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© Retsch Technology GmbH, 42781 Haan, Retsch-Allee 1-5, Germany | 21.06.2016 Version 0001
Copyright
© Copyright by
Retsch Technology GmbH
Retsch-Allee 1-5
D-42781 Haan
Germany
2
Table of Contents
1 Notes on the Manual ............................................................................................................................. 6
1.1 Disclaimer .......................................................................................................................................... 6
1.2 Copyright............................................................................................................................................ 6
1.3 Explanations of the Safety Instructions ............................................................................................. 7
1.4 General Safety Instructions ............................................................................................................... 8
1.5 Repairs............................................................................................................................................... 9
2 Confirmation Form for the Managing Operator ................................................................................ 11
3 Technical Data ..................................................................................................................................... 12
3.1 Protective Equipment....................................................................................................................... 12
3.2 Degree of Protection ........................................................................................................................ 12
3.3 Emissions......................................................................................................................................... 12
3.4 Electromagnetic Compatibility (EMC) .............................................................................................. 13
3.5 Rated Power .................................................................................................................................... 13
3.6 Dimensions and Weight ................................................................................................................... 13
3.7 Required Floor Space ...................................................................................................................... 13
3.8 Compressed Air Supply ................................................................................................................... 14
3.9 Receptacle Volume.......................................................................................................................... 14
3.10 Feed Grain Size ............................................................................................................................... 14
3.11 Measuring Principle ......................................................................................................................... 15
4 Packaging, Transport and Installation .............................................................................................. 17
4.1 Packaging ........................................................................................................................................ 17
4.2 Transport.......................................................................................................................................... 17
4.3 Temperature Fluctuations and Condensation ................................................................................. 18
4.4 Conditions for the Installation Site ................................................................................................... 18
4.5 Electrical Connection ....................................................................................................................... 19
4.6 Type Plate Description ..................................................................................................................... 19
4.7 Removing the Transportation Lock .................................................................................................. 20
5 First Commissioning ........................................................................................................................... 22
5.1 Connecting the Feeder Unit ............................................................................................................. 23
5.2 Connecting the X-Dry Module.......................................................................................................... 27
5.2.1 Inserting the X-Fall Cartridge ....................................................................................................... 28
5.2.2 Inserting the X-Jet Cartridge ........................................................................................................ 29
5.2.3 Inserting the Feed Chute ............................................................................................................. 30
5.3 Connecting the Vacuum Cleaner ..................................................................................................... 31
5.4 Connecting the X-Flow Module ....................................................................................................... 33
5.5 Conneting the PC ............................................................................................................................ 34
5.6 Software Installation ........................................................................................................................ 35
5.7 Switching On / Off ............................................................................................................................ 35
5.8 Software Start .................................................................................................................................. 35
5.9 Calibration ........................................................................................................................................ 36
5.9.1 Insertion of the Calibration Reticle ............................................................................................... 36
5.9.2 Performing a Calibration .............................................................................................................. 38
6 Operating the Device .......................................................................................................................... 40
6.1 Use of the Device for the Intended Purpose.................................................................................... 40
6.2 Views of the Instrument ................................................................................................................... 43
3
6.2.1 Front ............................................................................................................................................. 43
6.2.2 Back ............................................................................................................................................. 44
6.3 Measurement Methods .................................................................................................................... 45
6.3.1 X-Fall Measurement Method ....................................................................................................... 45
6.3.2 X-Jet Measurement Method ........................................................................................................ 46
6.3.3 X-Flow Measurement Method...................................................................................................... 46
6.4 Change of Module ........................................................................................................................... 47
6.5 X-Dry Module ................................................................................................................................... 48
6.5.1 Changing the Gravity Nozzle ....................................................................................................... 48
6.5.2 Changing the Dispersion Nozzle ................................................................................................. 49
6.6 X-Flow Module ................................................................................................................................. 50
6.6.1 Changing the Flow Cell ................................................................................................................ 50
6.6.2 Filling the X-Flow ......................................................................................................................... 53
6.6.3 Draining ........................................................................................................................................ 54
6.7 Wet Measurement with Highly Flammable Materials ...................................................................... 55
7 Cleaning, Wear and Maintenance ...................................................................................................... 57
7.1 Cleaning ........................................................................................................................................... 57
7.1.1 Basic Device ................................................................................................................................ 57
7.1.1.1 Calibration reticle ................................................................................................................. 57
7.1.2 Feeder Unit .................................................................................................................................. 58
7.1.3 X-Dry Module ............................................................................................................................... 58
7.1.3.1 X-Fall Cartridge .................................................................................................................... 58
7.1.3.1.1 Cleaning the Gravity Nozzle: ......................................................................................... 58
7.1.3.2 X-Jet Cartridge ..................................................................................................................... 58
7.1.3.2.1 Cleaning the Dispersion Nozzle: ................................................................................... 59
7.1.4 X-Flow Module ............................................................................................................................. 59
7.1.4.1 Flow cell ............................................................................................................................... 59
7.2 Wear .................................................................................................................................................. 60
7.3 Maintenance ...................................................................................................................................... 60
7.3.1 Replacing the Fuses .................................................................................................................... 60
8 Accessories ......................................................................................................................................... 62
9 Disposal ................................................................................................................................................ 63
9.1 Dust Filter Disposal ........................................................................................................................... 63
9.2 Disposal of Sample Material and Dispersant .................................................................................... 64
10 Index ..................................................................................................................................................... 65
CE Declaration .......................................................................................................................... following page
4
Notes on the Manual
5
Notes on the Manual
This manual is a technical guide on how to operate the device safely and it contains all the
information required for the areas specified in the table of contents. This technical
documentation is a reference and instruction manual. The individual chapters are complete in
themselves. Familiarity (of the respective target groups defined according to area) with the
relevant chapters is a precondition for the safe and appropriate use of the device.
