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Visualisation of Oil Recovery by Water Alternating Gas (WAG) Injection Using High
Pressure Micromodels - Water-Wet System
M. Sohrabi, G.D. Henderson, D.H. Tehrani and A. Danesh, Department of Petroleum Engineering, Heriot-Watt University
performance and hydrocarbon recovery prediction, needed for pictures and the recovery data obtained by the experiments
accurate economic evaluation. To achieve this, good reasonably well, then it can be confidently used to simulate
simulation incorporating proper reservoir fluid and rock and obtain the three-phase relative permeability and capillary
description is needed. This requires accurate sets of relative pressure functions, using realistic reservoir rock and fluid data
permeability functions for each fluid phase and capillary in three-dimensional space.
pressures, in a three-phase fluid flow regime. But it is
impractical to measure these for all the different rock types Experimental Facilities
and fluids present in a reservoir and describe them in terms of A high pressure micromodel rig is being used to perform the
IFT which, itself is a function of fluid composition and WAG experiments at pressures of up to 6000 psia and at a
pressure. The approach we have adopted at Heriot-Watt U. is temperature of 100 °F. It is shown schematically in Fig. 1.
to develop a 3-phase 3-D mathematical network simulator, The rig consists of the following major parts:
which has in it all the significant physical flow processes High Pressure Fluid Storage Vessels. Three high-pressure
involved in WAG injection, formulated as accurately as stainless steel vessels are used to store the injection fluids and
possible. But to gain confidence that such a simulator can one to collect produced fluids from the micromodel. All the
indeed reflect physics of the flow realistically, we need to test vessels are pressure rated to 6000 psia.
it against some actual physical experiments that involve the Constant Temperature Fluid Storage Chamber. This
flow of all the three phases in a process that closely mimics chamber is used as a constant temperature oil bath to maintain
the WAG injection in porous media. We have designed a the fluids in the fluid storage vessels, and all the necessary
micromodel system in which we can perform the actual WAG fluid path lines and fittings, at the constant test temperature of
injection, observe and record the flow processes and measure 100 °F.
the model wettabilities, fluid saturations and recoveries. To Constant Temperature Micromodel Housing Chamber.
enable us to magnify and view the pore scale images and to This is similar to that of the fluid storage chamber and is used
analyse the fluid flow, we have had to use 2-D glass to maintain the micromodel at constant temperature equal to
micromodels and to use model fluids with precisely known the temperature of the test fluids.
properties. Although the results will not be directly applicable Low Rate Pumps. Two accurate low rate pumps are used to
to real reservoirs, they can be used to verify the accuracy of control fluid flow through the micromodel. The rates of
the predictions made by our network model simulator. We injection and production range from a low of 0.01 cm3/h to a
will run the pore scale simulator to predict the fluid maximum of 100 cm3/h. With the micromodel that was used
distributions and the recoveries for a given set of pore in the set of experiments reported here, 0.01cm3/h is
geometry, wettability and fluid properties. If these agree with equivalent to an estimated velocity of about 1.2 m/d for single-
those observed and measured in the micromodel, we shall then phase flow.
have enough confidence, to operate it with real reservoir fluids Computer Controlled Linear Drive System. A computer
and rock properties in 3-D mode, to calculate the required pore controlled linear drive system is used in the tests, which
scale relative permeability and capillary pressure functions. allows a magnifying camera to be positioned automatically at
These will later be upscaled for use in the numerical reservoir any part of the micromodel, and sequentially or continuously
scale simulation. We have performed a series of WAG sweep the micromodel for video recording. The camera is
experiments with water-wet, oil-wet and mixed-wet systems. capable of working at a magnification of up to 400 times. Fig.
This paper presents only the results of our experiments with 2 shows the optical system of the rig.
water-wet models. The results for other wettabilities and the Glass Micromodels
description of the network model simulator will be presented A two-dimensional pore structure is etched onto the surface of
in separate papers. a glass plate, which is otherwise completely flat. A second
glass plate is then placed over the first, covering the etched
Objective pattern and thus creating an enclosed pore space. This second
The objective of the current micromodel studies is to improve plate, the cover plate, has an inlet hole and an outlet hole
our understanding of the physical principles underlying such drilled at either end, allowing fluids to be displaced through
processes in the reservoir and to develop a network model the network of pores (Fig. 3). Because the structure is only
simulator that can produce complex three-phase relative one pore deep, and the containing solid walls are all glass, it is
permeability and capillary pressure functions. Observing and possible to observe the fluids as they flow along the pore
recording the fluid flow behaviour within the micromodel channels and interact with each other. It is also possible to
during the WAG injection process will help to achieve this. observe how the geometry of the pore network affects the
The video record of the fluid displacements will be used to patterns of flow and trapping.
