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Failure prediction of composite materials

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BULLETIN OF APPLIED MECHANICS 4(14), 81–87 (2008)

Failure Prediction of Composite Materials

Vladislav Laš, Robert Zemčík, Tomáš Kroupa, and Radek Kottner


?
progressive failure analysis which uses material degradation
Abstract— The work focuses on the prediction of failure of approach [4, 12]. Three types of problems are analyzed in this
composite material under both static and dynamic loading. article: thin strips loaded in tension, thin unidirectional plate
Modern criteria are used in the calculations, such as LaRC04 or loaded by transverse impact, and delamination of
Puck’s criteria. The crack growth in composite material is
investigated using progressive failure analysis up to final rupture.
unidirectional composite under Mode I loading.
Three types of specimens are analyzed. One is thin flat strip
loaded in tension statically and dynamically. Second is thin
orthotropic plate loaded by low-velocity transverse impact. Third II. FAILURE CRITERIA
specimen is flat strip loaded in Mode I to induce delamination. All
cases were analyzed numerically using finite element method in
There exists a large number of criteria for the prediction of
MSC.Marc code and validated experimentally. Good agreement failure of composite material. Ranging from the simplest non-
was achieved in each case. interactive ones, such as maximum stress or maximum strain
criteria, to the interactive ones, such as Tsai-Hill, Tsai-Wu [3],
Index Terms— composite, failure criteria, progressive failure etc. Modern criteria have emerged recently which distinguish
analysis. between fiber failure (tensile and compressive) and matrix
failure. Several type or modes are considered in the case of
matrix failure and therefore these criteria are designated as so-
I. INTRODUCTION
called direct mode criteria. This work uses two direct mode

C OMPOSITE materials have been used more


extensively in the recent years in many areas of
industry. The main advantages of such materials are high
criteria, namely the Puck’s criterion [10] and LaRC04 criterion
[11].
Special type of composite failure is delamination of layered
strength and stiffness together with low weight, and the composites, i.e., the separation of the layers (laminae). This
possibility to design different desired mechanical properties of type of failure is caused either by normal stress components
a structure in different locations and directions. This fact between the layers or by shear stresses acting in the plane of
involves higher demands on the computational analysis, layers [9].
especially when compared to corresponding analysis of
conventional materials. One of the important tasks is to assess A Puck’s failure criterion
the critical stress state for static or dynamic loadings. There Puck’s criterion (direct mode) [10] avoids the deficiencies
are many criteria which are used to predict the failure of of both non-interactive and interactive criteria. It consists of
composite materials. The accuracy of the prediction of failure total five failure modes, two for fiber failure (tensile and
depends strongly on the criterion. compressive) and three for matrix failure (denoted as A, B and
In this work, modern criteria, such as LaRC04 [11] or C). The specific matrix failure types are shown in Figure 1
Puck’s criterion [10], are applied. Special type of failure is with corresponding mechanisms. The criterion is developed
delamination, which is failure between individual layers of a especially for the analysis of lamina under plane stress.
laminate [1]. The monitoring of the process of failure The mathematical formulae for the calculation of failure
propagation is performed with the method known as indices of fibers FIF and of matrix FIM are summarized in
Table 1, where XT and XC are material (lamina) tensile and
? ?
Manuscript received April 9, 2008. This work was supported by the
compressive strengths in the fiber direction, YT and YC are
research projects MSM 4977751303 and GA AV IAA200760611. tensile and compressive strengths in the transverse direction, S
V. Laš, University of West Bohemia, Faculty of Applied Sciences, is shear strength, and σL, σT and τLT are the normal
Department of Mechanics, Univerzitní 8, 306 14 Pilsen, Czech Republic,
phone: +420 377632326; fax: +420377632302; e-mail: las@kme.zcu.cz).
longitudinal, transverse and shear stresses, respectively. The
R. Zemčík, University of West Bohemia, Faculty of Applied Sciences, meaning of remaining symbols can be found for example in
Department of Mechanics, Univerzitní 8, 306 14 Pilsen, Czech Republic, [10]. The failure occurs when the corresponding failure index
phone: +420 377632336; e-mail: zemcik@kme.zcu.cz). exceeds the value of one.
T. Kroupa, University of West Bohemia, Faculty of Applied Sciences,
Department of Mechanics, Univerzitní 8, 306 14 Pilsen, Czech Republic, B LaRC04 failure criterion
phone: +420 377632367; e-mail: kroupa@kme.zcu.cz).
R. Kottner, University of West Bohemia, Faculty of Applied Sciences, This criterion, in contrast to the aforementioned, can be
Department of Mechanics, Univerzitní 8, 306 14 Pilsen, Czech Republic, applied also to three-dimensional state of stress. Another
phone: +420 377632373; e-mail: radek.kottner@kme.zcu.cz).
BULLETIN OF APPLIED MECHANICS 4(14), 81–87 (2008)

