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Test methods
9th Edition
FINAT
TECHNICAL
HANDBOOK
Test Methods - 9th edition
Copyright © 2014 by FINAT, The Hague, The Netherlands. All rights reserved.
No part of this publication may be translated, reproduced, stored or transmitted, in any form or by any
means, electronic or mechanical, photocopying, recording or otherwise, without the prior written permission
of the publisher.
FINAT
The Hague, May 2014
PREFACE
preface to the 9th edition
It is my pleasure to herewith present you with the 9th edition of the Technical
Handbook. The Handbook is globally acknowledged as being the authoritative
benchmark on test procedures for adhesive labels. The FINAT test methods
described in the Handbook are used to evaluate label stock and frequently
serve as a basis for specifications. Since the first edition 30 years ago the
Technical Handbook has been continually revised. New test methods were
added, existing ones revised and obsolete ones deleted.
This edition features two new test methods (FTM 28 and FTM 29) on bleeding
through paper and scratch resistance of an UV ink film on different print
materials, and also Section 2.10 on the light fastness of printing ink. A number
of proven test methods are now much easier to understand as some graphic
material has been added to them.
At this juncture I should like to thank all members of the Technical Committee
for their excellent contributions to the design, translation and revision of the
content. I am particularly grateful to the members of the Subcommittee on
Test Methods who are the driving force behind this edition and take the main
responsibility for it. We owe the quality and high acceptance of the FINAT test
methods all over the world to the composition of the Technical Committee
where specialists from the entire adhesive label industry meet. Although
English is the globally accepted language of the industry we shall nonetheless
try to translate the Technical Handbook into as many languages as our
resources allow us to do.
Hans Lautenschlager
Chairman of the Subcommittee on Test Methods
5
CONTENTS
section 1 | finat test methods
Method Description Construction Test relevant to
FTM 1 Peel adhesion (180°) at 300 mm per minute Face stock Adhesion 8
FTM 2 Peel adhesion (90°) at 300 mm per minute Face stock Adhesion 10
FTM 3 Low speed release force Laminate Delamination 12
FTM 4 High speed release Force Laminate Matrix stripping 13
FTM 5 Accelerated ageing – Extended storage Laminate Ageing 15
FTM 6 Resistance to ultra-violet light Laminate Ageing 16
FTM 7 Silicone Coat Weight by energy-dispersive
X-ray fluorescence spectrometry Liner Coating quality 18
FTM 8 Resistance to shear from a standard surface Face stock Adhesion 20
FTM 9 Loop’ tack measurement Face stock Adhesion 22
FTM 10 Quality of silicone coated substrates for
self-adhesive laminates: release force Liner Dispensing 24
FTM 11 Quality of silicone coated substrates for
self-adhesive laminates: subsequent adhesion Liner Silicone cure 26
FTM 12 Adhesive coat weight Face stock Coating quality 28
FTM 13 Low temperature adhesion Face stock Adhesion 29
FTM 14 Dimensional stability Face stock Stability 31
FTM 15 Surface tension of plastic films Face stock Printing 33
FTM 16 Chemical resistance – Spot method Face stock Stability 35
FTM 17 Chemical resistance – Immersion method Face stock Stability 36
FTM 18 Dynamic shear Face stock Adhesion 38
FTM 19 Recycling compatibility of self-adhesive labels Face stock Recycling 40
FTM 20 Fluorescence and whiteness Face stock Printing 41
FTM 21 Ink adhesion - basic Face stock Printing 43
FTM 22 Ink adhesion - advanced Face stock Printing 45
FTM 23a Testing for die-strike on paper Laminate Dispensing 46
FTM 23b Testing for die-strike on clear filmic liners Laminate Dispensing 48
FTM 24 Mandrel hold Face stock Adhesion 50
FTM 25 Evaluation of the silicone coverage of coated
papers by use of a water based stain test Liner Coating quality 52
FTM 26 Wash-off paper and film labels Face stock Adhesives 55
FTM 27 Ink rub test for UV printed labels ink surface
against substrate or ink surface Laminate Printing 56
FINAT TECHNICAL HANDBOOK 2014 |
6
section 2 | guidelines
Although the 29 FINAT Test Methods described in this publication have been prepared with the utmost care and
accuracy, it should be noted that the safety, efficiency and performance of these test methods and associated
procedures is the responsibility of the end-user. FINAT cannot be held liable for any loss, damage or injury resulting
from their application. Furthermore, the test methods and associated information do not in themselves imply any
specification of performance relating to the materials under test.
7
FTM1
peel adhesion (180°) at
300 mm per minute
scope
This test method is designed to quantify the permanence
of adhesion or peel ability of self-adhesive pressure
sensitive materials.
definition
Peel adhesion is defined as the force required to remove
pressure sensitive coated material, which has been applied
to a standard test plate under specified conditions from the
plate at a specified angle and speed.
Adhesion is measured 20 minutes and 24 hours after
application, the latter being considered as the ultimate
adhesion. procedure
Remove the backing material from each strip and place the
test equipment adhesive coated facing material, adhesive side down, on to
a clean test plate using light finger pressure.
A tensile tester or similar machine, capable of peeling a Roll twice in each direction with the standard FINAT test
laminate through an angle of 180° with a jaw separation roller at a speed of approximately 10 mm per second to
rate of 300 mm per minute with an accuracy of ± 2%. obtain intimate contact between the adhesive mass and
the surface.
Test plates made of float glass or similar plate glass.
After applying the strips to the test plate, leave for a period
A standard FINAT test roller. of 20 minutes before testing. Repeat the procedure with
a second set of strips and leave for a period of 24 hours
before testing.
test pieces
Fix the test plate and strip in the machine so that the angle
These should be strips taken from a representative sample of peel is 180°. Set the machine at 300mm per minute
of material. The strips should be 25 mm wide and have jaw separation rate. Carry out the test taking at least five
a minimum length of 175 mm in the machine direction. readings at 10 mm intervals from the centre section of each
The cuts should be clean and straight. At least three strips test strip.
should be taken from each material sample. Average the five or more readings for each strip.
test conditions
FINAT TECHNICAL HANDBOOK 2014 |
8
results Alternative methods which remove contamination
properly can be adopted e.g. ultrasonic cleaning.
Peel adhesion (180°) is expressed as the average result for
the strips tested in Newton per 25mm width for either 20 Prior to use, the cleaned plates should be left for 4
minutes or 24 hours application time. hours under standard test conditions. Care should be
taken to handle clean plates by the edge only.
Failure Description Code
2. Alternative surfaces to plate glass can be used such as
CP Clear Panel - no visible stain on panel. stainless steel (example: AFERA1 quality stainless steel
PS Panel Stain - discoloration of test area, but no plates), aluminium or polymeric substrates, but this
tacky residue of adhesive on both the panel and must be clearly stated alongside the results.
the front material.
CF Cohesive Failure - the adhesive film is split during 3. If adhesion values are required when paper tear has
the test, leaving residue of adhesive on both the occurred, then this test can be conducted at lower jaw
panel and the front material. separation rates quoting the latter against the results.
AT Adhesive Transfer - the adhesive separates clearly
from the front material, leaving adhesive film on 4. Conversion 1kgf- = 9.81 N
the test panel.
