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Chemical Engineering 1
VFSTR UNIVERSITY
UNIT IV - Distributions
Random variables, Discrete and Continuous variables, Introduction to
Distributions.
Binomial distribution : Definition, Mean and Standard deviation, Recurrence
relation, Applications, Fitting of binomial distribution.
Poisson Distribution : Definition, Mean and Standard deviation, Recurrence
relation, Poisson Distribution is an approximation of Binomial distribution,
Applications, Fitting of Poisson distribution.
Geometric Distribution : Definition, Properties.
Normal Distribution : Definition, Normal curve, Mean and Standard deviation,
Median, Mode, Normal Distribution applications, Normal Distribution is an
approximation to Binomial distribution.
Exponential Distribution : Definition, Properties.
TEXT BOOKS :
1. H. K. Dass and Er. Rajnish Verma, Higher Engineering Mathematics, S.
Chand & Co., New Delhi, 2011.
2. Miller and Fruinds, Fundamentals of Probability and Statistics, PHI
publication.
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REFERENCE BOOKS :
1. S.C. Gupta and V.K .Kapoor, “Fundamentals of Mathematical Statistics”,
Sultan Chand & Co., New Delhi, 2005.
2. B.V. Ramana, “Higher Engineering Mathematics”, 3 rd Edition, Tata
McGraw-Hill Publishing Co, 2008.
3. R K Jain, S R K Iyengar, “Advanced Engineering Mathematics”, 2 nd
Edition, Narosa Publishing House.
4. Erwin Kreyszig, “Advanced Engineering Mathematics”, 8 th Edition, John
Wiley & Sons (Asia) Pvt. Ltd. 2001.
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UNIT II - Catalysis
Types of catalysis, characteristics of catalytic reactions, Theories of catalysis,
Enzyme catalysis, characteristics of Enzyme catalysis. Adsorption: Types of
adsorption, adsorption Isotherm, Freundlich Adsorption isotherm, Langmuir
Adsorption isotherms, Adsorption of solutes from solutions, applications of
adsorption, Ion exchange adsorption, applications of ion exchange adsorption
UNIT V - Chromatography
Theory and types of chromatography.
Paper chromatography – Principle, Migration parameters, Types of paper
chromatography, Applications.
Thin layer chromatography – Principles, preparation of thin layers, Applications.
Gas Chromatography – Instrumentation, Detectors and Applications.
HPLC – Principles, Instrumentation, Pumps, Detectors, Applications.
TEXT BOOKS :
1. A. Bahl, B.S.Bahl and G.D. Tuli, “Essential of Physical Chemistry”, 1 st
ed., S. Chand, 2009.
2. Gurudeep Raj and Chatwal Sham Anand, “Instrumental Methods of
Chemical Analysis”, 1st ed., Himalaya Publications, 2007.
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REFERENCE BOOKS :
1. S. Glasstone and Lewis, “Physical Chemistry”, 2nd ed., Mac Million
Publications, 1998.
2. P.W.Atkins, “Physical Chemistry”, 8 th edition, Oxford up Publications,
2007.
3. D.A. Skoog and P.M. West, “Fundamentals of Analytical Chemistry”,
8thed., Harcourt Publications, 2006.
4. H.W. Willard and Demerit, “Instrumental Methods of Analysis”, 1st ed.,
CBS Pulications, 1986.
5. B.R. Puri and L.R.Sharma, “Principles of Physical Chemistry”, 1st ed.,
Shobanlan Nagin Chand & Co., 2006.
6. R.A.Day and A.L.Underwood, “Quantitative Analysis”, 6 th ed., Prentice
Hall.Publications, 2009.
Course Outcomes:
1. Knowledge of basic principles of fluid mechanics
2. Ability to analyze fluid flow problems with the application of the
momentum and energy equations
Capability to analyze pipe flows as well as fluid machinery
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TEXT BOOKS
1. W.L.McCabe, J.C.Smith & Peter Harriot, “Unit Operations of Chemical
Engineering”, 6th ed., McGraw-Hill, 2001.
2. Chattopadhyay P, “Unit Operations of Chemical Engineering”, Vol -1,
Khanna Publishers, 2003.
REFERENCE BOOKS
1. Christie J Geankoplis, “Transport Processes and Unit Operations”,
3rd ed., PHI Pvt Ltd, 1993.
2. Foust, Alan S., “Principles of Unit Operations”, 2nd ed., John Wiley and
Sons, 1980.
3. J.M. Coulson, J.F. Richardson, “Chemical Engineering”, Vol-I,
Oxford,Pergamon Press, 1968.
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TEXT BOOKS
1. Hougen O.A Watson K.M and Ragatz .R.A, “Chemical Process
Principles” Part – I: Material and Energy Balance ,John Wiley sons,
2nd ed., CBS Publishers & Distributors, 1965.
2. V. Venkataramani & N.Anantharaman,”Process Calculations”, 1st ed.,
PHI Publications, 2003.
REFERENCE BOOKS
1. B.I.Bhatt and S.M.Vora, “Stoichiometry”, 4th ed., Tata McGraw Hill, New
Delhi 2004.
2. D.H.Himmelblau, “Basic Principles and Calculations in Chemical
Engineers”, 5th ed., Prentice Hall, 1989.
Course Outcome:
The designing and preparation of most organic compounds and
pharmaceuticals is based on the reaction mechanism involved in the reaction.
This course is aimed at making the student familiar with reaction mechanism
and stereo chemical aspects.
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UNIT – III
a) Characteristic properties of Alcohols, Phenols, Carboxylic acids,
Aldehydes, Ketones, Amines.
b) Organic Named Reactions: Wolf – Kishner reduction, Hoffmann
rearrangement, Sandmaeyer reaction, Diels – Alder reaction.
TEXT BOOKS:
1. Arun Bahl and B.S. Bahl, “Text Book to Organic Chemistry”, 8th ed.,
S.Chand, 2009.
REFERENCE BOOKS:
1. I.L.Finar, “Organic Chemistry”, Vol – I, 6 th edition, Longman Scientific
Publications, 2006.
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Course Outcomes:
This lab will provide a firsthand knowledge of various analytical techniques of
Chemistry by laying special emphasis on real time spectrometers.
