Beruflich Dokumente
Kultur Dokumente
Operation
Microprocessor Manual
pH/ORP/ION
Benchtop Meter
1
CONTENTS
1. Specifications ................................................................................................................1
2. Panel Description ...........................................................................................................2
2.1 Front panel ...........................................................................................................2
2.2 Sockets...................................................................................................................2
2.3 Display...................................................................................................................3
2.4 Keypad ..................................................................................................................4
3. Operation ........................................................................................................................5
3.1 Measurement ........................................................................................................5
3.2 Block diagram of parameter settings .................................................................6
3.3 Parameter settings ...............................................................................................7
3.4 Auto/Manual data storage.................................................................................16
3.5 Data transmitting and display ..........................................................................18
3.6 Delet all of data...................................................................................................23
4. Calibration....................................................................................................................24
4.1 pH calibration.....................................................................................................24
4.2 Opearation of pH calibration............................................................................26
4.3 Auto calibration for preset buffers (CT/CN)...................................................26
4.4 Any Buffer manual calibration (CA) ...............................................................29
4.5 Define Buffers calibration (CD)........................................................................31
4.6 ORP relative potential adjustment...................................................................33
4.7 ION concentration calibration (SP-2500 only)................................................34
4.8 ION concentration calibration (CC) (SP-2500 only) ......................................35
5. Error message...............................................................................................................37
6. Maintenance .................................................................................................................38
6.1Battery replacement............................................................................................38
6.2 Electrode clean and maintenance .....................................................................38
7. Modbus protocol and instructions..............................................................................39
7.1 Function code .....................................................................................................39
7.2 Modbus name and address table ......................................................................40
8. Appenix .........................................................................................................................41
Note: The instrument software and hardware maybe modified to make progress of the better operation and
better accuracy. Thus, this may result in difference between this manual and your instrument. We can not
guarantee there are no errors in the manual. Therefore, we are sure that you understand that we cannot
accept any legal claims resulting from the data, figures or descriptions.
1. Specifications
Model SP-2300 SP-2500
Measuring Unit pH/ORP/TEMP pH/ORP/TEMP/ION
pH -2.00~16.00 pH/-2.000~16.000 pH
Measuring ORP -1999~1999 mV/-1999.9~1999.9 mV
Range TEMP -10.0~110.0 qC
ION 0.001~1999.9 ppm(mg/l)
pH 0.01 pH/0.001 pH
Resolution ORP 1 mV/0.1 mV
TEMP 0.1 qC
ION 1, 0.1, 0.01, 0.001 ppm(mg/l)
pH ±0.01 pH/±0.005 pH(±1Digit)
ORP ±0.05 %(±1Digit)
Accuracy
TEMP ±0.2 qC(±1Digit)
ION ±0.5 %(±1Digit)
Auto-Read(HOLD) Yes
Temperature Automatic with PT1000/NTC30K, auto recognition
Compensation Manual
pH: Tech./ NIST/ ANY/ Define Buffer mode
Calibration ION: Ion concentration calibration (SP-2500 only)
Up to 5-points calibration
Rel. ORP Relative potential adjustable range: ±300 mV
GLP Calibration
Timer or Counter selectable, range: 0~9999 times or hours
Timer/Counter
One way transmission: To the computer/ printer (ASCII)
RS232 Interface
Two way transmission: Modbus (RTU or ASCII)
500 data sets with time and date stamp
Data Storage
Continuously auto data storage & logging /Manual
Auto Power-off Yes, On/Off(Programmable time duration for auto power-off)
Ambient 0~50qC
Temperature
Storage -20~70qC
Temperature
Impedance Input Њ1012
Display LCD Display with backlight
Power Consumption Max. 1W
Power Supply 4 x AA Batteries or AC/DC 6V adaptor
Certification CE
Dimension 220x190x70mm(LxWxH)
Weight 0.7Kg
Note: The specifications and appearance of the instrument are subject to change without
notice.
1
2. Panel Description
2.1 Front Panel
2.2 Sockets
2
2.3 Display
Setting Measuring
Mode Mode
Unit
Reading
Display
Mode
Auto Temp.
Auto Read
Compensation
Calibration
Time/Date
Mode
Data Storage
Baud Rate
Mode
3
2.4 Keypad
UP
Increase values / Scroll upwards or leftwards.
DOWN
Decrease values / Scroll downwards or rightwards.