The approximate extent of transfer should be Issued October 1985
quoted as percentage. Revised March 1999
PT Paper Tear - the adhesive force exceeds the Revised May 2001
strength of a paper facing material. The results Revised February 2014
quoted should be the maximum reached before
the paper tears.
notes
1. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:
and made exclusively from virgin materials. A 50 mm by 125 mm no less than 1.1 mm thick stainless
steel 1.4301 in accordance with the 2R quality defined in
Dispense one of the solvents listed above on to the EN10088-2 having a bright annealed finish. The surface
panel, wiping it to dryness with fresh absorbent roughness height shall be (50 ± 25) nm arithmetical average
cleaning material. Repeat for a total of three washes deviation from the mean line. Panels showing stains,
with the solvent. Final wipe shall be with MEK or discoloration, or many scratches are not acceptable.
acetone. More details can be found in the AFERA test method manual.
9
FTM2
peel adhesion (90°) at
300 mm per minute
definition
Peel adhesion is defined as the force required to remove
pressure sensitive coated material, which has been applied
to a standard test plate under specified conditions, from
the plate at a specified angle and speed. Adhesion is
measured 20 minutes and 24 hours after application, the
latter being considered as the ultimate adhesion.
test equipment
A tensile tester or similar machine capable of peeling a procedure
laminate through an angle of 90° with a jaw separation
rate of 300 mm per minute and an accuracy of ± 2%. The Remove the backing material from each strip and place
apparatus must be equipped in a manner which ensures the adhesive coated facing material, adhesive side down,
that the test plate can move freely in a horizontal position on to a clean test plate using light finger pressure. Roll
when the pressure sensitive material is removed in order to twice in each direction with the standard FINAT test roller
maintain an angle of peel of 90°. at a speed of approximately 10 mm per second to obtain
intimate contact between the adhesive mass and the
Test plates made of float glass or similar plate glass. surface.
A standard FINAT test roller. After applying the strip to the test plate, leave for a period
of 20 minutes before testing. Repeat the procedure with
a second set of strips and leave for a period of 24 hours
test pieces before testing.
These should be strips from a representative sample of Fix the test plate and strip into the horizontal support
material. The strips should be 25 mm wide and have a which has been secured into the bottom jaw of the
minimum length of 175 mm in the machine direction. tensile tester. Set the machine at 300 mm per minute
The cuts should be clean and straight. At least three strips jaw separation rate. Carry out the test taking at least five
should be taken from each material sample. readings at 10 mm intervals from the centre section of the
test strip. Average the five or more readings for each strip.
FINAT TECHNICAL HANDBOOK 2014 |
10
results Alternative methods which remove contamination
properly can be adopted, e.g. ultrasonic cleaning.
Peel adhesion (90°) is expressed as the average result for
the strips tested in Newtons per 25 mm width for either 20 Prior to use, the cleaned plates should be left for 4
minutes or 24 hours application time. hours under standard test conditions. Care should be
taken to handle clean plates by the edge only.
Failure Description Code
CP Clear Panel - no visible stain on panel. 2. Alternative surfaces to plate glass can be used such as
PS Panel Stain - discoloration of test area, stainless steel(example: AFERA1 quality stainless steel
but no tacky residue. plates),aluminium or polymeric substrates, but this
CF Cohesive Failure - the adhesive film is split during must be clearly stated alongside the results.
the test, leaving residue of adhesive on both the
panel and the front material. 3. If adhesion values are required when paper tear has
AT Adhesive Transfer - the adhesive separates cleanly occurred then this test can be conducted at lower jaw
from the front material, leaving adhesive film on separation rates quoting the latter against the results.
the test panel.
The approximate extent of transfer should be 4. Conversion 1 kgf = 9.81 N
quoted as percentage.
PT Paper Tear - the adhesive force exceeds the Issued October 1985
strength of a paper facing material. The results Revised March 1999
quoted should be the maximum reached before Revised May 2001
the paper tears. Revised February 2014
notes
1. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:
11
FTM3 low speed release force
definition procedure
Low speed release force is defined as the force required Fix each strip to the plate by means of a double sided
to separate a pressure sensitive adhesive coated material tape (which should cover the full test area of the sample),
from its backing or protective sheet (or vice versa) at an so that the laminate can be peeled apart at an angle of
angle of 180° and a jaw separation rate of 300mm per 180°. The facing material may be peeled from the release
minute. substrate, or vice versa, depending on how the sample is
applied to the plate. The method of peel must be quoted
with the results.
test equipment
A tensile tester or similar
machine, capable of peeling
a laminate through an angle
of 180° with a jaw separation
rate of 300 mm per minute
with an accuracy of ± 2%.
The equipment should be
fitted with a back plate to
which the test strip can be
attached in order to maintain
an angle of peel of 180°. Picture 2: Test strips attached to the back plate
FTM4
scope test pieces
This test method allows the label user to assess the These should be taken from a representative sample of
separation force of a laminate at speeds comparable to material. The strips should be 25 mm wide and have a
those typically used to convert and dispense the material. minimum length of 300 mm in the machine direction. The
It therefore gives a far more meaningful assessment of testing device may require extra length for clamping the
the conversion characteristics than FTM 3. Very low values material. The strips must be free from damage (creases,
may create label fly during conversion or application. High blisters etc.) and cut with clean edges.
values may produce web break when skeleton stripping
die cut labels or dispensing failure during automatic
application. test conditions
The material under test is placed between two flat metal
definition or glass plates and kept for 20 hours at 23°C ± 2°C under
a pressure of 6.87 kPa (70 g/cm2) to ensure good contact
High speed release force is defined as the force required to between the release paper and the adhesive.
separate:
Up to 20 strips can be kept between the plates.
• (mode 1) a pressure sensitive adhesive coated material
from its backing or protective sheet After storage in this manner, the strips should be taken
• (mode 2) the backing from the adhesive coated from between the glass plates and kept for not less than
material, both at an angle of 180° and at jaw separation 4 hours at the standard test conditions of 23°C ± 2°C and
rates between 10 m and 300 m per minute. 50% RH ± 5% RH.
The two modes will mostly give different results. Accelerated ageing may be carried out by placing a similar
set of strips between two flat metal or glass plates and
keeping for 20 hours in an air circulating oven at 70°C ±
test equipment 5°C. The strips should then be removed and conditioned
for at least 4 hours as above. See also FTM 5.
A machine capable of peeling a laminate through an angle
of 180° with a jaw separation rate range of 10 - 300 m per
minute. The machine should preferably have a facility for
recording the release force continuously (see picture 1).
procedure
Mode 1:
Separating adhesive coated face material from release
backing
When the adhesive component is pulled from the backing
by a roller mechanism it may be necessary to prevent the
adhesive sticking to the rollers in the drive mechanism.
This may be achieved by a strip of glassine release base
FINAT TECHNICAL HANDBOOK 2014 |
13
FTM4 high speed release force
Mode 2:
Separating release backing from adhesive coated face
material
The procedure is as described above except that the
position of the laminate components is reversed and it is
not necessary to use a protective strip.
results
High speed release force is expressed as the peak or
average result for the strips tested in centiNewtons (cN)
per 25 mm width. This should be quoted alongside the test
speed used and the means of peeling employed:
• (mode 1) facing material from release backing or
• (mode 2) release paper from facing material. The type
of result (peak or average) should be quoted.
notes
1. Results based on merely peak and/or average release
force values may be misleading, particularly at high
separation speeds. It is strongly recommended that
the release test device be used with a high speed
trace recorder.
14
FTM5
accelerated ageing
– extended storage
Climate chamber
results
Paper cutter
Resistance to accelerated ageing by submitting test
samples to elevated temperature is expressed as the
procedure percentage reduction (any increase being denoted as such)
in each average value, when compared to the control.
Place the strips, still covered with their protective backing
material in the test oven under the test conditions without The discoloration and strike through should be reported
allowing them to come into contact with each other (i.e. descriptively as nil, slight, moderate or severe.
hanging freely). Retain the control set of strips at 23°C ±
2°C and 50% RH ± 5% RH. All conditions should be carefully reported.
