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revealed that the average particle size of the composite decrease from 40nm to
30nm when the PH value increased from 9-11. The raw materials that was used
for this purpose were iron nitrate nonahydrate [Fe (No3)3. 9H2OAR] Cobalt (II)
nitrate hexahydrate [CO (NO3)2. 6H2O AR] Zinc nitrate hexahydrate [Zn (NO3)2
following properties can be confirmed. When the PH value is 5 then the Fe 2O3
phase exhibits. Then the Fe2O3 impurity exhibits when the pH value approaches
to 8. The Fe2O3 phase disappears when the pH values becomes 9. When the
Fe2O3 phases disappear then all the diffraction peaks can be ascribed to Cobalt
Zinc ferrite phase. The TEM characterization shows that the particle size
increases with the increasing pH value when the pH is 9 than the particle size is
about 30nm, when the particle size is 40nm then the pH value is 11. It is known
that nucleation and aggregation are two important process during the particle
formation.
Manju Kurian and Co-workers worked on the nickel zinc ferrite nano-
samples were also calcinated at different temperature mean that at 500 oc.
Through XRD, bulk density and porosity can also be calculated properties of
nano-crystalline nickel Zinc ferrite particles prepared using the sol-gel auto-
were found to exhibit cubic spinel structure with size varying from 17 to 40nm.
The observed peaks in FIIR spectra confirmed the information of ferrites. It was
also found that the temperature has no effect on the agglomeration of the ferrite
samples except in the case of SGE sample. TEM pictures agree with the XRD
data. Yan Liang and co-workers studied the spinal structure of ZnO/Zn Fe2O4
electronic micro-scopy, high resolution TEM. All the main XRD diffraction
peaks can be well indexed to hexagonal Zno with Wurtzite structure and
crystallized Zn Fe2O4 in cubic spinel-type structure with the space group. FTTR