collet Type/PTFE 6mm 13443-06, 13443-08 9534-06, 9534-40
Collet Type/PTFE 8mm 13443-10 9534-06, 9534-40
8068, 8070, 8071, 8073, 8074, 8075,
Collet Type/PTFE 10mm 13443-12
9532, 9533
PTFE 6mm 13445-06, 13445-09 9534-40
PTFE 10mm 13445-30, 13445-32, 13445-34, 13445-36 8074, 8075
PTFE 19mm 13445-46, -44 8076
*Polished shaft not recommened for 8076.
Custom Pilot Plant Reactor Designs

Selecting components and designing a Pilot Plant System requires you to
consider specific site and application aspects, such as:
• Space limitations: what depth, width and height • How much distance is needed below the bottom of
are available for the support stand, stirrer motor, the reactor outlet?
condenser, etc.? • What type of stirring motor (air, electronic, for haz-
• Do you want a domed or flat head reactor? ardous or non-hazardous location)?
• What will be the operating temperature? • What type of stirrer shaft (glass or PTFE)?
• Vacuum or pressure? • Heat exchange coil needed? PTFE-covered copper or
• What type bottom outlet (standard, threraded, stop- other type metal?
cock, “sink” type valve, etc.? • What accessories are needed (condensers, take-offs,
• Do you want temperature monitoring/control? adapters, spargers, gas inlet/outlet, etc.?
Custom Assemblies
In addition to our standard 10 through 200 L Cylindrical and Spherical Assemblies, ACE can
assist you in designing a specific component reactor. Many of the dimensions and items listed
can be modified to accommodate your needs.
Consult ACE by calling our Technical Design and Support Staff toll-free at 1‑800‑223‑4524 or
visiting us on the web at www.aceglass.com.

ACE Stir Shaft Quick Reference Chart

Size Recommended Use
Ace Code O.D., mm L, mm Type Material Bearing Chuck Agitators
9534-04 5 318 9524-04, 9527-08, 9524-06,-08,
Solid Ground Borosilicate Glass
9534-06 318 9529, 9527-12, 9527-14
6 Button Bottom 9542
9534-40 318 Solid Polished Borosilicate Glass 8066-120
9535-06 318 Hollow Borosilicate Glass
9541-04 5 318 Solid Ground Borosilicate Glass 9524-04, 9527-08 8124, 8126 9541-06
Knob Bottom
9541-15 318 PTFE Coated Stainless Steel 9541-07
8134-15 380 With Paddles Attached
8134-25 9 610 Solid Polished Borosilicate Glass 8133, 9528, 8098, 8099 8083, 8084, 8085, 8086
9530 416 9530
8068-02 440 Button Bottom 8083, 8082, 8085,
8068-03 580
8068-04 690 8086,8087,8096
8068-06 740 Solid Ground Borosilicate Glass
8068-08 440 Multi-Blade 8036, 8038, 8039, 8040, 8041,
8068-17 580 Attached
Double Multi-Blade 8042, 8043, 8047, 8051, 8053,
8068-18 440
8068-25 440 8055, 13443,8050 8083, 8082, 8085,
Button Bottom Hollow Ground Borosilicate Glass
8068-27 580 8086,8087,8096
8068-30 440
8068-31 690 Bead Bottom Solid Ground Borosilicate Glass 8089, 8090,8088
8068-32 580
8070-05 440 8083, 8082,
8070-10 690 Button Bottom PTFE Coated Glass 8036, 8038, 8039, 8040, 8041, 8085,8086,8087,8096
8071-05 460 8042, 8043, 8047, 8051, 8053,
8071-07 640 Bottom Drilled Hole PTFE Coated Stainless Steel 8055, 8066, 8133,13443 8089, 8090, 8088
8071-10 690
8036, 8038, 8039, 8040, 8041,
8073 410 Crescent Shaft Solid Ground Borosilicate Glass 8042, 8043, 8047, 8051, 8053, Attached
10 8055, 8066, 8133, 13443, 8050
8074-02 420
8082,8083,8085,8086,
8074-04 450 Remove Button Bottom Stainless Steel 8044, 8055, 8066, 13443, 13445
8096, 8094, 8095
8074-07 580
8075-12 440 8083, 8082,
8075-14 580 Button Bottom
8075-15 690 8085,8086,8087,8096
8075-21 440 8044, 8066
8075-23 580 Plain Shaft Solid Polished Borosilicate Glass 8124, 8125, 8094, 8095
8075-24 690 8126
8075-32 440
8075-34 580 Bead Bottom 8044, 8066,8050,13443, 13445 8088, 8089, 8090
8075-36 690
8036, 8038, 8039, 8040, 8041,
9523 445 Hollow Polished Borosilicate Glass 8042, 8043, 8047, 8051, 8053,
8055, 8066, 8133,13443,8050
Complete W/Vanes Attached
8043, 8047, 8050, 8051, 8036,
9533 475 Solid Ground Borosilicate Glass 8038, 8039, 8040, 8041, 8042,
8053, 8055, 13443, 13000
8076-05 700
8076-07 900 Button Bottom Hollow Polished Borosilicate Glass 8085
8076-10 1200
8076-40 900 Bottom Drilled Hole Solid Polished Borosilicate Glass
8076-42 800 Bottom Knob Hollow Polished Borosilicate Glass 8067, 13445, 8050
8076-44 1200 Bottom Knob Hollow Polished Borosilicate Glass 8091, 8100,8092,8093
8076-46 1400 Bottom Knob Hollow Polished Borosilicate Glass
8076-48 19 1400 Bottom Drilled Hole Solid Polished Borosilicate Glass
8077-23 700
8059, 8060, 8061,8065,
8077-25 900 Button Bottom Solid Ground Borosilicate Glass 8085
8059, 13445
8077-27 1200
8078-05 900 8059, 8060, 8061, 8050,
Bottom Knob Hollow Ground Borosilicate Glass 8091, 8100, 8092, 8093
8078-10 1200 8065,13445
8079-03 700
8079-05 900 Bottom Drilled Hole PTFE Coated Stainless Steel 8059, 8060, 8061, 8065 8091, 8092, 8093,8100
8079-10 1200
8080-12 1010
8080-14 1140
8080-18 1320 6472-15,
8080-22 28 1470 Bottom Drilled Holes Solid Polished Borosilicate Glass 8067, 8050 6472-155, 8091, 8093, 8101
8080-24 1400 6472-156
8080-25 2030
8080-30 1600
5 & 6mm Shafts, Bearings & Agitators

9524 BEARING Trubore®, 5 & 6mm
Trubore® bearing with standard taper joint for use with our 9534, 9535 and 9541 precision 9524
ground stir shafts. Lubricant well at top will accept enough 8117 Stir-Lube to provide
hours of operation at up to 1000 rpm. Match bearing I.D. with stir shaft O.D.
Joint I.D., mm Order Code Each

14/20 5 9524-04 46.94
14/20 6 9524-06 48.34
19/22 6 9524-08 50.33
9527 BEARING Trubore®, Water Cooled, 5 & 6mm

Jacketed, Trubore® bearing with standard taper joint for use with our 9534, 9535 and
9541 precision ground stir shafts. Hose connections fit 5/16-inch or 3/8-inch ID tubing.
Match bearing ID of 5mm or 6mm to stir shaft O.D. 9527
Joint I.D., mm Order Code Each
14/20 5 9527-08 87.55
14/20 6 9527-12 90.02
19/22 6 9527-14 92.84
9529 BEARING Trubore®, Economy, 6mm

Trubore® bearing, heavy duty, standard taper joint, self-aligning. Unique design is forgiving
of slight misalignment of stir motor and shaft. Recommended for use with our 9534 6mm 9529
precision ground stir shaft. Glass member has  19/22 inner joint.
Order Order
Code Each Code Each
Inner Bearing, only 9529-04 33.13 Ace‑Thred Adapter 5030-04 27.92
Bushing, w/O‑Ring 9529-07 28.89 Complete 9529-10 89.94
Size –110 FETFE
7855-716 15.66
O‑Ring, Pk. 12
E-SA
AC
FE
ON
OR
C
N ECT
9534 STIRRING SHAFT 5 & 6mm, Glass

Button type solid glass stirring shafts, 5mm & 6mm O.D. Precision ground shafts, codes
-04 & -06, should be used in matching glass Trubore® 9524 and 9527 bearings. Polished 9534
shaft, code -40, should be used only in our 8066-120, 6mm PTFE inner bearing. All accept
our 9542 blades. Join to stirrer motor using 8124 series chucks. 318mm overall length
ideal for use in 250ml and smaller flasks.
Rod Size O.D., mm Glass Type Order Code Each

5 Ground 9534-04 35.53
6 Ground 9534-06 37.18
6 Polished 9534-40 42.71

180 Stirrers

13443 STIRRER BEARING PTFE, 6mm
13443 Inert PTFE stirrer bearing. Features a totally enclosed bearing body for non-shedding,
anti-whip, chemically resistant design. The bearing can also be used in slight vacuum or
slight pressure applications. The design has a composite PTFE/PEEK main internal seal
and a specially fabricated glass ball-bearing for rigidity and smoothness during lengthy
operation. Maximum recommended speeds up to 500 rpm continuous operation. Ideal for
glass, metal or PTFE stir shafts. Bottom is a molded, inner standard taper joint. Average
length is 96mm and 45mm OD at bearing center.
Joint Order Code Each

19/22 13443-06 349.97
24/40 13443-08 349.97
13445 BEARING Debris Free, PTFE, 6 mm

Vacuum tight (~5 Torr), flake free, chemically resistant stirrer bearing makes a mechanical
seal against a polished glass shaft. Debris trap section consists of a PTFE sleeve for a
wide range of joint and shaft diameter sizes. For use with 6 mm polished glass or stainless
steel shafts, NOT recommended for PTFE shafts. Bearing consists of a PTFE standard
taper body with added PEEK for better stability, glass filled polypropylene screw cap,
PEEK compression spring, PTFE/PEEK sleeve and a glass filled polypropylene loosening
nut. For use up to 500 rpm.

19/22 13445-06 171.73
24/40 13445-09 173.37
13445
Replacement Seals & Springs:
Order Code Each
PTFE/PEEK sleeve seal 13445-302 32.16
PEEK compression spring 13445-304 35.26
Stirrers 181

9535 STIRRING SHAFT Hollow Glass, 5mm
Precision ground, hollow, 5mm glass stirring shaft. Button type shaft accepts 9542 blades
and can be used in matching 9524 and 9527 bearings. Holes are provided in the side of
the shaft for material introduction and at the bottom for emission into the flask contents. 9535
Join to stirrer motor using 8124 series chucks.
Shaft Size O.D., mm Order Code Each

5 9535-06 49.32
9541 STIRRING SHAFT with PTFE Agitator, 5mm

Stirring shaft agitator combination available in either a solid, precision ground glass
shaft or all PTFE knob type shaft with a PTFE snap-fit agitator designed to fit through
 14/20 and 18/11 joints. Designed for use with our 5mm I.D. 9524 or 9527 bearings
and flasks of 50ml and smaller.
Rod Agitator Complete

Order Order Order
Type Rod Code Each Code Each Code Each 9541
Glass 9541-04 32.03 9541-06 71.08 9541-10 103.11
PTFE 9541-15 37.90 9541-07 71.08 9541-40 108.98
9542 STIRRING BLADE 5 & 6mm

PTFE stirring blades for use with our button type 9524 and 9527 stirring shafts. Blades
are 41mm wide x 12mm high and are designed for use in flasks 250ml and less. Match
blade to shaft O.D.
Rod Size O.D., mm Order Code Each 9542

5 9542-10 9.45
6 9542-20 9.45
8124 CHUCK “Flex-Grip,” 5 & 6mm

Nylon chuck for use with ACE stirring shafts or other shafts of the same dimensions. Chuck
has flexible insert which allows for misalignment of shaft without danger of breakage.
For Stirring For Motor
Shaft Size, mm Shaft, mm (In.) Order Code Each
8124
6 6.4 (1/4) 8124-04 39.72
5 8 (5/16) 8124-05 37.74
6 8 (5/16) 8124-07 37.51
Insert Only Size Qty. Order Code Per Package

6 mm 6 8124-24 17.04
5 mm 6 8124-26 17.04

182 Stirrers
9mm Shafts, Bearings & Agitators

8133 BEARING High Speed Vacuum,9mm
Used with 8111 aluminum packing box. For shaft speeds of 1000 r.p.m. and higher,
and vacuum operation down to 0.5mm Hg. The seal is made entirely by the packing
box. Only infrequent lubrication is required using 8122 packing and 8117 Stir-Lube. We
8133-10,
-15 recommend that you use 8113 vacuum adapter to avoid contaminating the flask contents
with lubricant. For use with 9mm O.D. shafts.
Bottom Joint Order Code Each

24/40 8133-10 54.03
29/42 8133-15 61.76
8133-40 35/25 8133-40 52.01
8098 STIRRER BEARING Vacuum, 9mm

A rugged, compact, inexpensive stirrer. The upper member turns with stirring shaft,
8098-12 bottom member remains stationary. Upper member supplied with vinyl connector. Use
with ACE 8134 size 9mm stirring shafts. Assembly may also be used to make your own
rotary evaporator.
Lower Member Upper Member Complete
Order Order Order
Joint Code Each Joint Code Each Code Each
24/40 8098-04 60.19 18/10 8098-01 25.02 8098-12 85.21
Qty. Order Code Per Dozen

Vinyl Connector only, for all sizes 12 8098-45 37.77
8134 STIRRING SHAFTS 9mm

E Unground, 9mm OD shaft for use in liquid seal bearings and our debris free 8098 and
8099 stirrer assemblies. Code -25 is a button type shaft which accepts our 8083, 8084,
8085 and 8086 blades. Shaft length accommodates flasks from 500ml to 5000ml.
Style Length, mm Order Code Each

C 380 8134-15 33.18
C
E 610 8134-25 18.85
8134
9528 VACUUM STIRRER BEARING ASSEMBLY 9mm

9528 Rotating ball joint seal gives vacuum-tight connection good into the micron range.
Ultimate vacuum is determined primarily by the tightness of the vinyl tubing connector
which fastens the unground shaft to the ball member. Operate below 500 rpm. Use with
unground stirring shafts (8134,9530). Lubricate the 18/11 rotating ball joint with our
8117 Stir-Lube. Bottom joint is  19/22. Upper member is supplied with a vinyl connector.
Order Order Per
Code Each Qty. Code Dozen
Upper Member 9528-02 32.30
Lower Member 9528-04 66.80 Vinyl Conn., only 12 8098-45 37.77
Complete 9528-10 99.10
Stirrers 183

8099 STIRRER BEARING Vacuum, Threaded, 9mm 8099
Modified version of 8098 in that upper member is internally threaded on the top. #7
Ace‑Thred nylon bushing and FETFE o‑ring form a compression seal on stirring shaft in
place of the conventional tubing arrangement. Easier to adjust shaft, suitable for vacuum
work. For use with 8134 stirring shafts.
E-SA
AC
FE
Lower Member Upper Member Nylon Bushing Complete
ON
OR
C
Joint Code Each Joint Code Each Code Each Code Each N ECT
24/40 8098-04 60.19 18/10 8099-03 40.77 8099-38 19.97 8099-40 119.90
9530 STIRRING SHAFTS 9mm

Unground, 9mm O.D. stirring shaft design for use with our 9528 vacuum and debris free
stirrer assembly. 380mm straight section, 416mm overall length. Use our 9530-08 blade. 9530
Order Code Each

Rod 9530-04 21.22
Blade 9530-08 10.73


8036 BEARING Trubore®, 10mm
Interchangeable bearing designed to be used with our precision ground stirring shafts
(8068, 8070, 8071, 8073, 9532, 9533). Recommended top stirring speed with our 8117
8036 Stir-Lube is 1500 rpm.
Order Code Each

8036-10 39.94

Interchangeable ground joint bearing for use with our precision ground stirring shafts
(8068, 8070, 8071, 8073, 9532, 9533). Recommended top stirring speed with our 8117
Stir-Lube is 1500 rpm.

19/22 8038-04 73.43 35/20 & 35/25 8038-40 77.20
19/38 8038-05 71.27 65/40 8038-55 92.20
24/40 8038-10 74.38
29/42 8038-20 74.96
34/45 8038-30 75.09
8038-10 8038-40 45/50 8038-32 80.41

Interchangeable ground joint bearing with top lubricant well for use with our precision
ground stirring shafts (8068, 8070, 8071, 8073, 9532, 9533). Recommended top stirring
8039-10 8039-35 speed with our 8117 Stir-Lube is 1500 rpm.

19/22 8039-03 79.08 35/25 8039-35 86.26
19/38 8039-05 79.08
24/40 8039-10 79.55
29/42 8039-20 84.01
34/45 8039-25 85.80
8040 BEARING Trubore®, Water-Cooled, 10mm

Interchangeable, ground joint bearing with jacket for water cooling. May be operated
as high as 2000 rpm using our 8119 high-speed lubricant. Can be operated at 1500
rpm unevacuated using our 8117 Stir-Lube. Hose connections for use with 5/16-inch
or 3/8-inch ID tubing. Available with PTFE-clad joint to eliminate the need for grease.
Use with our precision ground stirring shafts (8068, 8070, 8071, 8073, 9532, 9533).

24/40 8040-10 104.16 35/20 & 35/25 8040-40 114.01
29/42 8040-20 107.01 65/40 8040-55 217.99
34/45 8040-30 111.06
45/50 8040-35 120.39
8040 BEARING Trubore®, Water-Cooled, PTFE-Clad, 10mm

Similar to 8040, above, except bottom joint is PTFE-clad to eliminate the need for grease.
8040-40 8040-10
8040-60 Joint Order Code Each
24/40 8040-60 149.22
29/42 8040-64 149.33
34/45 8040-68 152.43
45/50 8040-70 156.31

Complete®
8041 STIRRER ASSEMBLY Glass Blade, 10mm
Trubore
Precision Trubore® Stirrer Assembly consisting of 10mm I.D. glass bearing, ground Assemblies
glass shaft with button, and glass blade. Bearing consists of inner glass bearing, #15
bushing, FETFE o‑ring and threaded glass adapter (see bearing only listing under 8042).
For Flask Order
Cap., mL Joint Bearing No. Shaft No. Blade No. Code Each
250- 500 24/40 8042-115 8068-03 8083-08 8041-11 135.83
500- 1000 29/42 8042-117 8068-03 8083-12 8041-15 158.66
2000- 3000 29/42 8042-117 8068-03 8083-16 8041-19 158.80
5000-12000 45/50 8042-121 8068-02 8083-20 8041-20 180.38
Replacement size –110 FETFE o‑ring, Pk. 12 7855-716 15.66
8041 STIRRER ASSEMBLY PTFE Blade, 10mm

Precision Trubore® Stirrer Assembly consisting of 10mm I.D. glass bearing, ground
glass shaft with button, and PTFE blade. Bearing consists of inner glass bearing, #15
bushing, FETFE o‑ring and threaded glass adapter (see bearing only listing under 8042).
For Flask Order
8041-11
250- 500 24/40 8042-115 8068-03 8085-07 8041-30 137.11
500- 1000 29/42 8042-117 8068-03 8085-11 8041-34 141.10 E-SA
AC
8041-30
FE
2000- 3000 29/42 8042-117 8068-03 8085-15 8041-38 144.99
5000-12000 45/50 8042-121 8068-02 8085-19 8041-40 169.77 ON
OR
C
N ECT
Replacement size –110 FETFE o‑ring, Pk. 12 7855-716 15.66
8042 BEARING Trubore®, Glass*, Ace‑Thred, 10mm

Self-aligning three-piece bearing. Complete consists of inner Trubore® glass bearing, #15
nylon bushing with FETFE o‑ring, and threaded adapter. Unique design eliminates costly E-SA
AC
FE
replacement since inner bearing will spin if shaft binds or will self-align at o‑ring seal in
the event the motor is slightly cocked. Inner bearing and bushing can be used with any ON
OR
C
joint size. For use with 10mm O.D. shafts 8068, 8070, 8071, 8073, 9532, and 9533. For N ECT
replacement size –110 FETFE o‑ring, order 7855-716.
Order Code Each

Inner Bearing, only 8042-05 27.48
#15 Bushing with size –110 FETFE O‑Ring 8042-09 27.69
Threaded Glass Adapter, only Complete Assembly

24/40 8042-15 31.22 24/40 8042-115 86.39
29/42 8042-17 33.38 29/42 8042-117 88.55
34/45 8042-19 39.78 34/45 8042-119 94.95
45/50 8042-21 50.57 45/50 8042-121 105.74
8042-35 35.92 8042-135 91.09
8042-135 8042-115
35/25 35/25
*For assembly with inner PTFE bearing, see 8066.


8043 BEARING Trubore®, Ace‑Thred, 10mm
8043 Designed for use with #25 Ace‑Thred bushing. Consists of a Trubore® bearing, pressure
bushing, gland with two FETFE o-rings and retainer bushing with FETFE o-ring. For use
with our precision ground stirring shafts (8068, 8070, 8071, 8073, 9532, 9533).
Order Code Each

Bearing, only 8043-08 85.78
E-SA Pressure Bushing 8043-16 26.94
AC
FE
Gland with Two O‑Rings 8043-20 15.14

ON Retainer Bushing with O‑Ring 8043-30 41.79
OR
C
N ECT Complete 8043-45 169.65
E-SA 8044 BEARING Pressure, with Ace‑Threds, 1 0mm

AC
FE
Glass bearing with #15 Ace‑Thred at each end and glass tubing between for use with
ON
10mm O.D. 8074 and 8075 stirring shafts. PTFE coupling, with internal FETFE o‑ring
OR
C
N ECT seal, connects bottom of bearing to either #15 or #25 Ace‑Thred on vessels such as 6433
pressure reactor head or one-piece pressure reactors. Top bushing also has an internal
FETFE o‑ring seal for additional seal on shaft to allow pressure reactions. Maximum
operating speed 600 rpm. Coupling and bushing supplied with FETFE o‑rings. For
replacement o‑rings: for #15–#15 coupling, 7855-730 external, 7855-716 internal; for
#15–#25 coupling, 7855-730 and 7855-742 external, 7855-716 internal; for #15 bushing,
7855‑730 external, 7855-716 internal.
For Coupling to #15 Ace‑Thred For Coupling to #25 Ace‑Thred
Order Order
Code Each Code Each
Glass Bearing, only, #15-#15 8044-07 39.14 Glass Bearing, only, #15-#15 8044-07 39.14
8044-24 8044-55 Coupling, PTFE, #15-#15 5840-60 113.73 Coupling, PTFE, #15-#25 5843-62 128.31
Bushing, PTFE, #15 8044-13 80.21 Bushing, PTFE, #15 8044-13 80.21
Complete 8044-24 233.08 Complete 8044-55 247.66
8047 BEARING Trubore®,10mm
This glass bearing is supplied with tubulation for feeding inert gases around the
bearing to balance any pressure possibly being developed in the flask. Can also
8047
be used for gas-liquid reactions and gas dispersions using hollow shafts as listed
under 8068 and 9532. I.D. is 10mm. Also for use with 8070, 8071, 8073, and 9533
10mm shafts. Use with 3/8-inch or 5/16-inch I.D. tubing, size C hose connection.
24/40 8047-10 127.94
29/42 8047-15 129.99

Used with 8111 aluminum packing box. It may be used for low positive pressure and
vacuum applications. Using the graphite-impregnated PTFE packing 8122 and 8117
ACE Stir-Lube, a very high film strength lubricant, pressures down to 7 microns have
been obtained at 170 rpm using only a mechanical pump. Speeds over 1000 rpm are not
advisable due to the heat generated. Lubrication (4 or 5 drops) is required at intervals
depending on the speed of operation (about every two hours at 200 rpm). Packing life
is indefinite. Frequent tightening of the packing box is unnecessary once the packing
has run in. The high-vacuum lubricant trap adapter, No. 8113, prevents lubricant from
running into material being stirred. I.D. is 10mm. For use with 8068, 8070, 8071, 8073,
9532, and 9533 shafts (10mm).

24/40 8051-10 136.81 35/20 & 35/25 8051-35 137.49
29/42 8051-15 137.49 8051-10 8051-35
34/45 8051-20 141.17
45/50 8051-25 100.15
8053 BEARING Trubore®,10mm
Especially useful for controlled atmospheric work. Used with 8068 solid shaft to balance
small pressure differentials across the bearing. Used with No. 8068 hollow shafts for
introduction and dispersion of gaseous catalysts, etc. Holes in bearing and shaft coincide.
I.D. is 10mm. Use with 3/8-inch I.D. tubing, size D hose connection. 8053
24/40 8053-10 204.41
8055 BEARING High Vacuum, Trubore®, 10mm 8055

This bearing is the standard liquid seal type except that the use of Trubore® tubing enables
this unit to perform very satisfactorily under high vacuum conditions. I.D. is 10mm. For
use with 8068, 8070, 8071, 8073, 9532, and 9533 10mm shafts.

24/40 8055-10 142.03
8050 STIRRER BEARING Mechanical Seal, PTFE, 10mm New

Newly designed mechanical stirrer bearing from ACE. All PTFE, Rulon or PEEK wetted
area construction provides for low extractables. Completely contained bearing and
internal parts also provides non-shedding of materials into the reaction. The bearing is
excellent for vacuum applications and can be operated at sub-torr levels. Rated for up
to 400 rpm speeds. It can be used on either glass polished or stainless steel 8068, 8073,
8074, 8075, 9532, and 9533 stir shafts. See below for joint sizes.
Joint Size Order Code Each

24/40 8050-02 547.19
29/42 8050-04 577.60
#15 Ace‑Thred 8050-10 596.17
#25 Ace‑Thred 8050-12 614.21 E-SA
AC
FE
8050
Replacement size –116 Outside FETFE o‑ring, Pk. 12 7855-726 26.57
ON
OR
C
N ECT

Complete 10mm Shafts, Bearings & Agitators

Trubore®
Assemblies 8064 STIRRER ASSEMBLY Glass Shaft, PTFE Blade, 10mm
Precision Trubore® stirrer sssembly consisting of 10mm I.D. glass and PTFE bearing,
polished glass shaft with button, and PTFE blade. Bearing consists of PTFE inner
bearing, glass-filled PTFE bushing and lock nut, compression saddle with FETFE o‑ring
and threaded glass adapter (see complete component listing under 8066).
For Flask Order
250- 500 24/40 8066-43 8075-12 8085-07 8064-13 177.93
500- 1000 29/42 8066-46 8075-12 8085-11 8064-18 183.27
2000- 3000 29/42 8066-46 8075-12 8085-15 8064-21 187.16
5000-12000 34/45 8066-50 8075-14 8085-19 8064-22 199.21
5000-12000 45/50 8066-55 8075-14 8085-19 8064-24 213.21
8064 STIRRER ASSEMBLY Stainless Steel Shaft, PTFE Blade, 10mm

8064-34 Precision Trubore® stirrer assembly consisting of 10mm I.D. glass and PTFE bearing,
polished stainless steel shaft with button, and PTFE blade. Bearing consists of PTFE
inner bearing, glass-filled PTFE bushing and lock nut, compression saddle with FETFE
o‑ring and threaded glass adapter (see complete component listing under 8066).
For Flask Order
8064-13 E-SA
250- 500 24/40 8066-43 8074-02 8085-07 8064-34 262.26
AC
FE
500- 1000 29/42 8066-46 8074-02 8085-11 8064-39 267.60

ON
OR
2000- 3000 29/42 8066-46 8074-04 8085-15 8064-42 277.76

C
N ECT
5000-12000 45/50 8066-55 8074-07 8085-19 8064-45 305.68
8066 BEARING Trubore®, PTFE, Ace‑Thred,10mm

Self-aligning, lubricant-free PTFE Trubore® glass and PTFE bearing for use with 8074
stainless steel or 8075 glass 10mm stirring shafts. Complete consists of PTFE inner
Trubore® bearing, Ace‑Thred glass adapter, non-flaking PTFE compression saddle with
Bushing 8066-12 o‑ring and glass-reinforced PTFE bushing and lock nut with FETFE o‑ring. The lock nut
Lock Nut 8066-13 permits stirring in either direction without fear of unthreading. The compression saddle
with o‑ring maintains constant force with little attention. Vacuum down to 1mm. Not
Compression Saddle
8066-15 With FETFE recommended for precision ground glass shafts. For replacement compression saddle
O‑Ring o‑ring, see 7855-718; for bearing o‑ring, see 7855-712.
FETFE O‑Ring 7855-712
Order Code Each
PTFE Inner Bearing PTFE Inner Bearing w/ FETFE O‑Ring, only 8066-06 31.08
8066-06 Glass Filled/PTFE Bushing, only 8066-12 30.46
Glass Filled/PTFE Lock Nut, only 8066-13 9.94
Thred Adapter
Compression Saddle w/ FETFE O‑Ring, only 8066-15 11.06
24/40 8066-20
29/42 8066-24
34/45 8066-28 Threaded Glass Adapter, only Complete Assembly
45/50 8066-32
E-SA 24/40 8066-20 29.21 24/40 8066-43 111.75
AC
FE
8066-43 29/42 8066-24 32.72 29/42 8066-46 115.26

34/45 8066-28 37.91 34/45 8066-50 120.45
ON
OR
C
N ECT 45/50 8066-32 51.91 45/50 8066-55 134.45

35/25 8066-33 34.43 35/25 8066-60 116.97

8066 BEARING/DEBRIS TRAP PTFE, Ace‑Thred,10mm
Combination all-in-one stirring shaft bearing and debris trap, designed to prevent particles
from entering reaction vessel. Lubricant free PTFE bearing with compression saddle o‑ring
makes a mechanical seal against a polished glass shaft. Debris trap section consists
of a PTFE washer and particle well. #7 Ace‑Thred on glass body side allows access
for clean out, or may be used for evacuation/gas purge port. Complete item supplied
with glass body, inner PTFE bearing, PTFE bushing and lock nut, Rulon saddle FETFE
o‑ring, “Ace-Safe” connector for 1/4‑inch tubing, and PTFE plug. Use with 8074 and
8075 10mm shafts.
Order Code Each 8066-320

PTFE Inner Bearing w/ FETFE O‑Ring, only 8066-08 44.46
Glass Filled/PTFE Bushing, only 8066-12 30.46
PTFE Washer 8066-03 28.78
PTFE Plug, #7 5846-44 22.15
“Ace-Safe” Connector, #7 x 1/4-inch 5853-06 13.53

E-SA
AC
FE
24/40 8066-220 106.83 24/40 8066-320 267.21
ON
OR
C
29/42 8066-224 109.53 29/42 8066-324 269.91 N ECT
34/45 8066-228 114.95 34/45 8066-328 275.33
45/50 8066-232 125.76 45/50 8066-332 286.14
35/25 8066-233 110.90 35/25 8066-333 271.28
Replacement FETFE o‑rings
FETFE, Size –014, Pk. 12 7855-712 12.93
NOTE: Glass Trap Body is also available without side port. Call or email for details.
8066 BEARING Trubore®, PTFE, Ace‑Thred,10mm

Self-aligning, lubricant-free PTFE Trubore® bearing for use with 8074 stainless steel or 8075
glass 10mm stirring shafts. Added side port hose connection allows purging flask contents with
a gas, or in airless work, allows for an inert gas blanket. Complete consists of PTFE inner
Trubore® bearing, Ace‑Thred glass adapter, non-flaking PTFE compression saddle with o‑ring,
and glass-reinforced PTFE bushing and lock nut with FETFE o-ring. The lock nut permits
stirring in either direction without fear of unthreading. The compression saddle with o‑ring
maintains constant force with little attention. Vacuum down to 1mm. Not recommended
for precision ground glass shafts. Use with 8074 and 8075 10mm shafts. For replacement 8066-130
compression saddle o-ring, order 7855-718; for bearing FETFE o-ring, order 7855-712.
Order Code Each

PTFE Inner Bearing w/ FETFE O‑Ring, only 8066-06 31.08
Side port hose
Glass Filled/PTFE Lock Nut, only 8066-13 9.94 connection

24/40 8066-70 39.50 24/40 8066-130 122.04
29/42 8066-71 42.98 29/42 8066-132 125.52 E-SA
AC
FE
34/45 8066-72 48.19 34/45 8066-134 130.73

45/50 8066-73 62.18 45/50 8066-136 144.72 ON
OR
C
35/25 8066-79 44.71 35/25 8066-140 127.25 N ECT

190 Stirrers

13445 BEARING Debris Free, PTFE, 1 0mm
wide range of joint and shaft diameter sizes. For use with 10mm polished glass or stainless
For Shaft Size, mm Joint Order Code Each

10 24/40 13445-30 173.35
10 29/42 13445-32 182.64
13445 10 34/45 13445-34 202.49
10 45/50 13445-36 204.60
Replacement Seals & Springs:

Order Code Each
PTFE/PEEK sleeve seal 13445-420 27.53
PEEK compression spring 13445-426 29.91
8068 STIRRING SHAFT Borosilicate, Precision Ground, 10mm

Precision ground glass stirring shafts, 10mm OD, paddled, button type and bead type.
Button type shafts accept 8083, 8085, 8086, 8087 and 8096 stir blades. Beaded shafts
accept 8088, 8089 and 8090 agitators. Use with Trubore® bearings 8036, 8038, 8039, 8040,
8042, 8043, 8047, 8051, 8053, 8050 and 13443. Join to motor using 8124 series chucks.
B
Lengths, mm
For Flask Order
Size, mL Ground Overall Code Each Description
250- 3000 420 440 8068-03 40.19 BUTTON TYPE, used with
A 3000- 5000 560 580 8068-02 42.86 any blade listed under 8083,
A 12000-22000 660 690 8068-04 44.97 8084, 8085, and 8086. For
bearings, see 8036, 8038,
50000 710 740 8068-06 48.00 8039, 8040, 8042, 8043, 8051
D or 8055.
B 250- 3000 420 440 8068-08 61.45 PADDLE TYPE, will fit through
45/50 joint on boiling flask.
250- 3000 360 440 8068-18 87.17 PADDLE TYPE, for large neck
D 3000- 5000 500 580 8068-17 89.77 boiling flask such as 71/60
or larger.
250- 3000 420 440 8068-25 67.23 HOLLOW TYPE, for material
F F 3000- 5000 560 580 8068-27 91.49 introduction. Use with 8053
bearing.
G 250- 3000 420 440 8068-30 53.04 BEAD TYPE, for use with
G 3000- 5000 560 580 8068-32 54.62 8088, 8089 and 8090 PTFE
12000-22000 660 690 8068-31 59.13 Agitators.
Stirrers 191

8070 STIRRING SHAFT PTFE-Coated Glass, 1 0mm
Precision ground glass stirring shafts, 10mm O.D., button type, PTFE coating permits 8070
higher stirring speeds with Trubore® bearings. If used unlubricated, 500 rpm max with
water-cooled 8040 bearing. Compatible with 8036, 8038, 8039, 8043, 8047, 8051, 8055
and 13443 bearings. Button type shafts accept 8083, 8085, 8086, 8087 and 8096 stir
blades. Join to stirrer motor using 8124 series chucks.

250- 5000 440 8070-05 75.72
12000-22000 690 8070-10 83.86
8071 STIRRING SHAFT PTFE-Coated Steel, 10mm

PTFE covered stainless steel stirring shafts, 10mm O.D., drilled type. If used unlubricated,
500 rpm max with water cooled 8040 bearing, 100 rpm maximum recommended with
8036, 8038, 8039, 8043, 8047, 8051 and 8055 bearings. With condensate film as added
heat transfer agent, 2000 rpm can be attained. Drilled type shaft accepts 8088, 8089
and 8090 agitators. Compatible with our 13443 collet-type bearing. Join to stirrer motor
using 8124 series chucks.

250- 5000 460 8071-05 207.66
12000-22000 640 8071-07 264.62
8071
12000-22000 690 8071-10 267.94
13443 STIRRER BEARING PTFE, 8, & 10mm

Inert PTFE Stirrer bearing. Features a totally enclosed bearing body for non-shedding, 13443
anti-whip, chemically resistant design. The bearing can also be used in slight vacuum or
slight pressure applications. The design has a composite PTFE/PEEK main internal seal
and a specially fabricated glass ball-bearing for rigidity and smoothness during lengthy
operation. Max recommended speeds up to 500 rpm continuous operation. Ideal for
glass, metal or PTFE stir shafts. Bottom is a molded, inner standard taper joint. Average
length is 96mm and 45mm O.D. at bearing center.