At the end of the accelerated ageing test period, remove Issued October 1985
the strips from the ageing cabinet and allow them to Revised March 1999
condition according to the appropriate FINAT test method Revised May 2001
(FTM 1, 2, 8 or 9). Test the aged strips, together with the Revised October 2008
control (non aged) strips.
To evaluate the migration – strike through, the single strip
and a control should also be evaluated for discoloration
and strike through of the adhesive, by removing them from
their protective release material, then adhering the samples
to black card and carrying out a visual examination.
Alternatively a spectrophotometer can be used.
test conditions
Ageing tests are typically carried out for a period of 4
weeks, and the tests are done once a week.
The test should always include a previously tested, known
FINAT TECHNICAL HANDBOOK 2014 |
15
FTM6 resistance to ultra-violet light
test pieces
results
These should be strips taken from a representative sample
of material. The strips should be 25 mm wide and have Resistance to ultra-violet light is expressed as the
a minimum length of 175 mm in the machine direction. percentage reduction (any increases being denoted as
The cuts should be clean and straight. A minimum of three such) in each average value when compared to the control
strips are required for each physical property being tested samples.
together with a single strip for evaluation of discoloration
and strike through. A duplicate set of strips is also required The discoloration and strike-through should be reported
to act as control. descriptively as nil, slight, moderate or severe.
16
notes
1. The exposure levels are taken from the International
Standard ISO 105: 1978
‘Textiles - Tests for Colour Fastness’. The equivalent
British Standard is BS 1006:1978 – ‘Colour Fastness of
Textiles and Leather’.
2. The Blue Wool Scales and Grey Scales are obtainable
from various national Standard Organisations
including:
Fax: +33-1-49179000
URL: www.afnor.fr
Issued 1985
Revised October 1995
Revised March 1999
Revised May 2001
Addresses revised January 2014
17
FTM7
silicone coat weight by
energy-dispersive x-ray
fluorescence spectrometry
test equipment
This method is based on the use of a ‘bench-top’ X-ray
fluorescence spectrometer (XRF) for laboratory and also
routine production measurement of silicone coat weight
using the principle of X-ray fluorescence. A number of
benchtop XRF analysers have been used in the past,
but the main commercially available equipment most
commonly used are from the Oxford Instruments Lab-X
series (which includes the Lab-X 3500 and X-Supreme
models as well as the older Lab-X 3000 and 2000 models).
procedure
The sample discs are placed into a special sample holder
designed by the manufacturers to handle paper or film
substrates, ensuring that a flat reproducible sample surface
is measured by the analyser. The samples are introduced
into the analyser where they are ultimately moved into
a special measurement chamber where irradiation
with primary X-rays results in the emission of resultant
FINAT TECHNICAL HANDBOOK 2014 |
4. Most calibration curves are established for silicone Issued April 2001
release coatings as ‘Polydimethlsilicone’. Whilst this Revised January 2014
19
FTM8
resistance to shear from
a standard surface
procedure
test equipment
A rack or jig to hold the test plate precisely 2° from the
vertical (see diagram below).
1 kg weight.
Remove the backing material from each strip and place the
adhesive coated facing material, adhesive side down, on
to a clean test plate using light finger pressure, so that a
square of pressure sensitive coated material, 25 mm x 25
mm, is in actual contact with the surface. Roll twice in each
direction with the standard FINAT test roller at a speed
of approximately 10 mm per second to obtain intimate
contact between the adhesive mass and the surface. Any
strips found by inspection to have air bubbles trapped
FINAT TECHNICAL HANDBOOK 2014 |
Note the time taken for the strips to part from the plate.
20
results 2. Alternative surfaces to plate glass can be used such as
stainless steel or aluminium but this must be clearly
Resistance to shear from a standard surface is expressed stated alongside the results.
as the average time taken for the three strips to shear from
the test plate. 3. Alternative weights can be used, but these must be
clearly stated alongside the results.
Failure Description Code:
CP Clear Panel - no visible stain on panel. Issued October 1985
PS Panel Stain - discoloration of test area, but no Revised March 1999
tacky residue. Revised May 2001
CF Cohesive Failure - the adhesive film is split during
the test, leaving residue of adhesive on both the
panel and the front material.
AT Adhesive Transfer - the adhesive separates cleanly
from the front material, leaving adhesive film on
the test panel.
The approximate extent of transfer should be quoted as
percentage
notes
1. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:
• Diacetone alcohol non-residual, technical grade or better
• Methyl Ethyl Ketone (MEK)
• Acetone
• Methanol 95 %
• n-Heptane
• Ethyl Acetate
21
FTM9 ‘loop’ tack measurement
definition
The ‘loop’ tack value of a pressure sensitive material is
expressed as the force required to separate, at a specified
speed, a loop of material (adhesive outermost) which
has been brought into contact with a specified area of a
standard surface.
test equipment
A tensile tester or similar machine with reversing facility procedure
and a vertical jaw separation rate of 300mm per minute
with an accuracy of ± 2%. It should also have a capability Remove the backing
of measuring direct loads up to at least 20 Newton with an material from each strip
accuracy of ±2%. immediately prior to
the test being carried
A flat plate made of float glass or equivalent plate glass out. Hold the two ends
measuring 25 ± 0.5 mm x 30 ± 2.0 mm x minimum of the adhesive coated
thickness 3.0 mm. A metal peg is attached at the centre of facing material strip and
one face of the plate. The dimensions of the peg should be from the strip into a
such that the peg can be clamped in the lower jaw of the loop, adhesive surface
tensometer. outermost, by bringing
the two ends together.
Clamp the ends of the
test pieces loop for a distance of
10 mm into the top
These should be strips taken from a representative sample jaw of the ensile tester
of material. The strips should be 25 mm wide and have a leaving the loop hanging
minimum length of 175 mm in the machine direction. The vertically downwards.
cuts should be clean and straight. At least five strips should The sides of the jaw
be taken from each sample. should be protected from the adhesive coating.
FINAT TECHNICAL HANDBOOK 2014 |
Clamp the glass plate in the lower jaw with the longer axis
of the plate positioned at right angles to the long axis of
the strip. Start the machine and bring the loop into contact
with the glass plate at a speed of 300 mm per minute.
When full contact over the glass plate has been achieved
(25 mm x 25 mm) immediately reverse the direction of the
machine and allow separation to take place at a speed of
300 mm per minute. It is important that delay in reversing
direction is kept to an absolute minimum.
22
If the force exceeds the strength of a paper facing material,
the result quoted should be the maximum reached before
the paper tears and this result should be followed by the
postscript PT (paper tear)
notes
1. The rigidity of the sample affects the results and must
be considered when comparing different adhesives on
different facing materials.
2. The test plates must be thoroughly cleaned so that no
trace of adhesive, grease, silicone or moisture is left
on the surface. The following solvents can be used to
clean the test plates:
Record the maximum force necessary to completely 3. Conversion 1 kgf- = 9.81 Newton.
separate each loop from the glass plate.
Issued October 1985
Revised March 1999
results Revised May 2001
Added pictures January 20
‘Loop’ tack is expressed as the average value (ignoring the
initial peak) and range for the five strips tested in Newton.
23
FTM10
quality of silicone coated
substrates for self-adhesive
laminates: release force
test pieces
test equipment
The silicone coated substrate may be tested either against
A tensile tester or similar machine, capable of peeling a the standard tape or against a standard pressure sensitive
laminate through an angle of 180° at a jaw separation rate adhesive coated facing paper, the adhesive chosen being
of 300 mm per minute and with an accuracy of ± 2%. that which will simulate the end application for which the
release paper is intended.