4
3. Operation
3.1 Measurement
Press POWER key to turn on the instrument and it will directly enter the last
measurement mode to start measurement. Press POWER key for a while when
the power is already on, then the display will show the model type and software
version. The user may set up auto turn-off timer. Users may select to switch on the
auto power-off function (with programmable timer) ,or to switch off the function.
3.1.1 Mode
Press MODE key to switch to pH, ORP, ION(for SP-2500 only)
measuring mode. (ION mode has 2 units: ppm and mg/l for selection.)
Press ENTER key +MODE key to switch on the decimal of resolution.
3.1.2 Temperature compensation
1. ATCΚAutomatically recognition of temperature probe NTC30K or
PT-1K and auto temperature measurement and compensation.
Under setting mode, the temperature can be adjusted ±5C for
temperature correction.
2. MTCΚEntering into manual temperature compensation mode when there
is no ATC probe plugged in. Press upward or downward key to
modify the temperature value. Press upward and downward key
simultaneously to restore default value 25C.
3.1.3 Auto Read Drift Control
Under measurement mode, press AUTO READ key to hold the present
reading(HOLD), and press ENTER key to confirm the Auto-Read function
and to activate new measurement. Wait until the measurement is stable, the
instrument hold the value automatically(HOLD) to finish the procedure. To
cancel the hold value, press AUTO READ key or MODE key to relieve the
Auto-Read hold value.
5
3.2 Block diagram of parameter settings
ʳ
Enter Parameter
Setting mode
RTU o Year
ASCII Glp.T Glp.H setting Set
AUTO OFF AUTO Temp. Buffer_1~5
OFF Counter Timer measure-
(On) (Off) (On) Setting Setting
Setting Setting ment
average
Times
Date
Parity
Setting
Preset:
Auto Timer Press
Setting RECALL
Key
Time
Baud rate
setting
Preset:
Auto
Κ Upward and
Downward key
Κ Enter key
Note: Under any setup mode, press MODE to back to measurement mode at any time.
(Except Buffer_1~5 Settings)
6
3.3 Parameter settings
3.3.1 Entering setting of parameter
While the instrument’s power is off, press MODE key and hold the
pressing continuously, and press POWER key until the display shows
model of the instrument. Release the POWER key and wait until the menu
display enter into parameter settings mode, and then release MODE key.
Press upward or downward key to select setting menu. To exit the parameter
settings mode, press MODE key to back to measurement mode.
7
3.3.3 RS-232 communication settings
Users may according to their communication needs with following table
to set transfer mode, (ASCII, RTU), parity (non, odd, even) and transmission
baud rate (1200, 2400, 4800, 9600).
ʳ
1. Communication setting format
8
2. Communication setting procedure
Press ENTER
key to enter
9
3.3.4 Calibration cycle settings(GLP calibration interval)
Users can set their own calibration cycle counter or timer.
1. Calibration Counter: Under pH measurement mode, press AUTO READ
key to activate the auto drift control measurement function.
Each press of ENTER key represent that one time of
measurement work has been done. After reaching the setup
times for counter, the instrument makes reminder.
2. Calibration Timer: After how many hours from last calibration, the
instrument makes reminder.
If it exceeds the set times or hours, under pH measurement mode the
symbol in the display continuously twinkles. The twinkling symbol will
disappear until the next execution of pH calibration
When the value twinkles, press When the value twinkles, press
upward or downward key to set upward or downward key to set
calibration counter from 0~9999 calibration time from 0~9999 hours.
times. If the value is set 0, it If the value is set 0, it represents the
represents the GLP calibration GLP calibration timer has been
counter has been turned off. turned off.
10
3.3.5 System time settings
Users may set the year, month, date, hour, and minute. When replacing the
batteries, it is necessary to enter to the setting to update the system time.
11
3.3.6 Digital Filter settings (Sample average of measurements)
Enter the setup of Digital filter. You may select the number of sample to be
averaged each time to become a reading which is gradually counted in order to
increase the stability of measurement.
12
3.3.7 Auto power-off settings
Enter the setup of auto power-off. Users may setup whether to activate
the auto power-off function, and there is a programmable timer for setting.
The auto power-off timer setting range is from 10 minutes minimum to 23
hours and 59 minutes maximum.
Note: Preset---OFF
Press ENTER
key to enter
13
3.3.8 Auto temperature compensation correction settings
Enter auto temperature compensation settings. If the ATC probe is
connected, it is allowed to correct the temperature value by pressing upward
or downward key of ̈́5̓C. Or press upward and downward key
simultaneously to zero the temperature modification value.