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TEXT BOOKS:
1. Vogel’s Textbook of Quantitative Chemical Analysis J.Maedham,
R.C.Denney, J.D.Barnes, M.Thomas & B.Siva Sankar, “Pearson
Publications” – Volume – 1, 6 th edition, 2009.
st
2. B.Viswanathan, P.S.Raghavan, “Practical Physical Chemistry”, 1 edition,
Viva Books Pvt., 2005.
Course Outcomes:
1. Identify, name, and characterize flow patterns and regimes.
2. Utilize basic measurement techniques of fluid mechanics.
3. Measure fluid pressure and relate it to flow velocity.
4. Demonstrate practical understanding of friction losses in flows.
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List of Experiments
1. Identification of Laminar and Turbulent Flows (Reynolds Apparatus).
2. Verification of Bernoulli’s Equation
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Training Methodology:
The training methodology is designed to bring about changes in attitudes
through experience-based learning. Activities in simulated environments
such as role plays, group discussions, micro-presentations, audio-video
clippings, case studies, psychometric tests etc., will provide students insights
into their strengths and weaknesses.
Learning Outcomes:
1. To help students to develop formal communication skills in a work place
2. To make them acquire team skill by working in group activities
3. To equip them with suitable language and speech patterns in a workplace
4. To enhance the ability of critical & lateral thinking while addressing the
issues at any situation
5. To enable them to present themselves confidently in job interviews
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REFERENCE BOOKS :
1. Edward Holffman, Ace the Corporate Personality, McGraw Hill,2001
2. Adrian Furnham, Personality and Intelligence at Work, Psychology
Press, 2008.
3. John Adair Kegan Page, “Leadership for Innovation” 1st edition, Kogan,
2007.
4. M.Ashraf Rizvi, “Effective Technical Communication”, 1st edition, Tata
McGraw Hill, 2005.
5. Krishna Mohan & NP Singh , “Speaking English Effectively” 1st edition,
Macmillan, 2008.
6. Soft Skills Material of Infosys Under the Academic Initiative of Campus
Connect
7. K.R. Lakshminarayana & T. Murugavel, “Managing Soft Skills”, Scitech
Publications. 2009
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Course Outcomes:
1. Explain, discuss and describe the principles and theories related to
basic process control instrumentation.
2. Read and analyze instrumentation diagrams.
3. Design a simple instrumentation system
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REFERENCE BOOKS
1. D.M.Considine, “Hand Book of Instrumentation”, 2 nd ed., Mc Graw
Hill, 1957.
2. Norman Anderson, “Instrumentation for Process Measurement and
Control”, 3rd ed., CRC Press, 1997.
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Course Outcomes:
Having successfully completed this course, the student will be able to:
(1) Apply advance C programming techniques such as pointers, dynamic
memory allocation, structures to developing solutions for particular
problems;
(2) Design and implement abstract data types such as linked list, stack,
queue and tree by using C as the programming language using static
or dynamic implementations;
(3) Evaluate and choose appropriate abstract data types to solve particu-
lar problems;
(4) Design and implement C programs that apply abstract data types.
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UNIT V - Graphs
Graphs – ADT, definitions and properties, modeling problems as graphs,
representation – adjacency matrix and adjacency list, basic graph traversals
– breath first search and depth first search. Applications of graphs.
TEXT BOOKS :
1. Richard F.Gilberg, Behrouz A. Forouzan, Data Structures - A Pseudo
code Approach with C, Second Edition, Cengage Learning.
2. Y. Langsam, M.J.Augeustein and A.M.Tenenbaum, “Data Structures
Using C”, Pearson Education Asia.
REFERENCE BOOKS :
1. Mark Allen Weiss, “Data Structures and Algorithm Analysis in C”,
Second Edition, Pearson Education.
2. Sartaj Sahni, Data Structures, Algorithms and Applications in C++ ,
Universities Press, Second Edition, 2005
3. Jean Paul Tremblay and Paul G. Sorenson, An Introduction to Data
Structures with Applications,Tata Mc-Graw Hill, Second Edition, 26th
Reprint 2004
4. KRUSE, Data Structures and Programming Design-PHI
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Course Outcomes:
1. Ability to apply fundamental concepts of thermodynamics to engineering
applications.
2. Ability to estimate thermodynamic properties of substances in gas and
liquid states.
3. Capability to determine thermodynamic efficiency of various energy
related processes.
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TEXT BOOKS :
1. J.M.Smith, H.C,Vanness, M.M.Abbot, “Introduction to Chemical
Engineering Thermodynamics”, 6th ed., Tata McGraw Hill – 2003.
2. Y.V.C.Rao, “Chemical Engineering Thermodynamics”, 1 st ed.,
University Publication, 1997.
REFERENCE BOOKS :
1. Dodge B.F. “Chemical Engineering Thermodynamics”. 1 st ed., Mc Graw
Hill, 1960.
2. Kyle B.G. “Chemical and Process Thermodynamics”, 1st ed., PHI,1990.
Course Outcomes:
The student will be able to
1. Understand and apply the basic methods of characterization of
particles and bulk solids.
2. How to crush and grind a solid material and separate ground material
in to various sizes.
3. Explain application of unit operations and can describe their
operational principles.
4. Describe the operation of filtration processes and types of filters
used to perform solid-liquid separations.
UNIT I - Properties of Solids
Properties, handling and mixing of particulate solids, Properties of particulate
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masses, Storage and mixing of solids, Mixers for cohesive and non-cohesive
solids.
UNIT II - Conveyors
Transportation of solid particulate mass. Belt, screw, apron conveyers, bucket
elevators, Pneumatic conveying.
TEXT BOOKS :
1. W.L.Mc Cabe, J.C.Smith & P.Harriott, “Unit Operations of Chemical
Engineering”, 5th ed.,McGraw-Hill, Inc, 1993.
2. Foust et.al, “Principles of Unit Operations” 2nd ed.,wiley, New York,
1980.
REFERENCE BOOKS :
1. W.L.Badger and J.T.Banchero, “Introduction to Chemical Engineering”,
1st ed., TMH, 1997.
2. Perry J.H , “Chemical Engineer’s Hand book”, 6th ed., McGraw-Hill
New York, 1984.
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Course Outcomes:
1. Ability to understand the manufacturing of various inorganic and
organic chemicals.
