Beruflich Dokumente
Kultur Dokumente
Apparatus/Chemicals/Equipment:
Chemical /Reagents:
0.02 M KMnO4
Procedure:
Prepare and standardize a 0.01 M solution of KMnO4. Then using a measuring pipette,
place 0.30, 0.50, 1.00, 1.50, 2.00, 3.00 and 4.00-mL portions into five 100-mL
volumetric flasks numbered 1 to 5, these will serve as your standard solution. Prepare
another 100 mL flask and place 1.30 mL of 0.01 M KMnO4, this will served as your
unknown solution. Dilute solution in each flask to the mark. Calculate the
concentration (ppm) of resulting standard solutions.
Measure the absorbance of the blank ( or a very dilute KMnO 4 solution) 10 times.
Calculate the standard deviation of the blank.
Experiment 7
Spectrophotometric Determination of Permanganate Concentration
A. Permanganate Standards
Concentration of KMNO4:_________________________________
Wavelength Absorbance
400
420
440
460
480
500
520
525
530
535
540
545
550
555
560
580
600
C. Determination of Calibration Curve
Blank Absorbance
1
2
3
4
5
6
7
8
9
10