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Premium Laboratory Equipment

2018
Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership
Support made easy
While you concentrate on research, we´ll look after your support needs
As we want you to have more time to concentrate thoroughly on your research,
the whole Heidolph team enthusiastically provides you with extensive support
and helps to reduce your workload.

www.heidolph.com

[ What‘s in it for me? [


Watch our corporate video and learn about all benefits
and services of Heidolph and our partners!

S
eit der Firmengründung vor über 75 Jahren steht Heidolph Instruments für hochqua-
litative und zeitgemäße Laborgeräte –Available at www.heidolph.com
Made in Germany. Unsere strikten Qualitäts- and
grundsätze und ein kundenorientierter Service haben on
unserour Youtube-Channel!
Wachstum untermauert
und doch muss man zu jeder Zeit die Zeichen der selbigen erkennen. In unserer schnellle-
bigen Umwelt, in der neue Technologien einen verkürzten Lebenszyklus aufweisen und der
rasante Fortschritt einen neuen Takt dirigiert, ist es wichtig, dass ein Unternehmen dyna-
Research made easy
misch und erfinderisch zu Werke geht und nichts als gegeben akzeptiert.

Unser neues Logo steht sinnbildlich für ein neues Kapitel in unserer Firmengeschichte
Our Service Commitment:
welches alte Stärken bewahren und neue mit sich bringen soll. Mit dem Engagement und • Guaranteed response to any • Repair turn-around time within • Installation and training on site
request within 24 hours 4 working days
der Kreativität unserer Mitarbeiter entwickeln wir Laborgeräte die neue Maßstäbe setzen
• Application support by
werden und die dem tiefsten Wünschen der Anwender gerecht werden. Neue Technologien • Lead times below 2 weeks for • The most common spare parts chemists
standard equipment are locally available
werden zudem ungeahnte Möglichkeiten aufzeigen, die das Forschen effektiver, einfacher
und sicherer machen wird, damit Sie auch in Zukunft sorgenfrei Forschen können. • Free demo evaluation units for • Immediate after-sales service
up to 14 days provided by more than 80
distributors worldwide

Our Quality Commitment:


• Increased lifespan of 10 years on • Long-lasting service life of • Low product failure rates
average all products due to corrosion-
resistant electronics and
• Reduced maintenance and spare maintenance-free motors
parts cost over the entire lifespan

3-year warranty - without compromises

2 3
As a leading manufacturer of laboratory equipment, we are an innovative and
globally active company. With a local footprint in more than 80 countries,
we support pharmaceutical research, the cosmetics industry, the biology as
well as the chemistry sector with our products and services, significantly
contributing to improving the quality of people’s lives all over the world.

Our organization is headquartered in Schwabach, a city within close proximity


to Nuremberg, Germany. It is here that the development and production of our
equipment as well as the coordination of our domestic and international sales,
marketing and customer support activities take place.

Respect for the personal and professional development of our employees has
created a strong commitment to success, resulting in a dynamic period of growth
and prosperity for the Heidolph organization. As a result, the Heidolph team is
continuously striving to achieve industry-leading product quality and customer
service while maintaining a strong customer-focused approach to developing
products and services that help to improve the efficiency of scientific research.

5
Summary
Hei-VAP Rotary Evaporators Intelligent Evaporation 10

Hei-VAP Industrial Large-Scale Rotary Evaporators Industrial Evaporation 36

Hei-VOLUME Automatic Modules Automated 24/7 Evaporation 50

Hei-PLATE Magnetic Stirrers Safe Heating and Mixing 62

Hei-TORQUE Overhead Stirrers Powerful Stirring 82

Hei-MIX Shakers and Mixers Temperature-Controlled Shaking 100

Made in Germany Hei-FLOW Peristaltic Pumps Precise Dosing and Dispensing 122

Hei-Lab App - Technical Service 144


“Made in Germany” is an internationally recognized quality seal for reliability, long
performance life and low failure rates. In an era of accelerated economic globalization ISO Certificate 146
this is becoming an important competitive factor. Heidolph Instruments is
committed to designing and manufacturing premium high-quality products Premium Distributors 147
exclusively in Germany.
Imprint 149
Schleswig-
Holstein
Mecklenburg-
West Pomeranai
For all components, Heidolph has defined the This accounts for product adjustments and Hamburg

highest quality standards: Maintenance-free for production volume equally. A high level
Bremen
Berlin
motors “Made in Germany” eliminate down of innovation in combination with short lead Lower Saxony

times, frequent warranty periods and costly times make your Heidolph purchase a truly
Saxony-Anhalt
repairs – it‘s for these reasons that we stand worthwhile investment, considering the North Rhine-
Westphalia
behind our products designed to provide you average operational lifespan of 10 years!
Saxony

years of continuous operation. Our Thuringia

Hesse
Germany-based R&D and production
Rhineland-
facilities allow for responding to customer Palatinate

requests quickly. Saarland

Schwabach

Baden-
Württemberg
Bavaria

6 7
Improve
your
evaporation process

8 9
Intelligent
Evaporation

Hei-VAP Rotary Evaporators

Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership


Leading Safety Standards

• Two independent safety circuits avoid an double wall for your protection against handles with safety grip to protect you
overheat situation of your heating bath: burns and scalding from scalding bath liquids and allow for
If bath temperature overshoots by 5 °C easy installation/removal of the bath
and if your water bath runs dry, heating • The guard hood covers the bath even if
will be switched off automatically the heating bath is adjusted horizontally • A separate on/off switch for heating
to its most extreme limit prevents unintentional heat-up. The
• To avoid an overtemperature situation button is illuminated for visual control
and potential thermal damage to your • A metal guide between the heating
sample, you can individually pre-program bath and the base unit prevents bath • In case of an overshoot of any parameter
a maximum temperature on the Hei-VAP instability setting, all models will show a warning
Precision, at which the bath powers off on the operating panel
• To protect your heating bath against
• In case of a power cut, all motor lift mod- short-circuits and systematic corrosion, • Glassware assemblies are optionally
els will remove the flask from the heating the cable coupling complies with the available with transparent plastic safety
bath preventing safety hazards and protection class IP 67 coating ensuring ultimate protection
potential thermal damage to your sample while allowing visual control at all times
• For your protection, the operating panel
• To protect you from splashes and is located underneath a protective canopy • IQ-OQ documentation is available
scalding, the Hei-VAP heating bath so as to keep your hands out of the for Hei-VAP models on request
features an integrated pour spout to dangerous zone of rotating flasks, steam
remove bath fluid safely and splashing bath fluids

• Heating bath is constructed with a • All heating baths feature non-slip

Do you demand the highest safety


standards, perfectly engineered ease Hei-VAP heating bath
of use and reduced cost of ownership?

YO UR ADVANTAGE S

• The Hei-VAP heating bath reaches


a temperature of 210 °C

Intelligent Evaporation... • The universal heating bath can even


accommodate 5-liter flasks

• The heating bath can be adjusted


horizontally up to 200 mm
... stands for an overheat protection design that prevents water baths
running dry, provides a detachable panel for superior ease of use from • To prevent short circuits and corrosion,
the cable coupling complies with the
outside closed fume hoods and offers a proven vacuum seal and vapor protection class IP 67
tube system guaranteed for years of operation!
• Non-slip handles for safe transportation
eliminate the risk of scalding

• An integrated pour spout to remove bath


fluid safely

Patented Grease-free
210 °C clamping sleeve IP 67 Easy-Clip sealing technology
Detachable panel XL condenser XL-Kühler

12 13
Superior Ease of Use

• The detachable operating panel enables • The universal heating bath can be • The optional automatic module
convenient handling from outside adjusted horizontally up to 200 mm and Distimatic Bench-top allows for
closed fume hoods offers efficient space to accommodate continuous and unattended
even 5-liter flasks automatic operations
• The patented evaporating flask clamp
Easy-Clip cannot be lost due to a • The innovative ventilation and • All components in direct or indirect
connection to the vapor tube replenishment valves no longer have contact with the medium are equipped
coupling ring ground joints, which enables maximum with FDA-compliant materials for an
tightness, grease-free operation and extended application range
• The integrated screwed ring allows you prevents glass breakage
to remove sticking evaporating flasks
from the vapor tube just in seconds in a • For your convenience, the height
safe manner of 160 mm and the angle of the
evaporating flask can be adjusted
easily from 20° to 80°

Reduced Cost of Ownership

• Achieve up to 40 % higher evapora- drive is made of PPS (Polyphenylene significantly: the automatic module
tion rates due to unique tightness and sulfide), a robust industrial-designed resin Distimatic Bench-top is an affordable
industry-leading condensing surface with with superior chemical resistance which and more flexible alternative to
the XL condenser provides more chemical resistance than large-scale rotary evaporators
stainless steel or welded aluminum. This
• The high resistant and durable PTFE reduces corrosion to a minimum which • Reduce your maintenance costs. The
vacuum seal achieves maximum tight- results in additional savings sealed housing protects your rotary
ness and reduces spare part budgets on maintenance and replacement evaporator from aggressive fumes,
components liquids and vapors to prevent internal
• The patented clamping sleeve ensures corrosion. This results in an increased
a long life performance of the vapor • Spend your working hours more lifespan of 10 years on average at a
tube effectively on other challenges which reduced maintenance and repair cost
require your attention and evaporate
• Increase your range of applications by large quantities continuously with the
using 5-liter flasks in the universal bath automatic module Distimatic Bench-top
at no additional cost

• Maintenance-free and non-sparking


motors reduce repairs and down
times significantly to ensure years of
continuous operation
• The flange on the condenser side of the • Maximize your initial investment

14 15
Intelligent
Vapor tube with patented clamping
sleeve
Evaporation
Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership
YO UR ADVANTAGE S

• The patented clamping sleeve system allows The average operational lifespan of 10 years is backed by a 3 year warranty and
easy removal of the vapor tube from the drive
makes your purchase a worthwhile investment.
• Years of performance life reduce your spare
parts budget up to 75 %

• The Hei-VAP vapor tube does not get stuck in Achieve up to 40 % higher evaporation rates
the drive, thus eliminating the risk of broken due to tightness and industry-leading 2,200 cm²
glass condensing surface with the XL condenser

• Immediate removal of the vapor tube from the New, FDA-compliant,


drive facilitates your work transparent and uv-resistant
The new highly resistant PTFE vacuum seals
tubing, with higher chemical
allow for long lasting constant application
resistance
and reduce spare parts budgets. Also
available as FFKM version for application
with extremely aggressive solutions