obtain qualitative and quantitative information on three phase
fluid flow during WAG injection. These will then be used to Test Fluid
compare with the results of the network model, which will The equilibrated fluids used in the experiments consisted of
attempt to simulate the same processes, using the micromodel distilled water, n-decane and methane. To distinguish between
fluids and geometrical data. If the simulated results match the the liquid hydrocarbon and the aqueous phase, the colour of
VISUALISATION OF OIL RECOVERY BY WATER ALTERNATING GAS (WAG) INJECTION USING HIGH
SPE 63000 PRESSURE MICROMODELS - WATER-WET SYSTEM 3
the n-decane was changed to red using a hydrocarbon soluble micromodel was used for saturation and recovery calculations.
dye (Sudan Red), and similarly, the colour of the water was As soon as oil injection was stopped at the bottom triangle of
changed to blue using a water soluble dye (Methyl Blue). the micromodel, a spontaneous imbibition of water into the
Both the blue water and the red n-decane were filtered using micromodel was observed. The volume of the imbibed water
fine filter papers to remove any undesolved dye particles. was, however, very small. The model was then waterflooded
Fluid Preparation. Filtered blue water and methane were at a low rate of 0.01 cm3/h from the base to establish the
brought into equilibrium at the desired pressure and waterflood residual oil saturation (Sorw). This rate corresponds
temperature. The same procedure was followed for the to a capillary number of 2.52E-7, using single-phase flow area,
equilibration of gas and oil. The solubility of oil in water was and 5.04E-7 for two-phase flow area. The magnitude of
considered to be negligible (at 500 psia and 100 oF). capillary number indicates a capillary dominated flow regime,
Fluid Properties. The equilibrium properties of the water, n- which is consistent with the observations. Water was
decane, methane system at 500 psia and 100 °F and the effect observed to flow mostly through the sharp corners of the pores
of dye, where shown, are estimated as follows: (as can be visualised in the corners of a square tube). This will
Density/ g.cm-3 be referred to as ‘corner filament flow’. The water filaments
2 19,20
Water (H O+C1+dye) 1.0026 were seen to thicken progressively leaving oil filaments in the
Oil (nC10+C1+dye) 21 0.7062 middle of pore bodies and finally causing oil snap off at some
Gas (C1+nC10) 21 0.0209 pore throats. The fluid distribution in the micromodel at the
end of water flooding is shown in Fig. 6. The whole flow
Viscosity/ mPa.s process was recorded on video, and still pictures of the final
Water (H2O +C1+ dye) 19 0.658 fluid distributions were taken digitally and stored in computer.
Oil (nC10+C1+dye) 23,21 0.597 Fig. 7 is a magnified image of a section of the micromodel at
Gas (C1+nC10) 21,23 0.010 the end of primary drainage of water (oil injection through
water saturated micromodel), which demonstrates the relative
Interfacial Tension/mNm-1 position of the wetting phase (blue water) and non-wetting
22
Gas/Oil 15 phase (red oil), in a strongly water-wet micromodel. The
Gas/Water26 65 small pores and the dead-end pores are mostly occupied by
Oil/Water26 41 water. The direction and the shape of the water-oil interfaces
are good indication of strongly water-wet conditions. Also
So/w.g = Spreading Coefficient of oil over water = + 9 mNm-1.
some relatively large pores in Fig. 8 are filled with water, as
these pores are surrounded by smaller pore throats from which
The effect of dye on density and viscosity of the liquids at
water could not be displaced by the oil, because its pressure
micromodel conditions of 100 oF and 500 psia has been
did not exceed the oil-water capillary pressure. Fig. 8 shows a
calculated20. The positive value of the spreading coefficient
magnified image of the same section of the micromodel at the
indicates that there will always be a visible layer or a film of
end of the waterflood.
oil spread between gas and water. The resolution of the
Comparison of Figs 7 and 8 highlights that during
images does not permit the viewing of the thin oil films, which
waterflooding oil was displaced by corner filament flow of
can be on the order of one nanometer across25.
