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FINAT TECHNICAL HANDBOOK

Test methods
9th Edition
FINAT
TECHNICAL
HANDBOOK
Test Methods - 9th edition

Copyright © 2014 by FINAT, The Hague, The Netherlands. All rights reserved.

No part of this publication may be translated, reproduced, stored or transmitted, in any form or by any
means, electronic or mechanical, photocopying, recording or otherwise, without the prior written permission
of the publisher.

FINAT
The Hague, May 2014
PREFACE
preface to the 9th edition

It is my pleasure to herewith present you with the 9th edition of the Technical
Handbook. The Handbook is globally acknowledged as being the authoritative
benchmark on test procedures for adhesive labels. The FINAT test methods
described in the Handbook are used to evaluate label stock and frequently
serve as a basis for specifications. Since the first edition 30 years ago the
Technical Handbook has been continually revised. New test methods were
added, existing ones revised and obsolete ones deleted.

This edition features two new test methods (FTM 28 and FTM 29) on bleeding
through paper and scratch resistance of an UV ink film on different print
materials, and also Section 2.10 on the light fastness of printing ink. A number
of proven test methods are now much easier to understand as some graphic
material has been added to them.

At this juncture I should like to thank all members of the Technical Committee
for their excellent contributions to the design, translation and revision of the
content. I am particularly grateful to the members of the Subcommittee on
Test Methods who are the driving force behind this edition and take the main
responsibility for it. We owe the quality and high acceptance of the FINAT test
methods all over the world to the composition of the Technical Committee
where specialists from the entire adhesive label industry meet. Although
English is the globally accepted language of the industry we shall nonetheless
try to translate the Technical Handbook into as many languages as our
resources allow us to do.

Hans Lautenschlager
Chairman of the Subcommittee on Test Methods

FINAT TECHNICAL HANDBOOK 2014 |

5
CONTENTS
section 1 | finat test methods
Method Description Construction Test relevant to

FTM 1 Peel adhesion (180°) at 300 mm per minute Face stock Adhesion 8
FTM 2 Peel adhesion (90°) at 300 mm per minute Face stock Adhesion 10
FTM 3 Low speed release force Laminate Delamination 12
FTM 4 High speed release Force Laminate Matrix stripping 13
FTM 5 Accelerated ageing – Extended storage Laminate Ageing 15
FTM 6 Resistance to ultra-violet light Laminate Ageing 16
FTM 7 Silicone Coat Weight by energy-dispersive
X-ray fluorescence spectrometry Liner Coating quality 18
FTM 8 Resistance to shear from a standard surface Face stock Adhesion 20
FTM 9 Loop’ tack measurement Face stock Adhesion 22
FTM 10 Quality of silicone coated substrates for
self-adhesive laminates: release force Liner Dispensing 24
FTM 11 Quality of silicone coated substrates for
self-adhesive laminates: subsequent adhesion Liner Silicone cure 26
FTM 12 Adhesive coat weight Face stock Coating quality 28
FTM 13 Low temperature adhesion Face stock Adhesion 29
FTM 14 Dimensional stability Face stock Stability 31
FTM 15 Surface tension of plastic films Face stock Printing 33
FTM 16 Chemical resistance – Spot method Face stock Stability 35
FTM 17 Chemical resistance – Immersion method Face stock Stability 36
FTM 18 Dynamic shear Face stock Adhesion 38
FTM 19 Recycling compatibility of self-adhesive labels Face stock Recycling 40
FTM 20 Fluorescence and whiteness Face stock Printing 41
FTM 21 Ink adhesion - basic Face stock Printing 43
FTM 22 Ink adhesion - advanced Face stock Printing 45
FTM 23a Testing for die-strike on paper Laminate Dispensing 46
FTM 23b Testing for die-strike on clear filmic liners Laminate Dispensing 48
FTM 24 Mandrel hold Face stock Adhesion 50
FTM 25 Evaluation of the silicone coverage of coated
papers by use of a water based stain test Liner Coating quality 52
FTM 26 Wash-off paper and film labels Face stock Adhesives 55
FTM 27 Ink rub test for UV printed labels ink surface
against substrate or ink surface Laminate Printing 56
FINAT TECHNICAL HANDBOOK 2014 |

FTM 28 Evaluation of bleeding through paper Face stock Printing 58


FTM 29 Scratch resistance of an UV ink film on
different print materials Face stock Printing 60

6
section 2 | guidelines

2.1 Recommended joins in self-adhesive laminates for roll labels 62


2.2 Processing recommendations 63
2.3 Surfaces requiring caution 65
2.4 Safety guide for users of self-adhesive label stock products 66
2.5 Handling and storage of label stock throughout printing and converting 68
2.6 Qualitative Adhesion testing 69
2.7 Adhesives 70
Nomenclature for adhesives used in self-adhesive laminates
2.8 Unwind roll chart 71
2.9 Recommendations regarding static electricity 72
2.10 Advices about light fastness of printing inks and light exposition 74

section 3 | test equipment



3.1 Standard FINAT Test Roller 76
3.2 Automatic Rolling Device 76
3.3 Sources of Test Equipment 76
3.4 Testing institutes 88
3.5 tesa test tapes product information and worldwide addresses
®
95

Note from the editor


FINAT TECHNICAL HANDBOOK 2014 |

Although the 29 FINAT Test Methods described in this publication have been prepared with the utmost care and
accuracy, it should be noted that the safety, efficiency and performance of these test methods and associated
procedures is the responsibility of the end-user. FINAT cannot be held liable for any loss, damage or injury resulting
from their application. Furthermore, the test methods and associated information do not in themselves imply any
specification of performance relating to the materials under test.

7
FTM1
peel adhesion (180°) at
300 mm per minute

scope
This test method is designed to quantify the permanence
of adhesion or peel ability of self-adhesive pressure
sensitive materials.

definition
Peel adhesion is defined as the force required to remove
pressure sensitive coated material, which has been applied
to a standard test plate under specified conditions from the
plate at a specified angle and speed.

Adhesion is measured 20 minutes and 24 hours after
application, the latter being considered as the ultimate
adhesion. procedure
Remove the backing material from each strip and place the
test equipment adhesive coated facing material, adhesive side down, on to
a clean test plate using light finger pressure.
A tensile tester or similar machine, capable of peeling a Roll twice in each direction with the standard FINAT test
laminate through an angle of 180° with a jaw separation roller at a speed of approximately 10 mm per second to
rate of 300 mm per minute with an accuracy of ± 2%. obtain intimate contact between the adhesive mass and
the surface.
Test plates made of float glass or similar plate glass.
After applying the strips to the test plate, leave for a period
A standard FINAT test roller. of 20 minutes before testing. Repeat the procedure with
a second set of strips and leave for a period of 24 hours
before testing.
test pieces
Fix the test plate and strip in the machine so that the angle
These should be strips taken from a representative sample of peel is 180°. Set the machine at 300mm per minute
of material. The strips should be 25 mm wide and have jaw separation rate. Carry out the test taking at least five
a minimum length of 175 mm in the machine direction. readings at 10 mm intervals from the centre section of each
The cuts should be clean and straight. At least three strips test strip.
should be taken from each material sample. Average the five or more readings for each strip.

test conditions
FINAT TECHNICAL HANDBOOK 2014 |

Temperature 23°C ± 2°C, 50% RH ± 5% RH.


The test sample or test strips and test panels should be
conditioned for not less than 4 hours before testing.

8
results Alternative methods which remove contamination
properly can be adopted e.g. ultrasonic cleaning.
Peel adhesion (180°) is expressed as the average result for
the strips tested in Newton per 25mm width for either 20 Prior to use, the cleaned plates should be left for 4
minutes or 24 hours application time. hours under standard test conditions. Care should be
taken to handle clean plates by the edge only.
Failure Description Code
2. Alternative surfaces to plate glass can be used such as
CP Clear Panel - no visible stain on panel. stainless steel (example: AFERA1 quality stainless steel
PS Panel Stain - discoloration of test area, but no plates), aluminium or polymeric substrates, but this
tacky residue of adhesive on both the panel and must be clearly stated alongside the results.
the front material.
CF Cohesive Failure - the adhesive film is split during 3. If adhesion values are required when paper tear has
the test, leaving residue of adhesive on both the occurred, then this test can be conducted at lower jaw
panel and the front material. separation rates quoting the latter against the results.
AT Adhesive Transfer - the adhesive separates clearly
from the front material, leaving adhesive film on 4. Conversion 1kgf- = 9.81 N
the test panel.
The approximate extent of transfer should be Issued October 1985
quoted as percentage. Revised March 1999
PT Paper Tear - the adhesive force exceeds the Revised May 2001
strength of a paper facing material. The results Revised February 2014
quoted should be the maximum reached before
the paper tears.

notes
1. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:

• Diacetone alcohol non-residual,


technical grade or better
• Methyl Ethyl Ketone (MEK)
• Acetone
• Methanol 95%
• n-Heptane
• Ethyl Acetate

The cleaning material must be absorbent, e.g. surgical


gauze, cotton wool or tissue. To be suitable, materials
must be lint-free during use, absorbent, contain no
additives that are soluble in the solvents listed above, 1
The AFERA defines stainless steel test substrates as:
FINAT TECHNICAL HANDBOOK 2014 |

and made exclusively from virgin materials. A 50 mm by 125 mm no less than 1.1 mm thick stainless
steel 1.4301 in accordance with the 2R quality defined in
Dispense one of the solvents listed above on to the EN10088-2 having a bright annealed finish. The surface
panel, wiping it to dryness with fresh absorbent roughness height shall be (50 ± 25) nm arithmetical average
cleaning material. Repeat for a total of three washes deviation from the mean line. Panels showing stains,
with the solvent. Final wipe shall be with MEK or discoloration, or many scratches are not acceptable.
acetone. More details can be found in the AFERA test method manual.

9
FTM2
peel adhesion (90°) at
300 mm per minute

scope test conditions


This test method differs from FTM 1 in that it can allow 23°C ± 2°C and 50% RH ± 5% RH
the end user to compare the repositionability of different The test sample or test strips and test panels should be
laminates. Measuring peel adhesion at 90° normally gives a conditioned for not less than 4 hours before testing.
lower value than at 180° and allows values to be measured
for materials normally giving paper tear.

definition
Peel adhesion is defined as the force required to remove
pressure sensitive coated material, which has been applied
to a standard test plate under specified conditions, from
the plate at a specified angle and speed. Adhesion is
measured 20 minutes and 24 hours after application, the
latter being considered as the ultimate adhesion.

test equipment
A tensile tester or similar machine capable of peeling a procedure
laminate through an angle of 90° with a jaw separation
rate of 300 mm per minute and an accuracy of ± 2%. The Remove the backing material from each strip and place
apparatus must be equipped in a manner which ensures the adhesive coated facing material, adhesive side down,
that the test plate can move freely in a horizontal position on to a clean test plate using light finger pressure. Roll
when the pressure sensitive material is removed in order to twice in each direction with the standard FINAT test roller
maintain an angle of peel of 90°. at a speed of approximately 10 mm per second to obtain
intimate contact between the adhesive mass and the
Test plates made of float glass or similar plate glass. surface.

A standard FINAT test roller. After applying the strip to the test plate, leave for a period
of 20 minutes before testing. Repeat the procedure with
a second set of strips and leave for a period of 24 hours
test pieces before testing.

These should be strips from a representative sample of Fix the test plate and strip into the horizontal support
material. The strips should be 25 mm wide and have a which has been secured into the bottom jaw of the
minimum length of 175 mm in the machine direction. tensile tester. Set the machine at 300 mm per minute
The cuts should be clean and straight. At least three strips jaw separation rate. Carry out the test taking at least five
should be taken from each material sample. readings at 10 mm intervals from the centre section of the
test strip. Average the five or more readings for each strip.
FINAT TECHNICAL HANDBOOK 2014 |

10
results Alternative methods which remove contamination
properly can be adopted, e.g. ultrasonic cleaning.
Peel adhesion (90°) is expressed as the average result for
the strips tested in Newtons per 25 mm width for either 20 Prior to use, the cleaned plates should be left for 4
minutes or 24 hours application time. hours under standard test conditions. Care should be
taken to handle clean plates by the edge only.
Failure Description Code
CP Clear Panel - no visible stain on panel. 2. Alternative surfaces to plate glass can be used such as
PS Panel Stain - discoloration of test area, stainless steel(example: AFERA1 quality stainless steel
but no tacky residue. plates),aluminium or polymeric substrates, but this
CF Cohesive Failure - the adhesive film is split during must be clearly stated alongside the results.
the test, leaving residue of adhesive on both the
panel and the front material. 3. If adhesion values are required when paper tear has
AT Adhesive Transfer - the adhesive separates cleanly occurred then this test can be conducted at lower jaw
from the front material, leaving adhesive film on separation rates quoting the latter against the results.
the test panel.
The approximate extent of transfer should be 4. Conversion 1 kgf = 9.81 N
quoted as percentage.
PT Paper Tear - the adhesive force exceeds the Issued October 1985
strength of a paper facing material. The results Revised March 1999
quoted should be the maximum reached before Revised May 2001
the paper tears. Revised February 2014

notes
1. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:

• Diacetone alcohol non-residual, technical grade or


better
• Methyl Ethyl Ketone (MEK)
• Acetone
• Methanol 95%
• n-Heptane
• Ethyl Acetate

The cleaning material must be absorbent, e.g. surgical


gauge, cotton wool or tissue. To be suitable, materials
must be lint-free during use, absorbent,
contain no additives that are soluble in the solvents
listed above, and made exclusively from virgin 1
The AFERA defines stainless steel test substrates as:
materials. A 50 mm by 125 mm no less than 1.1 mm thick stainless
FINAT TECHNICAL HANDBOOK 2014 |

steel 1.4301 in accordance with the 2R quality defined in


Dispense one of the solvents listed above on to the EN10088-2 having a bright annealed finish. The surface
panel, wiping it to dryness with fresh absorbent roughness height shall be (50 ± 25) nm arithmetical average
cleaning material. Repeat for a total of three washes deviation from the mean line. Panels showing stains,
with the solvent. Final wipe shall be with MEK or discoloration, or many scratches are not acceptable.
acetone. More details can be found in the AFERA test method manual.

11
FTM3 low speed release force

scope test conditions


This test method allows the end user to determine the Place the strips under test between two flat metal or
force required to separate the release backing from the glass plates and keep for 20 hours at 23°C ± 2oC under a
pressure sensitive adhesive coated face material. It may pressure of 6.86 kPa (70 g/cm2) to ensure good contact
be used in the preliminary evaluation of the conversion between the release material and the adhesive. Up to 20
aspects of the laminate, - very low values may create label strips can be kept between the plates. After storage in this
fly during conversion or application - high values may manner, take the strips from between the plates and keep
produce web break when skeleton stripping die cut labels for not less than 4 hours at the standard test conditions of
or dispensing failure during automatic application. 23 ± 2°C and 50% RH ± 5% RH.

definition procedure
Low speed release force is defined as the force required Fix each strip to the plate by means of a double sided
to separate a pressure sensitive adhesive coated material tape (which should cover the full test area of the sample),
from its backing or protective sheet (or vice versa) at an so that the laminate can be peeled apart at an angle of
angle of 180° and a jaw separation rate of 300mm per 180°. The facing material may be peeled from the release
minute. substrate, or vice versa, depending on how the sample is
applied to the plate. The method of peel must be quoted
with the results.
test equipment
A tensile tester or similar
machine, capable of peeling
a laminate through an angle
of 180° with a jaw separation
rate of 300 mm per minute
with an accuracy of ± 2%.
The equipment should be
fitted with a back plate to
which the test strip can be
attached in order to maintain
an angle of peel of 180°. Picture 2: Test strips attached to the back plate

Set the machine at 300 mm per minute jaw separation


Picture 1: Q-TEC ZPE Low Speed rate, carry out the test taking five readings at 10 mm
Release Peel Tester intervals from the centre section of the test strip. Average
the five readings for each strip.
Metal or glass pressure plates loaded to give a pressure of
6.86 kPa (70 g/cm2) on the test piece.
results
test pieces Low speed release force is expressed as the average result
for the strips tested in centiNewton per 50 mm width.
FINAT TECHNICAL HANDBOOK 2014 |

These should be strips taken from a representative sample


of material. The strips should be 50 mm wide and have
a minimum length of 175 mm in the machine direction. notes
The cuts should be clean and straight. At least three strips
should be taken from each sample. Conversion 1 kgf = 981cN.

Revised March 1990


Revised March 1999
Revised May 2001
Revised December 2013
12
high speed release force

FTM4
scope test pieces
This test method allows the label user to assess the These should be taken from a representative sample of
separation force of a laminate at speeds comparable to material. The strips should be 25 mm wide and have a
those typically used to convert and dispense the material. minimum length of 300 mm in the machine direction. The
It therefore gives a far more meaningful assessment of testing device may require extra length for clamping the
the conversion characteristics than FTM 3. Very low values material. The strips must be free from damage (creases,
may create label fly during conversion or application. High blisters etc.) and cut with clean edges.
values may produce web break when skeleton stripping
die cut labels or dispensing failure during automatic
application. test conditions
The material under test is placed between two flat metal
definition or glass plates and kept for 20 hours at 23°C ± 2°C under
a pressure of 6.87 kPa (70 g/cm2) to ensure good contact
High speed release force is defined as the force required to between the release paper and the adhesive.
separate:
Up to 20 strips can be kept between the plates.
• (mode 1) a pressure sensitive adhesive coated material
from its backing or protective sheet After storage in this manner, the strips should be taken
• (mode 2) the backing from the adhesive coated from between the glass plates and kept for not less than
material, both at an angle of 180° and at jaw separation 4 hours at the standard test conditions of 23°C ± 2°C and
rates between 10 m and 300 m per minute. 50% RH ± 5% RH.
The two modes will mostly give different results. Accelerated ageing may be carried out by placing a similar
set of strips between two flat metal or glass plates and
keeping for 20 hours in an air circulating oven at 70°C ±
test equipment 5°C. The strips should then be removed and conditioned
for at least 4 hours as above. See also FTM 5.
A machine capable of peeling a laminate through an angle
of 180° with a jaw separation rate range of 10 - 300 m per
minute. The machine should preferably have a facility for
recording the release force continuously (see picture 1).

procedure
Mode 1:
Separating adhesive coated face material from release
backing
When the adhesive component is pulled from the backing
by a roller mechanism it may be necessary to prevent the
adhesive sticking to the rollers in the drive mechanism.
This may be achieved by a strip of glassine release base
FINAT TECHNICAL HANDBOOK 2014 |

covering the exposed adhesive. The protective strip


should be 5-10 mm wider and 20-30 mm longer than the
Picture 1: Imass ZPE-1000 High Speed Release Peel Tester adhesive component test piece, to minimise the risk of
misalignment.

13
FTM4 high speed release force

The procedure is as follows:


1. Place the test piece in the machine and fix the release
backing in the load cell clamp.
2. Place the protective strip (silicone side) squarely on
and parallel to the adhesive side of the adhesive face
component, in such a way that the protective strip will
follow the adhesive component during the release test.
3. Set the machine at the desired test speed.
4. Place the adhesive component with protective strip in
the drive roller mechanism and carry out the test, noting
either the individual display reading or the average
reading from the recorder.
If a sample width of 50 mm is used, the adhesive
coated face paper cannot be removed in the described
way. Check the manual of the testing device whether
release values below 15 cN/25 mm are reliable.

Mode 2:
Separating release backing from adhesive coated face
material
The procedure is as described above except that the
position of the laminate components is reversed and it is
not necessary to use a protective strip.

results
High speed release force is expressed as the peak or
average result for the strips tested in centiNewtons (cN)
per 25 mm width. This should be quoted alongside the test
speed used and the means of peeling employed:
• (mode 1) facing material from release backing or
• (mode 2) release paper from facing material. The type
of result (peak or average) should be quoted.

notes
1. Results based on merely peak and/or average release
force values may be misleading, particularly at high
separation speeds. It is strongly recommended that
the release test device be used with a high speed
trace recorder.

2. Conversion 1 kgf = 981 cN


FINAT TECHNICAL HANDBOOK 2014 |

Issued October 1988


Revised October 1995
Revised March 1999
Revised May 2001
Revised December 2013

14
FTM5
accelerated ageing
– extended storage

scope Drying oven ageing


Typical purpose: testing of adhesive migration
This test method is suitable for rating laminate Temperature: ± 500°C
constructions according to their ability to withstand Samples kept under pressure of approximately 25g/
extended storage periods. The final test can be anything cm2 (15kg/A4 sheet)
(e.g. adhesion, migration, release) and is combined with
other FINAT Test Methods. Climate chamber testing
Typical purpose: testing of changes in adhesion
properties
test equipment Temperature: ± 350°C
Relative humidity: 75% RH
Ventilated oven Samples not kept under pressure

Climate chamber
results
Paper cutter
Resistance to accelerated ageing by submitting test
samples to elevated temperature is expressed as the
procedure percentage reduction (any increase being denoted as such)
in each average value, when compared to the control.
Place the strips, still covered with their protective backing
material in the test oven under the test conditions without The discoloration and strike through should be reported
allowing them to come into contact with each other (i.e. descriptively as nil, slight, moderate or severe.
hanging freely). Retain the control set of strips at 23°C ±
2°C and 50% RH ± 5% RH. All conditions should be carefully reported.

At the end of the accelerated ageing test period, remove Issued October 1985
the strips from the ageing cabinet and allow them to Revised March 1999
condition according to the appropriate FINAT test method Revised May 2001
(FTM 1, 2, 8 or 9). Test the aged strips, together with the Revised October 2008
control (non aged) strips.

To evaluate the migration – strike through, the single strip
and a control should also be evaluated for discoloration
and strike through of the adhesive, by removing them from
their protective release material, then adhering the samples
to black card and carrying out a visual examination.
Alternatively a spectrophotometer can be used.

test conditions
Ageing tests are typically carried out for a period of 4
weeks, and the tests are done once a week.
The test should always include a previously tested, known
FINAT TECHNICAL HANDBOOK 2014 |

product reference. This makes it easier to interpret the


results.

15
FTM6 resistance to ultra-violet light

scope The test may also be conducted under more severe


conditions when appropriate by using Blue Wool Scale No.
This test method offers a means of comparing the 5 or No. 6 as the starting point for the standard, each unit
weathering characteristics of self-adhesive laminates. step in the Blue Wool Scale approximately doubling the
exposure level.
Ultra-violet light is the high energy light which is largely
responsible for the deterioration of adhesive coated
materials during weathering. procedure

The resistance of a pressure sensitive material to ultra- Expose the strips to the lamp for the time and distance
violet light is defined as the reduction in peel adhesion defined under “Test Conditions”. The strips should be
(FTM 1 or 2), shear (FTM 8), loop tack (FTM 9) and the exposed as a laminate with the facing material towards
degree of adhesive discoloration and strike through after the lamp. Retain the control set of strips at 23°C ± 2°C and
exposure to a defined amount of radiation similar in 50% RH ± 5% RH.
spectrum to that of solar radiation.
At the end of the test period remove the strips from the
apparatus and, after allowing the specified conditioning
test equipment period appropriate to each test method, test the strips,
together with the control strips, by the appropriate test
Any apparatus capable of exposing samples to a mercury method (FTM 1, 2, 8 or 9).
vapour lamp, xenon arc or other radiation source with
similar spectral characteristics to that of solar radiation. The single strip and a control should also be evaluated for
The temperature reached by the sample should not exceed discoloration and strike through of adhesive by removing
50°C. them from their protective release material, then adhering
to black card and carrying out a visual examination.

test pieces
results
These should be strips taken from a representative sample
of material. The strips should be 25 mm wide and have Resistance to ultra-violet light is expressed as the
a minimum length of 175 mm in the machine direction. percentage reduction (any increases being denoted as
The cuts should be clean and straight. A minimum of three such) in each average value when compared to the control
strips are required for each physical property being tested samples.
together with a single strip for evaluation of discoloration
and strike through. A duplicate set of strips is also required The discoloration and strike-through should be reported
to act as control. descriptively as nil, slight, moderate or severe.

If conditions other than the standard (Blue Wool Scale 4 -


test conditions Grey Wool Scale 3) are used, then this must be stated.

The distance of the samples from the radiation source and


the time of exposure should be such that, at this distance/
time combination, a standard Blue Wool Scale No. 4 will
fade by Grey Scale step 3 (see Notes). This defines the
FINAT TECHNICAL HANDBOOK 2014 |

total quantity of radiation falling on the sample and is


approximately equivalent to 1 month summer sunlight.
Since lamp characteristics change with time, the distance/
time combination should be checked at intervals during the
life of the lamp.

16
notes
1. The exposure levels are taken from the International
Standard ISO 105: 1978
‘Textiles - Tests for Colour Fastness’. The equivalent
British Standard is BS 1006:1978 – ‘Colour Fastness of
Textiles and Leather’.
2. The Blue Wool Scales and Grey Scales are obtainable
from various national Standard Organisations
including:

BSI – UK National Standards Body


389 Chiswick High Road,
London W4 4AL, United Kingdom
Tel.: +44-845-0869001
E-Mail: cservices@bsigroup.com
URL: www.bsigroup.com

DIN Deutsches Institut für Normung e.V.


Am DIN-Platz
Burggrafenstrasse 6
D-10787 Berlin, Germany
Tel.: +49-30-2601-0
Fax: +49-30-26011231
URL: www.din.de

Japanese Standards Association


Mita MT Bldg., 3-13-12 Mita
Minato-ku, Tokyo 109-0073, Japan
Tel.: +81-3-42308503
Fax: +81-3-42318650
URL: www.jsa.or.jp

Bureau de Normalisation NBN


40, Rue Jozef II, Boite 6
B-1000 Brussels, Belgium
Tel.: +32-2-7380111
Fax: +32-2-7334264
URL: www.nbn.be

Association Française de Normalisation


11, rue Francis de Pressensé
F-93571 La Plaine Saint-Denis Cedex, France
Tel.: +33-1-41628000
FINAT TECHNICAL HANDBOOK 2014 |

Fax: +33-1-49179000
URL: www.afnor.fr

Issued 1985
Revised October 1995
Revised March 1999
Revised May 2001
Addresses revised January 2014

17
FTM7
silicone coat weight by
energy-dispersive x-ray
fluorescence spectrometry

scope should remain switched on to maintain optimum stability.