Note: If not ATC mode, it can not enter into auto temperature
compensation correction settings.
Press ENTER
key to enter
14
3.3.9Defien cal. table setting (Self-definition pH/Temp. table--CD mode )
Define mode has pre-set 5 buffer solution pH/Temperature(Range: 5~50̓C) table.
Users may modify the data sheet according to the buffer solutions set which they use.
The table can be modified and saved in the memory of the transmitter.
15
3.4 Auto/Manual Data Storage
Under data storage mode, users may store pH, ORP and ION(SP-2500 only)
measurement with No. and ID two kinds of classification. The “No.” represents
the order of storage sequence. When data is stored to the 500th data, the display
will shows “Full” to represent there is no more space for data logger memory.
While ID number 1~500 is for grouping the samples which the user requires. The
Auto data storage can be set according to the time interval setting, the minimum
interval is 5 seconds. If turn on the Data Rewritable Function, when the data
memory is full the data logger will overwrite the new data.
3.4.1 Auto data storage
Under measurement mode, press and hold ENTER key and press STORE
key simultaneously to enter auto storage settings.
When auto storage is not activated, press MODE key to exit the menu.
16
3.4.2 Manual data storage 3.4.3 Overflow of data storage
Under measurement mode, When the all the memory is
press STORE key to enter occupied and the data can not be
manual data storage mode. Press stored any more, the display
MODE key to exit at any time. twinkles the text for reminder for 5
seconds and back to the
measurement mode.
Press ENTER
key to enter
Users may delete all of the data
according to the ch 3.6
instruction.(When auto rewritable
function is turned on, there is no
this data full display reminder.)
17
3.5 Data transmitting and display
Under measurement mode, press ENTER key to manually transmit the real-time
measurement value by RS-232 interface.
Note: The output of the instrument is non-insulated signal. It may impact the
transmitting measurement value if the instrument connects with other
earth-related device.
3.5.1 Time interval auto transmitting 3.5.2 Data display & manual transmitting
(Transmit the real-time measurement to a Under measurement mode, press
computer or a printer through RS-232) RECALL key to roll up the data
Under measurement mode, press and hold display & manual transmitting menu.
ENTER key and then press RECALL key There are four kinds of operation mode.
to enter auto transmitting menu display. Press ENTER key to enter the menu.
After finishing setting, the data is 1.Display the stored data
transmitted through RS-232 interface.
18
2. Display the last calibration data
(1)Under pH measurement mode,
press RECALL key to show the
last pH calibration data in display.
(ex: 3-Point calibration)
Press ENTER
key to display the
Press ENTER mV value of Buffer 3.
key to display the
mV value of Buffer 1.
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳ
Press ENTER
key to display the
Press ENTER key to Slope value.
enter. The display shows
Buffer
ʳ 2 calibration data.
If no data, ignores the
procedure and display the
Slope value.
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳ
Press ENTER
key to display the
SENSITIVITY
ʳ value.
Press ENTER
key to display the
ʳ ʳ ʳ ʳvalue
mV ʳ ʳ ʳ ʳ ʳofʳ ʳBuffer
ʳ ʳ ʳ ʳ ʳ 2.
ʳ
19
ʳ
ʳ
ʳ
ʳ
ʳ
Press ENTER ʳ
key to display the Press ENTER key
ʳASYMMETRY
ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ value.
ʳʳʳʳʳʳʳʳ
ʳ
Back to measurement mode
ʳ
ʳ
(2) Under ORP measurement mode,
press
ʳ ʳ RECALL key to show the
last relative potential adjusted data
Press ENTER ʳʳʳʳ
in display.
ʳ key to display the
R2
ʳ ʳ ʳvalue.
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳ
ʳ
ʳ
ʳ
ʳ
ʳ Press ENTER key to display
Press
ʳ ʳ ʳ ʳ ʳENTER
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳ relative potential .
key to display the
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳ
cal. data storage year.
ʳ
ʳ
ʳ
ʳ
ʳ
Press
ʳ ʳ ʳ ʳ ʳ ENTER
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳ
key to display the Press ENTER key
ʳ data storage date.
cal.
ʳ Back to measurement mode
ʳ
ʳ
ʳ
ʳ
ʳ
Press ENTER
ʳkey to display the
cal. data storage time.