This manual does not contain any repair instructions. In case of any obscurities or questions
with regards to this document or the device, as well as if faults arise or repairs are necessary,
please contact your supplier or get in touch with Retsch Technology GmbH directly.
Revision status:
This document revision 0001 refers to the manual "Particle Size Analyser CAMSIZER X2" in
compliance with the Directive of Machinery 2006/42/EG.
1.1 Disclaimer
This document has been prepared with due care. Technical and software based modifications
are reserved. No liability is assumed for data loss, personnel injury or damage to the device
which results from the failure to observe the instructions and/or warnings in this document.
1.2 Copyright
This document or parts of it or its content may not be reproduced, distributed, edited or copied
in any form without prior written permission of Retsch Technology GmbH. Damage claims shall
be asserted in the case of infringements.
6
Notes on the Manual
In this document the following safety instructions warn of possible dangers and damages:
D1.0000
DANGER
Life-threatening personal injuries may result from disrespecting the safety instruction for
danger. There exists a very high risk of hazard of life or permanent injury to personnel.
Additionally, in continuous text or action instructions the signal word DANGER is used.
W1.0000
WARNING
Serious personal injuries may result from disrespecting the warning notice. There exists an
elevated risk of an accident or severe injury to personnel. Additionally, in continuous text or
action instructions the signal word WARNING is used.
7
Notes on the Manual
C1.0000
CAUTION
Moderate or mild personal injuries may result from disrespecting the safety instruction for
caution. There exists a medium or low risk of an accident or injury to personnel. Additionally, in
continuous text or action instructions the signal word CAUTION is used.
N1.0000
NOTICE
Property damages may result from disrespecting the notice. However, there exists no risk of
an injury to personnel. Additionally, in continuous text or action instructions the signal word
NOTICE is used.
C2.0002
CAUTION
Target group:
All persons concerned with this device in any form.
This device is a modern, high performance product from Retsch Technology GmbH and
complies with the state of the art. Operational safety is given if the device is handled for the
intended purpose and attention is given to this technical documentation.
8
Notes on the Manual
Safety manager:
The managing operator himself must ensure that the people entrusted with working on the
device…
− have noted and understood all the regulations regarding safety,
− are familiar before starting work with all the operating instructions and specifications for
the target group relevant to their work,
− have unrestricted and free access to the technical documentation for this device,
− are familiarising new personnel with the safe handling of the device and its use for its
intended purpose before starting work either by verbal instructions from a competent
person and/or by means of this technical documentation.
CAUTION Improper operation can result in personal injuries and material damage. The
managing operator himself is responsible for his own safety and that of his employees. The
managing operator himself is responsible that no unauthorised person has access to the device.
C3.0015
CAUTION
N2.0012
NOTICE
1.5 Repairs
This manual does not contain any repair instructions. For safety reasons, repairs may only be
carried out by Retsch Technology GmbH or an authorised representative or by qualified service
technicians.
9
Notes on the Manual
…the supplier, or
…Retsch Technology GmbH directly.
Service address:
10
Confirmation Form for the Managing Operator
The user of the device herewith confirms to the managing operator (owner) that he has received
sufficient instructions about the operation and maintenance of the system. The user has
received the manual, has read and taken note of its contents and consequently has all the
information required for safe operation and is sufficiently familiar with the device.
The managing operator should for legal protection have the user confirm the instruction about
the operation of the device.
I have read and taken note of the contents of all chapters in this manual as well as all
safety instructions and warnings.
User
11
Technical Data
3 Technical Data
3.1 Protective Equipment
− The device is equipped with module detection, compressed air and vacuum sensors. The
sensors prevent an X-Jet measurement from being started when in an unsafe state.
− The X-Jet measurement can only be started with the compressed air and the vacuum
working.
− The X-Fall measurement can also be started without compressed air and/or vacuum.
3.3 Emissions
C4.0025
CAUTION
C5.0026
CAUTION
Hearing damage
A high sound level may be generated depending on the type of material, the set
pressure and the duration of the X-Jet measurement
− Excessive noise in terms of level and duration can cause impairments or
permanent damage to hearing.
• Ensure suitable noise protection measures are taken or wear ear
protection.
Sound parameters:
Especially for X-Jet measurements, the sound parameters are strongly influenced by the
measurement conditions.
Example 1:
Module: X-Dry with X-Jet cartridge and dust protection cap
Dispersion pressure: 300 kPa (3 bar)
Vacuum: on
12
Technical Data
At these operating conditions, the workplace related equivalent continuous sound level
Leq = 81 dB(A).
Example 2:
Module: X-Dry with X-Jet cartridge and dust protection cap
Dispersion pressure: 30 kPa (0.3 bar)
Vacuum: on
Feed material: Quartz sand
At these operating conditions, the workplace related equivalent continuous sound level
Leq = 73.3 dB(A).
C6.0047
CAUTION
13
Technical Data
Location requirements:
The device must be placed on a vibration-free, plane, stable and free surface. For the
corresponding PC including monitor a free surface must be available in the immediate vicinity
(< 2 m) of the device. For the vacuum cleaner a free floor area must be available in the
immediate vicinity (< 2 m).
The supporting surface in front of the device must be sufficiently large to safely pull forward the
modules in order to change them.
The feed must be constant and the compressed air must be free of oil and water.
− Working pressure: 6 bar
− Compressed air volume: 140 l/min
CAUTION At a working pressure > 6 bar, the overpressure is blown off via a valve inside the
X-Dry module. A high sound level may occur during this process.
1)
The lower measurement limit depends on the material properties of the sample
(agglomeration).
2)
The upper measurement limit depends on the particle shape. The standard gravity nozzle
allows for a maximum upper limit of 5 mm for round, compact particles.
3)
The upper measurement limit depends on the particle shape. The standard dispersion nozzle
allows for a maximum upper limit of 3 mm for round, compact particles.