8 24/40 13443-10 428.93
10 24/40 13443-12 428.93

192 Stirrers

13850 AGITATOR, STIRRING SHAFT PTFE, 1 0mm
13850 Chemically resistant, PTFE, three bladed, retreat curve stir shaft. Fully molded bottom blade
is designed with a 30º retreat angle. 10mm shaft is PTFE encapsulated stainless steel.
Blade
Shaft O.D., mm Length, mm Height, mm O.D., mm Order Code Each
10 400 10 50 13850-01 309.15
New 10 400 10 70 13850-04 335.81
New 13852 AGITATOR, STIRRING SHAFT PTFE, 1 0mm

Chemically inert, four bladed, screw propeller design, PTFE stir shaft. The 10mm O.D.,
steel reinforced shaft has approximately 50mm exposed for easier/better connection to
the stir motor chuck.
Blade O.D.,
Shaft O.D., mm Length, mm mm Order Code Each
10 400 50 13852-10 335.81
10 400 70 13852-15 335.81
13852
Stirrers 193

8073 STIRRING SHAFT “C” Type, Borosilicate, 1 0mm
Precision ground glass stirring shafts,10mm O.D., crescent type. Useful for stirring viscous
materials at low rpm. Available for round bottom flasks of 1, 3 and 5 liters. Code -19,
three liter size will fit a two liter flask, but closely. Flask opening must be 29/42 or larger.
Use with Trubore® bearings 8036, 8038, 8039, 8040, 8043, 8047, 8051, 8053 and 8055.
Compatible with our 8050 PTFE mechanical seal and 13443 PTFE collet type bearings.
For Flask Cap., mL Order Code Each

1000 8073-16 63.11
3000 8073-19 63.11
5000 8073-23 63.11
8073
8074 STIRRING SHAFT Stainless Steel, 1 0mm

Polished stainless steel stirring shafts, 10mm O.D., drilled type with removable button.
When used with 8066 PTFE bearing, a lubricant-free vacuum seal can be realized at
speeds up to 200 rpm. Recommended for use with 8044, 8050, 8066, 13443 and 13445 8074
bearings. With button, shaft accepts 8083, 8085, 8086, 8087 and 8096 stir blades. With
button removed, shaft will accept 8094 and 8095 agitators secured with a set-screw
anywhere along its ground flat section. Join to stirrer motor using 8124 series chucks.
For Flask Lengths, mm
Cap., mL Flat Section Overall Order Code Each
250- 1000 100 420 8074-02 139.98
2000- 5000 200 450 8074-04 146.25
5000-12000 280 580 8074-07 150.06
Replacement Buttons:
Order Code Each
8074-40 248.02

194 Stirrers

8075 STIRRING SHAFT Borosilicate, Polished, 10mm
Polished glass stirring shafts, 10mm O.D. Only recommended for use with our 8050,
8075 8066, 13443 and 13445 bearings. Join 8083, 8085, 8086, 8087 & 8096 blades to button
type shafts. Join 8088, 8089 and 8090 agitators to beaded shafts. Plain shafts will ac-
cept 8094 and 8095 agitators secured with a set-screw anywhere along its ground flat
section. Join to stirrer motor using 8124 series chucks.
For Flask Cap., mL Type Length, mm Order Code Each

250- 3000 With Button 440 8075-12 55.65
3000- 5000 With Button 580 8075-14 57.59
12000-22000 With Button 690 8075-15 60.15
250- 3000 Plain, w/o Button 440 8075-21 47.14
3000- 5000 Plain, w/o Button 580 8075-23 49.17
12000-22000 Plain, w/o Button 690 8075-24 51.16
250- 3000 With Bead/Knob 440 8075-32 57.11
3000- 5000 With Bead/Knob 580 8075-34 60.33
12000-22000 With Bead/Knob 690 8075-36 65.83
Knob Button
Plain
9532 STIRRING SHAFT Hollow, Borosilicate, 10mm

Precision ground glass stirring shaft with attached vanes, 10mm. For use when agitation
and gas introduction are desired at the same time. Agitator will fit through a  45/50 joint.
Designed for use with our 9523 Trubore® bearing and 9443 or 9446 mini-lab flask heads.
9532 Introduced gas exits the hollow shaft within the agitator and produces a fine dispersion.
Join to stirrer motor with 8124 series chucks.
Order Code Each

9532-10 140.16
9533 STIRRING SHAFT Borosilicate, Ground, 10mm

Precision ground glass stirring shaft, 10mm OD, attached vanes. Vanes will fit through a
 45/50 joint and are contoured for use with our 9448 and 9456 series Mini-Lab flasks.
Use with Trubore® bearings 8036, 8038, 8039, 8040, 8042, 8043, 8047, 8051, 8053 and
9533 8055. Compatible with our 8050 mechanical seal and 13443 PTFE collet type bearings.
Order Code Each

9533-02 85.70
Stirrers 195

8082 STIRRER BLADES PTFE, Oval, 10mm
PTFE oval stir blades for 10mm O.D. button type stir shafts. 10mm O.D. shafts can be
found in our 8068, 8070, 8074 and 8075 series.
Width, mm Length, mm Flask Cap., mL Order Code Each

19 40 100- 500 8082-02 8.39
19 60 250- 500 8082-04 10.03 8082
24 80 1000-2000 8082-06 12.60
24 115 2000-3000 8082-08 14.04
8083 STIRRER BLADES Borosilicate Glass, 10mm

Glass stir blades for 10mm O.D. button type stir shafts. 10mm O.D. stir shafts can be
found in our 8068, 8070, 8074 and 8075 series.

19 48 100- 500 8083-04 9.16
19 60 250- 500 8083-08 9.25
19 76 500- 1000 8083-12 29.92
8083
23 113 2000- 3000 8083-16 30.06
24 134 5000-12000 8083-20 31.78
24 160 22000-72000 8083-24 31.95
8085 STIRRER BLADES PTFE, 10mm

PTFE stir blades for button type stir shafts. 10mm O.D. shafts can be found in our
product series 8068, 8070, 8074 and 8075. 19mm O.D. shafts can be found in our 8076
and 8077 series.

19 48 100- 500 8085-03 9.69
19 60 250- 500 8085-07 10.53 8085
19 76 500- 1000 8085-11 12.36
23 113 2000- 3000 8085-15 16.25
24 130 5000-12000 8085-19 21.17
24 160 22000-72000 8085-23 26.51
8086 STIRRER BLADES Stainless Steel, 10mm

304 stainless steel stir blades for 10mm O.D. button type stir shafts. 10mm O.D. stir
shafts can be found in our 8068, 8070, 8074 and 8075 series.

19 76 500- 1000 8086-04 31.06 8086
23 113 2000- 3000 8086-08 30.82
24 134 5000-12000 8086-12 36.19
24 160 22000-72000 8086-16 39.46
8126 STIRRING SHAFT Pass-through Assembly, 10mm

Item includes the 8126-10 stir shaft coupling with pin that is attached to 7mm O.D. 8126-24
stainless steel drive shaft. Shaft that is 305mm long and fits up through the chuck and
opening in the Heidolph RZR model and Caframo BDC model overhead stir motors and
allows for adjusting the height of the entire stir shaft assembly. For 10mm stir shafts.
Order Code Each

8126-24 75.13

196 Stirrers

8096 STIRRER BLADES Stainless Steel, 10mm
316 stainless steel, football shaped, stir blades for 10mm O.D. button type stir shafts.
Holed versions, codes -70 thru -74, provide even greater agitation. 10mm O.D. stir shafts
can be found in our 8068, 8070, 8074 and 8075 series.
Without holes
8096-06 Width, mm Length, mm Order Code Each

19 40 8096-04 31.43
24 80 8096-06 32.42
24 115 8096-10 37.65
8096-72 With holes
Width, mm Length, mm Order Code Each
19 60 8096-70 36.01
24 80 8096-72 36.66
24 115 8096-74 41.91
8087 STIRRER BLADES Banana Type, PTFE, 10mm

PTFE banana shaped stir blades for 10mm O.D. button type stir shafts. 3mm thick blades
have a number of perforations and are designed to closely fit various sizes of round bottom
flasks. 10mm O.D. stir shafts can be found in our 8068, 8070, 8074 and 8075 series.
For Flask Width, Lgth., Order For Flask Width, Lgth., Order
Cap., mL mm mm Code Each Cap., mL mm mm Code Each
500 21 87 8087-05 26.39 5000 35 175 8087-13 49.01
8087 1000 23 109 8087-07 31.94 12000 37 222 8087-15 51.67
2000 31 146 8087-09 34.59 22000 40 263 8087-19 72.10
3000 31 157 8087-11 41.36
8088 AGITATOR PTFE, Single Blade Type, 10mm

PTFE agitator with removable blade secured with a PTFE pin. Supplied 76mm long blade
8088 will fit through a  29/42 joint. Fits 10mm O.D. drilled type or beaded type 8068, 8071
and 8075 shafts.
Complete Replacement Blade

8088-10 222.39 8088-03 33.93
8089 AGITATOR PTFE, Multi-Paddle, 10mm

PTFE multi-paddle agitator for 10mm O.D. drilled or knob type shafts. Paddles are
8089 replaceable. Fits 10mm O.D. drilled or knob type 8068, 8071 and 8079 shafts.
Complete Blades, Only

Size, mm Order Code Each Order Code Each
38 8089-04 104.10 8089-14 18.50
64 8089-06 111.43 8089-16 24.15
76 8089-08 112.73 8089-18 26.33
Stirrers 197

8090 AGITATOR PTFE, Turbine, 10mm 8090
All-PTFE, turbine type agitator. Unique locking arrangement assures positive grip. Agitator
fits 10mm shafts. Shaft opening is drilled straight through to allow positioning of agitator
at any height on shaft as well as at the bottom. For use with glass stirring shaft, 8068,
8075 or PTFE shaft, 8071.
Blade Size, mm Order Code Each

38 8090-04 138.47
64 8090-08 151.38
8094 AGITATOR 316 Stainless Steel, Multi-Paddle, 10mm

For use with 8074 stainless steel shaft or 8075 borosilicate straight shaft. Center hole
is 10mm I.D. and one or more can be positioned on shaft at various locations using
set screws to secure. With stainless shaft use stainless set screw; with glass shaft use
Kel-F-tipped set screw. Both screws supplied with agitator.
Size,
mm Order Code Each Replacement set screws:
75 8094-23 193.83 Order Code Each
89 8094-27 205.47 8094
Stainless 8094-50 4.45
Stainless/Kel-F 8094-52 6.84
8095 AGITATOR 316 Stainless Steel, Turbine, 10mm

10mm steel agitator with multiple fins which may be bent, with care, to different angles.
See 8094 listing, above, for replacement set screws.
Size, mm Order Code Each

75 8095-31 204.88 8095
89 8095-35 218.88
8113 ADAPTER Lubricant Trap, High Vacuum, 10mm

Primarily designed for use with ACE 8051 bearings. The inner tube through which the
stirring shaft passes, plus the PTFE o‑ring supplied with each unit, prevents the lubricant
or foreign particles from contaminating the flask contents. For replacement PTFE ring, 8113
order 8113-89.
Top Joint Bottom Joint Order Code Each

24/40 24/40 8113-10 73.58
29/42 29/42 8113-20 76.73
29/42 34/45 8113-25 85.03
8124 CHUCK “Flex-Grip,” 10mm

Top has set screw for coupling to stir motor shaft. 8124
10 8 (5/16) 8124-10 43.92
10 9.5 (3/8) 8124-12 43.92
10 13 8124-13 43.92
Insert Only Size, mm Qty. Order Code Per Package

10 6 8124-25 17.04


8059 Trubore® 19mm I.D., stirrer bearing with standard taper joint bottom. Jacketed for water
cooling. Designed for use with 19mm O.D. 8077 and 8078 precision ground glass shafts
and 8079 PTFE shafts with stainless steel core. Hose connections are size D for use
with 3/8‑inch I.D. tubing.

45/50 8059-05 229.99
55/50 8059-09 234.51

Trubore® 19mm I.D., glass stirrer bearing with bottom spherical ground joint. Joint can
be clamped to prevent rotation. Length is 15.2cm (6 inches). Designed to accommodate
ACE 8112-10 packing box which sits directly into the top of the bearing. Designed for
use with 19mm O.D. 8077 and 8078 precision ground glass shafts and 8079 PTFE shafts
8060 with stainless steel core. Hose connections are size D for use with 3/8‑inch I.D. tubing.

65/40 8060-10 299.67
8061 BEARING Trubore®, Heavy Duty, 19mm

Heavy duty, 19mm I.D., Trubore® stir bearing with bottom standard taper joint. Designed
8061 to accommodate ACE 8112-10 packing box which sits directly into the top of the bearing.
Designed for use with 19mm O.D. 8077 and 8078 precision ground glass shafts and 8079
PTFE shafts with stainless steel core. Length is 20.3 cm (8 inches). Heavy duty style for
use with larger capacity flasks.

45/50 8061-04 178.71
8065 BEARING Trubore®, Glass, Heavy Duty, 19mm

8065 Trubore®, self aligning, heavy duty three piece bearing. Complete consists of inner 19mm
I.D. Trubore® bearing, compression seal nylon busing, with FETFE o-ring and #25 Ace‑Thred
adapter with standard taper, ground joint bottom. Design allows for slight misalignment
of stir motor and the bearing without breaking or shaft seizing, as the inner bearing will
spin. Designed for use with 19mm O.D. 8077 and 8078 precision ground glass shafts and
8079 PTFE shafts with stainless steel core. Heavy duty style for use with larger capacity
flasks. For replacement size –212 FETFE o‑ring, see 7855-734.
T
S 34/45 Bottom Joints T
S 45/50 Bottom Joints
E-SA Order Code Each Order Code Each
AC
FE
Inner Bearing, only 8065-06 66.43 8065-06 66.43

ON Bushing with O‑Ring 8065-10 40.49 8065-10 40.49
OR
C
N ECT #25 Ace‑Thred Adapter, only 8065-14 59.23 8065-16 62.67

Complete 8065-60 166.15 8065-64 169.59

8067 BEARING Trubore®, PTFE, Ace‑Thred, 19mm E-SA
AC
Self-aligning, lubricant-free PTFE Trubore® bearing for use with 8076, 19mm polished glass
FE
stirring shaft. Complete consists of PTFE inner Trubore® bearing, #25 Ace‑Thred glass adapter,
ON
OR
C
non-flaking PTFE compression saddle with o‑ring and glass-reinforced PTFE bushing and N ECT
lock nut with FETFE o‑ring. The lock nut permits stirring in either direction without fear of
unthreading. The compression saddle with FETFE o‑ring maintains constant force with little Bushing 8067-08
attention. Vacuum down to 1mm of Hg. Not recommended for precision ground glass shafts. Lock Nut 8067-11
For replacement “saddle” o‑ring, order 7855-730; for bearing FETFE o‑ring, order 7855-734.
Compression
Saddle 8067-13
Order Code Each With FETFE O‑Ring
PTFE Inner Bearing w/O‑Ring, only 8067-05 83.40
FETFE O‑Ring
Glass Filled/PTFE Bushing, only 8067-08 45.97 7855-734
PTFE Inner Bearing
Saddle O‑Ring, only 8067-13 16.49 8067-05
#25 Ace‑Thred Glass Adapter, only Complete Assembly Thread Adapter

Bottom 45/50 8067-18
Joint Order Code Each Joint Order Code Each 55/50 8067-20
45/50 8067-18 106.40 45/50 8067-30 269.05 71/60 8067-22
55/50 8067-20 102.13 55/50 8067-34 264.78
71/60 8067-22 112.06 71/60 8067-38 274.71
8067-30
8067 BEARING/DEBRIS TRAP PTFE, Ace‑Thred,19mm

Combination all-in-one stirring shaft bearing and debris trap. Designed to prevent E-SA
AC
FE
particles from entering the reaction vessel. Lubricant-free PTFE bearing with compression
saddle o‑ring makes a mechanical seal against 8076 polished glass shaft. Debris trap ON
OR
C
section consists of a PTFE washer and particle well. #11 Ace‑Thred on glass body side N ECT
allows access for clean-out, or may be used for evacuation/gas purge port. Complete
item supplied with glass body, inner PTFE bearing, PTFE bushing and lock nut, Rulon
saddle with FETFE o‑ring, “Ace-Safe” connector for 3/8‑inch tubing, and PTFE plug.
Order Code Each

Compression Saddle w/O‑Ring, only 8067-13 16.49
PTFE Washer 8067-09 33.16
PTFE Plug, #11 5846-46 32.14
8067-54
#25 Ace‑Thred Glass Adapter, only Complete Assembly
Bottom Bottom NOTE: Glass trap body
Joint Order Code Each Joint Order Code Each is available without side
45/50 8067-45 148.02 45/50 8067-54 392.92 port. Call or e-mail for
55/50 8067-47 162.68 55/50 8067-57 407.58 details.
71/60 8067-49 179.22 71/60 8067-59 424.12

200 Stirrers

8076 STIRRING SHAFT Borosilicate, Polished, 19mm
Polished glass stirring shafts, 19mm O.D. Available in solid and hollow styles and in
various lengths. Join 8085 blades to button type shafts, Join 8091, 8092, 8093 and 8100
agitators to either knob or drilled style shafts. Join all shafts to stirrer motor using 8124
8076-05 series chucks. Recommended for use with our 8050 mechanical seal, 8067 PTFE and
Button 13445 PTFE debris-free bearings.
For Flask Length, mm
Cap., Liters (Inches) Bottom Style Order Code Each
22 700 (28) Button 8076-05 190.01
22 900 (36) Button 8076-07 191.42
50-72 1,200 (48) Button 8076-10 192.26
8076 STIRRING SHAFT Borosilicate, Polished,19mm

19mm O.D. polished stirring shaft. Can be used with 8050, 8059, 8060, 8061, 8065, 8067,
or 13445 bearings and 8091, 8092 or 8093 agitators. Fits 8124 chuck.
For Flask Length, mm Order
Cap., Liters Type Shaft (Inches) Bottom Style Code Each
8076-40, 10 Hollow 800 (32) Knobed Bottom 8076-42 211.14
-43, -45, -48 10 Solid 800 (32) Drilled Holes 8076-43 240.03
8076-42, Drilled 20 Solid 900 (36) Drilled Holes 8076-40 248.02
-44, -46 30 Hollow 1,200 (48) Knobed Bottom 8076-44 211.14
Knobed 50 Solid 1,140 (45) Drilled Holes 8076-45 290.38
50 Hollow 1,400 (54.5) Knobed Bottom 8076-46 294.62
50 Solid 1,400 (54.5) Drilled Holes 8076-48 306.64
8077 STIRRING SHAFT Precision-Ground, Borosilicate, 19mm

19mm O.D. button type, hollow shaft for use with all 19mm I.D. ACE Trubore® bearings,
8059, 8060, 8061 or 8065. Also compatible with 8050 mechanical seal and 13445 PTFE
bearings. Fits 8124 or 8126 chucks. Ground surface approximately 380mm long. For
stir blades, see 8085.
8077 For Flask
Cap., Liters Length, mm (Inches) Order Code Each
22 700 (28) 8077-23 113.52
22 900 (36) 8077-25 127.93
50-72 1,200 (48) 8077-27 122.22
Stirrers 201

13852 STIRRING SHAFT PTFE, 19mm New
Chemically inert, four bladed, screw propeller design, PTFE stir shaft. The 19mm O.D.,
steel reinforced shaft has approximately 50mm exposed for easier/better connection to
the stir motor chuck.
Blade O.D.,
Shaft O.D., mm Length, mm mm Order Code
19 900 95 13852-19 522.36
13852
8126 STIRRING SHAFT Pass-through Assembly, 19mm

Item includes the 8126-19 stir shaft coupling with pin that is attached to 7mm O.D.
stainless steel drive shaft. Shaft that is 305mm long and fits up through the chuck and
opening in the Heidolph RZR model and Caframo BDC model overhead stir motors and
allows for adjusting the height of the entire stir shaft assembly. For 19mm stir shafts.
Order Code Each

8126-22
8126-22 276.11
8078 STIRRING SHAFT Precision-Ground, Heavy Duty, 1 9mm

Precision ground glass stirring shafts, 19mm O.D., hollow, heavy duty. Knob type shafts
accept 8091,8092,8093,8100 agitators and can be used in all 19mm I.D. Trubore® 8059,
8060, 8061 and 8065 bearings. Compatible with our 8050 mechanical seal and 13445
PTFE debris-free bearings. Join to stirrer motor using 8124 series chucks. Heavy duty
design intended for use with large flasks up to 72 liters. 8078
For Flask Length, mm
Cap., Liters (Inches) Order Code Each
22 900 (36) 8078-05 178.44
50-72 1,200 (48) 8078-10 194.12

202 Stirrers

8079 STIRRING SHAFT Precision, PTFE, Heavy Duty, 19mm
Precision PTFE covered stainless steel stirring shafts, 19mm O.D. Drilled type shafts
accept 8091, 8092, 8093, 8100 agitators and can be used in 19mm Trubore® bearings
(8059, 8060, 8061 & 8065). Not recommended for PTFE bearings 8050, 8067 and 13445.
For Flask
Cap., Liters Length, mm (Inches) Order Code Each
8079 22 700 (29) 8079-03 477.57
22 900 (36) 8079-05 484.69
50-72 1,200 (48) 8079-10 528.19
8085 STIRRER BLADE PTFE, 19mm

PTFE stir blades for button type stir shafts. 10mm O.D. shafts can be found in our
product series 8068, 8070, 8074 and 8075. 19mm O.D. shafts can be found in our 8076
and 8077 series.
Width, mm Length, mm Order Code Each

35 150 8085-52 62.91
8085-52
39 160 8085-54 81.66
44 175 8085-56 91.30
54 190 8085-58 94.72
8091 AGITATOR PTFE, Multi-Paddle, 19mm

PTFE agitators for use with large-scale reactors with 6-inch, 8-inch or 12-inch flanges.
8091-10 These heavy-duty agitators impart maximum energy and are offset at bottom to
accomodate slurries. 19mm agitators fit drilled type or knob type 8076, 8078 & 8079
shafts. 28mm agitators fit 8080 shafts.
Replacement Blades
102 8091-10 226.34 8091-14 45.75
152 8091-20 245.80 8091-15 50.33
Stirrers 203

8091 AGITATOR PTFE, Large Scale, Multi-Paddle, 19mm
PTFE agitators for use with large-scale reactors with 6-inch, 8-inch or 12-inch flanges.
These heavy-duty agitators impart maximum energy and are offset at bottom to
8091-40
accomodate slurries. 19mm agitators fit drilled type or knob type 8076, 8078 & 8079
shafts. 28mm agitators fit 8080 shafts.
Size, mm Replacement Blades

(Inches) Order Code Each Order Code Each
140 (5.5) 8091-26 318.61 8091-28 68.53
203 (8) 8091-40 352.23 8091-44 101.81
8100 AGITATOR PTFE, Multi-Paddle with Receptacle, 19mm

PTFE, large-scale, multi-paddle agitator design to accept pinned bottom valves, like
our 6482 flush-seal valve. The pin helps reduce wobble or flexing at higher rpm. 19mm 8100
agitators will fit drilled type or knob type 8076, 8078 and 8079 shafts. New
Size, mm Order Code Each
140 8100-09 369.95
200 8100-19 854.95
8092 AGITATOR PTFE, Single Blade, 19mm

PTFE bottom agitator, with single 152mm length, removable blade. Agitator body is
secured to 19mm shaft by removable PTFE “pin”. Top forked tines are then secured
with threaded PTFE nut. Blade will fit through a 45/50 joint opening. Fits 8076, 8078
and 8079 drilled or knob-type 19mm shafts.
8092
Complete Replacement Blade
8092-10 256.36 8092-14 32.82
8093 AGITATOR PTFE, Turbine, 19mm

A 102mm or 152mm total diameter agitator for 19mm O.D. 8076, 8078 or 8079 drilled
or knob-type shafts. Turbine blade unit is removable. Shaft opening is open straight
through to allow positioning of agitator at any height on shaft. NOT supplied with shaft.
Complete Replacement Blades
102 8093-12 186.56 8093-15 53.93
152 8093-22 430.35 8093-16 94.66
8093

204 Stirrers

8124 CHUCK “Flex-Grip,” 19mm
8124
19 8 (5/16) 8124-15 152.25
19 9.5 (3/8) 8124-17 152.25
19 12.7 (1/2) 8124-20 152.25
19 13 8124-22 152.25
19 15.9 (5/8) 8124-23 152.25
Insert Only Size Qty. Order Code Per Package

19 mm Pkg/3 8124-30 21.21
8050 STIRRER BEARING Mechanical Seal, PTFE, 19mm

Newly designed mechanical stirrer bearing from ACE. All PTFE, Rulon or PEEK wetted
8050 area construction provides for low extractables. Completely contained bearing and
excellent for vacuum applications and can be operated at sub-Torr levels. Rated for up
to 400 rpm speeds. It can be used on either glass polished or stainless steel stir shafts.
Shaft Size, mm Joint Size Order Code Each

19 45/50 8050-06 601.93
Replacement Outside size –128 o‑ring 7855-773 19.41
New
13445 BEARING Debris Free, PTFE, 1 9mm

wide range of joint and shaft diameter sizes. For use with 19mm polished glass or stainless

19 45/50 13445-46 329.01
13445 Replacement Seals & Springs:

Order Code Each
PTFE/PEEK sleeve seal, for 19 mm 13445-504 45.92
PEEK compression spring, for 19mm 13445-506 54.78
SS I N N OV
LA
AT
TH
AC E
I ON
28mm Shafts, Bearings & Agitators A N N I V E R S A R Y
1936 2011
NJ
VI
N ,
8050 STIRRER BEARING Mechanical Seal, PTFE EL
A ND
Newly designed mechanical stirrer bearing from Ace. All PTFE, Rulon or PEEK wetted
area construction provides for low extractables. Completely contained bearing and 8050
excellent for vacuum applications and can be operated at sub-torr levels. Rated for up
to 400 rpm speeds. It can be used on either glass polished or stainless steel stir shafts.
The 25.4mm size fits Chemglass size shafts.
Shaft Size, mm Joint Size Order Code Each

28 45/50 8050-08 667.58
25.4 45/50 8050-16 661.28
30 45/50 8050-18 661.28 New
Replacement Outside size –128 o‑ring, Pkg. 6 7855-773 19.41
8067 BEARING Trubore®, PTFE, Ace‑Thred, 28mm

8067-105
Self-aligning, lubricant-free PTFE Trubore® bearing for use with 8080, 28mm polished
glass stirring shaft. Complete consists of PTFE inner Trubore® bearing, Ace‑Thred glass Bushing 8067-58
adapter (#36 to  45/50), PTFE compression saddle with o‑ring and glass-reinforced PTFE Lock Nut 8067-60
bushing, and lock nut with FETFE o‑ring. The lock nut permits stirring in either direction
without fear of unthreading. The compression saddle with o‑ring maintains constant force Compression
with little attention. Vacuum down to 1mm Hg. Not recommended for precision ground Saddle 8067-65
glass shafts. For replacement “saddle” o‑ring, see 7855-739; for bearing size –217 FETFE With FETFE O‑Ring
o‑ring, see 7855-740. FETFE O‑Ring
7855-740
Order Code Each PTFE Inner Bearing
8067-55
Glass Filled/PTFE Lock Nut, only 8067-60 21.59 Thread Adapter
45/50 5030-78
Compression Saddle w/O‑Ring, only 8067-65 30.45
Threaded Glass Adapter, 45/50, only 5030-78 77.88
E-SA
Complete 8067-105 320.08
AC
FE
ON
OR
C
N ECT
8067 BEARING/DEBRIS TRAP PTFE, Ace‑Thred, 28mm

Combination all-in-one stirring shaft bearing and debris trap. Designed to prevent
particles from entering the reaction vessel. Lubricant free PTFE bearing with compression
saddle o‑ring makes a mechanical seal against an 8080 polished glass shaft. Debris 8067-80
trap section consists of a PTFE washer and particle well. #15 Ace‑Thred on glass
body side allows access for clean-out, or may be used for evacuation/gas purge port.
Complete item supplied with glass body, inner PTFE bearing, PTFE bushing and lock E-SA
nut, Rulon saddle o‑ring, “Ace-Safe” connector for 3/8-inch tubing, and PTFE plug.
AC
FE
 45/50 bottom joint. For replacement “saddle” o‑ring, see 7855-739; for bearing size
ON
OR
C
–217 FETFE o‑ring, see 7855-740. N ECT
Order Code Each

PTFE Inner Bearing w/O‑Ring, only 8067-70 102.42 NOTE:
Glass Filled/PTFE Bushing, only 8067-58 75.44 Glass Trap Body
Glass Filled/PTFE Lock Nut, only 8067-60 21.59 is available with-
Compression Saddle w/O‑Ring, only 8067-65 30.45 out side port. Call
PTFE Washer 8067-72 43.69 or e-mail for
PTFE Plug, #15 5846-48 38.41 details.
Glass Trap Body, only, 45/50 8067-75 193.24
Complete 8067-80 529.60

206 Stirrers
28mm Rods, Bearings & Agitators

8080 STIRRING SHAFT Polished, Heavy Duty, 28mm
Heavy duty, 28mm O.D. glass stirring shaft for use with ACE 6472, 6473 and 6474 reactors.
8080
Shaft has pre-drilled holes at top and bottom for positive attachment to motor coupling
and agitator, respectively. Recommended for use with 8067 PTFE Trubore® and 8050
mechanical seal bearings. Use with 8091, 8093, 8101 agitators for 28mm rods. Fits ACE
Upper hole 6472-155 swivel connector and 6472-157 chuck.
for turbine
agitator located For Flask Capacity Length, mm (Inches) Order Code Each
8 inches from 30L Cylindrical 1,140 (45) 8080-14 402.64
bottom.
50L Low Profile 1,010 (40) 8080-12 378.55
50L Cylindrical 1,320 (52) 8080-18 446.02
72L & 100L Spherical 1,140 (45) 8080-14 402.64
100L Cylindrical 1,470 (58) 8080-22 472.33
100L Cylindrical 1,600 (63) 8080-30 586.44
Position can 200L Spherical 1,400 (55) 8080-24 458.41
be changed 8 inches 200L Cylindrical 2,030 (80) 8080-25 634.97
to meet your
specifications.
6472 CONNECTOR Flexible Beam with Pin

Coated steel flex-beam connector, for attaching directly to stir motor drive shaft. Fits
three different standard motor shaft, sizes, (top). Comes with ½-in stainless steel pin,
(bottom) that attaches to top of 6472-157, 28mm nylon chuck.
Motor Shaft
Size, in. (mm) Order Code Each
6472-159 1/2 (12.7) 6472-155 55.71
5/8 (15.9) 6472-156 54.09
3/8 (9.5) 6472-159 55.71
6472 CHUCK for 28mm Stir Shaft

6472-157 Nylon chuck with nylon side pin for connecting to a 28mm glass stir shaft, (8080) to the
6472-155, -156 or -159 flex beam connectors or a 6462 telescoping chuck coupling. Top
hole fits onto 1/2-inch steel pin on 6472 flex beam or 6462 telescoping couplings.
Nylon Chuck Replacement Nylon Side Pin

6472-157 89.89 6472-158 13.58
Stirrers 207

8091 AGITATOR PTFE, Large Scale, Multi-Paddle, 28mm
A four-blade, multipaddle agitator, used at lower end of 8080, 28mm stirring shaft.
Supplied with PTFE bolt and nut for securing to 8080 shaft to prevent detachment during 8091-34, -36
operation. Blades on code -34 are 140mm (5.5 inches) long; on code -36 they are 178mm
(7 inches) long x 6.35mm (.25‑inch) thick. The increased length and depth of the blades
imparts more energy to the load. NOT supplied with shaft.
Complete Replacement Nut & Bolt

For Flask Capacity Order Code Each Order Code Each
72L & 100L Spherical 8091-34 616.11
200L Spherical; 30L, 8091-134 61.29
50L, 100L & 200L 8091-36 613.84
Cylindrical
8093 AGITATOR PTFE, Large Scale, Turbine, 28mm

A four-blade, 45-degree-pitch, turbine-type agitator, used at upper section of 8080,
28mm stirring shaft. Supplied with PTFE bolt and nut for securing to 8080 shaft to
prevent detachment during operation. Blades on code -25 are 140mm (5.5 inches) long,
overall; on code -35 they are 152mm (6 inches) long, overall x 6.35mm (.25-inch) thick.
The increased length and depth of the blades imparts more energy to the load. NOT
supplied with shaft.

For Flask Capacity Order Code Each Order Code Each
100L Spherical 8093-25 583.27
100L & 200L Spherical; 8093-25, -35
8093-125 59.17
30L, 50L, 100L & 200L 8093-35 628.06
Cylindrical
8101 AGITATOR PTFE, Multi-Paddle with Receptacle, 28mm

PTFE bottom agitator for large reactors. Multi-paddle solid assembly fits 8080, 28mm
glass shafts. Agitator is attached to the shaft by a PTFE bolt. The bottom of the center
piece is bored out to receive the pin from the 6482 flush seal valve. This agitator when New 8101
coupled to the 6482 valve greatly reduces flexing or wobble from the shaft. Each blade on
-28 is 180mm full length. Blades on –38 are 203mm overall length. Order shaft separately.

180 8101-28 583.27
8093-125 59.17
203 8101-38 628.06

Trubore® Stirrer Accessories

Use the ACE flexible shaft for added convenience and safety
• Safer when stirring corrosive liquids Safety and
convenience
• Safer when stirring liquids with explosive vapor at your
• Available in two lengths fingertips! Flexible Shaft
8081
ADAPTER (G) 8081 FLEXIBLE SHAFT

Fully flexible drive shaft connects the motor to any
MOTOR size or type of reactor stir shaft. Designed with a ball
COUPLING (C)
bearing motor coupling at one end, for connection to
any motor with an 8mm (5/16-inch) diameter shaft.
HANDPIECE (B)
The other end has a detachable handpiece with
an 8mm round aluminum pin adapter (8081‑24) for
connection to our 8124 chucks (supplied separately). Chuck
The handpiece can be supported by a standard
lab clamp or hand held. The shafts operate up to
FLEXIBLE SHAFT (A) 14,000 rpm. Shafts should run in a counter-clockwise
direction. Typical torque ratings: sharp bend in shaft,
(4‑inch loop) — 4.7 Kg‑cm, (4 in-lbs). Straight shaft —
28 Kg‑cm, (24 in-lbs). Shafts measure approximately
91.4 cm, (36 inches) or 152.4 cm, (60 inches) with
handpiece and motor coupling attached. Optional
adapter 8081-27 allows for connection to motors
with 9.5mm (3/8-inch) O. D. shaft. Operating and lubrication instructions included.
Complete units consist of: either shaft A -8081-05 or shaft A-1, 8081-06, motor
coupling for 8mm motor shaft, 8081-12, handpiece with 1/4-inch collett and adapter,
chuck wrench, and key chain.
Order
Code Each
8124 CHUCK “Flex-Grip,” Light Weight (A) Flexible shaft only, 91.4cm 8081-05 46.58
Nylon chuck for use with 8081 flexible shaft and with (A-1) Flexible shaft only, 152.4cm 8081-06 87.61
stirring shafts or other shafts of approximately the same (B) Handpiece with 8mm adapter (G), with 1/8-inch 8081-08 115.42
dimensions. Chuck has flexible insert that allows for and 1/4-inch collet, only
misalignment of stirring shaft without danger of breakage. (B-1) Handpiece with chuck wrench with key and 8081-07 101.21
Fits standard 5/16-inch motor shaft or flexible shaft. chain (E), only
(C) Motor coupling for 8mm shaft, only 8081-12 21.96
Order
Complete, 91.4cm (consists of A, B, C & E) 8081-30 187.03
Size Code Each
Complete, 152.4cm (consists of A-1, B, C & E) 8081-32 228.99
For Stirring Shafts
approximately 6mm 8124-07 37.51 Additional Parts:
For Stirring Shafts (E) Chuck wrench with key and chain 8081-15 4.46
approximately 10mm 8124-10 43.92 (F) Shaft lubrication, 30mL 8081-19 6.67
For Stirring Shafts (G) Adapter, handpiece 8081-24 14.21
approximately 19mm 8124-15 152.25
Adapter, connecting (3/8-inch O.D. motor shaft 8081-27 14.11
(H)
to motor coupling)
8117 “STIR-LUBE” ACE Trubore®, Stirrer Lubricant

A superior, low melting, silicone-base lubricant which liquifies at body temperature.
8117 Because of its composition, you need apply only a very thin film of “Stir-Lube” to a stirring
shaft to increase bearing and shaft life at least three times over that of bearing lubricated
with glycerine. Non-cooled ACE bearing can be operated at 1500 rpm and water-cooled
bearings up to 2000 rpm for many hours with negligible wear.
Size, grams Order Code Each

28 (1 oz.) 8117-10 20.34
113 (4 oz.) 8117-20 64.93
Stirrers 209
8118 LUBRICANT Stopcock 8118

A smooth, stable, odorless petroleum based (no silicone) lubricant for lubricating joints
and stopcocks. Melts at 52°C (125°F). Can be removed with Xylene.
Size, grams Qty. Order Code Each

75 (2.65 oz.) 1 8118-10 44.58
75 (2.65 oz.) 6 8118-10 240.72
8119 “HI-LUBE” Heavy-Duty Liquid Stirrer Lubricant

ACE chlorofluorocarbon grease for use at speeds up to 6000 rpm with ACE standard
glass assemblies. Use 8040 water-cooled type bearing for long-time stirring (over one
hour). Below one hour, 8038 type may be used at 1500 rpm; eight hours at 1000 rpm. 8119
High chemical inertness — unaffected by strong acids and alkalis. Soluble in most
organic solvents. Suitable for use with oxidizing gases.
High heat resistance — thermally stable up to 260°C (500°F). Non-flammable; does not
carbonize on decomposition. 30mL size.
Order Code Each

8119-07 28.19
8111/8112 ALUMINUM PACKING BOX for 10mm or 19 mm

10mm size designed to be used with 8051 and 8133 bearings; 19 mm with 8060 or 8061
bearings s upplied with PTFE packing. For replacement packing, see 8122. 8111
8112
For Shaft Size Order Code Each
10 mm 8111-10 147.99
19 mm 8112-10 184.14
Photochemical Equipment
ACE Photochemical Reactors
are ideal for:
• Environmental Applications
• Product Aging Tests P.O. Box 688
Vineland, NJ 08362-0688
• Polymerization
• Catalysis
• Photo-oxidation
• Nanotechnology
Toll-free: Toll-free fax:

800-223-4524 800-543-6752
856-692-3333 • Fax: 856-692-8919
www.aceglass.com

210 Stirrers
8115 KRYTOX® GPL Fluorinated Grease

Superior performance, non-contaminating, nonflammable, general purpose grease.
Excellent as a glass bearing lubricant, as a super-inert grease for stopcocks and joints,
as a high temperature grease in “baked-out” vacuum systems, or on distillation column
joints because it is insoluble in almost all solvents except Freon® 113. Easy removal with
fluorinated solvents.
CHEMICAL STABILITY
Krytox GPL grease has demonstrated an exceptional degree of inertness when contacted
with a wide range of reactive chemicals. There is no reaction with the following chemicals:
• oxygen • caustic • fluorine • hydrazine • diethylene triamine • hydrocarbons
• chlorine • hydrogen • ethanol • hydrogen peroxide • phosphoric acid
• red fuming nitric acid • sulfuric acid • methanol • aniline • ammonia
• hydrochloric acid • unsymmetrical dimethyl hydrazine
THERMAL STABILITY
Krytox GPL can be used at operating temperatures up to 204°C (400°F) for extended
periods of time and at 290°C (550°F) intermittently. Approximate minimum use
temperature is -35°F.
*Reg. U.S. Pat. & Tm. Office, DuPont Company. Fluorinated Greases are made only by DuPont.

2 oz. 8115-08 59.40
8116 KRYTOX® LVP High Vacuum Grease

Very low vapor pressure, highly inert, nonflammable grease. The grease for high-vacuum
systems. Superior performance in laboratory and pilot plant equipment, as a lubricant
and sealant for stopcocks, valves, fittings and o‑rings operating at high vacuum or in
hostile environments.
DESCRIPTION
8115/8116 Krytox LVP high vacuum grease is a combination of an extremely low vapor pressure
perfluoroalkylpolyether oil and a fluorocarbon resin thickener. This white, buttery grease
is designed to lubricate the fittings and accessories of high vacuum systems at operating
temperatures down to 10-12 torr at 20°C (1.33 x 10-13 kPa).
The optimum useful temperature range of Krytox LVP is -20° to 260°C (-5° to 500°F).
PROPERTIES
• Krytox LVP high vacuum grease has the following important properties:
• Very low vapor pressure
• High degree of chemical inertness
• Excellent lubricating properties
• Complete nonflammability
• Compatibility with metals, plastics and elastomers
• Excellent oxidation and thermal stability
• Vapor Pressure: torr at 20°C — 1 x 10-13; torr at 200°C — 1x 10-5
*Reg. U.S. Pat. & Tm. Office, DuPont Company. Krytox® LVP is made only by DuPont.