Patented flask clamp Easy-Clip Superior ease of use due to the patented
Easy-Clip, which provides an easy removal
of sticking flasks and non-sticking vapor
YO UR ADVANTAGE S tube with patented clamping sleeve that
eliminates broken glass and reduces
• Easy-Clip can’t get lost due to a direct spare parts cost significantly
connection to the drive

• The integrated screw thread allows an easy The innovative ventilation


210 °C Safety heating bath
with handles and pour spout
removal of sticking flasks
and replenishment valves
will power off if temperature
no longer have ground
• The Easy-Clip is made of highly resistant joints, which enables
overshoots by 5 °C or runs dry
synthetic material which ensures a long life
maximum tightness,
performance
grease-free operation and
prevents glass breakage

Operating panel Bath power cable


coupling complies with
protection class IP 67 to
The detachable operating prevent corrosion and
YO UR ADVANTAGE S
panel enables safe and short circuits

• Changing all parameters from outside closed easy handling from


outside closed fume hoods
fume hoods guarantees the highest safety
level

• Standard for all models is a panel with


1 m cable connection. Thus data security is
guaranteed at any time

• Immediate access to the panel ensures


ultimate control of the process while For unlimited evaporation: A separate on/off switch for A metal guide between
increasing your ease of use In conjunction with the automatic module heating prevents unintentional the heating bath and
Distimatic Bench-top allows you unlimited heat-up – the button is the base unit prevents
• A separate on/off switch for heating prevents and automated distilling in 24/7 operation. illuminated for visual control bath instability
unintentional heat-up – the button is An affordable alternative to large-scale rotary
illuminated for visual control evaporators

16 17
Hei-VAP Value / Hei-VAP Value Digital Hei-VAP Advantage

Superior ease of use due to direct control Wide range of possibilities for reproducible results
The Hei-VAP devices with hand lift are optimally suited for all standard applications. With the Hei-VAP Advantage you have a direct view on all parameter settings and
Controlling parameters is done so with the simple turn of a knob are able to expand your application range

• The convenience of large dial controls for adjustment of


rotation speed and bath temperature
• Available in hand lift or motor lift configurations
• Hei-VAP Value Digital models come with a digital display • Experience the advantages of our large digital 3.5“ LCD
for set and actual heating bath temperature display which indicates rotation speed, heating bath and
vapor temperature

• Experience the advantages of the automatic process


timer which turns off your evaporator at a pre-
programmed time and removes evaporating flasks from
bath on motor lift models

Adjust the required angle


• Upgrade your Hei-VAP Advantage to a Hei-VAP
Precision:
of the evaporating flask individually
according to your needs

Limit the height of your evaporating


flask in just seconds
Upgrade-KIT
Advantage Precision-HL
The patented flask clamp Easy-Clip P/N 569 - 30009 - 00
allows a simple and safe removing of
the evaporating flask due to the force Upgrade-KIT
of unscrewing the Easy-Clip Advantage Precision-ML
P/N 569 - 40009 - 00

Large digital LCD display which


For your protection, the detachable allows you to monitor all
operating panel is located below parameters even from a distance
the bath and outside the danger
zone. To conveniently run your unit
Convenient motor lift adjusts
from outside a fume hood, detach
height by the press of a
your panel and place it in your
button
preferred location

Hei-VAP Value Digital HL/G3 Hei-VAP Advantage ML/G3 XL


P/N 560 - 01302 - 00 P/N 562 - 01305- 00

Model Hei-VAP Value hand lift (HL) Hei-VAP Value Digital hand lift (HL)
Model Hei-VAP Advantage hand lift (HL) Hei-VAP Advantage motor lift (ML)
Glassware standard coated standard coated
Glassware standard coated standard coated
G1 Diagonal 560 - 01100 - 00 560 - 01110 - 00 560 - 01102 - 00 560 - 01112 - 00
G1 Diagonal 561 - 01100 - 00 561 - 01110 - 00 562 - 01100 - 00 562 - 01110 - 00
G3 Vertical 560 - 01300 - 00 560 - 01310 - 00 560 - 01302 - 00 560 - 01312 - 00
G3 Vertical 561 - 01300 - 00 561 - 01310 - 00 562 - 01300 - 00 562 - 01310 - 00
G3 XL Vertical 560-01305-00 560-01315-00 560-01307-00 560-01317-00
G3 XL Vertical 561-01305-00 561-01315-00 562-01305-00 562-01315-00
G5 Dry Ice Condenser 560 - 01500 - 00 560 - 01510 - 00 560 - 01502 - 00 560 - 01512 - 00
G5 Dry Ice Condenser 561 - 01500 - 00 561 - 01510 - 00 562 - 01500 - 00 562 - 01510 -00
G6 Vertical for Reflux 560 - 01600 - 00 560 - 01610 - 00 560 - 01602 - 00 560 - 01612 - 00
G6 Vertical for Reflux 561 - 01600 - 00 561 - 01610 - 00 562 - 01600 - 00 562 - 01610 - 00

18 19
Hei-VAP Precision

Maximum capabilities due to integrated vacuum control »» Reduce your process times significantly via automated distillation programs
The Hei-VAP Precision provides you with the maximum range of parameters, including
but not limited to, reproducible applications and fully automated processes. Even
For automated distillation choose between these three programm opportunities:
solutions with different boiling points can be identified and distilled

SETpressure
Program: SETpressure
Program for solvent separations
• Available in hand lift or motor lift • Now you can manage even the most • Each ramp offers 20 separate steps for Control parameter: manually set pressure

configurations demanding applications easily and demanding applications

1000 mbar
This program holds a pre-set vacuum constant. During the
prevent foaming, excessive bubbling or
evacuation you have the full flexibility to choose another level
• Experience the advantages of our large bumping • Apply an individual name to those ramps to of vacuum by the press of a button. Optionally, the process
4.3” color graphic display which features all avoid a mix-up
can be predefined via programmable ramps
parameters, integrated vacuum controller •
Save time with your individualized
and includes programs for automated pre-programmed parameter settings • Experience the advantages of the
distillations for your 30 most common applications automatic process timer which turns off
used on a daily basis by saving them in a your evaporator at a pre-programmed time
• Make your life easier by utilizing the ”Favorites” section by raising the flask on motor lift models
Manually set vacuum

integrated software support which leads you and releasing vacuum


through the capabilities of the evaporator
• Control your process individually by pre- AUTO easy
• For data management Hei-VAP Precision programming vacuum gradients
Program: AUTOeasy
models feature a USB interface Control parameter: pressure
Supports the automatic pressure control for solvent separations
• Hei-VAP Precision models feature a built-in
• Save time by configuring the unit - all

1000 mbar
vacuum controller as a standard The pressure level for the first boiling point is found automatically.
connected devices will be recognized This program can be used with all Heidolph glassware assemblies and
by the evaporator, which eliminates the does not require any accessories
need to configure the unit manually

Finds boiling point automatically and holds vacuum constant

AUTO accurate
Program: AUTOaccurate
Control parameter: vapor temperature Supports very precise automatic pressure control for solvent
Hei-VAP Precision ML/G3 separations
P/N 564 - 01300 - 00

1000 mbar
This program works similar to AUTOeasy but in addition is able to
For increased safety all bath identify multiple boiling points automatically by reducing vacuum
temperature adjustments can be accordingly. Also the AUTOaccurate program delivers the finest and
limited most precise vacuum control. To take advantage of this program,
the optional AUTOaccurate-sensor is required. This program cannot
Stop be used on Heidolph G1 and G5 glassware assemblies. Leading
Even from a distance you will be Final vacuum individually adjustable parameter of this program is the vapor temperature
able to monitor the numbers on the Finds multiple boiling points automatically
display easily

Large color graphic


Hei-VAP Precision Hei-VAP Precision
display for all parameters Model
hand lift (HL) motor lift (ML)
and automated programs
Glassware standard coated standard coated
G1 Diagonal 563 - 01100 - 00 563 - 01110 - 00 564 - 01100 - 00 564 - 01110 - 00

G3 Vertical 563 - 01300 - 00 563 - 01310 - 00 564 - 01300 - 00 564 - 01310 - 00

G3 XL Vertical 563-01305-00 563-01315-00 564-01305-00 564-01315-00

G5 Dry Ice Condenser 563 - 01500 - 00 563 - 01510 - 00 564 - 01500 - 00 564 - 01510 - 00

G6 Vertical for Reflux 563 - 01600 - 00 563 - 01610 - 00 564 - 01600 - 00 564 - 01610 - 00

20 21
Glassware Accessories
Evaporating flasks NS 29/32 NS 24/29
• Glassware set includes one 1,000-ml • Evaporating flasks and vapor tubes which • Innovative ventilation and replenishement Evaporating flask* 50 ml 514 - 70000 - 00 514 - 70000 - 01
evaporating flask and one 1,000-ml come with a standard NS 29/32 joint size valves without ground joints for easy
Evaporating flask 100 ml 514 - 71000 - 00 514 - 71000  - 01
receiving flask are also available with NS 24/29 ground handling and grease-free operation are
Evaporating flask 250 ml 514 - 72000 - 00 514 - 72000 - 01
joints included
• All glassware sets are also available with Evaporating flask 500 ml 514 - 73000 - 00 514 - 73000 - 01

transparent plastic coating for added • Also available upon request: glassware • Glassware sets G3 and G6 allow for Evaporating flask 1,000 ml 514 - 74000 - 00 514 - 74000 - 01
safety 1 sets for Soxhlet extraction and the automated distillation program Evaporating flask 2,000 ml 514 - 75000 - 00 514 - 75000 - 01
descending condenser system AUTOaccurate on Hei-VAP Precision
Evaporating flask 3,000 ml 514 - 76300 - 00 514 - 76300 - 01
models
Evaporating flask 5,000 ml 514 - 78000 - 00 514 - 78000 - 03

* Evaporating flask NS 14.5 incl. adaptor (NS 29 or NS 24)


XL Condenser
Receiving flasks standard coated
For maximum evaporation performance Receiving flask - S 35/20 100 ml 514 - 81000 - 00 514 - 81000 - 02

Receiving flask - S 35/20 250 ml 514 - 82000 - 00 514 - 82000 - 02


The new XL condenser with industry-leading condensing
surface of 2,200 cm2 achieve up to 40 % higher evaporation Receiving flask - S 35/20 500 ml 514 - 83000 - 00 514 - 83000 - 02

rates. Available in G3XL, G3B XL and G92 XL versions Receiving flask - S 35/20 1,000 ml 514 - 84000 - 00 514 - 84000 - 02