advantage is that it contains correction considering non-linear


behavior of the composite in shear loading. It is noticeable
from Table 2 that it consists of total six failure modes.
The first two rows represent two fiber failure modes,
whereas the third row denotes so-called combined mode when
fiber and matrix failures occur simultaneously. The remaining
three rows describe pure matrix failure. The symbol FIM/F
denotes the combined failure and the symbols SL and ST
represent the longitudinal and transverse shear strengths,
respectively. Symbols ηL and ηT denote the longitudinal and
transverse friction coefficients. The meanings of the remaining
symbols can be found for example in [11].
The combined mode (#6) not present in Puck’s criterion
assumes that the critical plane where failure occurs and the
transverse direction T form an angle ψ and that the influence
of compressive longitudinal stress causes the fibers to deflect
by an angle ϕ (see Figure 2), which is followed by the
simultaneous failure of fibers and matrix.
Mode A Figure 2. The combined mode of LaRC04 criterion.

D Delamination of composites
Mode B This type of failure is driven by the influence of interlaminar
shear stress or normal stress between adjacent laminae. The
mechanism of failure is similar to the problems of fracture
mechanics. The interlaminar fracture toughness is usually
Mode C
considered to be the critical value of the strain energy release
rate, denoted as Gc, or critical value of the stress intensity
factor Kc. Suitable experimental measurements must be carried
out to assess these values and for subsequent numerical
simulations. The interlaminar toughness GIc (corresponding to
Figure 1. Mechanisms causing matrix failure. Mode I loading) can be assessed according to the standard

Table I. Calculation of Puck’s criterion failure indices


Fiber tension EL  v 
 ε L + f mσ f σ T  = FI F , (K) ≥ 0
XT  Ef 
 
Fiber compression  
EL v
 ε L + f mσ f σ T  = FI F , (K) < 0
XC  Ef 
 
Mode A 2 2
τ TL
2
 Y T  σT  σ
+ 1 − p ⊥(+ )   T  + p ⊥(+ ) TT = FI M , σ T ≥ 0
S  S  Y  S
Mode B 1 2 σT R
 τ TL + ( p ⊥ σ T ) + p ⊥ σ T  = FI M ,
(−) 2 (−)
σT < 0 ≤ ≤
S  τ TL Sc
Mode C  τ TL R  2  σ T  2  Y C τ TL S
 C  +  C   = FI M , σT < 0 ≤ ≤ c
 Y S   Y   − σ T σT R

YC S
R= , p ⊥( + ) = p ⊥( − ) = p ⊥⊥
(−)
,
(−)
S C = S 1 + 2 p ⊥⊥
2(1 + p ⊥⊥
(−)
) R
BULLETIN OF APPLIED MECHANICS 4(14), 81–87 (2008)

ASTM D5528-01 [1] using DCB (Double Cantilever Beam) specimen (beam) is not clamped perfectly (there can occur
specimens. certain rotation in the cross-section at crack tip), the ASTM
The specimens are laminated rectangular strips with suggests using a correction with additional crack length ∆,
included non-adhesive aluminum foil which serves as the hence the GIc is actually calculated as
initial crack (see Figure 3). The specimen is placed in testing 3F δ c . (4)
G Ic =
machine using piano hinges and thus loaded by tensile force F. 2b (a + ∆ )
The dependence of force F on the grip opening δ is recorded,
E Progressive failure analysis
together with the crack length. The critical value GIc can then
be readily evaluated from this dependency. The strain energy Several failure criteria were mentioned in the preceding
release rate is mathematically defined, in general, as section. These criteria can be used the find the location and
1 dU , moment of failure but whether and how the failure is going to
G=− (1)
b da propagate cannot be decided. One of the methods that can be
where dU is the increase in potential energy of internal forces, used for such simulation is a combination of so-called
b is specimen width and da is increase in crack length. In case progressive failure analysis (PFA) with, for instance, the
of Mode I loading the formula can be transformed using the material degradation strategy. During the numerical simulation
solution of Euler-Bernoulli beam theory to performed usually by FEA (finite element analysis), the
12F 2 a 2 degradation is applied to the elasticity constants of the material
GI = 2 2 , (2) (characterized by stress-strain matrix C), thus reducing the
b h E
local stiffness. Three main types of failure can occur in general
where E is the Young’s modulus in the axial direction and h is – for matrix failure transverse to lamina plane C reduces to
half-thickness of the specimen. According to ASTM [1] the CM, for fiber failure to CF and for simultaneous failure (or
formula which is used for the evaluation of interlaminar subsequent failure of both matrix and fibers) to CM/F.
toughness is in the form The constitutive relation for unidirectional fiber composite
3F δ
GIc = c c , (3) (modeled as transversely isotropic material) in the case of
2b a undamaged element can be written as
where Fc and δc are the critical values of load und σ = C ε, (5)
displacement at which the crack propagation occurs. Since the
where σ and ε are stress and strain vectors and
Table II. Calculation of LaRC04 failure criterion failure indices.
Fiber failure conditions

