Beruflich Dokumente
Kultur Dokumente
1.3 REQUIREMENTS 1
1.4 EXEMPTIONS 1
4.0 DEFENITIONS 3
6.0 RESPONSIBILITIES 4
7.0 PERSONNEL QUALIFICATIONS 4
8.0 METHODS 5
9.0 SURFACE PREPARATIONS 6
11.0 PROCEDURES 8
15.0 INSPECTION 12
16.0 RECORDS & REPORTING 12
ATTACHMENTS
1 Scope
1.1 This procedure describes the method and procedure to be implemented by NDT
& CCS for Positive Material Identification (PMI) to verify the chemical
composition of Piping components (including pipe, fittings etc.), components of
pressured equipment and weldments which are manufactured from alloy steels,
stainless steels or non ferrous alloys (here in after referred to as alloys).
1.3 Requirements
1.3.1 The requirements in this standard shall apply to both new and repair or
replacement alloy (see exceptions in paragraph 1.4 regarding carbon steel)
components. The requirements apply to shop, field fabrication and plant.
1.3.2 The testing methods outlined in this procedure are not intended to establish the
complete conformance of a material to its specification.
1.3.3 PMI testing shall be performed at a point in time that ensures proper alloy
materials have been used in the fabrication of an identifiable assembly. Usually
this is during t fabrication or immediately prior to fabrication. Although
manufacturing quality control is an important issue , testing performed by the
manufacturer or supplier of raw material or loose components is not considered
for PMI testing.
1.3.4 Retroactive PMI Testing of existing systems and stocked materials shall be
performed upon the recommendation by the consulting services department or
by the decision of the plant manager.
1.4 Exemptions
1.4.1 Unless specifically required in the purchase order or SAMS catalog description or
SAMSS, the following components and materials are exempt from PMI:
Exceptions:
3) Rotating equipment internals and associated seal, lube oil, cooling water and
steam equipment and piping.
4) Valve internals(Trim)
5) Piping components in ASME B 31.3 category D service or equivalent
6) All instrumentation provided with isolation valves.
Commentary Note: Examples of non pressure components could include, but not
limited to, column trays, valve internals, internal attachment welds and certain load-
bearing supports.
2.0 OBJECTIVE
Objective of this procedure is to ensure that alloy (i.e, non-carbon steel) & carbon
steel (under certain conditions) bulk materials and weldments used in the
performance of work are as specified in the project specification.
3.0 References
3.1 SAES- A-206 Positive Material Identification
3.2 00-SAIP-07 Positive Material Identification Requirements
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 3 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
4.1 Alloy Material: Any metal (including filler metals for welding alloy materials)
containing alloying elements such as chromium, nickel, or molybdenum, that are
intentionally added to enhance mechanical or physical properties and/or
corrosion resistance. Does not include high-strength low-alloy (micro alloyed)
steels and impact-tested carbon steels.
4.2 PMI: Positive Material Identification – Verification that the nominal chemical
composition of an alloy material is as specified and ordered. The term applies to
programs, processes, procedures, and tests in accordance with this standard.
4.3 PMI Testing: Any physical evaluation or test of a material, meeting the
requirements of this standard, to confirm that the material which has been or will
be placed into service is consistent with the selected or specified alloy material.
4.4 Material Specifications: ASME Section II, Parts A, B and C, or the relevant
ASTM, or any other material specification required.
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 4 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
4.5 Non-Pressure Components: Items that are not part of the pressure-
containing envelops, and therefore, do not affect pressure retaining capacity of
piping
4.6 Pressure Product Components and Parts: Product forms used for the
fabrication f pressured piping, including but not limited to: forgings, flanges, pipe
and fittings such as tees, elbows, reducers, and special pipe components, valves
(body and bonnets), and alloy welds joining pressure parts to non-pressure parts.
4.7 Pressure Piping: Piping whose design pressure is 100 Kpa (15 Psig) and
above.