20
(2) Under ION measurement mode, press
RECALL key to show the last ISE
concentration calibration data in display.
(ex: 3-Point calibration)(SP-2500 only)
Press ENTER
Press ENTER key to key to display the
enter. The display shows Slope value.
Buffer 2 calibration data.
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳ
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳ
Press ENTER
key to display the
Press ENTER
SENSITIVITY value.
key to display the
mV value of Buffer 2.
21
ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ 3. Manual stored data transmitting
(1) Transmit all the stored data
Press ENTER
ʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳʳ
key to display the Press ENTER key
ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳR2 value.
ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ Transmission
ʳʳʳʳʳ completed
Back to measurement mode
Press
ʳ ʳ ʳ ʳ ʳENTER
key to display the
ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳcal.
ʳ ʳ ʳ data
ʳ ʳ ʳ storage date.
Press ENTER
ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ ʳ key to display the
cal. data storage time.
22
4. Calibration data transmitting 3.6 Delete all of the data
(1) Transmit the stored cal. data Under power off status, press &
hold STORE key and then
Through RS-232 interface
press & hold POWER key until
the display shows the model of
instrument. Release POWER
key. While the menu display
shows data clean text, release
STORE key.
Transmission completed
Press ENTER key to confirm
Back to measurement mode to delete all the data.
To abandon the deletion, please
press MODE key.
SP-2500 pH mode
23
4. Calibration
Under measurement mode, press CAL key to enter calibration mode, and press
MODE key to go back to measurement mode.
4.1 pH Calibration
The instrument provides multi-point standard buffer solution calibration. You may
decide how many points to calibrate the measurement system.(up to 5-point) The
principle is according to “Method of Least Squares”. Apply linear regression to
calibration the electrode’s slope and zero point (Asy, Offset or Zero point).
When calibrating a electrode, you may calibrate 1 to 5 point by any sequence to
provide linear regression for mV and pH multi-calibration of a electrode, and to show
the electrode’s slope and zero point(Asy, offset or Zero point) at 25C. The electrode’s
slope rate which is actual slope divided by theoretical slope and the sensitivity shows
in percentage in the display. In addition, the display shows the linear regression
determination coefficient, R2, of the electrode and buffer solution to provide you an
estimation of an electrode’s regression suitability. According to different combination
of standard buffers, the TECH, NIST, Any buffer solution calibration modes are
provided.
24
to theoretic slope and the temperature of standard solutions, the display shows a
approximate pH value. Then, you can calibrate the electrode by freely adjust the pH
value as those of the standard solutions’. There is not a zero point range failure
determination by the instrument but only the slope range determination. If the slope
is over the range, the display shows error message of slope failure.
You can calibrate the electrode by one point or up to three points of standard
solutions by any sequence. As different calibration point method is applied, the
definition of the zero point and slope different.
25
4.2 operation of pH calibration
26
4.3.3 After entering preset Buffer 1 menu display,
press ENTER or wait for 3 seconds to enter the
Buffer 2 calibration menu display.
27
4.3.7 After entering into Buffer 2 menu display, press
MODE key to leave the calibration menu to
finish it as a dual point calibration. The menu
display shows slope value; for multi points
calibration, clean the pH electrode with distilled
water, put the electrode into third buffer solution.
Press ENTER key to start to read the preset
Buffer 3 value for continuing calibration.
28
4.4 Any Buffer manual calibration (CA)
4.4.1 After entering calibration mode, clean the pH
electrode with distilled water, put the electrode
into first buffer solution. Press CAL key to
select CA1. If temperature mode is set as MTC
(Manual), the temperature value starts twinkling.
Press upward or downward key to adjust the
temperature value. Or press upward and
downward key simultaneously to back to the
preset value--25̓C. Press ENTER key to start to
read the preset Buffer 1 value.
29
4.4.5 When reading the value, the “Auto Read”
symbol in the display starts to twinkle. Wait
until the value is stable or directly press
ENTER key to read the present value, then the
menu enter into manual calibration for Buffer 2.
30
4.5 Define Buffers calibration (CD)
4.5.1 After entering calibration mode, clean the pH
electrode with distilled water, put the electrode
into first buffer solution. Press CAL key to select
CD1.. Press ENTER key to start to read the
user-tailored method Buffer 1 value.
4.5.2 After entering into define calibration menu
display, the buffer text in the display starts to
twinkle. Press upward or downward key to select
the user-tailored Buffer 1 value. Press ENTER
key to enter into temperature value setting menu
display.