Receiving flask - S 35/20 2,000 ml 514 - 85000 - 00 514 - 85000 - 02

Receiving flask - S 35/20 3,000 ml 514 - 87000 - 00 514 - 87000 - 02

Glassware set G1 Glassware set G3/G3 XL


Powder flasks NS 29/32 NS 24/29

• Diagonal condenser for all standard distillations; the option • Vertical condenser for all standard destillations; the Powder flask 500 ml 514 - 73200 - 00 514 - 73200 - 01
with the most affordable price option with the smallest space requirements, also Powder flask 1,000 ml 514 - 74200 - 00 514 - 74200 - 01
available as XL version
Powder flask 2,000 ml 514 - 75300 - 00 514 - 75300 - 01

Spider NS 29/32 NS 24/29


Spider with 6 distillation sleeves NS 14,5 20 ml 15 - 300 - 005 - 09 15 - 300 - 005 - 12

Spider with 12 distillation sleeves NS 14,5 20 ml 15 - 300 - 005 - 10 15 - 300 - 005 - 13

Spider with 20 distillation sleeves NS 14,5 20 ml 15 - 300 - 005 - 11 15 - 300 - 005 - 06

Glassware set G5 Glassware set G6


Spider NS 29/32 NS 24/29

• Dry Ice condenser for low-boiling solvents • Vertical condenser; centerpiece with valve for reflux
Glassatz G1 NS29/32
Glassatz G3 NS29/32 Spider with 5 flasks NS 24 50 ml 15 - 300 - 005 - 04 15 - 300 - 005 - 08

distillation Spider with 5 flasks NS 24 100 ml 15 - 300 - 005 - 07 15 - 300 - 005 - 05

Evaporating cylinder NS 29/32 NS 24/29


Evaporating cylinder 500 ml 514 - 00070 - 00 514 - 00070 - 01

Evaporating cylinder 1,500 ml 514 - 00071 - 00 514 - 00071 - 01

Foam brake NS 29/32 NS 24/29


Foam brake with flask clamp 514 - 00004 - 00 514 - 00005 - 00

1 Convenient for temperature range up to 80 °C


2 for the usage of Deistimatic Bench-top
Glassatz G5 NS29/32

Glassatz G6 NS29/32

22 23
Accessories Vacuum Pumps

Advantages of all chemical-resistant diaphragm vacuum pumps

• All components which come in contact • The direct pump drive (without belt) is
with media are built from chemically exceptionally quiet, creates a very low
resistant fluoropolymer vibrational environment and reduces
the need of wear and tear parts to a
• The durable PTFE design guarantees an minimum
superior diaphragm lifespan
Guard hood Guard shield Vapor temperature sensor • The gas ballast valve has been optimized
P/N 569 - 00010 - 00 P/N 569 - 00020 - 00 P/N 569 - 00030 - 00 • The head cover and clamping disc have to prevent media condensing
a stable core made of metal which offers in the pump
• Strong and transparent guard hood to • Strong and transparent guard shield for • For Hei-VAP Advantage and Hei-VAP unsurpassed long-term performance of
your operational parameters
protect you from implosions your protection while changing flasks Precision
• Provides easy and immediate access • Attached at the edge of the bath
to flask and bath

RPM-Regulated Vacuum Pumps


AUTOaccurate-sensor Tubing Vacuum seal
P/N 569 - 00040 - 00 P/N 591-35000-00 (package 12 m) P/N 23-30-01-01-30 (PTFE/FKM)
P/N 591-33000-01 (by meter) P/N 23-30-01-06-70 (PTFE/FFKM)
»» Highest distillation rates possible and reducing process time by 30 %
• For Hei-VAP Precision
• Only in combination with glassware set • Tubing for vacuum and water • Standard PTFE / FKM spare seal »» Stable distillation conditions account for solvent recovery up to 99 %
G3 and G6 connection. Available as package • Ultra resistant PTFE / FFKM seal
(12 meter piece incl. hose clamps) or in for applications with highly abrasive
YO UR ADVANTAGE S
individual length (by meter) solutions
• Inner diameter: 8 mm
• Speed adjustment stops
• Outer diameter: 13 mm
completely if vacuum is reached
and runs intermittently at very
Fully automatic control with speed adjustment
low speed to hold vacuum
recovery rate constant

Pressure
• Increased diaphragm performance
life due to periods of non-
operation

= continuous evaporation • Low energy consumption due to


intermittent operation
Aqua-Stop Spare clamping sleeve Heating bath liquid
P/N 569 - 00500 - 00 P/N 23 - 30 - 01 - 05 - 31 P/N 569-00600-00 Time
• Significant noise and vibration
reduction due to periods of non-
The integrated valve closes automatically • Heating bath liquid up to 220 °C (5 kg) RPM regulated pumps adjust their speed individually when the required vacuum
operation
by turning off the evaporator. The level is reached
system saves money by reducing your
consumption of cooling tap water.
Spare vapor tube NS 29/32
P/N 514 - 00000 - 01
• Operates without vacuum valve
Moreover the safety mechanism avoids
flouding in your laboratory. (Only for Hei-
• Most precise vacuum level at all
times
VAP Advantage and Hei-VAP Precision)

24 25
Valve-Regulated Vacuum Pumps RPM-Regulated Vacuum Pumps

Standard vacuum pumps can be controlled manually or via valve operated vacuum Controllable vacuum pumps for digital regulation of the vacuum via operation panel or
controllers directly at the unit (depending on version - see below)

Rotavac Valve Tec Rotavac Valve Control Rotavac Vario Tec Rotavac Vario Control Rotavac Vario Pumping Unit

Rotavac Valve Tec Rotavac Valve Control Rotavac Vario Tec Rotavac Vario Control Rotavac Vario Pumping Unit
P/N 591 - 00160 - 00 P/N 591 - 00130 - 00 P/N 591 - 00171 - 00 P/N 591 - 00141 - 00 P/N 591 - 00142 - 00
Condenser Condenser Condenser Condenser Condenser
P/N 591 - 00083 - 00 P/N 591 - 00083 - 00 P/N 591 - 00084 - 00 P/N 591 - 00084 - 00 P/N 591 - 00084 - 00

For all For all For For Fully controllable stand-alone pumping
Hei-VAP models Hei-VAP models Hei-VAP Precision Hei-VAP Precision unit including vacuum controller.
For Hei-VAP Value and Hei-VAP
Advantage

Diaphragm pump Two-stage Two-stage Two-stage Three-stage Three-stage

Suction capacity m3/h 0.75 2.0 1.0 1.7 1.7

Ultimate vacuum mbar 12 7 12 2 5

Combinable
yes yes yes yes yes
with a condensor

Power input Watt 80 180 160 160 160

Weight kg 6.0 12.8 4.3 5.4 6.0

Dimensions L/W/H mm
145 / 315 / 169 195 / 245 / 310 156 / 236 / 196 167 / 236 / 196 193 / 263 / 299
(without condenser)

Specifications per unit Recommended for solvents with low or medium Suction capacity for up to three rotary evaporators at the Recommended for solvents with low or medium Even if the gas ballast valve is open an excellent Precise vacuum control avoids bumping and eliminates
boiling points same time boiling points ultimate vacuum is reached when working with easily foaming of your evaporation solution
condensable vapors. This makes distilling high boiling
Vacuum can be controlled via valve operated or manual Vacuum can be controlled via valve operated or manual point solvents such as DMF or DMSO possible at low Due to automatic vacuum supply to the process
vacuum controllers vacuum controllers bath temperatures parameters you have more time for important
laboratory activities
Depending on your application you can switch on and off
the vacuum pump via switchbox

26 27
Vacuum Accessories Chillers

Switchbox Manual vacuum controller Vacuum valve RotaChill Large Rotacool Mini RotaChill Small
Connect up to three rotary evaporators For Hei-VAP Value and Hei-VAP Required to control vacuum for Highest cooling capacity Ideal for standard applications The affordable model
to one vacuum pump Advantage Hei-VAP Precision models with
valve-regulated pumps

Switchbox Manual vacuum controller Vacuum valve


P/N 569 - 00400 - 00 P/N 591 - 26000 - 00 P/N 569  -  00060  -  00

• Connect up to to three rotary • Control your house vacuum or any • External attachment design for easy
evaporators to one pump and control other vacuum source cleaning RotaChill Large Rotacool Mini RotaChill Small
vacuum individually P/N 591 - 00240 - 00 P/N 591 - 00210 - 00 P/N 591 - 00220 - 00
• Pressure range from 0 to 1,020 mbar • Can be combined with the Woulff
• Pump switches off automatically at Bottle to one unit
• Highest cooling capacity for any • Chiller for all standard applications • Temperature range from 0 °C to
required vacuum • Scaling on display in steps of 50 mbar application +100 °C
• Not required if you utilize a Manual • Temperature range from -10 °C to
• Reduces energy consumption of pump • Connection for tubes with 8 mm inner vacuum controller
• Temperature range from -20 °C to +40 °C • Precise temperature control accuracy
diameter
+40 °C of ±0.2 °C
• Increases performance life of the pump
• Temperature control accuracy of ±1 °C
due to a complete switch-off if vacuum • Support rod included • Temperature control accuracy • The RotaChill Small should be placed
is reached
• A vacuum valve is not required Woulff bottle of ±0.1 °C • Digital display for temperature settings directly besides the evaporator to
and reading out actual temperature ensure a sufficient pump performance
• Vacuum valve and non-return valve
• Digital display for temperature setting
are required for every evaporator if you • Dimensions: L80 / W80 / H150 mm P/N 569 - 00070 - 00
and reading out actual temperature • Cooling capacity at +20 °C: 580 W • Footprint of chiller:
work with different pressures at the
L450 / W210 / H570 mm
same time
• Additional recovery of solvent to • Cooling capacity at +20 °C: 1,290 W • Footprint of chiller:
protect vacuum valve and vacuum L360 / W310 / H520 mm
• Delivery includes three non-return pump
• Footprint of chiller:
valves
L607 / W254 / H483 mm
• Compatible with all Hei-VAP
• Designed for Hei-VAP Precision configurations

• Weight: 0.6 kg • Direct connection to the vacuum valve


is possible
• Dimensions: L80 / W160 / H45 mm RotaChill Large Rotacool Mini RotaChill Small

• Features connection to vacuum Temperature range [°C] -20 to +40 -10 to +40 0 to +100

controller Coolant volume [L] 2.7 3 6

Cooling capacity* at: +20 °C [W] 1,290 580 200

• Volume of 250 ml 0 °C 750 370 140

-10 °C - 80 -

-20 °C 260 - -

* at 20 °C ambient temperature

28 29
Equipment Combinations Overview of Hei-VAP units

With the Hei-VAP series you can easily assemble your individual laboratory equipment - Rotary Evaporator Vacuum source Accessories
exactly to your requirements.