Take a representative sample of the silicone coated
substrate of minimum dimensions 450 mm x 250 mm.
Apply to this, using light finger pressure, the adhesive tape
in strips along the machine direction. Alternatively apply a
suitable sized sheet of pressure sensitive adhesive coated
facing paper to the sample.
Cut test strips 25 mm wide and 175 mm in the machine
direction. The cuts should be clean and straight. Roll the
strips twice in each direction with the standard FINAT test
roller at a speed of approximately 10 mm per second. At
least six strips should be prepared from each sample if
subsequent adhesion tests are to be carried out. In the
case of samples showing very low release force, the width
(and hence the width of tape) may be 50 mm in order to
obtain a meaningful measurement. However, release force
should still be expressed as release force per 25 mm width.
test conditions
Place the strips under test between two flat metal or
glass plates and keep for 20 hours at 23°C ± 2°C under a
pressure of 6.86 kPa (70 g/cm2) to ensure good contact
between the silicone coated substrate and the adhesive.
FINAT TECHNICAL HANDBOOK 2014 |
24
procedure
Fix each strip in the machine so that the tape or facing
material can be stripped away from the silicone coated
substrate at an angle of peel of 180°. Set the machine to
operate at 300 mm per minute jaw separation rate. Carry
out the test taking at least five readings at 10 mm intervals
from the centre section of the test trip. Average the five or
more readings for each strip.
results
Release force is expressed as the average result for
the strips tested in Newton per 25 mm width either
under standard conditions or under accelerated ageing
conditions.
notes
1. The strips should be retained for subsequent adhesion
testing.
2. See FTM 11 for interpretation of results.
3. The adhesive tape or adhesive coated facing paper
used should be as stable to changes in temperature
as possible and of steady and reproducible adhesion
value.
4. Conversion 1 kgf- = 9.81 Newton.
FINAT TECHNICAL HANDBOOK 2014 |
25
FTM11
quality of silicone coated
substrates for self-adhesive laminates:
subsequent adhesion
definition
test conditions
Subsequent adhesion is defined as the force required, at a
specified angle and speed, to remove a pressure sensitive 23°C ± 2°C and 50% RH ± 5% RH.
adhesive coated material from a standard test plate after The test strips should be conditioned for not less than 4
it has previously been in contact with a silicone coated hours before testing.
substrate under specified conditions.
Percentage subsequent adhesion is expressed as the
percentage ratio of this result compared with the adhesion procedure
of similar material which has not been in contact with the
silicone coated substrate. Apply the test strips of adhesive coated tape or facing
paper from FTM 10, adhesive side down, on to a clean
test plate using light finger pressure. Roll twice in each
test equipment direction with the standard FINAT test roller at a speed
of approximately 10 mm per second to obtain intimate
A tensile tester or similar machine, capable of peeling a contact between the adhesive mass and the surface. After
laminate through an angle of 180° with a jaw separation applying the strip to the test plate leave for a period of 20
rate of 300mm per minute with an accuracy of ± 2%. minutes before testing. Prepare a second set of strips and
leave for a period of 24 hours before testing.
Test plates made of float glass or equivalent plate glass
(Kristallspiegelglas, verre glace). Fix the test plate and sample in the machine so that the
angle of peel is 180°. Set the machine at 300 mm per
A standard FINAT test roller. minute jaw separation rate. Carry out the test taking at
least five readings at 10 mm intervals from the centre
The test samples from FTM 10. section of each test strip.
Average the five or more readings for each strip.
A standard pressure sensitive tape, 25 mm wide, or a
standard pressure sensitive adhesive coated facing paper This procedure should then be repeated for the control set
(see Notes to FTM 10 and FTM 11). of tape or adhesive coated facing paper strips which have
not been in contact with the silicone coated substrate in
order to determine percentage subsequent adhesion.
FINAT TECHNICAL HANDBOOK 2014 |
27
FTM12 adhesive coat weight
28
low temperature adhesion
FTM13
scope test pieces
This test method allows a subjective assessment to be These should be cut from a representative sample of
made of the ability of a pressure sensitive material to material. The test piece should be 25 mm x 15 mm cut
adhere under low temperature conditions. with the machine direction parallel to the short edge.
29
FTM13 low temperature adhesion
results
For each surface average the score of the test pieces. To
obtain the overall score of the laminate average the score
per surface by the number of surfaces. For adhesives
designed for specific surfaces the results on those surfaces
should be quoted as well as the average (see notes 4 and 5).
notes
1. The test conditions listed in the method are only two
of many possibilities.
Other conditions that can be used are:
• apply the labels at -40°C, test at -40°C;
The labelled test surfaces should then be stored in the • apply the labels at ambient, test at 4°C, -25°C, -40°C;
test cabinets for the prescribed period. The recommended • apply the labels at ambient to moist test
periods are 1 hour and seven days though other time surfaces, test at 4°C, -25°C, -40°C;
periods are possible (see note 3). The time period used • apply the labels at -25°C,-40°C to icy surfaces,
should be reported with the results. test at -25°C, -40°C.
In all cases the test conditions chosen should reflect
After the test period, remove the test pieces from the test as closely as possible the final end use of
surfaces with the test surfaces remaining in the test cabinet the material. The chosen test conditions should be
and assess the adhesion. Removal of the test piece should recorded with the results.
start at one corner. If the label starts to tear removal should
be attempted from the opposite corner and continued even 2. The test surfaces listed in the method are
if the label tears again. recommended surfaces only. Each is subject to the
Rate the adhesion in the following manner: variations normal for commercial suppliers and the
test surfaces used should be representative of that
supplier’s product.
Rating Description
0 Label detached from the test surface. 6. Label constructions using plastic films such as PVC
1 Poor bond-no label tear. which may embrittle at low temperatures can give
2 Moderate bond - no label tear. high readings on this test but be unsuitable for the
3 Good bond - no label tear. final end use.
4 Very good bond - up to 50% of label surface left
on test plate after removal. Issued October 1985
5 Excellent bond greater than 50% of label surface Revised March 1999
left on test plate after removal Revised May 2001
30
dimensional stability
FTM14
scope procedure
This test method allows the user to assess the dimensional Remove the backing material and place the adhesive
stability of a pressure sensitive material when subjected coated facing material adhesive side down onto a clean
to specified test conditions. It is particularly relevant to test plate using light finger pressure and without stretching
synthetic film based materials such as Polyvinyl chloride the material. Roll twice in each direction with the rubber-
(PVC), Polyethylene, Polypropylene, Polyester etc. covered roller at a speed of approximately 10 mm per
second to obtain intimate contact between the adhesive
and the aluminium plate surface.
definition
This property is defined as the dimensional change of a
pressure sensitive material which has been applied to
a standard test plate under specified conditions when
subjected to elevated temperatures.
test equipment
An air circulating oven maintained at 70°C ± 2°C.
test pieces
These should be cut from a representative sample of
material min. 165 mm x 115 mm with the 165 mm edge
running parallel to the length-wise edge of the test
material.
Cut with a sharp knife, parallel to the sides of the test plate,
FINAT TECHNICAL HANDBOOK 2014 |
31
FTM14 dimensional stability
notes
Insert the test plate into the oven at 70°C ± 2°C for 1 week
after which it is removed and conditioned at 23°C ± 2°C for 1. The test conditions given can be varied to suit any
10 - 15 minutes to cool. particular application, whereby the conditioning time
and/or the exposure time and/or the substrate (e.g.