(Supplier addresses and websites ref. section 3.3 test
This test method provides a rapid and precise equipment). Along with the XRF equipment, it is generally
determination of the amount of silicone release coating advisable to use a suitable sample cutter to prepare sample
present on the surface of a range of different substrates discs to fit the XRF.
with minimal sample preparation. The test method is
applicable for all kinds of silicone-based release coatings
used in the manufacture of self adhesive tapes and labels test specimens
and when properly calibrated is capable of measuring coat
weights in the range of 0 to 4 g/m2. A suitable number of test specimens are taken from the
representative area of the self adhesive laminate or from
the pure siliconised release liner under investigation. Using
definition a suitable sample cutter for the XRF equipment being
used will guarantee a reliable positioning of the sample
Silicone coat weight is expressed as the quantity of cured within the XRF equipment. Contamination of the samples
silicone release coating on a standard area of release base especially from any silicone materials present in the area
material. It is expressed in grams per square metre (g/m2). must be avoided. Sample discs should be cut or punched
Silicone coat weight can be one of the key parameters in onto a dry and clean a surface and should then be handled
assessing the quality of release base performance. on the edge of the sample with tweezers. Samples require
no pre-conditioning.

test equipment
This method is based on the use of a ‘bench-top’ X-ray
fluorescence spectrometer (XRF) for laboratory and also
routine production measurement of silicone coat weight
using the principle of X-ray fluorescence. A number of
benchtop XRF analysers have been used in the past,
but the main commercially available equipment most
commonly used are from the Oxford Instruments Lab-X
series (which includes the Lab-X 3500 and X-Supreme
models as well as the older Lab-X 3000 and 2000 models).

procedure
The sample discs are placed into a special sample holder
designed by the manufacturers to handle paper or film
substrates, ensuring that a flat reproducible sample surface
is measured by the analyser. The samples are introduced
into the analyser where they are ultimately moved into
a special measurement chamber where irradiation
with primary X-rays results in the emission of resultant
FINAT TECHNICAL HANDBOOK 2014 |

secondary fluorescence X- rays characteristic of the element


being analysed, in this case silicon. After a period of time
Picture 1. – Oxford LAB-X 3500 XRF Analyser e.g. 30-60 second measurements are complete and the
software will provide a read out of coat weight directly in
These all utilise the same technique of Energy Dispersive g/m2 of silicone. (as Polydimethylsiloxane).
X-ray (EDX) fluorescence spectrometry to measure the
level of a characteristic energy band (in this case the one Several samples should be taken from a representative
corresponding to the Silicon atom), and by comparing this coated substrate, including samples along and across the
against a calibration curve to convert this into an equivalent web (particularly for wider webs), since variations can
silicone coat weight. Wherever possible, the instrument occur. In general the greater the count time the greater the
18
precision. Precision within the range of ±/- 0.05 to 0.01 (g/ can be used to represent many different kinds of
m2) has been reported within the industry. thermally cured silicone release coatings, there are
The exact procedure for the operation of these instruments still occasions where the release coating chemistry
has to be followed from the operator’s manual of the is different enough that a correction factor needs
appropriate instrument supplier. However some general to be applied to overcome these differences. It is
points are worth noting; recommended that the silicone release coating
supplier be contacted to confirm whether a correction
1. The XRF technique is a comparative rather than factor needs to be applied for a given release coating.
an absolute method of analysis and therefore a
calibration curve must be established before routine 5. In some cases it is recommended to purge the
analysis can be performed. The accuracy of the coat XRF measurement chamber with an inert gas
weight measurement will strongly be dependent on (typically Helium), to achieve accurate results.
the quality and accuracy of this calibration curve. This recommendation is based on the low level of
interference to the X-ray measurements which can
2. Typically the calibration procedure involves setting up come from air-borne contaminants, both industrial
the instrument for recording silicon X-ray intensities and naturally occurring (especially Argon). Whilst
followed by the measurement of known standards. the use of a Helium gas purge would improve
The precise procedure is explained by the supplier of reproducibility in the measurements it is not essential.
each instrument. However it has to be emphasized
that each base substrate will have a different
behaviour towards the secondary fluorescence X-rays results
(what is referred to as being a different “matrix”
in XRF), and this implies that each base substrate These are directly provided in grams per square meter
substrate requires its own specific calibration curve silicone (g/m²). As mentioned before, care should be
(and therefore a specific set of calibration standards is taken if the silicone release coating is based on a more
needed as well). unusual chemistry, as the majority of calibrations are based
In practice, though, it is possible to use the same upon silicone as polydimethylsiloxane. Some silicones, in
initial calibration for a range of substrates provided particular radiation cured may need a different conversion
that a “blank” re-calibration is carried out for each factor to allow for different chemistries. If in doubt consult
new grade of paper or film, and that the substrates do the silicone supplier.
not contain silicon (which will directly interfere with
the coat weight measurement), or significant levels
of some other elements which may also interfere quality control
with the X-ray measurement (such as Aluminium,
Chlorine and Argon). The suitability of any particular The use of quality control programmes can assist in
substrate can quickly be established during the “blank maintaining statistical control of this test method. For the
correction” measurement by comparing the level purpose of establishing the statistical control status of the
of the ‘background’ signal for the blank substrate testing process since the last valid calibration, a quality
against the value of the ‘blank’ substrate used for the control sample is to be regularly tested as if it was an
calibration itself. unknown production sample. Results are recorded and
analyzed by control charts to ascertain statistical control
3. One set of substrates which cannot be reliably tested status of the total testing process. Any out of control data
for coat weight using this standard XRF method are should trigger investigation which may result in instrument
the ‘Clay Coated’ substrates (such as CCK). The level recalibration.
of interference with the X-ray measurements for such
grades of paper is usually so high that the normal
reference
FINAT TECHNICAL HANDBOOK 2014 |

calibration curve cannot give reliable results. In certain


cases it is possible to use special filters to reduce the
interference of the clay on the X-ray analysis (e.g. an L. Price and L. Morrison, Spectroscopy, Vol. 7, No 6, July/
Aluminium filter for clay coated substrates), but it August 1992 pp 32-38.
is still necessary to have a specific set of calibration Coatings Technology Handbook, 2nd ed., edited by D. Satas
standards to establish a new calibration curve in these and A.A.Tracton, Marcel Dekker Inc., New York, 2001, pp.
cases. 97-101.

4. Most calibration curves are established for silicone Issued April 2001
release coatings as ‘Polydimethlsilicone’. Whilst this Revised January 2014
19
FTM8
resistance to shear from
a standard surface

scope test pieces


This test method measures the ability of an adhesive to These should be strips taken from a representative sample
withstand static forces applied in the same plane as the of material. The strips should be 25 mm wide and have
label stock. a minimum length of 175 mm in the machine direction.
It gives an indication of the likely mode of bond failure, i.e. The cuts should be clean and straight. At least three strips
adhesive failure or cohesion failure. should be taken from each material sample.

definition test conditions


Resistance to shear from a standard surface is defined as 23°C ± 2°C and 50 % RH ± 5% RH.
the time required for a standard area of pressure sensitive The test sample or test strips should be conditioned for not
coated material to slide from a standard flat surface in a less than 4 hours before testing.
direction parallel to the surface.

procedure
test equipment
A rack or jig to hold the test plate precisely 2° from the
vertical (see diagram below).

1 kg weight.

A standard FINAT Test roller.


Test plates made of float glass or similar plate glass
(Kristallspiegelglas, verre glace).

Remove the backing material from each strip and place the
adhesive coated facing material, adhesive side down, on
to a clean test plate using light finger pressure, so that a
square of pressure sensitive coated material, 25 mm x 25
mm, is in actual contact with the surface. Roll twice in each
direction with the standard FINAT test roller at a speed
of approximately 10 mm per second to obtain intimate
contact between the adhesive mass and the surface. Any
strips found by inspection to have air bubbles trapped
FINAT TECHNICAL HANDBOOK 2014 |

between the adhesive mass and test plate should be


discarded.

Place the test plate into the rack of jig and attach the 1
kg weight to the free end of the test strip (not less than 5
minutes and not more than 10 minutes after rolling).

Note the time taken for the strips to part from the plate.

20
results 2. Alternative surfaces to plate glass can be used such as
stainless steel or aluminium but this must be clearly
Resistance to shear from a standard surface is expressed stated alongside the results.
as the average time taken for the three strips to shear from
the test plate. 3. Alternative weights can be used, but these must be
clearly stated alongside the results.
Failure Description Code:
CP Clear Panel - no visible stain on panel. Issued October 1985
PS Panel Stain - discoloration of test area, but no Revised March 1999
tacky residue. Revised May 2001
CF Cohesive Failure - the adhesive film is split during
the test, leaving residue of adhesive on both the
panel and the front material.
AT Adhesive Transfer - the adhesive separates cleanly
from the front material, leaving adhesive film on
the test panel.
The approximate extent of transfer should be quoted as
percentage

notes
1. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:
• Diacetone alcohol non-residual, technical grade or better
• Methyl Ethyl Ketone (MEK)
• Acetone
• Methanol 95 %
• n-Heptane
• Ethyl Acetate

The cleaning material must be absorbent, e.g. surgical


gauze, cotton wool or tissue. To be suitable, materials
must be lint-free during use, absorbent, contain no
additives that are soluble in the solvents listed above,
and made exclusively from virgin materials.

Dispense one of the solvents listed above on to the


panel, wiping it to dryness with fresh absorbent
cleaning material. Repeat for a total of three washes
with the solvent. Final wipe shall be with MEK or
acetone.
FINAT TECHNICAL HANDBOOK 2014 |

Alternative methods which remove contamination


properly can be adopted, e.g. ultrasonic cleaning.

Prior to use, the cleaned plates should be left for 4


hours under standard test conditions. Care should be
taken to handle clean plates by the edge only.

21
FTM9 ‘loop’ tack measurement

scope test conditions


This test method describes a means of assessing probably 23°C ± 2°C and 50% RH ± 5% RH.
the most important and yet the hardest to measure
property of pressure sensitive materials, the tack. The The test sample or test strips should be conditioned for not
method described should allow the end user to compare less than 4 hours before testing.
the “initial grab” or “application tack” of different laminates
and can be extremely useful to those working with
automatic labelling equipment where this property is of
particular importance.

definition
The ‘loop’ tack value of a pressure sensitive material is
expressed as the force required to separate, at a specified
speed, a loop of material (adhesive outermost) which
has been brought into contact with a specified area of a
standard surface.

test equipment
A tensile tester or similar machine with reversing facility procedure
and a vertical jaw separation rate of 300mm per minute
with an accuracy of ± 2%. It should also have a capability Remove the backing
of measuring direct loads up to at least 20 Newton with an material from each strip
accuracy of ±2%. immediately prior to
the test being carried
A flat plate made of float glass or equivalent plate glass out. Hold the two ends
measuring 25 ± 0.5 mm x 30 ± 2.0 mm x minimum of the adhesive coated
thickness 3.0 mm. A metal peg is attached at the centre of facing material strip and
one face of the plate. The dimensions of the peg should be from the strip into a
such that the peg can be clamped in the lower jaw of the loop, adhesive surface
tensometer. outermost, by bringing
the two ends together.
Clamp the ends of the
test pieces loop for a distance of
10 mm into the top
These should be strips taken from a representative sample jaw of the ensile tester
of material. The strips should be 25 mm wide and have a leaving the loop hanging
minimum length of 175 mm in the machine direction. The vertically downwards.
cuts should be clean and straight. At least five strips should The sides of the jaw
be taken from each sample. should be protected from the adhesive coating.

FINAT TECHNICAL HANDBOOK 2014 |

Clamp the glass plate in the lower jaw with the longer axis
of the plate positioned at right angles to the long axis of
the strip. Start the machine and bring the loop into contact
with the glass plate at a speed of 300 mm per minute.
When full contact over the glass plate has been achieved
(25 mm x 25 mm) immediately reverse the direction of the
machine and allow separation to take place at a speed of
300 mm per minute. It is important that delay in reversing
direction is kept to an absolute minimum.

22

If the force exceeds the strength of a paper facing material,
the result quoted should be the maximum reached before
the paper tears and this result should be followed by the
postscript PT (paper tear)

If adhesive transfer occurs, this should be indicated by the


letters AT, and the approximate extend of transfer quoted
as percentage.

notes
1. The rigidity of the sample affects the results and must
be considered when comparing different adhesives on
different facing materials.
2. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:

• Diacetone alcohol non-residual,


technical grade or better
• Methyl Ethyl Ketone (MEK)
• Acetone
• Methanol 95%
• n-Heptane
• Ethyl Acetate

The cleaning material must be absorbent, e.g. surgical


gauze, cotton wool or tissue. To be suitable, materials must
be lint-free during use, absorbent, contain no additives
that are soluble in the solvents listed above, and made
exclusively from virgin materials.

Dispense one of the solvents listed above on to the panel,


wiping it to dryness with fresh absorbent cleaning material.
Repeat for a total of three washes with the solvent. Final
wipe shall be with MEK or acetone.

Alternative methods which remove contamination properly
can be adopted, e.g. ultrasonic cleaning.

Prior to use, the cleaned plates should be left for 4 hours
under standard test conditions. Care should be taken to
handle clean plates by the edge only.
FINAT TECHNICAL HANDBOOK 2014 |


Record the maximum force necessary to completely 3. Conversion 1 kgf- = 9.81 Newton.
separate each loop from the glass plate.
Issued October 1985
Revised March 1999
results Revised May 2001
Added pictures January 20
‘Loop’ tack is expressed as the average value (ignoring the
initial peak) and range for the five strips tested in Newton.

23
FTM10
quality of silicone coated
substrates for self-adhesive
laminates: release force

scope A circulating hot air oven capable of maintaining a


temperature of 70 ± 2°C.
This test method describes a simple method of assessing
the suitability of a siliconised (or indeed any other type of A standard FINAT test roller.
release) backing material for pressure sensitive lamination.
Metal or glass pressure plates loaded to give a pressure of
6.86 kPa (70 g/cm2) on the test pieces.
definition
A standard pressure-sensitive adhesive tape, 25 mm wide
Release force is defined as the force required to separate e.g. tesa 7475 PV2 (acrylic) or tesa 7476 (rubber), or a
a pressure sensitive adhesive coated material from its standard pressure sensitive adhesive coated facing paper
backing or protective sheet (or vice versa) under specified (see Notes).
conditions and at a specified angle and speed.

test pieces
test equipment
The silicone coated substrate may be tested either against
A tensile tester or similar machine, capable of peeling a the standard tape or against a standard pressure sensitive
laminate through an angle of 180° at a jaw separation rate adhesive coated facing paper, the adhesive chosen being
of 300 mm per minute and with an accuracy of ± 2%. that which will simulate the end application for which the
release paper is intended.
Take a representative sample of the silicone coated
substrate of minimum dimensions 450 mm x 250 mm.
Apply to this, using light finger pressure, the adhesive tape
in strips along the machine direction. Alternatively apply a
suitable sized sheet of pressure sensitive adhesive coated
facing paper to the sample.
Cut test strips 25 mm wide and 175 mm in the machine
direction. The cuts should be clean and straight. Roll the
strips twice in each direction with the standard FINAT test
roller at a speed of approximately 10 mm per second. At
least six strips should be prepared from each sample if
subsequent adhesion tests are to be carried out. In the
case of samples showing very low release force, the width
(and hence the width of tape) may be 50 mm in order to
obtain a meaningful measurement. However, release force
should still be expressed as release force per 25 mm width.

test conditions
Place the strips under test between two flat metal or
glass plates and keep for 20 hours at 23°C ± 2°C under a
pressure of 6.86 kPa (70 g/cm2) to ensure good contact
between the silicone coated substrate and the adhesive.
FINAT TECHNICAL HANDBOOK 2014 |

After storage in this manner take the strips from between


the plates and keep for not less than 4 hours at the
standard test conditions of 23°C ± 2°C, 50% RH ± 5% RH.
Accelerated ageing may be carried out by placing a similar
set of strips between two flat metal or glass plates and
keeping it for 20 hours in an air circulating oven at
Picture 1: Q-TEC ZPE Low Speed Release Peel Tester 70°C ± 5°C. The strips should then be removed and
conditioned for at least 4 hours as above.

24
procedure
Fix each strip in the machine so that the tape or facing
material can be stripped away from the silicone coated
substrate at an angle of peel of 180°. Set the machine to
operate at 300 mm per minute jaw separation rate. Carry
out the test taking at least five readings at 10 mm intervals
from the centre section of the test trip. Average the five or
more readings for each strip.

Picture 2: Test strips attached to the back plate

results
Release force is expressed as the average result for
the strips tested in Newton per 25 mm width either
under standard conditions or under accelerated ageing
conditions.

notes
1. The strips should be retained for subsequent adhesion
testing.
2. See FTM 11 for interpretation of results.
3. The adhesive tape or adhesive coated facing paper
used should be as stable to changes in temperature
as possible and of steady and reproducible adhesion
value.
4. Conversion 1 kgf- = 9.81 Newton.
FINAT TECHNICAL HANDBOOK 2014 |

See also notes for FTM 11.

Issued October, 1985


Revised March 1999
Revised May 2001
Revised January 2013

25
FTM11
quality of silicone coated
substrates for self-adhesive laminates:
subsequent adhesion

scope test pieces


This test method describes a technique whereby the effect These are the 175 mm x 25 mm tape or pressure sensitive
of the release surface on the adhesive properties can be adhesive coated facing paper strips which were peeled
assessed. It is of particular interest both to manufacturers from the silicone coated substrate in FTM 10, plus a
of release paper and also to pressure sensitive laminate control set of at least three strips from the standard tape
manufacturers in determining the key and degree of cure of or pressure sensitive adhesive coated facing paper which
the release system. have not been in contact with the silicone coated substrate
under test.

definition
test conditions
Subsequent adhesion is defined as the force required, at a
specified angle and speed, to remove a pressure sensitive 23°C ± 2°C and 50% RH ± 5% RH.
adhesive coated material from a standard test plate after The test strips should be conditioned for not less than 4
it has previously been in contact with a silicone coated hours before testing.
substrate under specified conditions.
Percentage subsequent adhesion is expressed as the
percentage ratio of this result compared with the adhesion procedure
of similar material which has not been in contact with the
silicone coated substrate. Apply the test strips of adhesive coated tape or facing
paper from FTM 10, adhesive side down, on to a clean
test plate using light finger pressure. Roll twice in each
test equipment direction with the standard FINAT test roller at a speed
of approximately 10 mm per second to obtain intimate
A tensile tester or similar machine, capable of peeling a contact between the adhesive mass and the surface. After
laminate through an angle of 180° with a jaw separation applying the strip to the test plate leave for a period of 20
rate of 300mm per minute with an accuracy of ± 2%. minutes before testing. Prepare a second set of strips and
leave for a period of 24 hours before testing.
Test plates made of float glass or equivalent plate glass
(Kristallspiegelglas, verre glace). Fix the test plate and sample in the machine so that the
angle of peel is 180°. Set the machine at 300 mm per
A standard FINAT test roller. minute jaw separation rate. Carry out the test taking at
least five readings at 10 mm intervals from the centre
The test samples from FTM 10. section of each test strip.
Average the five or more readings for each strip.
A standard pressure sensitive tape, 25 mm wide, or a
standard pressure sensitive adhesive coated facing paper This procedure should then be repeated for the control set
(see Notes to FTM 10 and FTM 11). of tape or adhesive coated facing paper strips which have
not been in contact with the silicone coated substrate in
order to determine percentage subsequent adhesion.
FINAT TECHNICAL HANDBOOK 2014 |

Picture 1: Cheminstruments Tensile Tester AR-1000


26
results 5. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
Subsequent adhesion is expressed as the average result for on the surface. The following solvents can be used to
the strips tested in Newtons per 25 mm width for either 20 clean the test plates:
minutes or 24 hours application time. • Diacetone alcohol non-residual,
Force required to remove test tape technical grade or better
Subsequent adhesion% = 100 X • Methyl Ethyl Ketone (MEK)
Force required to remove control tape • Acetone
If the adhesive force exceeds the strength of a paper facing • Methanol 95%
material the result quoted should be the maximum reached • n-Heptane
before the paper tears and this result should be followed • Ethyl Acetate
by the postscript PT. If adhesive transfer occurs, this should
be indicated by the letters AT. The cleaning material must be absorbent, e.g. surgical
gauze, cotton wool or tissue. To be suitable, materials
must be lint-free during use, absorbent, contain no
notes additives that are soluble in the solvents listed above,
and made exclusively from virgin materials.
1. Low values of release force (FTM 10) in conjunction Dispense one of the solvents listed above on to the
with high subsequent adhesion (FTM 11) usually panel, wiping it to dryness with fresh absorbent
indicate that the silicone coating has been properly cleaning material. Repeat for a total of three washes
applied and cured. with the solvent. Final wipe shall be with MEK or
acetone.
2. High values of release force (FTM 10) usually indicate Alternative methods which remove contamination
that the silicone coating is inadequate or uneven properly can be adopted, e.g. ultrasonic cleaning.
(unless the product is designed to give high release)
or that the adhesive has reacted with an improperly Prior to use, the cleaned plates should be left for 4
cured film. hours under standard test conditions. Care should be
taken to handle clean plates by the edge only.
3. Low values of release force (FTM 10) with low
percentage subsequent adhesion values indicate 6. Alternative surfaces to plate glass can be used such as
silicone migration. However, the subsequent adhesive stainless steel or aluminium but this must be clearly
strength of an adhesive after contact with silicone stated alongside the results.
coated paper is very much dependent on the surface
texture of the substrate to which the release coating 7. If adhesion values are required when paper tear has
has been applied. In general, the smoother the surface occurred, then this test can be conducted at lower jaw
of the substrate, the higher will be the percentage separation rates quoting the latter against the results.
subsequent adhesion value obtained. Values of 70-
80% are not unusual. 8. Conversion 1 kgf- = 9.81 Newton.

4. Care should be taken in the interpretation of the Issued October 1985


results obtained from the accelerated ageing release Revised March 1999
test carried out at elevated temperature as the Revised May 2001
rheological properties of adhesives are temperature
dependent. Excessive flow of adhesive at high
temperature can give high release values, particularly
FINAT TECHNICAL HANDBOOK 2014 |

with pinholed or imperfect silicone coatings.


27
FTM12 adhesive coat weight

scope test procedure


This test may be used to determine with reasonable 1. The specimen is placed in an oven at 105°C for five
accuracy the amount of dry adhesive material applied to minutes.
the surface of a pressure sensitive label construction. 2. It is removed and any release liner is detached.
3. Exactly one minute after removal from the oven,
the weight of the specimen is recorded to at least 3
definition decimal places.
4. Soak the specimen in the beaker of solvent to soften
Adhesive coat weight is expressed as the weight of dry the adhesive - approximately one minute.
adhesive on a standard area of material - in grams per 5. Remove from the beaker and carefully scrape the
square meter (g/m2). adhesive off completely, rinsing in clean solvent to
remove any residue.
6. When all adhesive has been removed, return
test equipment specimen to oven for further five minutes.
7. Exactly one minute after removal from the oven
A press or template enabling samples to be cut 100 cm2 in reweigh and record new weight of specimen.
area to a high degree of accuracy.

A circulated hot air oven capable of maintaining a results


temperature of 105°C ± 2°C.
Subtract the final weight from the initial weight and
A balance capable of recording sample weights to an multiply this figure by 100 to express the final result in
accuracy of at least ± 0.001 g. g/m2. Carry out the test taking five specimens per sample
and record the average coat weight obtained.
A beaker of solvent - suitably chosen to enable the
adhesive film to be softened prior to removal.
note
Recommendations:
a) for an acrylic adhesive - aliphatic solvent (e.g. Particular care should be taken when testing laminates
SBP 2) ± trace of aromatic solvent (e.g. toluene); manufactured from specialty papers or synthetic films
b) for a rubber/resin adhesive - aliphatic solvent. (particularly vinyls) since the solvent used to remove
the adhesive may also dissolve components of the face
material resulting in significant errors.
test specimens
Issued October, 1985
Samples of 100 cm2 cut from representative positions in Revised March 1999
the web. Revised May 2001
FINAT TECHNICAL HANDBOOK 2014 |

28
low temperature adhesion

FTM13
scope test pieces
This test method allows a subjective assessment to be These should be cut from a representative sample of
made of the ability of a pressure sensitive material to material. The test piece should be 25 mm x 15 mm cut
adhere under low temperature conditions. with the machine direction parallel to the short edge.

definition test surfaces


Low temperature adhesion is defined as the ability • Polyester
of a pressure sensitive coated material to adhere at • Glass
temperatures below 5°C. This test method allows a • Stainless steel
subjective assessment to be made of the ability of a • Aluminum foil
pressure sensitive material to adhere under chill (4°C) and • Low Density Polyethylene (PE - LD)
deep freeze (-25°C) conditions. Other test conditions are • High Density Polyethylene (PE - HD)
possible (see note 1) and if used should be reported with • Oriented Polypropylene (OPP)
the results. • Where laminates or adhesives are being designed for
specific applications the test surfaces should be chosen
to represent the final end use. Other test surfaces may be
test equipment used and should be reported with the results (see note 2).

A cabinet capable of maintaining a temperature of 4°C ± 1°C.


procedure
A chest freezer capable of maintaining a temperature of
-25°C ± 1°C. Place the test surfaces in the cabinet set at 4°C and the
chest freezer set at -25°C twenty four hours before the
Both should be large enough to allow examination of the start of the test. The surfaces should be dry before they
test specimens without removal. are placed into the test cabinets and any filmic materials
should be placed in contact with glass plates to ensure an
A standard FINAT test roller. even temperature distribution. The test surfaces should
remain in the test cabinets at all times during the test.
Holding the test pieces by the edge, remove the backing
material. Place the test piece, adhesive side down, on the
test surface - do not press down as this can lead to local
heating - then roll once in each direction with the standard
FINAT test roller, that has been conditioned for at least 4
hours to the test conditions, at a speed of approximately 10
mm/sec to obtain intimate contact between the adhesive
mass and the surface. At least three test pieces from each
laminate under test should be applied to each test surface.
FINAT TECHNICAL HANDBOOK 2014 |

29
FTM13 low temperature adhesion

results
For each surface average the score of the test pieces. To
obtain the overall score of the laminate average the score
per surface by the number of surfaces. For adhesives
designed for specific surfaces the results on those surfaces
should be quoted as well as the average (see notes 4 and 5).

notes
1. The test conditions listed in the method are only two
of many possibilities.
Other conditions that can be used are:
• apply the labels at -40°C, test at -40°C;
The labelled test surfaces should then be stored in the • apply the labels at ambient, test at 4°C, -25°C, -40°C;
test cabinets for the prescribed period. The recommended • apply the labels at ambient to moist test
periods are 1 hour and seven days though other time surfaces, test at 4°C, -25°C, -40°C;
periods are possible (see note 3). The time period used • apply the labels at -25°C,-40°C to icy surfaces,
should be reported with the results. test at -25°C, -40°C.
In all cases the test conditions chosen should reflect
After the test period, remove the test pieces from the test as closely as possible the final end use of
surfaces with the test surfaces remaining in the test cabinet the material. The chosen test conditions should be
and assess the adhesion. Removal of the test piece should recorded with the results.
start at one corner. If the label starts to tear removal should
be attempted from the opposite corner and continued even 2. The test surfaces listed in the method are
if the label tears again. recommended surfaces only. Each is subject to the
Rate the adhesion in the following manner: variations normal for commercial suppliers and the
test surfaces used should be representative of that
supplier’s product.

3. The test periods indicated in the method are


recommended periods only. Other time periods such
as 24 hours or 1 month can be used if required.
In all cases the chosen time period should reflect the
final application and be recorded with the results.

4. The label substrate has considerable effect on the


adhesion performance as described by this test
method. As such this method should be regarded as
measuring the low temperature adhesion of the label
construction rather than the adhesive in isolation.

5. The maximum rating possible for a removable


construction is 3.
FINAT TECHNICAL HANDBOOK 2014 |

Rating Description
0 Label detached from the test surface. 6. Label constructions using plastic films such as PVC
1 Poor bond-no label tear. which may embrittle at low temperatures can give
2 Moderate bond - no label tear. high readings on this test but be unsuitable for the
3 Good bond - no label tear. final end use.
4 Very good bond - up to 50% of label surface left
on test plate after removal. Issued October 1985
5 Excellent bond greater than 50% of label surface Revised March 1999
left on test plate after removal Revised May 2001

30
dimensional stability

FTM14
scope procedure
This test method allows the user to assess the dimensional Remove the backing material and place the adhesive
stability of a pressure sensitive material when subjected coated facing material adhesive side down onto a clean
to specified test conditions. It is particularly relevant to test plate using light finger pressure and without stretching
synthetic film based materials such as Polyvinyl chloride the material. Roll twice in each direction with the rubber-
(PVC), Polyethylene, Polypropylene, Polyester etc. covered roller at a speed of approximately 10 mm per
second to obtain intimate contact between the adhesive
and the aluminium plate surface.
definition
This property is defined as the dimensional change of a
pressure sensitive material which has been applied to
a standard test plate under specified conditions when
subjected to elevated temperatures.

test equipment
An air circulating oven maintained at 70°C ± 2°C.

Test plates made of smooth aluminium or aluminium alloy


150 mm x 100 mm x 0.6 mm gauge.