2. Ability to understand the process flow diagram and various process
parameters.
3. Ability to identify and solve engineering problems during production.
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TEXT BOOKS :
1. M.Gopal Rao and M. Sittig “Dryden’s outlines of chemical technology”,
2nd ed., East west press, 1973.
2. Shreve’s “Chemical Process Industries”, 5 th ed., Mc Graw Hill, 1984.
REFERENCE BOOKS :
1. Industrial Chemistry by B.K. Sharma.
2. Krishna Prakashan Media (P) Ltd., 1 st ed.,1985
Course Outcomes:
The student will be able to
1. Design and conduct experiments, as well as to analyze and interpret
data
2. Formulate hypotheses, design experiments
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2. Screen Effectiveness
3. Jaw Crusher
4. Ball Mill
5. Roll Crusher
6. Sedimentation
8. Froth Flotation
9. ICI Sedimentation
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Course Outcomes:
1. Predict the outcome of several common organic reaction types
through a basic understanding of starting materials, functional
groups, mechanism, and typical reaction conditions.
REFERENCE BOOK :
1. A.I Vogel Pearson, “Elementary Practical Organic Chemistry”,
Publications, 2000.
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Course Outcomes:
1. To enable students to write logical sentences and paragraphs, use
appropriate diction, grammar and punctuation.
2. To expose them to the world of business and business register
3. To make them compose clear and concise business messages
4. To produce business documents for mailing to external recipients or
intra-organizational circulation
5. To enable them to speak business English for handling various
business situations
UNIT I - Writing
- Elements of Technical Writing : Sentence structure - reducing verbosity -
arranging ideas logically – building coherence - paragraph level and
document level - topic sentence - cohesive devices – transitionals –
paraphrasing – précis-writing.
- Mechanics of Writing: Stylistic elements – the rapporteur- the purpose-
the reader (audience) - elementary rules of grammar- choice of diction -
elementary principles of composition - matters of form – punctuation -
conventions of business communication - language and tone - weak
links in business correspondence - ethical concerns in business writing.
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UNIT II - Reports
- Parts of the Report: Writing an abstract - features of a good abstract –
approach - compare and contrast - cause and effect.
- Types of Technical Reports : Drafting a technical proposal - formal and
informal proposals - factual reports, feasibility reports, survey reports –
parts of a report - title page –declaration – acknowledgements – table of
contents - abstract – introduction – conclusion – citations – references -
appendices - oral reports and presentations
UNIT III - Letter Writing
- Letter-Writing - Formal and informal letters - structure of formal letters -
expressions of salutations, introductory and concluding paragraphs -
different types of letters - sales letter - complaint letter - adjustment letter
- letter to the editor - covering letter - claim letter – letter of condolence.
UNIT IV - Correspondence
- Business Correspondence : E-mail – nature and scope - e-mail etiquette
- Common Errors in composing e-mails – Quotations - Inviting quotations
- sending quotations – placing orders - Office Communication - agenda -
notice - circular
- Effective Resume-Writing: Structure and presentation - defining career
objective - projecting one’s strengths and skill-sets
- Summarizing - formats and styles - covering letter.
UNIT V - Drafting
- Business Proposals: Drafting business proposals - calculating profit
and loss-averages - ratios and proportions – partnership - simple interest
- compound interest - calculating volumes and areas
· course of action - cause and effect- theme detection - making judgments
- logical deductions - analyzing arguments – syllogisms - Venn diagrams
- matching definitions -verbal reasoning - numerical reasoning - working
out justifications.
REFERENCE BOOKS :
1. Strunk , William, Jr.The Elements of Style, Fourth Edition
2. Rozakis, Laurie, Ph.D, (2003). English Grammar for the Utterly
Confused, McGraw-Hill.
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Course Outcomes:
1. Understand and use empirical equations to solve forced and natural
convection heat-transfer problems;
2. Analyze the heat transfer processes involved in boiling and
condensation;
3. Perform basic calculations of common heat exchangers to determine
relevant design parameters.
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TEXT BOOKS
1. W.L.McCabe, J.C.Smith & P.Harriott,”Unit Operations of Chemical
Engineering”, 6th ed., McGraw-Hill, Inc., 2001.
2. D.Q.Kern, “Process Heat Transfer”, 1 st ed., Tata McGraw Hill, 2002.
REFERENCE BOOKS
1. J.P.Holman, “Heat Transfer”, 8 th ed., McGraw Hill, New York, 1997.
2. Y.V.C.Rao, “Heat Transfer”, 1 st ed., University Press, 2001.
3. Donald Pitts, Leighton E, Sissom, “Schaum’s Outline of Heat Transfer”,
2nd ed., McGraw Hill publications, 1998.
4. J.M. Coulson. J.F.Richardson, “Chemical Engineering”, Vol-1, Oxford,
Pergamon Press, 1968.
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Course Outcomes:
The student will be able to recognize the various modes of mass transfer like
Determination of mass transfer rates using
1. Fick’s Law
2. Estimation of diffusion coefficients
3. Solving of unsteady state diffusion problems
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UNIT IV - Humidification
Introduction, Vapor – pressure curve, definitions, psychometric charts, Enthalpy
of vapor – gas mixtures, humidification and de humidification, operating lines
and design of packed humidifiers, cooling towers, spray chambers.
UNIT V - Drying
Introduction, Definitions of various moisture contents, drying conditions, Rate
of Batch drying under constant drying conditions, mechanism of batch drying,
Drying time, through circulation drying, batch and continuous drying,
equipment design of continuous counter current dryer.
TEXT BOOKS
1. R.E.Treybal “Mass Transfer Operations” 3rd ed., Mc-Graw Hill, 1981.
2. Binay. K.Dutta, “Principles of Mass Transfer and Separation
Processes”,Prentice Hall of India, New Delhi, 2007.
REFERENCE BOOKS
1. C. Judson King, “Separation Processes”, 2nd ed., McGraw Hill, 1982.
2. Seader. J. D, E. J. Henley & D.Keith Roper, “Separation
ProcessesPrinciples”, John Wiley & sons, New York, 2010.
3. Alapati Suryanarayana “Mass Transfer Operations”, 1st ed., New - Age,
International, 2006.
Course Outcomes:
1. On having completed the course, the student will be in a position to
design reactor, with some additional inputs.