included
Please refer to the overview by Hei-VAP units for the possible configurations or contact us - we are Vacuum controller
Rotavac Vario
happy to be at your service and will advise you in detail. Pumping Unit
not required Vacuum valve

»» Example configuration
Rotavac Valve Control
optional Manual vacuum
Rotary Evaporator Rotavac Valve Tec
controller
House vacuum

Hei-VAP Value / Hei-VAP Value Digital

Vacuum source included


Vacuum controller
Rotavac Vario optional Vapor temperature sensor
Pumping Unit (all glassware sets)
not required
Vacuum valve

Rotavac Valve Control Manual vacuum


optional controller
Rotavac Valve Tec
Vapor temperature sensor

+
House vacuum (all glassware sets)

Hei-VAP Advantage

Rotavac Vario included


Vacuum controller
Pumping Unit Rotavac Valve Control required
Vacuum valve
Rotavac Valve Tec
Hei-VAP Advantage Autoaccurate-sensor
optional (glassware G3/G6 only)
House vacuum
Vapor temperature sensor
Accessories (all glassware sets)

included
Vacuum controller
not required
Rotavac Vario Control Vacuum valve

Autoaccurate-sensor
Rotavac Vario Tec optional (glassware G3/G6 only)

included Vapor temperature sensor


Vacuum controller included in pumping unit, no further configuration required (all glassware sets)

Vapor temperature sensor optional optional available as accessory Hei-VAP Precision


(all glassware sets)

not required not required due to rpm regulation


Vacuum valve

As an aid to decision-making we have created different packages for you, from basic equipment up to
automatic destillation with RPM-regulated vacuum pumps - for details see the following pages. Rotavac Valve Control Rotavac Valve Tec Rotavac Vario Control Rotavac Vario Tec Rotavac Vario Manual vacuum Vacuum valve AUTOaccurate- Vapor
with with with with Pumping Unit controller with Woulff bottle sensor temperature sensor
condenser condenser condenser condenser with condenser

30 31
Hei-VAP Packages

Hei-VAP Silver 4 Package Hei-VAP Gold 3 Package Hei-VAP Platinum 2 Package Hei-VAP Platinum 5 Package
P/N 560 - 91302 - 00 P/N 562 - 91307 - 00 P/N 563 - 51310 - 00 P/N 564 - 31318 - 00

Hei-VAP Silver Packages Hei-VAP Gold Packages Hei-VAP Platinum Packages Hei-VAP Platinum Packages
Standard equipment for your lab For standard distillations with vacuum control Automatic distillations with Hei-VAP Precision hand lift Automatic distillations with Hei-VAP Precision motor lift
models and valve-regulated vacuum pumps models and RPM-regulated vacuum pumps

Hei-VAP Silver 4 Package Hei-VAP Gold 1 Package Hei-VAP Platinum 1 Package Hei-VAP Platinum 3 Package
P/N 560 - 91302 - 00 P/N 561 - 41300 - 00 P/N 563 - 61300 - 00 P/N 564 - 21300 - 00
Hei-VAP Value Digital with hand lift and vertical glassware set G3 • Hei-VAP Advantage with hand lift and vertical glassware set G3 • Hei-VAP Precision with hand lift and vertical glassware set G3 • Hei-VAP Precision with motor lift and vertical glassware
• Vacuum pump Rotavac Valve Tec • Vapor temperature sensor • Vapor temperature sensor set G3
• Manual vacuum controller • Vacuum pump Rotavac Valve Tec • Vacuum valve • AUTOaccurate-sensor
• Tube set • Manual vacuum controller • Vacuum pump Rotavac Valve Tec with condenser • Vacuum pump Rotavac Vario Tec with condenser
• Tube set • Tube set • Woulff bottle
Hei-VAP Silver 5 Package • Tube set
P/N 560 - 81312 - 00 Hei-VAP Gold 2 Package Hei-VAP Platinum 2 Package
Hei-VAP Value Digital with hand lift and coated vertical glassware P/N 562 - 11310 - 00 P/N 563 - 51310 - 00 Hei-VAP Platinum 4 Package
set G3B • Hei-VAP Advantage with motor lift and coated vertical glassware • Hei-VAP Precision with hand lift and coated vertical glassware P/N 564 - 31310 - 00
• Vacuum pump Rotavac Valve Control set G3B set G3B • Hei-VAP Precision with motor lift and coated vertical
• Manual vacuum controller • Vapor temperature sensor • AUTOaccurate-sensor glassware set G3B
• Tube set • Vacuum pump Rotavac Vario Pumping Unit • Vacuum valve • AUTOaccurate-sensor
• Tube set • Vacuum pump Rotavac Valve Control with condenser • Vacuum pump Rotavac Vario Control with condenser
Hei-VAP Silver 6 Package • Tube set • Woulff bottle
P/N 560 - 91309 - 20 Hei-VAP Gold 3 Package • Tube set
Hei-VAP Value Digital with hand lift and vertical glassware set G3 P/N 562 - 91307 - 00
• Vacuum pump Rotavac Valve Tec • Hei-VAP Advantage with motor lift and vertical glassware set G3 Hei-VAP Platinum 5 Package
• Manual vacuum controller • Vacuum pump Rotavac Valve Tec P/N 564 - 31318 - 00
• Chiller RotaChill Small • Manual vacuum controller • Hei-VAP Precision with motor lift and coated vertical
• Tube set • Chiller Rotacool Mini glassware set G3B
• Tube set Hei-VAP Safety Upgrade • AUTOaccurate-sensor
• Vacuum pump Rotavac Vario Control with condenser
Hei-VAP Gold 4 Package For highest safety • Woulff bottle
P/N 564-61310-00 • Chiller RotaChill Large
• Hei-VAP Precision with motor lift and vertical glassware set G3B • Tube set
• Vacuum pump Rotavac Valve Tec with condenser Hei-VAP Safety Upgrade
• Vacuum valve P/N 569 - 00311 - 00 Hei-VAP Platinum 5 XL Package
• Tube set Additional guard hood and coating of glassware P/N 564 - 31319 - 00
for your Hei-VAP Package • Hei-VAP Precision with motor lift and coated vertical
glassware set G3B XL
• AUTOaccurate-sensor
• Vacuum pump Rotavac Vario Control with condenser
• Woulff bottle
• Chiller RotaChill Large
• Tube set

32 33
Technical Specifications - Rotary Evaporators
Hei-VAP
Hei-VAP Hei-VAP Hei-VAP Hei-VAP
Model Value (HL) /
Advantage (HL) Advantage (ML) Precision (HL) Precision (ML)
Value Digital (HL)
Hand / Motor lift hand lift hand lift motor lift hand lift motor lift

Height adjustment speed manual manual 30 mm/s manual 30 mm/s

Height adjustment (mm) 155 155 155 155 155

Cer ti f i cate
Rotation speed (rpm) 10 – 280 10 – 280 10 – 280 10 – 280 10 – 280

Rotation speed setting scale 3.5" LCD display 3.5" LCD display 4.3" LCD color graphic display 4.3" LCD color graphic display

Drive brushless DC motor with electronic speed control

Heating capacity (W) 1,300 1,300 1,300 1,300 1,300

Temp. range heating bath (°C) 20 – 210 20 – 210 20 – 210 20 – 210 20 – 210

Temperature accuracy bath (°C) ±1 ±1 ±1 ±1 ±1

Overheat protection bath (°C) cut-off at 5 °C over set temperature via separate Pt 1000

Bath temperature setting**** scale / digital 3.5" LCD display 3.5" LCD display 4.3" LCD color graphic display 4.3" LCD color graphic display

Heating bath temperature control electronic / digital electronic / digital electronic / digital electronic / digital electronic / digital

Secondary overtemp. cut-off (°C) 250 250 250 250 250

Material heating bath stainless steel AISI 316L stainless steel AISI 316L stainless steel AISI 316L stainless steel AISI 316L stainless steel AISI 316L
To confirm the ability for
Diameter heating bath

Volume heating bath


(mm)

(L)
255

4.5
255

4.5
255

4.5
255

4.5
255

4.5
continuous operation
Display vapor temperature no yes yes yes yes
required accessories vapor temperature sensor vapor temperature sensor vapor temperature sensor vapor temperature sensor
of the Hei-VAP series Rotary Evaporators
Integrated vacuum controller no no no yes yes

Timer no yes yes yes yes

Vacuum program SETpressure** no no no yes yes

Vacuum program AUTOeasy** no no no yes yes

Vacuum program AUTOaccurate** requi- no no no yes yes


res AUTOaccurate-sensor

Remote control function


Hei-VAP series Rotary Evaporators feature overtemperature safety circuits according
- Lift no no yes no yes to DIN EN 61010-1:2001 and DIN EN 61010-2-010:2014 and therefore is designed for
- Start rotation yes yes yes yes yes continuous operation.
- Start vacuum no no no yes yes

- Start heating bath yes yes yes yes yes


This statement is made under the precondition that all units are operated in
Programmable ramps no no no yes yes
accordance with the operation manual and in accordance with good practice standards
Supply power (W) 1,400 1,400 1,400 1,400 1,400

Weight (w/o glassware assembly) (kg) 16 16 16 17 17


for safety in laboratories, rules for accident preventions, and compliance with directions
Dimensions with glassware set G3 (mm)
477 x max. 739 x 845 477 x max. 739 x 845 407 x max. 739 x 845 523 x max. 739 x 845 453 x max. 739 x 845
on hazardous materials.
Width on extended heating bath (l x w x h)
Dimensions with glassware set G3 XL (mm)
477 x max. 739 x 920 477 x max. 739 x 920 407 x max. 739 x 920 523 x max. 739 x 920 453 x max. 739 x 920
Width on extended heating bath (l x w x h)
Protection class*** (DIN EN 60529) IP 20 IP 20 IP 20 IP 20 IP 20

5 – 31 °C at 80 % rel. 5 – 31 °C at 80 % rel. 5 – 31 °C at 80 % rel. 5 – 31 °C at 80 % rel. 5 – 31 °C at 80 % rel.