A rubber covered roller of sufficient width and a mass of


1 kg per 25 mm width. Then condition the applied material for 72 hours at 23°C ±
2°C and 50% RH ± 5% RH.
A scaled magnifying glass.
After this conditioning procedure the applied material
should be trimmed to the dimension of the test plate.
test condition

The material to be tested should be conditioned at 23°C ±


2°C and 50% RH ± 5% RH for not less than 4 hours before
application.

test pieces
These should be cut from a representative sample of
material min. 165 mm x 115 mm with the 165 mm edge
running parallel to the length-wise edge of the test
material.

Cut with a sharp knife, parallel to the sides of the test plate,
FINAT TECHNICAL HANDBOOK 2014 |

a crosscut in the middle of the test sample.

31
FTM14 dimensional stability

failure description code :


CP Clean Panel - no visible stain on panel.
PS Panel Stain – discoloration of test area,
but no tacky residue.
CF Cohesive failure - the adhesive film is split during
the test, leaving residue of adhesive film on both
the panel and the front material.
AT Adhesive Transfer - the adhesive separates cleanly
from the front material, leaving the adhesive film
on the test panel.

notes
Insert the test plate into the oven at 70°C ± 2°C for 1 week
after which it is removed and conditioned at 23°C ± 2°C for 1. The test conditions given can be varied to suit any
10 - 15 minutes to cool. particular application, whereby the conditioning time
and/or the exposure time and/or the substrate (e.g.
Measure the shrinkage in the crosscut to the nearest 0.05 glass) and/or the temperature of the oven can be
mm in both the length-wise direction and cross to the changed. This should be clearly stated alongside the
length-wise direction of the label. test results.
2. The quality finish and thickness of the aluminium used
should be recorded.
3. Dimensions of the recommended test plate (150 mm
x 100 mm x 0.6 mm gauge) are those of a panel of the
QUV Accelerated weathering tester.
4. Dimensional stability quoted as a percentage can be
misleading and should be avoided e.g. 0.2% on 150
mm dimension cannot be related to a one meter
dimension.

Issued April 1991


Revised March 1999
Revised May 2001
Revised April 2003
Revised May 2004
results Revised December 2013

The dimensional stability (shrinkage) is expressed in mm,


as the change in dimensions at the cross cut, in both
the length-wise direction and cross to the length-wise
direction of the label.

optional
FINAT TECHNICAL HANDBOOK 2014 |

For removable application (advertising on coaches, etc.)


the type of adhesive failure can be observed by peeling
the label from the aluminium panel by hand at an angle of
approx. 135°.

32
surface tension of plastic films

FTM15
scope test condition
This method covers measurement of the surface tension 23°C ± 2°C and 50% RH ± 5% RH. The test sample should
of plastic film surfaces in contact with drops of specific preferably be conditioned for not less than four hours
test fluids. Surface tension (wettability) of plastic films is before testing, unless an immediate reading is required.
one of the properties used to judge surface characteristics
related to printability and adhesion of other coatings/
adhesives. Although the print key or adhesion property is test fluids
not dependent on the surface tension only, this method is
often used as a quick practical method. It is furthermore For polyethylene, polypropylene, polyester and/or similar
important to note that the determined wettability type of films, test fluids A, according to Table 1 are
characterises the immediate surface condition only, and prepared by mixing Formamide (surface tension = 58
that this condition can change during storage. mN/m and 2 ethoxyethanol (surface tension 30 mN/m).
These chemical raw materials may not be readily available.
In that case FINAT recommends the use of ready prepared
definition solutions as listed at the end of this test method.
Approximately 1 gram of a blue dye (e.g. Victoria blue or
The surface tension is measured by applying to the surface Methylene blue) is added to each litre of test fluid.
of the plastic film, a test fluid of known surface tension and For plastic films such as polyvinylchloride (PVC) which are
recording the time taken for the continuous film of the fluid affected (e.g. swelling) by the test fluids of series A, the test
to break into droplets. The surface tension is defined as fluids B shown in Table 2 are prepared by mixing methanol
that level when a continuous film of the test fluid remains (surface tension 23 mN/m) and distilled water, or water of
intact for 2 seconds. similar quality (surface tension 73 mN/m). Approximately 1
gram of a red soluble dye (e.g. Fuchsine) is added to each
litre of test fluid.

procedure
Lay the specimen on a smooth flat surface. Spread the
test fluid of known surface tension using a felt tip pen or
soft brush lightly over an area of approximately 200 mm x
10 mm of the test specimen. Note the time taken for the
continuous film of the fluid to break into droplets. Breaking
of the fluid into drops in less than two seconds, a lower
numbered test fluid should be tried.
Shrinkage of the liquid film on the sides of the applied fluid
does not necessarily indicate a lack of wetting. The aim is
to establish the lowest reading at an optimal dwell time of
Picture 1: example of test specimen staying as applied and two seconds.
breaking into droplets Extreme care must be taken to ensure that the film surface
is not touched or contaminated in the areas in which the
tests are to be made as this will influence the test results.
test equipment
results
FINAT TECHNICAL HANDBOOK 2014 |

A range of test fluids.

A stopwatch. The lowest reading (surface tension) at an optimum dwell


of two seconds is deemed equivalent to the surface tension
of the test piece, and is recorded in mN/m (see Notes).
test pieces
The test specimens must be at least 200 mm x 10 mm
taken with their length in the cross direction of the roll.

33
FTM15 surface tension of plastic films

notes Table 1 : Test Fluid Series A

Surface tensions
1. Ready made test fluids of series A (see Table 1) can be 2-Ethoxyéthanol Formamide
of Test Fluids
obtained from: vol.% vol.%
Series A [mN/m]

Pillar Technologies 30 100.0 -


www.pillartech.com 32 89.5 10.5
34 73.5 26.5
Arcotec GmbH
www.arcotec.com 36 57.5 42.5
38 46.0 54.0
For addresses please consult section 3.3 of this book. 40 36.5 63.5
42 28.6 71.5
2. The test fluids must be kept in brown glass containers.
The test fluids should be renewed depending on 44 22.0 78.0
frequency of use, e.g. when used on a daily basis 46 17.0 83.0
dispose of remaining fluid after three months. 48 13.0 87.0
50 9.3 90.7
3. All precautions must be maintained when handling
the chemicals used in the test fluids as they can be 52 6.3 93.7
injurious to health and can cause skin irritation. 54 3.5 96.5
56 1.0 99.0
4. The Sl unit for this property is mN/m and replaces the
formerly used Dyne/cm, conversion factor being one
to one. Table 2. Test Fluid Series B

5. Preparation of solution by volume is best done by Surface tensions


Methanol Water
measuring separately and adding together. of Test Fluids
vol.% vol.%
Series B [mN/m]
6. For more accurate determination of surface tension, 30 67.0 33.0
contact angle measuring equipment is used. Such
32 59.8 40.2
units can be purchased from Lorentzen & Wettre as a
L & W Surface Wettability Tester, Code 28. However, 34 53.5 46.5
it must be noted that the results obtained may not 36 47.9 51.1
necessarily be comparable. 38 42.8 57.2
40 38.3 61.7
7. DIN 53 364 and ASTM D2578-67 are standards
relating to surface tension measurement. 42 34.2 65.8
44 30.5 69.5
8. FINAT FTM 15 is an effective tool for quick and reliable 46 27.1 72.9
printability assessment of print substrates in terms
48 24.0 76.0
of their surface tension. Experience has shown that
print substrates tend to show poor printability if their 50 21.1 78.9
surface tension is below 38 mN/m. In this case, test 52 18.5 81.5
prints should 54 16.0 84.0
FINAT TECHNICAL HANDBOOK 2014 |

56 13.7 86.3
be produced. With surface tension levels below 31
mN/m, print substrates are no longer printable with
standard printing inks at all, but will generally require These chemical raw materials may not be readily available.
special inks. The surface tension limit value (38 mN/m) is In that case FINAT recommends the use of ready prepared
correspondingly valid for other upgrading processes, such solutions as listed previously.
as varnishing, gluing, laminating and hot film embossing.
Issued April 1991
Revised March 2005
Addresses revised January 2014
34
chemical resistance - spot method
FTM16
definition results
Chemical resistance here is defined as the ability of the Colour change is assessed against the untreated control
pressure sensitive coated material to resist colour change either descriptively as nil, slight, moderate or severe attack,
when subjected to a chemical substance placed on its rate 0 to 5 (5 excellent resistance, 0 non resistant) or by
surface for 24 hours or 7 days at 23°C ± 2°C. determining colour fastness against the Blue Wool Scale 4
or Grey Wool Scale 3 standards.

test equipment Printing ink permanency can be assessed by measuring the


key of the printing ink before and after the chemical test
Test plates. employing standard tesa tapes.

A standard FINAT test roller.


notes
Test chemical.
1. The time of surface contact can be varied to suit any
given end application.
procedure
Temperature can also be changed by placing the test
Remove the backing material from the test piece and place piece in an oven set at the required condition.
the adhesive coated facing material, adhesive side down, 2. This test method only allows an assessment of the
onto a clean test plate. Roll twice in each direction with the chemical resistance of the surfacing material. For total
standard FINAT test roller. product resistance, the immersion technique (FTM 17)
is employed followed by bond assessment.
Place the test specimen horizontally. Cover up to 50% of
the exposed surface area with the test substance ensuring 3. It is essential that detergents or inert solvents used
that it does not reach the edge of the sample, thus avoiding for cleaning purposes are such that they have no
edge attack. Leave undisturbed for 7 days at 23°C ± 2°C. influence on the perceived colour(s) after the
It may be necessary to cover the test container to prevent completion of chemical contact.
excess evaporation if a volatile chemical substance is used.
Issued October 1995
At the end of the test period, wash the test specimen Revised March 1999
in a detergent solution to remove all residual chemical Revised May 2001
substance and dry carefully employing an absorbent paper
or cloth. If the surface remains ‘wet’, indicating that the
chemical substance still remains, an inert solvent such as
industrial alcohol or white spirits should be used to remove
the test chemical. Dry again carefully using absorbent
paper or cloth.

Immediately assess any colour change of the material


or permanence of legend if a printed substrate has
been employed, either as a general colour change or for
individual printing ink colours.
FINAT TECHNICAL HANDBOOK 2014 |

35
FTM17
chemical resistance -
immersion method

definition procedure
Chemical resistance here is defined as the ability of the Remove the backing paper from each strip/sample and
pressure sensitive coated material to maintain its physical place the adhesive coated material, adhesive side down,
and adhesive characteristics after being completely onto a clean test plate using light finger pressure.
immersed in a chemical substance for 24 hours at Roll twice in each direction with the standard FINAT test
23°C ± 2°C. roller at a speed of approximately 10 mm per second, to
obtain intimate contact between the adhesive and the test
surface. Condition for 24 hours at 23°C ± 2°C.
test equipment
Carry out peel adhesion (180°) at 300 mm per minute (as
Test plates made of float glass or similar plate glass described in FTM 1) on a set of three strips.
(see Note).
Completely immerse the second set of test samples in the
A standard FINAT test roller. chemical substance for 24 hours at 23°C ±2°C (see note 1).
It may be necessary to cover the test container to prevent
Test chemical/large beaker. excess evaporation if a volatile chemical substance is used.

Metal rule.

test pieces
For subsequent testing against FTM 1, or assessing colour
change, strips should be taken from a representative
sample of material, which should be 25 mm wide and have
a minimum length of 175 mm in the machine direction.
The cuts should be clean and straight. At least two sets of
above strips should be taken from each material sample.

For measurement of dimensional change after chemical
immersion, a test piece of 10 cm x 10 cm is ideally required
cut with one edge running parallel to the lengthwise edge
of the product.
At the end of the test period, wash the test specimen
in a detergent solution to remove all residual chemical
test conditions substance and dry carefully employing an absorbent paper
or cloth. If the surface remains ‘wet’, indicating that the
23°C ± 2°C and 50% RH ± 5% RH. chemical substance still remains, an inert solvent such
as industrial alcohol or white spirits should be used to
The test substance or test strips should be conditioned for remove the chemical substance. Dry again carefully using
not less than four hours before testing. absorbent paper or cloth.

Condition for 1 hour at 23°C ± 2°C, then measure peel


adhesion (180°) as before.
FINAT TECHNICAL HANDBOOK 2014 |

Recovery of bond can be additionally assessed by repeating


the above but allowing the test samples to condition for
24 hours at 23°C ± 2°C before re-measuring peel adhesion
(FTM 1). Any colour change on the test samples should also
be noted. For assessment of dimensional change, immerse
the ‘100 mm x 100 mm’ test sample in the chemical
substance for 24 hours at 23°C ± 2°C. Dry as before and
re-measure in both directions.

36
In all of the above tests, assess any colour change of the
material or permanence of legend if a printed substrate has
been employed, either as a general colour change or for
individual printing ink colours. Any other deterioration of
the test piece, e.g. blisters, should also be noted.

results
1. Peel Adhesion
An average is taken of the three strips prior to and
after immersion. Determine the percentage loss in
peel adhesion (180°) against the non-immersed
sample.
Chemical resistance (bond) can be expressed as
follows:

Loss Resistance
0 Excellent
5% Good
50% Moderate
75% Poor
100% Non-resistant

2. Colour Fastness
Colour change is assessed against the untreated
control either descriptively as nil, slight, moderate
or severe, rated 0 to 5 as above (5 excellent, 0 non
resistant) or by determining colour fastness against
the Blue Wool Scale 4 or Grey Wool Scale 3 standard.

3. Dimensional Stability
This is expressed as the increase or reduction in
millimetres (denoted ± or -) after immersion of each
sample against its original length.

notes
1. The temperature and time of immersion can be varied
and alternative test substrates other than float plate
glass may be used to suit any given application.

2. This test method allows an assessment of the


chemical resistance of the total laminate. For an
assessment of the face material only, the Spot
FINAT TECHNICAL HANDBOOK 2014 |

Method (FTM 16) should be employed.

3. It is essential that detergents or inert solvents used


for cleaning purposes are such that they have no
influence on the perceived colour(s) after the
completion of chemical contact.

Issued October 1995


Revised March 1999
Revised May 2001
37
FTM18 dynamic shear

scope sample preparation


This method is designed to determine the resistance of an Laminate the aluminium foil or the polyester on the front
adhesive coated label stock on a standardised surface, to of the sample. Then cut five test pieces of 12.7 ± 0.1 mm
shear at a constant speed. width and at least 50 mm length in the machine direction.

definition procedure
Dynamic shear is defined as the maximum force per unit
width required to remove the adhesive coated label stock
from a specified area in the direction parallel to the surface.

principle
A test piece is partly adhered to a test panel under
controlled pressure. A constant speed of deformation
is applied to the free end of the test piece in the length
direction of the test piece. The adhesive layer resists
this deformation. This resisting force grows during the
increased deformation of the adhesive, until the adhesive
cannot follow the deformation anymore and starts to fail.
The maximum force during the test is measured. Prior to testing, clean five test panels thoroughly with
n-heptane.
Slowly remove the backing from a test piece.
test equipment Gently place the test piece in the middle of the panel,
without applying pressure. The small edge of the test piece
An electronic tensile tester with capability of jaw separation shall be placed against the scribed line, at 12.7 mm from
with an accuracy of 1% or better. The movable grip should the edge of the panel as shown in the next picture:
be capable of being driven at a rate of 5.0 mm/min.
Cover the adhesive of the free part of the test piece with a
An accurate cutting device to cut test pieces conforming to strip of material. Do not use siliconised material, to prevent
the required dimensions. slip in the grips. Support the free part of the test piece with
Flat stainless steel panels of at least 50 mm x 50 mm, with an extra panel and roll down the test piece with the roller,
two scribed lines over the total width of the panel: one at twice in each direction with a speed of 10 mm/s, without
12.7 mm and one at 25 mm as indicated in figure 1. applying any additional pressure. An automatic rolling
device is strongly recommended.
Rubber covered steel roller as described in FTM 1;
Automatic rolling device is strongly recommended. Set the tensile tester to the following conditions:
• initial distance between the grips: 40 mm
Aluminium foil or polyester coated with a permanent • grip separation speed: 5 mm/min
(pressure sensitive) adhesive to eliminate elongation
effects in the front material of the sample. The After a dwell time of 20 ± 2 minutes, the test panel shall
overlaminating film to withstand 100 Newton. be placed in the fixed grip of the tensile tester. The bottom
FINAT TECHNICAL HANDBOOK 2014 |

of the grip shall be in line with the scribed line at 25 mm.


In case of the fixed grip is connected to the load cell: set
test conditions the force reading of the tensile tester to zero, to adjust for
the weight of the panel. Move the lower grip to its starting
23°C ±2°C and 50% RH ± 5% RH. The samples shall be
conditioned for at least 4 hours before testing.

38
position and tighten the free end of the test piece firmly notes
to prevent slipping. Start the tensile tester and wait until
panel and construction are completely separated. Record 1. The test plates must be thoroughly cleaned so that no
the maximum force during this test and the mode of failure trace of adhesive, grease, silicone or moisture is left
for each test piece individually. The codes for the failures on the surface. The following solvents can be used to
modes are listed below. clean the test plates:

Failure description code • Diacetone alcohol non-residual,


CP Clear Panel - no visible stain on panel. technical grade or better
PS Panel Stain - discoloration of test area, • Methyl Ethyl Ketone (MEK)
but no tacky residue. • Acetone
CF Cohesive Failure - the adhesive film is split during • Methanol 95%
the test, leaving residue of adhesive on both the • n-Heptane
panel and the front material. • Ethyl Acetate
AT Adhesive Transfer - the adhesive separates cleanly
from the front material, leaving adhesive film The cleaning material must be absorbent, e.g. surgical
on the test panel. gauze, cotton wool or tissue. To be suitable, materials
The approximate extent of transfer should be must be lint-free during use, absorbent, contain no
quoted as percentage additives that are soluble in the solvents listed above,
and made exclusively from virgin materials.

results Dispense one of the solvents listed above on to the


panel, wiping it to dryness with fresh absorbent
Calculate and report the mean value as well as the cleaning material. Repeat for a total of three washes
standard deviation of the maximum forces in Newton with the solvent. Final wipe shall be with MEK or
per 12.7 mm width (N/12.7 mm). Also report the failure acetone.
code in case the same failure mode occurred for all five
measurements. In case different failure modes occurred, Alternative methods which remove contamination
calculate and report the mean, standard deviation and properly can be adopted, e.g. ultrasonic cleaning.
number of measurements for each code individually
(results with failure codes CP and PS can be combined). Prior to use, the cleaned plates should be left for 4
hours under standard test conditions. Care should be
taken to handle clean plates by the edge only.
repeatability
2. Static (FTM8) and dynamic shear do not correlate.
The variance coefficient for five measurements is about 3. Changes in speed and substrate need to be reported.
3-6%. 4. Panels of float glass can also be used.

Issued October 1995


remarks Revised March 1999
Revised May 2001
The relationship between shear force and test area is
curvilinear. The standard deviation increases with the width
of test piece.
FINAT TECHNICAL HANDBOOK 2014 |

39
FTM19
recycling compatibility of
self-adhesive labels

introduction test material


The method is based on research of the INGEDE, which Label paper coated with adhesive.
was conducted at TU Darmstadt and PTS Munich. The
testing procedure should provide the basis for further
developments in adhesive technology as well as for test methods
assessment of ex-istent techniques. It simulates the
recycling conditions applied in the Paper and Board
Industry. As some paper mills are converting 100%
recovered paper, “stickies” have become a serious INGEDE-methods 4 and 12
problem in the papermaking process. Self-adhesive labels www.INGEDE.Org.
are, among others, a source of adhesive residue within
the re-covered paper. Scattered labels are considered
insignificant. However, label supplements of magazines results
returned in batches may cause substantial interfer-ence
and expense in the process of papermaking from recovered European Recovered Paper Council (ERPC)
paper. http://www.paperforrecycling.eu/publications/erpc-
publications
Publications: 18 July 2011
scope Assessment of Printed Product Recyclability
Scorecard for the Removability of Adhesive Applications
This test method allows the user to determine the
behaviour of self-adhesive labels in the recycling process of Basis for the scorecard is INGEDE-project 129 09
recovered paper. “Preparation of an Adhesive Application Database and
Recovered paper contains variable types of labels which Development of a Recyclability Scoring System (Adhesive
may generate stickies and thus reduce the quality Applications) dated 13 October 2010, Paper Technology
of recovered paper products or lead to problems in and Mechanical Process Engineering (PMV),
processing. Technische Universität Darmstadt

definition evaluation
Recycling compatible labels are paper labels whose As described in the assessment of the scorecard, self
adhesive does not interfere with the processing of adhesive laminate must reach a positive score in order to
recovered paper. The adhesive should preferably form large attain a satisfactory recyclability.
stickies which can be removed via screening process. The
particle size should exceed 2000 µm. Issued December 1995
Revised March 1999
Revised May 2001
Addresses revised February 2009
Revised June 2012
FINAT TECHNICAL HANDBOOK 2014 |

40
fluorescence and whiteness

FTM20
introduction B. Whiteness
Whiteness is the result of basic white colour of the material
Fluorescent substances in papers, inks and coatings and the effect of optical brightener added. The effect of
are used in labels for spotting and identifying particular optical brighteners can only be appreciated under a light
types of labels. Fluorescent brighteners impart increased source containing ultraviolet similar to daylight.
brightness or whiteness to label papers. Assessment of
whiteness requires a specified standard light spectrum 1. A set of twelve whiteness calibration plates was
including a defined range and intensity of ultraviolet available from CIBA-GEIGY.
radiation. Steps 1 to 4 do not contain any optical brightener but
have decreasing doses of yellow pigment. Steps 5 to
Fluorescence is the emission of light in the visible or 12 have increasing doses of optical brightener. CIBA
adjacent UV or IR spectrum, from matter that is suitably GEIGY no longer produces this set, but it is still used
energized by incident radiation. The whiteness of paper or as common standard.
textiles may be enhanced by the fluorescence of ‘optical Based on the same concept, LAETUS has developed
brighteners’ that convert the invisible UV component a ruler with a twelve step whiteness scale allowing
of daylight into visible light. The material thus appears visual assessment of the whiteness of a paper surface.
brighter and whiter. Again, the light used for such an assessment should
combine UV-light, otherwise no fluorescence will
The whiteness of an optically brightened paper depends occur. Comparative testing is also possible using the
on: analogue output (in milliamps) of a fluorescence
1. chemical structure of the optical brightener; testing device.
2. concentration of brightener;
3. the ‘activation potential’ of paper fibres in relation to 2. The best assessment of whiteness is obtained using
the brightener; a spectrophotometer that allows UV calibration of its
4. the UV component of incident light (this means that light source (normally standard source D65).
for correct measurement of whiteness a well- One such device is the Datacolor Elrepho 3000.
defined standard light source is required). White is in fact a colour like red, green or blue and
may be determined with colorimetric methods. The
difference is that white has high brightness and low
test methods saturation, which makes measurement more difficult
than for a high saturation colour. In the literature one
For inspection and control purposes test methods outlined finds over 100 whiteness formulas. The most practical
here concern (A) fluorescence and (B) whiteness. whiteness formula is the one developed by E. Ganz
(see appendix). Ganz ratings correlate with the CIBA
A. Fluorescence GEIGY scale as follows:
1. A surface printed with fluorescent inks or optical
brighteners is viewed under UV light which reveals GANZ rating CIBA-GEIGY scale
whether the print is as intended. -2 1
2. Actual measurement of fluorescence is possible with 5 2
equipment (as supplied by SICK or LAETUS) that emits 25 3
ultraviolet light of controlled intensity and measures 50 4
reflected light at longer wavelengths. A pre-set 70 5
threshold allows the equipment to decide whether the 90 6
printing is satisfactory or whether a label is present or 105 7
not. 130 8
FINAT TECHNICAL HANDBOOK 2014 |

150 9
175 10
185 11
210 12

41
FTM20 fluorescence and whiteness

appendix test equipment


Fluorescence is a form of luminescence, the emission See Section 3 of this Handbook.
of radiation in the form of light when an electron
changes from a state of higher energy to a lower state. For any verification or calibration of the LAETUS scale,
In fluorescence this is caused by absorbed radiation, please contact the scale maker: Laetus (former Romaco).
mostly ultraviolet followed by emission in longer, visible
wavelengths. Luminescence covers fluorescence and
phosphorescence, fluorescence lifetimes being from 10-6 ganz whiteness formula
to 10-9 seconds, phosphorescence lifetimes being from
10-4 to 10-2 seconds. Judgment of neutral whiteness varies from person to
person. That is why in the GANZ formula (or Ganz-Griesser
For measurement of these phenomena a well-defined formula)
light source is important, i.e. constant output and constant
spectral characteristic. Three types of standard light sources W=(D.Y)+(P.x)+(Q.y)+C
have been defined: A, C, D65.
For FTM 20 only source type D65 is of interest, as it where Y, x, y are luminance or luminosity and chromaticity
approximates average daylight with a colour temperature of coefficients or tristimulus reflectance factors, GANZ
6500K. It emits sufficient ultraviolet to induce fluorescence parameters D, P, Q, C are introduced. They reflect the
of optical brighteners. judgment of the majority of observers.

light sources literature


1. For a first approximation, natural daylight may be used 1. E. Ganz, Whiteness: photometric specification and
instead of a standard light source. However, daylight colorimetric evaluation. Appl. Optics 15 (1976) 9 pp
varies in colour temperature and intensity. 2039-2058.
2. Rolf Griesser (1979), Methods and uses of colorimetric
2. Artificial daylight sources such as those available evaluation of paper. CIBA-Geigy pamphlet 7009, pp
from HERAEUS provide a much more constant source 25-29.
approximating D65.
Fluorescent marking standard negotiations are going on in
3. Light cabinets are offered on the market, having lamps the labelling industry to establish a standard for fluorescent
with different dominant wavelengths, E.S. 254 nm identification of labels, to ensure optimal detection by an
and 360 nm. With such a cabinet one can observe the appropriate luminescence probe. Enquiries: Sick Vertriebs
activity of different optical brighteners. GmbH, www.sick.de. (See also Section 3.3).

4. When the purpose is to test fluorescence as Issued March 1999


such, without a basic whiteness of the material Revised May 2001
(for instance, a transparent film overprinted with Revised May 2004
fluorescent ink), an ultraviolet source should be Addresses revised February 2014
used, normally a UV-A source with 380 nm dominant
wavelength.

5. The best source for testing whiteness is a standard


FINAT TECHNICAL HANDBOOK 2014 |

D65 source used under the standard lighting


conditions of an Ulbricht integrating sphere. Also, the
UV spectrum of the source (generally a flash tube)
needs to be calibrated.
These requirements are fulfilled in instruments such
as the Datacolor Elrepho 2000 and similar instruments
from other suppliers.