Measure the shrinkage in the crosscut to the nearest 0.05 glass) and/or the temperature of the oven can be
mm in both the length-wise direction and cross to the changed. This should be clearly stated alongside the
length-wise direction of the label. test results.
2. The quality finish and thickness of the aluminium used
should be recorded.
3. Dimensions of the recommended test plate (150 mm
x 100 mm x 0.6 mm gauge) are those of a panel of the
QUV Accelerated weathering tester.
4. Dimensional stability quoted as a percentage can be
misleading and should be avoided e.g. 0.2% on 150
mm dimension cannot be related to a one meter
dimension.
optional
FINAT TECHNICAL HANDBOOK 2014 |
32
surface tension of plastic films
FTM15
scope test condition
This method covers measurement of the surface tension 23°C ± 2°C and 50% RH ± 5% RH. The test sample should
of plastic film surfaces in contact with drops of specific preferably be conditioned for not less than four hours
test fluids. Surface tension (wettability) of plastic films is before testing, unless an immediate reading is required.
one of the properties used to judge surface characteristics
related to printability and adhesion of other coatings/
adhesives. Although the print key or adhesion property is test fluids
not dependent on the surface tension only, this method is
often used as a quick practical method. It is furthermore For polyethylene, polypropylene, polyester and/or similar
important to note that the determined wettability type of films, test fluids A, according to Table 1 are
characterises the immediate surface condition only, and prepared by mixing Formamide (surface tension = 58
that this condition can change during storage. mN/m and 2 ethoxyethanol (surface tension 30 mN/m).
These chemical raw materials may not be readily available.
In that case FINAT recommends the use of ready prepared
definition solutions as listed at the end of this test method.
Approximately 1 gram of a blue dye (e.g. Victoria blue or
The surface tension is measured by applying to the surface Methylene blue) is added to each litre of test fluid.
of the plastic film, a test fluid of known surface tension and For plastic films such as polyvinylchloride (PVC) which are
recording the time taken for the continuous film of the fluid affected (e.g. swelling) by the test fluids of series A, the test
to break into droplets. The surface tension is defined as fluids B shown in Table 2 are prepared by mixing methanol
that level when a continuous film of the test fluid remains (surface tension 23 mN/m) and distilled water, or water of
intact for 2 seconds. similar quality (surface tension 73 mN/m). Approximately 1
gram of a red soluble dye (e.g. Fuchsine) is added to each
litre of test fluid.
procedure
Lay the specimen on a smooth flat surface. Spread the
test fluid of known surface tension using a felt tip pen or
soft brush lightly over an area of approximately 200 mm x
10 mm of the test specimen. Note the time taken for the
continuous film of the fluid to break into droplets. Breaking
of the fluid into drops in less than two seconds, a lower
numbered test fluid should be tried.
Shrinkage of the liquid film on the sides of the applied fluid
does not necessarily indicate a lack of wetting. The aim is
to establish the lowest reading at an optimal dwell time of
Picture 1: example of test specimen staying as applied and two seconds.
breaking into droplets Extreme care must be taken to ensure that the film surface
is not touched or contaminated in the areas in which the
tests are to be made as this will influence the test results.
test equipment
results
FINAT TECHNICAL HANDBOOK 2014 |
33
FTM15 surface tension of plastic films
Surface tensions
1. Ready made test fluids of series A (see Table 1) can be 2-Ethoxyéthanol Formamide
of Test Fluids
obtained from: vol.% vol.%
Series A [mN/m]
56 13.7 86.3
be produced. With surface tension levels below 31
mN/m, print substrates are no longer printable with
standard printing inks at all, but will generally require These chemical raw materials may not be readily available.
special inks. The surface tension limit value (38 mN/m) is In that case FINAT recommends the use of ready prepared
correspondingly valid for other upgrading processes, such solutions as listed previously.
as varnishing, gluing, laminating and hot film embossing.
Issued April 1991
Revised March 2005
Addresses revised January 2014
34
chemical resistance - spot method
FTM16
definition results
Chemical resistance here is defined as the ability of the Colour change is assessed against the untreated control
pressure sensitive coated material to resist colour change either descriptively as nil, slight, moderate or severe attack,
when subjected to a chemical substance placed on its rate 0 to 5 (5 excellent resistance, 0 non resistant) or by
surface for 24 hours or 7 days at 23°C ± 2°C. determining colour fastness against the Blue Wool Scale 4
or Grey Wool Scale 3 standards.
35
FTM17
chemical resistance -
immersion method
definition procedure
Chemical resistance here is defined as the ability of the Remove the backing paper from each strip/sample and
pressure sensitive coated material to maintain its physical place the adhesive coated material, adhesive side down,
and adhesive characteristics after being completely onto a clean test plate using light finger pressure.
immersed in a chemical substance for 24 hours at Roll twice in each direction with the standard FINAT test
23°C ± 2°C. roller at a speed of approximately 10 mm per second, to
obtain intimate contact between the adhesive and the test
surface. Condition for 24 hours at 23°C ± 2°C.
test equipment
Carry out peel adhesion (180°) at 300 mm per minute (as
Test plates made of float glass or similar plate glass described in FTM 1) on a set of three strips.
(see Note).
Completely immerse the second set of test samples in the
A standard FINAT test roller. chemical substance for 24 hours at 23°C ±2°C (see note 1).
It may be necessary to cover the test container to prevent
Test chemical/large beaker. excess evaporation if a volatile chemical substance is used.
Metal rule.
test pieces
For subsequent testing against FTM 1, or assessing colour
change, strips should be taken from a representative
sample of material, which should be 25 mm wide and have
a minimum length of 175 mm in the machine direction.
The cuts should be clean and straight. At least two sets of
above strips should be taken from each material sample.
For measurement of dimensional change after chemical
immersion, a test piece of 10 cm x 10 cm is ideally required
cut with one edge running parallel to the lengthwise edge
of the product.
At the end of the test period, wash the test specimen
in a detergent solution to remove all residual chemical
test conditions substance and dry carefully employing an absorbent paper
or cloth. If the surface remains ‘wet’, indicating that the
23°C ± 2°C and 50% RH ± 5% RH. chemical substance still remains, an inert solvent such
as industrial alcohol or white spirits should be used to
The test substance or test strips should be conditioned for remove the chemical substance. Dry again carefully using
not less than four hours before testing. absorbent paper or cloth.
36
In all of the above tests, assess any colour change of the
material or permanence of legend if a printed substrate has
been employed, either as a general colour change or for
individual printing ink colours. Any other deterioration of
the test piece, e.g. blisters, should also be noted.
results
1. Peel Adhesion
An average is taken of the three strips prior to and
after immersion. Determine the percentage loss in
peel adhesion (180°) against the non-immersed
sample.
Chemical resistance (bond) can be expressed as
follows:
Loss Resistance
0 Excellent
5% Good
50% Moderate
75% Poor
100% Non-resistant
2. Colour Fastness
Colour change is assessed against the untreated
control either descriptively as nil, slight, moderate
or severe, rated 0 to 5 as above (5 excellent, 0 non
resistant) or by determining colour fastness against
the Blue Wool Scale 4 or Grey Wool Scale 3 standard.
3. Dimensional Stability
This is expressed as the increase or reduction in
millimetres (denoted ± or -) after immersion of each
sample against its original length.
notes
1. The temperature and time of immersion can be varied
and alternative test substrates other than float plate
glass may be used to suit any given application.
definition procedure
Dynamic shear is defined as the maximum force per unit
width required to remove the adhesive coated label stock
from a specified area in the direction parallel to the surface.
principle
A test piece is partly adhered to a test panel under
controlled pressure. A constant speed of deformation
is applied to the free end of the test piece in the length
direction of the test piece. The adhesive layer resists
this deformation. This resisting force grows during the
increased deformation of the adhesive, until the adhesive
cannot follow the deformation anymore and starts to fail.