humidity humidity humidity humidity humidity
Permissible ambient conditions 32 – 40 °C decreasing 32 – 40 °C decreasing 32 – 40 °C decreasing 32 – 40 °C decreasing 32 – 40 °C decreasing
linearly up to max. 50 % linearly up to max. 50 % linearly up to max. 50 % linearly up to max. 50 % linearly up to max. 50 %
rel. humidity rel. humidity rel. humidity rel. humidity rel. humidity
2 1,400 1,400 1,400 1,400 1,400
Condensing surface (cm )
2 2,200 2,200 2,200 2,200 2,200
Condensing surface XL Condenser (cm )
S c h w a b a c h , J a n u a r y 2 0 1 8

Rate of evaporation* (L/h) Toluene Acetone Ethanol Isopropanol (IPA) Water

G3 Vertical 6.5 6.0 2.5 4.0 1.4

G3 XL Vertical 8.5 7.5 3.5 4.9 1.4

Improvement with XL condenser (%) 31 25 40 23 system limit reached


with 1.4 L/h

* With maximum condenser efficiency *** IP 67 cable connection on heating bath


** Only in combination with vacuum systems **** Hei-VAP Value Digital: digital display
Stefan Peters Marcell Sarré
Standard supply voltage: 230 V - other voltages upon request, please specify for order Research and Development Manager Quality Manager

34 35
Industrial
Evaporation

Hei-VAP Industrial
Large-Scale Rotary Evaporators
Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership
Leading Safety Standards

• The EASY LOCK flask • Safety sensor stops rotation if bath • Receiving cassette system protects
attachment allows for safe flask change guard hood is opened during operation glassware while providing superior
thus providing user safety flask support. Easy access to receiving
• An emergency off button brings the cassettes via two latching high-impact
entire unit to a complete stop • A temperature sensor powers off the transparent PMMA doors
bath in case of any uncontrolled heat-up
• To promote a safe use of the Hei-VAP • Ultimate safety is provided with the
Industrial evaporator the interface panel • To effectively prevent accidents while Hei-VAP Industrial model which comes
not only has all parameters for operation monitoring parameters the speed, bath standard with: a guard hood consisting of
but also 5 key safety functions that temperature and vacuum setting must be a metal frame and safety glass
require operator action prior to confirmed on separate on/off buttons in completely covering the bath. This
resuming process order to start operation prevents any operator contact with
steam, splashing bath fluid and splinters
• Features water level regulation system • Automatic safety cut-off in an of glass in case of implosion
to prevent water spilling over bath and overpressure situation caused by
potentially flooding your lab glassware breakage or defective vacuum • Excellent user safety is achieved by a
circuit transparent high impact PMMA door on
a metal condenser housing covering the
main glassware assembly

Do you require safe and quick flask removal by one person


with industry leading safety standards?

Industrial Evaporation
With the Hei-VAP Industrial series you are always on the safe side with the
safety enclosure protecting you and your glassware! You can operate the
Hei-VAP Industrial just by yourself, change flasks in seconds and operate
the unit with ease.

Self-filling One-person Transparent


Touch-panel water bath flask changes EASY LOCK Visual control PMMA doors

38 39
Superior Ease of Use

• Intuitive touch screen control for easy • Unique self-aligning flask support system • Now you can manage even the most
operation allows for immediate one-person demanding applications easily and
operation eliminate foaming, excessive bubbling
• Touch screen with glass surface for or bumping of solutions
chemical resistance and easy cleaning • Reduce your process times by using the
exclusive AUTOaccurate program which • The automatic process timer turns off
• EASY LOCK flask attachment for quick automates your distillation using a vapor your evaporation at a pre-programmed
and easy flask changes temperature system that takes the time
guesswork out of finding the correct
• Illuminated bath and evaporation flask vacuum setting every time • The optional automatic module
allows for superior visual control Distimatic Industrial allows for
• No hassle and safety concern due to low continuous and unattended
• Integrated heating coils guarantee the fluid levels: self-filling water bath takes automatic operations
most convenient and fastest cleaning the worry out of running dry
of the bath • Optional Base Cart provides you with a
• Receiving flasks feature reinforced fully-maneuverable rotary evaporator
• Receiver cassettes guard against bottom drain valves as standard and while offering a storage space for vacuum
glassware breakage while providing a are protected by cassettes pump, glassware, solvents or accessories
self-standing flask support and quick
removal of receiving vessels • To prevent steam from building up within
the guard hood, two strong blowers
• Save time with up to 250 effectively ventilate the entire area to
pre-programmed steps of up give you a clear view of the
to 999 process ramps evaporating flask

Reduced Cost of Ownership

• Universal heating bath for water or • AUTOaccurate-evaporations drive your • Maximize your initial investment
other bath fluids allows for temperature solution to a variable quantity or dryness, significantly: the automatic module
settings up to 180 °C then shut off vacuum, heating bath and Distimatic Industrial is an
rotation, and ventilates the system to affordable and more flexible
• Utilize the pre-heating option for your give you semi-automated capabilities at alternative to common 50 or 100-liter
bath and start your application without significant cost savings evaporators
any loss of time
• Spend your working hours more • Increased throughput at reduced
• The water bath refill system allows you effectively on other challenges which energy consumption due to an industry
to step away from your evaporator at any require your attention and evaporate leading leak-proof vacuum seal:
moment and reduce your supervision large quantities continuously with the • final pressure below 1 mbar
responsibility to zero for baths that run automatic module Distimatic Industrial • pressure increase below 1 mbar/min
dry or overheat

• No hidden cost: all components to


control vacuum are included as a
standard. This includes vacuum valve,
vacuum controller, vacuum sensor and
vapor temperature sensor

41
Hei-VAP Industrial control panel Industrial
Evaporation
Menu Vacuum control mode Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

Height adjustment
Timer of heating bath
Vacuum (set & actual)
The average operational lifespan of 10 years is backed by a 3 year warranty
and makes your purchase a worthwhile investment.
Speed (set & actual) Separate on/off switches
for all process
Bath temperature (set & actual)
parameters A guard hood consisting of a metal
Vapor temperature
frame and safety glass covers the
Start/Stop all Indicating warm-up bath completely while providing
parameters
Illuminated bath and clear visible monitoring
evaporation flask allows for
superior visual control Increased throughput at reduced
energy consumption due to an
on/off switch industry leading vacuum leakproof

USB interface
The EASY LOCK flask Features level regulation
attachment allows for single- system to prevent from spilling
user safe flask exchange over and potential floods in lab

Unique self-aligning
flask support system allows for
Excellent user safety: immediate “one-person operation”
condenser and receiving
Two Programs for Process Control flasks are protected by high-
impact transparent PMMA Non-visible heating coils
doors guarantee the most convenient
SETpressure AUTOaccurate and fastest cleaning of the bath

Program for solvent separations Supports very precise automatic pressure control for Intuitive touch screen control for
solvent evaporation and separations ease of operation
• This program holds a set vacuum constant and uses a
hysteresis • This program identifies multiple boiling points
automatically by reducing vacuum
• Optionally, the process can be predefined via
programmable ramps

Receiver cassettes guard Unit powers off all relevant


Program: SETpressure Program: AUTOaccurate against glassware functions in case of a bath
Control parameter: manually set pressure Control parameter: vapor temperature
breakage while providing a overtemperature situation,
self-standing support overpressure and glassware breakage
1000 mbar

1000 mbar

No hassle or safety concerns


due to low bath fluid levels: the
Final vacuum individually adjustable stop self-filling water bath takes the
Manually set vacuum Finds multiple boiling points automatically worry out of running dry

Automatic module Distimatic Industrial - For batch and continuous Save time with up to 250
evaporation without limits - an affordable and more flexible alternative pre-programmed profiles of up
to common 50 or 100-liter evaporators to 999 process gradients

42 43
Hei-VAP Industrial Glassware – Hei-VAP Industrial

Highest safety and integrated vacuum control capabilities


Includes leading safety standards and features for superior ease of use and reduced cost
of ownership, plus:

Glassware Shorty R Glassware R

• Identical to glassware R, but features a condenser that is • This glassware assembly includes one ascending
320 mm shorter condenser, one 20-l evaporating flask, one 10-l receiving
Excellent user safety • Distillation capacity remains the same. This assembly is flask and is recommended for all standard distillations
ideal in laboratories for hood applications or where height
with high-impact
is restricted
transparent PMMA door

Glassware Shorty RC Glassware RC

• Identical to glassware assembly Shorty R, but features • Identical to glassware assembly R, but features two
two receiving flasks receiving flasks
Non-fogging safety glass and metal frame
Large touch screen control
guard hood provides excellent user protection
panel with illuminated displays
for all process parameters,
programmable ramps as
The evaporation flask is illuminated during
described on page 42
operation for increased visibility

Certification according Glassware A Glassware A2


Receiver cassettes and to GMP available for
additional PMMA door
housing protect against
this model: validation
for installation (IQ) and
• This glassware assembly includes one descending • This glassware assembly includes one ascending, one
condenser, one expansion vessel, one 20-l evaporating flask, descending condenser and one expansion vessel, one
threat of glassware operating qualification (OQ) one 10-l receiving flask and is recommended for solvents 20-l evaporating flask, one 10-l receiving flask
breakage that tend to splash and foam • For low-boiling solvents and highest recovery rates

Universal heating bath Glassware AC Glassware A2C


accommodates water or
other bath fluids allowing for
temperature settings up to
• Identical to glassware assembly A, but features two • Identical to glassware assembly A2, but features two
receiving flasks receiving flasks
180 °C

Comes as standard with


integrated refill water
system, spillover prevention
and a release valve at the
bottom
Optional Base Cart is fully-
maneuverable with removable
panels for storage of vacuum
pump, glassware, solvents or Glassware A1 Glassware K
accessories
• This glassware assembly includes one ascending, • Condensate trap for low-boiling solvents; cooling by
one descending condenser, one ascent pipe, one 20-l dry-ice
evaporating flask and one 10-l receiving flask • Comes with one 20-l evaporating flask and one 10-l
• For low-boiling solvents and highest recovery rates receiving flask

Hei-VAP Industrial with Glassware A1C Glassware KC


glassware set RC
(without Base Cart) • Identical to glassware assembly A1, but features two • Identical to glassware assembly K, but features two
P/N 518 - 12100 - 00 receiving flasks receiving flasks

44 45
Vacuum Pump Part Numbers – Hei-VAP Industrial

Valve-regulated vacuum pump Rotavac 20


P/N 591 - 07210 - 00

Includes secondary condenser and air intake separation vessel


Hei-VAP Industrial
This vacuum system can be applied in • Excellent compatibility with chemicals and
Without Base Cart
many different fields in order to evacuate, condensate
evaporate and pump out gases and vapors. • Excellent ultimate vacuum of 2 mbar
Thanks to the emission condenser it is • Very quiet and very low vibration
possible to achieve a chemical recovery of • Very high suction capacity of 3.0 m3/h
almost 100% • Weight: 19.9 kg Glassware