42
ink adhesion - basic
FTM21
scope procedure
This method allows rapid assessment of the degree of
adhesion of a printing ink or lacquer to a filmic label stock. 1. Tape test
Lay the specimen on a smooth, flat, hard surface and
apply the adhesive tape, leaving a small part of the
definition tape unfixed to the test piece, ensuring that no air
bubbles are trapped under the tape.
The printing ink or lacquer is applied to the substrate and
cured on the printing press or using a standard method Using the FINAT roller, press down the tape by passing
appropriate for the type of ink. the roller twice in each direction over the specimen,
and then bend the unattached part of the tape back
The ink adhesion is then estimated by the amount of ink on itself at an angle of 180°.
that can be removed when adhesive tape is applied and
peeled off. Within 20 minutes after rolling down the tape, mount
the specimen in a frame or use one hand to hold
The resistance of the ink to mechanical removal is also the specimen firmly, then pull the free piece of tape
measured by scratching the ink and by deformation under towards you using the other hand: at first slowly under
pressure. constant speed, then very rapidly and accelerating.
(The faster speed is the more aggressive test).

test equipment The performance of the specimen is recorded by


comparison with control samples which have been
A means of applying and curing the ink. previously measured, or by reference to the following
grading:
Adhesive tape of high peel adhesion (‘aggressive’), for
example tesa 4104 or 3M Scotch® 810 MagicTM tape. Grade 1 No removal of ink
Grade 2 Slight removal of ink (< 10%)
FINAT roller to smooth the tape over the test piece Grade 3 Moderate removal of ink (10 - 30%)
Grade 4 Severe removal of ink (30 - 60%)
Metal spatula Grade 5 Almost complete removal of ink (> 60%)

Gloves 2. Mechanical tests

Scratch test
test pieces Place the test piece against a firm, flat backing, and
rub a blunt metal implement (for example, a spatula)
If the required ink has not already been applied to the back and forth over the test piece until the ink starts
substrate as part of the printing process, prepare samples to be removed from the substrate. Record the number
for testing by coating the ink to a uniform thickness (for of rubs required to fail the sample, and compare this
example, with a Meyer bar for low-viscosity inks) and to standard samples to determine if the sample passes
curing the coating as recommended by the supplier. A-4 or fails.
sheets are a conveniently-sized sample for this test. Note: an instrument should be chosen which does not
cut the ink (a printer’s knife is not suitable) and which
is consistent between operators (a fingernail is not).
test condition
FINAT TECHNICAL HANDBOOK 2014 |

Rub test
23°C ± 2°C and 50% RH ± 5% RH. Place the test piece against a firm, flat backing, and
If practical, the test pieces should be conditioned for at press your thumb firmly onto the test piece and
least four hours prior to testing. twist it back and forth. Compare the test piece with
previously-assessed control samples to determine if
the piece has passed.
Note: it is recommended that appropriate Health
& Safety measures are taken in case the ink is
insufficiently cured.
43
FTM21 ink adhesion - basic

notes
1. The presence of waxes and silicones in some inks and
varnishes can result in poor adhesion between the
adhesive tape and the ink surface, and consequently
the tape is unable to separate ink from the substrate
even when the adhesion is poor, leading to a false
‘pass’ result. To address this risk, it is recommended
to adopt both a tape test and another method of
testing ink adhesion when evaluating unfamiliar inks.

2. Different batches of the same adhesive tape can


have very different peel strengths (in excess of the
minimum specified), and therefore give difference FTM22: International IGT Printability tester
results on the same print, so a possibly false “fail”
can arise. For rigorous work, or where ink adhesion
is critical, it is recommended to calibrate new lots of
tape by testing them on printed samples of known
performance before testing unknown samples.

3. If a numerical result from the adhesive tape test is


required, the percentage adhesion can be obtained by
using a cross-hatching tool to score the ink into 2 mm
squares before applying the tape, and then measuring
the number of squares remaining after the tape test is
performed. The cutting tool needs to be constructed
to cut entirely through the ink layer but through no
more than a small fraction of the substrate, otherwise
tear of the substrate will occur.

4. Substrates of weak cohesive strength may split during


this test. In this case the result of the test cannot be
used to determine the ink anchorage.

Issued March 1999


Revised June 2001
Revised May 2004
Revised October 2008
FINAT TECHNICAL HANDBOOK 2014 |

44
ink adhesion - advanced
FTM22
scope test condition
This method allows rapid assessment of the degree of 23°C ± 2°C and 50% RH ± 5% RH.
adhesion of a printing ink or lacquer to a label stock. It is If practical, the test pieces should be conditioned for at
designed for the testing of digital print media. least four hours prior to testing.

definition procedure
The printing ink or lacquer is applied to the substrate and 1. Tape test
cured on the printing press or using a standard method Lay the specimen (30 mm by 175 mm) on a smooth, flat,
appropriate for the type of ink. hard surface and apply the adhesive tape, ensuring that no
The ink adhesion is then estimated by the amount of ink air bubbles are trapped under the tape.
that can be removed when adhesive tape is applied and Using the FINAT roller, press down the tape by passing the
peeled off. roller twice in each direction over the specimen, and then
bend the unattached part of the tape back on itself at an
angle of 180°.
test equipment Fix each strip in the machine, so that the tape can be
stripped away from the printed substrate at an angle of
A means of applying and curing the ink. peel of 180°. Set the machine to operate at 300 mm/min
jaw separation rate.
Adhesive tape of high peel adhesion (‘aggressive’), for
example tesa 7475 PV2 (acrylic based), tesa 7476 (rubber
based), tesa 4104 or 3M Scotch® 810 MagicTM tape. evaluation
A standard FINAT test roller. The peel value is expressed as the average result for the
strips tested in Newton per 25 mm. The peel force gives
A tensile tester or similar machine, capable of peeling a an indication of the force that has affected the ink and
laminate through an angle of 180° at a jaw separation rate an approximate measurement of the adhesion of an
of 300 mm per minute and with an accuracy of ± 2%. overlaminate to the ink. The colour is measured on the
printed substrate before and after removing the tape. The
Spectrophotometer, e.g. X-Rite DTP22, Datacolor Elrepho colour difference is expressed in ΔE.
3000, Hunterlab Ultrascan XE.
ΔE measurements can be rated as:
ΔE = 0 - 3 Excellent
test pieces ΔE = 3 - 5 Very good
ΔE = 5 - 10 Good
The ink is brought onto the substrate. After that, a certain ΔE = 10 - 15 Acceptable
period of time has to be taken into consideration, to make ΔE = 15 - 20 Poor
absolutely sure that the ink is completely hardened and/ ΔE = 20 - 25 Unacceptable
or dry. If the print system works with a one or more colour
system, is preferred that the adhesion of the pure colours
is evaluated, and not that of a combination of colours. remark
The adhesion of the ink can be evaluated by measuring This test is based on FTM 21.
FINAT TECHNICAL HANDBOOK 2014 |

the colour before and after the application of the adhesive


tape. The amount of ink that has been removed can be
expressed, in ΔE, by the colour change measured by the note
spectrophotometer, on the ink coated sample before and
after application of the adhesive tape. The presence of waxes and silicones in some inks can lead
to false “pass” results. Therefore it is important to mention
the peel adhesion value.
Issued June 2001
Revised: October 2008
Revised: January 2014
45
FTM23 A die-strike for paper

scope procedure
This test method allows the converter to assess the Stain solution Preparation
degree and consistency of die strike and cutting during the If a pre-prepared stain solution is used (such as “Shirlastain
conversion process. A”), then no stain solution preparation is necessary and the
The method can be used during press make ready to solution can be directly used.
assess the condition and settings of cutters, to prevent For all other dyes a stain solution needs first to be
label dispensing failures or web breaks during high speed prepared. The following steps outline the procedure to
dispensing. The test is applicable to paper based liners. prepare a ‘typical’ stain solution where the concentration
level of dye is approximately 0.5 wt%.

definition a. Take a 1litre container (a capped polyethylene bottle is


suitable), and place on an electronic balance.
The display, by use of water based coloured dye solutions,
of silicone or paper damage caused by die-cutting. b. Wearing the appropriate safety equipment*, and
taking care when handling the dye, weigh out carefully
5g of dye into the container (Malachite Green Oxalate,
test equipment Neocarmine A, Methylene Blue or Chrystalline Violet
are some of the recommended materials).
Dye Solution
(See procedure for different dye solution preparations) c. Measure out 1 litre of distilled water using the
measuring cylinder and add to the container. Seal and
Electronic Balance shake the container thoroughly to dissolve the dye.

1 litre measuring cylinder *Safety comment


• Particular care should be taken to read and follow
Protective Gloves the safe handling instructions for the dye as many
of the materials are hazardous in their pure state.
Cotton swabs Although the final 0.5 wt% dye solutions are not usually
considered hazardous, it is still recommended to wear
Sample Bath protective gloves when handling them.

Clean Water Stain test


• 1. Quick – End of press Test
Stopwatch or Clock Remove the labels from the die cut sample.
Wet a cotton swab liberally with the dye solution.
Wipe the surface of the exposed silicone release liner,
test pieces where the labels have just been, with the dye-soaked
swab.
The test specimen should be at least one complete width Wipe off the excess dye solution from the silicone
and repeat of the cutter. release liner with a dry swab and assess the die-cutting.

test conditions
FINAT TECHNICAL HANDBOOK 2014 |

No special conditions apply.

46
Retain samples indicating acceptable results in envelopes
to support traceability. Note that some dyes (such as
Malachite), may fade over time when exposed to a strong
light source. To avoid this, electronic scanning and storage
of the image may be used.

safety
It is strongly recommended to carefully read and follow
the Safe Handling instructions for the dye being used
(especially when handling the undiluted dye during
solution preparation). In addition, it is recommended to
always wear protective gloves , even when handling the
final dye solution.

• 2. Formal Assessment - Laboratory Conditions notes


Wearing protective gloves, prepare two baths of
appropriate size, one containing not more than 1cm The most commonly used dye solution is Malachite
height of the prepared dye solution, and the other of solution. This based on using the dye Malachite Green
clean water. Oxalate (Basic Green 4), C.I. number 42000. Malachite
Slowly delaminate and remove labels from the die cut solutions should be stored in well closed containers and
sample under evaluation, taking care not to damage or kept away from exposure to daylight. Storage life of the
crease the liner in any way. solution is about 1 month.
Take the sample in both hands and ‘float’ it, silicone
side down, on the surface of the dye solution, taking Alternative dyes could be used to replace Malachite Green
care not to allow contact of the solution with the Oxalate, such as;
reverse side of the liner. • Chrystalline Violet
Allow the sample to remain in contact with the solution • Methylene Blue
for 30 sec and then remove the sample, allowing the • Neocarmine A – Recommended for yellow coloured
dye solution to drain back into the bath. liners as the colouration is red
Take the sample still in both hands and place, silicone
side down’ into the clean water bath and agitate gently If a pre-prepared dye solution is preferred, then one
to remove excess dye. recommendation is to consider SHIRLASTAIN ‘A’ which is
After cleaning, remove and place the sample between supplied by:
any suitable paper materials to dry (e.g. tissue paper or
cotton wool swab). SDL Atlas Ltd.
www.sdlatlas.com

results For addresses consult section 3.3. of this book.

Assess the die-strike pattern for intensity and consistency. Issued May 2001
Look at the reverse side of the liner for complete
penetration. There should be no signs of Dye penetration
FINAT TECHNICAL HANDBOOK 2014 |

through the backing.

The deeper and more visible the die-cutting, the greater


the risk of the adhesive adhering into the backing which
will cause the labels to fail to dispense. Excessive visible
damage of the backing can also give rise to liner web
breaks.

47
FTM23 B die-strike on clear filmic liners

scope test procedure


This test method describes a technique for assessing die- 1. Take a length of die-cut labels equivalent to at least
strike on filmic release liners. twice the repeat of the die-cutter.

2. Remove all labels from the backing liner and note the
definition position of each label relative to the die-cutter.

The evaluation of backing damage or marking to the liner 3. Visually inspect the die-cut quality to check for any
that may be caused due to kiss cutting via a die. obvious, excessive damage. If an area of damage
is observed that causes concern, particularly in the
transverse direction, then a tensile test should be
background carried out on this area.

Label stock generally consists of face stock on a backing 4. Cut a strip of appropriate width and length for the
liner. Once the matrix has been stripped from the face tensometer test in use (jaw width and separation) to
stock the web integrity is maintained by the liner. If a include the area of damage. Take care not to introduce
misaligned die should cut into the liner excessively this any edge knicks that may cause unrelated failure by
could reduce the tensile strength of the web sufficiently using a sharp cutting tool.
to cause a web break. As such, damage in the transverse
direction (TD) across the web can be more of an issue than 5. Place each end of the liner strip into the respective
in the machine direction (MD) along the web. jaws of the tensometer & secure tightly.
6. Perform a tensile test according to the standard
When placed under increasing tension most filmic materials operating conditions for the instrument.
will show elastic behaviour up to the yield point, after
which they will deform irreversibly and eventually break.
In labelling applications the tensions used will generally results
not be above the yield point and so if the liner can be
tensioned to this point successfully without breakage then 1. Each strip should achieve a yield point prior to
any die-strike impressions should not cause a problem. snapping – this constitutes a pass.
2.
For some materials, for example polyester films such as 3. If the liner snaps prior to reaching the yield point then
polyethylene terephtalate (PET), the yield point can be this is a fail.
difficult to locate accurately. • If this is achieved on the cut from the die, then
In this case measurement of F5 (ensuring that the liner can note & advise that the die cutter should be
be loaded to 5% strain) can be used as a substitute target. adjusted accordingly.
• If the sample damage has not occurred on the
die-cut portion of the sample then repeat the
test equipment test, as the break may have been initiated by
edge damage when cutting into strips, or similar
Tensometer (e.g. Instron, Hounsfield, Lloyds, etc.); miscellaneous damage.

Cutting implement.

test conditions
FINAT TECHNICAL HANDBOOK 2014 |

No special conditions apply.

48
note
Die-strike through filmic liners can be influenced by several
parameters. We recommend to carefully check them in
case of die-strike problems:

• the solidity and robustness of die-cutting unit;


• the tool diameter should be adjusted according to the
width of the printing equipment;
• the tolerance between magnetic and anvil cylinder;
• the quality of the flexible die (weareness - height profile
of the die);
• the consistency of the liner thickness;
• the temperature at which the die-cutting operation take
place (influence of UV light on the film and adhesive
softness;
• In case of problems:
• Adjust the cutting angle to improve the die-cutting
operation.
• Verify the tension of the web (avoid too high
tension).
• Strip the matrix immediately after the die-cutting
operation to avoid recovery of the adhesive
between the die-cutting and the stripping
steps. Cool down the laminate before die-cutting
operation.

Issued October 2005

FINAT TECHNICAL HANDBOOK 2014 |

49
FTM24 mandrel hold

scope procedure
This test is used to determine the ability of a pressure Use new test materials for any new test.
sensitive adhesive to adhere to cylindrical curved surfaces. Clean the glass tubes/rods with acetone or other suitable
solvent (heptane) before using them, to avoid any deposit,
grease or dust. Other tubes/rods not made from glass
definition should be used such as supplied. Avoid to touch them with
fingers before any test.
Mandrel adhesion is defined as the edge lifting (expressed Remove the backing from the face material avoiding curling
in mm) of pressure sensitive adhesive coated material of the face material, and touching the adhesive surface.
from standard cylindrical rod / tubes of small diameter, Apply the sample around the tube/rod with the long side of
after being applied with light finger pressure for a specified the sample perpendicular to the axis of the rod/tube.
amount of time.

test equipment
Rack to support tubes/rods without having contact
between test samples and supporting rack.

Rods/tubes of 8mm and 15mm diameter (the diameter


of the mandrel should be representative of the end-
use). Rods/tubes made of glass and polyethylene. Other
materials and diameters may be used as necessary, and
reported as such.

The results of the tests are very much dependant of the


face materials used. These materials need to be well
identified and their specification well known. Put some light finger pressure to obtain sufficient
adhesion/contact between the whole adhesive coating
area and the test tube/rod. (It may be easier to cut the
test pieces label longer than needed and to trim the excess of label
sample at time of application on the tubes/rods.)
The test piece dimensions should be adapted so that the
length of the sample label covers 3/4 of the circumference
of the test tube/rod.
The width of the sample should be half of the length of the
label.
Examples:
10 mm x 20 mm for a 8 mm diameter tube/rod
15 mm x 35 mm for a 15 mm diameter tube/rod

Test pieces should be cut in the machine direction AND


in the cross direction. 3 test pieces should be taken from
material sample. Cuts should be clean and straight.
FINAT TECHNICAL HANDBOOK 2014 |

test conditions
Test pieces should be conditioned at 23°C ± 2°C and
50% ± 5% RH during at least 16 hours before being cut.
Other conditions might be used, but this must be clearly
reported.

50
Failure Description Code
CF Cohesive Failure - the adhesive film is split during
the test, leaving residueof adhesive on both the
panel and the front material.
AF Adhesive Failure - the adhesive separates cleanly
from the front material, leaving adhesive film on
the test sample.
AT Adhesive Transfer - the adhesive separates cleanly
from the front material, leaving adhesive film on
the test panel.
The approximate extent of transfer should be
quoted as percentage

Indicate any deviations from above procedure.


The labelled tubes/rods are inspected after 1 week. The
edge lifting if any, is measured in mm at each side of the
label (l1, l2). note
Edge lift is the total length of each label no longer in contact
with the test tube/rod divided by 2, e.g.: (l1 + l2)/2. Specific application equipment can be used to reduce
variation of results due to “light finger” application
procedure.

Issued May 2001

results
Report identification of the samples and test tubes/rods
materials.
Calculate and report the mean value of the 3 tests for the
edge lift measurement described above for each sample/
testing material, and the time evolved since application of
the face material.
Describe the type of failure (AF, CF, AT).
FINAT TECHNICAL HANDBOOK 2014 |

51
FTM25
evaluation of the silicone
coverage of coated papers by use
of a water based stain test

scope test equipment


This test method describes a technique for assessing the Cobb Tester with ring of an approximate diameter of
quality of coverage of silicone coatings. This test can only 11.5 cm.
be carried out on paper based liners which can be coloured
by the stain test solution utilised. Count down stopwatch with alarm function.

Small container, marked to show level occupied by 200ml


definition of Stain.

Coverage quality is commonly evaluated by water soluble Test stain solution.


dye stain testing.
There are many dye stains used, available both in solution Absorbent cleaning paper.
and powder form (These include Shirlastain A, Malachite
Green, Methylene Blue, Hahn Stain, Rhodamine 6 GDN,
Neocarmine A).
For paper substrates only, a quantity of liquid dye stain is
applied to the silicone coated liner for a finite period of
time, rinsed or wiped off and the liner dried.
Coverage is evaluated either qualitatively by visual
inspection or quantitatively with a colorimeter. For
the water based stain test, an area where the dye had
contacted the coated paper should be totally uncoloured
or of uniform and light colour if the quality of the
silicone coating is perfect (i.e. uniform and complete
coverage of paper fibres and well cured). Imperfections
or discontinuities (such as exposed paper fibres) in the
coverage typically result in “dark” areas. These “dark”
areas are where the dye has been absorbed by the paper
substrate. The background colour and the colour associated
with the silicone defects is characteristic of the specific dye
stain employed. With a paper substrate and Shirlastain A
dye, a “well cured” silicone release coating with excellent
coverage will yield a “yellow” colour in the test area.
Defects will appear as red-to-brown coloured stained
areas.
test pieces
In general the darker the coloration from the stain solution,
the poorer the silicone coverage. Poor silicone coverage Where possible, several samples should be evaluated from
will, in many cases, lead to problems of release as the the release sheet.
adhesive will adhere strongly to any unprotected paper If these are from a known position on the web their
fibres thus causing elevated release values. location should be noted for reference.

test condition
FINAT TECHNICAL HANDBOOK 2014 |

No special conditions apply.

52
procedure results

    1. After five minutes visually examine the test sample.


There should be NO sign of penetration by the
stain solution. Penetration of the stain solution is
identified by the appearance of dark brown lines or
spots. If the sample is deemed satisfactory, it should
be used as a benchmark for future tested samples.
Each backing paper type should have a benchmark
sample (i.e. a siliconised sample with acceptable stain
performance/coverage).
2. For future tests compare results against the
benchmark sample for the backing paper type. Results
should be the same as or better than the accepted
For Shirlastain “A” standard.
1. Cut a 14 cm x 14 cm (or size suited to Cobb tester 3. Samples are commonly graded on a scale of 0 – 10
used) sample of release liner (or liner of self-adhesive 0= Total stain with coloration as for
laminate after removal of face material). Care must be 4. unsiliconised paper
taken to ensure that there are no holes or perforations 10 = Perfect stain with no sign of coloration
present in the backing paper. The acceptable level would need to be assessed in
In all cases, regardless of the substrate or dye used, correlation with other application tests.
care should be taken to avoid contact with the silicone 5. For more quantitative assessment the degree of
surface prior to testing since this may introduce coloration of the coated paper can be measured by
imperfections to the stain result. means of a colorimeter. In these cases a comparative
2. Place the backing paper sample on the base of the measure is made Vs the base paper and a delta E
Cobb tester, silicone side up, under the test ring. value is quoted. This method can give a quantification
3. Clamp the ring securely in place to prevent the stain of the stain test but attention must be paid to
leaking out during the test. regularity of the coating and usually this test must be
4. Add 200ml of Shirlastain ‘A’ solution to the Cobb and accompanied by a descriptive comment.
start the stopwatch.
5. At the time of exposure chosen for the test
immediately drain off the stain solution, unclamp the
test ring and lift away from the sample.
Shirlastain – typically 2 minute exposure time (for
other stain types see later section)
6. Blot the test piece dry with absorbent paper (DO NOT
RUB) and allow the dried sample to sit for a further
five minutes (method usually recommended with
Shirlastain ‘A’).
Alternatively the sample can be rinsed under a (Yellow glassine paper with different levels of silicone coverage,
running tap and then blotted dry (method usually stained with a solution of Methylene Blue.)
recommended with malachite green).
Typical stain solutions used
Shirlastain ‘A’ solution reacts with unsiliconised paper
fibres turning them dark brown. The better the quality
FINAT TECHNICAL HANDBOOK 2014 |

of the silicone coating, the better the paper fibres will


be protected to give a clean yellow stain. The darker
the stain, the poorer the coating quality.

Shirlastain ‘A’ is supplied by:


SDL Atlas Ltd.
www.sdlatlas.com
For addresses please consult section 3.3. of this book.

53
FTM25
evaluation of the silicone
coverage of coated papers by use
of a water based stain test

Whilst Shirlastain is a commonly used stain material 2. In all cases the hydrophobicity of the base paper
there are occasions where other materials are more should be taken into account and a test of the base
suitable (either due to toxicity constraints or from paper with the stain solution must show a deep
coloration of the base paper) coloration. In the case of some hydrophobic papers
where penetration of the liquid stain is much lower
Alternative stain solutions a moderate silicone coverage can give a perfect stain
Malachite green – typically 0.5% solution left in and in such cases the test may need to be adapted
contact for 1 minute (for example longer time in contact with stain solution
Grade - Malachite Green Oxalate (Basic green 4) or increased solution concentration).
Supplied as crystals for dilution in water; C.I. Number N.B. Care must be taken in interpretation of
- C.I.42000 phenomena mentioned in notes 1 & 2 as obviously
For yellow coloured papers it can be more suitable the heat treatment recommended in note 1 could lead
than Shirlastain. also to the phenomenon mentioned in note 2.

Neocarmine A – typical 1 minute exposure of 3. Larger areas of silicone coated release liner can be
prepared dye solution. This dye tends to show up evaluated by preparing a solution of dye in a large
faults in the coating as red spots. For yellow coloured shallow dish and then bringing the silicone surface of
papers it can be more suitable than Shirlastain. the liner into contact with the solution. Care should
be taken to avoid entrapment of air bubbles under the
Methylene Blue – typically 0.5% solution, 2 minute silicone surface or through foam on the surface of the
exposure time. dye solution.

Crystalline Violet - typically 0.5% solution, 2 minute 4. For films or polycoated kraft substrates a “powder
exposure time. dye test” is used to reveal faults in the silicone
coated surface. Whilst this method can not show the
differences in coating quality as well as the solution
notes based dyes used on papers it is useful to give an
overall picture of coating continuity, highlighting
1. It must be noted that a paper coated with a poorly miscoats, marks or streaks. A dry powder dye is lightly
cured silicone can absorb dye stain and provide false applied to the surface and carefully spread over the
results. For paper substrates, another sheet of coated area to be tested. The fine powder has a tendency to
substrate, ideally taken from an adjacent position to cling to the silicone coating and not the uncoated film
the first sample, can be re-heated in a laboratory oven or poly coating.
for two minutes at 120ºC for example. Of specific interest is the uniformity of colour which
After the sample has been allowed to cool back results after the dye stain is removed. For the powder
to room temperature, the dye stain test can be test on films or polycoated kraft substrates, light
performed. If there is no significant difference in the coloured areas are indicative of poor coverage (or
uniformity of the colour between the samples, it can conversely, a uniform dark colour is indicative of good
be assumed that the initial sample was “well-cured.” coverage) with the Waxoline violet powder dye.
If there is a significant difference, the state of cure of
the initial sample of coated liner is in question. Nigrosin dye for powder dye coverage test
This heat treatment works fine for thermally cured Grade Nigrosin, Alcohol soluble (Solvent black 5)
silicones; free radical curing silicone acrylates have Supplied as very fine powder for direct use as solid
their final properties immediately after exposure to C.I. Number C.I.50415
UV light or electron beam. The cationic curing silicone
FINAT TECHNICAL HANDBOOK 2014 |

epoxies need some time for a post curing process. Other dyes for powder test
Thermal treatment can accelerate this natural process • Waxoline blue, green & violet
for this type of radiation curing silicones. • Dark coloured “eye shadow”
• Any other fine powdered dye/pigment which
clings to silicone surface

Issued August 2005


Revised February 2014

54
wash-off paper and film labels

FTM26
scope procedure
This test procedure describes the preparations and testing
of pressure-sensitive adhesives, which can be washed off
with aqueous alkaline solution.

This test procedure can be used for the testing of the


detachability of pressure-sensitive adhesives in a hot,
aqueous alkaline solution.

definition
“Wash-off ability” is the ability of an adhesive to detach
itself quickly and completely in a 1.0-2.0% solution of
sodium hydroxide at 65 - 75°C.
The content of NaOH and the wash-off temperature has to
be noted in the report.

test equipment
Heatable magnetic stirrer.
Magnetic stirring bar. After storage, fill the bottles with water at the testing
2 - 5 litre glass beaker. temperature and immediately immerse the bottle in the
Thermometer. prepared solution of sodium hydroxide at the testing
Glass bottles (glass bottle type and the pre-treatment of temperature.
the glass surface, such as specific coatings, washings, etc.
have to be mentioned in the report).
results
preparation Indicate the time in seconds until the labels become
detached.
Label and adhesive should be adapted for wash-off
purpose. Report where you find the adhesive after the label has
The label material can be paper or filmic. detached:
Cut out labels with the dimensions 60 x 80 mm from the • On the bottle
finished coating. • On the label
Prior to testing, clean the glass bottles in a dishwasher at • Both on the label and the bottle
min. 65°C.
The use of an alkaline cleaner is recommended.
note
Most of the glass bottles are recycled or re-used bottles.
The life / cycling time of the glass bottle may influence the The type of face stock material, paper or filmic, its
test results. It is recommended to use new bottles after properties and condition such as porous, non porous, semi
FINAT TECHNICAL HANDBOOK 2014 |

the first washing. In any case, the state of the glass bottle permeable, etc, influence the “wash-off ability” significantly.
should be mentioned in the report. Furthermore, printing coverage, especially UV-varnish,
affects the wash-off times. It is recommended to perform
trials with printed labels. Additionally, ageing of the labeled
test pieces glass bottles e.g. outdoor storage, UV-light or humidity may
affect also the wash-off result. Deviations from the testing
Prior to testing, remove the silicone release backing from method have to be mentioned in the report.
the label and stick the label onto the glass bottle. Store
the bond for at least 24 hours under standard climate Issued October 2008
conditions: 23°C ± 2°C, 50% RH ± 5% RH Revised January 2014
55
FTM27
ink rub test for uv printed
labels ink surface against
substrate or ink surface

scope conditions
This test method is suitable for checking out rub resistance Condition should be at 23° ±-2°C / 70 - 77°F ±- ;
of printed UV ink: ink surface against substrate or ink 50% RH ±- 5% RH.
surface against ink surface.
Bad adhesion cannot be detected with this method as long
as scratch or rub resistance is good. The specific resistances preparation and procedure
must be elicited with different methods, e.g. FTM 21. In
difficult cases bad adherence and bad rub resistance can 1. Remove one label from the master reel sample.
occur together. 2. Cut of a short piece of blank substrate from the reel
in the size of the rubber bed on the right hand side of
This test procedure can be handled by lab personnel of a the Ink Rub Tester.
printing factory or a pressman / production manager who 3. Adhere blank substrate to the rubber bed on the right
is instructed to the Ink Rub Tester equipment. hand side of the Ink Rub Tester and adhere the printed
label to the rubber of the 2 lbs* weight. It is important
that the sample on the 2 lbs weight is covered with
definition ink all over the test area.
4. Place the 2 lbs weight completely with label onto the
Normally rub resistance is a question of through curing retaining clip. Both printed label and substrate should
or reactivity of an ink film. Rubbing off or scratching off be facing each other ink side to substrate surface.
describes the damage of an ink surface by mechanical 5. Set up the machine to 100 moves per minute
influence, e.g. two labelled bottles rubbing against each 6. Set the machine to 25 cycles and press start
other during transport. 7. At the end of the cycles, observe the labels for ink rub
Scratch or rub resistance describes the mechanical of or scratch of.
resistance of an ink or varnish surface. 8. If ink rub of or scratch of is present, repeat the test
after the following improvement trials using fresh
printed labels for every trial:
test equipment • decrease printing speed or
• add suitable photo initiator to the UV ink if
Ink Rub Tester by Testing Machines Inc. available
www.testingmachines.com • choose an anilox roll with less volume as long as
colour shade is still sufficient or
Heating cabinet. • add 5% of blending varnish as long as colour
shade is still sufficient
• replace UV bulb
• clean up UV lamp reflector

It is important to do the tests step by step to expose the


real cause of bad rub or scratch resistance. If the problem
cannot be solved 100% at any test take a second sample
and repeat the related test with the best result after 2 h in
an oven at 40°C – 104°F or 8 h at room temperature 21°C
– 70°F*. If the problem persists change the batch of ink. If
Pictures 1+2: Ink Rub Tester there is still no improvement contact the ink supplier.
FINAT TECHNICAL HANDBOOK 2014 |

*N.B. The radical UV system has an element of post


test pieces cure, which can take up to 24 hours.