2 oz. 8116-10 105.04
8122 STIRRER PACKING

PTFE packing for use in 8112 stuffing boxes. This material conforms readily to the contour
of the stuffing box and shaft.
8122 For Shaft Size, mm Qty. Per Jar Order Code Per Jar
10 6 8122-10 81.13
19 1 8122-40 16.13
Stirrers 211
8125 SHAFT COUPLING Stirring

Couples stir motor shaft to reactor stir shaft. Flexible neoprene rubber body with
PTFE sleeve inside corrosion-resistant metal end that provides angular and parallel
misalignment of glass or metal stirring shaft without danger of breakage. Rubber body
absorbs shock and provides quiet vibration free running with great torsional stiffness.
Measures four inches overall.
Easy to Use: (1) Slip coupling end with PTFE sleeve over stirring shaft as far as it will go,
approximately three inches. Motor PTFE Sleeve
(2) Bring motor shaft down and align visually approximately 1/2-inch above cou- Shaft Size
pling and shaft. Secure motor position and recheck alignment.

(3) After motor and reactor are securely in place, slide coupling over motor shaft
and tighten set screw.
(4) Slide stirring shaft up into coupling just enough to clear bottom of reactor.
Tighten PTFE sleeve over shaft, using brass set screw, just enough to prevent 4"
slippage.
8125
For 10mm Stirring Shaft For 19mm Stirring Shaft
For Motor Shaft Order For Motor Shaft Order
Size, in. Code Each Size, in. Code Each
1/4 8125-06 43.53 3/8 8125-21 72.94
5/16 8125-08 43.53 1/2 8125-25 72.94
3/8 8125-11 43.53 5/8 8125-27 72.94
1/2 8125-13 43.53 3/4 8125-29 80.00
8124 CHUCK “Flex-Grip,” Light Weight

Nylon chuck for use with 8081 flexible shaft and with stirring shafts or other shafts
of approximately the same dimensions. Chuck has flexible insert that allows for
misalignment of stirring shaft without danger of breakage. Fits standard 5/16-inch 8124
motor shaft or flexible shaft.

For Stirring Shafts approximately 6mm 8124-07 37.51
8126 STIRRING SHAFT COUPLING

Universal swivel coupling for connection to stir motor metal chuck. Compression 8126
connection secured via Allen screw for attaching various O.D. glass shafts.
For Glass Motor Coupling
Rod O.D., mm O.D. (Inches) Order Code Each
6 1/4 8126-05 95.17
8, 9 1/4 8126-08 106.94
10 1/4 8126-10 106.94
19 3/8 8126-19 113.26
8127 COLLAR with PTFE Gasket

Designed to be used with 8068, 8070, 8071, 8074 or 8078 stirring shafts. Handy for
positioning shaft in bearing, and preventing shaft from dropping into flask. Supplied with
PTFE gasket to prevent scratching top of bearing and to act as dust cover. 8127-10
For Rod Size, mm Type Order Code Each

10 Glass-Filled/PTFE 8127-10 24.66
19 Glass-Filled/PTFE 8127-20 36.68 8127-42
28 Glass-Filled/PTFE 8127-28 73.09
10 Stainless Steel 8127-42 26.57 New
19 Stainless Steel 8127-43 42.38
28 Stainless Steel 8127-44 80.60

212 Stirrers
8128 GASKET PTFE, Flat

Designed to fit 8068, 8070, 8071, 8074 or 8078 stirring shafts. Useful as dust cover and
as replacement for gasket supplied with 8127 collar. Twelve to a package.
For Rod Size, mm Qty. Order Code Each

10 12 8128-10 19.81 8128
19 12 8128-20 27.75
28 12 8128-42 42.21
Safety Shields
Ace Glass fabricates safety shields for all four-post style
reactor stands. The shields cover the full height of the stand
for extra safety. Made of high impact, 1/4-inch, clear Lexan,
the three side shields are attached to the stand with stainless
steel fittings and hardware. The door has a positive catch and
handle.
The shields can be placed on both standard wall and
jacketed style reactors. The jacketed style will have holes to
accommodate the chiller inlet/outlet hoses. Make sure you
specify which side, (left or right), will have the chiller hoses.
Since these are custom made and built on each stand, the
shields do not have standard ACE number codes. Just specify
on your requirements and request for quote regarding the
shields as an accessory. The image at left normal set-up for a
10L or 20L stand for a jacketed flask.
Stirring, Mixing 213
13365 AIR STIRRER Light Duty

Arrow Model A
This small, compact and quiet air motor is ideal for stirring all types of solvents, lacquers,
paints, oils, synthetics, and fine and heavy chemicals where danger of explosion may exist,
as there are no sparks. It is a complete unit, ready for mounting on a laboratory stand. Air
supply of only 30 to 100 PSI is necessary. Variable speeds range from 200 rpm to 10,000
rpm merely by turning the air supply line valve. For bath sizes to 20 liters, this smooth
running unit has little or no service cost. Unit adjusts itself to compensate for wear. The
shaft and propeller are made of stainless steel to resist most acids and chemicals and
for easier cleaning. Will start in most stalled positions with low air pressure and cannot 13365-05
burn out from overload. Air Motor — 0-1/3 hp. at 80 lbs. Coupler and stainless steel shaft
30.5cm overall. Propeller: stainless steel 6.4cm diameter. Shaft is 9.5mm (3/8‑inch) O.D.
For filter/regulator/lubricator, see 13372. Air consumption = 13 cfm.
Order Code Each

13365-05 357.03
13365 AIR STIRRER Heavy Duty

Arrow Model G
Specially designed air motor for use on the more viscous materials, provides speed
with power. More constant speed is attained through gear reduction, lowering speed
fluctuations due to changes in air pressure. Speeds range from 50 to 1200 rpm by
merely turning valve on air supply line. This smooth running unit is complete and ready
to mount on laboratory stand. Air supply of only 30 to 80 PSI is necessary. Another
outstanding feature of the unit is the muffler, which provides quiet operation. The shaft
and propeller are stainless steel to resist most acids and chemicals and for easier 13365-10
cleaning. Service costs are almost nil as the unit adjusts itself to compensate for wear.
Air Motor — 0-1/3 hp. at 80 lbs. Gear Ratio — 7–1. coupler and stainless steel shaft
30.5cm overall. Propeller: stainless steel 6.4cm diameter. Shaft is 9.5mm (3/8‑inch)
O.D. For filter/regulator/lubricator, see 13372. Air consumption = 13 cfm.
Order Code Each

13365-10 489.08

214 Stirring, Mixing
13370 AIR STIRRER Heavy Duty, High Torque

A compact, heavy duty air motor with highly damped muffler. Complete unit consists of
an air hose with a snap coupling on motor end and shut-off valve on the other end. Motor
will develop 1.5 hp. at 90 lbs. air pressure. Speeds are variable from 300 to 3000 rpm. It
consumes approximately 42 cfm at 3000 rpm. Shaft is 12.7mm (1/2-inch) diameter for
use with 8124 chuck, not included. For filter/regulator/lubricator, see 13372.
Order Code Each

13370 13370-10 411.74
13372 FILTER/REGULATOR/LUBRICATOR
13372 Arrow
Space-saving multiple unit, recommended for use with 13665 and 13370 air motors.
Pressurized air flows through louvered deflector in swirling pattern, with liquids and dirt
falling into lower baffle where they are prevented from re-entering the air stream. Element
removes impurities down to 40 microns. Clean air then passes through precision needle
valve feed mist lubricator that can be filled under pressure. 150 PSI maximum pressure
range is adjustable through spring action of T-handle. Maximum operating temperature
is 125°F. Manual drain. Shatter-proof polycarbonate bowls not recommended for use
in atmospheres containing acetone, benzene, carbon tetrachloride, ethylene dichloride,
gasoline or toluene. Inlet and outlet connections are 1/4‑inch NPT. Supplied complete
with gauge and mounting bracket.
Order Code Each

13372-45 237.98
13385 GAUGE Pressure

Pressure gauges for monitoring pressure in laboratories; especially suited for use with
the Michel-Miller HP/LPLC system (see our Laboratory Glassware & Equipment Cataog),
pressure reactors (page 23) or other applications when pressure monitoring is necessary.
Available with brass or 316 SS internals. Note: Code -52 is a compound gauge, pressure
and vacuum.
13385-12 Pressure Dial Size Male npt Order
Range, psi (Inches) Connector (In.) Internals Code Each
0–400 2-1/2 1/4 Brass 13385-12 58.50
0–400 2-1/2 1/4 Stainless Steel 13385-14 266.93
0–60 1-1/2 1/8 Stainless Steel 13385-44 171.92
13385-44 0–160 1-1/2 1/8 Stainless Steel 13385-48 181.80
13385-52
Full vacuum–60 1-1/2 1/8 Stainless Steel 13385-52 206.92
■■Digital or analog/dial speed display RZR

■■Two gear stages for high torque at low speeds Standard
■■Over-load protection — reset by power switch Series
■■Over-load protection LED display
Designed for power and reliability. Easy to operate, safe, and suitable for continuous operation.
Stirrers are equipped with a maintenance-free brushless D.C. capacitor motor with overheating
protection feature, reset by power switch. Large speed range of 40 to 2000 rpm has a mechanical
speed adjustment and is monitored via a digital speed display on 13501-21 and 13504-41 making
them ideal for reproducible applications; on 13500-10 the speed is adjusted and monitored with
the help of a scaled control knob.
Supplied with 13 mm O.D. x 160 mm long (approximately 1/2-inch x 6.3-inch) motor support rod and
key adjustable metal chuck, .5 to 10.5mm, for metal shafts like ACE 8074, 10mm O.D. (Units feature a
shaft that can be extended through the top to allow variable depth adjustment. To accomplish this,
you need to order 7mm O.D. shafts, see 8126-22 or 8126-24.)
To use 10mm O.D. glass or PTFE shafts, metal chuck should be replaced with ACE 8124-10 or
8124-15 flex‑grip chuck.
13500/13501/13504 STIRRERS Heidolph RZR Standard Series

Number of Gears 2 2 2
Speed Range [rpm] 40–2000 40–2000 40–2000
Speed Display Analog/Dial Digital Digital
Max. Torque [in-lb] 42.79 42.79 55.63
Torque at 100/1000 [in-lb] 17.12/1.71 17.12/1.71 24.07/2.35 13501-21
rpm
Max. Viscosity [cp] 60,000 60,000 100,000
Max. Mixing Vol. (H2O) [liters] 10 10 20
Dimensions (W x H x D) mm 82 x 206 x 176 82 x 206 x 176 82 x 211 x 176
in. 3.23 x 8.1 x 6.9 3.23 x 8.1 x 6.9 3.23 x 8.3 x 6.9
Weight [Kg/lbs] 3.0/6.62 3.0/6.62 3.3/7.28
Input Power* 115v/60Hz 115v/60Hz 115v/60Hz
Motor Input/Output [Watts] 50/27 50/27 70/37
Heidolph Model 2020 2021 2041
Order Code 13500-10 13501-21 13504-41
Each 1316.02 1659.48 1948.46
*230V/50Hz version also available. 13500-10 not pictured.
13504-41
See 8126, 8126-22, and 8126-24 for

pass-through chuck assemblies for
10 & 19mm stir shafts.

■■Digital speed display

RZR Control
Electronic ■■Two gear stages for constant speed
Series ■■Overheating protection — self reset
■■Over-load protection LED display
Similar to “Standard Series,” except with added features such as constant power. The
electronic automatic control allows almost constant torque over respective speed range.
The two-stage gear provides excellent mixing results even in highly viscous media, using
only as much energy as actually needed. The speed desired is kept constant under changing
loads, even in overload mode. (Power can be increased for a limited time to 175% or 200%,
so there is no premature cutoff when overloaded.)
Changes in viscosity during the process can be followed via a digital display of the torque
on both 13507 and 13511. Also, both models are equipped with an analog interface enabling
output of speed and torque reading to an external device (such as a chart recorder), or
specification of the desired speed via PC. Analog speed and torque output, along with
computer controllability (speed), is 0-10 V/4-20 mA. See 8126-22 or 8126-24 adjustable
pass-through chuck assemblies.
13507/13511 STIRRERS Heidolph RZR Control Series
Number of Gears 1 2
Speed Range [rpm] 50–2000 12–400, 60–2000
Speed Display Digital Digital
Torque Display Digital Digital
Controller Response Constant rpm under changes in viscosity
Overload Response Constant rpm under overload
Max. Torque (continuous/limited) [in-lb] 13.91/31.02 27.81/48.14
Torque at 100/1000 rpm [in-lb] 13.37/2.67 26.74/5.35
13511-02 Power Reserve under Overload up to 200% up to 200%
Max. Viscosity [cp] 10,000 100,000
Max. Mixing Volume (H 0)
2
[Liters] 20 40
Dimensions (W x H x D) mm 72 x 206 x 176 82 x 211 x 176
in. 3.23 x 8.1 x 6.9 3.23 x 8.3 x 6.9
Weight [Kg/lbs] 2.8/6.17 3.7/8.16
Input Power* 115v/60Hz 115v/60Hz
Motor Input/Output [Watts] 80/50 140/100
Heidolph Model 2051 2102
Order Code 13507-51 13511-02
Each 2363.71 3995.45
*230V/50Hz version also available. 13507-51 not pictured.
13507-51 is ideal for use with our Auto-Reactors

and ROBO Reactors.
Three State-of-the-Art Laboratory Stirrers

■ ■Totally enclosed, non-ventilated, ■ ■On/Off switch for quick stopping
permanent magnet D.C. motor if necessary
for long service life ■ ■Stirrers come complete as
■ ■Eye level, heavy cast aluminum shown, including 9/16-inch dia.
control box integrated with x 10 inches long aluminum
motor for safe and easy support rod
operation of stirrers ■ ■10 0 % b a c k e d b y t h e b e s t
■ ■Control knob electronically guarantee in the business:
regulates speed of application • 30-day satisfaction guarantee
required • Six-month unconditional
■ ■O v e r l o a d p r o t e c t i o n — a guarantee
m a n u a l l y re s e t a b l e c i rc u i t
breaker for total safety
Not supplied with shaft, propeller or coupling.

13542 13544
For stainless steel shaft, propeller and coupling, order 13542-60.
For glass shafts, agitators and coupling, see 8068–8124. 13543
13542 STIRRER Laboratory, Heavy Duty, Variable Speed

• Handles high viscosity fluids up to 4400 cps in 5-gallon batch or up to 100L water
• Variable speed — up to 1000 rpm, gear head
• Constant torque throughout speed range is 7.35 in-lbs. Optional Accessory
• 1/10 hp motor operates at 120 VAC, 60 hz
• Motor shaft is 3/8-inch (9.5 mm) 11082 CLAMP
“Power Hold”
Order Code Each
Fits stirring stand with 3/8-inch
13542-25 737.95 to 5/8-inch diameter shaft and
stirrers with mounting rod from
13543 STIRRER Laboratory, Light Duty 3/8-inch to 5/8-inch diameter.
• Handles watery to light syrupy mixtures, or up to 20L water Stop collar included.
• Variable speed — up to 6000 rpm, direct drive Order
• Constant torque throughout speed range is 1.05 in-lbs. Code Each
• 1/10 hp motor operates at 120 VAC, 60 hz 11082-07 54.12
• Motor shaft is 3/8-inch (9.5mm)
Order Code Each

13543-12 555.88
13544 STIRRER Laboratory, Medium Torque, Variable Speed

• Handles light to syrupy mixtures, or up to 100L water
• Variable speed — up to 2000 rpm, direct drive
• Constant torque throughout speed range is 2.43 in-lbs.
• 1/15 hp motor operates at 120 VAC, 60 hz
• Motor shaft is 3/8-inch (9.5mm)
Order Code Each

13544-20 582.32
SPECIFICATIONS
Model # Type Speed Range Constant Torque Motor Power Shipping Wgt.
13542-25 Gear Head to 1000 rpm 7.35 in-lbs 1/10 HP 120 VAC 8 lbs.
13543-12 Direct Drive to 6000 rpm 1.05 in-lbs 1/10 HP 120 VAC 8 lbs.
13544-20 Direct Drive to 2000 rpm 2.43 in-lbs 1/15 HP 120 VAC 8 lbs.

13514/13516 STIRRER DigitalLa oratory stirrer designed for simple tasks for quantities from
25L to
Laboratory stirrer designed for simple tasks for quantities from 25L to 40L of water. It
automatically adjusts the speed through microprocessor controlled technology within
the speed range of 0/30 to 2000 rpm. Safety circuits installed ensure automatic cut-off
in anti-stall or overload conditions. Continuous comparison of shaft speed to desired
speed is maintained and variations adjusted automatically. This guarantees a constant
speed even with changes in viscosities of the sample. Two-year manufacturer’s warranty.
Order Code 13514-10 Eurostar 40 13516-20 Eurostar 60

Price (each) 1171.00 1301.00
Stirring Quantity Max (H2O) 25L 40L
Speed Range 0/30-2000 rpm 0/30-2000 rpm
Viscosity Max 30000 mPas 50000 mPas
Setting Accuracy Speed 1 ±rpm 1 ±rpm
Weight 4.4 kg 4.4 kg
Chuck Range (Dia.) 0.5-10 mm 0.5-10 mm
Electrical Input 115V, 50/60Hz 115V, 50/60Hz
Output Max. (at Stir Shaft) 84 W 126 W
Torque Max. (at Stir Shaft) 40 Ncm 60 Ncm
IKA motors are available in 230v versions.
13517/13518 STIRRER Removable Wireless Control oratory stirrer designed for

simple tasks for quantities from 25L to
Universal laboratory stirrer designed with a removable wireless controller and a digital TFT
display. It automatically adjusts the speed through microprocessor controlled technology
with the speed range of 0/30 to 2000 rpm. The stirrer comes equipped with a RS232 and
USB interface to control and document all parameters. An integrated torque trend display
is provided for the measurement of viscosity changes. Safety circuits installed to ensure
automatic cut-off in anti-stall or overload conditions. Two-year manufacturer’s warranty.
Order Code 13517-30 Eurostar 60 13518-02 Eurostar 100

Price (each) 1483.00 2538.00
Stirring Quantity Max (H2O) 40L 100L
Speed Range 0/30-2000 rpm 0/30-2000 rpm
Viscosity Max 50000 mPas 70000 mPas
Setting Accuracy Speed 1 ±rpm 1 ±rpm
Weight 4.7 kg 4.7 kg
Chuck Range (Dia.) 0.5-10 mm 0.5-10 mm
Electrical Input 115V, 50/60Hz 115V, 50/60Hz
Output Max. (at Stir Shaft) 126 W 136 W
Torque Max. (at Stir Shaft) 60 Ncm 100 Ncm
13523 STIRRER Mechanical oratory stirrer designed for simple tasks for quantities from 25L to
Powerful, mechanically controlled stirrer with LED digital display. Suitable for quantities
up to 20 l (H2O) for use in laboratories and pilot plant stations. Two speed ranges within
60-2000rpm, for highly viscous media and intensive mixing. Push-through mixing tools.
Special motor overheating protection by means of self-locking temperature limiter.
Two-year manufacturer’s warranty.
Order Code 13523-10

Price (each) 730.00
Stirring Quantity Max (H2O) 20L
Speed Range 60-2000 rpm
Viscosity Max 10000 mPas
Setting Accuracy Speed 1 ±rpm
Weight 3.1 kg
Chuck Range (Dia.) 0.5-10 mm
Electrical Input 100V, 50/60Hz
Output Max. (at Stir Shaft) 26 W
Torque Max. (at Stir Shaft) 150 Ncm
*Contact ACE regarding IKA Labworld software.

13565-05 STIRRER O
verhead, Digital BDC6015
Rugged Ultra-Speed Model with range from 40-6000 rpm. Microprocessor controlled brushless
DC motor with automatic overload protection. Digital display of RPM and torque. Keypad
adjustable. Maintains set speed as viscosity changes. 2-speed transmission selects hi-torque
or hi-speed range. Adjustable steel chuck with hinged chuck guard. 120V version UL and CSA
approved. A 230V (CE approved) version is available via special order. Three–year warranty.
Specifications:
MODEL 13565-05 / BDC6015
Low Speed Range 40–1200 rpm
High Speed Range 1200-6000 rpm
Maximum torque (low speed range) 170 N-cm (15 in-lbs)
New
Maximum torque (high speed range) 34 N-cm (3 in-lbs)
Speed Accuracy +/- 1% of reading or +/- 1 rpm
Torque Accuracy +/- 5% of reading or +/- 1 in-lb
Electrical Input 120V, 50/60 Hz, 5 Amps
Output Power 1/5 Hp, 150W
Weight 11 lbs (5 kg)
Chuck accepts up to 3/8-in (10.1mm) shafts
Maximum Volume 6.6 US Gallons (25 Liters)
Maximum Viscosity 20,000 cps
Order Code Each

13565-05 1740.31
approved.
13565-10 STIRRER O
verhead, Digital BDC3030
Universal Model with all the specifications and features of the BDC 6015, except with lower
speed range (20-3000 rpm). Three-year warranty.
13565
Specifications:
MODEL 13565-10 / BDC3030
! Maximum torque (low speed range) 339 N-cm (30 in-lbs)
er ful Maximum torque (high speed range) 68 N-cm (6 in-lbs)
Pow Speed Accuracy +/- 1% of reading or +/- 1 rpm
Order Code Each

13565-10 1740.31
approved.
Caframo motors are available in 230v versions.
13566 STIRRER Overhead, Reversing, Digital BDC2010

The 2010 has a rugged DC brushless motor that delivers from 40-2010 RPM. This model
has a small footprint and is loaded with features such as “Stirlight” which lights a downward New
beam of light into the mixture, timer, reverse feature and xRx agitation for a controllable
vortex effect, automatic overload protection and maintains speed at all viscosities. The
2010 is the only stirrer of it’s kind and can be set up for automatic time and auto-reverse
for better mixing. Three-year warranty. 13566
Specifications:
MODEL 13566-05 / BDC2010
Speed 40–2010 rpm (clockwise and/or counterclockwise
Timer Set from 1-2000 minutes (33.3 hours)
Maximum torque 100 N-cm (8.8 in/lbs)
Electrical Input 100-240V, 50/60 Hz
Weight 8.2 lbs (5.6 kg)
Order Code Each
13566-05 1218.00
approved.
rse!
Reve
Auto
13565 STIRRER Overhead BDC1850

Compact size and powerful overhead stir motor. Rugged stir motor that delivers 12-1800 New
rpm with 1/5 horsepower DC brushless motor. Digital display of RPM and Torque. Keypad
adjusts speed and rotation. Set speed is automatically maintained and adjusts to torque
changes. 120V CSA and UL approved. Three year warranty. Also available in a 230V version.
Comes with adjustable chuck, chuck protective cover.
Specifications:
MODEL 13565-20 / BDC1850
Maximum torque (low speed range) 565 N-cm (50 in-lbs)
Maximum torque (high speed range) 113 N-cm (10 in-lbs)
Speed Accuracy +/- 1% of reading or +/- 1 rpm
Maximum Volume 21 US Gallons (80 Liters)
Maximum Viscosity 90,000 cps 13565
Order Code Each

13565-20 1740.31
approved.

13554 STIRRING MOTOR* AND CONTROLLER Pilot Plant,

for Hazardous Area (Motor Only)
MOTOR: For hazardous area*, heavy duty, 1/4 or 1/2 hp, permanent magnet, DC
* UL Classified: reversible, 90 volt DC armature type. This 56C base frame, continuous duty, ball bearing,
Hazardous motors only totally enclosed fan cooled (XPFC) motor has a variable speed range up to 1750 rpm.
Class I, Div. I, Group D
Operates at a maximum temperature of 40°C. With 5/8-inch O.D. motor shaft. Supplied
Atmospheres with 30-foot cord with mating twistlock cap. Overall length: code -40 is 10-1/2 inches;
(Flammable Gases or Vapors) code -50 is 12-3/4 inches. Maximum torque rating: code -40 is 9.1 in-lbs.; code -50
is 18.3 in-lbs., NEMA C-face. Shipping weight: code -40 is 34 lbs.; code -50 is 50 lbs.
Class II, Div. I, Group F & G
(Combustible Dust) CONTROLLER: Converts 120 volts AC to 90 volts DC. Supplied with 6-foot cord to a
twistlock connector for connection to motor. (NOTE: controller should be mounted remote
of hazardous area). NEMA classification 4/12 (water and dust proof for industrial use).
Maximum speed preset at factory at 900 rpm for safety, can be increased or decreased
internally, see instructions. Also has torque and current limit adjustments, all factory set.
Use 6472-872 mounting plate when using with some reactors. Use offset
adapters when using this motor with 6472 reactors to move condenser, etc.,
away from motor mount.
Order Code Each

Motor, 1/4 hp, only 13554-40 1577.48
Complete, 1/4 hp 13554-45 2670.40
Motor, 1/2 hp, only 13554-50 2276.62

Complete, 1/2 hp 13554-55 3369.54
13554-45, -55
13554 STIRRING MOTOR AND CONTROLLER Pilot Plant

MOTOR: Non-hazardous area, heavy duty, 1/4 or 1/2 hp, permanent
13554-07, -10 magnet, DC reversible, 90 volt DC armature type. This 56C base frame,
continuous duty, ball bearing, totally enclosed fan cooled (TEFC) motor
has a variable speed range up to 1750 rpm. Operates at a maximum
temperature of 40°C. With 5/8-inch O.D. motor shaft. No UL classification.
Supplied with 30-foot cord with mating twistlock cap. Overall length: code
-05 is 10-1/2 inches; code -09 is 12-1/2 inches. Maximum torque rating:
code -05 is 9.1 in-lbs.; code -09 is 18.3 in-lbs., NEMA C-face. Shipping
weight: code -05 is 17 lbs.; code -09 is 25 lbs.
CONTROLLER: Converts 120 volts AC to 90 volts DC. Supplied with
6‑foot cord to a twistlock connector for connection to motor. (NOTE:
controller should be mounted remote of hazardous area). NEMA
classification 4/12 (water- and dust-proof for industrial use). Maximum
speed preset at factory at 900 rpm for safety, can be increased or
decreased internally, see instructions. Also has torque and current
limit adjustments, all factory set. See listing below of offset adapters
necessary for use when using this motor with 6472 reactors. Use 6472-
872 mounting plate when using with some reactors.
IMPORTANT: Order Code Each OFFSET ADAPTER, only

The controller and connectors Motor, 1/4 hp, only 13554-05 718.72 Joints Order Code Each
between controller and motor Controller, only 13554-24 1092.92
should be in line of sight of the 24/40 5268-10 36.56
Complete, 1/4 hp 13554-07 1811.64 29/42 5268-15 40.74
motor. DO NOT disconnect
controller from motor while Motor, 1/2 hp, only 13554-09 765.49 45/50 5268-21 109.58
operating or when controller is Controller, only 13554-26 1092.92
powered; damage to motor or Complete, 1/2 hp 13554-10 1858.41
controller could result.
13557 STIRRING MOTOR AND CONTROLLER Offset, 13557

Hazardous Duty Series Hazardous Duty
Stirring motor, controller and right-angle, off-set drive. Same motor and analog
controller as 13554 — hazardous area unit except complete with right-angle
drive gear box.
Order Code Each

Analog, 1/4 horse power, complete 13557-110 3322.37
Stirring motor, controller and right-angle, off-set drive. Same motor and controller
as 13554 — hazardous area unit except complete with right-angle drive gear DIgital Controller
box and digital control.
Order Code Each

Digital, 1/4 horse power, complete 13557-220 4021.01 Analog Controller
Digital, 1/2 horse power, complete 13557-240 4779.56
13557 STIRRING MOTOR AND CONTROLLER Offset, 13557

Standard Duty
Standard Duty Series
Stirring motor, controller and right-angle, off-set drive. Same motor and analog
controller as 13554 — standard unit except complete with right-angle drive
gear box.
Order Code Each

Stirring motor, controller and right-angle, off-set drive. Same motor and controller
as 13554 — standard unit except complete with right-angle drive gear box and
digital control.
DIgital Controller
Order Code Each
Digital, ¼ horse power, complete 13557-420 3206.93
Digital, ½ horse power, complete 13557-440 3299.45
Analog Controller
13557 GEAR BOX Fits Both Standard & Hazardous Duty Series
Right-angle drive 5:1 gear box only. Bolts directly to motors with a 5/8-inch diameter shaft.
Order Code Each

For 1/4 or 1/2 horse power motors 13557-10 651.97
13557-10

8135 GEAR BOX Right Angle Side Drive

Right-angle, side drive gear box. Has 9-inch long aluminum support rod for attaching
to a clamp holder or flex-frame. Polished aluminum case. 10mm stainless connecting
rods on in/out drive. Can easily be used with ACE 8081 Flex-Shaft and either 8126‑10
or 8124 chucks. Using a flex shaft allows for use with any stir motor.
8135
Order Code Each
8135-10 831.74
New
New 13555 STIRRING MOTOR/CONTROLLER Digital, Haz Mat Series

Heavy-duty, 1/2 HP stirrer motors complete with the digital Microdrive
control box. The low-power, AC variable speed drive has a compact design
and is available in switched or non-switched enclosures. Its IP-55/NEMA 12
rating makes it ideal for use harsh environments. Control box is dust tight
construction. Easy to read LED display and flat panel controls. Controller is
wall or stand mountable. Control box has 12-ft cord to motor and control
box to plug cord is 24-ft long.
Motor is 230V 3-phase, 60Hz, which is wired to the Microdrive which steps
down to and is 115V, 50Hz. Sold complete only.
Order Code Each

1/2 HP motor with Microdrive controller 13555-50 3261.08
13555
13557 GEAR REDUCER 56C Flange, 4:1 Reduction

New In-line, offset 4:1 gear reducer. Top 56C flange accepts 13554 motor with 5/8-inch diameter
shaft. Bottom has 56C flange with 5/8-inch diameter shaft. Shaft is offset approximately
1-5/8 inches. Flange face-to-face distance is approximately 4-3/4 inches. Can be used
on new or existing reactor motor mounts to increase torque of reactor agitation system.
Order Code Each

13557-20 662.52
13557-20
New
13532 DUAL MOTOR SPEED & POWER CONTROLLER Solid State

Similar to 13530, but with buffered load control and DC filtration to provide more torque
at higher speeds and a higher top speed than motor rating.
Ratings: AC three-prong output socket, standard NEMA type, 1200 watts. 0-120 volts,
variable, 60 Hz. maximum 10 amps. DC four-prong output socket, “cinch” type. 360
watts, 0-150 volts, variable, filtered approximately 1/2 hp. maximum three (3) amps.
A compact 8.9 x 8.9 x 17.8cm (3-1/2 x 3-1/2 x 7 inches), lightweight 1 Kg. (2-1/4 lbs.)
solid state control with rugged control regulation and rectification circuitry. Two output
sockets AC and DC which work in conjunction. Fwd-Off-Rev. DC control switch only.
Fused for AC and DC outputs, 10 amps and three (3) amps respectively. Rear ring stand
clamp for easy mounting and access. Light blue modern type case with protective finish.
Red pilot light. Large dial plate with 0-100 divisions. Red control knob with Click-Off.
Heavy duty 1.8 meter neoprene, three-wire power cord with NEMA plug.
13532
Uses — AC output socket, rear mounted: Heating mantles • Universal motors • Hot plates
and heating baths • Incandescent lighting, resistive loads • Most loads accept 120v AC Use of 13649 motor (page 221) is
up to 10 amps — functions comparable to the autotransformer. recommended with this controller.
DC output socket, front mounted: Four-conductor output socket for DC reversible series
wound motors • Plug supplied with instructions to obtain a DC output of 0–150 volts
variable, maximum current three (3) amps at 360 watts.
Order Code Each

13532-10 623.28
13586 SUPPORT STAND

All-stainless-steel support stand. Heavy base, six pounds, can accommodate vessels
up to 18 inches in diameter within its “U” shape. Support rod is 5/8-inch diameter,
approximately 29 or 36 inches high, fastened to base with stainless steel lock nuts. Two
additional threaded holes in base legs to accommodate extra support rods. Complete
item consists of one base and one rod.
13586
Stand complete with support rod
Rod Height (Inches) Order Code Each
28 13586-10 274.82
36 13586-13 313.93
5/8-Inch Stainless Steel Support Rod, only
Rod Height (Inches) Order Code Each
60 13586-15 181.78
28 13586-25 104.64
36 13586-27 133.18

13649 STIRRER Laboratory, Solid State

Totally enclosed, 1/40 hp., permanent magnet motor with dual 8mm (5/16-inch) armature
and gear shafts with milled flats. Armature shaft with maximum speed of 4000 rpm; 18:1
ratio gear shaft rated 4.2 Kg.–cm (58.3 oz-in) torque, up to 333 rpm. Baked black enamel
Va finish, precision die-cast housing, lifetime lubricated ball bearings with steel inserts in
lu die-casting.
e
Motor: Supplied with 1.5 meter three-wire cable with plug and ground lead for connection
to controller. Measures: 5-1/2 x 4 x 4 inches. Weight: 4 lbs 7 oz.
13530-10 Controller: ACE 13530* solid state 120v, 10 amp AC maximum or 0–120v, 6 amp DC
maximum. Features rear ring stand clamp, Forward/Off/Reverse switch. Supplied with
heavy duty 1.8 meter three-wire power cord with NEMA plug. Supplied with one-amp
fuse to protect motor. Controller measures 102 (4 inches) x 54 (2-1/8 inches) x 41mm
(1-5/8 inches). Weight: 4.1 lbs. Complete consists of motor, controller and mounting rod.
Order Code Each

Motor, only, w/ Mounting Rod 13649-09 742.01
Complete 13649-19 1265.18
13649-09
MOTOR ATTACHMENTS (Optional):
Order Code Each
Three-jaw, keyless chuck, 9.5mm (3/8-inch) rod 13649-24 130.00
Nylon chuck, flex-grip, for shaft size approximately 10mm 8124-10 43.92
Set screw wrench 13649-26 6.10
Paddle, 3–6.4cm blades, S-S, on 22.2cm shaft 13649-32 104.00
Propeller, 3–3.8cm blades, S-S, on 22.2cm shaft 13649-34 97.00
(Stand Not Included)
Attachments Complete (Does not include 8124-10) 13649-40 369.04
*ACE 13530 motor controller offers better performance at slower speeds;

for more torque at higher speeds, use 13532.
13650 STIRRER Laboratory, High Torque, Economy

Motor: Totally enclosed, non-reversible, 1/17 hp. DC input with a 5/16-inch
diameter shaft 1-inch long. Recommended for use with 8081 flexible shaft (shaft
turns counter-clockwise when facing shaft) or general stirring. Motor is adjustable
from 280 to 2800 rpm and generates 60 oz-in. of nominal torque. (Note: torque
diminishes below 280 rpm with safety click off.) Cast aluminum motor case is
painted chemically resistant grey. Supplied with 6-foot cord with NEMA plug end
and 5/8-inch diameter mounting rod. Measures 4.65 x 3.25 x 3.65 inches. Weight:
4.75 lbs. Can only be plugged into controller.
Controller: Durable plastic case for table top use. Rated at 120 volts, 50/60 Hz, 1.5 amp
maximum to protect motor beyond its rated torque. Measures: 6W x 5D x 2.5H inches.
Weight: 1.8 lbs. including 6-foot power cord.
Order Code Each

Motor and Controller 13650-40 803.57
13650
(Stand Not Included)
Accessories 227
4048 BOTTLE Solution, Threaded Neck O‑Ring Seal
PYREX® brand borosilicate glass bottle designed for storage of solutions. Bottles have
GL120 external thread finish neck with large 106mm (4.2-inch) I.D. opening. The 9.5 liter
and 13.25 liter sizes have a conventional bottle shape. The 19 liter and 45.5 liter sizes are
similer in d
esign to a carboy. A glass-filled PTFE cap with CAPFE (PTFE encapsulated
silicone) O‑Ring is available. Cap sold separately.
Capacity, Capacity, Approx. Approx. Order

Liters Gallons Dia., mm Height, mm Code Each
9.5 2.5 187 460 4048-09 277.47
13.25 3.5 238 380 4048-13 343.50
19.0 5 292 480 4048-19 377.73
45.5 12 406 520 4048-45 708.30
CAP, PTFE, Solid, GL 120, with CAPFE O‑Ring 7622-155 184.15 4048-19
5393 BOTTLE Solution, Plastic Coated

Bottle is coated to the neck with PVC safety coating to reduce potential breakage and 5393
exposure to laboratory personnel when handling hazardous material. The 19L bottle is
Carboy style, with sloping shoulders. The 9.5L and 13.25L sizes are “bottle” shaped.
Necks are tooled for uniform fit with stoppers.
Approx. Approx. Approx. Rubber
Cap., Cap., Dia., Height, Stopper Plastic Coated
Liters Gal. mm mm No. Order Code Each
9.5 2.5 187 470 12 5393-06 332.57
13.25 3.5 238 445 12 5393-07 382.33
19.0 5 292 508 12 5393-09 451.44
5395 BOTTLE Solution, with “Ace-Safe,” Plastic Coated 5395

Same as 5393 bottle, except this bottle has a vacuum takeoff and is coated to the
neck with PVC safety coating to reduce potential breakage and exposure to laboratory E-SA
AC
FE
personnel when handling hazardous material. Takeoff has a #15 Ace‑Thred in place of a
serrated fitting for use with an “Ace-Safe” tubing connection barb for 3/8-inch I.D. tubing.
ON
OR
C
Supplied complete with hose connection, nylon bushing and O‑Ring. N ECT
Approx. Approx. Approx. Rubber Plastic Coated
Cap., Cap., Dia., Height, Stopper
Liters Gal. mm mm No. Order Code Each
9.5 2.5 187 470 12 5395-103 433.21
13.25 3.5 238 445 12 5395-105 482.76
19.0 5 292 508 12 5395-107 518.98
5393 and 5395 bottles are also available safety coated via special request.
Surlyn is a registered trademark of E.I. Dupont & Co.

228 Accessories
5539 BOTTLE Laboratory, GL Thread

Duran
Chemically resistant and stable laboratory bottles, fabricated from borosilicate glass.
Supplied graduated with or wtihout red plastic cap and removable pouring ring that allows
drip-free operation. Cap has PTFE liner. For use up to 180ºC. Not suitable for vacuum
or pressure use. Can be hot air sterilized or autoclaved. For extra caps or pour rings,
see 7622 in our Laboratory Glassware & Equipment catalog, or visit www.aceglass.com.
With Cap Without Cap

Cap., Approx. GL Thread O.D., Height, mm Order Order
mL Cap., Oz. Size mm w/Cap Code Each Code Each
5000 169 45 186 340 5539-30 148.44 5539-64 176.04
10000 338 45 234 415 5539-35 279.42 5539-66 328.70
15000 507 45 277 450 5539-41 374.19 5539-68 455.12
20000 676 45 300 510 5539-44 515.50 5539-70 687.42
5539-35 5539-66
5539 BOTTLE Laboratory, Safety Coated, GL Thread

Duran
Chemically resistant and stable laboratory bottles, fabricated from borosilicate glass
and plastic coated for protection against mechanical damage and to prevent leakage
of contents should the glass break. Supplied graduated with or without red plastic cap
and removable pouring ring that allows drip-free operation. Cap has PTFE liner. For use
up to 140°C. Not suitable for vacuum or pressure use. Height measurement is with cap.
Autoclavable or good for hot air sterilization. For extra caps or pour rings, see 7622 in
our Laboratory Glassware & Equipment catalog, or visit www.aceglass.com.