4)
The upper measurement limit depends on the density of the particles. 600 µm is a typical limit
3
for samples with a density of 2.5 g/cm .
14
Technical Data
The measurement range can be extended up to 8 mm with optional dispersing nozzles for X-Jet
and gravity nozzles for X-Fall. Further information are available in Chapter "X-Dry module" and
on the homepage http://www.retsch-technology.com/.
In the sample chamber two LED light sources and two cameras (one Basic and one Zoom
camera) are placed opposite each other.
− Total frame rate: 360 frames per second
D
F2 DF E1
E2
F1 PL
RP
PL Plano-convex lens Lens for beam shaping of the light source 1 and 2
15
Technical Data
The greyscale images are converted in real-time into binary images using a multi-step analysis
algorithm and the exact contour of the particles is determined. On this basis, all particle size and
shape parameters can be measured.
16
Packaging, Transport and Installation
N3.0001
NOTICE
4.2 Transport
N4.0017
NOTICE
Transport
− Mechanical or electronic components may be damaged.
• The device may not be knocked, shaken or thrown during transport.
N5.0025
NOTICE
Transport
Modular device
− Mechanical or electronic components may be damaged.
• Remove all modules, cartridges and accessories from the basic device
and transport these units separately in the provided packaging.
N6.0014
NOTICE
Complaints
− The forwarding agent and Retsch Technology GmbH must be notified
immediately in the event of transportation damage. It is otherwise possible that
subsequent complaints will not be recognised.
• Notify your forwarding agent and Retsch Technology GmbH within 24
hour.
17
Packaging, Transport and Installation
N7.0016
NOTICE
Temperature fluctuations
The device may be subject to strong temperature fluctuations during transport (e.g.
aircraft transport)
− The resultant condensed water may damage electronic components.
• Wait before commissioning until the device has been acclimatised.
Temporary storage:
Also in case of an interim storage the device must be stored dry and within the specified
ambient temperature range.
N8.0021
NOTICE
Ambient temperature
Temperatures outside the permitted range
− Electronic and mechanical components may be damaged.
− The performance data alter to an unknown extent.
• Do not exceed or fall below the permitted temperature range (5 °C to
40 °C ambient temperature) of the device.
For ambient temperatures UT between 31 °C and 40 °C, the maximum relative humidity value LF
linearly decreases according to LF = -(UT – 55)/0.3:
Ambient temperature Max. rel. humidity
≤ 31 °C 80 %
33 °C 73.3 %
35 °C 66.7 %
37 °C 60 %
39 °C 53.3 %
40 °C 50 %
18
Packaging, Transport and Installation
N9.0015
NOTICE
Humidity
High relative humidity
− Electronic and mechanical components may be damaged.
− The performance data alter to an unknown extent.
• The relative humidity in the vicinity of the device should be kept as low
as possible.
N10.0022
NOTICE
Electrical connection
Failure to observe the values on the type plate
− Electronic and mechanical components may be damaged.
• Connect the device only to mains supply matching the values on the type
plate.
2
6
3
4
8 7
9 10
11 12 13 14
1 Device designation
19
Packaging, Transport and Installation
2 Year of production
3 Part number
4 Serial number
5 Manufacturer’s address
6 CE marking
7 Disposal label
8 Bar code
9 Power version
10 Mains frequency
11 Capacity
12 Amperage
13 Number of fuses
14 Fuse type and fuse strength
In the case of queries please provide the device designation (1) or part number (3), as well
as the serial number (4) of the device.
N11.0018
NOTICE
Transportation lock
Transport without transportation lock, or operation with transportation lock
− Mechanical components may be damaged.
• Only transport the device with mounted transportation lock.
• Do not operate the device with built-in transportation lock.
20
Packaging, Transport and Installation
TP
Place the feeder unit on a plane, stable surface in such a way, that the bottom side is
accessible.
Loosen the M6 screw (TP) on the bottom side of the feeder unit by means of a 5 mm Allen
key.
Retain the screw and the washer. Before next transportation, the transportation lock must be
reinserted and tightened again.
21
First Commissioning
5 First Commissioning
W2.0002
WARNING
W3.0005
WARNING
For the first commissioning the basic device must be connected to the PC and, depending on
the desired measurement mode, completed with the X-Flow or the X-Dry module including the
feeder unit. The modules and feeder unit are delivered in separate packaging.
UK
22
First Commissioning
Grasp the basic device at the circumferential edge (UK) to lift it.
Place the basic device on a stable, level and vibration-free surface. Observe all requirements
for the installation site.
NOTICE The weight of the device amounts approx. 30 kg. The device should only be lifted by
two people.
Connect the supplied RS232 cable to the interface (O) on the backside of the basic device.
Connect the supplied synchronisation cable of the Basic camera to the interface (P) on the
backside of the basic device.
Connect the supplied synchronisation cable of the Zoom camera to the interface (R) on the
backside of the basic device.
Plug in the supplied 16 A power cable to the mains connection (J) on the backside of the
basic device.
NOTICE Secure all data cables by tightening the screws on the connectors.
NOTICE Disconnect the basic device from the power supply before installing the feeder unit.
NOTICE The feeder unit can only be installed and operated with removed transportation lock.
23
First Commissioning
SF4
SF3
S SF1
SF2
TD
Place the feeder unit on the back extension (TD) of the basic device in such a way, that the
rubber feet (SF1) of the feeder unit are positioned in the designated recesses (SF2) of the
back extension.
Connect the RS232 cable (SF3) of the feeder unit to the interface (S) on the back extension
of the basic device.
Connect the power cable (SF4) of the feeder unit to the mains connection (T) on the back
extension of the basic device.
NOTICE Secure the data cable by tightening the screws on the connector.
24
First Commissioning
RH
RB
RD
Check the correct fitting of the dust seals (RD) before mounting the feed chute holder.
