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I. Abstract
1. rgo/pva membrane
- High selectivity of 51.2
- Low permeate flux of 0.056 kg.m-2h-1)
2. go/pva exhibited an
- Acceptable selectivity of 34.9, however
- Equivalent permeate flux of 0.120 kg.m-2h-1
II. Materials and methods
Materials:
1. PVA (molecular weight and the degree ofsaponification were 80,000 and > 98 %, respectively)
2. Sulfuric acid (98wt%)
3. Sodium nitrate (99wt%)
4. Hydrogen peroxide (30wt%)
5. Hydrazine hydrate (35wt%)
6. MA (99 wt%)
7. Graphite (particle size: < 50 µm, density: 20-30 g/100 mL)
8. Potassium permanganate (> 99.5 wt%)
9. Ethanol (96 vol%)
Preparation
I. GO/rGO
1. Chemical oxidation modified Hummers’ method Graphite oxide GiO
2. 0.5gGiO
1. 500 ml deionized water
2. sonicated 12 h
GO(aq)
centrifugated
Wet GO washed
deionized water
GO( pH 6)
dried
60C ;24 h
GO
3. 0.1gGO 100 ml
deionized water
GO(suspension)
1. 5 ml hydrazine solution
2. stirred ;30 mins
1.centrifugation
2.washed (deionized water )
rGO
3. sonicated ;4 h 3. drying 60C ;24 h