Capacity, GL Thread O.D., Height,. mm Order Order
mL Size mm w/Cap Code Each Code Each
5000 45 186 340 5539-130 195.71 5539-160 229.74
5539-130 5539-160
5539 BOTTLE Laboratory, Ambered, GL Thread

Duran
Chemically resistant and stable laboratory bottles, fabricated from borosilicate glass and
ambered for protection of liquids sensitive to light. Supplied graduated with or without
red plastic cap and removable pouring ring that allows drip-free operation. Cap has PTFE
liner. For use up to 180°C. Not suitable for vacuum or pressure use. Height measurement
is with cap. Autoclavable or good for hot air sterilization. For extra caps or pour rings,
see 7622 in our Laboratory Glassware & Equipment catalog, or visit www.aceglass.com.

Capacity, GL Thread O.D., Height,. mm Order Order
mL Size mm w/Cap Code Each Code Each
5000 45 186 340 5539-230 249.98 5539-262 279.44
10000 45 234 415 5539-235 460.15 5539-264 530.96
15000 45 277 450 5539-241 547.29 5539-266 635.27
20000 45 300 510 5539-244 1022.69 5539-268 1204.27
5539-235 5539-264
Accessories 229
7621 CAP With Hole, GL Thread

Open top red polybutylene teraphthalate (PBT) cap for use with 7620 GL threads. When 7621
used with 7623 hose connection and 7624 sealing ring, will accommodate tubing of
approximate diameter.
For Thread Temperature. Aperature Size, O.D., Height, Order

Size Range, °C mm mm mm Qty. Code Each
25 –45 to +180 15 33 19 1 7621-15 2.91
32 –45 to +180 20 40 24 1 7621-22 3.46
45 –45 to +180 34 54 26 1 7621-25 6.10
7622 CAPS/POURING RINGS for GL Threaded Bottles

Screw caps and pouring rings for use with GL threads. Red caps have PTFE liner, all
others are with lip seal. For 5539, 5557, 5559, and 5560 bottles.
CAPS
For
Thread Temperature O.D., Height, Case Order Case
Size Material Color Range, °C mm mm Qty. Code Price
25 Polypropylene Blue -40 to +140 33 19 10 7622-02 26.89
25 Polybutylene Teraphthalate Red -45 to +180 33 19 10 7622-14 53.27
45 Polypropylene Yellow -40 to +140 54 26 10 7622-32 32.23
45 Polypropylene Green -40 to +140 54 26 10 7622-35 32.23
45 Polypropylene Grey -40 to +140 54 26 10 7622-37 32.28
POURING RINGS
For
Thread Temperature Height, Case Order Case
Size Material Color Range, °C mm Qty. Code Price
32 Polypropylene Blue -40 to +140 4 10 7622-52 11.39
45 Polypropylene Blue -40 to +140 4 10 7622-54 12.38 Color-Coded Caps
32 Polybutylene Teraphthalate Red -45 to +180 4 10 7622-56 30.10 and Pour Rings
45 Polybutylene Teraphthalate Red -45 to +180 4 10 7622-58 32.54
45 Polypropylene Green -40 to +140 4 10 7622-60 10.51
45 Polypropylene Yellow -40 to +140 4 10 7622-62 10.51
45 Polypropylene Grey -40 to +140 4 10 7622-64 10.51
80 Polypropylene Blue -40 to +140 7 10 7622-65 33.91

230 Accessories
New 7627 CAP & POUR RING Premium, for GL Threaded Bottles
This premium cap is designed for GL45 thread Duran bottles. It is made of colorless,
TPCh260 resin so that there are no leachables. High Chemical resistance and leak tight
7627 due to a PTFE coated silicone seal. Meets USP standards. Autoclavable. Retrace code.
Temperature. O.D., Height, Case Order Case

Description Range, °C mm mm Qty. Code Price
Cap –196 to +260 51 26 5 7627-02 106.30
Pour Ring –196 to +260 51 4 5 7627-03 25.89
New 7628 CAP & POUR RING for GL80 Threaded Bottles, Quick Release, PSU
Quick-release closure for new GL80 thread, wide-mouth bottles. Made of white
polyarylsulphone 1 resin, which gives high thermal, mechanical and chemical compatibility.
Inner-seal is coated both sides with PTFE. Pour ring also available in PSU.
Maximum O.D., Height, Case Order Case

Description Temp., °C mm mm Qty. Code Price
Cap +180 86 40 5 7628-03 255.71
7628 Pour Ring +180 86 6.85 5 7628-04 156.09
7629 CAP PTFE Membrane, for GL Threaded Bottles

New Polypropylene, blue cap with center-hole and welded-in, PTFE, inner gas permeable
membrane. Ideal for media sterilization and storage. For use on 5539, 5557, 5559 and
5560 bottles.
For Thread Temperature. O.D., Height, Case Order Case

Size Range, °C mm mm Qty. Code Price
25 –40 to +140 33 19 5 7629-25 77.65
7629 32 –40 to +140 41 24 5 7629-32 78.19
45 –40 to +140 54 25 5 7629-45 45.25
80 –40 to +140 86 40 2 7629-80 26.90
Accessories 231
7631 CAP GL80 Connection System New

The heart of the GL80 connection system is a GL80 polypropylene cap with 4, GL18
threaded ports. Modular accessories include polypropylene tube connection caps,
GL18 solid polybutylene terepthalate (PBT) caps, GL18 PBT pressure equalization
caps and PTFE cap inserts to accomodate various sizes of tubing. A typical
application is the safe transfer of liquid media within a closed and sterile system
for which you’d need one two-pack code -01 GL80 cap,two -04 equalization caps,
and some combination of solid caps and tubing connections with inserts.
Package Order Package

Description Qty. Code Price
4-Port (GL18) Polypropylene Cap 2 7631-01 247.94
GL18 Polypropylene Tube Connection 2 7631-02 23.98 7631
Solid GL18 PBT Cap 2 7631-03 10.75
GL18 PBT Cap wtih Pressure Equalizing Valve 1 7631-04 47.37
3.2mm I.D. PTFE Cap Insert 1 7631-10 29.14
7632 CAP GL45 Connection System New

The heart of the GL45 connection system is a GL45 polypropylene cap with GL18 threaded
ports. Modular accessories include polypropylene tube connection caps, GL18 solid
polybutylene terepthalate (PBT) caps, GL18 PBT pressure equalization caps and PTFE
cap inserts to accomodate various sizes of tubing. A typical application is the safe transfer
of liquid media within a closed and sterile system for which you’d need one two-pack
GL45 cap, two -07 equalization caps, and some combination of solid caps and tubing
connections with inserts.
Package Order Package

Description Qty. Code Price
7632
GL14 Polypropylene Tube Connection 2 7632-05 15.00
Solid GL18 PBT Cap 2 7632-06 8.21
GL14 PBT Cap wtih Pressure Equalizing Valve 1 7632-07 45.78
Extra Pressure Membranes for 7632-07 2 7632-08 30.00

232 Accessories
5559 BOTTLE Wide Mouth, Clear, Amber or Plastic Coated

5559 New Duran
Borosilicate glass wide-neck bottle with GLS 80 quick-release blue closure for use up to
140°C (plastic coated up to 135°C). Graduated. For extra caps or pour rings, see 7622
in our Laboratory Glassware & Equipment catalog, or visit www.aceglass.com.
Capacity, O.D., Height,. Order
mL Type mm mm Code Each
5,000 Clear 182 311 5559-09 205.05
10,000 Clear 227 395 5559-20 374.74
20,000 Clear 288 483 5559-24 810.21
5,000 Amber 182 311 5559-209 431.13
10,000 Amber 227 395 5559-220 628.98
20,000 Amber 288 483 5559-224 1289.29
5,000 Clear/Plastic Coated 182 311 5559-304 388.59
6989 BOTTLE Filtering, with Removable PP Hose Connection

Duran
6989
Heavy wall, bottle shaped, filtering flask with removable polypropylene hose connection.
Offered clear or plastic coated. Plastic coated bottles are steam autoclavable at 135°C.
For replacement hose connection assembly, order 6989-40.
CLEAR GLASS
Capacity, Body Height, Neck Order
mL O.D., mm mm I.D., mm Code Each
3,000 170 295 60 6989-15 135.99
5,000 185 360 70 6989-18 220.06
10,000 240 420 70 6989-21 324.62
15,000 255 500 70 6989-24 387.51
20,000 290 535 70 6989-27 486.59
PLASTIC COATED
Capacity, Body Height, Neck Order
mL O.D., mm mm I.D., mm Code Each
3,000 170 295 60 6989-115 178.60
5,000 185 360 70 6989-118 270.69
10,000 240 420 70 6989-121 407.69
15,000 255 500 70 6989-124 474.24
20,000 290 535 70 6989-127 560.73
12477 BOTTLE Aspirator with Spigot

Constructed of polyethylene with polyethylene spigot and screw closure. Quick-action
12477 spigot, for easy, positive control, leakproof operation and long life. Suitable for collecting
and dispensing distilled water, handling acids. Leakproof closures.
Cap., liters Quantity Order Code Each Case Price

4 Each or case of 6 12477-02 104.85 629.10
8 Each or case of 6 12477-04 148.35 890.10
20 Each or case of 4 12477-06 178.80 715.20
25 Each or case of 4 12477-08 201.55 806.20
Accessories 233
5332 BEAKER Heavy-Wall, Pilot Plant Size

Duran
Heavy wall beakers with spout.
Capacity, O.D., Height, Order

mL mm mm Code Each
5,000* 182 256 5332-28 169.97
10,000 225 340 5332-33 342.76 5332
15,000 260 390 5332-36 461.29
20,000 285 430 5332-39 532.25
*5,000mL size (only) is graduated.
6228/6231 BEAKER Pilot Plant

Large sizes for batch operations and mixing large volumes of measured liquids. Graduated. 6228/6231
Capacity, Subdiv., Approx. Order
mL mL Height, mm O.D., mm Code Each
5,000 100 457 152 6228-05 336.30
10,000 100 457 223 6228-10 532.31
15,000 500 390 260 6231-21 502.02
20,000 500 430 285 6231-27 552.35
6233 BIG JAR 6233

Cylindrical jars with side indents for easier handling. Made of heavy wall glass, the jars are
graduated and come with pour spout. Caution: Do not apply open flame or heat. Also
available with poly safety coating.
Subdiv., Approx.
Capacity, L mL Height, mm O.D., mm Order Code Each
7.25 500 254 222 6233-07 487.35
9.25 500 254 257 6233-09 557.00
17 1,000 305 305 6233-17 635.49
26.5 2,000 457 305 6233-26 778.53
32 2,000 305 406 6233-32 1263.38

234 Accessories
6472 SPRAYER Clean-In-Place
6472-210 Designed for cleaning ACE reactors without dismantling, or Clean-In-Place (CIP). One
moving part, a rotating disc at end of extension, produces heavy droplets in a 39-inch
diameter, 360° pattern to simultaneously cover entire surface of reactor. Rotating disc is
constructed of carbon-filled PTFE and stainless steel.
Wash fluid enters through a series of holes onto a precision- Pressure Flow Rate
shaped disc. The disc rotates freely at high speed and the (PSI) L/Min GPM
wash fluid is distributed in a dense spray. Can be operated 15 16 4.22
in any position. Working pressure is 15-60 psi; maximum 20 19 5.01
temperature is 120°C. For pressure and flow rates, see chart 30 23 6.07
at right. Fits through openings as small as 1-1/8-inch diameter, 40 26 6.86
including a  45/50 outer joint. Assembly consists of spray 50 29 7.65
disc, stainless steel coupling, extension tube, elbow, nipple, 60 33 8.71
and a  45/50 inner to #15 Ace‑Thred glass adapter with a
nylon bushing and FETFE o‑ring.

Spray Disc, 1/4-inch MPT 6472-200 623.81 Nipple, 1/4-inch MPT 6472-208 3.60
Coupling, 1/4-inch FPT 6472-201 8.45 Adapter, Glass, 45/50–#15 8042-21 50.57
Ext. Tube, 24-inch, 1/4-inch MPT 6472-204 32.51 Nylon Bushing & O‑Ring, #15 7506-06 12.35
Elbow, 1/4-inch FPT 6472-206 9.29 COMPLETE 6472-210 740.58
6472 SIDE SHELF Pilot Plant Support Stand

Removable side shelf add-on for ACE pilot plant reactor support stands. Suitable for
placement of motor controllers, temperature controllers, relay units, etc. The black
powder-coated aluminum plate has a 3/8-inch wide x 3/8-inch high ledge to prevent
items from falling or sliding off. Attaches to stand with galvanized iron clamp-on tee with
set screws and backing bolt.
For Support Shelf Size Order

Stand Reactor Capacity/Type (W x L, in.) Code Each
6473-34,-35, -36 100 & 150 Liter Cylindrical 12 x 28 6472-343 288.23
6472-37 200 Liter Cylindrical 12 x 32 6472-344 307.61
6474-370 50 Liter Spherical 12 x 26 6472-342 273.82
6472-342 6474-371 72 Liter Spherical 12 x 32 6472-344 307.61
6517 CLAMP Quick Release

Stainless steel quick release clamp for use with reaction flasks and heads with
Schott-Duran flanges. Available with or without extension rod, 5/8-inch O.D. x
12-inch long for clamping to a support frame. Welded extension is used to stabilize
reaction assemblies. Note: Reactors should be supported from below in usual
manner — namely mantles, rings, jacks, etc.
WITHOUT EXTENSION WITH EXTENSION
For Flange Size Order Code Each Order Code Each
6517-54, 56, 60 60 mm 6517-22 87.08 —
100 mm (4-inches) 6517-25 98.23 6517-54 158.10
120 mm (4.8-inches) 6517-24 114.57 —
6517-22, 25, 27, 31 150 mm (6-inches) 6517-27 117.67 6517-56 172.33
200 mm (8-inches) 6517-31 145.09 6517-60 199.11
6496 STANDARD CLAMP

6496
Anodized aluminum clamp with three stainless steel swing bolts and removable back
arm for attaching to racks. Clamp slides open to accommodate flasks. Used with 15305
conical flanges.
Qty. Order Code Each

Complete 1 6496-10 216.45
Extra Liners, only Set of 4 6496-30 20.00
Accessories 235
6508/6510 CLAMP
For use with all flat style flanges. 6508
For I.D., mm Order Code Each For I.D., mm Order Code Each
6510
100 6508-06 225.58 100 6510-05 169.50
130 6508-11 244.27 130 6510-10 192.87
6509 CLAMP
Positive, two-piece clamp with PTFE liner for securing the 76mm or 102mm size 7519 filter
support assembly. Bolt head is flanged to secure top half as bolt is threaded into bottom half. 6509
76mm 6509-03 142.49
102mm 6509-05 135.03
7669 CLAMPS Pinch Type, Stainless Steel

All stainless steel pinch clamps for use with O‑Ring spherical joints and ball and socket
joints. Sizes 12 and 18 are available either spring loaded or with a screw-locking device.
All other sizes have the screw-locking feature. Only screw-locking clamps should be
used with O‑Ring spherical joints.
7669
Spring Loaded
Size No. Joint Size Order Code Each
12 12/5 7669-03 7.79
18 18/9 7669-05 8.64
With Screw-Locking Device
12 12/5 7669-08 14.30
18 18/9 7669-10 14.33
28 28/15 7669-12 16.57
35 35/25 7669-14 18.51
40 — 7669-16 41.45
50 50/30 7669-18 32.03
65 65/40 7669-20 35.90
75 75/50 7669-22 72.92
102 102/75 7669-26 246.61
6495 GASKET PTFE
PTFE gaskets, white in color, for mating ground flange surfaces on reactor flasks and
matching heads. Can be used with all conical style and flat flange style flask and heads.
PTFE makes a leak-free seal with slight clamp pressure. They also provide the added 6495-10
chemical resistance and purity of PTFE.
6495-21
0.03/0.8 5.250 (133.4) 500-3000mL No 6495-10 11.28
0.03/0.8 5.375 (136.7) 500-1000mL Yes 6495-21 60.28
0.03/0.8 6.625 (168.4) 2000-4000mL Yes 6495-23 64.15
6495 GASKET FETFE
ACE FETFE gaskets, black in color, for mating ground flange surfaces on reactor flasks
and matching heads. Can be used with all conical style and flat flange style flask and
heads. FETFE makes a leak-free seal with clamp pressure. FETFE is an exclusive
6495-43 ACE product made from TFE impregnated fluoroelastomers with good chemical and
temperature resistance.
0.02/0.5 5.375 (136.7) 500-1000mL Yes 6495-43 19.53
0.02/0.5 6.625 (168.4) 2000-1000mL Yes 6495-47 20.12

236 Accessories
7855 O‑RING Replacement
Replacement o‑rings for use with 6310, 6521, 6522, 6523, 6533, 6535, 6536, 6537, 6540,
6469, and 6472 only reaction flasks with groove in ground flange.
7855 For Flange CAPFE Silicone

I.D., mm (In.). Order Code Each Order Code Each
60 (2) 7855-878 28.10 7855-251 13.76
100 (4) 7855-880 28.63 7855-254 21.39
150 (6) 7855-881 59.65 7855-260 40.00
200 (8) 7855-884 75.27 7855-288 49.76
11081 CLAMP HOLDER Pilot Plant

Used with 11065 versatile jaw clamp to secure condenser, etc., on 6472 pilot plant
reactor. Holder clamps to 1-inch bar frame of reactor stand; 11065 clamp is held in
clamp holder with thumb screw. Vertical hole to accommodate straight bar or clamp.
Fabricated of aluminum, epoxy powder coated black.
Order Code Each

11081-21 84.80
11081
11079 CLAMP Chain

Fast, sure way to secure large equipment to rods and lattices. Holds 76 to 165mm bottles,
flasks, and large objects. Loop steel chain around object. Attach to hook on movable
slide. Tighten slide with large nonslip knob. Holds equipment firmly in place at any angle.
You can vary distance from support rod.
Length (In.) For Vessel OD Order Code Each

7.4 170mm 11079-24 51.23
11079
8.11 280mm 11079-38 75.28
15.12 280mm 11079-40 79.46
11080 11080 CLAMP HOLDER Regular

Normally used to hold the Nos. 11065 through 11072 clamps to rods and lab frame
supports. Made of heavily nickel-plated zinc. Will grip rods up to and including 19mm
diameter. Attaches clamp at right angle.
Order Code Each

11080-19 18.82
12100 TILTING SUPPORT

Tilting support provides a finger-tip method of emptying flasks by pouring. Mantle support
ring may be adjusted to and locked at any convenient height. Upper cross member
strengthens assembly; serves as stop for tilted mantle. Base is compact, 91 x 98cm, but
extremely stable. Complete item sold with one set of rings.
For Flask
Size, mL Order Code Each Order Code Each
12000 12100-04 567.00 12100-34 1465.00
22000 12100-07 567.00 12100-38 1479.00
50000 12100-11 567.00 12100-42 1479.00
72000 12100-15 567.00 12100-46 1667.00 12100
Accessories 237
12094 EXTENSION SUPPORT 12094

Provide convenient supports for flasks up to five-liter capacity. Generally used with flasks
having aluminum housing.
Flask Cap., mL Order Code Each Flask Cap., mL Order Code Each
50-200 12094-02 79.00 2000/3000 12094-08 90.00
250-500 12094-04 83.00 5000 12094-12 90.00
1000 12094-06 86.00
13010 CLAMP Recirculator Hose Support, Stainless Steel

All stainless steel, fully adjustable clamp for securing and supporting circulator hoses
used with jacketed pilot plants. The universal clamp adjust to any pipe style pilot plant
stand, and the clip will accommodate any standard circulator hose size.
Order Code Each
13010-01 112.28
13010
12096 TRIPOD SUPPORT

For 5L, 12L and 22L heating mantles with soft glass outer covering instead of spun aluminum.
Flask Capacity, mL Order Code Each

5,000 12096-05 208.00
12,000 12096-10 214.00
22,000 12096-14 227.00
12096

For 3,000mL- 72,000mL Glas-Col Mantles.

3,000 12097-04 107.00
5,000 12097-06 111.00
12,000 12097-08 139.00
22,000 12097-10 186.00 12097-04
50,000 12097-12 201.00
72,000 12097-14 233.00

Support for 12 through 72-liter Glas-Col heating mantles. Adjustable height 24 to 36
inches in 3-inch increments. Twenty four (24) inches wide at base.

12,000 12097-45 467.00
22,000 12097-47 492.00
50,000 12097-49 521.00
72,000 12097-51 532.00
12097-47

238 Accessories
13219 CONTAINMENT TRAY Stainless Steel

13219 Trays are heavy 14-gauge, 304 stainless steel. For safe containment of spills from larger
reactors, see recommended sizes below.
Size (LxWxH, For Vessel or
inches) Reactor Size Order Code Each
24 x 24 x 2 10, 20L 13219-03 Call
24 x 24 x 3 3 post/30L 13219-05 Call
28 x 28 x 3 30, 50L 13219-07 Call
28 x 28 x 4 100, 150L 13219-09 Call
36 x 36 x 5 72, 100, 150, 200L 13219-11 Call
13220 CONTAINMENT TRAY Low Density Polyethylene

13220-16 Trays are made of rugged, molded Low Density Polyethylene (LDPE).
23 x 21 x 2 10L 13220-16 85.51
24 x 24 x 3 20L 13220-18 121.75
24 x 24 x 4 36L 13220-20 153.56
26 x 20 x 4 30L 13220-22 125.22
30 x 28 x 4 50L 13220-24 162.39
51 x 31 x 4 100L 13220-26 190.03
13220 CONTAINMENT TRAY Low Density Polyethylene, w/Spigot

13220-37
Trays are made of rugged, molded Low Density Polyethylene (LDPE). Models listed below
feature a wide lip at the top and a 1/2-inch spigot for easy draining of fluids.
12 x 16 x 3 up to 2L 13220-33 115.50
16 x 20 x 3 up to 6L 13220-35 120.70
21.5 x 25.5 x 4 up to 10L 13220-37 154.60
17.5 x 23.5 x 6 up to 20L 13220-39 178.95
12187 ADAPTERS Stainless Steel, Circulator Hose

304 stainless steel adapters designed for use with ACE jacketed glass pilot plant reactors 12187-100
and circulator hoses for popular circulating chillers. Connects o‑ring ball joints on jacket
inlet/outlet to hoses to/from circulator.
Order
Description Code Each
Adapter, flask to hose, Stainless Steel, 28/15 Socket to M16x1 Male 12187-05 88.40
Adapter, flask to hose, Stainless Steel, 35/25 Socket to M38x1.5 Male 12187-14 93.60
Adapter, Hose to Circulator, Stainless Steel, M16x1 Male to 3/4 inch NPT Male 12187-100 93.60 12187-05
Adapter, Hose to Circulator, Stainless Steel, M30x1.5 Male to 3/4 inch NPT Male 12187-101 93.60
Adpater, Hose to Circulator, Stainless Steel, M24x1.5 Male to 3/4 inch NPT Male 12187-102 93.60
12187 CLAMP Stainless Steel, Circulator Hose

304 stainless steel clamp designed for use with ACE jacketed glass pilot plant reactors
and circulator hoses for popular circulating chillers. Connects glass o‑ring ball joints on
jacket inlet/outlet to hoses to/from circulator. Powder coated aluminum with glass-filled
PTFE backing.

12187-28
28/15 12187-28 124.80
35/25 12187-35 135.20
Accessories 239
10015 PRESSURE RELIEF MANIFOLD for ACE Pilot Plants

This pressure relief manifold is designed to fit into process systems between the circulator
and the glass reaction vessel for added protection and safety. The manifold gives further
protection to the glass vessel itself and the vessel inlet fittings and alleviates excess
pressure build-up that could damage the reactor. Most circulators have an excess pressure
relief built-in, but may not be able to react fast enough to protect the glass. The system
is supplied complete with the anodized aluminum body-clamp, outlet connections and
hoses, inlet pressure gauge, relief valve assembly, which is factory preset and sealed at
10 PSI. The manifold will fit 10L and larger pilot plant systems.
See separate hose listings by manufacturer for inlet/outlet hoses and connector fittings.
See also stainless steel fittings to match to 3/4-in. female manifold inlet.
Order Code Each 10015

10015-10 2741.31
8250 STOPPERS Full Length

Sizes  7/25 and  10/30 are solid, all others are hollow.
Size Order Code Each Size Order Code Each

7/25 8250-02 14.40 29/42 8250-14 25.05
10/30 8250-04 15.28 34/45 8250-16 31.81
12/30 8250-06 15.40 45/50 8250-20 44.68
14/35 8250-08 18.53 55/50 8250-24 56.66
8250
19/38 8250-10 19.45 71/60 8250-28 161.88
24/40 8250-12 19.79
12631 STOPPERS PTFE,

Standard taper stoppers made of solid PTFE.

7/10 12631-02 11.51
12631 7/25 12631-03 11.55
10/10 12631-04 11.52
14/10 12631-06 11.55
14/20 12631-07 15.15
19/22 12631-09 16.97
24/25 12631-15 21.00
29/26 12631-17 29.24
12633 STOPPERS PTFE,

Standard taper, PTFE stoppers with easy-to-grip handle. Codes -05 and -09 are solid,
12633 all others are hollow.

14/20 12633-05 13.80
19/22 12633-09 14.55
24/25 12633-12 21.57
24/40 12633-15 21.70
29/42 12633-17 22.40
45/50 12633-23 71.00
12634 STOPPERS PTFE

Virgin TFE/PTFE stoppers with built-in black Delrin stopper extractor ring. Eliminates the
hazard of removing a frozen stopper from glass vessel. You need only turn red nut clock-
wise to exert a gentle force against the vessel’s lip and the non-stick stopper is extracted.
Stopper
Size Qty. Order Code Per Pkg.
19/22 3 12634-16 104.95
12634 24/40 2 12634-20 108.65
29/42 2 12634-24 122.55

240 Accessories
O-Rings 241
VITON A — A linear copolymer of Vinylidine Fluoride and Hexafluoropropylene.

SILICONE — A group of elastomeric materials made from Silicone, Hydrogen and Carbon.
BUNA-N — A copolymer of Butadiene and Acrylonitrile.
FETFE® — A fluoroelastomer with special TFE Additives.
EPDM (ETHYLENE-PROPYLENE) — An elastomer prepared from Ethylene and Propylene Monomers.
7855 O‑RINGS lu
e
Va
Dimensions VITON Per SILICONE Per BUNA-N Per FETFE Per EPDM Per
Size I.D.,mm W. Qty. Order Code Pkg. Order Code Pkg. Order Code Pkg. Order Code Pkg Order Code Pkg.
-006 2.9 1.78 12 7855-01 10.69 7855-201 13.71 7855-401 4.48 7855-701 13.19 — —
-007 3.7 1.78 12 7855-02 11.06 7855-202 13.85 7855-402 4.48 7855-702 13.11 — —
-008 4.5 1.78 12 7855-04 11.21 7855-204 14.78 7855-404 4.69 7855-704 13.68 7855-904 14.58
-009 5.3 1.78 12 7855-07 11.66 7855-207 15.45 7855-407 4.69 7855-707 14.77 — —
-010 6.1 1.78 12 7855-05 11.75 7855-205 15.21 7855-405 4.69 7855-705 14.78 — —
-011 7.7 1.78 12 7855-06 11.81 7855-206 15.45 7855-406 4.69 7855-706 14.77 7855-906 14.58
-012 9.2 1.78 12 7855-08 11.77 7855-208 15.97 7855-408 4.69 7855-708 15.45 7855-908 14.42
-013 10.8 1.78 12 7855-10 12.26 7855-210 16.30 7855-410 4.73 7855-710 15.45 7855-910 15.46
-014 12.4 1.78 12 7855-12 12.93 7855-212 15.97 7855-412 4.69 7855-712 15.94 7855-912 15.45
-015 14.0 1.78 12 7855-13 14.50 7855-213 17.25 7855-413 7.23 7855-713 17.16 — —
-016 15.6 1.78 12 7855-14 14.27 7855-214 17.17 7855-414 7.23 7855-714 17.07 7855-914 16.03
-018 18.8 1.78 12 7855-15 15.45 7855-215 18.26 7855-415 7.49 7855-715 19.10 — —
-021 23.5 1.78 12 7855-19 20.20 7855-219 22.40 7855-419 7.52 7855-719 19.18 — —
-022 25.1 1.78 12 7855-17 20.05 7855-217 22.07 7855-417 7.52 7855-717 18.32 — —
-105 3.6 2.6 12 7855-03 15.67 7855-203 16.38 7855-403 4.46 7855-703 20.06 — —
-107 5.2 2.6 12 7855-09 15.66 7855-209 15.91 7855-409 4.54 7855-709 20.59 — —
-108 6.0 2.6 12 7855-11 15.77 7855-211 16.38 7855-411 4.91 7855-711 19.85 — —
-110 9.2 2.6 12 7855-16 15.66 7855-216 16.10 7855-416 5.06 7855-716 19.78 7855-916 18.94
-111 10.8 2.6 12 7855-18 15.54 7855-218 16.42 7855-418 5.06 7855-718 20.46 — —
-112 12.4 2.6 12 7855-20 16.62 7855-220 16.85 7855-420 5.06 7855-720 21.62 — —
-113 13.9 2.6 12 7855-21 18.46 7855-221 17.17 7855-421 5.06 7855-721 23.76 — —
-114 15.5 2.6 12 7855-22 18.36 7855-222 17.28 7855-422 5.14 7855-722 24.88 7855-922 21.74
-115 17.1 2.6 12 7855-24 19.55 7855-224 17.32 7855-424 5.65 7855-724 26.89 — —
-116 18.7 2.6 12 7855-26 20.60 7855-226 17.89 7855-426 5.65 7855-726 26.57 7855-926 25.49
-118 21.9 2.6 12 7855-70 22.44 7855-270 19.35 7855-470 6.11 7855-770 31.64 — —
-121 26.6 2.6 12 7855-27 27.52 7855-227 26.30 7855-427 5.63 7855-727 34.55 7855-927 31.55
-122 28.2 2.6 6 7855-71 14.33 7855-271 11.12 7855-471 4.45 7855-771 18.39 — —
-123 29.8 2.6 6 7855-28 14.55 7855-228 13.60 7855-428 4.48 7855-728 20.19 7855-928 15.79
-125 33.0 2.6 6 7855-72 14.66 7855-272 13.39 7855-472 4.46 7855-772 20.31 — —
-127 36.2 2.6 6 7855-76 15.09 7855-276 16.28 7855-476 4.52 7855-776 19.37 — —
-128 37.8 2.6 6 7855-73 15.05 7855-273 16.48 7855-473 4.57 7855-773 19.41 — —
-136 50.5 2.6 6 7855-29 15.20 7855-229 15.22 7855-429 5.06 7855-729 19.70 7855-929 17.51
-210 18.6 3.5 6 7855-30 13.48 7855-230 15.71 7855-430 4.69 7855-730 17.57 7855-930 15.50
-211 20.2 3.5 6 7855-32 14.66 7855-232 15.93 7855-432 4.69 7855-732 18.65 7855-932 15.50
-212 21.8 3.5 6 7855-34 16.03 7855-234 15.69 7855-434 4.69 7855-734 20.14 7855-934 15.33
-213 23.3 3.5 6 7855-36 16.01 7855-236 15.75 7855-436 4.76 7855-736 20.17 — —
-214 25.0 3.5 6 7855-38 18.48 7855-238 15.99 7855-438 4.85 7855-738 24.80 7855-938 38.11
-215 26.6 3.5 6 7855-37 25.61 — — 7855-437 4.90 — — — —
-216 28.2 3.5 6 7855-39 25.41 7855-239 16.10 7855-439 4.90 7855-739 27.47 7855-939 39.29
-217 29.7 3.5 6 7855-40 25.45 7855-240 16.01 7855-440 4.90 7855-740 28.21 — —
-218 31.3 3.5 6 7855-41 25.66 — — 7855-441 4.91 — — — —
-219 33.0 3.5 6 7855-43 25.69 — — 7855-443 4.91 — — — —
-220 34.5 3.5 6 7855-42 25.57 7855-242 16.20 7855-442 4.95 7855-742 33.91 7855-942 16.56
-221 36.1 3.5 6 7855-51 25.62 — — 7855-451 4.91 — — — —
-222 37.7 3.5 6 7855-52 25.70 — — 7855-452 4.91 — — — —
-223 40.9 3.5 3 7855-74 14.69 7855-274 6.10 7855-474 2.80 7855-774 18.72 — —
-225 47.2 3.5 3 7855-44 16.69 7855-244 8.85 7855-444 3.23 7855-744 21.20 7855-944 12.24
-226 50.4 3.5 3 7855-46 17.46 7855-246 8.78 7855-446 4.48 7855-746 24.45 7855-946 12.81
-227 53.6 3.5 3 7855-45 18.20 7855-245 8.72 7855-445 4.48 7855-745 23.38 — —
-228 56.7 3.5 3 7855-47 19.55 7855-247 9.04 7855-447 4.48 7855-747 25.28 — —
-229 59.9 3.5 3 7855-48 20.07 7855-248 9.50 7855-448 4.48 7855-748 26.05 7855-948 13.13
-230 63.1 3.5 3 7855-75 21.10 7855-275 21.23 7855-475 4.57 7855-775 29.44 7855-975 15.78
Continued on following page

242 O-Rings
VITON A — A linear copolymer of Vinylidine Fluoride and Hexafluoropropylene.

SILICONE — A group of elastomeric materials made from Silicone, Hydrogen and Carbon.
BUNA-N — A copolymer of Butadiene and Acrylonitrile.
FETFE® — A fluoroelastomer with special TFE Additives.
EPDM (ETHYLENE-PROPYLENE) — An elastomer prepared from Ethylene and Propylene Monomers.
e
7855 O‑RINGS (listing continued from previous page) lu
Va
Dimensions VITON Per SILICONE Per BUNA-N Per FETFE Per EPDM Per
Size I.D.,mm W. Qty. Order Code Pkg. Order Code Pkg. Order Code Pkg. Order Code Pkg Order Code Pkg.
-233 72.6 3.5 3 — — — — — — 7855-778 29.40 — —
-235 78.9 3.5 3 7855-64 22.39 7855-264 10.06 7855-464 Call 7855-764 31.67 — —
-239 91.7 3.5 3 7855-69 Call — — — — — — — —
-240 94.9 3.5 3 7855-78 Call — — — — — — — —
-325 37.5 5.3 6 7855-65 28.79 — — 7855-453 5.50 — — — —
-326 40.6 5.3 6 7855-67 28.75 — — 7855-454 5.50 — — — —
-327 43.8 5.3 6 7855-68 28.62 7855-278 16.82 7855-455 5.50 — — — —
-329 50.2 5.3 3 — — 7855-283 17.20 — — 7855-783 40.56 — —
-335 69.2 5.3 3 — — — — 7855-499 146.28 — — — —
-336 72.4 5.3 3 7855-82 35.47 7855-282 18.60 — — 7855-782 48.61 — —
-338 78.7 5.3 3 7855-77 38.38 7855-277 19.32 — — 7855-777 55.09 — —
-341 88.3 5.3 3 7855-50 47.73 7855-250 19.97 7855-450 4.66 7855-750 63.72 — —
-343 94.6 5.3 3 7855-66 52.71 7855-266 21.73 — — 7855-766 63.72 — —
-348 110.5 5.3 3 7855-79 87.63 — — — — 7855-779 63.72 — —
-349 113.7 5.3 3 — — 7855-287 22.38 — — 7855-787 65.78 — —
-359 145.4 5.3 3 — — 7855-289 25.32 — — — — — —
5-101 2.5 0.97 12 7855-80 18.09 — — — — — — — —
2-105 12 7855-303 Call — — — — — — — —
5-193 4.5 1.0 12 7855-81 Call 7855-281 Call — — — — — —
5-017 6.1 2.6 12 — — — — 7855-482 Call — — — —
— 75.5 4.0 1 — — 7855-251 13.76 — — — — — —
— 110.0 5.0 1 — — 7855-254 21.39 — — — — — —
— 150.0 5.0 1 — — 7855-260 40.00 — — — — — —
— 215.0 5.0 1 — — 7855-288 49.76 — — — — — —
O‑Ring Kits — 30 Sizes 500 7855-99 244.86 — — 7855-499 146.28 — — — —
O‑Ring Sets: one box of 18 sets — — — — — — 8194-310 69.34 — —
*Sizes not listed are available via special order. Call or email for quotation.
CHEMICAL COMPATIBILITY CHART