• Dimensions: W350 / D275 / H495 mm R 518 - 11100 - 00

Shorty R 518 - 18100 - 00

RC 518 - 12100 - 00

Shorty RC 518 - 19100 - 00

Accessories - Hei-VAP Industrial A

AC
518 - 13100 - 00

518 - 15100 - 00

A1 518-14102-00

A1C 518-16102-00

A2 518 - 14100 - 00

Receiving flask A2C 518 - 16100 - 00


Evaporating flasks Powder flasks P/N 15 - 300 - 004 - 11 K 518 - 18102 - 00

KC 518 - 19102 - 00
Evaporating flask 6 l Powder flask 10 l With drain valves, 10 l
P/N 15-300-003-23 P/N 15-300-003-24 (Included as a standard for all
Evaporating flask 10 l Powder flask 20 l Hei-VAP Industrial models)
P/N 15-300-003-22 P/N 15-300-003-25
Evaporating flask 20 l
(Included as a standard)
P/N 15-300-003-21

Hei-VAP Industrial B
Limited budgets? As shown above (Hei-VAP Industrial) - without:
Hei-VAP Industrial B
• Metal frame and safety glass guard hood covering the bath
• High-impact PMMA door covering the glassware assembly
Tubing • High-impact PMMA latching door which cover the receiving
Vacuum sensor Vacuum valve P/N 591-34000-00 (package 16 m) flask cassettes
P/N 591 - 21000 - 00 P/N 591 - 20000 - 00 P/N 591-33000-01 (by meter)
Without Base Cart
(Included as a standard for all (Included as a standard for all Tubing for vacuum and water
Hei-VAP Industrial models) Hei-VAP Industrial models) connection. Available as package
(16 meter piece incl. hose clamps) or in Glassware
individual length (by meter)
R 518 - 21100 - 00

Shorty R 518 - 28100 - 00

RC 518 - 22100 - 00

Shorty RC 518 - 29100 - 00

A 518 - 23100 - 00

AC 518 - 25100 - 00

A1 518-24102-00

A1C 518-26102-00

Vapor temperature sensor Base Cart Heating bath liquid A2 518 - 24100 - 00


P/N 14 - 014 - 003 - 06 P/N 591 - 23000 - 00 P/N 569-00600-00 A2C 518 - 26100 - 00

K 518 - 28102 - 00
(Included as a standard for all For all Hei-VAP Industrial models Heating bath liquid up to 220 °C (5 kg)
KC 518 - 29102 - 00
Hei-VAP Industrial models)

46 47
Technical Specifications - Large-Scale Rotary
Evaporators

Model Hei-VAP Industrial Model Hei-VAP Industrial

Rotation speed (rpm) 6 – 160 Vacuum controller yes

Cer ti f i cate
Rotation speed setting digital Timer yes

Heating bath lift motor lift Vacuum control program SETpressure ** yes

Height adjustment speed (mm/s) 45  Vacuum control program AUTOaccurate **


yes
requires AUTOaccurate-sensor
Height adjustment (mm) 180
Programmable ramps yes
Drive EC-motor
Supply power (W) 4,600
Heating capacity (W) 4,000
Weight (without glass assembly) (kg) approx. 120
Temperature range (°C)
20 – 180 Dimensions (l x w x h) (mm) 970 x 690 x 1,600
heating bath

Temperature accuracy (°C) ±1 Protection class (DIN EN 60529) IP 20

Permissible ambient conditions 5 – 31 °C at 80 %


Overheat cut-off protection (°C) 110 (H2O) / 210 (oil)
rel. humidity
Bath temperature setting digital 32 – 40 °C decreasing linearly
up to max. 50 % rel. humidity
To confirm the ability for
Automatic heating bath control micro processor

continuous operation
Rate of evaporation (L/h) at 40 °C *
Material heating bath V4A (1.4404) temperature difference
- Toluene 26.0
Diameter heating bath (mm) 400 - Acetone 25.9
- Ethanol 12.9
Volume heating bath (l) 24 (H2O) / 22 (oil) - Water 4.7 of the Hei-VAP Industrial series Large-Scale Rotary Evaporators
Level regulation of water bath automatically due to level Maximum condensing surface (m2) 1.2
sensor and refill function
Display vapor temperature digital
(required accessories) temperature sensor
Indicating range vapor temperature (°C) 0 - 200
sensor (accuracy 0.1 °C)

The Hei-VAP Industrial series Large-Scale Rotary Evaporators feature overtemperature


safety circuits according to DIN EN 61010-1:2001 and DIN EN 61010-2-010:2014 and
* T = difference between heating bath temperature and boiling temperature
** Only in combination with vacuum systems therefore is designed for continuous operation.

Standard supply voltage: 400 V three-phase current - other voltages upon request, please specify for order
This statement is made under the precondition that all units are operated in
accordance with the operation manual and in accordance with good practice standards
for safety in laboratories, rules for accident preventions, and compliance with directions
on hazardous materials.

S c h w a b a c h , J a n u a r y 2 0 1 8

Stefan Peters Marcell Sarré


Research and Development Manager Quality Manager

48 49
Automatic 24/7
Evaporation

Hei-VOLUME Automatic Modules

Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership


General

• Automatic refill of the evaporation flask with • The automatic module is compatible with all
the solvent mixture according to your settings. bench-top and large-scale evaporators from
Continuous automatic discharge of condensate Heidolph

• The worldwide unique automatic residue • The storage and the collecting tank can be
drainage offers unattended distillation for days replaced during the process

Leading Safety Standards

• The complete system is sensor- • The system can be placed under • An easily accessible emergency-
controlled and turns off the a fume hood which ensures the button allows you to stop the
automatic module as well as all highest safety level for the operator process immediately by the
connected equipment completely operator
in case of an emergency

Superior Ease of Use


Do you require a system to evaporate unlimited • Take advantage of the wide range of • The process can be terminated • Integrated plug connectors enable
possibilities to adjust the settings automatically after evaporation is you to connect and to control
volumes in a continuous and unattended process according to your individual needs completed or manually at any time also peripheral equipment from a

24 hours a day/7 days a week? • The worldwide unique automatic


by the operator central point

residue drainage offers a wide


range of new possibilities for
automatic, continuous and
unattended distillation

Automatic 24/7 Evaporation


Save time by using the automatic module Distimatic and distill Reduced Cost of Ownership
large volumes in a continuous and unattended manner overnight
and during the weekend!
• Affordable alternative to common 50 or 100 • Increase your efficiency - the fully automatic
liter evaporators process avoids the need of visual control and
gives you time to focus on other tasks
• Reduce your investments by using your existing
equipment - the automatic module is compatible • The unattended and continuous reconditioning of
to all rotary evaporators from Heidolph solvent avoids any bottlenecks of availability of
24/7 Automatic discharge
of condensate
Automatic drainage
of residue Automatic refill No foaming solvents and reduce your investments in this way

52 53
The smart way to process large quantities Automated 24/7
automatically Evaporation
• The automatic module Distimatic is • Process rates with bench-top evaporators • Both modes are completed in an Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership
available for Hei-VAP rotary evaporators for the most common solvents are: automated and unattended process
(Distimatic Bench-top) and Hei-VAP • Water: 1.4 l/h of solvent separations of nearly 100 %
Industrial large-scale rotary evaporators • Acetone: 6.0 l/h The average operational lifespan of 10 years is backed by a 3 year warranty
(Distimatic Industrial) • Toluene: 6.5 l/h • Degree of concentration for final and makes your purchase a worthwhile investment.
• Ethanol: 2.5 l/h product can be determined to rule out
• For distillation select between these two dehydration, cristallisation and formation
modes: • Increased process rates with Hei-VAP of powder
• Sensor-Mode: Refill and drainage are Industrial large-scale evaporators, for
automatically sensor-controlled example: • Bumping is eliminated by continuously Automated in unattended distillation Automatic refill of the evaporation
• Time-Mode: All parameters controlled • Water: 4.5 l/h feeding small volumes flask and continuous automatic
in two different modes
by individually pre-programmed • Acetone: 25.0 l/h discharge of condensate
automatic time intervals

Compatible with all Hei-VAP rotary


Automatic drainage
evaporators (Distimatic Bench-top)
of residue: residue in
For distillation select between these two modes: the evaporation flask
and Hei-VAP Industrial large-scale
rotary evaporators (Distimatic
will be drained off
Industrial)

Applications are completed


in an automated and unattended
process of solvent seperations
of nearly 100 %

The automatic module


Distimatic Bench-top
can be used in common
fume hoods due to the
space saving design

Sensor-Mode: Time-Mode:

Distimatic
Refill and drainage are All parameters controlled by individually
automatically sensor-controlled pre-programmed automatic time intervals

• A sensor detects the fill-level inside the evaporation • The desired/requested fill-level can be set individually
flask
• Flask refill is achieved via valve control and under
• The desired/requested fill-level can be set individually system pressure according to pre-programmed cycles
Bumping is eliminated by
• Flask refill is achieved via valve control and under • The process is powered off once the pre-programmed continuously feeding small volumes
system pressure number of cycles have expired Wide range of possibilities to In case of an emergency the
adjust settings according complete system will power off
• A sensor monitors the quantity of the solvent mixture to your individual needs entirely
and powers off the unit once it is completely processed

54 55
Functional Principle Functional Principle

For unattended and continuous use – including automatic drainage of residue Distimatic Bench-top including automatic drainage of residue
Save time by distilling large volumes in a continuous and unattended manner
overnight and during the weekend

Automatic solvent supply of Automatic discharge of End of distillation 1 Vacuum valve


the evaporating flask condensate process
2 Collector valve

• Refilling with the Sensor-Mode runs


automatically and is based on the
• A valve matrix controls the continuous
discharge of the condensate from the
• The process can be terminated
automatically after evaporation is
3 Ventilation valve
desired level in the evaporation flask system into a temporary storage flask.
Afterwards the collected condensate
completed or manually at any time by
the operator 4 Condensate pump
• Refilling with the Time-Mode is will be discharged into the collecting
5 Residue pump
done according to individual time tank by a diaphragm pump
parameters

Emergency sensor
Automatic drainage of residue

• The residue in the evaporating flask will be drained into a collecting tank. Afterwards the process starts again automatically by refilling
the evaporating flask