The maximum force during the test is measured. Prior to testing, clean five test panels thoroughly with
n-heptane.
Slowly remove the backing from a test piece.
test equipment Gently place the test piece in the middle of the panel,
without applying pressure. The small edge of the test piece
An electronic tensile tester with capability of jaw separation shall be placed against the scribed line, at 12.7 mm from
with an accuracy of 1% or better. The movable grip should the edge of the panel as shown in the next picture:
be capable of being driven at a rate of 5.0 mm/min.
Cover the adhesive of the free part of the test piece with a
An accurate cutting device to cut test pieces conforming to strip of material. Do not use siliconised material, to prevent
the required dimensions. slip in the grips. Support the free part of the test piece with
Flat stainless steel panels of at least 50 mm x 50 mm, with an extra panel and roll down the test piece with the roller,
two scribed lines over the total width of the panel: one at twice in each direction with a speed of 10 mm/s, without
12.7 mm and one at 25 mm as indicated in figure 1. applying any additional pressure. An automatic rolling
device is strongly recommended.
Rubber covered steel roller as described in FTM 1;
Automatic rolling device is strongly recommended. Set the tensile tester to the following conditions:
• initial distance between the grips: 40 mm
Aluminium foil or polyester coated with a permanent • grip separation speed: 5 mm/min
(pressure sensitive) adhesive to eliminate elongation
effects in the front material of the sample. The After a dwell time of 20 ± 2 minutes, the test panel shall
overlaminating film to withstand 100 Newton. be placed in the fixed grip of the tensile tester. The bottom
FINAT TECHNICAL HANDBOOK 2014 |
38
position and tighten the free end of the test piece firmly notes
to prevent slipping. Start the tensile tester and wait until
panel and construction are completely separated. Record 1. The test plates must be thoroughly cleaned so that no
the maximum force during this test and the mode of failure trace of adhesive, grease, silicone or moisture is left
for each test piece individually. The codes for the failures on the surface. The following solvents can be used to
modes are listed below. clean the test plates:
39
FTM19
recycling compatibility of
self-adhesive labels
definition evaluation
Recycling compatible labels are paper labels whose As described in the assessment of the scorecard, self
adhesive does not interfere with the processing of adhesive laminate must reach a positive score in order to
recovered paper. The adhesive should preferably form large attain a satisfactory recyclability.
stickies which can be removed via screening process. The
particle size should exceed 2000 µm. Issued December 1995
Revised March 1999
Revised May 2001
Addresses revised February 2009
Revised June 2012
FINAT TECHNICAL HANDBOOK 2014 |
40
fluorescence and whiteness
FTM20
introduction B. Whiteness
Whiteness is the result of basic white colour of the material
Fluorescent substances in papers, inks and coatings and the effect of optical brightener added. The effect of
are used in labels for spotting and identifying particular optical brighteners can only be appreciated under a light
types of labels. Fluorescent brighteners impart increased source containing ultraviolet similar to daylight.
brightness or whiteness to label papers. Assessment of
whiteness requires a specified standard light spectrum 1. A set of twelve whiteness calibration plates was
including a defined range and intensity of ultraviolet available from CIBA-GEIGY.
radiation. Steps 1 to 4 do not contain any optical brightener but
have decreasing doses of yellow pigment. Steps 5 to
Fluorescence is the emission of light in the visible or 12 have increasing doses of optical brightener. CIBA
adjacent UV or IR spectrum, from matter that is suitably GEIGY no longer produces this set, but it is still used
energized by incident radiation. The whiteness of paper or as common standard.
textiles may be enhanced by the fluorescence of ‘optical Based on the same concept, LAETUS has developed
brighteners’ that convert the invisible UV component a ruler with a twelve step whiteness scale allowing
of daylight into visible light. The material thus appears visual assessment of the whiteness of a paper surface.
brighter and whiter. Again, the light used for such an assessment should
combine UV-light, otherwise no fluorescence will
The whiteness of an optically brightened paper depends occur. Comparative testing is also possible using the
on: analogue output (in milliamps) of a fluorescence
1. chemical structure of the optical brightener; testing device.
2. concentration of brightener;
3. the ‘activation potential’ of paper fibres in relation to 2. The best assessment of whiteness is obtained using
the brightener; a spectrophotometer that allows UV calibration of its
4. the UV component of incident light (this means that light source (normally standard source D65).
for correct measurement of whiteness a well- One such device is the Datacolor Elrepho 3000.
defined standard light source is required). White is in fact a colour like red, green or blue and
may be determined with colorimetric methods. The
difference is that white has high brightness and low
test methods saturation, which makes measurement more difficult
than for a high saturation colour. In the literature one
For inspection and control purposes test methods outlined finds over 100 whiteness formulas. The most practical
here concern (A) fluorescence and (B) whiteness. whiteness formula is the one developed by E. Ganz
(see appendix). Ganz ratings correlate with the CIBA
A. Fluorescence GEIGY scale as follows:
1. A surface printed with fluorescent inks or optical
brighteners is viewed under UV light which reveals GANZ rating CIBA-GEIGY scale
whether the print is as intended. -2 1
2. Actual measurement of fluorescence is possible with 5 2
equipment (as supplied by SICK or LAETUS) that emits 25 3
ultraviolet light of controlled intensity and measures 50 4
reflected light at longer wavelengths. A pre-set 70 5
threshold allows the equipment to decide whether the 90 6
printing is satisfactory or whether a label is present or 105 7
not. 130 8
FINAT TECHNICAL HANDBOOK 2014 |
150 9
175 10
185 11
210 12
41
FTM20 fluorescence and whiteness
42
ink adhesion - basic
FTM21
scope procedure
This method allows rapid assessment of the degree of
adhesion of a printing ink or lacquer to a filmic label stock. 1. Tape test
Lay the specimen on a smooth, flat, hard surface and
apply the adhesive tape, leaving a small part of the
definition tape unfixed to the test piece, ensuring that no air
bubbles are trapped under the tape.
The printing ink or lacquer is applied to the substrate and
cured on the printing press or using a standard method Using the FINAT roller, press down the tape by passing
appropriate for the type of ink. the roller twice in each direction over the specimen,
and then bend the unattached part of the tape back
The ink adhesion is then estimated by the amount of ink on itself at an angle of 180°.
that can be removed when adhesive tape is applied and
peeled off. Within 20 minutes after rolling down the tape, mount
the specimen in a frame or use one hand to hold
The resistance of the ink to mechanical removal is also the specimen firmly, then pull the free piece of tape
measured by scratching the ink and by deformation under towards you using the other hand: at first slowly under
pressure. constant speed, then very rapidly and accelerating.
(The faster speed is the more aggressive test).
Scratch test
test pieces Place the test piece against a firm, flat backing, and
rub a blunt metal implement (for example, a spatula)
If the required ink has not already been applied to the back and forth over the test piece until the ink starts
substrate as part of the printing process, prepare samples to be removed from the substrate. Record the number
for testing by coating the ink to a uniform thickness (for of rubs required to fail the sample, and compare this
example, with a Meyer bar for low-viscosity inks) and to standard samples to determine if the sample passes
curing the coating as recommended by the supplier. A-4 or fails.
sheets are a conveniently-sized sample for this test. Note: an instrument should be chosen which does not
cut the ink (a printer’s knife is not suitable) and which
is consistent between operators (a fingernail is not).
test condition
FINAT TECHNICAL HANDBOOK 2014 |
Rub test
23°C ± 2°C and 50% RH ± 5% RH. Place the test piece against a firm, flat backing, and
If practical, the test pieces should be conditioned for at press your thumb firmly onto the test piece and
least four hours prior to testing. twist it back and forth. Compare the test piece with
previously-assessed control samples to determine if
the piece has passed.