Use a Phillips screwdriver to remove the countersunk head screws from the two bolts (RB).
Place the feed chute holder (RH) on the bolts and tighten it with the previously removed
screws. Make sure that the feed chute holder is aligned correctly, i.e. with the open side
facing forward.
NOTICE Without a fixed connection between the feed chute and the bolts, no sufficient
transmission of the vibrations will take place and the feeding is not controllable.
Check that the screws are securely tightened.
25
First Commissioning
TR
TH1
TH2
TS
26
First Commissioning
MD3
MD4
MD5
MD2
MD6
MD7
Place the X-Dry module on the free supporting surface in front of the basic device.
Grasp the module at the recessed grips (MD1) and push it completely to the basic device.
While doing so, observe the correct orientation of the two guide pins (MD2) which must be
inserted in the respective receptacle (B) on the basic device.
Slide the collecting tray (MD6) into the X-Dry module.
Connect the compressed air hose to the compressed air connection (MD7) of the X-Dry
module.
The upper part (MD3) of the module (cartridge receptacle) is positioned in the sample chamber
with the suction socket (MD4) set flush to the suction (I) of the basic device. The plug-in
contacts (MD5) of the module are connected to the multipoint connector (C) of the basic device.
27
First Commissioning
The communication between module and PC, as well as the power supply is established via the
plug-in contacts.
The module can also be inserted or changed with the basic unit switched on.
FA3
FA2
FA1
FA2
FA3
Grasp the X-Fall cartridge by the handle (FA1) and insert the cartridge vertically from above
into the X-Dry module with the stainless steel hopper (FA2) of the X-Fall cartridge facing
towards the feeder unit (away from the operator).
Place the cover (FA3) on the X-Fall cartridge.
Insert the short feed chute for the X-Fall measurement. The insertion of the short feed chute
is done analogous to the long feed chute for the X-Jet measurement ( Chapter "Inserting
the feed chute").
28
First Commissioning
JE3 JE2
JE1
JE4
JE5
JE6
JE7
29
First Commissioning
For the X-Jet measurement, the long feed chute is required, whereas for the X-Fall
measurement, the short feed chute is inserted.
RI1
RI2
RH
Clamp the back edge (RI1) of the feed chute under the two lugs (RI2) of the feed chute
holder (RH).
30
First Commissioning
RI
RH
Press the feed chute (RI) into the feed chute holder (RH) until it latches.
For the X-Jet measurement, put the dust protection cap (JE7) on top of the stainless steel
hopper (JE5) of the X-Jet cartridge.
Before commissioning the vacuum cleaner, check if a vacuum cleaner bag is inside the
vacuum cleaner. For more information, please read the separate manual of the vacuum
cleaner.
Check that the vacuum cleaner hose is firmly mounted to the vacuum cleaner.
31
First Commissioning
TD
VC1
VC2
K VC4
VC3
VC4
Slide in the reducing adapter (VC1) at the end of the vacuum cleaner hose (VC2) as far as
possible into the vacuum cleaner connection (U) on the backside of the back extension (TD).
Ensure that the reducing adapter (VC1) is fitted firmly to the vacuum cleaner hose (VC2).
Plug the mains cable of the vacuum cleaner into the matching socket (VC3) of the supplied
mains adapter cable.
Plug the other end (VC4) of the mains adapter cable into the mains connection for the
vacuum cleaner (K) on the basic device.
Switch on the vacuum cleaner.
The power for the vacuum cleaner is supplied by the basic device and will be switched on at
measurement start via the software control. For the X-Jet measurement the suction power
should be set to maximum (level 2). For the X-Fall measurement it is recommended to use the
vacuum cleaner for very dusty samples in order to minimise contamination of the safety glasses
32
First Commissioning
in the sample chamber. A lower suction power (level 1) is sufficient here. Please read the
separate manual of the vacuum cleaner for further information on the setting of the suction
power.
MD11
MD1 MD2 B C
MD10
MD5
MD2
MD8
MD9
MD9
MD8
33
First Commissioning
Place the X-Flow module on the free supporting surface in front of the basic device.
Grasp the module at the recessed grips (MD1) and push it completely to the basic device.
While doing so, observe the correct orientation of the two guide pins (MD2) which must be
inserted in the respective receptacle (B) on the basic device.
Connect the two supplied hoses to the overflow outlet (MD8) and the outlet (MD9) of the X-
Flow module, respectively. Depending on the ordered version, the two outlets are located
either on the backside or on the left side of the X-Flow module.
Put the hose ends in a collecting vessel (not included in the delivery) with a capacity of at
least 5 l. Make sure that the collecting vessel is located below the X-Flow module and that
the hose has a continuous slope down.
Place the cover (MD11) on the X-Flow module.
The upper part (MD10) of the module (flow cell receptacle) is positioned in the sample chamber.
The plug-in contacts (MD5) of the module are connected to the multipoint connector (C) of the
basic device. The communication between module and PC, as well as the power supply is
established via the plug-in contacts.
The module can also be inserted or changed with the basic unit switched on.
PC8
PC3
PC2
PC4
PC7
PC5
PC6
PC1
34
First Commissioning
PC4 Sync Basic interface "Aux I/O A" Synchronisation cable connection of the Basic
camera (D-Sub 15-pin)
PC7 Sync Zoom interface "Aux I/O B" Synchronisation cable connection of the Zoom
camera (D-Sub 15-pin)
PC8 RS232 interface Data cable connection from the basic device
(D-Sub 9-pin)
Connect the mouse and the keyboard respectively to an available USB port on the backside
of the PC.
Connect the monitor to the DVI port (PC1) of the graphics card.
Connect all data cables of the basic device in accordance with the assignment to the PC.
NOTICE Secure all data cables by tightening the screws on the connectors.
Via the basic device, the module, the feeder unit and the vacuum cleaner are supplied with
power. The mains switch (A) is equipped with a blue LED which lights up when the basic device
is turned on.