Level sensor
Distimatic Bench-top / Distimatic Industrial
2 3
1
The automatic module Hei-VAP Distimatic is compatible with all bench-top and
large-scale evaporators from Heidolph Collector

5
Refill valve

4 Refill sensor

Overflow sensor Overflow sensor


Distimatic Bench-top Distimatic Industrial including automatic
including automatic drainage of residue and adaptor piece for
drainage of residue glassware set A / A2
P/N 591-53000-00 (G9B) P/N 591-54000-00
P/N 591-53000-02 (G9B XL)
Distimatic Industrial including Residue Solvent Condensate
automatic drainage of residue and
Distimatic Bench-top adaptor piece for glassware set R
without automatic P/N 591-55000-00 Rate of evaporation at continuous operation
drainage of residue
P/N 591-51000-00 (G9B)
P/N 591-51000-02 (G9B XL)
Distimatic Industrial without automatic • Reach outstanding evaporation rates of up to 6.5 l/h with the Distimatic Bench-top
drainage of residue and up to 25.0 l/h with the Distimatic Industrial
P/N 591-52000-00

56 57
Distimatic Bench-top Packages Distimatic Industrial Packages

Distimatic Bench-top Platinum Packages P/N Distimatic Industrial Platinum Packages P/N

Distimatic Bench-top Platinum 1 Package Distimatic Industrial Platinum 1 Package


Distimatic Bench-top including automatic drainage of residue, Hei-VAP Precision Rotary 563-01914-00 Distimatic Industrial including automatic drainage of residue and Hei-VAP Industrial with 518-11155-00
Evaporator with hand lift and coated, vertical glassware set G9B glassware set R

Distimatic Bench-top Platinum 2 Package Distimatic Industrial Platinum 2 Package


Distimatic Bench-top including automatic drainage of residue, Hei-VAP Precision Rotary 564-01914-00 Distimatic Industrial including automatic drainage of residue and Hei-VAP Industrial with 518-13154-00
Evaporator with motor lift and coated, vertical glassware set G9B glassware set A

Distimatic Bench-top Platinum 2 XL Package Distimatic Industrial Platinum 3 Package


Distimatic Bench-top including automatic drainage of residue, Hei-VAP Precision Rotary 564-01915-00 Distimatic Industrial including automatic drainage of residue and Hei-VAP Industrial with 518-14154-00
Evaporator with motor lift and coated, vertical glassware set G9B XL glassware set A2

Distimatic Bench-top Platinum 3 Package Distimatic Industrial Platinum 4 Package


Distimatic Bench-top without automatic drainage of residue, Hei-VAP Precision Rotary 563-01913-00 Distimatic Industrial without automatic drainage of residue and Hei-VAP Industrial with 518-14152-00
Evaporator with hand lift and coated, vertical glassware set G9B glassware set A2

Distimatic Bench-top Platinum 4 Package Distimatic Industrial Platinum 5 Package


Distimatic Bench-top without automatic drainage of residue, Hei-VAP Precision Rotary 564-01913-00 Distimatic Industrial without automatic drainage of residue and Hei-VAP Industrial with 518-13152-00
Evaporator with motor lift and coated, vertical glassware set G9B glassware set A

Distimatic Bench-top Platinum 4 XL Package Distimatic Industrial Platinum 6 Package


Distimatic Bench-top without automatic drainage of residue, Hei-VAP Precision Rotary 564-01917-00 Distimatic Industrial without automatic drainage of residue and Hei-VAP Industrial with 518-11152-00
Evaporator with motor lift and coated, vertical glassware set G9B XL glassware set R

Distimatic Industrial Platinum 7 Package


Distimatic Industrial including automatic drainage of residue and Hei-VAP Industrial with 518-14154-20
glassware set A1

Distimatic Industrial Platinum 8 Package


Distimatic Industrial without automatic drainage of residue and Hei-VAP Industrial with 518-14152-20
glassware set A1

Functional principle Distimatic

www.heidolph.com
58 59
Technical Specifications - Automatic Module Distimatic

Model Distimatic Bench-top without drainage of residue Distimatic Bench-top including drainage of residue

P/N (230 V) 591-51000-00 591-53000-00

Compatibility (Rotary Evaporators) Hei-VAP and Laborota 4000 series Hei-VAP and Laborota 4000 series

Separate control panel yes yes

Cer ti f i cate
Display digital digital

Automatic refill of sample yes yes

Automatic discharge of condensate yes yes

Automatic drainage of residue no yes

Power input control box (VA) 50 50

Noise level (dB(A)) < 80 < 80


Total power
3,500 3,500
multiple switched socket (W)
Weight (kg) 5 5

Measurements without mounted


300 x 200 x 120 300 x 200 x 120
components (W x D x H) (mm)

5 – 31 °C at 80 % rel. humidity 5 – 31 °C at 80 % rel. humidity


To confirm the ability for
32 – 40 °C decreasing linearly up to max. 50 % rel. humidity 32 – 40 °C decreasing linearly up to max. 50 % rel. humidity

continuous operation
Permissible ambient conditions
0 - 2000 m a.s.l., Contamination level 2 0 - 2000 m a.s.l., Contamination level 2
Overvoltage category II Overvoltage category II

Protection class (DIN EN 60529) IP 54 IP 54


of the Automatic Module Distimatic

Distimatic Industrial without drainage Distimatic Industrial including drainage


Model
of residue of residue
591-54000-00 Glassware A / A2
P/N (230 V) 591-52000-00
591-55000-00 Glassware R
The Automatic Module Distimatic features overtemperature safety circuits
Compatibility (Rotary Evaporators) Hei-VAP Industrial and Laborota 20 series Hei-VAP Industrial and Laborota 20 series
according to DIN EN 61010-1 : 2011-07 and therefore is designed for continuous operation.
Separate control panel yes yes

Display digital digital

Automatic refill of sample yes yes


This statement is made under the precondition that all units are operated in
Automatic discharge of condensate yes yes accordance with the operation manual and in accordance with good practice standards
Automatic drainage of residue no yes for safety in laboratories, rules for accident preventions, and compliance with directions
Power input control box (VA) 50 50 on hazardous materials.
Noise level (dB(A)) < 80 < 80
Total power
3,500 3,500
multiple socket (W)
Weight (kg) 5 5

Measurements without mounted


300 x 200 x 120 300 x 200 x 120
components (W x D x H) (mm)

5 – 31 °C at 80 % rel. humidity 5 – 31 °C at 80 % rel. humidity


32 – 40 °C decreasing linearly up to max. 50 % rel. humidity 32 – 40 °C decreasing linearly up to max. 50 % rel. humidity
Permissible ambient conditions
0 - 2000 m a.s.l., Contamination level 2 0 - 2000 m a.s.l., Contamination level 2
Overvoltage category II Overvoltage category II

Protection class (DIN EN 60529) IP 54 IP 54

S c h w a b a c h , J a n u a r y 2 0 1 8

All shown values relate on Automatic Module Disitmatic without any external accesory parts
To check the compatibility please contact your dedicated Heidolph contact person

Stefan Peters Marcell Sarré


Research and Development Manager Quality Manager

60 61
Safe
Heating and Mixing

Hei-PLATE Magnetic Stirrers

Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership


Leading Safety Standards

• To prevent accidents or laboratory • For your safety, the unit will power off • A separate on/off switch for heating
fires, all magnetic stirrers feature two in case of a short-circuit, a damage to prevents unintentional heat-up.
independent safety circuits which the temperature sensor, a motor failure If heating is switched on, the on/off
switch off heating in case of any or other incidences during operation button is illuminated for visual control
overtemperature situation
• To protect you from splashes and scal- • Even if the stirrer is exposed to the
• In combination with Heat-On attach- ding from bath media, rotation speed highest temperatures, damage is ca-
ments you can convert your lab into a ramps up slowly until unit has reached tegorically ruled out – all models come
“safety zone” the pre-programmed speed with a fire-resistant aluminum die-cast
housing
• A residual heat indicator for all models
prevents you from potential burning
hazards

Have you ever heard of hotplates with


fast heat-up times and chemical
resistance?

Safe Heating and Mixing


The unique Kera-Disk® heating plate of aluminum provides fast
heating times, and the wafer-thin ceramic coating makes the
heating plate both chemically and scratch resistant!

35 % faster Highly resistant Separate button Prevents Sealed housing


heat-up times hot plate for heating unintentional heat-up

64 65
Reduced Cost of Ownership

• Reduce your process times! The • The maintenance-free non-sparking


extended heating capacity of 800 W motors reduce down times
reduces your heat-up time by 35 %
compared to other units at 600 W • The design and features give an
increased lifespan of 10 years along
• The hermetically-sealed housing with significantly reduced maintenance
protects all mechanical and electronic and repair costs
components from aggressive
environments

Superior Ease of Use

• All units with digital display allow for • The unique Kera-Disk ®
coating is
easy setting and monitoring values on extremely chemical-resistant and
the illuminated readout scratch-proof, and therefore the plate
can be cleaned easily from solvents,
• You can even work with dry ice – oil or other contaminations
a robust thermal insulation prevents
corrosion inside the housing by • The chemically resistant Kera-Disk ®
hot
preventing condensate from collecting plate allows for immediate heat
and dripping on any electronic transfer resulting in quick heat-up
components times

• A free software program is available for • In case the heating function fails, stirring
the MR Hei-Connect and MR Hei-End will not be discontinued to avoid
which supports you to automate and to thermal damage to your sample
safe your process parameters

• The strong magnetic field allows for


easy stirring of even higher viscosity
media

66 67
Kera-Disk® top plate
Safe
Heating and Mixing
With Kera-Disk material coating, fast
®
YO UR ADVANTAGE S
heat-up times and chemical resistance! Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership
• Glass ceramic top plates offer the benefits
of chemical and scratch resistance but
produce longer heat-up times
The average operational lifespan of 10 years is backed by a 3 year warranty
• Aluminum top plates allow for immediate and makes your purchase a worthwhile investment.
heat transfer but are not chemical-resistant
or scratch-proof

• Kera-Disk ®
top plates take the best of two
The standard RS 232 interface of the The extended heating capacity of 800 W
worlds: The aluminum top plate allows for
immediate heat transfer for quick heat-up MR Hei-Connect and MR Hei-End reduces heat-up times by 35 % compared
times and a thin layer of ceramic coating enables the documentation and to other units at 600 W
makes the top plate chemical-resistant and controlling via PC. A free software The chemically resistant Kera-Disk®
scratch-proof is available on our website hot plate allows for immediate heat
transfer resulting in quick heat-up
times