LaRC #3 σL ≥ 0 σL
FI F =
XT

LaRC #4 σ L < 0 , σ 2m 2m < 0 τ 1m 2 m


FI F =
S − η L σ 2m 2m
L

LaRC #6 σ L < 0 , σ 2m 2m ≥ 0  σ 2m 2m   σ 2m 2m
2
  σ 1m 2 m 
2

FI M / F = (1 − g )  T  +  T  +  L 
 Y   Y   S 

Matrix failure conditions

LaRC #1 σT ≥ 0 σ   σ  τ 
2 2

FI M = (1 − g ) TT  + g  TT  +  LTL 
Y  Y   S 
2 2
LaRC #5 σ T < 0 , σ L < −Y C  τ Tm   τ Lm 
FI M =  T 
T m 
+ 
 L

L m 
 S −η σ n   S −η σ n 
2 2
LaRC #2 σ T < 0 , σ L ≥ −Y C  τT   τL 
FI M =  T T

 + 
 L L

 S −η σ n   S −η σ n 
BULLETIN OF APPLIED MECHANICS 4(14), 81–87 (2008)

C11 C12 C13 0 0  0 III. NUMERICAL AND EXPERIMENTAL EXAMPLES


C C 22 C 23 0 0 0  Numerical simulations of failure of composite materials
 12 
C C 23 C33 0 0 0 . (6) were carried out together with corresponding experiments for
C =  13  three types of specimens. First case considered thin rectangular
 0 0 0 C 44 0 0 
panels made of unidirectional composite loaded in tension,
 0 0 0 0 C55 0 
  secondly, thin unidirectional plate loaded by transverse impact,
 0 0 0 0 0 C 66  and finally, Mode I delamination of unidirectional laminates.
In case the failure index FIM > 1 in any element, the All specimens were cut out using water jet from plates made of
corresponding matrix CM is autoclaved prepreg layers (Toray T600SC fibers, volume ratio
C11 θ C13 0 0 0  vf = 0.51) with material properties displayed in Table 3 [8].
 θ θ θ 0 0 0
  Table III. Material properties of carbon-epoxy composite.
C13 θ C33 0 0 0  , (7)
C M
=  EL [GPa] 109 XT [MPa] 2128
 0 0 0 θ 0 0
ET [GPa] 7.7 XC [MPa] 1160
 0 0 0 0 C55 0 
  νLT 0.28 YT [MPa] 27
 0 0 0 0 0 θ
C
where θ is null (or very small number for the sake of numerical GLT [GPa] 4.5 Y [MPa] 200
stability). If failure index FIF > 1, then the matrix CF is applied ρ [kg⋅m-3] 1510 SL [MPa] 52
as
θ θ θ 0 0 0
θ C C 23 0 0 0 A Unidirectional composite panels loaded in tension
 22

θ C 32 C33 0 0 0 (8)
The tensile tests were performed on specimens with (type
CF =   A) and without (type B) stress concentrators having thickness
0 0 0 C 44 0 0 
1.05 mm. Each specimen was equipped with aluminum tabs at
0 0 0 0 θ 0 the ends. The specimens were rectangular having three
  different fiber orientations θ measured clockwise from the
0 0 0 0 0 θ
and if both matrix and fibers fail within one element the matrix loading direction. The effective length was 150 mm and width
reduces to either 25 mm (θ = 90°), 20 mm (θ = 45°), or 15 mm (θ = 0°);
θ θ θ 0 0 0  the width of specimens with stress concentrators (circular hole
θ θ θ 0 0 0  of diameter 10 mm in the center) was always 20 mm (see
  Figure 4). The grip speed was approx. 1 mm/min.
 θ θ θ 0 0 0 . (9)
CM / F =  
0 0 0 θ 0 0
0 0 0 0 θ 0
 
 0 0 0 0 0 θ 
The overall methodology of PFA is shown in the chart in
Figure 3 for quasi-static and non-stationary cases.