Printed labels should be fresh from the press.
Blank substrate should be from the same real currently is
printed on.

56
results remark
To give an impression of good and bad test results please For sure the ink surface will be scratched by this test
look at the following pictures. method also if there is a proper curing (Level 1). But it
should not be scratched of (please view picture 3)! Level 1
is always that one to be achieved.
Depending on the substrate quality also this can be
scratched by this test method (please view picture 4).
If the ink should be peeled of by this test than ink adhesion
is an issue together with poor reactivity (picture 5).

silicone in inks
If inks consist of silicone this migrates to the surface and
Picture 3: Slightly scratched ink surface: sufficient result works like a lubrication. Then a rub resistance test can
end in a “faked” good result. Silicone residues should be
carefully wiped of with a 70% isopropyl alcohol before
starting this test.

note
This test is to be repeated with ink side to ink side if
required. Then also the sample on the rubber bed should
have an ink coverage all over the test area.
If wet rub resistance shall be checked repeat the test with
Picture 4: Substrate in comparison: surface is scratched a drop of water applied onto the sample mounted on the
rubber bed on the right hand side of the Ink Rub Tester.

combination printing
In cases of combining water born inks with a UV Flexo
overprint varnish it is reasonable to set up the test as a
wet rub resistance test. Then beside damage of the varnish
surface ink bleeding can be the indicator for bad curing of
the overprint varnish. If ink bleeding occurs not only the
curing of the overprint varnish might be insufficient but also
Picture 5: Bad rub resistance caused by bad ink reactivity or through the curing/drying of the waterborne ink. Then the curing of
curing. Ink can be scratched and rubbed easily. ink and varnish should be checked individually.

Rating scale Required material


Level 1: Slightly scratched surface < 5% damage, no • pipette
scratch off, no rub off, no substrate visible • water
FINAT TECHNICAL HANDBOOK 2014 |

Level 2: Scratched of ink film or rubbed of ink film, • L abels und substrate as described on page two in
< 10% substrate visible chapter “test pieces”
Level 3: Scratched of ink film or rubbed of ink film,
10 - 30% substrate visible * 1 lb = 453.6 g
Level 4: Scratched of ink film or rubbed of ink film, Issued October 2008
30 - 60% substrate visible
Level 5: Scratched of ink film or rubbed of ink film,
> 60% substrate visible

57
FTM28 evaluation of bleeding through paper

scope procedure
This procedure describes the spectrometric assessment Ageing:
of the migration of a label adhesive through the paper • Place the strip (sample B) to be tested in oven, by
substrate at elevated temperature. piling up the strips of samples on top of the other with
polyester films between the samples.
• Do the same for sample C.
test equipment • Take the samples out of the oven after 2 weeks ageing.
Allow to cool to room temperature.
Ventilated ovens.
Testing:
Paper cutter. Differences between aged samples (B) and references
(A and C) can be observed either visually or measured with
Substrate: Label paper, release liner as appropriate, and a spectrophotometer.
polyester film.
1 - Visual comparison:
Reflectance Spectrophotometer Example: Hunterlab
Ultrascan XE. The aged samples are compared to reference A, to detect
any bleed through.
The samples are either ranked on bleed through
test pieces characteristics or on their non acceptance if any bleeding
occurs.
These should be strips from representative samples of label
material. (e.g. of the 3 layers: label paper, adhesive and 2 - Use of a spectrophotometer
release paper)
Reference sample:
For each sample being evaluated, and for each temperature
at which the test will be done, prepare 3 strips of samples • Place the center of sample A or C at the reflectance
of about 5 cm x 20 cm, cut in the machine coated direction. port, with the label paper facing the transmittance port.
• Set the spectrophotometer as follows:
Prepare following samples: • Scale: CIELAB
• Illuminant: C
Sample A: label laminate • Observer: 2°
(face paper ± adhesive ±release paper) • Area view: Large
Sample B: label laminate • Selected Indices: WI E313-98
Sample C: non coated face paper
• Measure whiteness index (according to ASTM E 313) in
the middle of each of the three samples which have
test conditions been prepared.

Sample A is kept as reference for further testing. Aged samples:


Sample B and C are exposed to accelerating aging at 60oC
during 2 weeks. Measure whiteness index (according to ASTM E 313) in
the middle of each of the three samples which have been
Samples B can be tested either : prepared.
FINAT TECHNICAL HANDBOOK 2014 |

• under light pressure from a carton board which will


ensure that the sample remains flat after test,
• or under a pressure of about 70 g/cm2 which would
simulate roll pressure during storage.

Sample C will be aged, and kept under light pressure under


a cardboard to ensure it will remain flat (see samples B).

Above time and temperature can be adjusted to fit special


requirements.
58
results
Calculate the average for each set of 3 readouts.

Average whiteness index of the aged coated samples B = WI(B)


Average whiteness index of reference sample A = WI(A)
Average whiteness index of reference sample C = WI(C)

The bleed through resistance BTR (%) is measured as:

The smaller the drop, the lower the degree of bleed


through and the better the quality of the label.

notes
Detailed information on how to use the Hunterlab
Ultrascan XE spectrophotometer are provided in the
Hunterlab operating manual.

The following internet site:

http://www.hunterlab.com/manuals/appendixa2_5.pdf

is providing explanations on the various color scales, color


difference scales, indices, and procedures available for
display in the data views of Universal Software used by the
Hunterlab equipment.
Universal Software performs integration of reflectance/
transmittance values over the visible spectrum to arrive at
tristimulus X, Y, and Z values. The ASTM 308 is providing
more information on how to calculate the tristimulus
values.

Issued March 2012


FINAT TECHNICAL HANDBOOK 2014 |

59
FTM29
scratch resistance of an uv ink
film on different print materials

scope
This test method describes how to test the scratch resistance
of a UV ink film applied to different printed surfaces.
For this test to give reliable results it is important that the
ink has been cured to a sufficient level, and this can be
checked in advance using FTM. 2, or as a quick check a
thumb smear test can be used.

This test method is also suitable for water based and


solvent based inks and varnishes, although the original test Picture 2: Tip of the Tungsten Carbide Tool
development has been done with UV inks.

This relatively simple test procedure can be performed by specimen


lab personnel of a printing facility or any other who has
been instructed in use of the test equipment. The printed labels should be fresh from the press. The
test can be performed directly after printing or after 24 h
storage.
definition Non printed label material should also be tested to confirm
that the unprinted surface is not being damaged by too
The scratch resistance of an ink is normally dependent on high a spring force, rather than the ink layer itself being the
the level of curing of the ink film both at the surface curing point of failure. This will avoid confusing a failure of the
and within the bulk of the ink. The scratching of the ink film printing with a failure of the label material being printed.
describes the damage of an ink surface through mechanical
means, e.g. by the edge of a metallic spatula.
conditions
test equipment Temperature 23° ±-2° C / 70 - 77° F ±- ;
Humidity: 50% RH ±- 5% RH.
Elcometer 3092 Sclerometer Hardness Tester (referred to
as a „Sclerometer“).
The Sclerometer is provided with three springs which preparation and procedure
operate at different levels of force:
• natural: 0 – 3 N (0 lbf to 0.67 lbf) Preparation of print sample
• Red: 0 – 10 N (0 lbf to 2.2 lbf) 1. Remove one label from the master reel.
• Blue: 0 – 20 N (0 lbf to 4.5 lbf) 2. Put it on a hard surface. A polished steel plate is
prefered. The surface should be free of any scratches/
For each spring a different scale is engraved on the shank marks. If necessary fix the sample in place with
of the Sclerometer matched to the colour of the spring. adhesive tape avoiding any wrinkles.

The tip of the Scleromteter consists of a tool with a 0,75 Preparation of Sclerometer
mm (0,03“) diameter tungsten carbide tip. This is moved Loosen the knurled screw and slide of the collar off the
over the specimen with different preset spring force. Sclerometer. Select the appropriate spring and insert into
the Sclerometer. Always choose the natural sprint as the
weakest to begin. Refit the collar. Find the scale on the
FINAT TECHNICAL HANDBOOK 2014 |

Sclerometer which matches the colour of the spring and


adjust the tip force by sliding the collar to the required
setting on the scale. Tighten the knurled screw.

Procedure
1. Place the Sclerometer perpendicular to the surface
being tested and apply sufficient downwards force to
compress the spring by approx. 2 mm. Do not allow
the bottom of the Sclerometer (other than the tip), to
Picture 1: Elcometer 3092 Sclerometer Hardness Tester touch the surface being tested.
60
2. Move the Sclerometer to produce a linear scratch of Level 3: Ink film is scratched off; surface of printing
approximately 20 mm in length material is visible
3. Inspect the tested surface of the sample for any sign
of damage.
remarks
If the ink surface is not damaged set the spring
compression to the next required force position and repeat There will nearly always be some slight distortion of the
steps 1 – 3. ink surface depending on the selected spring force, even if
the curing of the ink is excellent (level 1 on the scale), but
Once a scratch becomes visible it should be examined the ink film should not be so scratched that the printing
using a magnifying glass, to determine whether there has material surface becomes visible (see image 3 on page 4).
only been a deformation on the ink surface or whether The target should always be to achieve a “Level 1” result.
the ink has been scratched away from the surface. If it
is confirmed that the ink has been scratched from the The wide range of printing materials and printing inks
surface then it is important to identify whether it is only available in the market means that it is not possible to
the upper layers of ink that have been removed (indicating specify a single spring force that can be applied for all
cohesive failure within the ink), or whether the ink has testing. This has to be evaluated for each print sample
been removed down to the printing material. Both the individually. The target should be to identify the highest
level of curing of the ink and the spring force used for possible spring force at which a “level 1” result can still be
the Sclerometer will have an impact on this result. This achieved for that print material and then use this is as a
investigation is important to create comparable test results. minimum for the final printed product using that material.

The advantage of this method is the simplicity with which


results it can be used to reproduce the same level of scratch
resistance for repeated print jobs with the same materials
or jobs using similar materials.

Different self adhesive materials have different softness.


This leads to a different deformation of substrate and ink
and substrate together. The softer a material is, the easier
it might be damaged/scratched. This means that the same
ink on a harder substrate can be tested with a higher spring
force than on a softer material.

Picture 3: Distorted ink surface alongside scratched ink surface silicone and wax in printing inks
Silicone and waxes inside the ink intend to migrate to
the surface after curing. Waxes also have the function of
increasing scratch resistance. These migratory materials
can be pushed aside with increasing spring force, but these
inks can still be tested by this method.

combination printing
FINAT TECHNICAL HANDBOOK 2014 |

Picture 4: Substrate in comparison: the surface is distorted above Where ink is applied in several layers using different
the blue line printing techniques on the same line, it is important to
measure each ink layer separately directly on the printing
The scratch appearance as described in the “procedure” material. This does not mean however that overprinting ink
leads to the following rating scale: layers are not also tested, as it is important to understand
adhesion between different ink layers. This is especially the
Level 1: distorted surface; no ink scratched off; only case if printed using different print processes. The skilled
the ink surface distorted knowledge of the ink supplier is then important.
Level 2: Scratched ink surface; ink has been removed
from surface but surface of printing material is not visible Issued September 2013
61
It is important that a join in a self-adhesive laminate should be
made in such a way that it will minimize problems
joinswhen

2.1
recommended in
converted into roll labels. The join should
self be angled
-adhesive so that the
laminates
feed-in is gradual, the width of facing tapelabels
and backing tape
SECTION for roll
should differ so that there is not too great a step in increased
thickness and the total thickness of the join should be kept to a
minimum in order to avoid damage to or misplacement of the
cutters.
conversion
The following specification is recommended:
a) The angle of the join should be 10° - 30° from the cross
It is important that a join in a self-adhesive laminate should be
made in suchdirection.
a way that it will minimize problems when
converted into roll labels. The join should be angled so that

b) The width of tape on the facing paper should be at least >


the feed-in is gradual, the width of facing tape and backing
tape should differ so that there is not too great a step in
30 mm.
increased thickness and the total thickness of the join should
be kept to a minimum in order to avoid damage to or mis-
placement of the cutters.
c) The width of tape on the backing paper should be broader
than
The following the is tape
specification of the face material > 36 mm.
recommended:

a. The angle of the join should be 10° - 30° from the


d) The tape between the face and the backing paper should be
cross direction.

b.
a smaller tape, at least < 20 mm.
The width of tape on the facing paper should be at
least > 30 mm.
e) The tapes should have a thickness of no more than
c.
0.063mm inclusive of adhesive.
The width of tape on the backing paper should be
g. Where applicable the tapes should withstand the
broader than the tape of the face material > 36 mm.
temperatures involved in label printing processes.

d. f) The tape used on the backing paper should be a colored


The tape between the face and the backing paper Issued October 1985

tape for ease of identification but the tape on the Revised faceOctober 2008
should be a smaller tape, at least < 20 mm. Revised March 1999

e. material
The tapes should have can either
a thickness bethan
of no more a colored tape for a similar reason, or
a white printable tape for use with laminates which are to be
0.063 mm inclusive of adhesive.

f. converted
The tape to paper
used on the backing security
should beor
a sequentially numbered labels, i.e.
coloredwhen alloflabels
tape for ease must
identification but thebe
tape accounted
on for.
the face material can either be a colored tape for a
similar reason, or a white printable tape for use with
g) Where applicable the tapes should withstand the
laminates which are to be converted to security or
temperatures involved in label printing processes.
sequentially numbered labels, i.e. when all labels must
be accounted for.

Tape

Adhesive Face material


FINAT TECHNICAL HANDBOOK 2014 |

Adhesive
Adhesive

Tape
Silicone

Adhesive
Backing paper
Tape

62
processing recommendations

SECTION 2.2
roll stock

1. Generally, self-adhesive paper roll stock can be 10. With UV cured inks, always check the cure before
considered as normal paper with respect to ink choice proceeding. Checks should be made at regular
etc. synthetics, filmic and foil roll stock, however often intervals on UV output of the lamps . It is advisable to
need special materials involving consultation with ink keep the web temperature on re-wind under 24°C.
suppliers.
11. It is advisable to use an antistatic bar at the point
2. Corona treatment is required for filmic face stock of matrix de-lamination for easy matrix removal
to enhance the ink adhesion. When the substrate by neutralizing the generated static charge by de-
is corona pre-treated, it is advisable to refresh the lamination. This prevents matrix break.
corona treatment on press.
12. Avoid excessive tension in reels of finished labels. This
3. Chemically top coated filmic face stock substrates will prevent bleeding and label shifting.
should not be corona treated on press without prior
contact with the supplier. 13. Wind finished labels on to cores of an appropriate size.
Large labels should not be wound on to small cores. It
4. Always check with the Supplier if his material is therefore advisable to use 6” core instead of 3” core
can withstand the intended process conditions, to prevent the label curling.
particularly if excessive temperatures or unusual web
feed patterns are involved. 14. Finished work should be shrouded in polythene prior
to packing.
5. Do not change the winding direction of the roll prior to
conversion, as this will alter the release properties and 15. Wherever possible, the manufacturer’s batch/order
could affect curl problems. references should be retained in case of complaints.

6. Always use the correct die for the product. Therefore 16. To take dust out of the roll stock it is advisable to use
it is advisable to mention to die manufacturer the type a web cleaner on un-wind section.
of face stock substrate.
17. To reduce the static electricity mainly from the filmic
7. Labels should be designed with matrix stripping in roll stock it is advisable to use antistatic devices
mind. Refer to the supplier if complex shapes are between the printing units and before web rewinding.
involved. Wherever possible, use round corners for
labels and avoid narrow matrices. Revised May 2001
Revised October 2008
8. Check the depth of die-cutting before proceeding with
any lengthy run.
Excessive die pressure will cause weakening of
the backing paper / liner and should be avoided
in products intended for high speed automatic
application. Check also the dimensional size of the
label because on filmic you can have a retraction
of the material generally on wide press or during
FINAT TECHNICAL HANDBOOK 2014 |

processing.

9. Use the minimum amount of heat for hot air drying


inks e.g. water and solvent based inks to avoid the
temperature increase of the web. It is advisable to
keep the web temperature on re-wind under 24°C.

63
SECTION 2.2 processing recommendations

filmic sheet stock paper sheet stock

1. Check that the ink is compatible with the product to 1. Self-Adhesive paper sheet stock can be considered
be used and is approved or recommended by the ink as normal paper with respect to ink type, dryers,
supplier. retarders, etc.

2. Allow sufficient unprinted edge trim on the screen to 2. When using self-adhesive sheet stock in offset litho
prevent edge lift due to shrinkage. printing, however the following points should be
noted:
3. Avoid excessive amounts of thinners or retarders to
prevent shrinkage. a) Reset the impression nip between the
blanket and plate cylinder to allow for the extra
4. Ensure that all machinery in the vicinity of solvent thickness. This will reduce problems of tail edge
fumes is fitted with anti-static devices and solvent creasing, misregister etc.
extractors where possible. b) The double sheet trip should always be used to
prevent any damage to plates, etc.
5. Use a minimum of heat to dry the ink in order to avoid c) Always use minimum of damping to prevent
sheet curl. edge waving, etc.
d) To prevent edge curl, always shroud sheets in
6. When using a jet drier for multi-colour runs, shroud polyethylene between colors if multi-colour
the sheets in polythene between runs to prevent machines are not being used.
sheet curl.
3. Finished work should be shrouded in polyethylene
7. When rack drying, avoid changes in temperature or until cut and boxed.
humidity between runs to prevent sheet curl.
4. The Manufacturer’s recommendations on guillotining
8. Always allow sufficient time between passes for each and slitting should be used.
colour to dry. This is of particular importance in the
case of flood coating. 5. Wherever possible, retain the Manufacturer’s batch/
order references in case of complaint.
9. Print successive close-register colors as soon as
possible after each other. Printing separate colors Issued May 1987
under different atmospheric conditions will cause
difficulties with register.

10. Finished work should be shrouded in polythene until


cut and boxed.

11. Always follow the Manufacturer’s recommendations


on guillotining and slitting.

12. Wherever possible, retain the Manufacturer’s batch/


order references in case of complaint.
FINAT TECHNICAL HANDBOOK 2014 |

64
surfaces requiring caution

SECTION 2.3
Caution should be exercised when labeling surfaces listed Ageing
below. In many cases products are available which will Surfaces where adhesive may be significantly exposed
overcome the problems of application and you are strongly over time to severe environmental conditions resulting
recommended to contact your material supplier. in eventual breakdown and failure of the adhesive, e.g.
drum labeling, exposure to salt water, and or high levels of
surfaces where damage can be caused by application or sunlight.
removal of self-adhesive products
Weaker bonded surface finishes e.g. (plasticized/soft) Applications where specific advice should be sought
PVC, flock coated fabric, acrylic vehicle paint, paper, card. Direct food labeling, toy labeling, any medical or
Animal skins and natural fibres, e.g. suede, leather wool. pharmaceutical applications, e.g. direct skin contact,
Tarnishable metal surfaces, e.g. copper, brass, silver. blood bags, phials, items requiring sterilization processes.
Some coated glass surfaces e.g. self cleaning, and optical Apparel and fabric labeling, leather, luxury goods, extreme
lenses. environment exposures e.g. temperatures 80°C or -20°C,
direct/continuous exposure to sunlight, UV, seawater or
Surfaces to which it is difficult to obtain satisfactory chemicals.
adhesion
Low energy surfaces where ‘wetting’ is difficult e.g. See also Section 2.6 Qualitative Adhesion testing
PT.F.E., untreated polyolefins, silicone treated or
contaminated surfaces, surfaces chemically treated for Issued March 1987
corrosion resistance, waxed surfaces, printed polyethylene Revised May 2001
(polyamide inks), greasy surfaces. Surface energy changes Revised October 2008
due to migration or loss of effectiveness of pre-treatment.

Rough surfaces where surface contact is likely to be


low, lacquered finishes, cork, foam, open weave fabrics,
embossed finishes, unglazed pottery.

Moist and/or cold surfaces where adhesive tack will


be momentarily deadened by either water or the low
temperature e.g. surfaces with condensation bloom, ice,
deep frozen food and chilled packs.

Irregular shaped surfaces in particular curved surfaces of


less than 25 mm diameter where label is applied to the
convex surface (phials, ampoules, bottle miniatures).

Dusty, friable, oily surfaces where adhesive tack may be


destroyed on surface contact, e.g. plaster, rusty metal,
masonry, concrete and tires.

Surfaces prone to gassing (caused by undercure) which if it


occurs after label application, may lead
to eventual bond failure, e.g. polycarbonate, fibreglass,
sealant.
FINAT TECHNICAL HANDBOOK 2014 |

65
safety guide for users of

SECTION 2.4 self-adhesive label stock


products

storage fire
Normal storage principles should be applied when storing The laminates will burn in the event of contact with a
and stacking laminate rolls. See also section 2.5. flame, smoky fumes being given off by the adhesive itself.
Materials involved are generally flammable and therefore Fires may be extinguished with water provided that live
should be stored away from all sources of heat and electrical equipment is not in the vicinity. Otherwise
ignition. powder or C02 should be used. The advice of your Fire
Officer should be initially sought having regard for the
Consideration should be given to listing types of material layout of your premises and the particular operations
stored to assist the Fire Brigade in the event of fire. involved. The following extra precautions are applicable to
the products stated.

usage 1. Films
Plastic films pass through a melt stage and will
1. Handling therefore drip before burning - this may cause severe
Safe methods of roll and pallet handling should be burns if skin contact is made. In the event of a fire,
applied. During un-banding pallets, care should be the use of self contained breathing apparatus is
exercised to avoid whiplash when banding is cut – recommended during fire-fighting.
eye protection and gloves are recommended. It is
important to remember that the outside wrappers, or 2. PVC (vinyl)
laps, of a roll are for protection only and should not During combustion, hydrochloric acid gas is evolved,
be relied upon to support the roll if excessive stresses as well as dense smoke and other acrid fumes which
are applied. Ideally, lifting and movement should be can have a corrosive and irritant effect. Self contained
conducted in a safe horizontal manner using centre positive-air breathing equipment should be readily
core support where possible. available for fire fighting and rescue work.
Operators should be forewarned that self-adhesive
laminate rolls show a greater tendency to
telescope than rolls of plain paper and therefore health and safety
greater care should be exercised.
Under normal conditions of handling, no hazards are
2. Conversion anticipated, but good industrial hygiene should always
Care should be taken to avoid cuts from exposed be observed. For specialized applications e.g. food, toy
paper or laminate edges during handling. During or surgical labeling, advice should be sought from the
the conversion of pressure sensitive laminates static individual supplier.
build-up may occur. Therefore, conversion equipment
should be adequately earthed. In situations where
highly flammable solvents or inks are being used,
specialist recommendations on static elimination may
be necessary.
FINAT TECHNICAL HANDBOOK 2014 |

66
waste disposal
Waste laminate is usually classified in most countries as
“non-hazardous” but local and national regulations must
be examined and complied with.

The following points should be noted:

Vinyl laminate should only be considered for incineration


if the incinerator is suitably constructed to cope with
corrosive fumes and dense smoke, and operates under
conditions that prevent the formation of dioxins.

FINAT Solutions
While research and development efforts continue towards
material recycling solutions, FINAT has arranged a disposal
system for release liners in a number of countries.

For laminate waste, thermal recycling is recommended.


This is based on high temperature combustion as a
substitute for fuel in the cement industry and in power
stations.

For release liner there are possibilities for material


recycling, provided the waste is clean. Several collection
schemes for release liner waste are available to label
converters and users.
Such schemes can only be set up and implemented in a
collective approach for the industry.

For information, contact the FINAT secretariat or visit the


sustainability/recycling portal at the FINAT website: www.
finat.com.

other information

The Technical Department of the Supplier should be


contacted for any additional specific information required.

Issued January 1987


Supplement FINAT Waste Management Systems Issued
December 1995
FINAT TECHNICAL HANDBOOK 2014 |

Revised March 1999


Revised October 2008

67
2.5
handling and storage of
label stock throughout

SECTION printing and converting

roll stock sheet stock


Receipt of goods Receipt of goods
On receiving goods into premises, inspect for signs of On receiving goods into premises, inspect for signs of
damage. Inform supplier of any shortage or damage damage. Inform supplier of any shortage or damage
immediately. immediately.
Store all material on a clean dry floor. Where goods are Store all material on a clean dry floor.
supplied on pallets, it is advisable to retain the material on Transport and store the material supported on a flat base to
these, and in the original package, until needed. prevent bending.
Rolls can be stored in horizontal or vertical position. If
stored horizontally, there is a risk for pressure mark in the Storage Conditions
area touching the ground Store in a cool and dry place.
Ideal storage conditions are 20-25°C and 40-50% RH.
High temperatures might cause adhesive bleeding.
Fluctuations in humidity might cause cockles or wavy
edges.
Avoid stacking more than 10 packages on a pallet. Do not
stock pallets with stacked reams on top of each other.
Materials should not be stored near to sources of heat and
ignition, or in direct sunlight.
Horizontal storage = Vertical storage = Do not unwrap pallets and reams until required.
core aligned horizontally core aligned vertically Pay particular attention to the supplier’s recommended
shelf-life and ensure correct stock rotation.
Storage conditions
Store in a cool and dry place. Preparation of material for processing
Ideal storage conditions are 20-25°C and 40-50% RH. The material should be allowed to condition (still in the
High temperatures might cause adhesive bleeding. wrapper) for at least 24 hours at printing room conditions.
Fluctuations in humidity might cause cockles or wavy Longer times might be needed if the storage conditions are
edges. radically different from the conditions in the print room.
Materials should not be stored near to sources of heat and Failure to condition sheets at print room conditions may
ignition, or in direct sunlight. create curling or wavy edges.
Do not unwrap rolls until required. If sheets require cutting before printing, then the knife of
Pay particular attention to the supplier’s recommended the guillotine should be sharp and clean. Cut the minimum
shelf-life and ensure correct stock rotation. number of sheets practicable, referring to the manufacturer
for advice if necessary. Use minimum pressure to avoid
Preparation of material for processing adhesive bleed.
Pay attention not to damage the reels when transporting Some filmic materials are best cut face down.
material with forklift trucks. If stacks are left overnight, protect from humidity changes
Remove moisture-proof wrapping and leave to attain print by shrouding with polythene.
room conditions for at least 24 hours before processing, Before printing, fan out the sheets.
as handling cold or hot material in a shop with normal
temperatures may cause wavy edges and curling. Storage and Handling of finished product
Store in a cool and dry place.
Storage and Handling of finished product Ideal storage conditions are 20-25°C and 40-50% RH.
FINAT TECHNICAL HANDBOOK 2014 |

Store in a cool and dry place. Wrap in polythene and pack flat in boxes or on pallets to
Ideal storage conditions are 20-25°C and 40-50% RH. give protection during transport and further handling.
Store finished coils on end (vertical storage), ideally use Take care, if banding, to avoid pressure marking.
two-side silicone release coated interleaving sheets
between the coils. Issued April 1987
Wrap in polythene and pack in boxes or on pallets to give Revised March 1999
protection during transport and further Revised October 2008
handling.