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2. The homogeneous reactions & hence the reactors are fairly easy to
design. But, with increasing complexity like in multiple rxns &
heterogeneous rxno.
3. The student has to exercise some caution in designing the reactors.
4. The reactor history coupled with personal experience and sound
judgment are necessary.
TEXT BOOK
1. Octave Levenspiel, “Chemical Reaction Engineering”, 3rd ed., WEE, 1999.
REFERENCE BOOKS
1. H.S.Fogler, “Elements of Chemical Reaction Engineering”, 3 rd ed., PHS,
1992.
2. J.M.Smith, “Chemical Engineering Kinetics”, 3 rd ed., MGH, 1981.
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Course Outcomes:
. 1. Develop mathematical models of chemical processes by writing unsteady-
state mass and energy balances.
2. Ability to design controllers.
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TEXT BOOKS
1. Donald R Coughanowr, “Process System Analysis and Control”
2nd ed., Mc Graw Hill, 1993.
2. G.Stephanepolous, “Chemical Process Control”, 1st ed., Prentice
Hall, 1998.
REFERENCE BOOK
1. Peter Harriott, “Process Control”, Tata McGraw Hill, 2008.
2. R.W.Gaikwad,S.A.Misal “Process Dynamics and Control”,1 st
ed.,Central Techno publications,2004.
Course Outcomes:
The student will be able to
1. Understand the present and future enery demands of the energy resources,
2. Know about various energy auditing and energy conservation methods.
3. Obtain in detail knowledge about the stem distribution and utilization.
4. Know about various renewable energy resources.
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TEXT BOOKS
1. O.P.Gupta, “Elements of Fuels, Furnaces & Refractories”, 3 rd ed.,
Khanna Publications, 1996
2. Sami Sarkar, “Combustion”, 2nd ed., Orient Longman, 1998.
REFERENCE BOOKS
1. Conventional Energy Technology, Fuel and Chemical Energy, Tata Mc
Graw Hill, 1987.
2. G.D.Rai, “Non – Convectional Energy Sources”, 4th ed., Khanna
Publications, 1997.
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Course Outcomes:
1. This course will enable the student to identify and understand safety
hazards in a business or industrial setting.
2. The principles learned in this course will allow the student to use
current safety theory and guidelines in making the workplace safer
for workers.
3. The intention is for the student to be able to: Identify basic safety
hazards.
UNIT I - Safety
Safety programs, engineering ethics, accident and loss statistics, acceptable
risk, public perception.
UNIT II - Toxicology
How Toxicants enter biological organisms & are eliminated from biological
organisms, government regulations, Industrial Hygiene: identification,
evaluation, control.
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TEXT BOOKS
1. DA.Crowl & J.F.Louvar, “Chemical Process Safety”, Vol. 2, Prentice
Hall, 1980.
2. H.H.Fawcett and W.S.Wood, “Safety & Accident Prevention in Chemical
Operations”, 2nd ed., John Wiley and Sons, New York, 1982.
REFERENCE BOOKS
1. R.K.Sinnoot, “Coulson and Richardson’s - Chemical Engineering”,
Vol 6, Butterworth - Heinmann Limited, 1996.
2. Roye Sanders, “Chemical Process Safety”, 1st ed., Elsevier, 2007.
Course Outcomes:
1. Describe how to design experiments, carry them out, and analyze
the data they yield.
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UNIT I - Introduction
Modeling and study of systems in Chemical Engineering leading to systems
of algebraic, ordinary differential and partial equations (both linear and non-
linear systems). Methods of solution of systems of linear algebraic equations,
linear homogeneous ordinary differential equations and linear non-
homogeneous ordinary differential equations observed in systems of interest
to chemical engineers.
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TEXT BOOKS
1. S. Pushpavanam, “Mathematical Methods in Chemical Engineering”,
1st ed., Prentice Hall of India, New Delhi, 2005.
2. Douglas C. Montgomery, “Design and Analysis of Experiments”, 5th
ed., John Wiley and Sons INC, 2007.
REFERENCE BOOKS
1. W.L. Hines and D.C. Montgomery, “Probability and Statistics in
Engineering and Management”, John Wiley and Sons, 1980.
2. Ed. Oven L. Davies Longman Group, “Design and Analysis of Industrial
Experiments”, 2nd ed., 1978.
3. Jenson and Jeffereys, “Mathematical Methods in Chemical
Engineering”, Academic Press, 1963.
4. C.F. Jeff Wu & Michael Hamada 2009, Experiments-Panning, Analysis,
and Parameter Design Optimization, 2 nd edn, John Wiley & Sons. Inc.
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Course Outcomes:
The course will provide a sound practical knowledge of the three main heat
transfer phenomena namely conduction, convection and radiation.
List of Experiments
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Course Outcomes:
1. Ability to understand the manufacturing of various inorganic and organic
chemicals
2. Ability to estimate melting / boiling points, preparation, analysis of
different chemical compounds.
List of Experiments
1. Estimation of Glucose
2. Estimation of Sucrose
3. Iodine value of oil
4. Saponification value of oil
5. Acid value of oil
6. Preparation of Acetanilide
7. Preparation of Aspirin (Acetyl Salicylic acid)
8. Preparation of Azodye (Phenyl Azo – 2 – Naphthol)
9. Preparation of Nitrobenzene from benzene
10. Preparation of M – Dinitro Benzene from Nitro Benzene
11. Preparation of Urea formaldehyde resin
12. Preparation of Phenol formaldehyde resin
13. Determination of Alkalinity of water
14. Determination of Percentage purity of lime stone
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Course Outcomes:
To provides a sound practical knowledge of different control systems,
controllers, and control valves that are used in industries.
List of Experiments:
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Course Outcomes:
Students will be able to:
1. Apply the economic way of thinking to individual decisions and
business decisions
2. Understand how prices get determined in markets, how market
participants benefit in the form of consumer surplus and producer
surplus, and what are the consequences of government intervention
3. Understand the roles of managers in firms
4. Understand the internal and external decisions to be made by
managers
5. Design competition strategies, including pricing, product
differentiation, research & development, and marketing, according
to the natures of products and the structures of the markets
6. Analyse real-world business problems with a systematic theoretical
framework.