Note: it is recommended that appropriate Health
& Safety measures are taken in case the ink is
insufficiently cured.
43
FTM21 ink adhesion - basic
notes
1. The presence of waxes and silicones in some inks and
varnishes can result in poor adhesion between the
adhesive tape and the ink surface, and consequently
the tape is unable to separate ink from the substrate
even when the adhesion is poor, leading to a false
‘pass’ result. To address this risk, it is recommended
to adopt both a tape test and another method of
testing ink adhesion when evaluating unfamiliar inks.
44
ink adhesion - advanced
FTM22
scope test condition
This method allows rapid assessment of the degree of 23°C ± 2°C and 50% RH ± 5% RH.
adhesion of a printing ink or lacquer to a label stock. It is If practical, the test pieces should be conditioned for at
designed for the testing of digital print media. least four hours prior to testing.
definition procedure
The printing ink or lacquer is applied to the substrate and 1. Tape test
cured on the printing press or using a standard method Lay the specimen (30 mm by 175 mm) on a smooth, flat,
appropriate for the type of ink. hard surface and apply the adhesive tape, ensuring that no
The ink adhesion is then estimated by the amount of ink air bubbles are trapped under the tape.
that can be removed when adhesive tape is applied and Using the FINAT roller, press down the tape by passing the
peeled off. roller twice in each direction over the specimen, and then
bend the unattached part of the tape back on itself at an
angle of 180°.
test equipment Fix each strip in the machine, so that the tape can be
stripped away from the printed substrate at an angle of
A means of applying and curing the ink. peel of 180°. Set the machine to operate at 300 mm/min
jaw separation rate.
Adhesive tape of high peel adhesion (‘aggressive’), for
example tesa 7475 PV2 (acrylic based), tesa 7476 (rubber
based), tesa 4104 or 3M Scotch® 810 MagicTM tape. evaluation
A standard FINAT test roller. The peel value is expressed as the average result for the
strips tested in Newton per 25 mm. The peel force gives
A tensile tester or similar machine, capable of peeling a an indication of the force that has affected the ink and
laminate through an angle of 180° at a jaw separation rate an approximate measurement of the adhesion of an
of 300 mm per minute and with an accuracy of ± 2%. overlaminate to the ink. The colour is measured on the
printed substrate before and after removing the tape. The
Spectrophotometer, e.g. X-Rite DTP22, Datacolor Elrepho colour difference is expressed in ΔE.
3000, Hunterlab Ultrascan XE.
ΔE measurements can be rated as:
ΔE = 0 - 3 Excellent
test pieces ΔE = 3 - 5 Very good
ΔE = 5 - 10 Good
The ink is brought onto the substrate. After that, a certain ΔE = 10 - 15 Acceptable
period of time has to be taken into consideration, to make ΔE = 15 - 20 Poor
absolutely sure that the ink is completely hardened and/ ΔE = 20 - 25 Unacceptable
or dry. If the print system works with a one or more colour
system, is preferred that the adhesion of the pure colours
is evaluated, and not that of a combination of colours. remark
The adhesion of the ink can be evaluated by measuring This test is based on FTM 21.
FINAT TECHNICAL HANDBOOK 2014 |
scope procedure
This test method allows the converter to assess the Stain solution Preparation
degree and consistency of die strike and cutting during the If a pre-prepared stain solution is used (such as “Shirlastain
conversion process. A”), then no stain solution preparation is necessary and the
The method can be used during press make ready to solution can be directly used.
assess the condition and settings of cutters, to prevent For all other dyes a stain solution needs first to be
label dispensing failures or web breaks during high speed prepared. The following steps outline the procedure to
dispensing. The test is applicable to paper based liners. prepare a ‘typical’ stain solution where the concentration
level of dye is approximately 0.5 wt%.
test conditions
FINAT TECHNICAL HANDBOOK 2014 |
46
Retain samples indicating acceptable results in envelopes
to support traceability. Note that some dyes (such as
Malachite), may fade over time when exposed to a strong
light source. To avoid this, electronic scanning and storage
of the image may be used.
safety
It is strongly recommended to carefully read and follow
the Safe Handling instructions for the dye being used
(especially when handling the undiluted dye during
solution preparation). In addition, it is recommended to
always wear protective gloves , even when handling the
final dye solution.
Assess the die-strike pattern for intensity and consistency. Issued May 2001
Look at the reverse side of the liner for complete
penetration. There should be no signs of Dye penetration
FINAT TECHNICAL HANDBOOK 2014 |
47
FTM23 B die-strike on clear filmic liners
2. Remove all labels from the backing liner and note the
definition position of each label relative to the die-cutter.
The evaluation of backing damage or marking to the liner 3. Visually inspect the die-cut quality to check for any
that may be caused due to kiss cutting via a die. obvious, excessive damage. If an area of damage
is observed that causes concern, particularly in the
transverse direction, then a tensile test should be
background carried out on this area.
Label stock generally consists of face stock on a backing 4. Cut a strip of appropriate width and length for the
liner. Once the matrix has been stripped from the face tensometer test in use (jaw width and separation) to
stock the web integrity is maintained by the liner. If a include the area of damage. Take care not to introduce
misaligned die should cut into the liner excessively this any edge knicks that may cause unrelated failure by
could reduce the tensile strength of the web sufficiently using a sharp cutting tool.
to cause a web break. As such, damage in the transverse
direction (TD) across the web can be more of an issue than 5. Place each end of the liner strip into the respective
in the machine direction (MD) along the web. jaws of the tensometer & secure tightly.
6. Perform a tensile test according to the standard
When placed under increasing tension most filmic materials operating conditions for the instrument.
will show elastic behaviour up to the yield point, after
which they will deform irreversibly and eventually break.
In labelling applications the tensions used will generally results
not be above the yield point and so if the liner can be
tensioned to this point successfully without breakage then 1. Each strip should achieve a yield point prior to
any die-strike impressions should not cause a problem. snapping – this constitutes a pass.
2.
For some materials, for example polyester films such as 3. If the liner snaps prior to reaching the yield point then
polyethylene terephtalate (PET), the yield point can be this is a fail.
difficult to locate accurately. • If this is achieved on the cut from the die, then
In this case measurement of F5 (ensuring that the liner can note & advise that the die cutter should be
be loaded to 5% strain) can be used as a substitute target. adjusted accordingly.
• If the sample damage has not occurred on the
die-cut portion of the sample then repeat the
test equipment test, as the break may have been initiated by
edge damage when cutting into strips, or similar
Tensometer (e.g. Instron, Hounsfield, Lloyds, etc.); miscellaneous damage.
Cutting implement.
test conditions
FINAT TECHNICAL HANDBOOK 2014 |
48
note
Die-strike through filmic liners can be influenced by several
parameters. We recommend to carefully check them in
case of die-strike problems:
49
FTM24 mandrel hold
scope procedure
This test is used to determine the ability of a pressure Use new test materials for any new test.
sensitive adhesive to adhere to cylindrical curved surfaces. Clean the glass tubes/rods with acetone or other suitable
solvent (heptane) before using them, to avoid any deposit,
grease or dust. Other tubes/rods not made from glass
definition should be used such as supplied. Avoid to touch them with
fingers before any test.