A description of the individual functions can be found in the separate software manual.
35
First Commissioning
5.9 Calibration
The CAMSIZER X2 has been calibrated by the manufacturer. However, a calibration at the
operator's location is recommended after a transport of the device, or on a regular basis to
comply with the quality assurance guidelines. A tested and certified calibration reticle is
available from your supplier or directly from Retsch Technology GmbH.
NOTICE Before calibration, the two safety glass panes (G) and (H) should be checked for
cleanliness. Dirt and dust can be removed with ethanol or a household glass cleaner and a lint-
free cloth. Be careful not to leave any streaks on the panes.
KN1
KN3
KS3
KS
KN2
KS2
KN
KS1
For the calibration of the basic device, the sample chamber (D) must be freely accessible.
Remove, if present, the X-Dry or X-Flow module. It is not necessary to remove the feeder
unit, but no feed chute should be present in the feed chute holder.
Take the calibration reticle (KN) with the mount (KS) from the calibration case and separate
the two units.
Put the calibration reticle (KN) back into the calibration case for safekeeping and later use.
Two threaded holes (KS4) are located in the base plate of the sample chamber (D). The front of
the two threaded holes is marked by a red arrow. An identical arrow is located on one side of
the mount (KS).
36
First Commissioning
KS2
KS1
KS4
Place the mount in such a way in the sample chamber that the two arrows are pointing to
each other and both threaded bolts (KS1) fit in the threaded holes (KS4).
Screw the mount (KS) by means of the two knurled screws (KS2) to the base plate of the
sample chamber.
CAUTION Avoid any contact with the two safety glass panes (G) and (H) by hard objects,
such as the mount itself, a ring or a watch. The glass of the safety glass panes is not break or
scratch resistant! Glass shards can cause lacerations to the hands.
KN
KS
37
First Commissioning
During the calibration process, the CAMSIZER X2 programme requests the operator to insert
the calibration reticle (KN).
Grasp the calibration reticle on the handle (KN1) and align it in such a way that the pane
(KN2) of the calibration reticle is facing the illumination side (F).
Insert the calibration reticle vertically from above into the mount. Pay attention on the correct
position of the guidance V-block (KN3) on the mount rods (KS3).
By means of a dot pattern on the pane (KN2) of the calibration reticle, the CAMSIZER X2
programme now determines the magnification in pixel per inch for both cameras, respectively.
The newly determined values are compared with the values stored in the configuration file. The
calibration is considered okay, if the difference between the old and new values does not
exceed ± 0.5 %. If the deviation is greater, the adjustment should be optimised.
The result of the calibration is displayed in a dialogue box. Depending on the result, answer the
question of optimising the adjustment as follows:
Click [No], if the calibration is OK.
Click [Yes], if the calibration is NOT OK. The CAMSIZER X2 programme now stores the new
values in the configuration file. However, if the deviation turns out to be too high, the service
must be contacted. This is indicated by a corresponding dialogue box.
After the calibration, a calibration record can be printed. A corresponding dialogue box is
displayed.
Click [No], if no calibration record is to be printed.
Click [Yes], to print the calibration record. The "Print" window opens.
Finally, the CAMSIZER X2 programme requests the operator to remove the calibration reticle
again.
Remove the calibration reticle (KN) from the mount and confirm the corresponding dialogue
box with [OK].
Unscrew the mount (KS) and put it back into the calibration case together with the calibration
reticle.
38
First Commissioning
39
Operating the Device
C7.0005
CAUTION
N12.0007
NOTICE
N13.0024
NOTICE
Device damage
Ingress of dust into the device
− Dust and material residues inside the device can cause damage to the
electrical components.
• Remove any spilled material residues immediately.
• Operate the device in a dust free environment.
• Turn off the device immediately if material residues have entered the
interior of the device and contact the service.
This Particle Size Analyser of the Retsch Technology GmbH is an opto-electronic laboratory
device for measuring and analysing particle size distributions and particle shape parameters.
The device is suitable for both, dry and wet analysis of various materials in a size range of 1 µm
to 8 mm. Wood fibres, synthetic fibres, plastics powders, food powders and granules, metal and
ore powders, pharmaceutical powders, granules and fine pellets, salt, sand, abrasives (medium-
size and small grit), detergent powders and raw materials, cement, sugar, coffee and many
other substances can be easily and quickly analysed
The Particle Size Analyser of the Retsch Technology GmbH is successfully deployed in almost
all areas of industry and research within the scope of quality control, especially where there are
high demands regarding easy operability, speed, precision and reproducibility.
40
Operating the Device
The device has a modular design and hence, depending on the configuration, allows for the
appropriate measurement method for the sample material:
− Gravity dispersion (X-Dry module with X-Fall cartridge)
− Compressed air dispersion (X-Dry module with X-Jet cartridge)
− Wet dispersion (X-Flow module)
Gravity dispersion:
The gravity dispersion measurement with the X-Fall cartridge inside the X-Dry module is
suitable for dry, free flowing materials with low content of fines. Depending on the selected
gravity nozzle this method is also suitable for coarser particles up to 8 mm. The sample material
is collected in a collecting tray after the measurement.
Wet dispersion:
The wet dispersion measurement with the X-Flow module is suitable for fine materials, which
tend to agglomerate. Agglomerates can be broken up by ultrasonic sound. Furthermore, the wet
dispersion measurement is also suitable for cost-intensive materials as only a small quantity is
needed for the measurement. The dispersant including the sample material is collected in a
collecting vessel after the measurement.
Clean, lime-free water or ethanol is suitable as dispersant. The use of highly flammable
dispersants is permitted. However, in this case please note the additional comments in Chapter
"Wet measurement with highly flammable materials". The X-Flow module is suited to operate
with many dispersing agents, but if in doubt, please contact the service.