water rather than by a piston-like displacement. The slow
thickening of water filaments at the sides and corners of oil
Test Procedure
filled pores during water flooding was a consequence of a
The following procedure was followed for all the tests
capillary dominated flow regime.
reported. Initially, the micromodel was saturated with clear
Each WAG cycle begins with gas injection and ends with
distilled water and pressurised to 500 psia and subsequently
water injection. Five cycles of WAG injection were
displaced with blue live water, equilibrated with gas at 500
conducted. In each cycle, the injection of gas or water
psia and 100 oF. To simulate the primary drainage (initial
continued until no further oil production or change in fluid
migration of oil into the water bearing porous medium),
distribution occurred. To distinguish the colourless gas from
equilibrated oil (red n-decane), was injected from the top of
the colourless glass (resembling grains in a natural porous
the vertical micromodel, and continued until oil reached the
medium), gas was digitally coloured in yellow, using an image
base of the micromodel. To avoid oil getting into the lower
analysis computer program. Fig. 9 shows the fluid
pipes containing the water and gas phases, the oil flood was
distribution in the micromodel after the first cycle of gas
stopped at the bottom of the micromodel. Fig. 4 shows an
injection, with the blue, red and yellow colours representing
example of a section of the micromodel when 100% saturated
water, oil and gas respectively. Due to the relatively low
with equilibrated blue water, with Fig. 5 showing the connate
interfacial tension between gas and oil (15 mNm-1) and
water saturation, established after oil injection. In both cases
adverse viscosity ratio (0.017), gas has channelled mainly
the micromodel was scanned vertically in 10 separate sections.
through the oil occupied pores of the micromodel. At the end
In these Figures, and throughout this report, only the image of
of gas injection, water injection commenced again at the same
the middle section is presented, although the entire
rate of 0.01 cm3/h (~ 1.2 m/d). During water injection, corner
4 M. SOHRABI, G.D. HENDERSON, D.H. TEHRANI, A. DANESH SPE 63000
flow of water resulted in water filaments surrounding the gas cycle of gas injection is different from that of the first cycle.
occupied pores and thickening until the gas blobs became This was also observed for the first and second cycles of water
unstable and finally collapsed. The snap-off of the gas phase injection. Comparison of Figs. 9 to 14 shows that the fluid
occurs as a result of capillary competition between the distribution within the micromodel changed each time a new
different phases. Fig. 10 shows the fluid distribution in the fluid was injected. However, further change in fluid
micromodel after the water injection period of the first cycle. distribution diminishes as the WAG injection proceeds. After
The fragmentation of the gas blobs is clearly observed. the third WAG cycle no significant change of fluid
Fig. 11 shows the fluid distribution in the model after the distribution is observed to take place within the micromodel.
second gas injection, and comparison with Fig. 9, reveals that Fig. 15 depicts the recovery of additional oil after
more pores have been invaded by gas. Fig. 12 shows the waterflooding, attributable to WAG injection. The initial oil
micromodel after water injection period of the second cycle, saturation, Soi was 47% of the pore volume and the residual oil
and water has again resulted in further gas snap-off and fluid saturation (Sorw) at the end of initial waterflood in this
redistribution. Alternating gas and water injection continued experiment was 25% PV, i.e., 53% of the initial oil in place.
until five cycles were completed. Five cycles of WAG injection produced 21.7% of that
Figs. 13 and 14, show the results of the fifth WAG cycle. A remaining oil, which is 11.5% of initial oil in place. The extra
sequence of events similar to the previous WAG cycles oil recovered after two cycles of WAG was 18.8% of Sorw,
occurred. Comparison of Fig. 14 with Fig. 9 shows that more which is 10% of initial oil in place. This shows that the
gas has been trapped and more oil has been recovered. majority of the benefit of WAG injection has come after the
Fig. 15 depicts the recovery of oil during the test with the first two cycles. It should, however, be remembered that these
vertical axis showing the percentage of oil recovered, at each are the results of an experiment carried out with a 2-D water-
stage of the experiment, as percentage of the initial waterflood wet micromodel. The figures are not directly applicable to
residual oil. This Figure shows that the majority of the real field conditions, but can be used to verify the validity of
additional oil (some 14%) is recovered during the first two the network simulator, when it is also run with a 2-D water-
cycles and as the result of five cycles of alternating injection wet system. Relative permeability functions applicable to real
of gas and water a total of 15% of the remaining oil, after field conditions will be obtained later, using the network
water flooding, has been produced. simulator in 3-D and 3-Phase mode with realistic rock and
fluid data.