Key: 1=Recommended; 2=Satistfactory; 3=Poor; 4=Marginal; 5=Not Recommended; A=Acceptable; NA=Not Acceptable
Viton Silicone Buna-N EPDM Chemraz 514 Kalrez 4079 FETFE CAPFE
Temperature Range °C –26 to 204 –62 to 204 –37 to 121 –54 to 149 –30 to 220 –15 to 316 –18 to 204 –60 to 204
Compression set 2 2 2 2 2 2 2 3
Durometer 75 70 70 70 70 75 70 70
Steam < 120 °C 3 4 4 4 1 1 1 5
Acetone 4 3 3 2 1 1 5 1
Toluene 2 3 3 3 1 1 2 2
Tetrachloroethane 1 3 3 3 1 1 1 2
THF 4 4 4 4 1 1 5 3
Methyl Ethyl Ketone 5 5 5 2 1 1 5 2
Acetonitrile 5 5 5 5 1 1 5 2
Hydrochloric Acid (conc) 2 5 4 5 1 1 2 4
Ammonia Gas (cold) 4 1 2 2 1 1 4 2
Tetrachloroethylene 3 5 3 3 1 1 3 2
Sulfuric Acid (dilute) 2 5 1 5 2 2 2 2
Nitric Acid (conc) 2 5 4 5 1 1 2 4
Calcium Carbonate 2 5 1 1 1 1 2 2
Xylene 2 4 4 3 1 1 2 2
Mineral Oils 1 2 1 4 1 1 1 1
Sodium Carbonate 1 1 1 1 1 1 1 2
Vacuum 1 4 2 4 4 4 1 2
FDA A A A A NA NA NA A
Chemical compatibility information courtesy of the respective manufacturers of each o-ring type. Ace is not responsible for errors.
O-Rings 243
ACE Exclusive!
CAPFE — A “Rubbery” PTFE O‑Ring • Low friction
• High chemical resistance
7855 O‑RINGS CAPFE • Low compression set compared to
A totally different O‑Ring having a resilient rubber core encased in a continu- solid PTFE O‑Rings
ous, thick, non-porous FEP/PTFE encapsulation. This unique O‑Ring solves
the sealing problems where the chemical inertness of PTFE is a MUST and • Low gas and water vapor
where maintenance-free dependability and long service life are required. permeability compared to “flash”
coated O‑Rings
CAPFE Advantages
Chemically
• Continuous encapsulation of thick, pure • Resistant to all chemicals except molten Resistant
PTFE offers no seams or weak spots to alkali metals, hot fluorine and certain PTFE
break and leak. complex halogenated compounds. Encapsulation
• CAPFE offers both resilience and chemical • Extreme slipperiness of PTFE reduces
resistance. friction in dynamic applications.
• Thick PTFE encapsulation permits wide • CAPFE ranges from –60°C to +204°C,
application without leakage or deterioration. deterioration vacuum to 10,000 psi. Resilient
Rubber Core
Dimensions Dimensions
Size I.D.,mm W., mm Order Code Each Size I.D.,mm W.,mm Order Code Each
e
-010
-011
5.3
6.1
1.78
1.78
7855-805
7855-806
15.87
16.79
-213
-214
23.4
25.0
3.5
3.5
7855-836
7855-838
Call
22.79 Valu
-012 7.7 1.78 7855-808 17.85 -217 29.7 3.5 7855-840 22.88
-013 9.2 1.78 7855-810 19.51 -220 34.5 3.5 7855-842 22.88
-015 12.4 1.78 7855-813 17.39 -223 40.9 3.5 7855-874 26.72
-018 17.7 1.78 7855-815 19.94 -225 47.2 3.5 7855-844 26.72
-021* 22.0 1.78 7855-819 19.94 -226 50.4 3.5 7855-846 26.72
-022 23.5 1.78 7855-817 19.94 -227 53.6 3.5 7855-845 27.54
-110 9.2 2.6 7855-816 15.53 -228 56.7 3.5 7855-847 27.54
-111 10.8 2.6 7855-818 16.79 -229 59.9 3.5 7855-848 27.54
-112 12.4 2.6 7855-820 16.48 -230 63.1 3.5 7855-875 27.54
-113 13.9 2.6 7855-821 17.57 -232 69.4 3.5 7855-877 27.54
-114 15.5 2.6 7855-822 17.57 -235 78.9 3.5 7855-864 28.62
-115 17.1 2.6 7855-824 17.57 — 134.37 3.5 7855-885 35.07
-116 18.7 2.6 7855-826 17.57 -317 23.2 5.3 7855-860 30.70
-118 21.9 2.6 7855-870 19.29 -329 50.2 5.3 7855-883 29.07
-121 26.6 2.6 7855-827 19.29 -341 88.3 5.3 7855-850 33.84
-122 28.2 2.6 7855-871 19.29 -348 110.5 5.3 7855-879 51.96
-123 29.8 2.6 7855-828 19.29 -349 113.7 5.3 7855-887 52.49
-125 33.0 2.6 7855-872 20.57 -359 145.4 5.3 7855-889 56.31
-127 36.2 2.6 7855-876 20.57 -361 151.8 5.3 7855-861 63.29
-128 37.8 2.6 7855-873 20.57 — 75.0 4.0 7855-878 28.10
-136 50.5 2.6 7855-829 23.39 — 110.0 5.0 7855-880 28.63
-210 18.6 3.5 7855-830 20.67 — 150.0 5.0 7855-881 59.65
-211 20.2 3.5 7855-832 20.67 — 215.0 5.0 7855-884 75.27
-212 21.8 3.5 7855-834 20.67
BEFORE DURING AFTER

TYPE OF SEAL COMPRESSION COMPRESSION COMPRESSION EFFECT
CAPFE “bounces” back—
➧
CAPFE O‑RING retains sealing capability

like elastomeric ring.
➧

244 O-Rings
KALREZ ® 4079
7855 KALREZ 4079 O‑RINGS
Offer the resilience and sealing force of an elastomer with
chemical inertness and thermal stability similar to PTFE
fluorocarbon resin.
Sealing Performance
Dim., mm Order Per
• Compared with other elastomers, KALREZ is normally more resistant
to swelling and embrittlement and will retain these properties for a Size I.D. W Code Pkg. (Use)
longer period of time. -006 2.6 1.78 7855-601 38.44
-007 2.9 1.78 7855-602 38.41 (S)
• Compared with metal seals, KALREZ is easily installed and conforms -008 3.7 1.78 7855-604 42.11 (T,C,S)
to the sealing surface despite irregularities due to improper assembly -009 4.5 1.78 7855-607 43.34
or wear. -010 5.3 1.78 7855-605 44.52
• Compared with PTFE seals, KALREZ is not likely to creep or cold flow. -011 6.1 1.78 7855-606 44.17 (T,J,S)
-012 7.7 1.78 7855-608 44.97 (C,T,J)
Chemical Resistance -013 9.2 1.78 7855-610 46.66 (C,T)
-014 10.8 1.78 7855-612 47.85 (O)
KALREZ has excellent chemical resistance, far above that of other
-015 12.4 1.78 7855-613 33.55 (O,G)
commercial elastomers. KALREZ should be considered for service in
-016 15.6 1.78 7855-614 51.77 (T,J)
hot, corrosive environments, including:
-018 18.8 1.78 7855-615 49.01 (J,S)
• Polar solvents (ketones, esters, ethers) -110 9.2 2.6 7855-616 79.58 (J,S)
• Strong organic solvents (benzene, dimethyl formamide, -021 23.5 1.78 7855-617 62.93 (C,T,G)
perchloroethylene, tetrahydrofuran (THF) -111 10.8 2.6 7855-618 71.84 (C,T,S)
-022 25.1 1.78 7855-619 64.25 (C,T,G)
• Inorganic and organic acids (hydrochloric, nitric, sulfuric, -112 12.4 2.6 7855-620 90.10
trichloroacetic) and bases (hot caustic soda) -113 13.9 2.6 7855-621 75.60
• Strong oxidizing agents (dinitrogen tetroxide, fuming nitric acid) -114 15.5 2.6 7855-622 112.39 (J,S)
-115 17.1 2.6 7855-623 91.63
• Metal halogen compounds (titanium tetrachloride, diethylaluminum
-116 18.7 2.6 7855-626 104.23 (C,T,G)
chloride)
-121 26.6 2.6 7855-627 139.74 (C,T,G)
• Hot mercury/caustic soda -136 50.5 2.6 7855-629 333.16 (C,T,G)
• Chlorine, wet or dry -210 18.6 3.5 7855-630 197.70
-211 20.2 3.5 7855-632 200.92 (T,G)
• Inorganic salt solutions -212 21.8 3.5 7855-634 169.41 (T)
• Fuels, (ASTM Reference Fuel C, JP-5 Jet Fuel, aviation gas, kerosene) -217 29.7 3.5 7855-640 194.56 (C,T,G)
-220 34.5 3.5 7855-642 251.95 (T,G,J)
• Hydraulic fluids (SKYDROL1, 500A, PYDRAUL1 312, ANDEROL2
-225 47.2 3.5 7855-644 395.72 (C,T,G,J)
L-774, and transmission fluids)
-229 59.9 3.5 7855-648 482.38 (C,T,G,J)
• Heat transfer fluids (DOWTHERM3A) -105 3.6 2.6 7855-650 46.21 (C,T,G)
• Oil well sour gas (methane, hydrogen sulfide/carbon dioxide/steam) -108 6.0 2.6 7855-653 55.66 (T,G)
-118 21.9 2.6 7855-655 109.44 (O)
• Steam -122 28.2 2.6 7855-657 97.46 (C,T,J)
Thermal Stability -123 29.8 2.6 7855-658 86.16 (C,T)
-125 33.0 2.6 7855-659 97.09 (O)
KALREZ O‑Rings retain their elastic properties in long-term service at -127 36.2 2.6 7855-670 108.51 (T,J)
temperatures as high as 316°C and in intermittent service up to 327°C. -128 37.8 2.6 7855-671 109.66 (J,S)
®
Registered DUPONT Trademark -213 23.3 3.5 7855-675 97.37 (C,T,G)
1
U.S. Trademark of Solutia Co., 2U.S Trademark of Tenneco Chemicals, -214 25.0 3.5 7855-676 85.93 (T,G)
3
U.S. Trademark of Dow Chemical Co. -216 28.2 3.5 7855-677 107.77 (C,T,G)
-223 40.9 3.5 7855-680 158.72 (C,T,G,J)
-226 50.4 3.5 7855-684 163.52 (C,T,G,J)
-227 53.6 3.5 7855-685 169.46
-228 56.7 3.5 7855-686 192.32
-230 63.1 3.5 7855-689 189.54
-327 43.8 5.3 7855-690 297.53
-341 88.3 5.3 7855-691 703.41
-348 110.0 5.3 7855-692 738.57
USE REFERENCE CODES
T = Ace‑Threds S = Stopcocks C = Chromatographic Fittings
G = Gaskets J = O‑Ring Joints O = Special
O-Rings 245
CHEMRAZ ® 514 Size

Dimensions, mm
I.D. W
Order
Code
Per
Pkg. (Use)
-006 2.6 1.78 7859-501 31.37 (O)
THE WHITE O‑RING -007 2.9 1.78 7859-502 31.37 (S)
-008 3.7 1.78 7859-504 41.80 (T,C,S)
-009 4.5 1.78 7859-507 33.24 (O)
-010 5.3 1.78 7859-505 34.35 (T,J,S)
-011 6.1 1.78 7859-506 34.97 (T,J,S)
-012 7.7 1.78 7859-508 36.07 (C,T,J)
-013 9.2 1.78 7859-510 36.43 (C,T)
-014 10.8 1.78 7859-512 43.72 (O)
-015 12.4 1.78 7859-513 40.88 (J,S)
-016 14.0 1.78 7859-514 39.05 (T,J)
-018 17.7 1.78 7859-515 45.33 (J,S)
-021 22.0 1.78 7859-519 54.39 (C,T,G)
-022 23.5 1.78 7859-517 54.80 (C,T,G)
-105 3.6 2.6 7859-503 41.76 (C,T,G)
-108 6.0 2.6 7859-511 45.80 (T,G)
7859 CHEMRAZ O‑RINGS White -110 9.2 2.6 7859-516 47.17 (J,S)
Molded of a perfluoroelastomer polymer, CHEMRAZ has the broadest -111 10.8 2.6 7859-518 48.87 (C,T,S)
chemical resistance of any elastomeric material. Combines the -112 12.4 2.6 7859-520 51.87 (T,G,J)
resilience and sealing force of an elastomer with chemical resistance -113 13.9 2.6 7859-521 56.31 (C,T,G,J)
approaching that of PTFE. -114 15.5 2.6 7859-522 56.52 (J,S)
-115 17.1 2.6 7859-524 65.28 (S)
Sealing Performance -116 18.7 2.6 7859-526 65.17
-118 21.9 2.6 7859-570 72.73 (O)
• Compared with other elastomers, CHEMRAZ is normally more resistant
-121 26.6 2.6 7859-527 75.46 (C,T,G)
to swelling and embrittlement and will retain these properties for a -122 28.2 2.6 7859-571 77.16 (C,T,J)
longer period of time. -123 29.8 2.6 7859-528 81.65 (C,T)
• Compared with metal seals, CHEMRAZ is easily installed and -125 33.0 2.6 7859-572 101.18 (O)
conforms to the sealing surface despite irregularities due to improper -127 36.2 2.6 7859-576 108.65 (T,J)
assembly or wear. -128 37.8 2.6 7859-573 122.43 (J,S)
-136 50.5 2.6 7859-529 164.55 (C,T,G)
• Compared with PTFE seals, CHEMRAZ is not likely to creep or cold -210 18.6 3.5 7859-530 95.43 (J,S)
flow. -211 20.2 3.5 7859-532 95.46 (T,G)
-212 21.8 3.5 7859-534 96.98 (T)
Chemical Resistance -213 23.3 3.5 7859-536 108.05 (C,T,G)
-214 25.0 3.5 7859-538 112.41 (T,G)
CHEMRAZ has excellent chemical resistance, far above that of other -216 28.2 3.5 7859-539 145.43 (C,T.G)
commercial elastomers. CHEMRAZ should be considered for service -217 29.7 3.5 7859-540 121.58 (T,G,J)
in hot, corrosive environments including: -220 34.5 3.5 7859-542 142.13 (T,G,J)
• Polar solvents (ketones, esters, ethers) -223 40.9 3.5 7859-574 174.81 (C,T,G,J)
-225 47.2 3.5 7859-544 196.17 (C,T,G,J)
• Strong organic solvents (benzene, dimethyl formamide,
-226 50.4 3.5 7859-546 215.23
perchloroethylene, tetrahydrofuran (THF) -227 53.6 3.5 7859-545 229.30
• Inorganic and organic acids (hydrochloric, nitric, sulfuric, -228 56.7 3.5 7859-547 233.76
trichloroacetic) and bases (hot caustic soda) -229 59.9 3.5 7859-548 230.10 (C,T,G,J)
-230 63.1 3.5 7859-575 247.82
• Strong oxidizing agents (dinitrogen tetroxide, fuming nitric acid)
-327 43.8 5.3 7859-578 326.55
• Metal halogen compounds (titanium tetra-chloride, diethylaluminum -341 88.3 5.3 7859-550 607.06
chloride) -348 110.5 5.3 7859-579 779.45
• Hot mercury/caustic soda
USE REFERENCE CODES
• Chlorine, wet or dry T= Ace‑Threds S= Stopcocks C= Chromatographic Fittings
• Inorganic salt solutions G= Gaskets J= O‑Ring Joints O= Special
• Fuels, (ASTM Reference Fuel C, JP-5 Jet Fuel, aviation gas, kerosene)
• Hydraulic fluids (SKYDROL1, 500A, PYDRAUL1 312, ANDEROL2 CHEMRAZ O‑Rings retain their elastic properties longer in
L-774, and transmission fluids) harsh chemical environments at temperatures from -30°F to
• Heat transfer fluids (DOWTHERM3A) higher than 220°C.
• Oil well sour gas (methane, hydrogen sulfide/carbon dioxide/steam) ®
Chemraz is a Registered Trademark of Greene Tweed & Co.
1
U.S. Trademark of Solutia Co., 2U.S Trademark of Tenneco
• Steam Chemicals,
3
U.S. Trademark of Dow Chemical Co.
Thermal Stability

246
Recirculators & Chillers
Presto Series
Air Cooled Closed System

Circulators
Contact ACE
for complete
information
on Julabo
recirculators
and
accessories.
Presto A30 Presto A40 Presto A80

Ace Order Code Call 12262-52 12262-38
Operating Temp Range –30º to 250º –40º to 250º –80º to 250º
Temperature Stability +/– .01 to .05 +/– .01 to .05 +/– .01 to .05
Heating Capacity 2.3kW 2.3kW 1.5kW
Cooling Capacity @ 100ºC .50kW 1.2kW 1.2kW
Cooling Capacity @ 20ºC .50kW 1.2kW 1.2kW
Cooling Capacity @ 0ºC .40kW .90kW 1.2kW
Cooling Capacity @ –20ºC .20kW .60kW 1.1kW
Cooling Capacity @ –40ºC — .10kW 1.1kW
Cooling Capacity @ –60ºC — — .65kW
Flow Rate @ 10 PSI 25 LPM (7.25 PSI) 20 LPM 27 LPM
Pump Connection M24 x 1.5 Male M24 x 1.5 Male M24 x 1.5 Male
Condeser Cooling Air Cooled Air Cooled Air Cooled
Dimension (LxWxH) 9.53" x 22.95" x 24.09" 12.72" x 22.95" x 26.06" 16.93" x 25.59" x 49.53"
Weight 137 lbs 174 lbs 362 lbs
Power Requirement 208V, 1PH, 60Hz, 13.5A 208V, 1PH, 60Hz, 15A 208V, 1PH, 60Hz, 20A
Each Call 21350.00 33125.00
Recirculators & Chillers 247
Presto Series
Water Cooled Closed System

Circulators
Contact ACE
for complete
information
on Julabo
recirculators
and
accessories.
Presto W40 Presto LH50 PLUS Presto W80

Ace Order Code 12262-50 12262-40 Call
Operating Temp Range –40º to 250º –50º to 250º –80º to 250º
Temperature Stability +/– .01 to .05 +/– .01 to .05 +/– .01 to .05
Heating Capacity 2.30kW 6.00kW 1.5kW
Cooling Capacity @ 100ºC 1.20kW 5.50kW 1.20kW
Cooling Capacity @ –20ºC .60kW 2.60kW 1.10kW
Cooling Capacity @ –40ºC .10kW .50kW 1.10kW
Flow Rate @ 10 PSI 20 LPM 20 LPM 27 LPM
Pump Connection M24 x 1.5 Male M16 x 1 Male M24 x 1.5 Male
Condeser Cooling Water Cooled Water Cooled Water Cooled
Cooling Water Connection G 3/4 G 3/4 G 3/4
Dimension (LxWxH) 12.72" x 22.95" x 26.06" 15.7" x 21.7" x 50" 16.93" x 25.59" x 49.53"
Weight 172 lbs 401 lbs 351 lbs
Power Requirement 208V, 1PH, 60Hz, 15A 230V,3PH,60Hz, 27A 208V, 1PH, 60Hz, 20A
Each 22175.00 33750.00 Call

248
Magnum 91 Temperature Control System
12274 JULABO MAGNUM 91 TEMPERATURE CONTROL

SYSTEM
Standard Features:
■■ Two splash proof keypads, one remote
■■ VFD and LCD displays
■■ RS232 & 485 interfaces
■■ Water cooled
■■ 3 point calibration
■■ Rapid cool and heat-up
■■ External Pt temperature sensor
■■ Doesn’t absorb any air humidity into the bath and prevents the
formation of ice
■■ Compensates quickly for exothermic and endothermic reactions
■■ Integrated high and low temperature safety cut-off and low liquid
level
■■ Integrated warning, safety and supervision functions via 9
different sensors
■■ Built-in castors for easy mobility
■■ Electronically adjustable pump stages and pressures
Julabo Model Magnum 91

Operating Temperature Range-ºC –91 to +250
Temperature Control ICC
Temperature Stability, External-ºC ±0.05
Display Resolution-ºC 0.01
Heater Capacity-W 6000
Cooling Capacity @ –20ºC-kW 4.5
Refrigerant R404a+R23
Contact ACE for full
Fill Volume-L 21.5
information on Julabo
Overall Size, Inches 28 x 34.7 x 65
recirculators and accessories.
Weight-Lbs. 926
Pump Flow Maximum-L/min. 24-35 @ 11.6…31.9 psi
Ambient Temperature-ºC 5…40
Electrical 230v, 3p, 60Hz
ACE Order Code 12274-100
Priced upon request
Recirculators & Chillers 249
HighTech Series
12254 JULABO RECIRCULATORS/CHILLERS

Standard Features:
■■ For external applications.
■■ Simultaneous display of three temperature values
■■ Bright backlit LCD display
■■ Powerful pressure and suction pump with electronically
adjustable pump capacity
■■ RS 232 interface
■■ Temperature switchable between °C and ºF
■■ The workhorse series for pilot plants and jacketed
reaction vessels
■■ Upgrade feature
■■ Energy saving performance
■■ Front panel access and drain valve
■■ External Pt temperature senor available
12254-51
Julabo Model FP50HL FP51SL

Operating Temperature Range-ºC –50 to +200 –51 to +200
Temperature Stability-ºC 0.01 0.05
12254-33
Cooling Capacity @ 0ºC-kW 0.8 1.5
Pump Flow Maximum-L/min. 22-26 22-26
Fill Volume-L 8 11
Overall Size, Inches 16.6 x 19.3 x 28.3 18.1 x 21.6 x 35.0
Weight-Lbs. 125.4 198.4
Electrical* 230v, 60Hz 230v 3 ph, 60Hz
ACE Order Code 12254-33 12254-51
Each 9975.00 12812.00
*Ultra-low temperature series HighTechs also available down to –90ºC
14108 14108 BATH FLUIDS

New thermal series bath fluids for Julabo circulators. Available in five liter jugs. Ten liter
size available upon request. Please note fluid color, temperature ranges, and flash points
to match your circulator. Other ranges are available — just call Ace Glass!
Quantity, Temperature Flash Order
Liters Range, °C Point Color Code Each
5 –30 to +80 120 Light Yellow 14108-21 179.00
5 –60 to +250 135 Clear 14108-26 604.00
5 –90 to +170 75 Clear 14108-27 735.00
5 –90 to +60 75 Clear 14108-28 473.00
5 –60 to +110 135 Clear 14108-30 473.00

250 Recirculators & Chillers
12675 TUBING & INSULATION 12675-08

Temperature Qty., Order
Type Range, °C Meters Code Each
Viton Tubing, 8mm I.D. –50 to +200 1 12675-08 116.00
Insulation for 8 & 10mm Viton Tubing –50 to +100 1 12675-40 16.00
Insulation for 12mm Viton Tubing –50 to +100 1 12675-42 18.00
Contact ACE for other Julabo chillers

and accessories.
12675-40, -42
12677 TUBING & INSULATION For Julabo Presto Series Recirculators

Metal tubing, flexible and triple insulated, with two M24 x 1.5 female fittings. Temperature
range of –100 to +350°C.
12677
Qty., Order
Meters Code Each
1.0 12677-10 379.00
1.5 12677-15 497.00
3.0 12677-20 928.00
12299/12300 MISCELLANEOUS ACCESSORIES 12299-16

Common fittings and adapters for Julabo circulators. Additional fittings are available.
Please call ACE with your requirements.
Order 12299-28
Description Qty. Code Each
Nut M16x1 female, pair 2 12299-16 22.00
Adapter M16x1 male to M16x1 male 1 12299-20 39.00
Elbow 90° M16x1 female to M16x1 male 2 12299-25 221.00 12299-20
Adapter 1/4-inch NPT male 2 12299-28 49.00
Adapter M16x1 female to 3/8-inch NPR male 2 12300-08 89.00
Adapter M16x1 female to 1/2-inch NPR male 2 12300-12 107.00
Adapter 1/4-inch tube 2 12300-24 89.00
Adapter 3/8-inch tube 2 12300-28 89.00 12299-25
Adapter 1/2-inch tube 2 12300-30 89.00
12307 TEMPERATURE PROBES*

For all heating and refrigerated circulators equipped with a Pt100 temperature sensor
connection to measure and control the temperature of your external system.
Item Order Code Each

PLAIN Stainless Steel Sheath
Pt 100 Sensor, 12" long, ¼" O.D., with 5' Cord 12307-12 353.00
PTFE COATED Stainless Steel Sheath
Pt 100 Sensor, 12" long, ¼" O.D., with 10' Cord 12307-42 573.43
Pt 100 Sensor, 24" long, ¼" O.D., with 10' Cord —
12307-44 609.00
For 5, 10 & 20L REACTORS 12307
Pt 100 Sensor, 48" long, ¼" O.D., with 10' Cord —
12307-48 877.00
For 50L REACTOR
Extension Cable
3.5 meters long (11.5') for Pt 100 Sensors 12307-02 279.00
*Supplied with plug for connecting to Circulators.
Rotary Evaporators 251
HEIDOLPH LABOROTA 20 Control

Large-Scale Rotary Evaporators
Up to 20 Liter Capacity
For safe, unattended, large-scale distillation of any solvent or mixture
in any research lab, pilot plant or scale-up facility, the LABOROTA 20
series provides the perfect tool for basic solvent purification, recovery
and scale-up applications! Glassware
The LABOROTA 20 series has been designed to incorporate all
leading safety features, giving you trust not only in the product and
the results of the distillation, but also in the safety and well-being
of the laboratory and your sample. In addition, the LABOROTA 20
series is available with a wide range of options, including 10 different
condenser configurations from which to choose, water and oil baths
for various heat load requirements, integrated vacuum controllers and Evaporation Flask
a host of other exclusive features that offer the benefit of the most
efficient distillations and the highest recovery rates.
Product Features:
■■ Totally programmable through digital
operating panel
■■ Designed for 24-hour continuous use
■■ Condensate is automatically drained off to Digital
any receptacle Operating
■■ Auto system automatically delivers sample Panel
to evaporating flask via an intricate, Features individually
accurate sensor system programmable ramps
for all parameters
■■ Auto controlled self filling bath system
■■ Affordable alternative to 50 and 100L
evaporators
■■ Integrated vacuum sensor and valve
■■ Auto distillation capability through the use Receiving
of either the constant set-point pressure Flasks
feature (P const program) or via the vapor
temperature control feature
■■ Built-in timer can automatically stop and
start reaction
■■ Wide choice of glassware sets
■■ Three-year manufacturer’s warranty from
Heidolph
Need high-capacity cooling?

Use your Heidolph LABOROTA 20 Series Rotary Evaporator with the
Julabo Model W40 Recirculating Chiller.

252 Rotary Evaporators
Non-Fogging Safety Glass
LABOROTA 20 Control — Safety
13302-55
Metal Framed Safety Shield
13302 LARGE SCALE ROTARY EVAPORATOR Safety

Designed for maximum safety and user protection, the LABOROTA 20 Control, Safety,
includes all the features listed on page 246, and includes a safety shield and glass
panels. It is ideal for large-scale distillations where maximum protection is needed.
Its safety shield is contructed of a metal frame, and the safety glass completely
covers the bath and evaporating flask — providing excellent protection against
implosion and splashing. A safety sensor stops the rotation if the safety shield is
opened during the distillation process, and the non-fogging safety glass provides
clear, visible monitoring of the process in your evaporation flask. 230V, 60Hz.
Bath Type Glassware Style Order Code Each

Water R 13302-55 35603.05
Water R Shorty 13302-59 38080.75
Water RC 13302-63 38401.08
Water RC Shorty 13302-67 39767.42
Water A 13302-71 40440.77
Water AC 13302-75 42081.67
Water A2 13302-79 43036.14
Water A2C 13302-83 44716.27
13302 BASE/SUPPORT STAND Fits all LABOROTA 20 Units 13302

This fully maneuverable, optional base unit features removable panels for storage of
glassware, solvents or accessories.
Order Code Per Package

Base/Support Stand 13302-310 1923.76
Ask ACE how you can get this item for FREE!
Rotary Evaporators 253
HEIDOLPH LABOROTA 20 Automatic

Large-Scale Rotary Evaporators
Up to 20 Liter Capacity LABOROTA 20 Control —
Automatic
Automatic Version
Designed for unattended distillations, especially for the most demanding
production and scale-up requirements!
With the unique LABOROTA 20 Control, Automatic, solvents or samples intended for
distillation are automatically delivered into the evaporating flask via an intricate and
highly accurate sensor system that detects the need for replenishing the evaporating
flask. Throughout the distillation, the condensate is automatically drained off to any
receptacle, carboy drum or vessel of choice. Upon completion of the distillation,
and once the distillate has been collected, the LABOROTA 20 Control, Automatic
completely shuts down and prepares itself for your next application.
In addition, the self-filling, digitally controlled heating bath allows for use over an
unlimited time, including evenings and weekends, so there's no need to worry
about manually replenishing the bath liquid, either — the LABOROTA 20 Control,
Automatic does that, too!
13302 LARGE SCALE ROTARY EVAPORATOR Automatic, Economy

Unit includes all the product features listed on page 246, plus choice of water bath
with temperatures up to 100ºC for low-boiling solvents, or oil bath (available upon
request) with temperatures up to 180ºC for high boiling point solvents and more
demanding distillations. 230V, 60Hz.

Water A 13302-108 62537.41
Water A2 13302-112 65015.11
13302 LARGE SCALE ROTARY EVAPORATOR
Automatic, Safety
Designed for maximum safety and user protection, the LABOROTA 20 Control, Safety,
includes all the features listed on page 246, and also includes a safety shield and glass
panels. It is ideal for large-scale distillations where maximum protection is needed. Its
safety shield is contructed of a metal frame, and the safety glass completely covers
the bath and evaporating flask providing excellent protection against implosion and
splashing. A safety sensor stops the rotation if the safety shield is opened during the
distillation process, and the non-fogging safety glass provides clear, visible monitoring
of the process in your evaporation flask. 230V, 60Hz.

Water A 13302-208 66224.81
Water A2 13302-212 68473.43
Control Panel
Contact ACE for Bench-Scale Rotary Evaporators and

Rotary Evaporatore Glassware.

254 Replacement Glassware
Glassware Assemblies for Heidolph 13302 Rotary Evaporators

Glassware Assembly R Glassware Assembly A
This glassware assembly This glassware assembly
includes one ascending includes one descending
condenser, one 20L condenser, one expansion
evaporating flask and one vessel, one 20 L evaporating
10L receiving flask and is flask, and one 10L receiving
recommended for all flask, and is recommended
standard distillations. for solvents that tend to
splash and foam.
Also comes in a “shorty” version

that features a condenser
320mm shorter than standard
version. Distillation capacity
remains the same. Ideal for use
with hoods where height is
restricted.
Glassware Assembly A2 Glassware Assembly RC

This glassware assembly This glassware assembly is
includes one ascending and identical to Assembly R and
one descending condenser, features two receiving
one expansion vessel, one flasks.
20L evaporating flask and
one 10L receiving flask, for
low-boiling solvents and
highest recovery rates.
Also comes in a “shorty” version

that features a condenser
320mm shorter than standard
version. Distillation capacity
remains the same. Ideal for use
with hoods where height is
restricted.
Glassware Assembly AC Glassware Assembly A2C

This glassware assembly is This glassware assembly is
identical to Assembly A and identical to Assembly A2 and
features two receiving features two receiving
flasks. flasks.
Replacement Glassware 255
Replacement Items for Use with

Heidolph Rotary Evaporators
(Turn to page 246 for Rotary Evaporators)
6701 LARGE EVAPORATOR FLASKS

6701-12 Used with Heidolph 20L rotary evaporators. These large flasks are from blanks selected
for balance and quality. Necks are carefully welded to prevent “rotational whip.” Flasks
can be plastic coated upon request.
Overall Flange
Cap., Height, A B C Heidolph Order
Liters mm O.D., mm I.D., mm mm Part # Code Each
10 345 143 118 18 036303000 6701-12 394.14
20 383 143 118 18 036302990 6701-22 506.07
Valu
e
6701 LARGE RECEIVER FLASKS

6701-44
Used with Heidolph 20L rotary evaporators. This receiver flask is fabricated from blanks
selected for balance and quality. Center neck is a polished  40/25 joint; side neck is a
GL-18 thread, supplied with solid cap. At bottom is a 0-10mm Easy-Action stopcock
with a GL-18 side arm, supplied with a 3/8-inch hose connection tube. Flasks can be
plastic coated upon request.
Overall
Cap., Hght., Center Side Bottom Heidolph Order
Liters mm Neck Neck Outlet Part # Code Each
10 355 40/25 GL18 0-10mm/GL-18 03630340 6701-44 858.37
Replacement GL-18 Cap 7622-107 3.59
lue
Va
13286 VAPOR TUBE for Heidolph 4000 Series

Used as replacements with Heidolph Bench-Top Series rotary evaporators. Tube is
secured in rotary drive with low-stress plastic clip that seats into groove behind  joint.
13286-30 Available plain or with Firestone “splash guard” to protect against splash-up. The
13286-30 vapor tube comes standard with all Heidolph bench-scale rotary evaporators.
Type Joint Heidolph Part # Order Code Each

Plain 24/25 — 13286-28 76.83
Plain 24/40 036301110 13286-30 76.83
Plain 29/42 — 13286-32 79.18
Plain 45/50 — 13286-34 91.66
w/Splash Guard 24/40 — 13286-37 99.75
w/Splash Guard 29/42 — 13286-39 102.12
Color Coated Glassware

Ace Glass offers many of our existing glass vessels in various
coated versions. Flasks, Pressure Bottles, B eakers, Bottles
and many other items listed in this catalog can be amber or
color coated on request. The coating is a proprietary process
and gives excellent UV protection characteristics. Contact
ACE for more details and pricing.

3965-10,
-15
New
3965-05,
-07
3965-36,
-34
3965-30,
-32
3965-26,
3965-19, -28
-22
3965 CONDENSERS, COOLERS

Replacement borosilicate glass components for Buchi® R220, R220EX, R220SE rotary evaporators. The condensers are available
in either poly-coated or plain, non-coated versions. All condensers fit easily into the glass sets listed below. ACE also offers a
non-jacketed version of the 3965-32 lower condensate cooler. Inner ball joints include CAPFE (PTFE-encapsulated silicone rubber)
o-rings. Black caps (included) are SVL-22 threads; red cap (included) is GL-14 thread.
Fits Similar Ball/Socket
Glassware to Buchi® Fits DN Joint Uses O-Ring Order
Description Set Coated? Part No. Buchi® Models Sizes Size / Code Code Each
Triple-Coil Condenser R, D2 Yes 41159 R220, 40 –225 / 7855-844 3965-05 3114.32
Triple-Coil Condenser R, D2 No 41399 R200EX, SE 40 –225 / 7855-844 3965-07 3008.75
Triple-Coil Condenser D, D2 Yes 27308 R220 40 –225 / 7855-844 3965-10 3747.74
Triple-Coil Condenser D, D2 No 41333 R200EX, SE 40 –225 / 7855-844 3965-15 3642.17
Glass Condenser (Bullfrog) DB, DB2 Yes 27825 R220 40 –225 / 7855-844 3965-19 5273.22
Glass Condenser (Bullfrog) DB, DB2 No 46516 R220EX, SE 40 –225 / 7855-844 3965-22 5162.37
Glass Condenser (Bullfrog) RB, DB2 Yes 27824 R220 40 –225 / 7855-844 3965-26 5273.75
Glass Condenser (Bullfrog) RB, DB2 No 41458 R220 40 –225 / 7855-844 3965-28 5067.36
Condensate Cooler, Jacketed C, RB, R Yes 41162 R220 25 –217 / 7855-840 3965-30 843.50
Condensate Cooler, Jacketed C, RB, R No 46510 R220EX 25 –217 / 7855-840 3965-32 738.99
Condenser Cooler, Plain C, RB, R Yes — R220 25 –217 / 7855-840 3965-34 791.78
Condenser Cooler, Plain C, RB, R No — R220EX 25 –217 / 7855-840 3965-36 765.38
3967 EXPANSION TANK

Replacement borosilicate glass components for Buchi® R220, R220EX, R220SE rotary
evaporators. Upper expansion tanks for Buchi® glass sets available in either poly-coated
New or plain non-coated versions. DN40 ball joints on top and bottom. Inner bottom ball joint
includes 7855‑844 CAPFE (PTFE-encapsulated silicone rubber) o-ring, size –225.
Similar to
Fits Buchi® Fits Buchi® Order
Description Glassware Set Coated? Part No. Models Code Each
Expansion Tank D, D2, DB, DB2 Yes 01165 R220 3967-10 1472.70
Expansion Tank D, D2, DB, DB2 No 41442 R220EX, SE 3967-15 1367.13
3967-10,
-15
3970-15, 3970 HEAD Distribution

-18 Replacement borosilicate glass components for Buchi® R220, R220EX, R220SE
rotary evaporators. Lower distribution heads with improved design with easy to use
Ace‑Threds, PTFE stem valves. 3970-30 PTFE 0-20mm valve stem includes three
Kalrez o-rings. Stems are replaceable. Available poly-coated or plain non-coated.
Upper joint is DN40 outer ball joint. Red caps (included) are GL-14 thread; black cap
(included) is SVL-15 thread. DN25 inner ball joint on 3970‑05 and 3970‑10 includes
7855‑840 CAPFE (PTFE-encapsulated silicone rubber) o-ring, size –217. End thread
is #15 Ace‑Thred, for connection to 3978 valve assembly.
New Similar to
Fits Buchi® Fits Buchi®
Description Glassware Set Coated? Part No. Models Order Code Each
Distribution Head-R C, RB, R No 41373 R220 3970-05 1372.41
Distribution Head-R C, RB, R No 46511 R220EX, SE 3970-10 1266.84
Distribution Head-D D, D2, DB, DB2 Yes 41335 R220 3970-15 1008.19
Distribution Head-D D, D2, DB, DB2 No 41307 R220EX, SE 3970-18 902.62
Replacement 0-20mm PTFE valve stem

(only) for 3970-05 / -10 distribution
heads. Includes two 7855-626 size –116 No — R220EX, SE 3970-30 237.53
and one 7855-622 size –114 Kalrez
o-rings.
3970-05,
-10

3971 TRAPS C Set

Replacement borosilicate glass components for Buchi® R220, R220EX, R220SE 3971-03,
rotary evaporators. Inner and outer cold trap components for Buchi® C glassware Set. -05
Available poly-coated or plain non-coated. DN40 inner ball joints include 7855-844
CAPFE (PTFE-encapsulated silicone rubber) o-rings, size –225. Black cap (included)
is SVL-22 thread. Top 7855-881 CAPFE o-ring (included) for 3971‑03 and 3971‑05 is
New
for 150mm grooved top flat flange. 150mm clamp and PFA cap, listed below, must be
ordered separately.
Fits
Glassware Similar to Buchi® Fits Order
Description Set Coated? Part No. Buchi® Models Code Each
Inner Cold Trap C No 25124 220, 220EX, 220SE 3971-01 1689.12
Outer Cold Trap C Yes 25978 220 3971-03 3483.81
Outer Cold Trap C No 46518 220EX, 220SE 3971-05 3378.24
PFA Cap (Lid) C No 25979 All 3971-21 526.79
Duran Quick Clamp C No — All 6517-27 117.67
3971-01
3976 TUBES Vapor Duct Steam Tube, Glass

Replacement borosilicate glass vapor tubes for Buchi® R220, R220EX, R220SE rotary
evaporators. 3976-05 contains a Porosity C (25-50 micron) glass frit. 3976-03
Fits Similar to
Glassware Buchi® Fits Buchi®
Description Set Coated? Part No. Models Order Code Each
Vapor Duct Tube All No 41084 R220 3976-03 918.46 New
Vapor Duct Tube w/C Frit All No 41100 R220 3976-05 1055.70
3976-05
3976 TUBE Vapor Duct Steam Tube, Stainless Steel

Replacement 316 stainless steel vapor tube for Buchi® R220, R220EX, R220SE rotary
evaporators. New
Fits Similar to
Glassware Buchi® Fits Buchi® Order
Description Set Coated? Part No. Models Code Each
Vapor Duct Tube All No 41084 R220 3976-10 2164.19
3976-10
New
3973-01, -03
3973-08, -10
3973-04, -06
3973-30
3973 TUBES Connecting Tubes, Receiving

Replacement borosilicate glass tubes for Buchi® R220, R220EX, R220SE rotary evaporators. Connecting glass tubes for Buchi®
receiver assembly. Available either poly-coated or plain, non-coated. 3973-30 PTFE 0-20mm valve stem includes three Kalrez
o‑rings. See page 257 for 6726 receiver flasks. DN25 inner ball joints have 7855-840 CAPFE (PTFE-encapsulated silicone rubber)
o-rings, size –217.
Similar to Fits Buchi® Order
Description Coated? Buchi® Part No. Models Code Each
For Double Receiver Assembly
Upper Branching Piece — #1 Right, ACE Valve Yes 41048-1 R220 3973-01 791.78
Upper Branching Piece — #1 Right, ACE Valve No 41447-1 R220EX, SE 3973-03 686.21
Upper Branching Piece — #2 Left, ACE Valve Yes 41049 / 41047-2 R220 3973-04 1055.70
Upper Branching Piece — #2 Left, ACE Valve No 46520-2 R220EX, SE 3973-06 950.13
For Single Receiver Assembly
Upper Branching Piece — ACE Valve Yes 41053 R220 3973-08 791.78
Upper Branching Piece — ACE Valve No 46521 R220EX, SE 3973-10 686.21
Replacement 0-20mm PTFE valve stem (only) for 3973

branching tubes only. Includes two 7855-626 size –116 and No — All 3973-30 237.53
one 7855-622 size –114 Kalrez o-rings.