Hermetically-sealed housing
protects all mechanical and electronic
components from aggressive
environments In case the heating function fails,
Performance and Accuracy stirring will not be discontinued
to prevent bumping
Take advantage of a built-in PID controller
temperature

that ensures fastest heat-up times while 800 W


600 W

preventing an overtemperature situation of


your sample
time

Sealed housing

The sealed housing of the MR series YO UR ADVANTAGE S


The temperature sensor
guarantees extended performance life and
reduced maintenance!
• Protection against aggressive fumes, consists of two independent
safety circuits which switches
liquids and vapors which prevents internal
corrosion. This results in an increased off heating in case of any
liquid lifespan of 10 years on average at reduced overtemperature situation
maintenance and repair cost

• Protection of all mechanical and


electronic components against aggressive In case of a short-circuit, a A separate on/off button for heating
environmental conditions
damage or removal of the Damage to the stirrer is categorically prevents unintentional heat-up – the
temperature sensor from the ruled out even if exposed to highest button is illuminated for visual control.
media, the unit powers off temperatures – all models come with In addition, the residual heat indicator
PC board
gas completely a fire-resistant aluminum die-cast prevents from potential burning
motor
housing hazards

The hermetically-sealed housing that protects the PC motor but is drained off. The other line marked in orange significantly increases the durability of the magnetic
board and the motor is marked in black. The way a liquid shows that gas can neither ingress to the PC board nor stirrer. For protection against liquid and gas, the heating
would take flowing down from the hotplate is marked in to the motor. The apparent gap is due to temperature elements are completely embedded in ceramic.
orange. As one can see, even if the liquid reaches the insulation. Because of that gap the temperature inside the
heat shields, it cannot ingress to the PC board and the magnetic stirrer stays substantially lower, which

68 69
Magnetic Stirring Hotplates MR Hei-Tec
Preferred use of the MR Series magnetic stirrers includes smooth to intense mixing and Model for higher requirements with temperature sensor
heating of low-viscosity fluids. Your first choice for decomposing organic and inorganic A digital display enables full process monitoring and precise setting of all parameters
substances

• With a heating power of 800 W the hotplate reaches • The strong magnetic field allows for stirring even higher • This unit features a digital display and • A separate on/off switch for heating • Upgrade this magnetic stirrer with the
a maximum temperature of 300 °C in a significantly viscosity media or volumes of 20 liters of water with allows for easy setting and monitoring of prevents an unintentional heat-up. optional Pt 1000 temperature sensor for
reduced time period ease values in the illuminated readout If heating is switched on the on/off precise temperature control, overshoot
button is illuminated for visual control. protection and reproducible results
• Safety circuits avoid an overheat situation of your • Speed is adjustable from 30 respectively 100 to 1,400 rpm • For your protection an independent safety In addition, a residual heat indicator
hotplate: if the temperature overshoots the heating at an accuracy of up to ± 1 % for gentle mixing circuit will switch off heating if hotplate prevents from burning hazards when heat • To protect your sample from overheating,
will be powered off immediately temperature exceeds 25 °C over set function is switched off a safety circuit switches off heating if
temperature the temperature sensor is not inserted
• An illuminated button indicates clearly if into your media vessel when heating is
• Digital speed setting from 100 to the stirring mode is activated commenced
1,400 rpm at an accuracy of ± 2 % and
For standard applications For higher For comprehensive For highest safety temperature setting up to 300 °C
without temperature sensor requirements process documentation

MR Hei-Tec
P/N 505 - 30000 - 00

MR Hei-Tec with Pt 1000


P/N 505 - 30081 - 00

MR Hei-Standard MR Hei-Tec MR Hei-Connect MR Hei-End


MR Hei-Connect
Model for comprehensive process documentation and reproducible results
MR Hei-Standard The MR Hei-Connect includes all features of the MR Hei-Tec unit but comes with an
additional RS 232 interface
Model for standard applications without temperature sensor
Easy handling and direct access to all parameters due to two separate knobs • Monitor and control your process with • Benefit from reproducible results and the • Hei-Control software included in the
the Hei-Control software or your own option to program ramps and interval scope of delivery
program processes

• For your protection an independent safety circuit will


switch off heating if hotplate temperature exceeds
25 °C over set temperature

• A separate on/off switch for heating prevents an


unintentional heat-up. If heating is switched on
the on/off button is illuminated for visual control.
In addition, a residual heat indicator prevents from
burning hazards when heat function is switched off
MR Hei-Connect

• Analog knobs allow for convenient speed setting P/N 505 - 40000 - 00


from 100 to 1,400 rpm at an accuracy of ± 2 % and
temperature setting up to 300 °C MR Hei-Connect with Pt 1000
P/N 505-40081 - 00

MR Hei-Standard
P/N 505 - 20000 - 00

70 71
MR Hei-End Accessories

Model for highest safety


Exact settings and individual definition of safety parameters for highly sensitive media

• An independent safety circuit switches off heating at • A separate on/off switch for heating prevents an unintentional heat-up. 1-l Heating bath
PTFE-coated
2-l Heating bath
PTFE-coated
4-l Heating bath
PTFE-coated
Concave block adaptor
For 1-l round-bottom flasks
an operator-programmed temperature value above If heating is switched on the on/off button is illuminated for visual control
your set temperature P/N 504 - 93100 - 00 P/N 504 - 92100 - 00 P/N 504 - 91100 - 00 P/N 504 - 94000 - 00
• Upgrade this magnetic stirrer with the optional Pt 1000 temperature
• An additional operational safety step is required sensor for precise temperature control, overshoot protection and
to change parameters which prevents unwanted reproducible results
changes to the actual setting

• The digital display allows for easy setting and


monitoring of values on the illuminated readout.
Speed setting from 30 to 1,400 rpm at an accuracy of
± 1 % and temperature setting up to 300 °C
1-l Heating bath for oil 2-l Heating bath for oil 4-l Heating bath for oil Holding device MR

• Hotplate residual heat indicator in the digital display Max. temperature 250 °C
P/N 504 - 93000 - 00
Max. temperature 250 °C
P/N 504 - 92000 - 00
Max. temperature 250 °C
P/N 504 - 91000 - 00
For safe fixation on lab
frames to gain extra lab space.
illuminates when unit is turned off and hotplate
temperature is above 50 °C to prevent accidental Comes with clamp as standard
operator injury P/N 509 - 96000 - 00

• To protect your sample from overheating a safety


circuit switches off heating if the temperature sensor
is not immersed in your media vessel

MR Hei-End MR Hei-End with Pt 1000


P/N 505 - 50000 - 00 P/N 505 - 50081 - 00

Pt 1000 clamping system Pt 1000 temperature sensor RS 232 cable RS 232 cable
(includes support rod and stainless steel (9-pole) (15-pole)
attachment with cable inlet) For MR Hei-Tec, For MR Hei-Connect and For MR Hei-End
P/N 509-63100 - 00 MR Hei-Connect Hei-TORQUE Precision models P/N 14-007-045 - 17
Pt 1000 clamping system and MR Hei-End P/N 14-007-040 - 72
for bath attachments from P/N 509-67910 - 00
3 to 5 liter
Software Hei-Control (includes support rod and Pt 1000 temperature sensor
Stirring bars P/N
attachment with cable inlet) glass-coated
• Utilize the optional software to control and document the P/N 509-63200 - 00 For MR Hei-Tec,
Stirring bars - cylindrical shape
entire process MR Hei-Connect 509 - 56000 - 00
(25, 40, 50 mm each)
and MR Hei-End
• MR Hei-End and MR Hei-Connect featuring a digital P/N 509-67920 - 00
Stirring bars - cross shape (16.5 mm)
RS 232 interface for connecting the optional 509 - 58500 - 00
pack of 20 pcs. for 25-ml to 50-ml flasks
software easily

Stirring bars Evaluation Kit


• Connect up to four units at the same time pack of 10 pcs.
509 - 58300 - 00

• Included in scope of delivery with MR Hei-Connect Silicone protective cover Stirring bars - oval shape (15x6 mm)
509 - 53000 - 00
• Compatible with MR Hei-End and Hei-TORQUE devices Free download of Hei-Control Software for
Replaceable cover against
splashes and dripping water
pack of 3 pcs. for 10-ml flasks

MR Hei-Connect and MR Hei-End at Stirring bars - oval shape (25x10 mm)


www.heidolph.com/support 509 - 54000 - 00
For MR Hei-Tec, pack of 3 pcs. for 25-ml to 50-ml flasks
MR Hei-Connect and
MR Hei-End Stirring bars - oval shape (30x10 mm)
P/N 23 - 07 - 06 - 05 - 59 509 - 55000 - 00
pack of 3 pcs. for 100-ml to 250-ml flasks
For MR Hei-Standard
P/N 23 - 07 - 06 - 05 - 63

72 73
Heat-On Attachments Heat-On Attachments

The Heat-On attachments are suitable to replace oil baths and heating mantles in your lab Heat-On blocks Multi-Well holder and inserts
and reduce the risk of fire hazards. Moreover the attachments minimize the messy oil clear-
Each Heat-On block is a stand-alone product that can be This unique Multi-Well holder is designed to hold either
ups that result from changing oil or removing flasks from an oil bath! placed directly onto the stirring hotplate one or two inserts for flasks*.
The inserts are available for 10-ml, 25-ml, 50-ml, 100-ml and
Heat-On 100-ml block 505 - 80066  - 00 150-ml flasks. Flask inserts also feature cut-away sides for
with flask sidearm cutouts use with two or three-neck flasks and accept the optional
• Our attachments are by far the safest, fastest Heat-On 250-ml block 505 - 80067 - 00 safety lifting handles
and most efficient method for heating and mixing Heat-On 250-ml block 505 - 80067 - 01
solutions in round-bottom flasks from 10 ml to 5 liter with flask sidearm cutouts * Only accepts one 150-ml insert
Heat-On 500-ml block 505 - 80069 - 00
• Heat-On fits precisely to every flask, thus ensuring Heat-On 1-l block 505 - 80071  - 00
maximum surface contact and fast heat transfer. Heat-On 2-l block 505 - 80073 - 00
Eliminates the mess from cleaning flasks after Heat-On 3-l block 505 - 80075 - 00
removal from an oil bath or hazardous spills when an Heat-On 4-l block 505 - 80078 - 00
oil bath slips off a stirring plate. As a result, oil as a Heat-On 5-l block 505 - 80076 - 00
heat transfer media is made redundant and your lab is
a safer place with the Heat-On block system

Heat-On Multi-Well holder


Flask Volume of Hotplate Time to P/N 505 - 80060 - 00