Discussion
During the initial waterflood, as water was the wetting phase Conclusions
and the rate of water injection was well within capillary The results of the reported experiment, which was performed
dominated regime, water flowed in the corners of the pores in in strongly water-wet glass micromodel, can be summarised as
the form of filaments surrounding the oil present in the larger follows:
pore bodies. These water filaments were seen to thicken 1. During the initial waterflood, water advances in pores by
progressively leaving oil filaments in the middle of pores and the process of ‘corner filament flow’. The water filaments,
finally causing oil snap off at some pore throats27. Fig. 16 that surround the oil present in the larger pore bodies, thicken
shows how the wetting phase can imbibe in the sharp corners progressively and leave oil filaments in the middle of pores
of a square tube. The micromodel pores, etched by and finally cause oil snap off at the pore throats.
hydrofluoric acid on a glass, are not exactly in square shape, Consequently, during water flooding oil production is
but they do have some sharp corners in which the wetting controlled by filament flow rather than by piston-like
phase can advance. The oil recovery by waterflood occurred displacement at the pore level.
as the result of this corner filament flow of water rather than 2. The positive spreading coefficient, in the reported
by piston-like displacement. experiment, results in a layer and or a film of oil to be always
As the IFT between gas and oil is less than that between gas present between gas and water, in pores that contain all three
and water, when faced with pores of equal radius, gas prefers phases. During gas injection, when gas is faced with pores of
to enter those pores filled with oil. The invasion of oil filled equal radii, it preferentially enters the oil filled pores, because
pores by gas causes a small bank of oil to move ahead of gas gas has lower IFT with oil than it has with water. The invasion
front. The oil flowing ahead of the gas is added to the oil of oil filled pores by gas causes a small bank of oil to move
already present in those pores, resulting in an improvement in ahead of gas front causing some redistribution by thickening
the oil mobility. The oil recovery by gas injection alone, of the waterflood residual oil. This increases the mobility of
however, is very small, in the order of 6% of the water flood oil in presence of water, in those pores, resulting in improved
residual oil. During the subsequent water injection, water oil recovery.
invades the gas filled pores. Consequently, the gas channels 3. During the subsequent water injection, gas channels
are observed to become narrower as the water filaments grow, become narrower as the water filaments grow in thickness, and
and finally the gas becomes fragmented due to snap off which finally due to the interplay of capillary forces and local gas
takes place at some pore throats. After switching from water pressure fluctuations, gas blobs snap off at many of the pore
injection to gas injection, some more pores are invaded by gas. throats and become fragmented.
Thus the fluid distribution in the micromodel for this second 4. By injecting gas and water alternately more oil can be
VISUALISATION OF OIL RECOVERY BY WATER ALTERNATING GAS (WAG) INJECTION USING HIGH
SPE 63000 PRESSURE MICROMODELS - WATER-WET SYSTEM 5
produced than would otherwise be produced by water or gas 11. Larsen, J.K. and Skauge, A. “Simulation of the Immiscible
injection alone. WAG Process Using Cycle-Dependent Three-Phase Relative
5. The major portion of the improved oil recovery is Permeabilities”, SPE 56475, SPE Annual Technical Conference
obtained only after a few cycles of WAG injection. In the and Exhibition, Houston, Texas 3-6 Oct 1999.
12. Christensen, J. R., Stenby, E.H. and Skauge, A. “Compositional
reported experiment (water-wet system) this occurred after the and Relative Permeability Hysteresis Effects on Near Miscible
second cycle.(Fig. 15) WAG”, SPE/DOE Improved Oil Recovery Symposium, Tulsa
Oklahoma, 19-22 April 1998.
Nomenclature 13. Cullick, A.S., Lu, H.S., Cohen, M.F., Watson, J.P. and Jones,
IFT = interfacial tension L.G. "Water-Alternating-Gas May Improve Gas-Condensate
Sorw = residual oil saturation to waterflood Recovery", SPERE, V. 8, No. 3, pp 207-213, Aug. 1993.