5.1 Any conflicts between this standard and other applicable Saudi Aramco
Engineering Standard (SAESs), Materials System Specifications (SAMSSs),
Standard Drawings (SASDs), or industry standard, codes and forms shall be
resolved in writing by the Company or Buyer Representative through the
Manager, Consulting Services Department of Saudi Aramco, Dhahran.
5.2 Direct all request to deviate from this standard in writing to the Company or
Buyer Representative, who shall follow internal company procedure SAEP-302
and forward such requests
6.0 Responsibilities
6.1 For all new projects, Project Management or their designated representatives
shall be responsible for ensuring that proper PMI Programs and procedures are
developed and PMI testing is performed by the equipment manufacturer or the
fabricator, as applicable prior to equipment installation and start-up. Project
management is normally supported by Project Inspection and Vendor inspection.
6.2 For existing facilities, the plant manager or his designated representative, e.g.
Inspection, shall be responsible for ensuring that a PMI Program is developed
and implemented based on 00-SAIp-07
7.1 Personnel performing PMI shall have a minimum training of two days with 16 hours
in understanding of the operation & application of the PMI equipment and the underlying
the principles. The training can be performed by the equipment manufacture or an
individual trained by NDT & CCS using training program outlines by the equipment
manufacturer including theory and practical. The training certificate shall be submitted to
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 5 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
the customer for their approval one week prior to start of job. Valid calibration
certificates for equipment and calibration blocks shall be available from company / 3 rd
party.
7.2 Prior to commencing PMI testing, instrument operators shall be qualified to operate
approved equipment on a representative sample of the alloy materials with 100%
correct assessment as the performance criteria. The instrument operator shall work to
a written procedure and shall have been trained to use the instrument in accordance
with that procedure. Training shall be documented.
7.3 If sample removal is used, a written procedure for identification and traceability to
original material is required.
8.0 Methods
8.1 The primary acceptable method is X-ray emission analysis, also known as X-ray
fluorescence (XRF) analysis with a calibrated portable instrument such as INNOV – X
Systems, Alpha Series.
8.2 Standard calibration blocks have been provided with the equipment. Every time the
machine is switched on the equipment calibration verification shall be carried out using
standard alloy samples that are representative of the material to be tested, prior to first
reading being taken and whenever there is a significant change of the material to be
tested.
8.4 The date of the latest calibration of the instrument shall be stated in the PMI
report. (qf 091-20)
8.5 Because of inherent limitations of XRF, it is not possible to detect all elements.
Elements lighter than sulfur (S) cannot be detected using portable X-ray fluorescence
spectrometers. Therefore, this technique cannot be used to detect carbon (C).
8.6 An optical emission spectrograph shall be used to check for all the required
elements, including carbon. Spectrotest , TXC- 02/TXC- 03/TXC- 25 ,Bruker Q4 Mobile
Arc/Spark alloy analyzer shall be used for this purpose.
8.7 The person(s) performing PMI testing shall calibrate and/or verify the test equipment
performance as specified by the equipment manufacturer. Calibration shall be carried
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 6 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
PMI testing of welds shall be done after removal of slag and/or oxide from the weld
surface. The surface of material to be analyzed shall be clean and free from paint, rust
and debris. Generally a fresh 60 grit finish is required for the Arc Spark type instrument
and the clean bare metal surface required for XRF INNOV-X system equipments. For
Arc/Spark instrument, the small arc burn created by the analysis technique shall be
removed by lightly abrading the surface after test.
10.2 PMI testing of weld material shall be performed in the same manner as for the
adjacent base metal.
10.4 The elements of the basic alloy materials to be verified shall be in accordance
with Table 1.
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 7 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
TABLE - 1
11.0 Procedures
11.1 PMI when specified shall be performed any time prior to, during fabrication for
pressure components and that alloy verification of welds and for field assembled items
not previously PMI tested, is completed prior to shipment to ensure proper materials
have been used in the fabrication of an assembly.
