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10.2.1.1 Scope. An alternative to the penetration test for checking the consistency of
bitumen, is the ring and ball softening point test. The scope of this test is to provide a
method for determining the consistency of semi-solid and bituminous materials in
which the sole or major constituent is either bitumen or tar pitch.
10.2.1.2 Definition. The softening point of a bituminous material is the temperature at which
the material attains a certain degree of softness under specified conditions of test.
10.2.1.3 Equipment. The equipment required to carry the penetration test in the laboratory
are listed below:
The sample obtained in accordance with section 2.7 is heated carefully in an oven or
on a hotplate until it has become sufficiently fluid to pour. When using a hotplate, the
bitumen should be stirred as soon as possible, to prevent local over-heating. In no
case should the temperature be raised more than 900C above the expected softening
point and samples must not be heated for more than 30 minutes. The brass rings to
be used for the test are placed on a flat smooth brass plate, which has been coated
immediately prior to use, with a thin covering of a mixture of glycerin and china clay.
The coating is to prevent the bitumen sticking to the plate.
When the bitumen is sufficiently fluid to pour, the rings should be filled with bitumen.
A tight excess of bitumen should be used. The bitumen is allowed to cool for a
minimum of 30 minutes. If the bitumen is soft at room temperature, it must be cooled
artificially for a further 30 minutes. After cooling the excess material on the top of the
specimen must be cut off cleanly using a moral palette knife.
20.5 - 20.7
20.54 - 20.7 DIA
17.4 - 17.6 DIA 15.76 - 15.96
6.25 - 6.45
6.25 - 6.45
2
2
18.9 - 19.1 DIA OPTIONAL
SHOULDER
Figure 10.2.1 Tapered Ring Material Brass Figure 10.2.2 Straight Ring
22.9 - 23.1
19.74 - 19.94
6.15 - 6.45
2.7 - 2.9
15.76 - 15.96
2
18.9 - 19.1
GUIDE FITS ON
TOP OF RING
(FIG. 1 OR 2) TO
POSITION THE BALL
ON CENTRE OF
SAMPLE
1.59
76
67
1.59
85 ID
LIQUID
LEVEL THERMOMETER 1P60C
OR 1P61C
SHOULDERED RING
FIG. 10.2.3
50
25
Figure 10.2.7 Assembly of ring-and-ball apparatus for two rings (stirrer not shown)
The apparatus is assembled with the rings, ball centering guides and thermometer in
position and the beaker is filled with water to a depth of not less than 102mm and not
more than 108mm. The water used for the test must be distilled and allowed to cool in
a stoppered flask, this is to prevent air bubbles forming on the specimen during the
test. The initial water temperature must be 5 ± 10C and this temperature must be
maintained for 15 minutes, placing the beaker in a bath of iced water if necessary.
On completion of the 15-minute period, the steel balls are positioned using forceps,
and heat is applied to the beaker, preferably with a gas burner, at such a rate that
the water temperature rises at 50C per minute. The rate of temperature rise is critical
and if after the first 3 minutes the rise varies from the 50C in any minute period, by
more than ± 0.50C, the test must be abandoned.
As the temperature rises, the balls will begin to cause the bitumen in the rings to sag
downwards, the water temperature at the instant the bitumen touches the bottom
plate is taken for each ball. If the two temperatures differ by more than 10C, the test
must be repeated using fresh samples.
10.2.3 Calculation
The ring and ball softening point is simply the average of the two temperatures at
which the bitumen just touches the bottom plate. A typical data sheet is shown as
Form 10.2.1.