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Text Books:
1. Gupta: Managerial Economics, 1/e TMH, 2005
2. A.R.Arya Sri, Managerial Economics and Financial Analysis, TMH, 2/
e, 2010
Reference Books:
1. Dominic Salvatore, Managerial Economics, Thomson, 2/e, 2006
2. Mote Paull, Managerial Economics, 1/e, TMH, 2004
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Course Outcomes:
The student will be able to recognize the various Principles like design of
operating line equation, design of Distillation units, Tower sizing, design of
single and multi stage cross current, co-current, counter current extractors,
design of adsorption and leaching equipments.
UNIT I - Distillation
Introduction, Fields of application, VLE for miscible liquids, immiscible liquids,
steam distillation, VLE phase diagrams, tie lines, mixture rules, Flash
vaporization and differential distillation for binary and multicomponent
mixtures, Batch distillation with reflux.
UNIT IV - Leaching
Introduction, Fields of application, Preparation of solid for leaching, types of
leaching, Leaching equilibria, Constant under flow conditions, Single and
multistage leaching calculations, equipment for leaching operation.
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TEXT BOOKS
1. R.E.Treybal, “Mass Transfer Operations”, 3rd ed., Mc-Graw Hill, 1981.
2. Binay. K.Dutta, “Principles of Mass Transfer and Separation
Processes”,Prentice Hall of India, New Delhi, 2007.
REFERENCE BOOKS
1. C. Judson King, “Separation Processes”, 2nd ed., McGraw Hill, 1982.
2. Alapati Suryanarayana, “Mass Transfer Operations”, 1st ed., New -
Age, International, 2006.
Course Outcomes:
1. On having completed the course, the student will be in a position to
design reactor, with some additional inputs.
2. The homogeneous reactions & hence the reactors are fairly easy to
design. But, with increasing complexity like in multiple rxns, &
heterogeneous rxno.
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TEXT BOOKS:
1. Octave Levenspiel,”Chemical Reaction Engineering”, 3rd ed., WEE,
1999.
2. H.S.Fogler, “Elementary Chemical Reaction Engineering”, 3rd ed.,
PHS, 1981.
Course Outcomes:
1. State the thermodynamic equations and explain them for solving
actual thermodynamic problems.
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TEXT BOOKS
1. J.M.Smith, H.C.Vanness, “Introduction to Chemical Engineering
Thermodynamics”, 6th ed., TMH, 2003.
2. Kyle.B.G. “Chemical and Process Thermodynamics”, 2 nd ed., PHI,
1990.
REFERENCE BOOKS
1. Dodge B.F “Chemical Engineering Thermodynamics”, 1 st ed., MGH,
1960.
2. Sandler, S.I “Chemical and Engineering Thermodynamics”, 2 nd ed.,
Wiley, 1989.
Course Outcomes:
Students will be able to
1. Apply various transport models for the calculation of membrane fluxes
and the extent of separation for various membrane systems.
2. Identify the types of experimental data needed for the calculation of
membrane parameters.
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TEXT BOOKS
1. M.H.V.Mulder, “Membrane Separations”, Springer Publications, 2007.
2. R.Philip C.Wanket, “Rate-Controlled Separations”, 1st ed., Springer,
2005.
REFERENCE BOOKS
1. S.P.Nunes, K.V.Peinemann, “Membrane Technology in the Chemical
Industry”, Wiley-VCH, 2nd ed., 2006.
2. Rautanbach and R. Albrecht, “Membrane Process”, John Wiley & Sons,
1st ed., 1986.
3. J.G.Crespo, K.W.Bodekes, “Membrane Processes in Separation and
Purification”, Kluwer Academic Publications, 1st ed., 1994.
4. C .J. Geankoplis, “Transport Processes and Unit Operations”,
3rd ed., PHI, 2003.
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Course Outcomes:
Mathematical tools are indispensable to process modeling, analysis,
engineering design and research. The theme of the course is to introduce a
spectrum of widely used mathematical methods in chemical engineering
useful to solve problems commonly encountered.
UNIT I - Introduction
Mathematical formulations of the physical problem, formulation of differential
equations, application of the law of conservation of mass and energy, flow
systems, rate equations.
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TEXT BOOKS
1. T.S.Sherwood & C. Reed, “Applied Mathematics in Chemical
Engineering”, 2nd ed., Tata McGraw Hill Publishers, 1998.
2. V.G.Jenson & G.V.Jeffreys, “Mathematical Methods in Chemical
Engineering”, 2nd ed., Academic Press, London, 2000.
REFERENCE BOOKS
1. Steve Chopra, “ Numerical Methods for Chemical Engineering” 5th
ed., Tata McGraw Hill Publishers, 2009.
2. Pushpavanam ,Kondaswamy, “Numerical Methods for Chemical
Engineering” 1st ed., PHI Publishers, 2005.
Course Outcomes:
1. The course will help the students to understand and apply the
principles of biochemical engineering in the analysis and design of
industrial biochemical processes.
2. Understanding of biological basics and bio processing.
3. Understanding the difference between bioprocesses and chemical
processes.
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TEXT BOOK
1. J.E.Bailey & David F. Ollis, “Bio Chemical Engineering Fundamentals”,
2nd ed., McGraw Hill Publishers, 1986.
2. Michael L. Shuler & Fikret Kargi, “Bioprocess Engineering”, 1st ed., Pearson
Education International Series, 2002.
REFERENCE BOOKS
1. James – Lee , “BioChemical Engineering”, 1st ed., Prentice Hall
Publishers, 1992.
2. Pauline M. Doran, “Bioprocess engineering principles” Elsevier
Publishers, 1995.
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Course Outcomes:
Provides a practical knowledge to students of the different chemical reactors
used in chemical engineering industries.
List of Experiments:
Chemical Engineering 57
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Course Outcomes:
1. Provides to students the knowledge of various mass transfer operations
used in industries.
2. Provides to students able to design equipments.
List of experiments:
58 Chemical Engineering
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Course Outcomes:
The student will be able to
1. Compare projects using the methods of net present value, discounted
cash flow and equivalent minimum investment period
2. Develop a plant capital cost estimate based on published data,
3. Determine the impact of taxation, depreciation and investment incentives
on the economic viability of a project.