11.2 Weld metal PMI shall be performed prior to any PWHT, radiography or other NDE
and or surface coating.
11.3 Weld metal PMI will be performed on the final deposited pass.
11.4 Saudi Aramco Inspector shall have the option to witness any or all the PMI testing
11.5 Material test reports will not be considered as an acceptable positive material
identification and alloy verification shall not be considered as a substitute for the
required materials test reports.
12 Acceptance Criteria
12.1 For acceptance, it must be demonstrated that materials contain the amounts of
alloying elements shown in the material specification. Alloys shall be acceptable if the
alloying elements are each within 10% of the specified range of values.
12.2 Welds with consumables that match, or nearly match, the base metal
composition shall be within ±12.5% of the ranges allowed in ASME Section II C for each
element.
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 9 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
12.3 For weld overlays, the chemistry on the surface of overlays shall be in
accordance with SAES W -014
12.4 For dissimilar metal alloy welds (other than weld overlays), the effect of dilution
from the different base metals and the filler metal shall be taken in to account for
determining the nominal as-deposited weld metal composition.
13. 1 If the PMI testing results fall outside the acceptable range using, the Equipment
Manufacturer or the Fabricator, as applicable, has the option to conduct a more
accurate analysis at his own expense to determine the component acceptance such as
obtaining a chemical analysis performed by an independent testing laboratory. The
alternative test method or independent laboratory must be acceptable to the Saudi
Aramco Inspector. The results of the more accurate test method or independent
chemical analysis shall govern.
13.2 If any component or weld is found unacceptable, it shall be replaced and the
replacement shall be alloy verified in accordance with this standard.
13.3 Procedures shall be in place to ensure that rejected components are segregated
and properly identified to prevent reuse.
13.4 If one of the tubes for heat exchangers and boilers is found unacceptable, all
remaining tubes of the particular alloy shall be tested for the individual equipment. This
also applies to the weld metal.
13.5 All rejected tubes shall be replaced and 100% of the replacement tubes shall be
PMI-tested in accordance with this standard.
14.1.1 Paint marking shall be done with water-insoluble material that contains no
substances that harmfully affect the metal at ambient or elevated temperatures. In
particular, the marking material shall be free of lead, sulfur, zinc, cadmium, mercury,
chlorine, or other halogens.
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 10 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
14.1.2 All components, and welds that are found unacceptable, shall be marked
immediately with a circled red "X".
14.1.3 All verified materials with an acceptable analysis shall be marked with the letters
"P" using a certified low-stress stamp or otherwise directed by Project Inspection.
Marking shall be adjacent to the manufacturer’s marking .The marking shall be placed
as follows: (Refer Attachment-III)
14.1.4 When heat treating is performed after PMI, the identification marking must be
recognizable after heat treatment. PMI markings shall be transferred when a plate or
pipe is cut.
14.2.1The principal purpose of color coding is visual identification during storage and
after the components have been cut for fabrication.
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 11 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
14.2.2 Color coding is not a substitute for PMI Testing or other, permanent
manufacturer’s markings required by ASTM or other specifications. Permanent
manufacturers markings shall not be obscured by color coding.
14.2.3 Color coding may be done by the material manufacturer or the material supplier.
Color coding need not be retained after painting.
14.2.4 Prior to coding, surfaces shall be clean and free of dirt, loose scale and oil.
Paints used for coding shall be durable, bright and distinctive and shall not contain
substances that would harmfully affect the material at ambient or elevated
temperatures. Particularly paint shall be free of lead, sulfur, zinc, cadmium, mercury,
chlorine and other halogens.
14.2.5 Each component shall be coded in accordance with PFI-ES-22 and attachment 3
of 00-SAIP-07, and shall have painted characters indicating the specification number of
the material if it is not permanently marked or tagged according to the applicable
material specification
14.2.6 Valves, flanges and fittings do not require color coding if these components are
permanently stamped or tagged by the manufacturer. If the materials are not easily
legible, valves, flanges and fittings shall be coded with a stripe of 5 mm minimum width.