Figure 4. Fractured specimens in experiment.

Figure 3. Progressive failure analysis for quasi-static and non- In numerical simulation using FEA and Puck’s criterion, the
stationary problems (dashed). specimens were loaded in tension in displacement control, thus
BULLETIN OF APPLIED MECHANICS 4(14), 81–87 (2008)

assuming perfectly rigid area of the attached tabs in machine


grips. The load-displacement curves were calculated and they
are compared with the corresponding experimental data in
Figure 5. Artificial flaws had to be used in case of the two
panels without stress concentrators (A45, A00) in order to
initiate the matrix cracking in the desired location. The flaw
was modeled by element with strength YT reduced by 1%
[7,13].

Figure 7. Time dependence of transverse velocity of plate.

Also, the approach velocity of the impactor which is able to


damage the plate was investigated. The agreement of
experimental and numerical results is acceptable. Damaged
FEM model is shown in Figure 8. Matrix failure mode LaRC
#1 was driving the cracking of the plate. Hence the stress-
strain matrix of the damaged elements had the form (7). This
test showed the capability of selected PFA in the field of
impact loaded thin composite structures. The numerical
analyses show good agreement with the experiments [5, 6].

Figure 5. Comparison of experimental and numerical force-


displacement dependencies.
B Thin unidirectional plate loaded by transverse impact
The material of the plate was described above. Dimensions
of the plate were
50 mm × 50 mm × 1 mm. The impactor was steel cylinder
with rounded contact area. The direction of the impact is
obvious from Figure 6.
The transverse velocity of the plate was measured in chosen
points by laser vibrometer with sampling frequency of 1 MHz
and compared with numerical results showing good agreement.
The comparison between numerical and experimental results Figure 8. Numerical results showing damaged elements of the
for one specimen is shown in Figure 7. plate (dark elements).

C Delamination of unidirectional laminates


The DCB specimens were having dimensions 154.5 × 21 ×
4 mm. The inserted aluminum foil, which served as the initial
crack, was 11 µm thick. The opening force was applied using
the piano hinges as suggested in ASTM (see Figure 9). During
the testing process the dependence of the opening force F vs.
transverse displacement δ was recorded. The crack
propagation in time (crack length a) was measured optically
using a digital still camera. The optical measurement also
served as a verification of the transverse displacement values,
which might differ, in general, from the grip movement as
recorded by the testing machine due to its unknown internal
stiffness. The speed of the grip movement was chosen in the
range between 1 and 5 mm/min.
Figure 6. Configuration of the experiment. The numerical simulation was performed using FEA in
BULLETIN OF APPLIED MECHANICS 4(14), 81–87 (2008)

MSC.Marc. Different finite element mesh was prepared for Table IV. Measured and calculated parameters on pre-
each calculated case with certain crack length a [16]. The cracked DCB specimen.
equality between values of energy release rate and J-integral in
Initial crack length [mm] a 60.37
the case of elastic analysis was used in the simulations. The
code calculates the J-integral using the DeLorenzi method [2].
Crack length correction [mm] |∆| 7.41

piano hinge Min. energy release rate [kJm–2] GIcmin 0.4579


fibers
Max. energy release rate [kJm–2] GIcmax 0.6468

foil
IV. CONCLUSION
The failure analysis of three different composite specimens
is performed in this work. The problems were both static and
dynamic. It can be concluded that the choice of failure criteria
plays an important role. Another important aspect is the
piano hinge reliability of the computational model, namely the material
properties used therein. The manufacturer of the composite
provides certain set of data which must be considered as
referential only. One option is to calculate the properties from
the properties of constituents but in order to obtain reliable
data it is necessary to carry out series of experiments and
foil corresponding numerical simulations [14, 15]. Currently, new
methodologies for faster and more precise identification of
Figure 9. DCB specimen (Mode I) experimental setup. material properties are investigated, as it shows that the failure
analysis has been of constantly growing importance by the
The values of GIc (and its limits GIcmin and GIcmax as shown in practice.
Table 4) were calculated from experimental data using (4) and
then used in the numerical model. As opposed to the theory, REFERENCES
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