W4.0010
WARNING
41
Operating the Device
C8.00006
CAUTION
C9.0018
CAUTION
Chemical reactivity
Mixing of different substances
− The successive analysis of different substances may cause undesirable
chemical reactions that can lead to fires or explosions.
− The substances can also react with each other in the vacuum cleaner.
• Do not use any substances in this device which carry the risk of
increasing chemical reactivity by contact with a previously measured
substance.
• Do not use any substances in this device which carry the risk of
increasing chemical reactivity by contact with the dispersant.
• In case of doubt, clean the device, the suction and the vacuum cleaner
(incl. change of vacuum cleaner bag and filter) before measuring another
substance.
• Observe the material safety data sheets of the grinding material.
C10.0023
CAUTION
42
Operating the Device
F H G E
I B C A
B Receptacle for the guide pins Serves as guide for mounting the module
G Safety glass pane of the camera Protects the camera side (E) against
side contamination
H Safety glass pane of the Protects the illumination side (F) against
illumination side contamination
43
Operating the Device
6.2.2 Back
Z U
N
X J K L O P R T S W V
K Mains connection vacuum cleaner Connection for the 16 A mains plug of the
vacuum cleaner (power supply via the basic
device)
T Mains connection feeder unit Connection for the power cable of the feeder
unit (power supply via the basic device)
U Vacuum cleaner connection Plug socket for the vacuum cleaner hose
44
Operating the Device
Y Base and Full camera link cables Connection (image transmission) cables
of the Basic camera between Framegrabber and Basic camera
Z Base and Full camera link cables Connection (image transmission) cables
of the Zoom camera between Framegrabber and Zoom camera
The X-Fall measurement method is one of the two possible dry dispersion measurements, in
which the sample material is fed into the hopper and transported via the vibration feed chute to
the sample chamber. The dosage of the material quantity is computer controlled using the
vibration intensity of the chute.
In the X-Fall measurement, the sample material falls from the chute into the stainless steel
hopper of the X-Fall cartridge, and then, accelerated by gravity, through the sample chamber
and the field of view of the cameras. The sample material is collected in the collecting tray of the
X-Dry module. Material loss and contamination are minimal and thus the sample can be reused
after the measurement for further analysis purposes.
45
Operating the Device
The X-Jet measurement method is a dry dispersion measurement using the same sample
supply as the X-Fall measurement method.
In the X-Jet measurement, the sample material is sucked in the stainless steel hopper of the X-
Jet cartridge by means of negative pressure. Subsequently, the sample is accelerated via
controllable compressed air through the dispersion nozzle, during which existing agglomerates
are broken up without destroying the particles themselves. The dispersed particles then fly
through the sample chamber and the field of view of the cameras, and are sucked off behind the
measuring window. The sample material is either collected in a vacuum cleaner, or optionally
deposited by means of a cyclone.
46
Operating the Device
In the wet dispersion measurement of the X-Flow measurement method, the sample material is
dispersed in a dispersant. The optimal dispersion parameters can be set via the pump speed
and the integrated ultrasonic sound.
The circulation system is closed during the measurement, i.e. the same particles are
transported through the flow cell and the field of view of the cameras repeatedly and thus
measured several times. The duration of the measurement can be set in the CAMSIZER X2
programme. After the measurement, the sample material is drained together with the dispersant
via the outlet in a collecting vessel.
C11.0030
CAUTION
Danger of crushing
Improper change of modules
− During the change of modules (or cartridges) falling components can cause
injuries or bruises.
• Remove the compressed air hose, the cartridge, the collecting tray and
the feed chute before changing the X-Dry module.
• Remove the drain hoses before changing the X-Flow module.
• Grasp the module only at the recessed grips and pull it out without haste.
N14.0023
NOTICE
Device damage
Improper change of modules and/or cartridges
− During the change of modules or cartridges falling components can cause
damage to the device and/or components themselves.
• Grasp the module only at the recessed grips and pull it out without haste
to avoid tilting or falling.
• Use the handle only to remove the cartridge in upwards direction.
47
Operating the Device
L 14 mm 10 mm 4.3 mm 7.2 mm
XL 14 mm 14 mm 6 mm 8 mm
If present, remove the complete gravity nozzle from the X-Fall cartridge by pulling it vertically
out on the stainless steel hopper (FA2).
FA2
FA10
FA9
FA4
FA6
FA5
FA7
FA8
Insert the desired gravity nozzle (FA4) from above in the X-Fall cartridge in such a way, that
the rounded support (FA5) is lowered down the rear guide rod (FA7), and the angular
support (FA6) is fitted over the front guide rod (FA8).
Place the cylinder (FA9) over the gravity nozzle (FA4). Please observe the correct
orientation of the cylinder (the top opening (FA10) is centrally located over the thread in the
gravity nozzle (FA4)).
48
Operating the Device
Screw the stainless steel hopper (FA2) onto the gravity nozzle (FA4).
Loosen the two fastening screws (JE8) to remove the fixation plate (JE9).
If a dispersion nozzle is already present, disconnect the ground cable (JE10) from the
housing of the X-Jet cartridge and remove the complete dispersion nozzle.
JE8
JE9
JE10
JE11
49
Operating the Device
Insert the desired dispersion nozzle from above in the X-Jet cartridge. Make sure that it is
properly seated on the guide pin (JE11).
Connect the ground cable (JE10) with the housing of the X-Jet cartridge.
Place the fixation plate (JE9) with the fastening screws (JE8) on the dispersion nozzle.
Fix the dispersion nozzle by symmetrically tightening the two fastening screws (JE8).
C12.0029
CAUTION
Cutting injuries
Danger caused by glass splitters
− Flow cells may shatter when falling down or being inserted incorrectly.
• Ensure the correct positioning of the flow cell in the mounting before
tightening the flow cell holder.
• Replace damaged flow cells.
• Do not touch glass splitters with your hands.