The color coding on the valves should indicate the valve body material.
14.2.7. ASTM A 193, Grade B7 stud bolts do not require color coding if the grade of the
material is stamped on one end of each bolt.
14.2.8 Spiral wound gaskets shall be color coded in accordance with ASME B 16.20.
Sheet type gaskets do not require color coding.
14.2.9 Pipe & Fittings: each length of pipe and firings shall have 5 mm or larger stripe
running full length. One inch NPS and smaller may have a 3 mm stripe running full
length.
14.2.10 Valves: When required, stripe across the body from flange to flange or end to
end.
14.2.12. Bolting: When required stripe around the mid point of each bolt or stud.
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 12 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
14.2.13 Plate, sheet, and strip: stripe on surface near two perpendicular edges for entire
length.
15.0 Inspection
15.1The concerned contractor shall ensure and verify that alloy materials have been
verified by PMI testing as required.
15.2 During repairs or alterations of materials required to be PMI tested, the responsible
contractor shall verify the correct compositions of the shop & field welds.
16.1.2 The log shall identify each component and weld corresponding to an
individual equipment item or piping spool and shall include the equipment or
spool number and purchase order number.
16.1.3 The log shall identify all components and welds that have been alloy
verified and the results of testing.
16.1.4 Test results shall include measured percentages of alloying elements for
components that were accepted or rejected.
16.1.5 The Equipment Manufacturer shall prepare a detailed PMI map of the
pressured equipment being fabricated. The map shall show the alloy material
specification of each alloy component and the extent of PMI required in
accordance with this standard.
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 13 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
16.2.1 At least two weeks prior to the commencement of fabrication, the field
Fabricator shall establish and present to the Saudi Aramco Inspector for review
the proposed testing, logging, identification, and final installation procedures for
all components requiring PMI testing onsite (such as fabricated pressured
equipment, piping, valves, and welds).
16.2.3 The field Fabricator shall prepare a detailed PMI map of the pressured
equipment being fabricated. The map shall show the alloy material specification
of each alloy component and the extent of PMI required in accordance with this
standard.
16.3.2 The PMI Report form (Attachment-I) shall be completely filled out by the
assigned inspector/technician for each PMI analysis.
16.3.3 A log shall be maintained (as per form Attachment-II) to identify each
component that has been alloy verified and the results.
16.3.4 The PMI Testing Report shall be reviewed by the Saudi Aramco Inspector
prior to final acceptance.
16.4 Attachments.
Attachment I): PMI Report Form
Attachment II): Positive Material Identification Log Sheet
Attachment III): Color Code for Material Identification
Attachment-IV): PMI Procedure Flow Chart
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 14 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
Item Type: (weld, valve, pipe, Item Description: ( Manufacturer & Heat #)
etc.)
This is to certify that the above materials verification is done accordance with the requirement of
SAES-A206 and the above alloying element percentages were evaluated in accordance with the
criteria stated in the above-mentioned standard and this SAIP procedure. The items above were
also color coded/marked in accordance with above tow documents.
Note: Any product manufactured by welding shall have an additional white stripe. Any additional alloy material not
included in this table or PFI ES-22 shall be referred to the Operation Inspection Division of the Inspection
Department for obtaining a color Code.
NDT & Corrosion Control Services
Examination Procedure
Document # NDT/PMI/06 Rev-05
Page 17 of 17
Approved By: Sr.Operations Manager
Date-29th July-2012
Title: POSITIVE MATERIAL IDENTIFICATION (PMI) PROCEDURE
Attachment IV
Request by Originator
Identify item for PMI completely filling out top
Section of Form on Attachment # I
Fail
PMI Test Mark Item Circled
Result red “X”
No Fail