4.know the procedures involved in optimum designing
Chemical Engineering 59
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TEXT BOOK:
1. K.D. Timmerhaus & M.S. Peters, “Plant Design and Economics for “
Chemical Engg.”, 3 rd ed., McGraw Hill, 1981.
Course Outcomes:
1. Able to design heat transfer equipment and mass transfer equipmet.
2. Able to design cooling and heating systems of chemical reactors.
3. Able to use software tools for the analysis of process equipment.
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Design of Packed Towers for Absorption: Flow of liquid over packing’s, limiting
gas velocities, Pressure-drop calculations, design of packed towers using
absorption coefficients, design of packed tower using transfer-unit method.
TEXT BOOKS
1. D.Q. Kern, “Process Heat Transfer”, 1 st ed., Tata McGraw Hill, 2001.
2. S. D. Dawande, “Process Equipment Design”, Vol 1 & 2, 4 th ed., Central
Techno Publishers, 2005.
REFERENCE BOOKS
1. Robert E. Treybal, “Mass Transfer Operations”, McGraw Hill, 1982.
2. Morris and Jackson, “Absorption Towers”,Butter Worth’s Scientific
Publications, 1985.
3. Pring and Osborn Butter Worth,”Cooling Tower Principles and Practice”,
Heinemann - Hill, 1986.
4. Coulson & Richardson Series, “Chemical Engineering”, Volume 6, Pergaman
Press, 1983.
IV Year B.Tech. Chemical Engg. I - Semester
L T P To C
4 0 - 4 4
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Course Outcomes:
1. Understand the important physical phenomena from the problem
statement.
2. Develop model equations for the given system.
3. Demonstrate the model solving ability for various processes/unit
operations.
4. Demonstrate the ability to use a process simulation.
UNIT I - Fundamentals
Mathematical models for chemical engineering systems, fundamentals,
introduction to fundamental laws, examples of mathematical models of
chemical engineering systems, constant volume CSTRS, two heated tanks.
UNIT II - Examples
Gas phase pressurized CSTR, non-isothermal CSTR, single component
vaporizer, batch reactor, reactor with mass transfer, ideal binary distillation
column, batch distillation with holdup.
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TEXT BOOKS
1. William L. Luyben, “Process Modeling, Simulation and Control for
Chemical Engineers”, 2 nd ed., McGraw - Hill International, 1990.
2. Santosh.K. Gupta, “Numerical Methods in Engineering”, 2 nd ed., New
Age International (P) Ltd., 2003.
REFERENCE BOOK
1. K.Balu and K.Padmanabhan, “Modeling and Analysis of Chemical
Engineering Processes”, IK International Private Limited, 2007.
UNIT I -
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UNIT II -
Characterization of effluent streams, oxygen demands and their determination
(BOD, COD, and TOC), Oxygen sag curve, BOD curve mathematical, controlling
of BOD curve, self purification of running streams, sources and characteristics
of pollutants in fertilizer, paper and pulp industry.
UNIT III -
General methods of control and removal of sulfur dioxide, oxides of nitrogen
and organic vapors from gaseous effluent, treatment of liquid and gaseous
effluent in fertilizer industry.
UNIT IV -
Air pollution sampling and measurement: Types of pollutant and sampling
and measurement, ambient air sampling: collection of gaseous air pollutants,
collection of particulate air pollutants. Stack sampling: sampling system,
particulate sampling, and gaseous sampling. Analysis of air pollutants:
Sulphur dioxide, nitrogen oxides, carbon monoxide, oxidants and Ozone,
hydrocarbons, particulate matter.
UNIT V -
Air pollution control methods and equipments: Source collection methods:
raw material changes, process changes, and equipment modification.
Cleaning of gaseous equipments particulate emission control: collection
efficiency, control equipment like gravitational settling chambers, Cyclone
separators, fabric filters, scrubbers, packed beds and plate columns, venturi
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TEXT BOOKS
1. Environmental pollution and control engineering, Rao C. S. - Wiley
Eastern Limited, India, 1993.
2. Pollution control in process industries by S.P. Mahajan TMH.,1985.
REFERENCE BOOKS
1. Waste water treatment by M.Narayana Rao and A.K.Datta,Oxford and
IHB publ. New Delhi.
2. Air pollution control by P.Prathap mouli and N.Venkata subbayya. Divya
Jyothi Prakashan, Jodhpur.
3. “Industrial Pollution Control and Engineering.” Swamy AVN, Galgotia
publications, 2005, Hyderabad
Course Outcomes:
Students have an understanding and appreciation for the implications of the
science of transport phenomena on society as a whole, and recognize
connections between transport phenomena and other areas of study.
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TEXT BOOK:
1. R.B.Bird, W.E. Stewart, “Transport Phenomena”, 1st ed., Mc Graw Hill,
2003.
REFERENCE BOOKS :
1. James. R. Welty, Robert. E. E. Wilson, “Fundamentals of Momentum,
Heat and Mass Transfer”, 2nd ed., John Wiley & sons, 2002.
2. L. Theodore, “Transport Phenomena”, 2nd ed., John Wiley & Sons,
2002.
3. J. Geankoplis, “Transport Processes & Unit Operations”, 3rd ed., Prentice
Hall of India, 2003.
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Studying this subject the students will learn about the extraction and production
of oil and gas to meet energy needs, as well as refining of crude oil for a wide
spectrum of useful products, such as petrochemicals, Chemicals, Plastics.
Course Outcomes:
1. Introduction with the petroleum refinery worldwide.
2. Develop knowledge of different refining processes.
3. To find the suitable refining technology for maximizing the gasoline
yield.
4. Students will be well-veresed with some aspects of Petrochemical
Technology in detail.
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TEXT BOOKS
1. B.K.Bhaskara Rao, “Modern petroleum refining processes” 4 th edition,
Oxford and IBH Publication, 2002.
2. B.K.Bhaskara Rao, “ A Text book on Petrochemicals” 2nd edition, Kanna
publishers
REFERENCE BOOKS
1. O.P.Gupta, “Fuels, furnaces & Refractories” Kanna publishers.
2. Lahari, Biswas, “Petrochemical Industries”.
Course Outcomes:
This Is The course to Provide A Practical Working Guide To Understanding
And Developing Successful PI Solutions That Deliver Savings And
Efficiencies. It Will Appeal To Engineers Working With Leading-Edge Process
Technologies And Those Involved Research
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UNIT – I Introduction
Definition of process intensification; Benefits and drawbacks; Techniques
for PI application – passive and active techniques.