The following flow cells are available for the X-Flow module:
1)
Flow cell size Gap width Max. particle size
XS 1 mm 150 µm
S 2 mm 300 µm
M (standard) 4 mm 600 µm
1)
The maximum particle size depends on the density of the particles. The listed values refer to a
3
mean density of 2.5 g/cm .
The flow cell must be clean both inside and outside ( Chapter "Cleaning") and should only be
handled with gloves. Contamination can lead to measurement errors.
50
Operating the Device
FL1
FL2
FL3
FL4
FL5
FL7
FL6
Loosen the locking screw (FL1) and open the cover lid (FL2) of the flow cell mount.
If present, remove the flow cell.
Check the correct fit of the two O-rings (FL3) and (FL4) in the cover lid (FL2) and in the
adjustable base (FL5) of the flow cell mount, respectively.
Insert the desired, clean flow cell.
Close the cover lid (FL2) and tighten the locking screw (FL1) firmly.
By the tightening of the locking screw (FL1), the flow cell is slightly raised on the screw's side.
As a result, the lower O-ring does not seal properly on this side (the O-ring only seals correctly
at those places where it is visible through the glass).
51
Operating the Device
In order to correct the position of the flow cell, the cover lid (FL2) must be raised on the side
held by two springs (FL6).
Hold the outlet tube (FL7) with two fingers and pull the cover lid (FL2) briefly upwards.
FL7
FL6
Fig. 32: Correction of the flow cell position by pulling up the cover lid
The flow cell is properly positioned and now sealed completely by the O-ring.
52
Operating the Device
W5.0006
WARNING
W6.0008
WARNING
DB1
DB2
53
Operating the Device
F1.2
F1.1
F1.3
Set the pump speed to 40 % of the maximum power in the edit box (F1.1).
Click on [Set]. The pump is now running at 40 % of its capacity. Alternatively, the slider
(F1.2) can be set to 40 %.
If necessary add more dispersant until the fill level is located just below the overflow outlet
(DB1).
The sensor (DB2) permanently monitors the filling level and indicates with an "x" in the status
section (F1.3) whether the upper or lower filling level is reached. If the upper level is exceeded,
the excess dispersant flows off the overflow outlet (DB1). If the lower level falls below the limit,
bubble formation in the dispersant can occur due to the circulation and thus lead to
measurement errors.
6.6.3 Draining
The X-Flow module can only be drained via the software. The solenoid valve in the X-Flow
module is a "normally closed" valve. Therefore, it is closed when currentless and opens only
with applied voltage. If the basic device is switched off or the X-Flow module is separated from
the basic device, the dispersant including the sample material will remain in the module, as long
as no draining has occurred via the software.
54
Operating the Device
NOTICE The X-Flow module should always be drained and flushed when not used for longer
periods of time.
The drain of the X-Flow module is either performed automatically after the measurement or by
manual control.
Automatic drain:
The automatic drain is set in the task file for the wet measurement ( Chapter "X-Flow task
file".
Manual drain:
Use the main menu function │Extras│X-Flow…│in the software to open the window for
manual control of the X-Flow module. Alternatively, the window can also be accessed by
clicking on the icon.
Click on [Drain]. The solenoid valve opens for ten seconds, and the pump conveys the entire
dispersant through the outlet out of the circulation system.
When using highly flammable materials as dispersant, such as hexane, isopropanol, ethanol,
petrol, acetone or similar, it is to be assumed that the inside of the circulation system should be
classed as zone 0, i.e. a constantly present explosive mix.
Therefore it is necessary to prevent potentially explosive vapours during the measurement from
escaping from the X-Flow module and from entering areas in which the requisite ignition energy
is present.
It is therefore urgently recommended that the managing operator (employer) using the device
assesses the dangers that exist before using corresponding solvents, taking local conditions
into account, as part of a coherent explosion protection concept. If necessary, supplementary
organisational measures should be recorded in writing in an explosion protection document.
55
Operating the Device
This procedure is regulated in the EU under Articles 118 and 118a of Directive 89/391/EEC.
Please observe comparable provisions in other countries outside the EU.
56
Cleaning, Wear and Maintenance
W7.0003
WARNING
C13.0031
CAUTION
Risk of injury
Blown off sample material
− When using compressed air for cleaning purposes dust and remnant of the
sample material can be flung around and injure eyes.
• Always wear safety glasses when cleaning with compressed air.
• Observe the material safety data sheets of the sample material.
N15.0009
NOTICE
57
Cleaning, Wear and Maintenance
Remove persistent contaminations with ethanol or a household glass cleaner and a lint-free
cloth.
58
Cleaning, Wear and Maintenance
JE5
JE13
JE14
JE12
Loosen the knurled screw to remove the stainless steel hopper (JE5) from the venturi nozzle
(JE14).
Loosen the two set screws (JE12) with a 2.5 mm Allen key.
Loosen the eight countersunk screws (JE13) with a 2 mm Allen key. The dispersion nozzle
can now be disassembled into two nozzle halves and the venturi nozzle (JE14).
Clean the individual components with compressed air and a clean, fine brush.
Reassemble the dispersion nozzle after the cleaning. Make sure that all screws are firmly
tightened.
Insert the dispersion nozzle into the X-Jet cartridge as described in Chapter "Changing the
dispersion nozzle".
59
Cleaning, Wear and Maintenance
7.2 Wear
Parts of the suction, such as the corrugated rubber gaiter and the connection to the vacuum
cleaner hose, as well as the venturi nozzle may become worn depending on the frequency of
the X-Jet operation and the sample material. The suction on the back extension and the
dispersion nozzle should be regularly checked for wear and parts of it replaced if necessary.
In X-Flow operation, the two O-rings of the flow cell should be regularly checked for wear and
replaced if necessary.
For spare parts, as well as detailed information on its replacement, please contact your supplier
or get in touch with Retsch Technology GmbH directly.