4.5.3 Under temperature setting menu display(the
temperature twinkles), press upward or downward
key to adjust the temperature value. Or press
upward and downward key simultaneously to
back to the preset value--25̓C. Press ENTER
key(if as ATC mode) to start to read the present
value.
4.5.4 When reading the value, the “Auto Read” symbol
in the display starts to twinkle. Wait until the
value is stable or directly press ENTER key to
read the present value.
4.5.5 After entering into define calibration of Buffer 1
menu display, press ENTER key or wait for 3
seconds to enter into CD2 calibration menu
display.
4.5.6 Under CD2 calibration menu display, if press
MODE key to leave the calibration menu to
finish it as a single point calibration. The menu
display shows slope value; for multi-point
calibration, clean the pH electrode with distilled
water, put the electrode into second buffer
solution and press ENTER key to enter
user-tailored calibration value menu display.
4.5.7 After entering into define calibration menu
display, the buffer text in the display starts to
31
twinkle. Press upward or downward key to select
the user-tailored Buffer 2 value. Press ENTER
key to enter into temperature value setting menu
display.
4.5.8 Under temperature setting menu display(the
temperature twinkles), press upward or downward
key to adjust the temperature value. Or press
upward and downward key simultaneously to
back to the preset value--25C. Press ENTER
key(if as ATC mode) to start to read the present
value.
4.5.9 When reading the value, the “Auto Read” symbol
in the display starts to twinkle. Press ENTER key
to read the present value.
4.5.10 After entering into define calibration of Buffer 2
menu display, press ENTER key or wait for 3
seconds to enter into CD3 calibration menu
display.
4.5.11 Under CD3 calibration menu display, if press
MODE key to leave the calibration menu to
finish it as a dual point calibration. The menu
display shows slope value; for multi-point
calibration, clean the pH electrode with distilled
water, put the electrode into third buffer solution
and continue the calibration procedures.
4.5.12 After finishing whether single, dual to five points
calibration, press ENTER or wait for 3 seconds
to show the slope value, the SENSITIVITY value,
the ASYMMETRY value, the R2 value. Then
after 3 seconds or press ENTER key to go back
to measurement mode.
32
4.6 ORP relative potential adjustment!
!! Under pH measurement mode, press MODE key to
switch to the mV measurement mode. Press CAL key
to enter relative potential adjustment mode. Press
MODE key at any time to back to measurement mode.
ʳʳʳ
ʳ
ʳ
4.6.1 Clean the ORP electrode with distilled water,
put the electrode into ORP standard solution,
and press CAL key enter into ORP relative
potential adjustment.
33
4.7 ION concentration calibration (SP-2500 only)
The instrument applies the easiest and widely used ion-selective electrode
direct potentiometry—ISE, to measure the potential reaction of the solution.
Establishing the relationship of ion concentration(activity) and electrode potential
by calibration, the instrument then is able to start measurement. The measurement
and calibration of electrode is necessary to refer to the operation manual of ION
selective electrodes(ISE).
ʳʳʳ
ʳ ʳ The method of calibration standard solution usually applies continuous
dilution from high concentration standard solution in sequence to get 1000, 100,
10, 1 ppm(mg/l). In order to prevent from the difference of ISE activity and actual
concentration, it is usually necessary to add ISAB (Ionic Strength Adjustment
Buffer) when calibration for making the sample solution has similar ionic
strength.
ʳʳʳʳ
ʳ ʳ It is recommended to use the calibration standard solution from low to high
to prevent contamination of standard solution. If the concentration range of
sample solution is known, it should be applied the nearest value of standard
solution for calibration. If the sample measurement range and the standard
solution calibration range have been confirmed to be in the linear range of the
electrode, it is acceptable to make dual points calibration. However, making three
of more points calibration can help to confirm whether the measurement is within
the linear range or not. ʳ
ʳʳʳ
ʳ ʳ The calibration is up to 5 points calibration, and the instrument provides
“log(A) = the logarithm of the activity of the measured ion” of linear regression
calculation for the electrode potential(mV) and ion concentration(activity). It
measures and displays the electrode’s slope under 25̓C and the ratio of electrode
actual slope with theoretical slope. It also displays the percentage of electrode
sensitivity for judgment whether electrode is aged or contaminated. It also
displays the linear regression R2 value (determination coefficient) of electrode
and standard solution as the judgment of electrode regression suitability. ʳ
ʳʳʳʳ
ʳ ʳ ʳ ʳ ʳ Because the calibration slope is related the temperature, the
measurement is compensated with temperature value. However, it is
better to measure the standard solution and sample solution within ±2˚C
temperature difference.