Sori = residual oil saturation after cycle ‘i’. 14. Nguyen, T.A. and Farouq Ali, S.M. "Immiscible Carbon
So/w.g = spreading coefficient of oil over water Dioxide Floods, Using Impure Gas in the WAG Mode", 44th
for a water wet solid surface. Annual CIM Pet. Soc. Tech. Mtg., Calgary, Canada, 9-12 May
1993.
Acknowledgements 15. Mattax, C. C. and Kyte, J. R., “Ever see waterflood?”, Oil and
The WAG project at Heriot-Watt U. is equally sponsored by: Gas Journal, 59:115-128 (1961)
The UK Department of Trade and Industry, BP Amoco plc, 16. Oren, P.E. and Pinczewski, W.V. “The effect of film flow on the
mobilisation of waterflood residual oil by gas flooding”, 6th
Marathon International (GB) Ltd, Mobil (North Sea) Ltd, European IOR Symposium,Stavanger, Norway, May 21-23,
Norsk Hydro a.s.a, SAGA Petroleum a.s.a, and Total Oil 1991.
Marine plc, and this support is gratefully acknowledged. 17. Oren, P.E., Billiotte, J. and Pinczewski, W.V. “Mobilisation of
waterflood residual oil by gas injection for water-wet conditions,
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WAG Field Experience”, SPE 39883, SPE International WAG Injection: Micromodel Experiments and Network
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460-468. System”, Industrial and Engineering Chemistry, Vol.34, No. 12
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Pilot In the Lower Brent Formation at the Gullfaks Field", 7th 22. Stegemeier, G. L., Pennington, B. F., Brauer, E. B. and Hough,
EAPG IOR Europe, Moscow, Russia, 27-29 October 1993, pp E. W., “Interfacial Tension of the Methane-Normal Decane
460-468. System”, SPEJ, Sept. 1962, pp. 257-260.
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Water-Alternating-Gas Injection at Kuparuk River Unit, North Viscosities of Reservoir Fluids from Their Compositions”, JPT,
Slope, Alaska", 69th Ann. SPE Tech. Conf., New Orleans, 25-28 October 1964, pp 1171-76.
Sept. 1994. 24. MCdougall, S. R., Dixit, A.B. And Sorbie, K. S. “Network
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Alternating-Gas Pilot Evaluation for the Snorre Field", 7th the Developments in Petrophysics Conference, 19-20 September
EAPG IOR Europe, Moscow, Russia, 27-29 October 1993, pp 1995, Royal Geological Society, London. To be published in
460-468. Royal Geological Society Special Publication.
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1992.
6 M. SOHRABI, G.D. HENDERSON, D.H. TEHRANI, A. DANESH SPE 63000
PT 3 15
gas
14 charging
16
13 12
PT 4
micro
model return
retract
vesel water oil gas
fluid
PT 5
Micromodel tank
PT 1
Pressure transducers
8 7 4 3 2
PT1 inj. pump 6 5 1
PT2 ret. pump
PT3 MM outlet Fluid Storage Tank
PT4 MM inlet
PT5 Overburden
9 injection pump
pump
pump charging
lines
PT 2
10
11 retract pump
Moving
Directions
Light source
Camera
Monitor Monitor
Micromodel
Inlet Outlet
Cover plate
Fig. 4-100% water saturation Fig. 5-Primary drainage of water Fig. 6-Initial waterflood
Fig. 7-Water/oil distribution before waterflood Fig. 8-Water/oil distribution after waterflood
Fig. 9-First cycle gas injection Fig. 10-First cycle water injection Fig. 11-Second cycle gas injection
Fig. 12- 2nd cycle water injection Fig. 13-Fifth cycle gas injection Fig. 14-Fifth cycle water injection
8 M. SOHRABI, G.D. HENDERSON, D.H. TEHRANI, A. DANESH SPE 63000
25
20
Oil Recovery, %Sorw
15
10
0
waterflood
2 gas
3 gas
5 gas
1 water
2 water
3 water
4 water
5 water
1 gas
4 gas
Fig. 15-Oil recovery at each stage of the experiment as percentage of initial waterflood trapped oil
(c)
(d)
(a) (b)
Fig. 16 - Corner Filament Flow in a Square
Water-Wet Tube. (a) – Profile along the
diagonal line. (b) – Profile along the middle
of the tube parallel with sides. (c) – Water in
the corners on top of the tube. (d) – Water in
the corners on top of the water column.