UNIT – II Flow Patterns
Mixing, flow patterns, heat transfer: Scales of mixing; Flow patterns in reactors,
Mixing in stirred tanks, Scale up of mixing; Mixing in intensified equipment;
TEXT BOOKS
1. Stankiewicz, A. and Moulin, (Eds.), “Engineering: the Chemical Process
Plants.
2. Process Intensification”, Marcel Dekker.
REFERENCE BOOKS
1. Process intensification by David Reay, Colin Ramshaw, Adam Harvey.
Chemical Engineering 69
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3 1 - 4 4
Course Outcomes:
1. Identify different types of optimization problems.
2. Understanding of different optimization technique.
3. Ability to solve various single and multivariable optimization problems.
4. Ability to solve problems by using least square analysis.
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TEXT BOOK
1. T.F.Edgar and Himmelblau DM, “Optimization of Chemical Processes”,
McGraw Hill, 2001.
REFERENCE BOOK
1. Kalyan Moy Deb, “Optimization for Engineering Design”, PHI, 2000.
(ELECTIVE-IV)
Course Outcome:
The course aims to offer a sound base in the knowledge of various polymers
and plastics used in industries, their properties etc.
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Polyethylene (LDPE & HDPE), Polypropylene, PVC and its copolymers, acetals,
PTFE, Condensation compounds: polyester – PMMA, PET, Alkyd, Epoxy resins,
Polyurethanes, Silicons, PF, UF, MF resins.
TEXT BOOKS:
1. Bill Meyer, “Text Book of Polymer Science”, 3rd ed., John Wiley and
Sons, 1984.
2. J.A Bryson Newness – Butterwarths, “Plastic Materials”, London, 1989.
REFERENCE BOOKS :
1. J.H.Briston and C.C.Gosselin, “Introduction to Plastics”, Newnes,
London, 1968.
2. C.C Winding and G.D.Haitt, “Polymeric Materials”, Mc Graw Hill
Book,1961.
3. M.S.Bhatnagar, “A Text Book of Polymers”, 1st ed., S. Chand and
Company, New Delhi, 2007.
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5. Mechanical
Course Outcomes: Aspects of Chemical equipment design and drawing of 1-2
shell and tube
Mathematical toolsheat
areexchanger.
indispensable to process modeling, analysis,
6. Mechanical
engineering designAspects of Chemical
and research. The equipment
objective ofdesign and drawing
the course of 2-4
is to introduce
shell and
a spectrum of tube heat
widely exchanger.
used mathematical methods in chemical engineering
7. Mechanical
useful Aspects ofcommonly
to solve problems Chemical encountered.
equipment design and drawing of Feed
forward evaporator.
UNITDrawing
8. I - BasicofConcepts ofcolumn
distillation Colloids byand Interfaces
using Mc - Cabe Thiele method
Introduction,
9. Drawing of Examples
distillation
of column
Interfacial
by using
Phenomena,
PonchonSolid-Fluid
- Savarit method
Interfaces,
Colloids.
10. Design of Adsorption Column
Properties
11. DesignofofColloid
Absorption
Dispersions:
Tower Introduction, Sedimentation under Gravity,
Sedimentation
12. Design of Batchin a Centrifugal
Reactor Field, Brownian Motion, Osmotic pressure,
Optical
13. Design
properties,
of CSTR. Electrical Properties, Rheological Properties of Colloid
Dispersions.
IV Year B.Tech. Chemical Engg. I - Semester
UNIT II - Surfactants and their Properties L T P To C
Introduction, Surfactants and their Properties, Emulsions and - Microemulsions,
- 3 3 2
foams.
CH423
Surface CHEMICAL
and Interfacial Tension:PROCESS
Introduction, SIMULATION LAB
Surface tension, Interfacial
Tension, Contact Angle and Wetting, Shape of the Surfaces and interfaces.
Course Description & Objectives:
UNIT
To III - Surface
provide and Interfacial
experience Tension
and knowledge in chemical process simulation. the
Measurement
material covered of Surface
integrates andtheInterfacial Tension, in
use of simulation Measurement
the followingofsubjects:
Contact
Angle; Intermolecular
material and Surface
and energy balances, Forces:
heat and Introduction, Vanderwalls
mass transfer, Forces.
thermodynamics,
Intermolecular and
multicomponent Surface Forces:
vapor-liquid Electrostatic
equilibrium, double layer force, The DLVO
and others.
theory, Non-DLVO forces.
Course Outcomes:
UNIT1.IVThe
- Adsorption at Interfaces
course provides a sound practical knowledge about chemical
Introduction,
process Themodeling,
Gibbs Dividing surface, Gibbs Adsorption Equation,
Simulation.
Langmuir and Frumkin
2. Students will beAdsorption
able to Isotherms,
design of Surface
various Equation
chemicalofengineering
state(EOS),
Effect of equipments.
Salt on Adsorption of Surfactants.
3. Students will be able to gaining experience in simulation packages.
List of Experiments
UNITSimulation
1. V - Adsorption at Interfaces
of gravity flow tank system
Adsorption
2. Simulation
Isotherms
of three
incorporating
constant holdup
the Electrostatic
CSTRs in series
Effects, Calculation of
Free Simulation
3. energy of Adsorption,
of three variable
Adsorption
holdup
of inorganic
CSTRs salts
in series
at interfaces, Dynamics
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TEXT BOOKS
1. William L. Luyben, “Process Modeling, Simulation and Control for
Chemical Engineers”, 2 nd ed., McGraw - Hill International, 1990.
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Course Outcomes:
The course will enable students to interpret the process of Industrial pollution
control through consideration of appropriate experiments, to gain enough
knowledge to handle equipments besides kindling their interest towards
carrying out R & D activities.
List of Experiments
1. Water Analysis
2. Neutralization of acids by titration
3. Neutralization of bases by titration
4. Absorption of color
5. Adsorption of phenol
6. Adsorption of gaseous pollutants
7. Toxic metal analysis
8. Filtration of suspended solids
9. Flocculation
10. Settling, particulate matter collection
76 Chemical Engineering
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Course Outcomes:
The student will be able to
1. Explore the design, development, manufacture, and evaluation of
traditional and novel drug delivery systems
2. Emphasize practical solutions and applications to theoretical and
research-based problems.
