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Lightweight Aggregate Concrete Blended with Rice Husk Ash and Para Rubber
Wood Fly Ash
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KEY WORDS: Lightweight concrete / Rice husk ash / Para rubber wood fly ash / Pumice aggregate
1. INTRODUCTION and also the lumber and other waste is used in the
Rice husk is by product of rice mill around the biomass power plant, rubber glove factories and
world, particulary in Asean Economic Community seafood factories. Rubberwood is become ash about
(AEC) countries and China. In Thailand, each the 25% which collected at the bottom of the boiler and
annual output in 2003 Year from 29.474 to 36.175 the remaining 75% is blown out efflux as fly ash is
million tons in 2012 Year [1]. Nowaday, benefication called Para rubber wood fly ash (PRWFA) and
of rice husk is used as an energy source for biomass extracted by electrostatic precipitators and filler bags.
power plants and rice mills. After burning, rice husk Pumice aggregate (PA) can be found largely in
ash (RHA) with approximately one-fifth of the Lopburi province, Thailand. Moreover, neighbour
original weight is obtained as a by-product. RHA contries such as Phillippines and Indonesia are
contains over 80% of silica and small amounts of important exported it. It is glass volcanic rock and
impurities such as K2O, Na2O and Fe2O3 [2]. The chatacterised light and plain porosity [6].
RHA has been used as a highly reactive pozzolanic Development of non-expensive and environmentally
material to improve the microstructure of the friendly PA concrete (PAC) with acceptable strength
interfacial transition zone between the cement paste and durability characteristics can be extremely
and the aggregate in high-performance concrete. helpful for the sustainable construction and
Mechanical experiments of RHA blended Portland rehabilitation of volcanic disaster areas around the
cement concretes revealed that in addition to the world. The aim of this research work was to explore
pozzolanic reactivity of RHA [3], the particle grading the effects of binary and ternary mixtures of RHA
of cement and RHA mixtures also exerted significant and PRWFA on some fresh and hardened PAC
influences on the blending efficiency [4]. The properties.
strength development increase (relative to the
concrete made with plain cement, expressed in %) is 2. EXPERIMENTAL PROGRAM
higher for gap-graded cement [5]. 2.1 Materials
Moreover, Para rubber tree plantations are an
Ordinary Portland cement (OPC), Type I was
important economic crops especially in the south of
used. Its chemical compositions and physical
Thailand. The economic life cycle of the tree, which
is generally 25–30 years. After its yields become properties are given in Tab. 1 and particle size
extremely low latex, the Para rubber trees were distributions of cementitious materials as shown in
carried out cutting and replantation. The rubberwood Fig 1.
RHA and PRWFA ashes were collected waste
log is usually supplied to fabrict in furniture industry
biomass fuel from the electrical power plants. There
Fig. 1 Particle size distributions of OPC, RHA and or called Control, total sixteen binary and tertary
PRWFA. mixtures carried out with proportion of 10, 20, and
30%RHA and 10, 20, and 30%PRWFA by mass,
Tab. 1 Chemical compositions and physical whole replacements consisting from 0 to 60% were
properties of materials used. performed with water:binder:sand = 0.55:1:1.80 by
mass, for each test property. The amount of fine
Compositions
OPC PA RHA PRWFA aggregate (river sand) was 700 kg/m3 and to maintain
(%)
the PA content at 230 kg/m3. In order to prevent the
SiO2 21.2 60.70 87.48 2.57
mixing water being absorbed by the PA, therefore
Al2O3 5.22 18.36 - 0.53 minimizing the slump loss during pumping [11],
Fe2O3 3.08 4.61 0.11 0.56 prewetting or pre-soaking method was adopted on
CaO 64.73 5.09 0.70 41.19 PA. The water-to-binder ratio was constant at 0.55
MgO 1.04 1.07 - 4.52 throughout this study. Tab. 3 shown the masses of
K2O 0.42 2.92 1.65 16.11 materials used for each of the binder mixtures.
Na2O - 0.67 - -
P2O5 - - 0.72 3.06 Tab. 3 Ingradient of the PAC batches (kg/m3)
SO3 2.01 - 0.22 5.54 Batch OPC RHA PRWFA
MnO2 - - 0.32 1.36 Control 390 0 0
LOI 1.45 6.47 8.34 23.28 PRWFA10 350 0 40
Specific gravity 3.15 0.60 2.05 2.15 PRWFA20 310 0 80
Specific surface PRWFA30 270 0 120
1.63 - 33.13 9.23
area-SSA (m2/g) RHA10 350 40 0
Pore porosity RHA10PRWFA10 310 40 40
0 - 30.66 17.72
(m2/g) RHA10PRWFA20 270 40 80
RHA10PRWFA30 230 40 120
are several physical properties that are important to RHA20 310 80 0
know about for RHA and PRWFA before that ashes RHA20PRWFA10 270 80 40
can be used to reach its highest potential. The RHA20PRWFA20 230 80 80
chemical compositions and physical properties of are RHA20PRWFA30 190 80 120
given in Tab. 1. It was found LOI of both ashes be
RHA30 270 120 0
high due to unburnt carbon content in residue mixed
RHA30PRWFA10 230 120 40
with amorphous SiO2 content. It can be less effective
RHA30PRWFA20 190 120 80
pozolanic reaction in concrete [7].
