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Intensity (counts)
especially WET CHEMICAL METHOD (WCM) due to its simplicity and 6000
cost effective 5000 20000
Intensity (counts)
4000
Drying of precipitate is on of the crucial step in WCM
3000 15000
However
Available literatures mainly used conventional oven drying which 2000
takes almost 16 hours for the precipitate to dry thoroughly 1000 10000
>> very time consuming 0
Therefore 0 20 40 60 5000
Microwave drying was used in this project as an alternative to dry 2 Ɵ (degree)
the precipitate. The process is rapid as precipitate can be dried
rapidly in 15 minutes. (b) TEM Analysis: Nano-sized HA particles, needle-like morphology 0
20 30 40 50
2 Ɵ (degree)
OBJECTIVE Particle size: Length = 66.7 nm
Width = 23.6 nm
To synthesize pure HA powder by wet chemical method via (c) Mechanical Properties of HA sintered at 1200ºC
microwave drying and to investigate the HA powder properties as BET :
well as sinterability of HA sintered samples. Specific Surface area =111.07 m2/g