3. Know the manufacturing and testing procedures of various
pharmaceuticals and fine chemicals.
4. Acquire knowledge in tablet making, coating and sterilization.
Chemical Engineering 77
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UNIT V - Sterilization
Sterilization: introduction, risk factor, methods of sterilization, heat (dry and
moist), heating with bactericide, filtration, gaseous sterilization and radiation
sterilization, suitable example to be discussed.
TEXT BOOKS:
1. Remington’s, “Pharmaceutical Science”, 13th ed., Mac Publishing
Company,1965.
2. Blently and Driver, “Text Book of Pharmaceutical Chemistry” 8th ed.,
Oxford University Press, London, 1960.
REFERENCE BOOKS :
1. H A Rawlins, B Tindell and Box Blently’s,”Text Book of Pharmaceutical
Chemistry”, 8th ed., OU Press, London, 1977.
2. Faith, Kayes and Clark, “Industrial Chemicals”, John Wiley & Sons,
3rd ed., 1965.
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Course Outcomes:
1. Analyze and interpret raw field data in order to design structures in
fractured rock masses using various methods (mapping surface and
underground exposures; drilling, i.e. manual core logging and
geophysical logging, etc.).
2. Design basic surface and underground structures in rock for mining
and heavy civil applications (i.e. slope, underground openings, tunnels,
stopes, shafts, etc).
3. Assess the life cycle of a mineral project from exploration to
decommissioning and final closure.
4. Apply basic understanding of soil mechanics in order to discern whether
a design problem requires more comprehensive understanding.
5. Determine the economic feasibility of a rock engineering design.
6. Determine environmental factors that impact on a rock engineering
design.
7. Assess social, cultural, political and legal impact of a rock engineering
design.
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UNIT III -Beneficiation circuits for hematite and magnetite iron ores
Dry and wet processes – their scopes and limitations. Pulp densities at
different stages of wet operations. Estimation of water requirements and
pumping loads.
TEXT BOOKS
1. A.F.Taggart “ Elements of Mineral Dressing” John Wiley and Sons, 1956.
2. Barty A. Wills and Tim Napier Munn “Mineral Processing Technology”
Elsevier Publishers, 2006.
REFERENCE BOOKS
1. A.F.Taggart “Handbook of Mineral Dressing “ John Wiley and Sons, New
York. 1956.
2. A.Gupta and D.S.Yan,” Mineral Processing Design and Operation”
Elsevier 2006.
3. T.Simon “Ore Dressing Principles and Practice” McGraw Hill Co., 1924.
4. S.J.Truscott , “Ore Dressing” ,London Macmillan. 1923.
6. Handbook of Ore Dressing by A.W.Allen – McGraw Hill Co., 1920.
7. Complete Technology Book on Mineral Processing by NPSC Board –
Asia Pacific Business Press 2008.
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Course Outcomes:
1. Outline the process of red and white meat slaughter, explain meat
structure and inspect meat quality parameters
2. Process manufactured meat products to produce variety of animal
food products.
3. Identify the areas of concern in the processing of meat products, in
relation to process control, undesirable microbes and export
4. Explain the requirements for meat export and chemical and
physiological structure of meat.
5. Demonstrate processing techniques used to produce a variety of
milk products.
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TEXT BOOKS
1. Norman N.Potler Joseph .H. Hotchk’ss, “ Food Science” 5 th Edition,
CBS Publishers & Distributors India, 1987.
2. Owen .R.Fennema, “Principles of Food Science Part I & II”, Marcel
Dekker Inc New York, 1976.
REFERENCE BOOKS
1. Heid, J.L., Joslyn M.A, Fundamentals of Food Processing Operation,
3rd Edition, The AVI Publishing Co., Westport,1967.
2. Heldman, D.R., Food Process Engineering, 2 nd Edition, The AVI
Publishing Co.,1965
Course Outcomes:
1. Understand and apply basic concepts of nanotechnology and
nanoscience.
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TEXT BOOKS
1. Jean-Marie Lehn. Supramolecular Chemistry, 1 st Edition, W iley
Publications, 1995.
2. Novailhat, Alain, Introduction to Nano technology, 2 nd Edition, Wiley
Publications, 2007.
REFERENCE BOOKS
1. Hovnyax G., Moore J., Tibbals J., Fundamental of Nanotechnology,
1st Edition, CRC Press.
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Course Outcomes:
1. Understanding of fundamental mathematics and to solve problems
of algebraic and differential equations, simultaneous equation,
partial differential equations
2. Ability to convert problem solving strategies to procedural algorithms
and to write program structures
3. Ability to solve engineering problems using computational
techniques
4. Ability to assess reasonableness of solutions, and elect appropriate
levels of solution sophistication
UNIT I - Introduction
Review on programming languages, basic, FORTRAN, Review on operation
system Commands, Numerical solution of first order differential equations
with initial conditions, Euler’s Method, Runge kutta method.
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TEXT BOOKS:
1. Leon Lapidas, “Digital Computation for Chemical Engineering”, 2nd
ed., MGH, 1962.
2. Jerry, O. Breneman GL., “Spread Sheet Chemistry”, PH, Englewood
Cliffs,1991.
REFERENCE BOOKS:
1. Hanna OT Scandell O.C, “Computational Methods in Chemical
Engineering”, PH, 1995.
2. Taxali R. K. T. K, “ D Base IV Made Simple”, 1st ed.,TMH, 1991.
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Course Outcomes:
1. Ability to estimate pressure drop, bubble size, TDH, voidage, heat
and mass transfer rates for the fluidized beds
2. Ability to write model equations for fluidized beds
3. Ability to design gas-solid fluidized bed reactors
UNIT V - Design
Fluidized bed for physical operations, catalytic reactions and non-catalytic
reactions.
TEXT BOOKS
1. Kunii, D. and Levenspiel, O., “Fluidization Engineering”, John Wiley &
Sons, Inc.
2. Leva, M., “Fluidization”, McGraw-Hill Book Co.
3. Davidson, J.F. and Harrison, D., “Fluidized Particle”, Cambridge
University Press.
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