68
qualitative adhesion testing

SECTION 2.6
recommended adhesion test surfaces to be labeled

1. Cut out several labels, same size and in the same 1. Surfaces may not be what they appear to be. For
machine direction as the proposed printed label. example glass may have a protective coating or
antiscuff agent on the surface. There is no substitute
2. Peel off backing and apply to object to be labelled in for a test carried out on the actual object to be
the same position as the eventual requirement. Rub labeled.
down lightly with fingers or a rubber pad.
2. Test for adhesion under conditions which are as close
3. Ideally, prepare several samples and place one in a dry as possible to the end application. This should take
atmosphere and one in high humidity or other specific into consideration temperature and humidity.
conditions simulating potential end applications.
3. Do not carry out the test on a flat, empty plastic bag
4. Leave for 24 hours minimum before assessment of when the end user is labeling one filled with product.
adhesion.
4. Check whether the label is to be applied to a plain or a
printed part of the pack.

5. On plastic or filmic surfaces, materials that can migrate


to the surface may be present. Advice should be
assessment of adhesion sought from suppliers since these materials can have a
detrimental effect on adhesion.

1. Examine visually for edge lift. Issued 1987


Revised March 1999
2. Lift up corner of the label and peel with a firm, slow Revised October 2008
pull.

3. Good adhesion should result in at least 30% fibre tear


(by area) in the label paper.
Filmic labels can only be assessed by the peel force
required to remove the label.
Removable labels can be tested in the same way, but
should not give any fibre tear or surface damage when
removed.
FINAT TECHNICAL HANDBOOK 2014 |

69
SECTION 2.7 adhesives

Pressure sensitive adhesives were first developed in the mid nineteenth century for self-adhesive bandages. However, it
was only ninety years later that the idea was used to make self-adhesive labels.
At that time the adhesive used was made from natural rubber and applied by coating from a solvent solution. Today
solvents are not very popular any more, and alternative self-adhesive materials are available. Acrylic adhesives which are
also available as water-based emulsions, have excellent ageing properties. They are easy to coat and clearly eliminate the
hazards linked with solvent coating.
Hot melt adhesives can be coated at very high coating weights, because there is no drying or curing process involved.
Due to modern coating and drying technology both types of adhesives are able to be applied at high machine speeds.

types of pressure sensitive nomenclature for adhesives


adhesives and major used in self-adhesive laminates
applications
• Purpose:
To offer a standard nomenclature for describing
• Permanent different types of adhesives used in self-adhesive
An adhesive with high ultimate adhesion, where laminates. This nomenclature can be used in technical
labels are not intended to be removed. Available from leaflets, brochures and other documents, and it
standard to very high coating weights, depending on makes it easier to describe and understand the basic
the end application. composition and character of each adhesive.

• Removable, Peelable • Content:


An adhesive with a low ultimate adhesion to a wide Each adhesive should be categorized in four ways. The
range of surfaces. Careful choice of adhesive must be three first categories are compulsory, the last one optional:
made, particularly for surfaces like fabrics, paper and 1. Chemical basis
plastic films. 2. Physical state + drying/curing
3. Mains final use
• Water removable 4. Additional significant properties
An adhesive which releases the label by contact with
water. Certain adhesives already lose their adhesion 1. Chemical basis:
force with plain water, others need alcaline water. • Acrylic (pure, tackified)
• Rubber (natural, synthetic)
• Low Temperature • Other
An adhesive capable of functioning at temperatures
below +5°C, i.e. chill conditions (+5°C to -5°C), deep 2. Physical state + drying/curing
freeze conditions (-5°C to -25°C) and blast freeze • Water borne
conditions (-25°C to -50°C). • Solvent borne
• Hot melt
• Re-positionable • Radiation cured hot melt
An adhesive which permits removal and repositioning
shortly after application, prior to the development of 3. Main final use
ultimate adhesion. • Permanent
• Removable
• Food Contact • Deep-freeze
An adhesive with the appropriate F.D.A., BfR. or other • Re-positionable
appropriate approval for application to foodstuffs. • Food contact
FINAT TECHNICAL HANDBOOK 2014 |

• Wash-off
• Recycling friendly • Other
An adhesive which is designed to be less harmful to
paper recycling; already used in N.A. for self-adhesive 4. Additional significant properties, e.g. “direct food
stamps these adhesives support the trend of trouble contact according to FDA 175.125”
free recycling of self-adhesive materials. or for pharmaceutical purposes.

Issued May 2005


Revised October 2008

70
unwind roll chart

SECTION 2.8
indicate unwind direction by number as follows

FINAT TECHNICAL HANDBOOK 2014 |

Extract from TLMI Manual of Recommended Standards (where the chart has 16 positions).

71
2.9
recommendations
regarding static electricity
SECTION

what is static electricity? factors influencing


When a material holds a net electrical charge, either static electricity
negative or positive, it is said to have a static charge.
Polymeric substrates (plastics) generally have high Among the many factors that affect the generation and
resistivities. This allows them to maintain static charges for retention of static electricity are humidity, the substrate
long periods of time; on the other hand metals have very type, repetition and change in temperature.
low resistances. Paper has lower resistivity than plastics,
due to moisture content and polarity. Substrate
Generally all polymeric substrates and polymeric coated
Static electricity is usually measured in volts. The voltage or laminated paper tend to become charged with static
present on a material is dependent of two factors: electricity, and some of them are more readily charged
a) the amount of charge on the material than others. Paper is less prone to become charged, but
b) the capacitance of the material it can happen especially in very dry conditions. Whether a
The simple relationship is Q=CV where Q is the charge, V substrate charges positively or negatively depend on the
the voltage and C the capacitance of the material. other material with which it has come into contact. For
example, when a polyamide (PA) film passes over a rubber
There are two major type of static electricity, volumetric nip roller, it becomes negatively charged, a polyethylene
and surface. Volumetric static charges are charge will be positively charged
imbalances within the body of a material, whereas surface
static electricity is only present on the very outer surface Humidity
of a material. All the static electricity problems found in The dryer the environment of the print room, the higher
the web printing and converting industry relate to surface the level of static charge, and conversely the higher the
charges. Whether the charge is volumetric or on the humidity, the lower the static charge.
surface of the substrate depends of the conductivity of the
substrate. Repetition
Repeated action such as friction or separation will increase
the level of static electricity on the web. When the web
how is static electricity created? passes over many idler rollers the static charge will be
higher.
Static charges are generated by friction, contact and
separation of the material as it is being pulled from the Battery effect
feed roll and as the material passes over the idler rollers of Rewinding the many layers of a low charged web can lead
a press or a converting machine. to extremely high voltage charges. This is noticeable on the
Friction leads to closer contact thus more contact points roller of a rewind unit on a printing press or a slitter.
and therefore increases the level of charge generation.
As two materials are rubbed together the electrons Change in temperature
associated with the surface atoms on each material come As a material cools down, it has a tendency to generate
into very proximity with each other, and can be moved charge. For example, when a web passes UV-lamps or IR-
from one material to the other. dryer it gets heated; then the surface temperature of the
When static electricity is created by separation of materials, web will be cooled down by passing over a chill roller or
the faster the separation, the higher the charge generated the web will cool down by itself at the room temperature,
and conversely, the slower the separation the lower the Overall, this will create static charge on the surface.
charge. As an example, when printing a PVC substrate the
FINAT TECHNICAL HANDBOOK 2014 |

web is moving over a PTFE (Teflon®) coated roller. When


the materials separate, the electrons tend to adhere to
the PTFE, generating a negative charge on the PTFE and a
positive charge on the PVC-film.

72
problems and elimination neutralize each other or be dissipated to earth. However
with the presence of a nearby static charged surface an
of static electricity ion will be attracted to an opposite charge on the surface
of the substrate and the surface will be completely
Problems neutralized.
Static charges result in electrostatic attraction to the
substrate surface, of dirt and airborne particles present
around the press and converting machines. Web speeds measuring the static charge
complicate this process, because the faster the web speed
the higher the static charge level. This problem affects all There is a variety of measuring instruments for static
printers and converters, especially when converting filmic electricity available in the market.
substrates. In the label printing industry dust attraction Some instruments are calibrated to measure the field at
decreases the print quality. a given distance. The surface voltage and the polarity are
then displayed on the screen. Other instruments indicate
Material misbehavior is another type of electrostatic the electrical field strength in kV/m. To calculate the surface
attraction. This can be noticed on a sheeter, stacker, voltage, the reading has to be multiplied by the distance
conveyer, where the sheets would stick to themselves or between instrument and surface.
will be misrouted or repelled each other on the equipment,

Elimination glossary
The basic principle for neutralization of static charges is
the same whatever the technique used: one should re- Coulomb: The unit of measure of electrical charges.
establish the electrical neutrality of the surface by adding (Symbol : C)
or removing the electrons which create the imbalance of
the surface charge. As previously mentioned the moisture Electron: A small atomic particle with a negative
in the press room has an impact on static charge, therefore charge (1.6x10ˉ19 coulombs).
it makes sense to control the moisture. We suggest to
maintain the relative humidity at 50-65% and the room Ion: A molecule or atom with an electrical
temperature at about 22-24°C. imbalance (a negative ion has an excess of
electrons, a positive ion has a deficit
Passive ionisation of electrons)
Carbon or stainless steel fibre earthed brushes placed
closely over the surface of the web of a press or a Resistance: The higher the resistance of a material,
converting machine will leach away the static charges the harder it is for a charge to flow through
down to earth. Passive eliminators are thus useful for it. Insulators e.g. all polymeric substances
reducing very high level of static charges, say tens of kV’s (plastics) are very resistive.
down to medium high levels of a few kV’s. However by
their very nature, they are not able to completely neutralize Unit: Ohm (Ω)
the surface electricity, therefore residual charges remains
on the substrate surface. Capacitance: A measure of the ability of a substrate to
hold the charge. Unit: farad (F)
Active ionisation
By using high voltage AC or DC bars over the web of a Issued October 2008
press or converting machine, ionized air can be produced
FINAT TECHNICAL HANDBOOK 2014 |

which can be used to neutralize the surface charge of


the substrate. Around the ionizing pin/head a cloud of
positive and negative ions will be produced. In the absence
of outside influences, the positive and negative ions are
attracted to each other or a nearby earth, and would either

73
2.10
advices about light fastness of
printing inks and light exposition
SECTION

light fastness Light Fastness


Life time number Summer number
of days of days
Over time, prints that are exposed to light will fade because
the UV radiation of pigments and dyes has a decomposing BWS 1 (very low) 5 2,5
effect. The resistance to this decoloration or colour change
process is termed “light fastness”. In accordance with ISO BWS 2 (low) 10 5
2835 (DIN 16525) it is classified numerically from BWS 1
(= poor) to BWS 8 (= outstanding). BWS 3
20 10
(moderate)
(BWS stands for “Blue Wool scale”; originally, the BWS 4 (rather
standardized incrementation was a testing instrument of 40 20
good
the textile industry.) The light fastness according to ISO
2835 is tested with a daylight-simulating xenon lamp. BWS 5 (good) 80 40
In this test only the influence of direct exposure to light
is taken into account. Other influencing factors such as BWS 6 (very
160 80
fluctuations in temperature and humidity (weather!) good
remain unaccounted for.
BWS 7
350 175
(excellent)
For a short-lived advertising brochure it is not necessary
for the light fastness to be particularly high; a standard BWS 8
700 350
pigment can be used. For printers of magazines, books (outstanding)
and commercial print work the light fastness BWS 4 (=
rather good) is normally adequate. By contrast, inks of
automobile stickers or outside signs are expected not to remark
fade as quickly, which requires the use of pigments with
high light fastness. Quoted light fastness of the ink supplier will normally be
High lightfastness pigments are usually more costly than indicative of a standard printing condition (film weight,
equivalent lower lightfastness equivalents and may differ in density, substrate etc), and standard test condition/
colour shade. exposure scenario. As well above listed level and duration
is concerned to a 100% full solid print.
The actual time during which the ink of a print is resistant
is dependent on the accumulated incident light radiation, The actual printed labels shall be tested at a certified
which however, as is known, varies with season, but also laboratory or by the ink supplier if he has the appropriate
with geographic altitude. testing equipment available to determine the actual light
fastness of the printed label which might be different from
The table below of the BWS incrementation shows an the quoted value.
approximate indication (without guarantee) of the duration
of resistance of the ink on direct exposure to the sun Prints have to be made under so-called standard conditions
under Central European daylight conditions ISO 2835 (DIN concerned to film weight, density and substrate applicable
16525). to the required print job.

For the printer, in particular the following points are


important:
FINAT TECHNICAL HANDBOOK 2014 |

• In the case of mixed inks the ink with the lowest light
fastness is decisive because it governs the earliest time
of fade-out.

• M
ixed inks are frequently mixed in very different ratios.
As a result of the mixing an ink could be very intensively
thinned, thereby losing its original light fastness. (For
example, a certain orange could be comprised of 1

74
part red and 20 parts yellow. Thinned by a factor of
20 the inherently good light fastness of the unmixed
red exhibits a significantly poorer light fastness. When
exposed to light, the orange quickly becomes yellow.)

• In lightened colours (mixed with white or extended


with pastes) the pigment concentration is lower; the
light fastness is correspondingly lower. For pastel
shades of adequate light fastness only printing inks of
fastness categories BWS 6 to BWS 8 should therefore
normally be used.

• Weak ink deposit / screens: the light fastness of inks


of categories BWS 7 and BWS 8 printed in thinner ink
films or in screens is scarcely reduced. By contrast, with
decreasing ink film thickness the light fastness of inks
of category BWS 5 or lower declines noticeably. Screen
dots fade more rapidly than solids.

• The effect of daylight fluorescent prints is so intensive


because they reflect a part of the light from the
ultraviolet spectrum as visible light. But it is this
very conversion capability that suffers strongly from
the effect of light; it is destroyed by the UV rays. On
exposure to light the fluorescent power is sustained
only for a short time. Daylight fluorescent inks normally
have a light fastness of BWS 1 to BWS 2.

• Manufacturers data: The light fastness data always


relate only to the resistance to incident light, without
taking into account other influencing factors such as
the effects of the weather. Moreover, the printing ink
manufacturer’s warranty covers only the fastness of the
unmixed, non-extended ink printed as a solid tone and
on a white substrate in a film thickness commonly used
in practice.

• The requirements on resistance to the weather go


beyond those on light fastness. The resistance to the
weather (frequently confused with light fastness) is
measured according to DIN 54071. Weather-resistant
inks are fully exposed to the weather and have to be
resistant to moisture, fluctuations in air temperature
and humidity and to the influence of certain air
FINAT TECHNICAL HANDBOOK 2014 |

pollutants. In addition to light-fast pigments, weather-


resistant binder resins are also required. Appropriate
overvarnishing provides additional protection.

75
SECTION 3 test equipment (manufacturers)

3.1 standard finat test roller


Performance requirements for this test roller are that it applies a standard pressure irrespective of the variation in hand
pressure on the handle.

Specifications
Diameter of roll: mm 85 ± 2.5
Roll cover: rubber to hardness scale Shore A 80 ± 5
Width of roll: mm 50 ± 1
Weight of roller: kg 2 ± 0.05
Rollers made to the earlier specifications
92 – 98 mm diameter are still acceptable.

3.2 automatic rolling device


The FINAT automatic roller unit ensures correct guidance of the contact roll and electronic adjustment of the rolling
speed. The number of roll movements can be set at between 1 and 9 by a selector switch. The roll can easily be taken
from its mounting. Rolls to other standards can also be used. The roll can also be safely lifted from the substrate in the
end position.

Technical data
Roller speed 3 levels 5, 10, 200 (± 1 %) mm/s
Length of roll area adjustable max 300mm Mains connection 220 V/50 or 110V/60

Roll data
Diameter: mm 85 ± 2.5
Width: mm 50 ± 1
Weight: kg 2 ± 0.05
Hardness of rubber surface: Shore A 80 ± 5
Thickness of rubber layer: mm 6 ± 0.5
Rolls can be supplied to other standards

3.3 test equipment manufacturers


Test equipment is available in a wide variety. A number of manufacturers of such equipment is listed below, where
possible with an indication of the type of their equipment. Please note that the list is far from complete and that it may be
subject to change. We advise you to consult the websites of the respective manufacturers for more details and updates.

Company Country Test equipment Page

Adhesive Technical Services Ltd. United Kingdom adhesion 84


Ametek GmbH Germany adhesion 79
Arcotec GmbH Germany ready made test fluids 79
FINAT TECHNICAL HANDBOOK 2014 |

Atlas Material testing Technology UK, USA textile testing machines 84,86
Brookfield Viscometers United Kingdom viscometers 84
Brookfield Engineering Laboratories Vertriebs GmbH Germany, India, USA viscometers 79,82,86
BRK Instruments India India viscometers 82
Büro Mayr Germany standard test rollers 79
Cheminstruments USA 86
Datacolor Switzerland colour measurement 83
Elcometer Belgium, France, Germany
Japan, Netherlands scratch resistance 78,79,82

76
Company Country Test equipment Page

Erichsen GmbH & Co KG Germany tensile, adhesion testers,


agent Chemsultants 79
Frank PTI GmbH Germany tensile, adhesion testers 79
Gretag Macbeth AG (see X-rite) Germany colorimetric equipment 81,83,87
Hach Lange GmbH Germany colour measurement 80
Heraeus Noblelight Fusion UV Inc USA UV Curing systems 86
Hermann Klemmt Mess- und Prüftechnik GbR Germany agent Sneep: release testers 80
Dr. Hönle AG (European headquarters) Germany UV curing equipment 80
Hönle UV America, Inc. USA UV curing equipment 86
Hunter Associates Laboratory Inc. USA colour measurement 86
IGT Testing Systems Netherlands, USA viscometers, tensile testers 82,86
Imass Inc USA high speed release tester 86
Instron Germany, UK, USA tensile, adhesion testers 80,84,87
Kiffe Engineering GmbH Germany dynamic cohesion 80
Konica minolta Sensing europe B.V. Switzerland colour measurement 83
Köttermann GmbH & Co. KG Germany humidity tester 80
Labthink Instruments Co. Ltd. China tensile testers 78
Laetus Gmbh Germany colour measurement 80
Lloyd Materials Testing United Kingdom tensile, tear, peel, adhesion testers 84
Lorentzen & Wettre Gmbh Sweden Paper & pulp testing 84
M.C. TEC B.V. Netherlands, UK hand rollers, rub testers,
colorimeters, spectrophotometers 82,84
Mecmesin Ltd. United Kingdom peel and adhesion 84
Metorex International oy (see Oxford Instruments) Finland X-ray spectometers 85
MTS Systems France, USA tensile testers for release,
tack and peel, specimen cutters 79,87
Oxford Instruments United Kingdom X-ray spectometers 85
Pausch Messtechnik Germany shear testers, hand rollers,
colour measurement 80
Pearson Panke Equipment Ltd. United Kingdom tensile testers, loop tack,
viscometers, rub testers 85
Phoseon Technology (headquarters) USA UV curing applications 87
Pillar Technologies Surface Treatment USA ready made test fluids 87
Printech Tools & Technology Switzerland standard test rollers, peel,
release and tensile testers 83
RK PrintCoat Instruments Ltd. United Kingdom peel and adhesion 85
Rocholl GmbH Germany test panels 80
Romaco Pharmatechnik GmbH (See Laetus) Germany colour measurement 80
SDL Atlas China, Hong Kong, USA textile testing, shirlestain 78,87
Sheen Instruments Singapore, UK, USA abrasion, coating thickness,
colour match 83,85,87
Sick Vertriebs-GmbH Germany Fluorescence 81
Sneep Industries BV Netherlands shear testers, high and low speed
peel and release testers, automatic
roll down machine 82
Spectro Analytical Instruments Gmbh Germany X-ray spectometers 81
Stable Micro Systems Ltd. United Kingdom tensile/compression equipment 85
Techkon Gmbh Germany colorimetric equipment 81
tesa AG Germany test tapes 81
Testing Machines Inc Canada, Germany, USA ink rub tester 78,81,83,87
The Testometric Company Ltd. United Kingdom tensile, dynamic shear,
FINAT TECHNICAL HANDBOOK 2014 |

adhesion, peel tester 85


Thermo Fisher Scientific Inc USA viscometers 87
Thomas Systeme Gmbh Germany barcode readability tester 81
3M United Kingdom test tapes 85
Tinius Olsen UK, USA tensile testers 85,87
TQC Netherlands hardness, scratch resistance 83
Weiss Umwelttechnik GmbH Austria, Germany humidity tester 78,81
X-Rite Switzerland, USA X-rite equipment to FTM 22 81,83,87
Zwick G+A1:B71mbH & Co. Prüfmaschinen Germany tensile testers 81

77
SECTION 3.3 test equipment manufacturers

austria

Weiss Umwelttechnik Oberlaaerstr. 316 Humidity tester


A-1230 Wien
Ges.m.b.H. Tel.: +43-1-6166697
Fax: +43-1-616669713
E-mail: wien.office@wut.com
URL: www.weiss-umwelttechnik.at

belgium

Elcometer SA Rue Vallée 13 Scratch resistance FTM29


B-4681 Hermalle/s Argenteau Viscometers
Tel: +32-4-3799610
URL: www.elcometer.com

china

Labthink Instruments 144 Wuyingshan Road Adhesive strength test


Jinan
Co. Ltd. Tel.: +86-531-85068566
Fax: +86-531-85812140
E-mail: trade.en@labthink.cn
URL: www.labthinkinternational.com.cn

SDL Atlas Hong Kong 3J Garment Centre Textile testing machines


576 Castle Peak Road Shirlestain
Kowloon
Tel.: +852-34434888
Fax: +852-3443-4999
E-mail: info@sdlatlas.com.cn

SDL Atlas China 1/F (South East) & 2/F Textile testing machines
Shenjian Mansion Shirlestain
Central District (West) Hi-Tech Park
Nanshan, Shenzhen 518057
Tel.: +86-755-26711168
Fax: +86-755-26711337
E-mail: info@sdlatlas.com.cn

canada

TMI Canada PO Box 203 Ink rub tester


FINAT TECHNICAL HANDBOOK 2014 |

Pointe Claire-Dorval FTM 27


Quebec H9R-4N9
Te.l: +1-302-6135600
+1-800-678-3221 (Toll-free)
Fax: +1-302-6135619
E-mail: canada@testingmachines.com
URL: www.testingmachines.com

78
france

Elcometer Sarl 97 Route de Chécy Scratch resistance FTM29


F-45430 BOU Viscometers
Tel: +33-2-38863344
URL: www.elcometer.com

MTS Systems 58, Rue Auguste Perret, Europarc Tensile testers for release,
F-94200 Creteil tack and peel
Tel.: +33-1-58439000 Specimen cutters, rollers
Fax: +33-1-58439001
E-mail: contact.ance@mts.com
URL: www.mts.com

germany

Ametek GmbH Rudolf-Diesel-Strasse 16 Adhesion test apparatus


D-40670 Meerbusch
Tel.: +49 – 2159 – 91360
Fax: +49 – 2159 – 913639
E-mail: info@ametek.de
URL: www.ametek.de

Arcotec GmbH Rotweg 24 Corona treatment


D-71297 Mönsheim Ready made test fluids
Tel.: +49-7044-92120 FTM 15
Fax: +49-7044-921212
E-mail: info@arcotec.com
URL: www.arcotec.com

Brookfield Engineering Hauptstrasse 18 Viscometers


D-73547 Lorch
Laboratories Vertriebs, GmbH
Tel.: +49 -7172-927100
Fax: +49-7172-927105
E-mail: info@brookfield.eu
URL: www.brookfieldengineering.com

Büro Mayr Forststrasse 81 Standard test roller


D-85521 Riemerling
Tel:. +49 – 89 - 6099679
Fax: +49 – 89 - 6098436

Elcometer Instruments GmbH Ulmer Strasse 68 Scratch resistance FTM 29


D-73431 Aalen Viscometers
Tel.: +49-7361-528060
URL: www.elcometer.com

Erichsen GmbH & Co KG Am Iserbach 14 Tensile, adhesion testers


FINAT TECHNICAL HANDBOOK 2014 |

D-58675 Hemer Humidity cabinets


Tel.: +49 – 2372 - 96830 Thickness gauges
Fax: +49 – 2372 - 6430 Agent of Chemsultants
E-mail: info@erichsen.de
URL: www.erichsen.de

Frank PTI GmbH Auf der Aue 1 Tensile, adhesion testers


D-69488 Birkenau
Tel.: +49 – 6201 – 840
Fax: +49 – 6201 – 84290
E-mail: office@frank-pti.com
URL: www.frank-pti.com
79
SECTION 3.3 test equipment manufacturers

germany

Hach Lange GmbH Willstätterstr. 11 Colour measurement


D-40549 Düsseldorf
Tel.: +49-211-52880
Fax: +49-211-5288143
E-mail: info@hach-lange.de
URL: www.hach-lange.de

Hermann Klemmt Mess- Kabisstrasse 3 Agent Sneep Industries


und Prüftechnik GbR D-86570 Inchenhofen Shear testers, high and low speed
Tel.: +49 – 8257 - 9976770 peel and release testers
Fax: +49 – 8251 - 9976775
E-mail: info@klemmt.de
URL: www.klemmt.de

Dr. Hönle AG UV - Technologie For more locations visit:


(European headquarters) Lochhamer Schlag 1 www.hoenle.de/en/uv-supplier-
D-82166 Gräfelfing locations/
Tel.: +49 89 856 08 - 0
Fax: +49 89 856 08 – 148 UV curing equipment
URL: www.hoenle.de

Instron Structural Testing Landwehrstrasse 55 Tensile, adhesion testers


64293 Darmstadt
Systems GmbH (IST) Tel.: +49 – 6151 – 39170
Fax: +49 – 6151 – 3917500
URL: www.instron.de

Kiffe Engineering GmbH Am Krebsgraben 18 Dynamic cohesion


D-78048 VS-Villingen
Tel.: +49 – 7721 – 80030
Fax: +49 – 7721 – 800330
E-mail: info@kiffe.net
URL: www.kiffe.net

Köttermann GmbH & Co KG Industriestrasse 2-10 Humidity tester


D-31311 Uetze-Hänigsen
Tel.: +49 – 5147 – 9767000
Fax: +49 – 5147 – 977777
E-mail: systemlabor@koettermann.com
URL: www.koettermann.com

Laetus GmbH Sandwiesenstrasse 27 Colour measurement


D-64665 Alsbach-Hähnlein FTM 20, 22
Tel.: +49 – 6257 – 50090
Fax: +49 – 6257 – 3119
E-mail: contact@laetus.com
URL: www.laetus.com
FINAT TECHNICAL HANDBOOK 2014 |

Pausch Messtechnik Karlstrasse 6 Q-sun and QUV weathering testers


D-42781 Haan Outdoor weathering services
Tel.: +49 – 2129 - 93960 Colour measurement
Fax: +49 – 2129 - 939610 Shear testers (FTM 8) for ambient
E-mail: info@pausch.com and oven shear testing
URL: www.pausch.com Hand rollers

Rocholl GmbH Schwarzacher Strasse 15 Test panels


D-74758 Aglasterhausen
Tel.: +49-6272-916780
Fax: +49 – 6272 - 9167810
E-mail: post@rocholl.eu
URL: www.rocholl.eu
80
germany