NOTICE Only use spare parts recommended or supplied by Retsch Technology GmbH.
C14.0013
CAUTION
Personal injury
Improper repairs
− This manual does not contain any repair instructions.
• For safety reasons, repairs may only be carried out by Retsch
Technology GmbH or an authorised representative or by qualified service
technicians.
7.3 Maintenance
7.3.1 Replacing the Fuses
W8.0014
WARNING
NOTICE Depending on the mains supply different fuses are used. The correct electrical
protection is listed on the type plate (V).
60
Cleaning, Wear and Maintenance
For the basic device (M) and the vacuum cleaner (N) two fuses each are located behind the four
protective covers on the backside of the basic device. Fuses can be replaced by trained
qualified personnel.
Open and remove the protective cover by means of a suitable slotted screwdriver.
Replace the defective fuse.
Close the protective cover again.
61
Accessories
8 Accessories
Information on available accessories as well as the respective manuals are accessible directly
on the Retsch Technology GmbH homepage (http://www.retsch-technology.com/) under the
heading "Information & Downloads" of the device.
Information on wear parts and small accessories can be found in the Retsch Technology GmbH
general catalogue also available on the homepage.
In case of any questions concerning spare parts please contact the Retsch Technology GmbH
representative in your country, or Retsch Technology GmbH directly.
62
Disposal
9 Disposal
In the case of a disposal, the respective statutory requirements must be observed. In the
following, information on the disposal of electrical and electronic devices in the European
Community are given.
Within the European Community the disposal of electrically operated devices is regulated by
national provisions that are based on the EU Directive 2002/96/EC on Waste Electrical and
Electronic Equipment (WEEE).
th
Accordingly, all devices supplied after August 13 2005 in the business-to-business area, to
which this product is classified, may no longer be disposed of with municipal or household
waste. To document this, the devices are provided with the disposal label.
Since the disposal regulations worldwide and also within the EU may differ from country to
country, the supplier of the device should be consulted directly in case of need.
rd
This labelling obligation is applied in Germany since March 23 2006. From this date on, the
manufacturer must provide an adequate possibility of returning all devices delivered since
th th
August 13 2005. For all devices delivered before August 13 2005 the end user is responsible
for the proper disposal.
It is the responsibility of the managing operator to exclude the potential thread of third parties
through the dust filter and to make appropriate arrangements.
63
Disposal
It may be necessary to dispose of the dust filter as hazardous waste. The managing operator is
responsible for ensuring that local requirements and regulations are met and adhered to.
Observe thereto the instructions in the material safety data sheets of the measured sample
materials.
64
Index
10 Index
A Configuration file ................................................ 38
Accessories ........................................................62 Confirmation form for the managing operator .... 11
Action instructions ................................................. 7 Connecting the feeder unit ................................. 23
Agglomerates ..........................................41, 46, 47 Connecting the PC ............................................. 34
Ambient temperature ..........................................18 Connecting the vacuum cleaner ........................ 31
Amperage ...........................................................20 Connecting the X-Dry module ............................ 27
Application-technical information .......................... 6 Connecting the X-Flow module .......................... 33
Aux I/O A ............................................................ 35 Copyright .............................................................. 6
Aux I/O B ............................................................ 35 Cyclone ........................................................ 41, 46
B D
Back .................................................................... 44 Degree of protection .......................................... 12
Back extension .............................................24, 32 Depth.................................................................. 13
Back view base ................................................................ 14
basic device ....................................................44 Device designation............................................. 19
Background measurement..................................38 Dimensions ........................................................ 13
Bar code ............................................................. 20 Disclaimer ............................................................ 6
Basic camera ......................................................15 Dispersant .............................................. 41, 47, 55
Base camera link .............................................45 disposal .......................................................... 64
Full camera link ...............................................45 Dispersing bath ............................................ 47, 53
Basic device ..................................................22, 57 Dispersing liquid
cleaning ...........................................................57 disposal .......................................................... 64
C Dispersing noises ............................................... 12
Calibration ...........................................................36 Dispersion nozzle............................................... 41
not OK ............................................................. 38 assembly ........................................................ 59
OK ................................................................... 38 cleaning .......................................................... 59
performing .......................................................38 installation ...................................................... 49
Calibration record ...............................................38 sizes ............................................................... 49
Calibration reticle ................................................36 Dispersion parameters ....................................... 47
cleaning ...........................................................57 Disposal ............................................................. 63
inserting .....................................................36, 37
Disposal label ............................................... 20, 63
Camera unit ........................................................43
Disposal regulations........................................... 63
Capacity .............................................................. 20
Dosage ............................................................... 45
CE marking .........................................................20
Drain
Changing the dispersion nozzle .........................49 automatic ........................................................ 55
Changing the flow cell.........................................50 manual ............................................................ 55
Changing the gravity nozzle ...............................48 Draining .............................................................. 54
Channel 0 ...........................................................35 Dry dispersion measurement ....................... 45, 46
Channel 1 ...........................................................35 Dust filter
Channel 2 ...........................................................35 disposal .......................................................... 63
Channel 3 ...........................................................35 Dust protection cap ............................................ 31
Cleaning .............................................................. 57 DVI interface ...................................................... 34
Complaints ..........................................................17 Dynamic digital image analysis .......................... 15
Compressed air ..................................................46 E
Compressed air dispersion .................................41 Electrical connection .......................................... 19
Compressed air dispersion measurement ..........41 Electromagnetic compatibility ............................ 13
Compressed air supply .......................................14 EMC ................................................................... 13
Compressed air volume ......................................14 Emissions ........................................................... 12
Condensation ......................................................18 Equivalent continuous sound level .................... 13
65
Index
66
Index
67
Index
68
69
70
Copyright
© Copyright by
Retsch Technology GmbH
Retsch-Allee 1-5
D-42781 Haan
Germany