3974-25,
-27
3974-30,
3974-30,
-33 -33
3974-12,
-13
New
3974-15,
-18
3974-20,
-22
3974 TUBES Connecting, Glass Sets

Replacement borosilicate glass tubes for Buchi® R220, R220EX, R220SE rotary evaporators. Upper and lower connecting tubes for
glass distillation sets available poly-coated or plain non-coated. The 3973-20 codes through -27 have two GL14 thread ports (with
red caps) on top for thermosensor, or for easy clean out. DN40 inner ball joints on -12, -13, -20, -22, -25, and -27 include 7855-844
CAPFE (PTFE-encapsulated silicone rubber) o-rings, size –225. Bottom DN25 ball joint on -15 and -18 includes 7855-840 CAPFE
o-ring, size –217. 3974-12 and -13 both include an SVL-22 thread black cap and a GL‑14 thread red cap.
Fits Buchi® Order

Description Fits Glassware Set Coated? Buchi® Part No. Models Code Each
Vacuum Connector Tube DB, D Yes 01129 R220 3974-12 633.42
Vacuum Connector Tube DB, D No 41443 R220EX, SE 3974-13 527.85
“Y” Bottom Tube DB, D2, D Yes 01169 R220 3974-15 1425.20
“Y” Bottom Tube DB, D2, D No 46513 R220EX, SE 3974-18 1319.63
“U” Top Connect Tube DB, DB2 Yes 27837 R220 3974-20 2109.29
“U” Top Connect Tube DB, DB2 No 46515 R220EX, SE 3974-22 1979.44
“U” Top Connect Tube D, D2 Yes 27150 R220 3974-25 3035.14
“U” Top Connect Tube D, D2 No 46512 R220EX, SE 3974-27 2929.57
“Y” Bottom Tube DB2 Yes 41166 R220 3974-30 1476.92
“Y” Bottom Tube DB2 No 46514 R220EX, SE 3974-33 1371.35
New
3978-05
3978-07
3978 VALVES
Replacement borosilicate glass for Buchi® R220, R220EX, R220SE rotary evaporators. PTFE valve stem parts and valve assemblies,
with Kalrez o-rings, for receiving flasks and 3970 lower distribution heads. Socket joint on 3978-07 is DN25. Joints on 3978-05 are
PTFE, Ace‑Thred #11 and #15, and they include CAPFE (PTFE-encapsulated silicone rubber) o-rings. Hose coupling on -07 is size
G, for 5/18-inch I.D. tubing. Replacement o-rings for the bushings on 3978-05 are CAPFE size –110 (7855-816) for side port and
CAPFE size –112 (7855-820) on end.
Fits Similar to Buchi® Fits Buchi®
Description Glassware Set Coated? Part No. Models Order Code Each
Glass Body (only) for 3978-05 Inlet Valve All No 41346 All 3978-01 626.03
Complete Inlet Valve Assembly for
All No 41348 All 3978-05 791.78
Distribution Head
Bottom Drain Valve (Receiver) — No 41061 All 3978-07 332.55
Replacement PTFE valve stem (only) for valves. Includes two
No — All 3978-33 142.52
7855-606 size –011 and one 7855-618 size –111 Kalrez o-rings.
ACE Glass introduces...

A full line of Replacement Glassware
for Bench-Scale Rotary Evaporators! Contact
us
r a copy
Ace Glass, founded in 1936, continues our long tradition of manufacturing high today fo ew
quality specialty glassware. We would like to introduce a new, comprehensive of our n
e!
line of glassware to fit today’s popular rotary evaporators. Ace also offers brochur
both custom glass and glass repair services for rotary evaporators. Ace Glass
rotary evaporator replacement glass, all manufactured in the USA to exacting
specifications and standards.
Toll-free: Toll-free fax:
800-223-4524 800-543-6752
856-692-3333 • Fax: 856-692-8919
www.aceglass.com P.O. Box 688
Vineland, NJ 08362-0688
sales@aceglass.com

6726 FLASKS Receiving
Replacement borosilicate glass for Buchi® R220, R220EX, R220SE rotary evaporators.
Receiving flasks are designed to fit all large-scale rotary evaporators. Now available in 6726-20
coated, plain, non-coated, amberized and 6727 jacketed versions. Side necks include
7647-40 SVL-22 threaded black caps. Top and bottom socket joints are DN25, and bottom
joint includes 7855-840 CAPFE (PTFE-encapsulated silicone rubber) o-ring, size –217.
Similar to Fits
Buchi® Buchi® Order
Description Coated? Part No. Models Code Each
Receiving Flask 10L Yes 37569 All 6726-10 1102.95
Receiving Flask 10L No 46519 All 6726-15 992.10
Receiving Flask 20L Yes 41446 All 6726-20 1441.03
Receiving Flask 20L No 28671 All 6726-25 1330.18
Receiving Flask 10L — Amber No — All 6726-30 1102.95
Receiving Flask 20L — Amber No — All 6726-32 1441.03
SVL-22 vent cap wtih PTFE insert 7647-40 36.23

New
6726-30
6727 FLASKS Receiving, Jacketed New

Standard receiving flask for all rotary evaporators. Same as 6726 except, with outer jacket 6727
for cooling/heating of contents. Inlet/outlet connections are 28/15 o-ring ball joints and
include 7855-726 FETFE o-rings, size –116. Top and bottom joints are DN25. Bottom
inner ball joint includes 7855-840 CAPFE (PTFE-encapsulated silicone rubber) o-ring,
size –217. Side joint is SVL-22 thread, with 7647-40 black cap included.
Fits Rotavap
Description Coated? Models Order Code Each
Receiving Flask 8L No All 6727-10 1291.39
SVL-22 Vent cap with insert 7647-40 36.23
ACE Custom Glass

Design Service
www.aceglass.com
1-800-223-4524
Large Evaporator Flasks

for All Rotary Evaporators
6702 FLASKS Evaporation, Large Scale
These large sized evaporation flasks are fabricated from heavy wall flask blanks
selected for balance and quality. Necks are carefully fabricated to prevent “rotational
whip”. Flask are now available in clear plain glass or poly-coated or amberized.
Amber coated flask can protect light sensitive contents. The “XL” sizes flange,
(see table), is compatible with the 150mm and standard for Buchi® Model R220
rotary evaporators.
1. Select Flange Size.

A A B C
C Flange Size O.D., mm I.D., mm Thickness
B Designation (Inches) (Inches) (mm)
S (Small) 90 (3.5) 67 (2.7) 18
M (Medium) 100 (3.9) 72 (2.8) 19
OVERALL L (Large) 110 (4.3) 83 (3.3) 23
HEIGHT
XL (Extra Large) 149.5 (5.9) 118.8 (4.7) 21
2. Select Flask Capacity and match

with Flange Size.
Similar to
Capacity, Buchi® Part Overall Flange Order
Liters No. Height, mm Size Code Each
6 27470 300 S 6702-05 201.28
6 27470 325 M 6702-07 212.20
6 27470 380 M 6702-10 212.20
6 27470 295 L 6702-15 260.37
6 27470 380 L 6702-17 269.08
6 27470 351 XL 6702-19 279.48
Easy Order Instructions 10 27469 350 S 6702-20 316.12
1. Determine flange size (A) O.D., (B) I.D., 10 27469 335 M 6702-25 334.46
(C) thickness (see diagram). 10 27469 413 M 6702-27 340.41
10 27469 410 L 6702-30 378.48
2. Match flask capacity with overall height 10 27469 380 XL 6702-33 419.03
and flange size. 20 27468 375 M 6702-35 506.66
20 27468 435 M 6702-37 495.78
20 27468 435 L 6702-40 516.96
20 27468 413 XL 6702-44 564.94
6702 COVER For Evaporating Flask, Polyethylene

Polyethylene dust cover for evaporating flasks with 149.5mm I.D. Has integral o-ring to
keep a tight seal. Comes complete with Viton o-ring.
Similar to Buchi® Order

Part No. Code Each
New 42895 6702-300 50.13
6702

6702 FLASKS Evaporation, Large Scale, Poly-Coated

Same as 6702 on previous page, but poly-coated for added safety. Plastic coated flasks
are clear and will withstand temperatures up to 100°C.
6702
Capacity, Similar to Buchi® Overall Flange Order New
Liters Part No. Height, mm Size Code Each
6 — 300 S 6702-105 276.56
6 — 325 M 6702-107 288.27
6 — 380 M 6702-110 288.27
6 — 295 L 6702-115 339.91
6 — 380 L 6702-117 376.40
6 27470 351 XL 6702-119 678.90
10 — 350 S 6702-120 399.68
10 — 335 M 6702-125 419.34
10 — 413 M 6702-127 427.81
10 — 410 L 6702-130 466.54
10 27469 380 XL 6702-133 900.68
20 — 375 M 6702-135 603.97
20 — 435 M 6702-137 594.73
20 — 435 L 6702-140 617.70
20 27468 413 XL 6702-144 973.30
6702 FLASKS Evaporation, Amberized

Same as 6702 above, except with an amber coating to protect light sensitive contents.
The XL size matches Buchi® large-scale rotary evaporators. Plain, not coated. 6702 New
Capacity, Similar to Buchi
®
Overall Flange Order
6 — 351 XL/149.5 6702-219 495.71
10 — 380 XL/149.5 6702-233 634.95
20 — 413 XL/149.5 6702-244 818.75
6720 FLASKS Evaporation, Indented

These flasks are also referred to as drying flasks. They are particularly suited for drying
of powdered samples. The baffles, indented into the glass, provide better circulation and 6720
mixing of the powders while rotating. Plain, not coated. NOT suitable for vacuum operation. New
Capacity, Similar to Buchi® Overall Flange Order
10 28592 380 XL/149.5 6720-10 692.81
20 28593 413 XL/149.5 6720-20 859.08
Spare Parts, Glassware Assemblies
R RB
3965-05, -07 3965-26, -28
3978-05
3973-30
3978-05
3973-30
3970-05
3970-05 3965-30, -32
3965-30, -32
3973-01,
C 3971-21 Interchangeable -03
Receiver (W)
6517-27
3973-04, -06
3971-01
6726 Series
3971-05, -03
3978-05
3973-30 3978-07
Single Receiver
(E) 3973-08, -10
3970-05
6726 Series
3965-30, -32
3978-07

Spare Parts, Glassware Assemblies
D D2
3974-25, -27 3974-25, -27
3965-10, -15 3965-10, -15
3967-10, -15 3967-10, -15
3965-05,
-07
3974-12, -13
3970-15, -18
3970-15, -18
3978-05 3974-15, -18 3978-05

3974-15, -18
DB DB2
3974-19, -22 3974-19, -22 3967-10,
-15
39651-26,
-28
3965-20, -22
3967-10,
3974-12, -13 -15
3970-15, 3965-20,
-22
-18
3978-05
3978-05 3974-30 -33 3970-15,
3974-30, -33 -18
Big Columns 267
BIGCOLUMNS
All types of 5844 ADAPTER for Swagelok
special combinations PTFE adapter for use at top of 5860 column head or at bottom of 5862 column to connect
tubing via Swagelok type connector to #50 Ace‑Thred, other end has 1/4-inch NPT female
made to order thread. Supplied with one FETFE o‑ring. For extra o‑rings, see 7855-729.
• Heads can be supplied with
additional threads or joints or Order Code Each
combination of both 5844-78 172.15
• Columns available in various

lengths and diameters 5860 COLUMN HEAD
For use with 5862 chromatography column. With #50 Ace‑Thred center neck and/or
5844 two #15 Ace‑Thred side necks and 4- or 6-inch flange at bottom, ground flat. Use with
6517 clamp.
Flange Size Center Neck Side Necks Order Code Each

5860 4-inches 50 None 5860-24 234.29
6-inches 50 None 5860-28 285.18
6-inches 50 15 5860-32 398.71
6517 5862 COLUMN (#50)

Large size chromatography columns with o‑ring grooved flat flange at top for easy access
to column. Flange is supplied with silicone o‑ring to make seal when using 5860 head
with 6517 clamp. 4- and 6-inch I.D. columns are tapered to #50 Ace‑Thred at bottom that
accepts 5844 adapter, or 5848 and 5835 adapters. For replacement o‑rings, see below.
5862 Flange Size/

(#50) Col. I.D., in. Length mm (in.) Order Code Each
4 300 (12) 5862-43 475.82
5862 4 450 (18) 5862-45 497.89
(#80) 4 600 (24) 5862-47 542.43
4 1200 (48) 5862-49 636.16
6 450 (18) 5862-58 804.61
6 600 (24) 5862-62 884.11
6 1200 (48) 5862-65 999.53
6 1800 (72) 5862-68 1062.72
5857 Replacement Silicone O‑Rings

5843 Order Code Each
5848
For 4-inch Flange 7855-254 21.39
5857 For 6-inch Flange 7855-260 40.00
Replacement CAPFE O‑Rings

7506-03 Order Code Each
B For 4-inch Flange 7855-880 28.63
5835-17 For 6-inch Flange 7855-881 59.65
A
5835

268 Big Columns
BIGCOLUMNS 5862 COLUMN (#80)

Large size columns with o‑ring grooved flat flange at top for easy access to column.
Flange is supplied with silicone o‑ring to make seal when using 5860 head with 6517
clamp. Columns are tapered to #80 Ace‑Thred at bottom that accepts 5857 adapter.
5862
Length Flange Size Inner Diameter Order Code Each
18 inches 6 inches 6 inches 5862-10 910.45
6517 CLAMP
Stainless steel quick release clamp with three retaining clips for connecting 5860 head
and 5862 column.
6517
For Flange Size Order Code Each
4 inches 6517-25 98.23
6 inches 6517-27 117.67
5848 SUPPORT PLATE Perforated

73mm diameter glass plate with 1x3mm rectangular slits for supporting column packing.
Used with 5857.
5848 Order Code Each

5848-60 86.83
5843 COUPLING Reducing, with Support

For connecting 5835 bottom drip stopcock adapter to bottom of 5862 chromatography
column with leak-tight o‑ring seals. One end is #50 Ace‑Thred for connecting to
column, the other #25 Ace‑Thred is for connecting to 5835B adapter. #50 end of
coupling is supplied with Porosity A glass packing support, press fitted, with taper
below disc to 25 I.D. For replacement supports, see below. Supplied with two FETFE
o‑rings. For replacement o‑rings, see 7855-729 (for #50); or 7855-727 (for #25).
Order Code Each

5843 5843-74 248.13
Replacement Glass Packing Supports
Order Code Each
Porosity A (145-175 micron) 5848-49 130.80
Porosity B (70-100 micron) 5848-58 130.80
Big Columns 269
BIGCOLUMNS
5835 ADAPTER Bottom Drip, with 1:5 PTFE Stopcock
Drip tip for bottom of 5862 column using 5843 coupling. One end has #25 Ace‑Thred, 5835-17
other with drip tip and 4mm bore PTFE stopcock for controlling flow.
Order Code Each

5835-17 129.37
5835 BOTTOM OUTLET VALVE with or without Stopcock

Type A — With 0-8mm threaded stopcock for controlling flow. B
Type B — Straight stem without stopcock. Both stems to take 3/8-inch Swagelok fittings. A
Secured to 5857 bottom adapter with 7506-03 bushing.
Type Order Code Each 5835
A 5835-32 126.39
B 5835-34 35.94
5857 BOTTOM ADAPTER UHMWPE* or PTFE

Fits #80 Ace‑Thred. Recessed for 5848 perforated support plate and 5857 retaining ring. Your
choice of bottom threaded for #11 Ace‑Thred bushing 7506-03 to secure 5835 outlet valve,
or threaded to accept 3/8-inch NPT fitting. For replacement FETFE o‑rings, order 7855-764.
#11 Ace‑Thred Hole 3/8-inch NPT Hole

UHMWPE* Order Code Each Order Code Each
Adapter, #80 Thred 5857-30 124.06 5857-35 104.22
Support Plate 5848-60 86.83 5848-60 86.83
Retaining Ring 5857-50 13.98 5857-50 13.98
Bushing 7506-03 11.86 —
Connector, 3/8-inch — 12770-27 31.59
COMPLETE 5857-44 236.73 5857-46 236.62
#11 Ace‑Thred Hole 3/8-inch NPT Hole

PTFE Order Code Each Order Code Each
Adapter, #80 Thred 5857-60 267.57 5857-64 267.57 5857
Support Plate 5848-60 86.83 5848-60 86.83
Retaining Ring 5857-52 15.30 5857-52 15.30
Bushing 7506-03 11.86 — —
Connector, 3/8-inch — — 12770-27 31.59
COMPLETE 5857-67 381.56 5857-69 401.29
*UHMWPE — Ultra High Molecular Weight Polypropylene
5861 ADAPTER
Bottom filter adapter for use with our 6384,6386 & 6388 glass reactor bodies and our 6390
all PTFE reactor bodies. Adapter differs from our codes 5838-83 & 5857-86 in that the 5861
3/8-inch female NPT is located as a side discharge rather than thru the bottom. Adapters
are PTFE and include a CAPFE o-ring, PTFE retaining ring, 100 micron polyethylene filter
disc and 350 micron polypropylene filter screen. Code -07 includes a glass filter support
from our 5848 product family. See also our 5814 family for filter support screen options.
For Thread Size Order Code Each

50 5861-03 234.71
80 5861-07 323.51

270 Big Columns
5820 COLUMNS Large Size, with Ace-Threds

Borosilicate glass columns for liquid chromatography, ion-exchange or activated carbon
work featuring Ace-Thred connections. Threaded ends are compatible with fittings shown
with other chromatography systems listed. Fittings can be used with these columns and
offer easy-to-change support screens with a variety of openings never before offered.
50 psi maximum pressure.
Minimum Approx.
Column Effective Length, Capacity, Ace-Thred Order
I.D., mm mm (Inches) mL Size Qty. Code Each
75 300 (12) 1,320 50 1 5820-105 512.43
5820 75 600 (24) 2,650 50 1 5820-107 554.17
75 1200 (48) 5,300 50 1 5820-109 642.86
100 1200 (48) 9,430 50 1 5820-116 733.03
100 1800 (72) 14,940 50 1 5820-119 808.54
150 600 (24) 10,600 50 1 5820-121 1094.99
150 1200 (48) 21,200 50 1 5820-125 1175.85
150 1800 (72) 31,800 50 1 5820-129 1256.70
150 2400 (96) 42,200 50 1 5820-133 1338.87
Note: Columns of larger I.D. and longer than listed above can be fabricated.
Also, most sizes can be jacketed. Call or email for details.
Support stand for 100 and 150mm columns listed under 12099.
5862 COLUMN EXTENDER

Glass extenders that can be added to 5862 columns to increase column height. Extenders
have an o‑ring grooved flat flange on one end to attach 5860 column head and ground
flat flange at other end to attach the 5862 column. Supplied with one silicone o‑ring. Use
6517 quick release clamp to secure sections.
Flange Size/
Column I.D., in Length mm (in) Order Code Each
4 300 (12) 5862-72 266.26
4 450 (18) 5862-73 266.26
4 600 (24) 5862-74 307.74
5862 6 300 (12) 5862-77 554.83
6 450 (18) 5862-78 597.85
6 600 (24) 5862-79 639.61
5867 SUPPORT STAND for Large Columns

Newly designed four-post stands for large scale chromatography columns feature all
stainless steel construction. Each stand is designed to accept either 24-, 48-, or 72-inch
length 5862 columns. With 150mm (6-inch) flange and 6-, 8-, or 12-inch diameter body.
Supplied with two (2) column support rings with 140mm and 175mm openings. Each
5867 stand is designed to accommodate the height of the column and has a PTFE collar at
the bottom that accepts and supports the tapered bottom of the column. Each stand
has an adjustable stainless upper collar assembly that supports the top of the column.
All stands have locking casters for mobility.
Fits Column Dimensions, Inches
(Height) Order Code (W x D x H) Each
24 inches 5867-24 15 x 15 x 40 2391.36
48 inches 5867-48 15 x 15 x 60 2858.84
72 inches 5867-72 15 x 15 x 85 3099.77
Custom sizes are available!
Big Columns 271
5868 SUPPORT STAND for Bench-Scale Columns

Newly designed single-post stand for 12- and 18-inch height chromatography columns.
“H” shaped base and a single 122cm high x 1-inch diameter stainless steel bar give great
stability for the large-scale columns. Stand comes complete with base, rod, base plate, 5868
clamp holder and chain clamp.
Overall Height Order Code Each

125cm 5868-122 583.61
5848 FILTER DISC

5848
Filter disc for use with 5837 and 5838 adapters. Available in polyethylene (100 micron
pore size), and borosilicate glass — Porosity A (145-174 microns), B (70-100 microns),
C (25-50 microns) and D (10-20 microns). Sold in packages. (Caution: These discs are
intended to be removable. However, because of the tight fit, the glass disc may break
when being removed.)
Polyethylene Borosilicate Glass

Porosity A Porosity B Porosity C Porosity D
100 microns 145-174 microns 70-100 microns 25-50 microns 10-20 microns
For
Adapter Pkg. Order Per. Order Per Order Per Order Per Order Per
Size,mm Qty. Code Pkg. Code Pkg. Code Pkg. Code Pkg. Code Pkg.
11 6 5848-07 14.44 5848-43 58.53 5848-52 58.53 5848-21 58.53 5848-31 58.53
15 6 5848-10 14.44 5848-44 58.53 5848-54 58.53 5848-23 58.53 5848-33 58.53
25 6 5848-14 16.58 5848-47 66.12 5848-56 66.12 5848-25 66.12 5848-35 66.12
50 6 5848-17 34.99 5848-49 130.80 5848-58 130.80 5848-28 130.80 5848-38 130.80
80 1 5848-19 9.03 5848-100 126.50 5848-120 129.55 5848-122 147.23 5848-124 161.95
5814 SCREEN SUPPORT FILTER DISCS Polypropylene

Screen support filter pre-cut discs used with 5857 and 5861 end fitting adapters.
For 350 295 210 105
Ace‑Thred Micron Micron Micron Micron Each
Size Qty. Order Code Order Code Order Code Order Code Pkg/12
11 12 5814-42 5814-52 5814-62 5814-82 9.67
15 12 5814-44 5814-54 5814-64 5814-84 11.56
25 12 5814-46 5814-56 5814-66 5814-86 19.33
50 12 5814-48 5814-58 5814-68 5814-88 36.45
Note: Discs can also be supplied in polyethylene and fluorocarbon; however, since they 5814
are not stock items, a minimum quantity will be supplied. Phone for quotation.

272 Big Columns
S I N C OR
S P
A
O
L
RA
ACE G
TH
A N N I V E R S A R Y TED
1936 2011
VI USA
N
J
NE ,
LAND
Process Pipe 273
Beaded Process Pipe

Ace Glass has been manufacturing and fabricating Low Maintenance Cost
glassware and equipment for the scientific and research
communities for over 75 years. ACE fabricates glass Over the life of a piping system this can be the smallest
process pipe here in the USA, from medium- and heavy- cost component for glass piping systems and the largest
wall borosilicate tubing such as Scimax and Schott cost consideration for many other competitive piping
Duran, to provide you with a high quality product to fit systems. Chances are that low maintenance cost is the
into your process stream. From glass process pipe to prime reason for considering, specifying, and operating
glass reactors and pilot plants, to temperature equipment a glass piping system.
and sensors, ACE offers a broad line of products to the
process engineer. ACE will also fabricate custom sizes Properties of Borosilicate Glass
and shapes for your needs — if you don’t see what you
need in this catalog, contacts us at www.aceglass.com Chemical Composition
to discuss your needs with our engineering staff. The borosilicate glass used in the manufacture of our
Glass meets an ASTM spec for borosilicate glass, ASTM pipeline components conforms to the standard ASTM
E-438 and Federal spec DD‑G‑541B. The “system” can be E 438 and has the following approximate composition.
constructed by a contractor to meet ASTM spec C1053-
90, ASTM spec C1053-00, Federal spec DD‑G‑541B, Component % By Weight
Military spec MIL‑P 2256B(YD) when it is all put together SiO2 81%
using the same pipe and couplings.
B2O3 13%
Glass also meets specs for USP Type 1 glass.
Na2O 4%
Process Piping Systems Al2O3 2%
Industry has long regarded borosilicate glass piping Chemical Resistance
components to be one of the best corrosion resistant
materials of construction. For a wide range of Borosilicate glass is resistant to almost all substances
manufacturing and process piping applications Ace Glass except hydrofluoric acid, phosphoric acid and hot strong
brand glass pipe installations have provided excellent caustic solutions. Of these, hydrofluoric acid has the
service in the most difficult piping applications, positive most serious effect and, even when a solution contains
evidence of its outstanding performance. The use of glass a few parts per million, corrosion will occur. Phosphoric
offers many advantages over other conventional piping acid and caustic solutions at elevated temperatures will
materials such as: also attack glass.
Under service conditions, the effects of turbulence and
Long Service Life some trace chemicals in solution may increase or decrease
Low-expansion borosilicate glass is resistant to the rate of attack. Therefore, it is not possible to give
almost all substances except hydrofluoric acid, hot precise figures for corrosion by hydrofluoric acid and
concentrated phosphoric acid and strong alkalis at caustic solutions, but Figures 1 and 2 show typical rates.
elevated temperatures.
Product Purity
All glass piping systems are comprised of chemically
inert borosilicate glass and TFE gaskets to ensure no
chemical contamination of process fluids. Materials that
do not corrode do not contaminate.
Smooth Interior Surface

The hard, liquid smooth surface inhibits or prevents scale
formation and product buildup. For example, sticky latex
dispersions easily move through smooth glass pipe. Glass
resists fouling and is easy to clean.
Transparency
You can see what is happening inside glass systems.
Process and product can be inspected at a glance.
Trouble cannot hide behind glass, so processes stay in
better control.

274 Process Pipe
Beaded Process Pipe

Physical Properties — Borosilicate Beaded Pressure System
Glass
A large bead design feature assures a tight leak-free joint
Coefficient of mean linear expansion under pressure conditions.
Between 20°C and 300°C (3.3 ±0.1) x 10-6 K-1 The one-bolt compression coupling shell is made from
Mean thermal conductivity 300-series stainless steel. The flexible, elastomeric sleeve
Between 20°C and 200°C 1.3 W/mK is lined with a tough layer of TFE fluorocarbon plastic. The
flexibility feature allows deflections up to 3° per joint from the
Mean specific heat capacity
axis under bending loads due to misalignment or pitching.
Between 20°C and 200°C 0.98 kJ/kgK
Density at 20°C 2.23 g/cm3
Pressure
Operating Temperature (Maximum) Short term: Do not
operate below 0ºC The permissible operating pressure for ACE beaded pipe

Normal Use: 230ºC and fittings depends on the pipe diameter.
Pipe Diameter Maximum Working Pressure

Versatility
1-inch 100 psig
For comparison purposes, weights of various 2-inch
pipes are given in the table below. 1-1/2-inch 75 psig
2-inch 75 psig
Material Approx. Weight of 2-inch Pipe, Lbs/Ft.
3-inch 50 psig
Glass Process Pipe 1.13
4-inch 50 psig
Steel (Schedule 40) 3.65
6-inch 30 psig
High Silicon Iron 7.70
Stainless Steel (Schedule 40) 3.65 When a system is assembled from several glass
components with different pressure ratings, the maximum
TFE Lined Steel 4.10 operating pressure of the system is limited to the pressure
Glass Lined Steel 3.95 rating of the component with lowest permissible working
gauge pressure.
FRP 1.25
All sizes of glass piping are suitable for full vacuum
service. Full vacuum is defined as 29.92-inch (760mm)
Relative Thermal Expansion of Hg below standard sea-level pressure. Of course the
The thermal expansion of ACE brand pipe is 0.022 inches vacuum actually achieved is a function of system design,
per 100 feet of pipe and 100°F temperature change. Values tightness of the gasket joints, types of gasket used and
of other materials relative to this (assuming glass Pipe = 1) other operating factors.
are given below. These relative thermal expansions should Permissible operating pressures require the use of ACE
be considered when connecting glass pipe into other bead to bead process couplings. ACE process pipe is
materials. When other materials expand more than glass tested at 1.5x the stated maximum working pressure.
pipe, allowance must be made for the expansion difference.
A common way to accommodate this differential expansion
is with flexible “bellows” or hose at critical locations. Anchor Points
An anchor point is a rigid support for the glass line t ying it
Material Relative Thermal Expansion into the building structure, or to fixed equipment such as
Glass Process Pipe 1.00 tanks, pumps or independently supported valves. There
should be one — and only one — anchor point in each
Steel (Schedule 40) 3.60 straight run of pipe. The diagrams that follow show the
High Silicon Iron 4.90 correct and incorrect installation methods between a nchor
points. Note the use of right-angle bends to obtain flexibility.
Stainless Steel (Schedule 40) 6.20
TFE Lined Steel 3.65
Glass Lined Steel 3.65
FRP 7.00
Process Pipe 275
Beaded Process Pipe

Vibration
Connection to vibrating machinery such as a pump can
be made with the use of a flexible connection consisting
of either hoses, or PTFE “bellows” as determined by the
characteristics of the service.
Pressure Surges
Pressure surges must be controlled to prevent end
motion in a line. If lines have hydraulic pressure surges,
(positive displacement pumps or shutoff valves), it may
be necessary to provide a pressure relief valve. It is
usually necessary to provide a protected air dome to
reduce the pressure surge. The domes can be installed
on the discharge side of the pump, next to a valve, or at
the highest point in the vertical rise of the discharge line.
Use a tee at the top of the riser, plus a straight section
and a cap.
All valves, strainers, meters or other heavy equipment

must be supported rigidly and independently of the glass
pipeline. This prevents transmitting the dead weight to
the glass pipeline. It also prevents transmitting stresses
to the line when valves are operated; equipment shifts
positions, or expands more than the glass pipe. Rigidly
supported equipment such as the above are considered
anchor points. No more than one anchor point should be
used in any straight run of glass pipe. Flexible “bellows”
or hose can be used at the tie-in place.
Pipe Hanging and Support

Glass piping must be installed without mechanical restraint
and the pipe should be free to move to prevent stresses.
A mechanical restraint may set up a tensile stress that
over a period of time will cause the pipe to fail. Hangers
should not clamp the pipe tightly. Some lengthwise and
sidewise movements are desirable. Padded hangers
should always be used and spaced 8-10 feet apart. Use
an extra hanger where there are two or more couplings
in an 8-10 foot span. Do not pull or spring the pipe into
place. Always move the hanger to the pipe do not force
the pipe to the hanger.
Vertical Line Support

Vertical lines should be supported by plates beneath
the couplings or by padded saddles beneath 90-degree
elbows at the bottom of vertical rises. Do not support by
rigid clamp anchorages around the vertical pipe. Usually
only one rigid support is used. Lateral guides should be
used approximately every 20 feet of unsupported riser.
The horizontal run at the top of the riser should not be
supported within 7 feet of the riser. This reduces bending
strains in the horizontal run.

276 Process Pipe
Beaded Process Pipe

Protection Cleaning
It is usually desirable to run glass pipe close to structures Flush line clean with water, other cleaning fluids, or
such as walls, columns, ceilings, etc., where conditions atmospheric pressure steam (open drain). Do not use
are favorable for obtaining a firm support. This also would hydrofluoric acid, hot caustic solutions, abrasives or metallic
keep the pipelines away from the heaviest traffic. When tube cleaners.
the pipelines are run through congested areas, provision
should be made for protection. Angle or channel iron,
or expanded metal guards, should be provided around
Tools Required
exposed sections of glass pipe. Tools need to install glass piping (installation tools):
a) Wrenches 7/16-inch Open End, 1/2-inch Open End
Testing 9/16-inch Open End, 3/4-inch Open End
Tighten bolts on all couplings and flanges at the time of b) Ratchet 3/8-inch Drive
installation. The pipeline, when empty, should be examined
for stresses by gently shaking the line. There should be c) Sockets 7/16-inch Deep Socket, 1/2-inch Deep Socket
some limited movement the lines. To make sure all joints 9/16-inch Deep Socket, 3/4-inch Deep Socket
are tight when line is ready for service, test at 1‑1/2 times
d) Torque Wrench Calibrated in inch-lbs. Preferred
the working pressure. However, do not test at more than
ratchet type 3/8-inch Drive.
the maximum working pressure. All air must be removed
from the pipeline so there is no trapped air. DO NOT TEST e) Water-pump pliers 3/8-inch Drive
WITH AIR PRESSURE. If a joint leaks, carefully check the f) Various screw-drivers
joint assembly, retighten to recommended torque value,
and retest. If leaking persists, remove coupling, check g) Hammer Plastic or rubber head
the gasket surface to be sure they are free from dirt, sand Structural Tools:
or other particles, and replace if necessary.
a) Allen wrenches 5/16-inch and 3/8-inch
Spare Parts b) Hammer

c) Hack saw
Generally, one spare for every twelve should be provided.
The proper storage of spare parts will ensure they are
available when required. Keep lengths of pipe on racks
and store them in a protected area. Keep fittings in their
original packaging.
Making Joints with Process Pipe Couplings

1. Dip coupling in water or wipe beaded ends with damp cloth.
2. Snap coupling over one end of pipe making certain TFE liner is behind bead...
then insert other section of pipe into opposite side of coupling.
3. Tighten coupling bolt with 6-inch ratchet wrench until the gap between segments
is approximately 3/16-inch.
1 2 3
Process Pipe 277
8828 BEADED PIPE

All pipe is available from stock in lengths shown; special lengths available at slightly higher cost.
1/2-inch A B 3/4-inch A B 1-inch A B 1-1/2-inch A B

I.D. 57/64-inch 3/4-inch I.D. 1-5/32-inch 1-inch I.D. 1-17/32-inch 1-5/16-inch I.D. 2-1/16-inch 1-27/32-inch
Length Order Length Order Length Order Length Order
(Inches) Code Each (Inches) Code Each (Inches) Code Each (Inches) Code Each
3 8828-02 26.86 3 8828-102 35.47 3 8828-202 48.48 — — —

4 8828-03 27.67 4 8828-103 36.55 4 8828-203 48.48 4 8828-303 66.47
6 8828-05 26.87 6 8828-105 36.55 6 8828-205 48.48 6 8828-305 66.47
12 8828-09 29.74 12 8828-109 37.69 12 8828-209 51.36 12 8828-309 70.84
18 8828-11 32.84 18 8828-111 41.35 18 8828-211 55.06 18 8828-311 75.53
24 8828-13 34.95 24 8828-113 42.95 24 8828-213 59.89 24 8828-313 80.62
30 8828-15 36.55 30 8828-115 46.61 30 8828-215 64.43 30 8828-315 86.06
36 8828-20 39.01 36 8828-120 49.06 36 8828-220 69.03 36 8828-320 90.75
48 8828-25 43.34 48 8828-125 54.49 48 8828-225 76.69 48 8828-325 95.57
60 8828-30 46.29 60 8828-130 58.88 60 8828-230 86.43 60 8828-330 102.44
72 8828-38 51.24 72 8828-138 63.95 72 8828-238 95.68 72 8828-338 123.13
84 8828-45 55.23 84 8828-145 69.14 84 8828-245 104.69 84 8828-345 138.55
96 8828-56 59.89 96 8828-156 74.07 96 8828-256 111.79 96 8828-356 163.08
108 8828-260 118.69 108 8828-360 184.44
120 8828-262 131.83 120 8828-362 204.59
A B A B 4-inch A B A B
2-inch I.D. 2-9/16-inch 2-5/16-inch 3-inch I.D. 3-11/16-inch 3-7/16-inch I.D. 4-7/8-inch 4-9/16-inch 6-inch I.D. 7-1/8-inch 6-5/8-inch
Length Order Length Order Length Order Length Order
(Inches) Code Each (Inches) Code Each (Inches) Code Each (Inches) Code Each
4 8828-403 87.31 4 8828-503 138.15 — — — — — —

6 8828-405 84.76 6 8828-505 138.15 6 8828-605 250.50 6 8828-705 408.88
12 8828-409 95.34 12 8828-509 145.24 12 8828-609 260.65 12 8828-709 431.45
18 8828-411 102.90 18 8828-511 151.84 18 8828-611 271.74 18 8828-711 453.86
24 8828-413 110.16 24 8828-513 158.27 24 8828-613 283.38 24 8828-713 526.80
30 8828-415 118.00 30 8828-515 160.38 30 8828-615 293.38 30 8828-715 551.99
36 8828-420 121.17 36 8828-520 171.75 36 8828-620 295.28 36 8828-720 691.94
48 8828-425 132.74 48 8828-525 174.74 48 8828-625 314.23 48 8828-725 721.81
60 8828-430 138.93 60 8828-530 186.43 60 8828-630 314.66 60 8828-730 839.77
72 8828-438 167.75 72 8828-538 223.62 72 8828-638 389.30 72 8828-738 965.57
84 8828-445 195.96 84 8828-545 261.27 84 8828-645 454.01 84 8828-745 1052.05
96 8828-456 224.62 96 8828-556 297.81 96 8828-656 518.90 96 8828-756 1206.16
108 8828-460 251.53 108 8828-560 334.50 108 8828-660 583.79 108 8828-760 1358.71
120 8828-462 278.66 120 8828-562 372.26 120 8828-662 627.20 120 8828-762 1445.22

278 Process Pipe
8830 SWEEP ELBOW

90° 45° 60° 22½°
Size A Order Size A Order Size A Order Size A Order
(inches) (In.) Code Each (inches) (In.) Code Each (inches) (In.) Code Each (inches) (In.) Code Each
1/2 – 90° 2¼ 8830-03 41.33 1/2 – 45° 2¼ 8830-103 42.57 1/2 – 60° 2¼ 8830-203 42.57 1/2 – 22° 2¼ 8830-303 42.57
3/4 – 90° 2½ 8830-05 50.15 3/4 – 45° 2½ 8830-105 50.15 3/4 – 60° 2½ 8830-205 50.15 3/4 – 22° 2½ 8830-305 50.15
1 – 90° 2¾ 8830-07 66.37 1 – 45° 2¾ 8830-107 66.37 1 – 60° 2¾ 8830-207 65.97 1 – 22° 2¾ 8830-307 67.96
1-1/2 – 90° 5 8830-09 69.87 1-1/2 – 45° 3½ 8830-109 69.87 1-1/2 – 60° 3½ 8830-209 69.87 1-1/2 – 22° 3½ 8830-309 69.87
2 – 90° 6 8830-11 93.82 2 – 45° 4 8830-111 93.82 2 – 60° 4 8830-211 93.82 2 – 22° 4 8830-311 93.82
3 – 90° 7 8830-13 164.88 3 – 45° 5 8830-113 164.88 3 – 60° 5 8830-213 164.88 3 – 22° 5 8830-313 164.94
4 – 90° 10 8830-15 278.32 4 – 45° 7 8830-115 278.12 4 – 60° 7 8830-215 279.25 4 – 22° 7 8830-315 278.58
6 – 90° 12 8830-17 725.54 6 – 45° 9 8830-117 726.86 6 – 60° 9 8830-217 725.50 6 – 22° 9 8830-317 725.50
Use catalog dimensions for piping layout as gasket thickness allowance is included.
8831 REDUCER ELBOW

Size A B
(inches) (inches) (inches) Order Code Each
3/4 x 1/2 2-1/2 2-1/2 8831-02 78.26
1 x 1/2 2-3/4 2-3/4 8831-04 93.63
1 x 3/4 2-3/4 2-3/4 8831-06 100.46
1-1/2x 1/2 3-1/2 3 8831-08 100.46
1-1/2x 3/4 3-1/2 3 8831-10 100.46
1-1/2x 1 3-1/2 3 8831-12 100.46
2 x 1/2 4 3 8831-14 127.54
2 x 3/4 4 3 8831-16 153.32
2 x1 4 3 8831-18 153.32
2 x 1-1/2 4 3-1/2 8831-20 153.32
3 x1 5 3-1/2 8831-22 233.39
3 x 1-1/2 5 4 8831-24 233.39
3 x2 5 4-1/2 8831-26 233.39
4 x1 7 4 8831-28 422.94
8831
4 x 1-1/2 7 4-1/2 8831-30 422.94
4 x2 7 5 8831-32 422.94
4 x3 7 5-1/2 8831-34 422.94
6 x 1-1/2 9 5-1/2 8831-36 834.77
6 x2 9 6 8831-38 834.77
6 x3 9 6-1/2 8831-40 834.77
6 x4 9 8 8831-42 834.77
Process Pipe 279
8832 MITERED ELBOW 90°

Size (inches) A (inches) Order Code Each
1-1/2 3-1/2 8832-03 97.35
2 4 8832-05 134.04
3 5 8832-07 202.77
4 7 8832-09 386.37
6 9 8832-11 729.38
8832
8833 SHORT RADIUS ELBOW 90°

1-1/2 3-1/2 8833-32 77.16
2 4 8833-34 106.01
3 5 8833-36 182.72
4 7 8833-38 326.89
8833
8836 TEE
Straight
Size (inches) A (inches) B (inches) Order Code Each
1/2 4-1/2 2-1/4 8836-02 70.67
3/4 5 2-1/2 8836-04 72.80
1 5-1/2 2-3/4 8836-06 81.03
1-1/2 7 3-1/2 8836-08 119.15
2 8 4 8836-10 141.36
3 10 5 8836-12 309.49
4 14 7 8836-14 395.01
6 18 9 8836-16 689.80
8836
Custom lengths, O.D. and shapes are available — Just ask!