Sick Vertriebs-GmbH Willstätterstrasse 30 Fluorescence measurement


D-40549 Düsseldorf Industrial sensors
Tel.: +49- 211 53010
Fax: +49-0211 5301302
E-mail: info@sick.de
URL: www.sick.de

SPECTRO Analytical Boschstrasse 10 X-ray spectometers (XRF)


Instruments GmbH D-47533 Kleve FTM 7
Tel.: +49 – 2821 – 8920
(member of Ametek) Fax: +49 – 2821 – 8922200
E-mail: spectro.nfo@ametek.com
URL: www.spectro.com

TECHKON GmbH Wiesbadener Straße 27 Colorimetric equipment


D-61462 Königstein
Tel.: +49-6174-924450
Fax: +49-6174-924499
E-Mail: info@techkon.com
web: www.techkon.de

tesa AG Quickbornstrasse 24 Test tapes 7475, 7476, 4104


D-20253 Hamburg FTM 10, 11, 21, 22
Tel.: +49-40-49093400 See also list of agends worldwide
Fax +49-40-49093520
URL: www.tesa.com

TMI Europe GmbH & Co. KG Taubenstrasse 22 Ink Rub tester


Textilbedarf Langen GmbH & Co.KG D - 41236 Moenchengladbach (FTM 27)
Tel: +49-2166-2882 |
Fax: +49-2166-24645
Email: rhollweg@testingmachines.com
URL: www.testingmachines.com

Thomas Systeme GmbH Wilhelmstrasse 8 Barcode readability tester


D-32602 Vlotho-Bonneberg
Tel.: +49 – 5733 – 91000
Fax: +49 – 5733 – 910050
E-mail: info@thomassysteme.de
URL: www.thomassysteme.de

Weiss Umwelttechnik GmbH Simulationsanlagen - Messtechnik Humidity tester


Greizer Strasse 41-49
D-35447 Reiskirchen-Lindenstruth
Tel.: +49 – 6408 – 840
Fax: +49 – 6408 – 848710
E-mail: info@wut.com
URL: www.wut.com

X-Rite GmbH Fraunhoferstr. 14 X-rite equipment FTM 22


FINAT TECHNICAL HANDBOOK 2014 |

82152 Martinsried / München


(former Gretag Macbeth)
Tel.: +49-89-857070
Fax: +49-89-85707111
URL: www.erx50.com

Zwick GmbH & Co. August Nagel Strasse 11 Tensile tester


D-89079 Ulm
Prüfmaschinen Tel.: +49 - 7305 - 100
Fax: +49 - 7305 - 10200
E-mail: info@zwick.de
URL: www.zwick.de

81
SECTION 3.3 test equipment manufacturers

india

Brookfield Engineering India Nilay Shah – India Representative Viscometers


Tel.: +91-98-19749837
E-mail: info@brookfield.co.in

BRK Instruments India LLP ANM House Viscometers


Plot no. A-141, Road no. 23
Wagale Industrial Area
Thane (W) 400 604
Tel.: +91-22-66141666
E-mail: info@brkindia.net

japan

Elcometer KK Nisso Dai 23 Building, Scratch resistance FTM 29


Room 804, 3-8-25, Viscometers
Toranomon, Minato-ku,
Tokyo 105-0001
Tel.: +81-3-68690770
Fax: +81-3-68091442
URL: www.elcometer.com

netherlands

Elcometer NL Newtonlaan 115 Scratch resistance FTM 29


NL-3584 BH Utrecht Viscometers
Tel: +31-30-2107005
URL: www.elcometer.com

IGT Testing Systems Circular sample cutters


Keienbergweg 25 Printability testes for liquid and
P.O.box 12688 paste inks for coating, proofing and
1100 AR Amsterdam printing
Tel.: +31-20-4099300 Rub/scratch and abrasion testers
Fax: +31-20-6974842 Cobb testers
E-mail: info@igt.nl Horizontal tensile testers for peel and
URL: www.igt.nl loop tack tests, Viscometers
Lab UV curing devices, Tack testers
Gloss meters, Viscometers

M.C. TEC B.V. Distributiestraat 27 Hand rollers, Rolling ball track


4283 JN Giessen testers, contact o meter for surface
Tel.: +31-183-445050 wetting properties, viscometers, rub
Fax: +31-183-445059 testers, gloss meters, colorimeters
E-mail: info@mctec.nl and spectrophotometers
FINAT TECHNICAL HANDBOOK 2014 |

URL: www.mctec.nl FTM 1, 2, 3, 8, 9

Sneep Industries BV P.O. Box 5726 Shear testers, hot melt/holding power
NL-3290 AA Strijen at elevated temperature
Tel.: +31 – 78 – 6107690 High and low speed peel and release
Fax: +31 – 78 – 6107691 testers
E-mail: info@sneepindustries.com Hand rollers, testplates of stainless
URL: www.sneepindustries.com steel and glass
Automatic roll down machine
Custom built testers
FTM 1, 2, 3,4, 5, 8, 9

82
netherlands

TQC Thermimport Quality Molenbaan 19 Adhesion tester


Control NL-2908 LL Capelle aan den IJssel Tapes for adhesion testing
Tel.: +31-10-7900100 FTM 3
Fax: +31-10-7900129
E-mail: info@tqc.eu
URL: www.tqc.eu

singapore

Sheen Instruments 3A International Business Park #08-02 Instruments for use in coating
ICON@IPB, Tower A and paint industry, incl. Abrasion,
Singapore 609935 coating thickness, colour match,
Tel.: +65-69337680 gloss, hardness, moisture
E-mail: info@sheeninstruments.com measuring
URL: www.sheeninstruments.com

switzerland

Datacolor AG Loorenstrasse 9 Colour measurement


CH-8305 Dietikon/Zürich FTM 20, 22
Tel.: +41-44-8353830
Fax: +41-44-8353820
E-mail: info@datacolor.eu
URL: http://spyder.datacolor.com

Konica Minolta Sensing Riedstrasse 6 Colour measurement


CH-8953 Dietikon
Europe B.V. Tel.: +41 – 43 - 3229800
Fax: +41 – 43 - 3229809
E-mail: service.switzerland@seu.
konicaminolta.eu
URL: www.konicaminolta.eu
(For more locations, visit http://www.
konicaminolta.com/selector/index.html)

Printech Tools & Technology Trön 9 Standard FINAT test roller


CH-9225 St. Pelagiberg Special peel, release and tensile
Tel.: +41 – 71 – 430 0440 testers
Fax: +41 – 71 – 430 0441 FTM 1, 2, 3, 8, 9, 10, 11
E-mail: info@printech.ch Resistance spot proofer FTM 16
URL: www.printech.ch UV light spectrometer (to check UV
curing and exposure units for exact
wave length and intensity)

Testing Machines Mr. Joern Krueger Ink rub tester FTM 27


Albert Isliker & Co. AG
CH-8057 Zurich
E-mail: switzerland@testingmachines.
FINAT TECHNICAL HANDBOOK 2014 |

com
URL: www.testingmachines.com

X-Rite Europe GmbH Althardstrasse 70 X-rite equipment to FTM 22


CH-8105 Regensdorf
(European headquarters)
Tel.: +41-44-8422400
+1-800-70030001 (toll free)
Fax: +41-44-842 22 22
URL: www.xrite.com

83
SECTION 3.3 test equipment manufacturers

sweden

Lorentzen & Wettre Box 4 Paper testing equipment


SE-16493 Kista
Tel.: +46 – 8 – 477 9000
Fax: +46 – 8 - 4779199
E-mail: info@l-w.com
URL: www.lorentzen-wettre.com

united kingdom

Adhesive Technical Services Beacon Hill Industrial Estate Adhesive, label and tape testing
PO Box 51, Botany Way according to FINAT, AFERA, PSTC,
Purfleet, Essex RM19 1SY PSMA and ASTM.
Tel.: +44–1708–867355 Agents for Cheminstruments
Fax: +44–1708–869804
E-mail: sales@adhtechnical.com
URL: www.adhtechnical.com

Atlas Material Testing 2 New Star Road Textile testing machines Shirlestain
Leicester LE4 9JD
Technology Ltd. Tel.: +44-116-2462957
E-mail atlas.service@ametek.co.uk
URL: www.atlas-mts.co.uk

Brookfield Viscometers Ltd Brookfield Technical Center Viscometers


Stadium Way
Harlow, Essex CM19 5GX
Tel.: +44 -1279 - 451 774
Fax: +44 -1279 - 451 775
E-mail: sales@brookfield.co.uk
URL: www.brookfieldengineering.com

Instron (European headquarters) Coronation Road Tensile, adhesion testers


High Wycombe, Bucks HP12 3SY
Tel.: +44 – 1494 456815
URL: www.instrom.co.uk

Lloyd Materials Testing Steyning Way Adhesion testers


Bognor Regis, West Sussex, PO22 9ST FTM 1, 2, 3, 9, 10,11, 18
Tel.: +44-1243-833 370
Fax: +44-1243-833401
E-mail: uk-far.general@ametek.co.uk
URL: www.lloyd-instruments.com

M.C. TEC England P.O. Box 1067 Hand rollers, Rolling ball track
FINAT TECHNICAL HANDBOOK 2014 |

BB9 4DD testers, contact o meter for surface


Tel.: +44-1282-798086 wetting properties, viscometers, rub
Fax: +44-1282-798224 testers, gloss meters, colorimeters
E-mail: info@mctec.co.uk and spectrophotometers
URL: www.mctec.co.uk FTM 1, 2, 3, 8, 9

Mecmesin Ltd. Newton House Peel and adhesion testers


Spring copse Business Park
Slinfold, West Sussex RH13 0SZ
Tel.: +44-1403-887511
E-mail: info@mecmesin.com
URL: www.mecmesin.com
84
united kingdom

Oxford Instruments Tubney Woods X-ray spectometers (XRF) FTM 7


Abingdon, Oxfordshire OX13 5QX
Tel.: +44-1865-393200
Fax: +44-1865-393333
URL: www.oxinst.co.uk

Pearson Panke Pearson Panke 1-3 Special tensile testers


Hale Grove Gardens Release FTM 3, peel (FTM1, 2), loop
Equipment Ltd. London NW7 3LR tack (FTM 9)
Tel.: +44 – 20 – 89593232 Rolling ball tack testers
Fax: +44 - 20 – 89595613 Contact o meter for surface wetting
E-mail: 50years@pearsonpanke.co.uk properties
URL: www.pearsonpanke.co.uk Viscometers, Rub testers, gloss meters
Colorimeters and spectrophotometers

RK PrintCoat Litlington, Royston Sample preparation equipment


Instruments Ltd. Herts SG8 0QZ (coating, proofing and printing)
Tel.: +44 – 1763 – 852187
Fax: +44 – 1763 – 852502
E-mail: sales@rkprint.com
URL: www.rkprint.com

Sheen Instruments Broers Building Instruments for use in the coating


JJ Thomson Avenue and paint industry, incl. abrasion,
Cambridge CB3 0FA coating thickness, colour match,
Tel: +44-1803-407728 gloss, hardness, moisture
Email: info@sheeninstruments.com measuring
URL: www.sheeninstruments.com

Stable Micro Systems Ltd. Vienna Court, Lammas Road Tensile/compression equipment
Godalming, Surrey GU7 1YL FTM 1, 2, 3, 5, 6, 9, 18, 22
Tel.: +44 - 1483 - 427345
Fax: +44 - 1483 - 427600
E-mail: stable@stablemicrosystems.com
URL: www.stablemicrosystems.com

The Testometric Unit 1, Lincoln Business Park Tensile, compression, loop tack,
Company Ltd. Lincoln Close, Rochdale probe tack, 90 & 180 degree
Lancashire OL11 NR peels, friction, dynamic shear and
Tel.: +44 - 1706 - 654039 adhesion/peel tests, conducted
Fax: +44 - 1706 - 646089 at cryogenic and elevated
E-mai:l info@testometric.co.uk temperatures
URL: www.testometric.co.uk

3M United Kingdom Plc 3M Centre TTapes 810 magic TM tape FTM 21,
Cain road 22
Bracknell, Berkshire RG12 8HT
Tel.: +44-8705-360036
URL: www.3direct.co.uk
www.3m.com
FINAT TECHNICAL HANDBOOK 2014 |

Tinius Olsen, Ltd. 6 Perrywood Business Park, Tensile testers


Honeycrock Lane,
Salfords (Near Redhill), Surrey RH1 5DZ
Tel.: +44-1737-765001
Fax: +44-1737-764768
E-Mail: sales@tiniusolsen.co.uk
URL: www.tiniusolsen.com

85
SECTION 3.3 test equipment manufacturers

usa

Atlas Material (headquarters) Textile testing machines Shirlestain


Testing Technology 4114 North Ravenswood Avenue www.atlas-mts.com
Chicago, Illinois 60613
Tel.: +1-773-3274520
Fax: +1-773-3275787
E-mail: atlas.info@ametek.com
URL: www.atlas-mts.com

Brookfield Engineering 11 Commerce Boulevard Viscosity, Texture Analysis and


Laboratories Middleborough, MA 02346 Powder Flow
Tel.: +1-508-9466200
+1-800-6288139 (toll free)
Fax: +1-508-9466262
E-mail: web.sales@brookfieldengineering.com
URL: www.brookfieldengineering.com

ChemInstruments, Inc. 510 Commercial Drive FTM 1, 2, 3, 4, 5, 7, 8 9, 10, 11, 13, 14,
Fairfield OH 45014 15,18, 21, 24
Tel. +1-513-8601598 Chemsultants International
Fax +1-513-8601597 Network is a source for contract
URL www.chemsultants.com research, laboratory testing,
pilot coating, consulting, test
instruments and hands-on
Chemsultants, Inc. Chemsultants, Inc. seminars.
9079 Tyler bvd
Mentor OH 44060
Tel. +1-440-9743080
Fax +1-440-9743081
URL www.chemsultants.com

Heraeus Noblelight 910 Clopper Road Supplier of UV curing systems


Gaithersburg, Maryland 20878
Fusion UV Inc. Tel.: +1-301-5272660
Fax: +1-301-5272661
URL: www.fusionuv.com

IGT Testing Systems Inc. Arlington Center Circular sample cutters


543 West Golf Road Printability testes for liquid and paste
Arlington Heights, IL 60005 inks for coating, proofing and printing
Tel.: +1-847-9522448 Rub/scratch and abrasion testers
Cobb testers
Fax: +1-847-9522449 Horizontal tensile testers for peel and
E-mail: usa@igt.nl loop tack tests, Viscometers,
URL: www.igt.nl Lab UV curing devices
Tack testers, Gloss meters

Hönle UV America, Inc. 261 Cedar Hill Street UV curing equipment


Building C, Marlboro
MA 01752
Tel. +1- 508-229 7774
E-mail: main@honleuv.com
URL: www.honleuv.com
FINAT TECHNICAL HANDBOOK 2014 |

Hunter Associates 11491 Sunset Hills Road Colour measurement FTM 20, 22
Reston, VA 20190-5280
Laboratory Inc. Tel.: +1 - 703 - 4716870
Fax: +1 - 703 - 4714237
E-mail: info@hunterlab.com
URL: www.hunterlab.com

Imass Inc P.O. Box 134 High speed release tester


Accord, MA 02018
Tel.: +1-781-8343063
Fax: +1-781-8343064
E-mail: sales@imass.com
URL: www.imass.com
86
Instron Worldwide 825 University Avenue Tensile, adhesion testers
Norwood, MA 02062-2643
Headquarters Tel.: +1-800-8776674
E-mail: web@instron.com
URL: www.instron.com

MTS Systems 14000 Technology Drive Tensile testers for release,


Eden Prairie, MN 55344 tack and peel
Tel.: +1-800-3282255 Specimen cutters, rollers
Fax: +1-952-9374515
E-mail: info@mts.com
URL: www.mts.com

Phoseon Technology 7425 NW Evergreen Parkway UV curing applications


Hillsboro OR 97124 USA
(headquarters) Tel: +1 503 439 6446
Fax: +1 503 439 6408
URL: www.phoseon.com

Pillar Technologies 475 Industrial Drive Ready made test fluids


Surface Treatment Hartland, WI 53029 FTM 15
Tel.: +1-262-9127200
+1-888-PILLAR6 (toll free)
Fax: +1-262-9127272
E-mail: info@pillartech.com
URL: www.pillartech.com

SDL Atlas 3934 Airway Drive Textile testing machines


Rock Hill, SC 29732-9200 Shirlestain
Tel.: +1-803-3292110
Fax: +1-803-3292133
E-mail: info@sdlatlas.com
URL: www.sdlatlas.com

Sheen Instruments 5856 Corporate Ave, Instruments for use in the coating
Suite 220, Cypress, and paint industry, incl. abrasion,
CA 90630 coating thickness, colour match,
Tel.: +1-760-3433650 gloss, hardness, moisture
Email: info@sheeninstruments.com measuring
URL: www.sheeninstruments.com

Testing Machines Inc. 40 McCullough Drive, Ink rub tester FTM 27


New Castle, DE 19720
Tel.: +1-302-613-5600
+1-800- 6783221 (toll free)
Fax: +1-302-6135619
E-mail: info@testingmachines.com
URL: www.testingmachines.com

Thermo Fisher Scientific Inc. 81 Wyman Street Viscometers


Waltham, MA 02454
Tel.: +1-781-6221000
+1-800-6785599 (toll free)
Fax: +1-781-6221207
URL: www.thermoscientific.com
FINAT TECHNICAL HANDBOOK 2014 |

Tinius Olsen 1065 Easton Road Tensile testers


Horsham, PA 19044-8009
Tel.: +1-215-6757100
Fax: +1-215-4410899
E-mail: info@tiniusolsen.com
URL: www.tiniusolsen.com

X-Rite Inc. 4300 44th Street SE X-rite equipment FTM 22


Grand Rapids, Michigan 49512
(Corporate Headquarters)
Tel.: +1-800-2489748
+1-616-8032100
E-mail: info@xrite.com
URL: www.xrite.com
87
SECTION 3.4 testing institutes

This is a list of independent testing laboratories/institutes that can carry out specific tests in relation to packaging, food
contact (migration) and other industry areas. Except for IGT-Netherlands and SGS France (= FINAT members) FINAT does
not have any business relations or agreement with them.

belgium

CELABOR, Research and Mr David Berck, M.Sc. All FTMs except for 4, 7 and 19.
(Dept. Manager, Packaging – Raw
Testing Centre materials)
Avenue du Parc 38
B-4650 Herve
Tel. +32-87-322456
Fax +32 -87-341387
E-mail david.berck@celabor.be
URL www.celabor.be

china
Shanghai Rubber Product Mr Jiang Honggui All FTMs except for 4, 7 and 19.
381, PanYu Road
Research Institute 200052 Shanghai
Tel. +86-21–62815008
Fax +86–21-62816790
E-mail webmaster@china-sirp.com
URL www.china-sirp.com

denmark

Eurofins Product Testing Smedeskovvej 38 All FTMs except for 4, 7 and 19.
DK-84y64 Galten
Denmark A.S. Tel. +45-70-224276
Fax +45-70-224275
E-mail product-testing@eurofins.dk
URL www.eurofins.dk
www.dti.dk/
services/#p=23739
(English version)

Dansk Teknologisk Institut Gregersensvej 1 Migration testing


DK-2630 Taastrup
Tel. +45-72-202000
Fax +45-72-202019
E-mail info@dti.dk
URL www.teknologisk.dk/
laboratorier
www.dti.dk
(English version)
FINAT TECHNICAL HANDBOOK 2014 |

finland

KCL P.O. Box 70 KCL carries out research in pulping


FIN-02151 Espoo and papermaking. Research
Tel. +358-20-7477100
Fax +358-9-464305
covers the entire process from raw
E-mail kcl@kcl.fi materials to the four-colour printed
URL www.kcl.fi end-product.

88
finland

VTT Technical Research P.O. Box 1000 VTT is an impartial expert


FIN-02044 VTT
Centre of Finland Tel. +358-20-722111
organisation that carries out
Fax +358-29-7227001
technical and techno-economic
E-mail kirjaamo@vtt.fi research and development work. VTT
URL www.vtt.fi also produces information services.

france

Casimir P.O. Box 1000 Migration testing


24,avenue des Landais Polymers, nanomaterials, plastic,
BP 154
63173 AUBIERE Cedex
paper, carton
Tel. +33-4-73288528
Fax +33- 4-73286414
E-mail casimir@casimir.org
URL www.casimir.org

CTP Domaine Universitaire Migration testing


Mrs. Martine Deroche, DG Polymers, nanomaterials, plastic,
(Centre Technique du Papier)
BP 251
F-38044 Grenoble Cedex 9
paper, carton
Tel. +33-4-76154011
Fax +33-4-76154016
E-mail martine.deroche@webCTP.com
URL www.webCTP.com

I.A.N.E.S.C.O. Mrs. Marise Favard Migration testing


6, rue Carol Heitz, Biopole
(Institut d’Analyses et d’Essais
BP 90974
en Chimie de l’Ouest) F-86038 Poitiers Cedex
Tel. +33-5-49447614
+33-5-49447604 (lab)
E-mail m.favard@ianesco.fr
info@ianesco.fr
URL www.ianesco.fr

Ligépack 27-29 Rue Grémillion Migration testing


F-72000 Le Mans
Tel. +33-2-43289797
Fax +33-2-43281420
E-mail contact@ligepack.com
URL www.ligepack.com

LNE 1 rue Gaston Boissier Migration testing (food contact),


F-75724 Paris cedex calibration tests
(Laboratoire national de
Tel. 33-1-40433700
métrologie et d’essais) Fax 33-1-40433737
E-mail info@lne.fr
URL www.lne.eu or www.lne.fr
FINAT TECHNICAL HANDBOOK 2014 |

SGS - CTS Bat 8, Parc du Golf FTM 1, 2, 3, 5, 6, 7, 8, 10, 11, 12 13, 14,
F-13594 Aix-en-Provence Cedex 3 15, 16, 17, 18, 20 21, 22, 23 25
Tel. +33-4-42977213
Mob. +33-4-11738138
E-mail fabien.mille@sgs.com
URL www.sgsgroup.fr

89
SECTION 3.4 testing institutes

germany

Eurofins Dr. Specht Grossmoorbogen 25 Migration testing


D-21079 Hamburg
Laboratorien GmbH Tel. +49-40-8814480
Fax +49-40-881448101
E-mail specht@eurofins.de
URL www.labor-specht.de

Fabes Forschungs-GmbH Schragenhofstrasse 35 Migration testing


D-80992 München
für Analytik und Bewertung von
Tel. +49-89-149009-50
Stoffübergangen Fax +49-89-149009-80
E-mail: kontakt@fabes-online.de
URL www.fabes-online.de

FOGRA Forschungsgesellschaft Streitfeldstrasse 19 The purpose of the FOGRA is to


Druck (Graphic Technology Research D-81673 München promote research into, and the
Tel. +49-89-43182 0 development and application of
Association) Fax +49-89-43182 100 printing technology and to make
E-mail info@fogra.org the result available to the printing
URL www.fogra.org industry.

Fraunhofer Process engineering & packaging Migration testing


Giggenhuaser Strasse 35
Institut für Verfahrenstechnik und
D-85354 Freising
Verpackung IVV Tel. +49-8161-4910
Fax +49-8161-491491
E-mail info@ivv.fraunhofer.de
URL www.fraunhofer.de

Innoform GmbH Testservice Matthias Bösel FTM 1, 2


Industriehof 3 Test service provider for film
D-26133 Oldenburg packaging
Tel. +49-441-94986-0 (switchboard) Migration testing
+49-441-9498611
Fax +49-441-94986-29
E-mail info@innoform.de
Matthias.boesel@innoform.de
URL www.innoform.de

Institut Kuhlmann GmbH Analytik-Zentrum Ludwigshafen FTM 1, 2


Hedwig-Laudien Ring 3 Migration testing (foodstuffs,
D-67061 Ludwigshafen environmental analysis, REACH)
Tel. +49-621-6694490
Fax +49-621-66944999
E-mail labor@institut-kuhlmann.de
URL www.institut-kuhlmann.de

Institut Nehring GmbH Heesfeld 17 Migration testing, specifically


FINAT TECHNICAL HANDBOOK 2014 |

D-38112 Braunschweig analysis of pesticides in foods and


Tel. +49-531-238990 tobacco
Fax +49-531-2389977
E-mail info@institut-nehring.de
URL www.institut-nehring.de

ISEGA GmbH Zeppelinstraße 3 - 5 ISEGA is an independent testing


D-63741 Aschaffenburg institute with the capability for
Tel. +49-6021-49890 analytical and consulting work in:
Fax +49-6021-498930 • pulp, paper and board
E-mail info@isega.de • plastics
URL www.isega.de • packagings and consumer goods
• colours, lacquers, additives and
90 other chemicals
germany

PTS Papiertechische Stiftung Hessstr. 134 PTS conducts materials tests and
(The Paper Technology Specialists) D-80797 München analyses in:
Tel. +49-89-121460 (switchboard) Pulps and recovered paper, coating
URL www.ptspaper.de pigments, process additives; Paper,
paperboard, Adhesives, films,
Pirnaer Straße 37 composites and coatings; Paper
01809 Heidenau converting products and paper coating
Tel. +49-352-955160 products; Food microbiological and
Fax +49-352-9551899 food chemistry testing, environmental
E-mail irene.pollex@ptspaper.de compatibility; Water/effluents, sludge,
URL www.ptspaper.de solid wastes/waste

SGS NATEC Behringstrasse 154 Migration testing


D-22763 Hamburg
Institut für naturwissenschaftlich-
Tel. +49-40-883090
technische Dienste GmbH Fax +49-40-88309170
E-mail sgsnatec@sgs.com
URL http://natec-institut.de

SGS Institut Fresenius GmbH Im Maisel 14 Migration testing


D-65232 Taunusstein the security and quality of food,
Tel. +49-6128-7440 beverages and consumer products,
Fax +49-6128-7449890 REACH
E-mail info@institut-fresenius.de
URL www.institut-fresenius.de

Wessling Laboratorien GmbH – Oststrasse 6 Migration & sensory testing


Produktanalytik D-48341 Altenberge quality, safety, health and
Tel. +49-2505-890 environmental protection
Fax +49-2505-89119 applications
E-mail info@wessling.de
URL http://de.wessling-group.com

japan

JCII ITOHPiA hashimoto bldg. 7F Low temperature tests, tensile tests


(Japan Chemical Innovation and 11-9, Iwamoto-cho 2-chome thermal properties tests, optical
Chiyoda-ku, Tokyo, 101-0032 and weathering (light) tests
Inspection Institute) Tel. +81-3-5823-5521
E-mail info@jcii.or.jp
URL www.jcii.or.jp/en/

Chemitox, Inc. 1-14-18, Kamiikedai, Ohta-ku Weathering, product safety,


Tokyo 145-0064 photovoltaic modules, static
Tel.: +81-3-37277111 electricity, tensile strength tests
FINAT TECHNICAL HANDBOOK 2014 |

Fax +81-3-27281710
URL www.chemitox.co.jp/eng/

DJK Corporation 5376-1, Shimo-shinjuku, Kimagase, Peel adhesion, release force, coat
Noda-shi, Chiba 270-0222 weight, chemical resistance
Tel +81-4-71984111
Fax +81-4-71983358
E-mail info@djklab.com
URL www.djkrc.co.jp

91
SECTION 3.4 testing institutes

japan

IGT Testing Systems K.K. 1229-1, Mawatashi, Sakura-shi, Printability testing, maintenance &
Chiba-ken 285-0804 calibration
Tel. +81-43-3087302
Fax +81-43-3087304
E-mail japan@igt.nl
URL www.igt.nl

netherlands
Hechtingsinstituut Delft Kluyverweg 1 Adhesive bonding tests
2629 HS Delft
Tel +31-015-2785353
Fax +31-015-2787151
E-mail: info@hechtingsinstituut.nl :
URL www.hechtingsinstituut.nl

IGT Testing Systems Keienbergweg 25 CEPI comparative testing,


P.O.box 12688 printability testing, maintenance &
1100 AR Amsterdam calibration
Tel +31-20-4099300
Fax +31-20-6974842
E-mail info@igt.nl
URL www.igt.nl

TNO Tel. +31-88-8660000 (switchboard) REACH Migration service for food


+31088-8660866 (infodesk) contact. Research themes, for TNO
URL www.tno.nl Science and Industry: Equipment
for ultra precise production and
measurement

singapore

IGT Testing Systems Pte. Ltd. Blk. 3 Ang Mo Kio Printability testing, maintenance &
Ind. Park 2A calibration
#05-11 AMK Tech 1
Singapore 568050
Tel. +65 6481 8993
Fax: +65 6481 9685
URL www.igt.nl

spain

BIP Barcelona Institute of Packaging Tel. +34-9-34454437 Packaging testing: chemical


E-mail info@barcelonapackaging.org properties, physical mechanical
URL www.barcelonapackaging.org properties; aging tests; rheological
properties; logistic tests
FINAT TECHNICAL HANDBOOK 2014 |

sweden

INNVENTIA Box 5604 STFI carries out research in pulping


Drottning Kristinas väg 61 and papermaking. Research
SE-11486 Stockholm covers the entire process from raw
Tel. +46-8-6767000 materials to the four-colour printed
Fax +46-8-4115518 end-product.
E-mail info@innventia.com
URL www.innventia.com
92
united kingdom

Adhesive Technical Services Beacon Hill Industrial Estate Adhesive, label and tape testing
PO Box 51, Botany Way according to FINAT, AFERA, PSTC,
Purfleet, Essex RM19 1SY PSMA and ASTM.
Tel. +44–1708–867355 Agents for Cheminstruments
Fax +44–1708–869804
E-mail sales@adhtechnical.com
URL www.adhtechnical.com

Element (Materials Technology) Wilbury Way Accelerated ageing,


Hitchin Limited Hitchen, Herts SG4 0TW expertise in elastomers,
Tel. +44-1462-427850 thermoplastics, composites and
Fax +44-1462-427851 structural adhesives in diverse
E-mail info.hitchin@element.com applications and industries.
URL www.merl-ltd.co.uk Services include independent
www.element.com consultancy, mechanical testing,
chemical exposure testing, FEA,
rubber compound development,
inspection, test equipment and
software design.