Locally available natural sand with 4.75 mm RHA30PRWFA30 150 120 120
maximum size was used as fine aggregate according
to ASTM C136 [8], and PA as coarse aggregate with 2.3. Testing procedures
12.5 mm maximum size satisfied the ASTM C330
grading requirement for lightweight aggregate [9] as The electrical resistivity of the concrete mixes
shown in Fig 2. The fine and coarse aggregates had was determined using the McOhm meter. In this
specific gravity of 2.51 and 0.6, water absorptions of method, two electrodes are inserted in the concrete
1.48% and 56.69% which tested according ASTM after demolding the casting of the test specimens. An
C127 [10] and compact oven dry bulk density 1,587 AC current source is aligned and placed at each sides
and 424 kg/m3, respectively. Summary of physical of concrete. and the voltage difference between the
properties of aggregates are tabulated in Tab. 2. inner electrodes is measured [12]. Setting time of
paste was tested as ASTM C191 [13].
2.2 Mixture proportions
Six binary mixtures and nine ternary were 3. RESULT AND DISCUSSION
tested in this work, a reference mixture of 100%OPC 3.1 Fresh concrete properties
The initial and final setting times of blended
A RW A0
A RW 10
W 20
30
A RW A0
A2 RW 10
0
30
A RW A0
A RW 10
W 20
30
A W ol
RHA20PRWFA30 0 20 0.0
RW 2
RH 0PR ontr
PR FA
FA
RH 10P FA
PR FA
RH 20P FA
FA
PR FA
RH 0PR FA
FA
0P FA
RH 30P FA
FA
RH 0P F
RH 30P WF
RH 20P WF
W
A C
A R
A PR
A PR
P
RHA30 20 55 2.5
RH A10
RH 20
RH A30
10
30
1
A
RH
RH
RH
RH
RHA30PRWFA10 0 35 1.0 Type of PAC
RHA30PRWFA20 0 0 0.0
RHA30PRWFA30 0 0 0.0 Fig. 3 Water absorption of binary and ternary
mixtures of PAC.
200
Drying shrinkage x10 (%)
1740
180 7-day 28-day
-3
Bulk density (kg/m )
Fig. 2 Bulk density of binary and ternary mixtures of Fig. 4 Drying shrinkage of binary and ternary
PAC. mixtures of PAC.
1600
20%RHA and 20%PRWFA (RHA20PRWFA20) was
1400 Uncured 7-day 28-day
1200
about 77% of the control strength.
1000
3.7 Microstructural characterization
800
600 The common constituents of the ITZ
400
microstructure in ternary mixture of specimens were
200
0
clear to different distinguish [20,21,22]. All of the
l 0 0 0
ro 1 2 3
0 10 20 30 0 10 20 30 0 10 20 30 examined ITZ sections, the polymineralic such as
nt FA FA FA FA A A A FA A A A FA A A A
Co RW RW RW W WF F F W F F F W F WF F
P P P 0 PR PR PRW PRW 0PR PRW PRW PRW 0 PR PRW PR PRW calcium silicate hydrate (CSH) calcium hydroxide
0 0 0 1 0 0 0 A2 A20 A20 A20 A3 A30 A30 A30
A A A A A1 A1 A1
RH RH RH RH RH RH RH RH RH RH RH RH RH RH RH and ettringite formed around micropore of PA in Fig
Type of PAC 7a). Furthermore, bonding strength of ITZ decreased
Fig. 5 Electrical resistivity of binary and ternary causing of failure microcracks after compression test
mixtures of PAC. between boundary of past and the PA (Fig. 7 b).
Effects of the hydration and pozzolanic reactions
supported ITZ hardening.
3.6 Compressive strength
The compressive strength of PAC blended
binary and ternay of RHA and PRWFA as illustrated a)
in Fig 6. Comparison of the compressive strength
among curing for 1, 7 and 28 days. It was observed
that compressive strength increase gradually with
their increasing with RHA up to 20% and then gain a
tendency to decrease. A 28-day highest compressive
PA
strength was obtained 22.55 MPa from 20%RHA.
Thus, in order to meet ensuring the optimum level ITZ
may be restricted with about a 20% RHA
replacement of OPC. The characterization of
compressive strength reduction has been often found
in a lot of the previous literatures [16,17,18]. Most
rely reason of the pozzolanic reaction is responsible
high strength as well as high specific surface area
and the existing a lot of reactive silica content in
RHA. It is discussed in lots of previous works [19] . PA b)
Compressive strength (MPa)
25
28-day
20 7-day
Uncured
15
E
10
5
ITZ
0
A W 10
0
30
A RW A0
A RW 1 0
30
A RW A0
A RW 1 0
W 20
A RW A0
A RW 10
W 20
30
W 20
30
A W ol
RW 2
RH 0PR ontr
RH 0PR FA
0P F A
FA
RH 10P FA
FA
RH 20P FA
PR FA
FA
RH 3 0 P F A
PR FA
FA
PR FA
RH 10P WF
RH 20P WF
RH 0 P F W
A C
A PR
A PR
A PR
RH 10
RH 2 0
RH 3 0
10
20
30
A
A
3
RH
RH
RH
RH
Type of PAC
Fig, 7 SEM microphotograph of 20RHA10PRWFA
Fig. 6 Compressive strength of binary and ternary mixture cured 28 days a) ITZ between cementitious
mixtures of PAC. and PA and b) microcrack propagation (dot line).