34
4.8 ION concentration calibration (CC) (SP-2500 only)!
!!!!!!For concentration calibration(CC) (up to 5 points calibration), select ppm or
mg/l unit under measurement mode. Press CAL key to enter into ION
concentration calibration mode. The instrument has built-in 10 sets selection of
different standard solution value from:
1.002.005.0010.0020.050.0100.02005001000. The
minimum is 2 points calibration and up to 5 points calibration. Users may press
MODE key at any time to finish the calibration and back to measurement
mode.
ʳ
4.8.1 Press CAL key to select CC1. If temperature
mode is set as MTC (Manual), the temperature
value starts twinkling. Press upward or
downward key to adjust the temperature value.
Or press upward and downward key
simultaneously to back to the preset value--25̓C.
Press ENTER key to start to read the preset
standard solution No.1 value.
35
4.8.6 Under standard solution No.2 menu display. The
concentration value starts twinkles, press CAL
key to select concentration value, press upward or
downward key to adjust it to the required value.
Press ENTER key to read and to display the
standard solution No.2’s mV value.
36
5. Error messages
37
6. Maintenance
c. Put into the new AA batteries, and close the battery cover.
The cleaning cycle for the electrode depends on the pollution degree of the
measurement sample. Normally, it is recommended to make weekly cleaning. The
following chart gives introductions of different cleaning methods according to
different type of contaminations to provide the operators with reference for
cleaning and maintenance.
Acid and alkaline soluble Rinsing the electrode with 0.1mol/l NaOH or 0.1mol/l
contaminations HCl for a few minutes.
Apply clean water to flash the electrode after above cleaning steps and immerse the
electrode in 3M KCl solution for 15 minutes at least, and then calibrate the electrode.
The electrode should only be rinsed and never rubbed or mechanically cleaned, since this
would lead to electrostatic charges. This could cause an increase in the response time.
In cleaning the platinum electrode, the platinum ring of the electrode can be rubbed
gently with a wet soft piece of cloth.
ϡ The frequency of electrode cleaning depends on the type and degree of
contamination. However it is recommended that the electrode be cleaned once a
week.
38
7. Modbus protocol and instructions
39
7.2 MODBUS name and address table
40
8. Appendix
Table 1
CT Mode Tech. Buffers
TEMPк Buffer 4.01 Buffer 7 Buffer 10
5 3.999 7.087 10.241
10 3.998 7.053 10.155
15 3.999 7.031 10.116
20 4.002 7.011 10.047
25 4.006 6.996 9.998
30 4.011 6.985 9.952
35 4.018 6.976 9.925
40 4.031 6.971 9.874
45 4.047 6.969 9.843
50 4.055 6.969 9.810
Table 2
CN Mode NIST. Buffers(DIN 19266)
TEMPк Buffer 1.68 Buffer 4.01 Buffer 6.86 Buffer 9.18 Buffer 12.45
5 1.668 4.004 6.951 9.395 13.207
10 1.670 4.000 6.923 9.332 13.003
15 1.672 3.999 6.900 9.276 12.810
20 1.675 4.001 6.881 9.225 12.627
25 1.679 4.006 6.865 9.180 12.454
30 1.683 4.012 6.853 9.139 12.289
35 1.688 4.021 6.844 9.102 12.133
40 1.694 4.031 6.838 9.068 11.984
45 1.700 4.043 6.834 9.038 11.410
50 1.707 4.057 6.833 9.011 11.705
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Table 3
CD Mode Define standard buffers table
TEMPк Buffer 1 Buffer 2 Buffer 3 Buffer 4 Buffer 5
5 2.010 4.040 7.070 9.160 12.410
10 2.010 4.020 7.050 9.110 12.260
15 2.000 4.010 7.020 9.050 12.100
20 2.000 4.000 7.000 9.000 12.000
25 2.000 4.010 6.980 8.950 11.880
30 2.000 4.010 6.980 8.910 11.720
35 2.000 4.010 6.960 8.880 11.670
40 2.000 4.010 6.950 8.850 11.540
45 2.000 4.010 6.950 8.820 11.440
50 2.000 4.000 6.950 8.790 11.330
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