280 Process Pipe
8837 TEE
Reducing
Size Run x Branch
(Inches) A (inches) B (inches) C (inches) Order Code Each
3/4 x 1/2 5 2-1/2 2-1/2 8837-03 72.80
1 x 1/2 5-1/2 2-3/4 2-3/4 8837-05 89.47
1 x 3/4 5-1/2 2-3/4 2-3/4 8837-07 89.47
1-1/2 x 1/2 7 3 3-1/2 8837-09 119.15
1-1/2 x 3/4 7 3 3-1/2 8837-11 119.15
1-1/2 x 1 7 3 3-1/2 8837-13 119.15
2 x 1/2 8 3 4 8837-15 144.07
2 x 3/4 8 3 4 8837-17 144.07
2x1 8 3 4 8837-19 144.07
2 x 1-1/2 8 3-1/2 4 8837-21 144.07
3x1 10 3-1/2 5 8837-23 178.79
3 x 1-1/2 10 4 5 8837-25 178.79
3x2 10 4-1/2 5 8837-27 178.79
4x1 14 4 7 8837-29 370.23
4 x 1-1/2 14 4-1/2 7 8837-31 370.23
4x2 14 5 7 8837-33 370.23
4x3 14 5-1/2 7 8837-35 370.23
6 x 1-1/2 18 5-1/2 9 8837-37 716.14
6x2 18 6 9 8837-39 716.14 8837
6x3 18 6-1/2 9 8837-41 716.14
6x4 18 8 9 8837-43 716.14
8842 REDUCER Straight
Size A Order Size A Order
(Inches) (Inches) Code Each (Inches) (Inches) Code Each
3/4 x 1/2 4 8842-03 41.61 3 x 1-1/2 5 8842-25 96.49
1 x 1/2 4 8842-05 43.57 3x2 5 8842-27 96.49
1 x 3/4 4 8842-07 44.90 4x1 7 8842-29 138.70
1-1/2 x 1/2 4 8842-09 54.08 4 x 1-1/2 7 8842-31 147.58
1-1/2 x 3/4 4 8842-11 54.08 4x2 7 8842-33 174.53
1-1/2 x 1 4 8842-13 54.08 4x3 7 8842-35 210.11
2 x 1/2 4 8842-15 64.93 6x1 9 8842-37 383.78
2 x 3/4 4 8842-17 64.93 6 x 1-1/2 9 8842-39 383.78 8842
2x1 4 8842-19 66.87 6x2 9 8842-41 407.76
2 x 1-1/2 4 8842-21 66.87 6x3 9 8842-43 435.95
3 x 1 5 8842-23 96.49 6x4 9 8842-45 449.34
8845 END CAP Extended

1/2 2 8845-03 23.89
3/4 2 8845-05 24.62
1 2 8845-07 42.46
1-1/2 3 8845-09 52.71
2 4 8845-11 62.45
3 4-3/4 8845-15 96.73 8845
4 6 8845-17 179.81
6 7 8845-19 210.04
8847 END CAP Short

1-1/2 7/8 8847-02 29.35 8847
2 1 8847-04 33.27
3 1-1/8 8847-06 44.82
4 1-1/4 8847-08 91.50
6 1-1/2 8847-10 125.03
Process Pipe 281
8849 U BEND
Size A (inches) Order Code Each
1/2 2-1/4 8849-03 65.95
8849
3/4 2-1/2 8849-05 78.07
1 5-1/2 8849-07 121.13
1-1/2 7 8849-09 172.94
2 7 8849-11 257.44
3 9 8849-13 417.86
4 12 8849-15 777.09
8856 PROCESS PIPE COUPLINGS Bead to Bead

Coupling assemblies consist of a 0.300 series stainless steel outer band with T-Bolt and
hex nut; Buna-N liner and a TFE seal ring.
No. 8856 coupling is designed for temperature service up to 450°F.
High Temperature – Buna-N Liner (450°, Black)

Max.
A B C D Torque, Order
Size (inches) (inches) (inches) (inches) in-lbs Code Each
1/2 1-5/8 1-3/8 7/8 3/16 20 8856-03 75.13
3/4 1-3/4 1-1/2 7/8 3/16 25 8856-05 89.96
1 2-5/8 1-7/8 1 3/16 35 8856-07 112.13
1-1/2 3 2-5/8 1-5/16 3/16 50 8856-09 126.08
2 3-1/2 3-1/8 1-5/16 3/16 60 8856-11 150.55
3 4-3/4 4-1/4 1-7/16 3/16 75 8856-13 266.40
4 6 5-1/2 1-1/2 3/16 80 8856-15 320.70
6 8-3/4 8 1-3/4 1/4 90 8856-17 607.58
Use catalog dimensions for piping layout as gasket thickness allowance is included.
8856
8862 PADDED PIPE HANGER with Mounting Foot

8862 Size Order Code Each
1-inch (25mm) 8862-03 14.82
2-inch (50mm) 8862-07 16.16
3-inch (76mm) 8862-11 32.43
8863 PADDED PIPE HANGER without Mounting Foot

8863 All hangers are zinc coated and have factory applied plastic sleeve to prevent glass-to-metal
contact. Use one hanger every 8 or 10 feet. Support all valves and gauges individually.
Size (inches) Order Code Each

1/2 8863-02 8.19
3/4 8863-04 8.19
1 8863-06 8.67
1-1/2 8863-08 11.91
2 8863-10 13.19
3 8863-12 19.52
4 8863-14 21.79

282 Process Pipe
8866 COUPLING ASSEMBLY Beaded to Conical End Pipe

To join beaded end pipe to conical end pipe. Kit includes two flanges, inserts,
bolts and TFE sheath gasket.

1" 8866-03 300.43
1½" 8866-05 316.33
2" 8866-07 334.87
3" 8866-09 360.90
Assembly Consists of...

Size (In.) Flange Insert Gasket 7190 Nuts & Bolts Qty.
1 8867-68 8867-76 8868-16 3/8 –16 x 2-1/4 4
8867-77
1-1/2 8867-69 8867-78 8868-17 3/8 –16 x 2-1/4 4
8867-79 Pressure rating limited to that of conical pipe
2 8867-70 8867-80 8868-18 3/8 –16 x 2-1/2 4 stem. Not to be used with beaded armored pipe.
8867-81
3 8867-71 8867-82 8868-19 3/8 –16 x 3 4
8867-83
8871 ADAPTER Beaded Process Pipe to Female NPT, 304 Stainless Steel
A 304 stainless steel adapter for matching glass beaded process pipe to male NPT
fittings, gauges and flanges.

3/4-inch beaded pipe to 3/4-inch female NPT 8871-20 219.66
1-inch beaded pipe to 1-inch female NPT 8871-22 285.01
1.5-inch beaded pipe to 1.5-inch female NPT 8871-24 338.95 8871
2-inch beaded pipe to 2-inch female NPT 8871-28 361.26
8872 ADAPTER Beaded Process Pipe to Sanitary Flange, 304 Stainless

Steel
A 304 stainless steel adapter with sanitary type flange on one end. Mates glass beaded
pipe to sanitary type flanges.

3/4-inch beaded pipe to 3/4-inch sanitary flange 8872-04 145.10
3/4-inch beaded pipe to 1-inch sanitary flange 8872-06 192.47
1-inch beaded pipe to 1-inch sanitary flange 8872-08 192.47
1-inch beaded pipe to 3/4-inch sanitary flange 8872-10 192.47
1-inch beaded pipe to 1.5-inch sanitary flange 8872-12 192.47
1.5-inch beaded pipe to 1.5-inch sanitary flange 8872-14 207.29
8872
1.5-inch beaded pipe to 1-inch sanitary flange 8872-16 192.47
1.5-inch beaded pipe to 2-inch sanitary flange 8872-18 209.64
2-inch beaded pipe to 1.5-inch sanitary flange 8872-22 207.29
8870 MALE THREADED ADAPTER 304 Stainless Steel 8870

Used to join threaded female fittings, valves and flanges to beaded pipe. Size, below, refers
to the bead and the NPT thread. Length, below, refers to the overall length of the adapter.
Size (Inches) Length (Inches) Order Code Each

1/2 2-9/16 8870-02 210.31
3/4 2-9/16 8870-04 219.66
1 2-9/16 8870-06 285.01
1-1/2 2-9/16 8870-08 338.95
2 2-5/8 8870-10 361.26
3 3-1/8 8870-12 420.48
Vacuum Controllers 283
14063 PRECISION VACUUM REGULATOR J-Kem Infinity II

Perfect for vacuum distillation, unit automatically compensates for leaks in the equipment
under test and maintains precise pressure, even in systems with a continuous gas purge.
This computer (built-in) controlled vacuum regulator maintains pressure in the range of 0.1
to 760 Torr (atm pressure) in test instruments with volumes as small as 1 mL. Standard
features include 16-step programmable pressure ramp and serial communications for
PC control and data logging. Specifications: Transducer — diaphragm is stainless
steel, accuracy to 0.1%, proof pressure 200%. Controller — regulation 0.015% of range;
Resolution 0.1 Torr of 0.01 psi; Vapor path materials are stainless steel and PTFE; Ramp
Rates are 100 Torr/sec to 0.1 Torr/hr.; Serial communications, RS232 (RS485 or USB
upon request).
14063 Description Power Order Code Each
Includes Netbook and pre-loaded control software 120v, 60Hz 14063-10 2741.60
Includes Windows 7 & XP compatible software 120v, 60Hz 14063-15 2373.60
Includes Windows 7 & XP compatible software 230v, 50Hz 14063-212 2373.60
14066 PROPORTIONING VALVES J-Kem, Stainless Steel

14066 Select one for use with digital vacuum regulator 14063-10, above.
J-Kem Model For Reactor Volumes Cv Orifice Size Order Code Each
PSV-2 1 mL to 2 L 0.033 0.040 in. 14066-01 485.00
PSV-3 25 mL to 4 L 0.055 0.055 in. 14066-02 485.00
PSV-4 100 mL to 22 L 0.068 0.063 in. 14066-03 485.00
PSV-5 1 L to 50 L 0.12 0.093 in. 14066-04 485.00
PSV-6 Large Capacity 0.37 0.147 in. 14066-05 1097.00
DVR-PNV Stainless Steel Needle Valve, improves regulation 14066-20 138.20
14061 VACUUM REGULATOR J-Kem, No Mercury

Connect to any vacuum pump or vacuum source, and then to any piece of equipment, to
regulate pressure, in most cases to ±1 Torr. A standard pressure ramp feature evacuates
equipment at a user-defined rate to eliminate bumping due to solvent degassing or
over-evacuation. Ideally suited for large volume distillations, rotary evporators and
vacuum chambers. Not recommended for small volume distillations or applications
which involve a continuous purge with gas. Designed for vacuum systems that run
continuously, such as oil-filled vacuum pumps, aspirators, or with systems that are
“always on,” like in-house vacuum systems. The unit regulates pressure by opening and
closing a valve that separates the vacuum source from the system being evacuated.
14061 J-Kem Model VAC Order Code Each

DVR-200 120 14061-08 1127.00
DVR-300 230 14061-20 1136.20
Recovers >99% of solvent 14062 VACUUM REGULATOR J-Kem, No Mercury

from rotary evaporators Designed for use with diaphragm vacuum pumps. In some systems,
Solvent DVR Pressure Solvent Time To Percent pressure is regulated by turning the vacuum pump itself on and off. This
(mm Hg) Volume ryness
D Recovery unit extends the life of diaphragm pumps by never forcing the pump to
start against an established vacuum, which can increase pump life by
Ether 475 Torr 340 mL 14.6 min. 99.6%
100%. Not pictured.
CH2CI2 300 Torr 360 mL 21.9 min. 99.8%
CH2CI2 100 Torr 255 mL 5.9 min. 99.5% J-Kem Model VAC Order Code Each
EtOAc 90 Torr 316 mL 17.0 min. 99.9% DVR-280 120 14062-10 1191.40
Toluene 50 Torr 273 mL 15.7 Min. 99.4% DVR-380 230 14062-20 1191.40

284
A Turbine..............................................................193, 199, 203
INDEX Accessories
Big Jar with Handles.........................................................229
Clamp Holder....................................................................232
Clamp, Hose Support, Stainless Steel................................233
Clamp, Quick Release.......................................................230
Clean-In-Place Sprayer.....................................................230
Containment Tray, Polyethylene.........................................234
Containment Tray, Polyethylene, with Spigot......................234
Containment Tray, Stainless Steel......................................234
Air Stirrers......................................................................209, 210
Allihn Condenser.....................................................................136
Amber Bottle...................................................................224, 228
Angled Condenser..................................................................141
Angled Funnel.........................................................................132
Arrow Stirrers.........................................................................209
Aspirator Bottle.......................................................................228
Auto-Reactor............................................................................88
B
O-Rings.............................................................................232
Side Shelf Support Stand...................................................230 Baffles
Solution Bottle, Plastic Coated...........................................223 Glass.................................................................................148
Solution Bottle, Plastic Coated, “Ace-Safe”........................223 PTFE.................................................................................148
Solution Bottle, Threaded Neck..........................................223 Temperature Probe............................................................148
Tilting Support Stand.........................................................233 Barret Type Receiver...............................................................140
Ace-Thred Adapter..........................................................124, 149 Bath Fluid...............................................................................244
Beaded Process Pipe..................................................... 268–276
Adapters
10mm...............................................................................193 Beakers
75° Side Arm....................................................................125 Big Jar with Handles.........................................................229
105 degree Side Arm........................................................125 Heavy Wall........................................................................229
105 degree Side Arm with Ace-Thred................................125 Pilot Plant..........................................................................229
Ace-Thred..................................... 48, 49, 123, 124, 125, 149 Pilot Plant Size..................................................................229
Beaded Pipe for Flush Valve..............................................129 Bearings
Bottom Drip, 1:5 PTFE Stopcock........................................265 5mm.................................................................................175
Bottom, UHMWPE or PTFE.................................................265 6mm.........................................................................175, 176
Bushing...............................................................48, 123, 124 8mm.................................................................................187
Circulator Hose.................................................129, 145, 235 9mm.........................................................................178, 179
Connecting, Heat Exchange Coil........................................129 10mm........................180, 181, 182, 183, 184, 185, 186, 187
Connecting, Outer Socket Joint.........................................126 19mm...............................................................194, 195, 200
Distillation.................................................................127, 129 28mm...............................................................................201
Electrode...........................................................................123 Aluminum Packing Box......................................................205
Giant.........................................................................124, 149 Debris Free.......................................................176, 186, 200
High Vacuum.....................................................................193 Debris Trap........................................................185, 195, 201
Lubricant Trap...................................................................193 Economy...........................................................................175
Maxi..........................................................................124, 149 Heavy Duty........................................................................194
Midi..................................................................................149 High Speed Vacuum..........................................................178
Mini..................................................................................123 High Vacuum.....................................................................183
Multineck, #7 Ace-Thred...................................................126 Mechanical Seal................................................183, 200, 201
Offset..................................................................49, 125, 126 Pressure.....................................................................48, 182
pH Probe...........................................................................127 PTFE..................176, 183, 184, 185, 186, 187, 195, 200, 201
Process Pipe.....................................................................277 PTFE-Clad.........................................................................180
PTFE.......................................................................18, 19, 44 Stainless Steel..................................................................184
PTFE, Bottom......................................................................19 Stirrer Assembly........................................................181, 184
PTFE Ferrule......................................................................123 Vacuum.....................................................................178, 179
Reducing...........................................................................123 Vacuum Stirrer Bearing Assembly......................................178
Stainless Steel..................................................129, 145, 235 Water Cooled....................................................175, 180, 194
Swagelok....................................................................44, 263 Bench Reactor Stand................................................................52
Thermometer......................................................................48 Big Jar with Handles...............................................................229
Twin Ace-Thred.................................................................124 Blanket, Flask Insulating.........................................................169
with Side Port......................................................................19 Bottles
Adjustable Pressure Relief Valve...............................................45 Ace-Safe Takeoff...............................................................223
Agitators Amber.......................................................................224, 228
10mm.......................................................................192, 193 Aspirator...........................................................................228
19mm.......................................................................198, 199 Cap, PTFE Lined........................................................226, 227
28mm...............................................................................203 Caps/Pouring Rings...........................................................225
Large Scale...............................................................199, 203 Carboy..............................................................................228
Multi-Paddle..................................... 192, 193, 198, 199, 203 Filtering.............................................................................228
PTFE................................................. 192, 193, 198, 199, 203 GL Thread.........................................................................224
Single Blade..............................................................192, 199 Laboratory........................................................................224
Stainless Steel..................................................................193 Plastic Coated...................................................................223
285
Polyethylene......................................................................228 Extended Arm......................................................................53
INDEX
Safety Coated....................................................................224 For 7519 Filter Support.....................................................231
Schott-Duran............................................................224, 228 For 15305 Conical Flange..................................................231
Solution.............................................................................223 For Flat-Style Flanges.......................................................231
Threaded Neck..................................................................223 For Lab Frames...........................................................51, 232
Wide Mouth.......................................................................228 Jumbo................................................................................52
with Removable Hose Connection......................................228 Pinch Type..........................................................................51
Bulb Condenser......................................................................141 Pinch Type, Stainless Steel................................................231
Buna-N O-Rings.............................................................237, 238 PTFE Lined........................................................................231
Bushings Quick Release.............................................................51, 230
Nylon..........................................................................44, 124 Stainless Steel.............................................. 52, 53, 235, 264
PTFE...........................................................................44, 124 Three-Prong........................................................................53
Vinylized Jaws....................................................................53
C Clean-in-Place Sprayer...........................................................230
Cold Finger Condenser............................................................137
Caframo Overhead Stir Motors................................................217 Collar, Glass-Filled PTFE..........................................................207
CAPFE O-Rings.......................................................................239 Collar, Stainless Steel..............................................................207
Caps Column Extenders for 5862 Column................................265, 266
GL Thread.........................................................................226 Column Heads For 5862 Column.............................................263
Gl Thread, Solid.................................................................260 Columns
GL Thread with Hole..........................................................260 #50 Ace-Thred..................................................................263
Pouring Rings....................................................................225 #80 Ace-Thred..................................................................264
PTFE Lined................................................................226, 227 Ace-Thred.........................................................................266
PTFE Membrane........................................................226, 227 Distillation................................................................ 263–264
Solid, SVL..........................................................................260 Large Size.........................................................................266
Tamper Evident.................................................................226
With Hole, SVL...................................................................260
Condensers
Allihn, with Ace-Thred.......................................................136
Carboys..................................................................................228
Allihn, with Ace-Thred Connectors.....................................136
Cart, Safety Lift.......................................................................236
Angled..............................................................................141
Chain Clamp...........................................................................232
Buchi........................................................................142, 251
CHEMRAZ O-Rings..................................................................241
Bulb Type..........................................................................140
Chiller.....................................................................................244
Coiled...............................................................................137
Chillers...........................................................................242, 243
Cold Finger................................................................136, 137
Chromatography High Capacity, Double Coil.................................................138
Ace-Thred Column............................................................266 Horizontal, Single Tube......................................................139
Large Size Column............................................................266 Internal Baffling.................................................................138
Polypropylene Screen Support Filter Discs.........................267 Large-Scale Rotary Evaporators................................142, 251
Screen Support Filter Discs...............................................267 Long Path..........................................................................137
Chucks Reflux, Bulb.......................................................................141
5mm.................................................................................177 Spiral................................................................................139
6mm.........................................................................177, 204 Splitter..............................................................................145
10mm.......................................................................193, 204 Triple Coil, High Capacity...................................................139
19mm.......................................................................200, 204 West...................................................................................49
28mm...............................................................................202 With Ace-Thred Connectors...............................................138
Flex-Grip................................................... 177, 193, 200, 204 Connecting Tubes, Large-Scale
Pass-through Assembly.............................................191, 197 Rotary Evaporator Glassware......................................254, 255
Circulator................................................................................244 Connectors
Circulator Hose Adapter..........................................................129 28mm...............................................................................202
Circulator Hose Clamp............................................................235 Motor Shaft to Chuck........................................................202
Clamps Tubing, Ace-Safe...............................................................128
76mm...............................................................................231 Tubing, Polypropylene.......................................................128
102mm.............................................................................231 Containers, Polyethylene.........................................................228
Chain................................................................................232 Containment Tray....................................................................234
Chain Clamp.......................................................................51 Cooler, Circulating...................................................................244
Circulator Hose.................................................................233 Couplings
Circulator Hose Clamp.......................................................235 Beaded to Conical End Pipe...............................................277
Clamp Holder..............................................................51, 232 Bead to Bead....................................................................276
Clamp Holder for LawJaws Extension Clamps.....................52 Process Pipe.....................................................................276
Clamp Holder for Pilot Plants...............................................53 Reducing, with Support.....................................................264
Clamp-To-Rod.............................................................51, 232 Stirring Shaft.....................................................................207
Conical Flanges.................................................................231 Cover, Evaporating Flask.........................................................258
286
D Receiving..........................................................................257
INDEX Digital Temperature Monitor....................................................151

Digital Vacuum Monitor...........................................................278
Disc, Rupture............................................................................45
Distillation
Apparatus, High Boiling.....................................................144
Splitter..............................................................................144
Distillation Adapter..................................................................129
Distillation Columns
Perforated Plate................................................................143
Robo Reactor Flask...........................................................111
Spherical, with Bottom Outlet..................................... 95–111
Spherical with ZDS Valve.....................................................96
Stainless Steel..................................................................110
Three-Neck.................................................................94, 112
Unjacketed....................................................................40, 41
Valve Types for Reaction Flasks...........................................92
Volumetric, Pilot Plant.......................................................112
with 4mm Bore Stopcock..............................................97, 98
ZDS Valve.......................................................... 41, 94, 96, 99
Flat Side Funnel......................................................................132
Perforated Plate, Internal Bellows, Silvered........................144 Flexible Stirring Shaft..............................................................204
Vacuum Jacketed..............................................................145 Fluorinated Grease..................................................................206
Distribution Head, Large-Scale Rotary Evaporator Glassware.....252 Fluorine Reactor, PTFE..............................................................55
Dual Motor Speed And Power Controller..................................220
Funnels
E Addition..............................................................50, 133, 134
Buchner, Polyethylene.......................................................130
Electrode Adapter...................................................................123 Buchner, Stainless Steel....................................................130
Electro-Flo Shut-Off Valve, Photochem....................................158 Filter Paper for Buchner Funnel.........................................130
End Cap, Extended..................................................................275 Flange Bottom...................................................................133
End Cap, Short........................................................................275 Heavy Wall........................................................................132
Ethylene-Propylene O-Rings...........................................237, 238 Jacketed...........................................................................134
Expansion Tank, Large-Scale Rotary Evaporator Glassware.....252 Offset................................................................................133
Powder.....................................................................132, 133
F Powder, Angled.................................................................132
Powder Dispensing...............................................49, 50, 131
FETFE O-Rings................................................................237, 238
Powder, Flat Side......................................................132, 133
Filter Disc.........................................................................48, 267
Powder, Heavy Wall...........................................................132
Filtering Bottle........................................................................228
Powder, Offset...................................................................132
Filter Reactors Pressure Equalizing.....................................................50, 134
Instatherm..........................................................................17 Pressure Equalizing, Graduated.................................133, 134
Jacketed.......................................................................14, 18 Pressure Equalizing, Pilot Plant..........................................134
Jacketed, Pressure Version..................................................15 Pressure Equalizing, PTFE Needle Valve Stopcock.............134
PTFE...................................................................................55 Vertical................................................................................50
Unjacketed..............................................................12, 16, 18
Unjacketed, Pressure Version..............................................13 G
Flange Styles, Guide...........................................................8, 112
Flask Heater...........................................................................171 Gasket, PTFE..................................................................207, 208
Flask Insulating Blanket..........................................................169 Gasket, Stainless Steel...........................................................207
Gauge, Pressure.....................................................................210
Flasks General Stirring Information....................................................172
4-Inch Flange......................................................................95 Girdle Mantle..........................................................................171
Amberized, Large-Scale Rotary Evaporator Glassware.......259
Glas-Col Heating Products......................................................166
Beaded Drain......................................................................93
Glass Frit Characteristics........................................................110
Bottom Outlet................................................................40, 43
Glass Glossary........................................................................290
Cylindrical, Piston Type Drain...............................................93
Glassware Assemblies for 13302 Rotary Evaporators..............249
Cylindrical, Sink Type Drain.................................................93
Glassware Assemblies for
Extension Support.............................................................233
Large-Scale Rotary Evaporators................................. 261–262
Flush Seal Drain..................................................................94
Heavy Wall..................................................................94, 112 GL Thread Bottle.....................................................................224
Indented............................................ 47, 95, 97, 99, 100, 259 GL Threaded Caps..................................................................225
Indented, Large-Scale Rotary Evaporator Glassware..........259 Graphite Rupture Disc...............................................................45
Instatherm..................................................................47, 111 Grease, Fluorinated.................................................................206
Jacketed............................................... 40, 43, 100, 112, 257 Grease, High Vacuum..............................................................206
Jacketed, Large-Scale Rotary Evaporator Glassware.........257 Guide to Flange Styles............................................................112
Large Evaporator...............................................................250 Guide to Ordering Custom Pilot Plants.......................................57
Large Receiver..................................................................250
Large-Scale Rotary Evaporator Glassware.................257, 259 H
Large-Scale Rotavap Glassware................ 250, 257, 258, 259 Hazardous Duty Overhead Stir Motor......................................219
Poly Coated, Large-Scale Rotary Evaporator Glassware.....259 Head, Distribution, Large-Scale Rotary
Pressure.................................................................40, 41, 43 Evaporator Glassware.........................................................252
Reaction, Spherical.............................................................96
287
Heads Filter Reactor.......................................................................17
INDEX
3 Necks.................................................... 114, 115, 116, 118 Robo Reactor Flask...........................................................111
4 Necks.................................... 113, 114, 115, 116, 117, 118
5 Necks............................................................113, 117, 119 J
6 Necks............................................................................118
Jacketed Flask................40, 43, 95, 97, 100, 105–109, 112, 257
7 Necks....................................................................118, 119
Julabo Bath Fluid....................................................................244
60mm...............................................................................119
Julabo Magnum 91 Recirculator.............................................243
60mm Side Port........................................................118, 119
Julabo Presto Series Recriculators..........................................242
100mm.............................................................115, 117, 120
Julabo Recirculator.................................................................244
100mm Side Port......................................................118, 119
Julabo Recirculator Accessories..............................................245
150mm.............................................................117, 118, 120
200mm.............................................................118, 119, 120 Julabo Tubing & Insulation......................................................245
300mm.....................................................................118, 119
Ace-Thred................................................... 41, 113, 114, 116
K
Conical Flange..........................................................114, 115 KALREZ O-Rings.....................................................................240
Coupling for KF Style Flange..............................................122
Domed......................................................................118, 119 L
Filter Reactor.................................................................41, 42
Filter Reactors...................................................................113 Lab Safety Controller..............................................................157
Flat Flange................................................................115, 116 Large-Scale Rotavap Glassware
Flat Glass..........................................................................113 Amberized Flasks..............................................................259
Flat Ground Flange....................................................117, 118 Cap...................................................................................260
Flat Stainless Steel............................................................113 Condensers/Coolers..................................................142, 251
Gasket for KF Style Flange................................................122 Connecting Tubes......................................................254, 255
Inserts for PTFE Heads......................................................121 Evaporating Flask Cover....................................................258
Joint Insert........................................................................113 Evaporation Flasks....................................................258, 259
KF-Style Flange.........................................................118, 119 Evaporator Flasks..............................................................250
Pressure Reactor.................................................................41 Expansion Tank.................................................................252
Pressure Reactors.............................................................113 For Heidolph Rotavaps......................................................250
PTFE.........................................................................119, 120 Glassware Assemblies.......................................................261
Schott-Duran Style Flange......................... 116, 118, 119, 120 Head.................................................................................252
Stainless Steel..................................................................115 Indented Flasks.................................................................259
Thermometer Joint............................................................116 Jacketed Receiving Flasks................................................257
Heater, Circulating..................................................................244 Poly-Coated Flasks............................................................259
Heating/Cooling Coil...............................................................152 Received Flasks................................................................250
Heating/Cooling Coil, Halar Coated..........................................152 Receiving Flasks...............................................................257
Receiving Tubes................................................................254
Heating/Mantles
Steam Tubes.....................................................................253
Aluminum Housing............................................................168
Traps.................................................................................253
Aluminum Housing Mantle........................................165, 167
Tubes................................................................253, 254, 255
Fabric Heating Tops...........................................................166
Valves...............................................................................256
For Cylindrical Flasks........................................................171
Vapor Duct Tubes..............................................................253
Girdle Type Mantle............................................................165
Vapor Tube........................................................................250
Hemispherical Mantle........................................................164
Spherical Mantle...............................................................164
Voltage Controller......................................................169, 170
M
Heavy Wall Flask.....................................................................112 Manifold.............................................................................20, 46
Heavy Wall Funnel..................................................................132 Mantles
Heidolph Overhead Stir Motors................................................212 Fabric Heating Tops...........................................................166
Heidolph Rotary Evaporators For Cylindrical Flasks........................................................171
Glassware Assemblies.......................................................249 Girdle Type........................................................................165
Labarota 20 Control Features....................................246, 248 Hemispherical...................................................................164
Labarota Control Economy................................................247 Spherical...........................................................................164
Laborota Automatic, Economy...........................................248 Metal Reaction Flask..............................................................110
Laborota Automatic, Safety................................................248 Metal Reaction Head...............................................................115
Laborota Safety.................................................................247 Mitered Elbow........................................................................274
High Boiling Distillation Apparatus...........................................144 Moisture Test Receiver, Barrett Type........................................140
High Vacuum Grease...............................................................206 Moisture Test Receiver, Pilot Plant...........................................140
Moisture Test Receiver, Pressure...............................................44
I
IKA Overhead Stir Motors........................................................215
N
Instatherm® Nylon Bushing..................................................................44, 124
288
O Adapter, Male Threaded.....................................................277
INDEX Offset Adapter.........................................................................125

Offset Funnel..........................................................................132
Offset Overhead Stir Motors....................................................219
O-Rings
Buna-N.....................................................................237, 238
CAPFE.......................................................................239, 263
Chemraz...........................................................................241
EPDM........................................................................237, 238
Ethylene-Propylene...................................................237, 238
Adapter, Sanitary Flange....................................................277
Adapter, Stainless Steel.....................................................277
Beaded Pipe......................................................................272
Coupling Assembly, Beaded to Conical..............................277
Couplings, Bead to Bead...................................................276
End Cap............................................................................275
End Plug...........................................................................275
Padded Pipe Hanger..........................................................276
Reducer Elbow..................................................................273
Reducer, Straight...............................................................275
FETFE.......................................................................237, 238 Sweep Elbow....................................................................273
For Ground Flanges...........................................................232 “U” Bend...........................................................................276
Kalrez...............................................................................240 Process Scale Filtration Reactors..............................................91
Silicone.............................................................237, 238, 263 Proportioning Valves...............................................................278
Viton.........................................................................237, 238 PTFE
Overhead Stir Motor Gear Box.................................................219 Adapter.......................................................................44, 123
Overhead Stir Motor Gear Reducer..........................................220 Agitator............................................. 192, 193, 198, 199, 203
Overhead Stir Motors...................... 212, 215, 217, 218, 221, 222 Baffles..............................................................................148
Bearing.............................................................................195
P Bushing.......................................................................44, 124
Packing Support...............................................................48, 267 Filter Reactor.......................................................................55
Padded Pipe Hanger...............................................................276 Gasket......................................................................207, 208
Perforated Glass Plate...............................................................19 Reaction Head Inserts.......................................................121
Reactor...............................................................................55
Photochemical Equipment Sparger Tube.......................................................................45
“Electro-Flo” Shut-Off Valve..............................................158 Stirrer Bearing............176, 183, 184, 185, 186, 187, 200, 201
Pilot Plant Reactor, 10L.................................................74, 75 Stirrer Blade......................................................191, 192, 198
Pilot Plant Reactor, 20L.................................................74, 75 Stirring Shaft.............................................................177, 198
Water Filter.......................................................................158 Stopper.............................................................................236
Water-Flo Power Cut-Off...................................................158 PTFE Lined Caps.....................................................................226
ph Probe.................................................................................127
Pilot Plant Support Stand........................................................230 Q
Pinch Clamp...........................................................................231
Pipe, Process................................................................. 268–276 Quick Disconnect Tubing...........................................................46
Plastic Safety Shield.................................................................47 Quick Release Clamp..............................................................230
Plate Support Shelf...................................................................53
Plug, Nylon...............................................................................44 R
Plug, PTFE................................................................................44 Reactors
Polypropylene Filter Discs.......................................................267 10 Liter..................................... 60, 61, 72–73, 74, 74–75, 75
Polypropylene Tubing................................................................45 10 Liter Pilot Plant Package.................................................89
Powder Funnel........................................................131, 132, 133 12 Liter.........................................................................58, 59
Pressure Equalizing Funnel.....................................................134 20 Liter..................................... 60, 61, 72–73, 74, 74–75, 75
Pressure Gauge......................................................................210 20 Liter Pilot Plant Package.................................................89
Pressure Manifold...............................................................20, 46 22 Liter.........................................................................58, 59
Pressure Reactors 30 Liter.............................................................62–67, 76–79
1 Liter...........................................................................21, 22 30 Liter Pilot Plant Package.................................................90
2 Liter...........................................................................21, 22 50 Liter...........................................59, 62–65, 76–79, 82–85
All-in-One.....................................................................21, 22 50 Liter Pilot Plant Package.................................................90
Bottom Outlet............................26–27, 30–31, 34–35, 38–39 72 Liter...................................................................59, 84–85
One-Piece Jacketed..........................................36–37, 38–39 100 Liter...............................................68–69, 80–81, 84–85
One-Piece Unjacketed.......................................32–33, 34–35 200 Liter.....................................................70, 70–71, 86–87
Two-Piece Jacketed..........................................28–29, 30–31 All-in-One...............................................................21, 21–22
Two-Piece Unjacketed.......................................24–25, 26–27 Auto-Reactor................................................................ 88–90
Pressure Relief Manifold.........................................................235 Complete......................................................................58, 59
Pressure Relief Valve................................................................45 Cylindrical.........................................................60–73, 76–81
Pressure Rupture Disc..............................................................45 Domed Head.................60–63, 68–73, 76–77, 80–81, 84–87
Probe, pH................................................................................127 Filter.............................................................................12, 55
Process Pipe Flask...................................................................................96
90° Short Radius Elbow....................................................274 Flat Head..............................................64–65, 78–79, 82–83
Adapter, Female NPT.........................................................277 Guide to Ordering Custom Pilot Plants.................................57
Jacketed...........................................................62, 66, 72–83
289
Low-Profile.................................................................. 82–83 Stainless Steel
INDEX
Offset Overhead Stir Motor................................................219 Adapter.............................................................................129
Overhead Stir Motor..................................................218, 219 Agitator.............................................................................193
Photochem....................................................................74, 75 Bearing.............................................................................184
Photochemical............................................................. 74–75 Clamp.................................................................53, 231, 235
Pilot Plant Beaker..............................................................229 Clamp Holder......................................................................52
Pilot Plant Clamp Holder......................................................53 Head.................................................................................115
Pilot Plant Condenser........................................136, 137, 140 Process Pipe Adapter........................................................277
Pilot Plant Standard Design Specs.......................................56 Proportioning Valves..........................................................278
Pressure Equalizing Funnel...............................................134 Stirrer Blade..............................................................191, 192
Process Scale Filtration.......................................................91 Stirring Shaft.....................................................187, 188, 189
PTFE...................................................................................55 Tubes, Large-Scale Rotary Evaporator Glassware..............253
Receiver, Moisture Test......................................................140 Stand..................................................................................51, 52
ROBO..................................................................................54 Stands
Spherical...........................................................84–85, 86–87 Bench Reactor....................................................................52
Three-Post Stand......................................................... 66–67 For Kilo Class Reactors................................................. 60–87
Unjacketed............................................60, 61, 64–71, 84–87 “H” Support Stand...............................................................51
Volumetric Flask................................................................112 Three-Post..........................................................................66
Receiver, Moisture Test...........................................................140 “T” Support Stand...............................................................52
Receiving Tubes, Large-Scale Rotary Evaporator Glassware....254 Steam Tubes, Large-Scale Rotary Evaporator Glassware.........253
Recirculator............................................................................244
Recirculators..................................................................242, 243 Stirrer Blades
5mm.................................................................................177
Recirculator Tubing & Insulation..............................................245
6mm.................................................................................177
Reducer Elbow.......................................................................273
10mm.......................................................................191, 192
Reducer, Straight....................................................................275
19mm...............................................................................198
Reflux Condenser............................................................141, 142
Banana Type.....................................................................192
Retainer Ring, PTFE..................................................................19
Oval..................................................................................191
RMI-1001-DH...........................................................................54
PTFE.................................................................191, 192, 198
RMI-1002-DH...........................................................................54 Stainless Steel..........................................................191, 192
RMI1003-DH.............................................................................54 Stirrer Lubricant..............................................................204, 205
RMI-1004-DH...........................................................................54
RMI-1005-DH...........................................................................54 Stirrers
RMI-1006-DH...........................................................................54 5-6mm Bearing.................................................................175
RMI-1007-DH...........................................................................54 5-6mm Bearing, Water Cooled..........................................175
5-6mm Blade....................................................................177
ROBO Reactor 5-6mm Economy..............................................................175
Complete............................................................................54 5-6mm Flex-Grip Chuck....................................................177
Instatherm Reaction Flask.................................................111 5-6mm Glass....................................................................175
Rotary Evaporator Glassware 5mm Shaft, Hollow Glass..................................................177
Heidolph Replacement Flasks............................................250 5mm Shaft w/PTFE Agitator..............................................177
Vapor Tube for Heidolph 4000 Series.................................250 6mm Bearing, Debris Free.................................................176
Rotary Evaporators.................................................246, 247, 248 6mm Bearing, PTFE...........................................................176
Rupture Disc, Pressure.............................................................45 6mm PTFE........................................................................176
9mm Bearing, High Speed Vacuum....................................178
S 9mm Bearing, Threaded....................................................179
9mm Bearing, Vacuum..............................................178, 179
Safety Coated Bottle...............................................................224
9mm Shaft................................................................178, 179
Safety Lift Cart........................................................................236
9mm Vacuum Bearing Assembly.......................................178
Safety Shield............................................................................47
10mm Adapter, High Vacuum............................................193
Screen Support Filter Discs.....................................................267 10mm Adapter, Lubricant Trap...........................................193
Screen Support, Polypropylene.................................................19 10mm Agitator, PTFE, Multi-Paddle....................................192
Short Radius Elbow.................................................................274 10mm Agitator, Single-Blade.............................................192
Side Shelf...............................................................................230 10mm Agitator, Stainless Steel, Multi-Paddle.....................193
Silicone O-Rings.............................................................237, 238 10mm Agitator, Stainless Steel, Turbine.............................193
Spargers 10mm Bearing..................................................180, 182, 183
Easy Action Stopcock, #7 Ace-Thred Connection...............146 10mm Bearing, Ace-Thred........................ 181, 182, 184, 185
Easy Action Stopcock, Hose Connection............................146 10mm Bearing, Debis Trap................................................185
Sparger Tube.......................................................................45 10mm Bearing, Debris Free...............................................186
Straight, #7 Ace-Thred Connection....................................147 10mm Bearing, Glass........................................................181
Straight, Hose Connection.................................................147 10mm Bearing, High Vacuum............................................183
Splitter....................................................................................144 10mm Bearing, Pressure...................................................182
Splitter Condenser..................................................................145 10mm Bearing, PTFE................................. 184, 185, 186, 187
290
10mm Bearing, PTFE-Clad................................................180 28mm Shaft, Heavy Duty...................................................202
INDEX 10mm Bearing, Water Cooled............................................180