National Physical Laboratory Hampton Road NPL maintains world-class


Teddington, Middlesex TW11 0LW metrology facilities and offers
Tel. +44-20-89773222 calibration services with the
Fax +44-20-89436458 highest available accuracy in
E-mail enquiry@npl.co.uk or physics and materials science.
measurement_services@npl.co.uk
URL www.npl.co.uk

Smithers PIRA Cleeve Road FTM 1, 2, 3, 9


Testing Services Europe Leatherhead Food contact testing
Surrey, KT22 7RU Adhesive and label tests
Tel. +44-1372-802000
Fax +44-1372-802079
E-mail testingservices@pira.co.uk
URL www.smitherspira.com

Smithers Rapra Shawbury Smithers Rapra is an independent


Shrewsbury, Shropshire SY4 4NR plastics and rubber consultancy.
Tel. +44-193 9393357 Rapra provides comprehensive
Fax +44-1939-251118 consultancy, technology and
E-mail info@smithers.com information services for the
URL www.rapra.net polymer industry and industries
using plastics and rubber in any
component, product or production
process.

usa
FINAT TECHNICAL HANDBOOK 2014 |

Adherent Laboratories Inc. 3804 Dunlap Street North Product development, consulting
Saint Paul, MN 55112 and testing laboratory specialising
Tel. +1- 651-4821264 in adhesives, sealants, coating and
E-mail info@adherentlabs.com material science.
URL www.adherentlabs.com

93
SECTION 3.4 testing institutes

usa

Brookfield Engineering 11 Commerce Boulevard Viscosity, Texture Analysis and


Laboratories Middleboro, MA 02346 U.S.A. Powder Flow
Tel. +1-508-9466200
+1-800-6288139 (toll free)
Fax +1-508-9466262
E-mail web.sales@
brookfieldengineering.com
URL www.brookfieldengineering.com

ChemInstruments, Inc. 510 Commercial Drive FTM 1, 2, 3, 4, 5, 7, 8 9, 10, 11, 13, 14,
Fairfield OH 45014 15,18, 21, 24
Tel. +1-513-8601598 Chemsultants International
Fax +1-513-8601597 Network is a source for contract
URL www.chemsultants.com research, laboratory testing,
pilot coating, consulting, test
instruments and hands-on
Chemsultants, Inc. Chemsultants, Inc. seminars.
9079 Tyler bvd
Mentor OH 44060
Tel. +1-440-9743080
Fax +1-440-9743081
URL www.chemsultants.com

IGT Testing Systems Inc. Arlington Center Printability testing,


543 West Golf Road maintenance & calibration
Arlington Heights, IL 60005
Tel. +1-847-9522448
Fax +1-847-9522449
E-mail usa@igt.nl
URL www.igt.nl

Smithers Pira 19 Northbrook Drive FTM 1, 2, 3, 9


Portland, Maine 04105
Tel. 1-207-7819800
Fax 1-207-7812150
E-mail mkuebler@smithers.com
URL www.smitherspira.com
FINAT TECHNICAL HANDBOOK 2014 |

94
3.5
tesa test tapes product information
and worldwide addresses
SECTION

tesa® 4104 transparent tesa® 7476


Transparent filmic packaging tape test tapes for the characterisation of silicone coatings

Productinformation Productinformation
tesa® 4104 is a premium packaging tesa® 7475 and 7476 are especially
tape based on a PVC-film backing designed for the characterisation of
and a natural rubber adhesive It silicone coated liners.
shows excellent performance on A typical test method represents
all kind of cardboards and secures FINAT 10 and FINAT 11.
a safe closure. The natural rubber For a comprehensive characterisation
adhesive system is designed to of release properties it is
show best results for applications recommended to use both tapes.
on different kind of surfaces.
tesa® 7475 features a typical modified a crylic adhesive to
Main Application record the interaction of a silicone and an acrylic adhesive.
• sealing small boxes (card-board or plastic) Additionally it shows a significant interaction with SiH
• sealing tins and bags Groups for measurement of the grade of curing of a silicone
• sealing of cartons of medium to heavy-range weight. by measuring the subsequent adhesion according FINAT 11.

Technical Data tesa® 7476 features a typical rubber adhesive to


• Backing material - PVC film characterise the interaction between a silicone and a
• Total thickness - 65 µm rubber adhesive.
• Type of adhesive - natural rubber
• Adhesion to steel - 2.3 N/cm Both tapes feature a significant adhesion even to
• Elongation at break - 60% easy-release silicone coatings to provide reproducible
• Tensile strength - 60 N/cm measurements.

Additional Info Main Application


tesa® 4104 is easily printable. • Test tapes for the characterisation of silicone coatings

Technical Data
tesa® 7475 pv2 • Backing material - cotton cloth
• Type of adhesive - natural rubber
Productinformation • Type of liner - glassine
tesa® 7475 has been successfully • Shelf life time - 12 months
deployed for many years, both when
it comes to assessing the release
properties of silicone coatings
(FINAT 10 or similar) and testing the latest information
curing of silicone coatings (FINAT
11 or similar). For a comprehensive tesa® 4104 - http://l.tesa.com/?ip=04104
characterization of release properties tesa® 7475 - http://l.tesa.com/?ip=07475
it is recommended to use both tesa® tesa® 7476 - http://l.tesa.com/?ip=07476
7475 (acrylic adhesive) and tesa®
FINAT TECHNICAL HANDBOOK 2014 |

7476 (natural rubber adhesive).

Main Application
• Characterization of silicone coatings

Technical Data
• Backing material - PET film
• Type of adhesive - acrylic
• Type of liner - glassine For the latest information on these
• Shelf life time - 24 months test tapes visit www.tesa.com
95
3.5
tesa test tapes product information
and worldwide addresses
SECTION
AFGHANISTAN BRAZIL CHINA CROATIA
tesa Export tesa Brasil Ltda. - Curitiba tesa tape (Guangzhou) Co., Ltd. tesa tape Kft.
Quickbornstraße 24 Ave. João Gualberto, No. 1259 - 18th Floor Room 1002-03, Zhongzhou Trading Representative Office
20253 Hamburg Centro Empresarial Lais Peretti Center, No. 1008, Xin Gang East Road, Tijardoviceva 8
Germany Alto da Gloria Haizhu District, Huangzhou 510335 10.000 Zagreb
Phone: +49 (40) 49094095 80030-000 Phone: +86 (20) 89300200 Phone: +385 (1) 3882929
Fax: +49 (40) 49092265 Curitiba-PR Fax: +86 (20) 89300201 Fax: +385 (1) 3882929
Manager: Jakob Ravn Phone: +55 (41) 30218100 Manager: Dick Li Manager: Gyula Behumi
Fax: +55 (41) 30218110
www.tesatape.com.br
Manager: Antonia Marques
ALL AFRICAN COUNTRIES CHINA CZECH REP.
tesa Export tesa tape (Hong Kong) Ltd. tesa tape s.r.o.
Quickbornstraße 24 The gate way tower 2, Suite 712, Pekarská 14
20253 Hamburg BULGARIA 25 Canton Road, Tsim Sha Tsui Kowloon, 155 00 Praha 5
Germany tesa tape A.E. Hongkong Phone: +420 (296) 824546
Phone: +49 (40) 49094095 Representative Office Phone: +852 (2) 25839980 Fax: +420 (296) 824549
Fax: +49 (40) 49092265 2, Agiou Nektariou Str. Fax: +852 (2) 25839244 www.tesa-tape.cz
Manager: Jakob Ravn GR-153 44 Gerakas / Attiki Manager: Dick Li Manager: Tomas Kuska
Phone: +30 (210) 6600290
Fax: +30 (210) 6610657
Manager: Kostas Theodoropoulos
ARGENTINA CHINA DENMARK
tesa tape Argentina S.R.L. tesa tape (Shanghai) Co., Ltd tesa A/S
Av. Del Libertador 6966 5° B No.1, 2500 Lane Xiu Pu Road, Klintehøj Vaenge 12
(C1429BMP) CHILE Pudong Shanghai 3460 Birkerød
Ciudad Autonoma de Buenos Aires tesa tape Chile S.A. Phone: +86 (27) 68183110 Phone: +45 (45) 998200
Argentina Av. Presidente Riesco 5561. Oficina 1104 Fax: +86 (27) 68183860 Fax: +45 (45) 810145
Phone: +54 (11) 47811846 Las Condes, Santiago Manager: Dick Li www.tesa.dk
Fax: +54 (11) 47869107 Phone: +56 (2) 3693600 Manager: Steve Plastow
www.tesatape.com.br Fax: +56 (2) 3693699
Manager: Antonio Marques www.tesa.cl
Manager: David Paz CHINA
tesa tape (Shenzhen) Co., Ltd ESTONIA
Room 11f, Jingyun Century tesa A/S Estonia
AUSTRALIA Mansion , No.6033 Shennan Street, Sepise 1
tesa tape Australia Pty. Ltd. CHINA Futian District, Shenzhen 518040 11415 Tallinn
Unit 8, 2 Southridge Street, tesa (Suzhou) Co., Ltd Phone: +86 (755) 33958620 Phone: +372 (640) 1366
Eastern Creek NSW 2766, Room 1716, Century Fiernancial Tower, Fax: +86 (755) 33958621 Fax: +372 (640) 1359
Sydney No.1 West Suzhoudadao, Suzhou Manager: Dick Li www.tesa.dk
Phone: +61 (2) 98303929 Industrial Park, Jiangsu 215021 Manager: Sergei Pljassunov
Fax: +61 (2) 98303928 Phone: +86 (512) 62965613
Manager: Gary Robinson Fax: +86 (512) 62965693
Manager: Mr. Dick Li CHINA
tesa Tape (Tianjin) Co., Ltd FINLAND
Room 11D1 Building A, DaAn Mansion, tesa Oy
AUSTRIA No.41, Friendship Road, HeXi Dist, Puutarhakatu 53
tesa GmbH CHINA Tianjin 300211 20100 Turku
Laxenburger Str. 151 tesa tape (Beijing) Co. Ltd. Phone: +86 (22) 28362660 Phone: +358 (2) 2103400
1100 Wien Room A704, Zhengjia Mansion, Fax: +86 (22) 28361990 Fax: +358 (2) 4103291
Phone: +43 (1) 614000 No.7, Jian Guo Road, Chaoyang Manager: Dick Li www.tesa.dk
Fax: +43 (1) 61400455 District, Beijing, 100024 Manager: Steve Plastow
www.tesa.at Phone: +86 (10) 85931022
Manager: Gabriele Kosar Fax: +86 (10) 85931021
Manager: Dick Li CHINA
tesa Tape (Wuhan) Co., Ltd FRANCE
Room 710, 7/F New World Centre, tesa s.a.s.
BAHRAIN Tower A, Hangkong Road, Jiefang La Croix du Sud - ZAC CARRE SENART
tesa Export CHINA Avenue, Wuhan 430022 2 Allée de la Mixité
Quickbornstraße 24 tesa tape (Changchun) Co. Ltd. Phone: +86 (27) 68838713 77127 Lieusaint
20253 Hamburg Room 1101, Fax: +86 (27) 68838710 Phone: +33 (1) 78482000
Germany ZhongTian Mansion No. 2066, Manager: Dick Li Fax: +33 (1) 78482001
Phone: +49 (40) 49094095 Puyang Street, Lvyuan Dist, www.tesa.fr
Fax: +49 (40) 4909 2265 Changchun 130062 Manager: Bruno Derouet
FINAT TECHNICAL HANDBOOK 2014 |

Manager: Jakob Ravn Phone: +86 (431) 87060978


Fax: +86 (431) 87060986 COLOMBIA
Manager: Dick Li tesa tape Colombia Ltda.
Calle 67 Norte #7N-59 piso 3 GREECE
BELGIUM Barrio Menga tesa tape A.E.
tesa sa-nv CALI - Valle del Cauca 2, Agiou Nektariou Str.
Chaussée de Ruisbroek, 76 CHINA Servicio al cliente: 018000 950505 GR-153 44 Gerakas / Attiki
Ruisbroeksesteenweg, 76 tesa tape (Chongqin) Co., Ltd Phone: +57 (2) 6878484 Phone: +30 (210) 6600290
1180 Bruxelles Room1103, Tower, No. 38, Jianxin North Fax: +57 (2) 6878475 Fax: +30 (210) 6610657
Phone: +32 (2) 5250811 Road, Jiangbei District, Chongqing Manager: Juan Carlos Sarassa www.tesa.gr
Fax: +32 (2) 5250833 40020 Manager: Kostas Theodoropoulos
www.tesa.be Fax: +86 (23) 67612062
Manager: Ferdy Denie Manager: Dick Li

96
GUATEMALA ITALY JORDAN MEXICO
tesa tape Centro América S.A. tesa SpA tesa Export tesa tape México
Diagonal 6, 10-50 Zona 10 Via L. Cadorna 69 Quickbornstraße 24 Av. Santa Fe No. 170
Edificio Interamericas WFC 20090 Vimodrone (Milano) 20253 Hamburg German Centre P 6-3-3
Torre Norte nivel 12, oficina 1202 Phone: +39 (02) 25010811 Germany Col. Lomas de Santa Fe
Guatemala, C.A. Fax: +39 (02) 25010841 Phone: +49 (40) 49094095 D.F. C.P. 01210
Phone: +502 (2) 2449100 Manager: Matteo Martinelli Fax: +49 (40) 49092265 Phone: +52 (55) 52926978
Fax: +502 (2) 2449191 Manager: Jakob Ravn www.tesatape.com
Manager: Carlos Blanco Manager: Fernando Cruz

JAPAN
tesa tape K.K. KOREA
HUNGARY 8F, Shirokanetakanawa Station Bldg. tesa tape Korea Ltd. NETHERLANDS
tesa tape Kft. 1-27-6 Shirokane, Minato-ku City Air Tower 159-9, Room 1805 tesa BV
2040 Budaörs Tokyo 108-0072 Samseong-dong, Gangnam-gu Stationsplein 3-1
Szabadság út 117. Phone: +81 (3) 68332300 Seoul 135-973 1211 EX Hilversum
Phone: +36 (23) 814154 Fax: +81 (3) 34737440 Korea Phone: +31 (35) 6250200
Fax: +36 (23) 814160 www.tesa.jp Phone: +822 (569) 8451 Fax: +31 (35) 6250240
www.tesa.hu Manager: Andreas Walkembach Fax: +822 (569) 8455 www.tesa.nl
Manager: Gyula Behumi Manager: Detlev Radloff Manager: Ferdy Denie

JAPAN
INDIA tesa tape K.K. (Nagoya) KUWAIT NEW ZEALAND
tesa Tapes (India) Pvt. Ltd. 7F, arex Bldg, tesa Export tesa tape New Zealand Ltd.
301, 3rd Floor, Lakhani Centrium, 1-4-12, Marunouchi, Naka-ku, Nagoya- Quickbornstraße 24 PO Box 33-121
Plot No 27, Sec 15, CBD Belapur, shi, 20253 Hamburg Takapuna, 0740
Navi Mumbai - 400614 Aichi-ken 460-0002 Germany Auckland
Maharashtra Phone: +81 (52) 2234511 Phone: +49 (40) 49094095 Phone: +64 (0800) 837269
Phone: +91 (22) 47419200 Fax: +81 (52) 2234512 Fax: +49 (40) 49092265 Fax: +64 (0800) 837267
Fax: +91 (22) 47419299 www.tesa.jp Manager: Jakob Ravn Manager: Gary Robinson
Manager: Venkatesh Inamdar Manager: Andreas Walkembach

LATVIA NORWAY
INDONESIA JAPAN tesa A/S tesa AS
tesa tape Asia Pacific Pte. Ltd. tesa tape K.K. (Osaka) Vienibas gatve 109 Karihaugveien 89
11th Floor, Suite A, Perwata Tower 4F, Risoshinosaka Bldg, 4-3-7-Miyahara, LV 1058, Riga 1086 Oslo
CBD Pluit, Jl Pluit Selatan Raya Yodogawa-ku. Osaka-shi, Phone: +371 (679) 30180 Phone: +47 (22) 907979
Jakarta Utara 14440 Osaka-fu 532-0003 Fax: +371 (679) 30179 Fax: +47 (22) 300376
Phone: +62 (21) 66672978 Phone: +81 (6) 63965811 www.tesa.dk www.tesa.dk
Fax: +62 (21) 66672985 Fax: +81 (6) 63967648 Manager: Andris Kranevskis Manager: Steve Plastow
Manager: Tanaka Takafumi www.tesa.jp
Manager: Andreas Walkembach

LEBANON OMAN
IRAN tesa Export tesa Export
tesa Export JAPAN Quickbornstraße 24 Quickbornstraße 24
Quickbornstraße 24 tesa tape K.K. 20253 Hamburg 20253 Hamburg
20253 Hamburg Technical Center (tTC) Germany Germany
Germany 10F, Shirokanetakanawa Station Bldg Phone: +49 (40) 49094095 Phone: +49 (40) 49094095
Phone: +49 (40) 49094095 1-27-6 Shirokane, Minato-ku Fax: +49 (40) 49092265 Fax: +49 (40) 49092265
Fax: +49 (40) 49092265 Tokyo 108-0072 Manager: Jakob Ravn Manager: Jakob Ravn
Manager: Jakob Ravn Phone: +81 (3) 68332321
Fax: +81 (3) 54235753
www.tesa.jp
Manager: Andreas Walkembach LITHUANIA PAKISTAN
IRAQ tesa A/S tesa Export
tesa Export V.Gerulaicio str.1 Quickbornstraße 24
Quickbornstraße 24 08200 Vilnius 20253 Hamburg
20253 Hamburg JAPAN Lithuania Germany
Germany tesa tape K.K. Warehouse Phone: +370 (5) 2191555 Phone: +49 (40) 49094095
Phone: +49 (40) 49094095 C/O Japan transcity Corp, Fax: +370 (5) 2191554 Fax: +49 (40) 49092265
Fax: +49 (40) 49092265 1221 Minamibansyu, Mitsubuchi, www.tesa.dk Manager: Jakob Ravn
FINAT TECHNICAL HANDBOOK 2014 |

Manager: Jakob Ravn Komaki-shi, Aichi-ken 485-0075 Manager: Stasys Jonynas


Phone: +81 (568) 427161
Fax: +81 (6) 63967648
www.tesa.jp PHILIPPINES
ISRAEL Manager: Andreas Walkembach MALAYSIA tesa tape Asia Pacific Pte. Ltd.
tesa Export tesa tape (Malaysia) Sdn Bhd. Rep. Office Philippines
Quickbornstraße 24 No 49, Jalan P10/21 164 Gul Circle
20253 Hamburg Taman Industri Selaman, Seksyen 10 Singapore 629621
Germany 43650 Bandar Baru Bangi, Selangor, Phone: +65 (68) 612026
Phone: +49 (40) 49094095 West Malaysia Fax: +65 (68) 612361
Fax: +49 (40) 49092265 Phone: +60 (3) 89273010 Manager: Tanaka Takafumi
Manager: Jakob Ravn Fax: +60 (3) 89273028
Manager: Tanaka Takafumi

97
3.5
tesa test tapes product information
and worldwide addresses
SECTION
POLAND SLOVENIA TAIWAN UNITED ARAB EMIRATES
tesa tape Sp. z o.o. tesa tape d.o.o. tesa tape (Hong Kong) Ltd. - tesa Middle East
ul. Gnieznienska 32 Pot k sejmiscu 30 Taiwan Branch Office No.: LOB 15-604C
61-021 Poznan 1231 Lj.-Crnuce 9F-1, 3, Sec 1 Min Sheng Road Jebel Ali Free Zone,
Phone: +48 (61) 8746147 Phone: +386 (1) 5602409 Panchiao 220, Taipei Hsien PO Box 261534
Fax: +48 (61) 8746019 Fax: +386 (1) 5602415 22069 Taiwan Dubai, United Arab Emirates
www.tesa.pl www.tesa.si Phone: +886 (2) 29579662 Phone: +971 (4) 8808933
Manager: Tomasz Badyda Manager: Gylua Behumi Fax: +886 (2) 29579433 Mobile: +971 (5) 54056706
Manager: Dick Li Manager: Richard Dunn

PORTUGAL SOUTH AFRICA


tesa Portugal, Lda. tesa SA TAIWAN UNITED KINGDOM
Rua Soeiro Pereira Gomes, 59 21 Lighthouse Drive tesa tape (Taiwan) Co., Ltd tesa UK Ltd.
Queluz de Baixo, Apartado 87 Umhlanga Rocks 4319 9F-1, No.3, Sec. 1 Mingsheng Rd, Yeomans Drive, Blakelands
PT 2746-901 Queluz South Africa Panchiao Dist, New Taipei City 220, Milton Keynes, Bucks MK 14 5LS
Phone: +351 (21) 4349600 Phone: +27 (31) 2678534 22069 Taiwan Phone: +44 (1) 908 211333
Fax: +351 (21) 4351499 Mobile: +27 (82) 9084752 Phone: +8 (52) 25839980 Fax: +44 (1) 908 211555
www.tesa.pt Manager: Stuart Gannon Fax: +8 (52) 25989244 www.tesa.co.uk
Manager: Jordi Senespleda Manager: Mr. Dick Li Manager: Stephen Hauber

SPAIN
QATAR tesa tape S.A. THAILAND USA
tesa Export Ctra. de Mataró a Granollers, P. Km. 5,4 tesa tape Thailand Limited tesa tape inc.
Quickbornstraße 24 08310 Argentona 1858/80, 17th Floor, Nation Tower 800 W. El Camino Real - Suite 180
20253 Hamburg Phone: +34 (93) 7583300 Bangna-Trad Road, Bangna Bangna Mountain View, CA 94040
Germany Fax: +34 (93) 7583444 Bangkok 10260 electronics.tesa.com
Phone: +49 (40) 49094095 www.tesatape.es Phone: +66 (2) 751 4025 to 4029
Fax: +49 (40) 49092265 Manager: Jordi Senespleda Fax: +66 (2) 7514030
Manager: Jakob Ravn Manager: Tanaka Takafumi
VIETNAM
tesa tape Asia Pacific Pte Ltd.
SRI LANKA Unit 705A, 7th Floor, Me Linh Point Tower
ROMANIA tesa Export TURKEY No. 2 Ngo Duc Ke Street
tesa tape SRL Quickbornstraße 24 tesa Bant Sanayi ve Ticaret A.S. District 1
str.Observatorului , nr.113A, etaj 1, 20253 Hamburg Merdivenköy Mah. Bora Sokak No:1 Ho Chi Minh City
Cluj-Napoca, 400363 Germany Nida Kule Göztepe K:4 Phone: +84 (8) 823 7850 Ext 2805 &
Romania Phone: +49 (40) 49094095 34732 Kadıköy İstanbul 2806
Phone: +40 (364) 401140 Fax: +49 (40) 49092265 Phone: +90 (216) 5789000 Fax: +84 (8) 8237840
Fax: +40 (364) 401141 Manager: Jakob Ravn Fax: +90 (216) 5789001 Manager: Tanaka Takafumi
www.tesatape.ro www.tesabant.com.tr
Manager: Magnus Becker Manager: Mete Konuralp

SWEDEN VIETNAM
tesa AB tesa tape Asia Pacific Pte Ltd.
RUSSIA Box 10275 TURKEY Unit 210, 2nd Floor, V-Tower
tesa tape OOO 434 23 Kungsbacka tesa scribos Turkey 649 Kim Ma Street, BaDinh District
Shabolovka 10, Building 2 Phone: +46 (300) 55350 Merdivenköy Mah. Bora Sokak No:1 Hanoi
119049 Moscow Fax: +46 (300) 19494 Nida Kule Göztepe K:4 Phone: +84 (4) 7667800
Phone: +7 (495) 2584024 www.tesa.dk 34732 Kadıköy İstanbul Fax: +84 (4) 7667801
Fax: +7 (495) 7923245 Manager: Steve Plastow Phone: +90 (216) 5789000 Manager: Tanaka Takafumi
www.tesatape.ru Fax: +90 (216) 5789001
Manager: Audrius Petryla www.tesa-scribos.com
Manager: Ms. Tuba Olak
SWITZERLAND YEMEN
tesa tape Schweiz AG tesa Export
SAUDI ARABIA Industriestr. 19 Quickbornstraße 24
tesa Export 8962 Bergdietikon UKRAINE 20253 Hamburg
Quickbornstraße 24 Phone: +41 (44) 7443444 Representative Office Germany
20253 Hamburg Fax: +41 (44) 7412672 tesa tape KFT Phone: +49 (40) 49094095
Germany www.tesa.ch 104 Saksaganskogo street Fax: +49 (40) 49092265
Phone: +49 (40) 49094095 Manager: Claus Grobe Office 4 Manager: Jakob Ravn
Fax: +49 (40) 49092265 Kyiv 01032
FINAT TECHNICAL HANDBOOK 2014 |

Manager: Jakob Ravn Phone: +380 (44) 2357692


Fax: +380 (44) 2341810
SYRIA Manager: Sebastian Sattler
tesa Export
SLOVAKIA Quickbornstraße 24
tesa tape s.r.o. - organizacna 20253 Hamburg
zlozka Slovensko Germany
Riznerova 5 Phone: +49 (40) 49094095
81101 Bratislava Fax: +49 (40) 49092265
Phone: +421 (257) 101620 Manager: Jakob Ravn
Fax: +421 (257) 101600
www.tesa.sk
Manager: Tomas Kuska

98
World-wide Association for self-adhesive labels and related products
P.O. Box 85612
2508 CH The Hague
The Netherlands
Tel.: +31 (70) 312 39 10
Fax: +31 (70) 363 63 48
E-mail: info@finat.com
Internet: www.finat.com

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