10mm Blade, Banana Type................................................192
10mm Blade, Borosilicate Glass........................................191
10mm Blade, PTFE............................................................192
10mm Blade, PTFE, Oval...................................................191
10mm Blade, Stainless Steel.....................................191, 192
10mm Complete Assembly w/Glass Blade.........................181
10mm Complete Assembly w/Glass Shaft.........................184
10mm Complete Assembly w/PTFE Blade.................181, 184
10mm Complete Assembly, w/PTFE Blade.........................184
28mm Shaft, Polished.......................................................202
Aluminum Packing Box......................................................205
Collar, Glass-Filled.............................................................207
Collar, w/PTFE Gasket.......................................................207
Flex-Grip Chuck................................................................204
Flexible Shaft....................................................................204
Gasket, PTFE.....................................................................208
Heavy Duty Stirrer Lubricant..............................................205
Hi-Lube Stirrer Lubricant...................................................205
Krytox Fluorinated Grease.................................................206
10mm Complete Assembly, w/SS Shaft.............................184 Krytox High-Vacuum Grease..............................................206
10mm Flex-Grip Chuck.....................................................193 Matching Bearings to Shafts.............................................173
10mm Mechanical Seal.....................................................183 Shaft Coupling..................................................................207
10mm PTFE, Turbine.........................................................193 Stir-Lube...........................................................................204
10mm Shaft......................................................................186 Stirrer Packing..................................................................206
10mm Shaft, Borosilicate Glass.........................186, 189, 190 Stir Shaft Quick Reference................................................174
10mm Shaft,”C” Type........................................................189 Stopcock Lubricant...........................................................205
10mm Shaft, Ground Glass................................................190 Stirring/Mixing
10mm Shaft, Hollow Glass................................................190 Air Stirrer, Arrow, Heavy Duty.....................................209, 210
10mm Shaft, Polished Glass..............................................190 Air Stirrer, Arrow, High Torque............................................210
10mm Shaft, Precision Ground..........................................186 Air Stirrer, Arrow, Light Duty..............................................209
10mm Shaft, PTFE............................................................183 Air Stirrer Filter/Regulator/Lubricator.................................210
10mm Shaft, PTFE-Coated Glass.......................................187 Air Stirrer Pressure Gauge.................................................210
10mm Shaft, PTFE-Coated Steel.......................................187 Caframo Overhead Stirrers........................................216, 217
10mm Shaft, Stainless Steel.....................................188, 189 Dual Motor Speed And Power Controller............................220
19mm Agitator, Large-Scale..............................................199 Gear Reducer, 4:1 Reduction.............................................220
19mm Agitator, Multi-Paddle.....................................198, 199 Gear Reducer, 56C Flange.................................................220
19mm Agitator, PTFE.................................................198, 199 Heidolph RZR....................................................................212
19mm Agitator, Single Blade.............................................199 IKA Eurostar..............................................................214, 215
19mm Agitator, Turbine.....................................................199 IKA RW16 Basic................................................................214
19mm Bearing, Ace-Thred................................................195 IKA RW20 Digital...............................................................215
19mm Bearing, Debris Free...............................................200 Overhead Stirrers...................... 212, 216, 218, 219, 221, 222
19mm Bearing, Debris Trap...............................................195 Overhead Stirrers, Caframo...............................................217
19mm Bearing, Glass........................................................194 Overhead Stirrers, Gear Box..............................................219
19mm Bearing, Heavy Duty...............................................194 Overhead Stirrers, Hazardous Duty............................218, 219
19mm Bearing, Mechanical Seal.......................................200 Overhead Stirrers, IKA.......................................................215
19mm Bearing, PTFE.................................................195, 200 Overhead Stirrers, Offset...................................................219
19mm Bearing, Water Cooled............................................194 Overhead Stirrers, Pilot Plant.....................................218, 219
19mm Blade, PTFE....................................................198, 199 Overhead Stirrers, Reversing.............................................217
19mm Blade, Single Blade................................................199 Overhead Stirrer Support Stand.........................................221
19mm Borosilicate Glass...................................................197 Pressure Relief Manifold....................................................235
19mm Flex-Grip Chuck.....................................................200
19mm, Multi-Paddle w/Receptacle....................................199
Stirring Shafts
5mm.........................................................................175, 177
19mm Precision-Ground Glass..........................................197
6mm.................................................................................175
19mm, PTFE.....................................................................199
9mm.........................................................................178, 179
19mm Shaft, Borosilicate Glass.........................191, 196, 197
10mm....................................... 186, 187, 188, 189, 190, 191
19mm Shaft, Heavy Duty...........................................197, 198
19mm....................................................... 191, 196, 197, 198
19mm Shaft, Polished Glass..............................................196
28mm...............................................................................202
19mm Shaft, Precision-Ground Glass................191, 196, 197
C Type...............................................................................189
19mm Shaft, Precision PTFE.............................................198
Flexible.............................................................................204
28mm Agitator, Large-Scale..............................................203
Ground Glass.....................................................................190
28mm Agitator, Multi-Paddle.............................................203
Heavy Duty........................................................197, 198, 202
28mm Agitator, Multi-Paddle w/Receptacle.......................203
Hollow Glass.............................................................177, 190
28mm Agitator, PTFE.........................................................203
Pass-Thru.........................................................................191
28mm Agitator, Turbine.....................................................203
Polished Glass...................................................190, 196, 202
28mm Bearing, Ace-Thred................................................201
Precision-Ground Glass............................. 186, 191, 196, 197
28mm Bearing, Debris Trap...............................................201
PTFE......................................................... 177, 188, 197, 198
28mm Bearing, Mechanical Seal.......................................201
PTFE-Coated Glass............................................................187
28mm Bearing, PTFE.........................................................201
PTFE-Coated Steel............................................................187
28mm Connector, Flexible Beam.......................................202
Stainless Steel..........................................................188, 189
28mm Connector, Motor Shaft to Chuck............................202
Stopcock Lubricant.................................................................205
291
Stoppers Sensor Probes...................................................160, 161, 162
INDEX
PTFE.................................................................................236 Single Channel..................................................................156
Standard Taper, Full Length...............................................235 Thermocouples, J-Type.....................................................162
Standard Taper, PTFE........................................................236 Thermocouples, K-Type.....................................................162
Support Plate, Perforated, 73mm............................................264 Thermocouples, PFA..................................................160, 161
Supports Thermocouples, Plain................................................160, 161
Extension..........................................................................233 Thermocouples, PTFE........................................................160
Tripod........................................................................233, 234 Thermocouples, RTD-Type........................................161, 162
Support Shelf............................................................................53 Thermocouples, T-Type.....................................................162
Support Stand for 12” and 18” Columns.................................267 Water Flow Monitor...........................................................159
Support Stand for 24”, 48” or 72” Columns............................266 Temperature Probe.................................................................245
Support Stand for Heidolph Rotary Evaporators.......................247 Thermocouples
Support Stand, Overhead Stir Motor........................................221 Dual Sensor Cords............................................................163
Swagelok Adapter.....................................................................44 “J” Type....................................................................160, 162
Sweep Elbow..........................................................................273 “K” Type............................................................160, 161, 162
Needle Tip.........................................................................163
T PFA...........................................................................160, 161
Plain.........................................................................160, 161
Technical Information PTFE.........................................................................160, 161
ACE Glass Fiber Filter Discs...................................................7 PTFE Coated.....................................................................162
Chemical Resistance for Plastic Resins @ 20˚C...................10 RTD Type...................................................................161, 162
Conversion Factors................................................................6 Sensor Cords....................................................................163
Flask Stoppers......................................................................7 “T” Type............................................................................162
Fraction Conversion...............................................................5 Thermowell......................................................................42, 123
Glass Properties....................................................................7 Three-Neck Flask.............................................................94, 112
Guide to Flange Styles...........................................................8 Tilting Flask Support...............................................................233
Hose Connection Size Guide..................................................5 Traps, Large-Scale Rotary Evaporator Glassware....................253
O-Ring Compatibility Chart....................................................6 Tray, Containment...................................................................234
Plastic Properties..................................................................6 Tray, Containment, with Spigot................................................234
Pressure Conversions............................................................7 Tripod Support................................................................233, 234
Reference Guide to ACE Boiling Flasks..................................8 Tubes, Large-Scale Rotary Evaporator Glassware............253, 255
Reference Guide to Ace-Thred Sizes......................................5
Tubes/Tubing
Specifications for Joints........................................................5
Connector...................................................................46, 128
Specifications for Stopcocks.................................................5
Insulation..........................................................................245
Specifications for Threads.....................................................5
Metal................................................................................245
Standard Pipe Thread Fittings................................................9
Polypropylene......................................................................45
Sterilization Reference Guide.................................................9
Sparger Tube.......................................................................45
Viscosity Conversion Factors.................................................9
Tee, Reducing.........................................................................275
Tee, Straight...........................................................................274
U
Temperature Control “U” Bend................................................................................276
Complete Package............................................................150
Digital, Time Proportional Controller...................................153
V
Heat Exchanger Tubing......................................................153 Vacuum Apparatus
Heating/Cooling Coil..........................................................152 Digital Vacuum Monitor.....................................................278
Thermometer, Digital.........................................................151 Proportioning Valves..........................................................278
Thermowell, Without Joint.................................................151 Regulator, No Mercury.......................................................278
Temperature Controllers Regulator, Precision...........................................................278
230VAC.............................................................................156 Valves
Ace...........................................................................154, 155 0-20mm..........41, 96, 99, 103, 104, 105, 106, 108, 252, 254
Alarm for Water Flow Monitor............................................159 Adjustable...........................................................................45
Digital Temperature Monitor..............................................151 Bottom Outlet....................................................................265
Dual Channel....................................................................157 Large-Scale Rotary Evaporator Glassware.........................256
Dual Sensor Cords............................................................163 Pressure Relief....................................................................45
Dual Sensors, PTFE Coated...............................................163 PTFE Bottom Shut-Off.........................................................18
Economy...................................................................154, 156
Vapor Tube, Heidolph Rotary Evaporator..................................250
Four Channel.....................................................................157
Vapor Tubes, Large-Scale Rotary Evaporator Glassware..........253
General Laboratory............................................................155
Viton O-Rings..................................................................237, 238
Instatherm........................................................................156
Voltage Controller...................................................................170
J-Kem....................................................... 151, 156, 157, 159
Volumetric Flask.....................................................................112
Lab Safety.........................................................................157
Sensor Cords....................................................................163
292
INDEX Water Filter, Photochem..........................................................158

Water-Flo Power Cut-Off, Photochem......................................158
Water Flow Monitor................................................................159
Well, Thermometer..................................................................123
Wide Mouth Bottle..........................................................225, 228
Z
ZDS™ Valve.......................................................................94, 96
293
Cat. Page Cat. Page Cat. Page Cat. Page Cat. Page Cat. Page
No. No. No. No. No. No. No. No. No. No. No. No.
D120676................54, 111 6020........................... 139 6496............................231 7621....................225, 260 8094............................193 9541............................177
GLASS GLOSSARY
D120677........................54 6021........................... 139 6497........................... 110 7622....................225, 260 8095............................193 9542............................177
D124780........................54 6022........................... 139 6498........................... 110 7626............................226 8096............................192 9655......................47, 111
D127507........................54 6024......................49, 141 6499............................115 7627............................226 8098............................178 9656......................47, 111
D127590........................54 6029......................49, 141 6500............................123 7628............................226 8099........................... 179 10000......................89, 90
3965....................142, 251 6042............................141 6508............................231 7629............................226 8100........................... 199 10015..........................235
3967............................252 6046............................141 6509............................231 7631............................227 8101............................203 10165............................54
3970............................252 6087............................145 6510............................231 7632............................227 8111............................205 11057............................53
3971............................253 6088............................144 6512............................115 7633............................227 8112............................205 11065............................53
3973............................254 6228........................... 229 6513............................116 7647........................... 260 8113............................193 11067............................53
3974............................255 6231........................... 229 6515............................116 7669......................51, 231 8115............................206 11069............................53
3976............................253 6233........................... 229 6516............................. 99 7701..............................44 8116............................206 11079..........................232
3978............................256 6300........................... 110 6517..............51, 230, 264 7744........................... 140 8117............................204 11080....................51, 232
4048............................223 6310........................... 109 6518........................41, 99 7855............232, 237–240 8118............................205 11081....................53, 232
5021......................48, 123 6381..............................16 6519........................... 100 7859............................241 8119............................205 11082..........................213
5028......................48, 123 6384..................12, 13, 18 6525............................122 7885........................74, 75 8122............................206 11083............................52
5029............................124 6386..................14, 15, 18 6526......................47, 100 8036........................... 180 8124............177, 193, 200, 11160............................54
5030....................124, 149 6388..............................17 6527......................42, 116 8038........................... 180 204, 207 11173............................53
5031............................124 6390..............................55 6528.............. 42, 116, 117 8039........................... 180 8125............................207 12031..........................164
5032............................125 6391..............................55 6529..............42, 116–118 8040........................... 180 8126............ 191, 197, 207 12032......................... 169
5040............................125 6412............................113 6530....................118, 119 8041............................181 8127............................207 12035..........................164
5050............................125 6423..................24, 25, 40 6533............................107 8042............ 124, 149, 181 8128............................208 12036..........................165
5090............................125 6425..................26, 27, 40 6534............................108 8043............................182 8133............................178 12041..................165, 171
5221............................126 6427..................28, 29, 40 6535............................108 8044......................48, 182 8134............................178 12043..........................165
5263............................126 6429..................30, 31, 40 6536........................... 109 8047............................182 8250............................235 12044..........................165
5268....................126, 218 6433......................41, 113 6537........................... 109 8050............ 183, 200, 201 8318............................151 12045..........................166
5269............................. 49 6436.................. 32, 33, 41 6539..............................22 8051............................183 8767..............................45 12047..........................166
5278............................127 6437..................34, 35, 43 6540..............................96 8053............................183 8828............................272 12050..........................166
5299....................127, 129 6438..................36, 37, 43 6542..............................21 8055............................183 8830............................273 12053..................167, 171
5332........................... 229 6439..................38, 39, 43 6559........................82, 83 8059............................194 8831............................273 12058..........................168
5393............................223 6444..............................45 6563............................144 8060............................194 8832............................274 12067..........129, 152, 153
5395............................223 6445..............................45 6565............................143 8061............................194 8833............................274 12069..........................152
5539............................224 6448........................20, 46 6566............................144 8064............................184 8836............................274 12075......................... 169
5559............................228 6452............................146 6569............................145 8065............................194 8837............................275 12085..................169, 170
5814......................19, 267 6453............................147 6650..............................54 8066....................184, 185 8842............................275 12087......................... 170
5820............................266 6460..............................88 6701........................... 250 8067.... 124, 149, 195, 201 8845............................275 12094..........................233
5835............................265 6465........................72, 73 6702....................258, 259 8068............................186 8847............................275 12096..........................233
5838............................. 19 6469................58, 96, 132 6720........................... 259 8070............................187 8849............................276 12097..................233, 234
5839..............................18 6470......................59, 151 6726............................257 8071............................187 8856............................276 12100..........................233
5843............................264 6471..............................42 6727............................257 8073........................... 189 8862............................276 12110......................... 160
5844................18, 44, 263 6472 60–65, 72, 73, 6810........................... 140 8074........................... 189 8863............................276 12111..........................153
5846..............................44 76–79, 93, 94, 106, 129, 6945............................112 8075........................... 190 8866............................277 12113......................... 160
150, 202, 230 8870............................277
5848........ 19, 48, 264, 267 6989............................228 8076............................196 12125..........................154
6473.... 66–71, 80, 81, 107 8871............................277
5853............................128 7127............................112 8077............................196 12126..........................155
6474..................84–87, 96 8872............................277
5857......................19, 265 7233......................50, 131 8078............................197 12127..........................156
6478....................164, 171 9061............................123
5858............................128 7234......................49, 131 8079............................198 12135......................... 160
6482..............................94 9074............................125
5860............................263 7236............................132 8080............................202 12136..........................161
6483..............................94 9089............................126
5861......................19, 265 7238............................132 8081............................204 12140......................... 160
6484............................114 9485......................50, 131
5862................... 263–266 7239............................131 8082............................191 12141..................160, 161
6485............................114 9488............................132
5867............................266 7245............................132 8083............................191 12160..........................158
6486............................114 9524............................175
5868............................267 7250....................132, 133 8085....................191, 198 12162..........................158
6487............................114 9527............................175
5945............................136 7252............................133 8086............................191 12164..........................158
6488............................114 9528............................178
5946............................136 7278............................134 8087............................192 12165..........................158
6489............................115 9529............................175
5958............................136 7281.........................., 134 8088............................192 12167..........................157
6490............................115 9530........................... 179
5960............................137 7295............................133 8089............................192 12168......................... 159
6491..............................97 9532........................... 190
6012............................137 7297....................133, 134 8090............................193 12169......................... 159
6492..............................98 9533........................... 190
6015............................138 7298......................50, 134 8091............198, 199, 203 12177..........................148
6494....................169, 171 9534............................175
6016............................138 7299............................. 50 8092........................... 199 12180..........................162
6495...... 54, 101, 231, 232 9535............................177
6017........................... 139 7506..............44, 124, 149 8093....................199, 203 12181..........................162
294
Cat. Page Cat. Page Cat. Page Cat. Page Cat. Page Cat. Page
No. No. No. No. No. No. No. No. No. No. No. No.
12182..........................162 12314..........................157 12840............................52 13302..................247, 248 13523..........................215 13650..........................222

GLASS GLOSSARY
12183..........................162
12184..........................163
12318..........................156
12322..........................156
12858....................55, 119
12860......................... 120
13365......................... 209
13370......................... 210
13530..........................221
13532......................... 220
13850..................188, 197
13852..................188, 197
12187..................129, 235 12327..........................151 12862......................... 120 13372......................... 210 13542..........................213 14061..........................278
12190..........................163 12477..........................228 12864......................... 120 13385......................... 210 13543..........................213 14062..........................278
12191..........................163 12517............................46 12866..........................121 13443..................176, 187 13544..........................213 14063..........................278
12193..........................148 12560......................... 130 12867..........................121 13445..........176, 186, 200 13550............................51 14065..........................278
12254..........................244 12563......................... 130 12869..........................121 13500..........................211 13554..........................218 14066..........................278
12256..........................244 12631..........................236 12871..........................121 13501..........................211 13555......................... 220 14108..........................244
12262..........................242 12633..........................236 12990..........................127 13504..........................211 13557..................219, 220 15616..........................236
12274..........................243 12634..........................236 13010..........................233 13507....................54, 212 13565..................216, 217
12299..........................245 12675..........................245 13219..........................234 13511..........................212 13566..........................217
12300..........................245 12677..........................245 13220..........................234 13514..........................214 13586....................52, 221
12307..........................245 12681............................45 13270............................47 13517..........................215 13590............................54
12312..........................157 12770............................18 13286......................... 250 13520..........................214 13649..........................221
Manufactured Products in this catalog:

Manufacturer Pages
Arrow.................................................................... 211–212, 215
Baldor................................................................... 222
Briskheat.............................................................. 169
Caframo................................................................ 218, 219
Cowie................................................................... 119 –121, 178, 188–190, 199, 202
Dupont.................................................................. 239, 240, 242
Glas-Col............................................................... 164 – 169
Greene, Tweed & Co............................................. 243
IKA........................................................................ 216 – 217
Heidolph............................................................... 213–214 , 248 – 251
J-Kem................................................................... 156, – 158, 161 – 162, 280
Julabo................................................................... 244 – 247
Contact Ace for our full reusable glassware catalog and general laboratory catalog.
295
Airline —A long, straight line within the glass piece. This is Check —A fissure in the glass not extending through the
GLASS GLOSSARY
usually caused by a long, gaseous inclusion. thickness of the glass. A surface crack.
Anneal, Lehr —The same meaning or end result: remov- Chill Mark —A wrinkled surface condition caused by working
ing the strain from the glass. Different processes, however. glass below the working point or working glass too cold.
Annealing is usually accomplished with a flame or annealing
oven where the part is stationary and is brought up to the Chip —A small piece of glass broken away from the main
strain point temperature and then cooled, thus removing any piece of glass, or the residual mark left after a piece is broken
strain in the glass. Lehring or annealing can also be accom- off.
plished via a long belt lehr that gradually takes the glass up Cold Seal —When glass is incompletely joined at a tempera-
to the annealing point and then gradually takes it back down ture below the working or softening point. Usually has bubbles
to room temperature as it moves on the belt through the hot or waves at the joint. Incomplete glass flow.
zone.
Concentricity —A measure of, or the lack of uniformity of,
Annealing Point —The temperature corresponding to a rate the wall thickness throughout a tube.
of elongation of 0.0136cm/min when measured by ASTM
method C336 test for annealing point and strain point of glass Cord —A narrow band of glass having a stringy appearance
by fiber elongation. The test describes a cooling rate of ap- different from the main glass. Streak of differing glass within a
proximately 4cm/min with a fiber of approximately 0.065cm tube or rod. Sometimes caused by an un-melted compound in
O.D. and a suspended load of 1000g. The annealing point the mixture.
numerically approximates log = 13 poises, where internal Crack —A fissure that goes all the way through the surface.
stress is substantially relieved in a few minutes. To state this
more simply: the temperature at which the glass is relieved of Crystallization —A crystalline structure. A mass of glass
strain and stress. particles or silica particles clumped together. Sometimes used
to describe a clump of un-dissolved material.
Bead —Enlarged edge on a tube or piece of glass. Beakers
have a bead on the top edge or lip. Devitrification —A crystal-like growth on the surface of the
glass. Appears frosted.
Belt Center-less Grind —Removes glass from the outside of
a tube or rod in a horizontal motion with an abrasive belt. Dielectric Constant —The ratio of the parallel capacitance
of a capacitor with the material as the dielectric to the capaci-
Bevel —To grind away an edge at an angle, or to take off a tance of the same capacitor with a vacuum as the dielectric.
sharp edge on the glass. Customer may call out break edge or The dielectric constant determines the amount of electrostatic
chamfer edge. Can be on the I.D. or O.D. energy, which can be stored in a material per unit volume, per
Blank —The parison or preliminary shape from which a unit potential g
radient.
finished piece is formed. Any glass piece that further work will Dielectric Loss Factor —The product of the dielectric
be performed to finish it. constant and the dissipation factor. At low values (below one),
Blister —A gaseous inclusion trapped in the glass. Also the dissipation factor is less than 5% different than the power
called a bubble. factor, so the power factor can be used for most calculations.
The power loss in a dielectric is directly proportional to the
Bloom —A cloudy surface that reappears on the glass due to loss factor if voltage gradient and frequency remain constant.
aging and other factors. Sometimes it shows as cloudy area
after reworking glass from excess carbon vapor. A condensing Dimple —An imperfection, usually a bump or depression,
vapor or compounds in the glass that reform after molding. caused by forming the glass.
Blown-ware —Term for glass pieces that are predominately Discolored Glass —A lead deposit or surface discoloration
blown free or partially in a mold while still hand blowing the caused by carbon or etching. Not removed by cleaning.
glass. Volumetric lab ware is still blown by free hand. Some Etch or Etched —Usually means chemically altered glass,
large bottles or flasks are still called blown-ware. such as acid etched glass. “Etch” can also mean weathering.
Bow or Camber —Straightness of tubing measured as the We actually etch the markings on pieces with acid.
maximum deviation from a straight line connecting any two Expansion Coefficient —The average increase in length per
points on the tube. More accurately, it’s the LACK of straight- unit length per degree C change in temperature over the range
ness. 0 -300 degrees C.
Bubble —See inclusion or blister. Forming —The shaping of hot glass.
Center-less Grinding —To remove glass from the outside End Work or End Finish —The end of a tube or rod is held
diameter of a tube or rod without regard to the inside diameter against a moving belt or a disk perpendicular to the belt.
or wall tolerance.
Finish —Has several similar meanings: the threads on a
Concentric Grinding —To remove glass from the outside threaded piece or neck; the joint on a neck; a bead; the polish
of a tube using the inside diameter as a reference. Usually or grind; the stage that a piece of glass is free of seeds.
ground on end centers on a lathe or mandrel.
Fire Cracks —Cracks in the glass caused by temperature
shock form overheating a specific point.
296
Fire Polish —Using fire, torch, hand-held torch or bottomer Mandrel —Generally a round device or reverse “mold” that
GLASS GLOSSARY
line to fire polish the end of a tube or rod. To actually melt and
seal the end and to “glaze” it.
Flame Cut —Heating by direct flame a piece of glass and
pulling until it separates.
hot glass is pulled over or shrunk onto. Used for precision
bore shrinking and redraw tube pulling. Also used for capillary
tube pulling. Can be made of steel or other metals and materi-
als.
Melting Temperature —The temperature in the furnace
Flat Glass —Window panes, microscope slides and micro- where the molten state of the particular glass formula is
scope cover glasses, usually “floated” molten onto a water or reached.
oil bath. Collected when it’s cooled down. Floated or poured
into a flat mold and cooled. Sometimes pressed or “cast” Molded Glass —Molten glass that is poured or blown into
flat. The Pilkington process —glass is poured and rolled flat mold. The glass with air pressure then takes on the shape of
between rollers and annealed in continuous sheet. the mold. Also, see paste mold. Beakers, flasks and most art
glass and all types of consumer ware products are “molded”.
Fold —A surface line caused by incomplete joining of two The I.S. process —the process for molding bottles which
pieces of glass. blows a parison first and then the full bottle in a second mold.
Glass Lathe —Used to horizontally hold a piece of glass and Mold Mark —The mark left on a piece of glass after molding,
rotate while working it. Can also be used vertically. Can have A seam.
fire ring or burner ports or be used with blowtorch or hand
torch. Opaque —Dense, or not clear.
Glass “Tank” or Furnace —Where the batch is injected or Open Blister —An open gaseous inclusion at the surface of a
dumped into a tank made of refractory brick and heated to piece of glass.
molten temperatures. This is where raw molten glass is pulled
from to be pulled, blown, or shot into molds. A borosilicate Out of Round —A different way of expressing concentricity,
tank can be at temperatures as high as 1800-2000 degrees C. or stating that the piece is more oval than round.
Glass Tubing or Rod —Pulled downward through a bell or Plunge Grind —Set up a stop in the grinder so as to grind
mandrel out of a furnace and then pulled horizontally on a only a portion of the length of the tube.
“draw,” or line, that is heated in stages to keep the glass at its Pressed Glass —Hot glass that is poured molten into a
working point while air is blown back up the center to keep two-piece mold and then formed in the mold by mechanical
the I.D. Solid rod or cane is formed the same way, except pressure.
without the air stream. The bell, air pressure and speed of the
draw determine the basic O.D. and I.D. (See Danner Process, Reboil —This phenomenon, which results in the formation of
Down-draw). tiny visible bubbles, shows as white lines in the surface and
interior of the glass. Usually caused by water vapor or other
Glaze —The same as fire polish contaminants. Sometimes caused by pulling tubing to fast.
Grinding —Remove layers of glass or imperfections using an Redraw —The process whereby you reheat glass tubing or
abrasive belt or wheel. rod and re-pull it through heat zones to lengthen it and make
Hackle Marks —Fine ridges on the fracture surface of glass it smaller in O.D. NOT shrinking. The difference between
parallel to the direction of the crack propagation on the sur- re-draw and precision bore is that the tolerances of precision
face. bore are tighter and more consistent throughout the tube sec-
tion.
Hand Tooling —To shape glass while hot by using a hand
tool that is shaped to the desired form. Can be turned on roll- Refractive Index —The ratio of the speed of light in vacuum
ers or a lathe and worked. to the speed of light through the particular glass. The value of
the refractive index is given for the sodium D line (589.3mu)
Hard Glass —Generally denotes borosilicate glass. Refers to and the values listed are for annealed glass.
glass possessing extremely high viscosity at elevated temper-
atures. A glass with a high softening point. Difficult to scratch. Scale —A small piece of extraneous oxide or carbon embed-
ded in the glass. Can be caused by dirty mandrels.
Interface —Where two pieces of glass, particularly different
types of glass, meet. Score —Significantly scratch the surface in a straight line.
Knot —A transparent stone in the glass. Non-homogeneous Scratch —A major surface abrasion. A long surface indenta-
glass. tion caused by reworking or an outside force.
Lathe Shrink —Mandrel is held horizontally and tube is Seals, Graded —Glass “seals” made from gradients or rings
shrunk onto mandrel that is attached to a lathe and rotated. of different glasses, usually shaped into a tube that can be
The burner is moved horizontally along the length. used to join glass pieces or components with wide variation in
coefficient of expansion.
Lead Glass —Glass with high lead content as in crystal ware,
stem ware. Also, flint glass. Seam —Either a mold mark or the area where two pieces of
glass are joined together.
Liquid Hone —Same as above, only more of a slurry.
Seed —Small blister (gaseous inclusion), less than .030 in
diameter.
297
Silk Screen Process —The process of decorating glass by TIR (Total Indicator Reading) —This is the maximum dial
GLASS GLOSSARY
applying paint or ink through a steel mesh screen. variation from the data or reference point when measurements
of the I.D., O.D., wall thickness, camber, etc. of a precision
Snap Cut —Score and apply hand pressure on the score until bore tube are taken.
it snaps.
Tubing, Redraw —Process in which glass tubing or rod is
Stability —Resistance to weathering; chemically durability. reheated and redrawn (pulled), to make a smaller I.D. or O.D.
Standard Taper —Is the diameter of the large end on the tube or rod. Capillary tubing is usually redrawn. Micropipettes
joint and the length of the taper, i.e. ST 19/22 is 2mm length are usually from redrawn tubing.
and 19mm diameter at the top. Tubing, Shrinking (Precision bore) —Glass tubing is reheat-
Stones —An imperfection or crystalline contamination in the ed and shrunk, by pulling a vacuum on to a precision mandrel.
glass. Type I Glass —Often misunderstood, it is US Pharmacopeia
Strain/Stress —A condition of tension or compression from (USP) standard for glass for containers for pharmaceutical
molding, working, cutting, grinding or drawing of raw molten packaging. Not ASTM. It does denote or describe a clear
glass. Usually can’t be seen but may be seen with a Polari- borosilicate glass formula. The slightest deviation in % of an
scope. Shows as a rainbow or interference patterns. ingredient for borosilicate would knock it out of Type I class.
Even amber borosilicate is not Type I. “Type I” doesn’t denote
Strain Point —The temperature corresponding to a rate of glass lab ware classes.
elongation of 0.00043 cm/min. when measured by ASTM
method C336. This test prescribed a linear extrapolation of Type I, Class A —Conforms to Federal Specification DD-G-
the data obtained in the annealing point determination to the 541b and ASTM E-438 is for borosilicate glass lab ware for-
above designated rate. Internal stress is substantially relieved mulation and specifications. Some glass meets all three specs
at the strain point in a few hours. such as Corning 7740 (Pyrex).
Stringer —An imperfection usually running along the length Wall —Thickness of the piece between the I.D. and O.D.
of a tube, usually caused by the slow solution of a large grain There is standard, medium, and heavy wall tubing.
of sand or foreign material. Wave —An uneven optical effect due to uneven glass distri-
Stones —An imperfection of crystalline contaminations in bution.
glass. Wet Cut —Cutting a piece of glass by using a water-cooled
Taper —The maximum gradual dimensional change in the wheel or saw. Actually, the new definition is where water is
O.D. of a tube or rod from one end to the other or from one introduced at extreme pressure and cuts through a surface
point to another on a rod or tube. “S over T” is standard taper (water jet).
used on joints. Working Range —The temperature range that a piece or
Temper —The degree of residual stress in annealed glass type of glass is heated to be able to be “worked” or formed.
measured polarimetrically against a standard. The temperature at which the glass becomes slightly elastic
but holds its main shape and can be reshaped.
Tempering —To improve strength, a heat treatment or
chemical treatment that can induce controlled compression Young’s Modulus —The measure or modulus of elasticity.
on the surface of the glass. Vycor is chemically strengthened The stress required to produce a unit change of length.
or tempered glass. Glass can be rapidly cooled (iced) after
being heated to the softening point and create a tempering vs
annealing.
Thermal Shock —A sudden, very rapid change in tempera-
ture that causes the glass to crack or break.
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P.O. Box 688 • Vineland, NJ 08362-0688 • 856-692-3333 • Fax: 856-692-8919

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www.aceglass.com email: sales@aceglass.com

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Specifications In case of Shortage:

Special Apparatus PLEASE NOTE:

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Order by Code ACE Glassware Discounts

Shipments are F.O.B. our factory

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Reference Guide to Ace‑Thred Sizes Fraction Conversion

24/40 24/40 35/25 35/25 #25 O‑Ring

Threads, and Stopcocks

Symbol designates spherical joints 25 16.2/56

0-5 mm Orifice Oblique

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Low Density High Density

O‑Ring Compatibility Chart

Length Volume Power

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Flask Stoppers ACE Glass Fiber Filter Discs

76 760 760000 1 14.7 1.06 1033 33.9 29.9 0.00 0.00

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Reference Guide to ACE Boiling Flasks

Guide to Flange Styles

Uses Clamp: 6508, 6509, 6510 Flat clamp

Conical Flange I.D. O.D. Thickness

Uses Clamp: 6496 Standard clamp

KF Plane Flange I.D. O.D. Thickness

Uses Clamp: 6525 Coupling

Uses Clamp: 8856 Coupling

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Standard Pipe Thread Fittings

The illustrations are

Sterilization Reference Guide

Viscosity Conversion Factors

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Chemical Resistance for Plastic Resins @ 20˚C

Resin Codes Chemical Resistance Classifications

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ACE Filter Reactors allow single

Major Design Chuck Typical

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See page 51 for stands.

(For #80, bottom also available with 1/2" MNPT.)

Glass Filter Discs

(For #80, bottom also available with 1/2‑inch MNPT.)

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6386 JACKETED FILTER REACTOR «

#50 / 5838 or / #80 5857

(For #80, bottom also available with 1/2‑inch MNPT.)

6386 JACKETED FILTER REACTOR, PRESSURE VERSION «

Stand (13586) and Support #50 / 5838 or / #80 5857

See page 219 for stands.

(For #80, bottom also available with 1/2‑inch MNPT.)

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Head, only Body, only Complete

Filter Reactor Accessories and Replacement Parts

Instatherm Heated Filter Reactor ®

Use with either regular or pressure version head and accessories.

Flange Bottom Body Approx. Top

ACE Custom Glass

Filter Reactor Accessories and Replacement Parts

6384 FILTER REACTOR Unjacketed, Body only

6386 FILTER REACTOR Jacketed, Body only

5839 VALVE PTFE, Bottom Shut Off