Mandrel adhesion is defined as the edge lifting (expressed Remove the backing from the face material avoiding curling
in mm) of pressure sensitive adhesive coated material of the face material, and touching the adhesive surface.
from standard cylindrical rod / tubes of small diameter, Apply the sample around the tube/rod with the long side of
after being applied with light finger pressure for a specified the sample perpendicular to the axis of the rod/tube.
amount of time.
test equipment
Rack to support tubes/rods without having contact
between test samples and supporting rack.
test conditions
Test pieces should be conditioned at 23°C ± 2°C and
50% ± 5% RH during at least 16 hours before being cut.
Other conditions might be used, but this must be clearly
reported.
50
Failure Description Code
CF Cohesive Failure - the adhesive film is split during
the test, leaving residueof adhesive on both the
panel and the front material.
AF Adhesive Failure - the adhesive separates cleanly
from the front material, leaving adhesive film on
the test sample.
AT Adhesive Transfer - the adhesive separates cleanly
from the front material, leaving adhesive film on
the test panel.
The approximate extent of transfer should be
quoted as percentage
results
Report identification of the samples and test tubes/rods
materials.
Calculate and report the mean value of the 3 tests for the
edge lift measurement described above for each sample/
testing material, and the time evolved since application of
the face material.
Describe the type of failure (AF, CF, AT).
FINAT TECHNICAL HANDBOOK 2014 |
51
FTM25
evaluation of the silicone
coverage of coated papers by use
of a water based stain test
test condition
FINAT TECHNICAL HANDBOOK 2014 |
52
procedure results
53
FTM25
evaluation of the silicone
coverage of coated papers by use
of a water based stain test
Whilst Shirlastain is a commonly used stain material 2. In all cases the hydrophobicity of the base paper
there are occasions where other materials are more should be taken into account and a test of the base
suitable (either due to toxicity constraints or from paper with the stain solution must show a deep
coloration of the base paper) coloration. In the case of some hydrophobic papers
where penetration of the liquid stain is much lower
Alternative stain solutions a moderate silicone coverage can give a perfect stain
Malachite green – typically 0.5% solution left in and in such cases the test may need to be adapted
contact for 1 minute (for example longer time in contact with stain solution
Grade - Malachite Green Oxalate (Basic green 4) or increased solution concentration).
Supplied as crystals for dilution in water; C.I. Number N.B. Care must be taken in interpretation of
- C.I.42000 phenomena mentioned in notes 1 & 2 as obviously
For yellow coloured papers it can be more suitable the heat treatment recommended in note 1 could lead
than Shirlastain. also to the phenomenon mentioned in note 2.
Neocarmine A – typical 1 minute exposure of 3. Larger areas of silicone coated release liner can be
prepared dye solution. This dye tends to show up evaluated by preparing a solution of dye in a large
faults in the coating as red spots. For yellow coloured shallow dish and then bringing the silicone surface of
papers it can be more suitable than Shirlastain. the liner into contact with the solution. Care should
be taken to avoid entrapment of air bubbles under the
Methylene Blue – typically 0.5% solution, 2 minute silicone surface or through foam on the surface of the
exposure time. dye solution.
Crystalline Violet - typically 0.5% solution, 2 minute 4. For films or polycoated kraft substrates a “powder
exposure time. dye test” is used to reveal faults in the silicone
coated surface. Whilst this method can not show the
differences in coating quality as well as the solution
notes based dyes used on papers it is useful to give an
overall picture of coating continuity, highlighting
1. It must be noted that a paper coated with a poorly miscoats, marks or streaks. A dry powder dye is lightly
cured silicone can absorb dye stain and provide false applied to the surface and carefully spread over the
results. For paper substrates, another sheet of coated area to be tested. The fine powder has a tendency to
substrate, ideally taken from an adjacent position to cling to the silicone coating and not the uncoated film
the first sample, can be re-heated in a laboratory oven or poly coating.
for two minutes at 120ºC for example. Of specific interest is the uniformity of colour which
After the sample has been allowed to cool back results after the dye stain is removed. For the powder
to room temperature, the dye stain test can be test on films or polycoated kraft substrates, light
performed. If there is no significant difference in the coloured areas are indicative of poor coverage (or
uniformity of the colour between the samples, it can conversely, a uniform dark colour is indicative of good
be assumed that the initial sample was “well-cured.” coverage) with the Waxoline violet powder dye.
If there is a significant difference, the state of cure of
the initial sample of coated liner is in question. Nigrosin dye for powder dye coverage test
This heat treatment works fine for thermally cured Grade Nigrosin, Alcohol soluble (Solvent black 5)
silicones; free radical curing silicone acrylates have Supplied as very fine powder for direct use as solid
their final properties immediately after exposure to C.I. Number C.I.50415
UV light or electron beam. The cationic curing silicone
FINAT TECHNICAL HANDBOOK 2014 |
epoxies need some time for a post curing process. Other dyes for powder test
Thermal treatment can accelerate this natural process • Waxoline blue, green & violet
for this type of radiation curing silicones. • Dark coloured “eye shadow”
• Any other fine powdered dye/pigment which
clings to silicone surface
54
wash-off paper and film labels
FTM26
scope procedure
This test procedure describes the preparations and testing
of pressure-sensitive adhesives, which can be washed off
with aqueous alkaline solution.
definition
“Wash-off ability” is the ability of an adhesive to detach
itself quickly and completely in a 1.0-2.0% solution of
sodium hydroxide at 65 - 75°C.
The content of NaOH and the wash-off temperature has to
be noted in the report.
test equipment
Heatable magnetic stirrer.
Magnetic stirring bar. After storage, fill the bottles with water at the testing
2 - 5 litre glass beaker. temperature and immediately immerse the bottle in the
Thermometer. prepared solution of sodium hydroxide at the testing
Glass bottles (glass bottle type and the pre-treatment of temperature.
the glass surface, such as specific coatings, washings, etc.
have to be mentioned in the report).
results
preparation Indicate the time in seconds until the labels become
detached.
Label and adhesive should be adapted for wash-off
purpose. Report where you find the adhesive after the label has
The label material can be paper or filmic. detached:
Cut out labels with the dimensions 60 x 80 mm from the • On the bottle
finished coating. • On the label
Prior to testing, clean the glass bottles in a dishwasher at • Both on the label and the bottle
min. 65°C.
The use of an alkaline cleaner is recommended.
note
Most of the glass bottles are recycled or re-used bottles.
The life / cycling time of the glass bottle may influence the The type of face stock material, paper or filmic, its
test results. It is recommended to use new bottles after properties and condition such as porous, non porous, semi
FINAT TECHNICAL HANDBOOK 2014 |
the first washing. In any case, the state of the glass bottle permeable, etc, influence the “wash-off ability” significantly.
should be mentioned in the report. Furthermore, printing coverage, especially UV-varnish,
affects the wash-off times. It is recommended to perform
trials with printed labels. Additionally, ageing of the labeled
test pieces glass bottles e.g. outdoor storage, UV-light or humidity may
affect also the wash-off result. Deviations from the testing
Prior to testing, remove the silicone release backing from method have to be mentioned in the report.
the label and stick the label onto the glass bottle. Store
the bond for at least 24 hours under standard climate Issued October 2008
conditions: 23°C ± 2°C, 50% RH ± 5% RH Revised January 2014
55
FTM27
ink rub test for uv printed
labels ink surface against
substrate or ink surface
scope conditions
This test method is suitable for checking out rub resistance Condition should be at 23° ±-2°C / 70 - 77°F ±- ;
of printed UV ink: ink surface against substrate or ink 50% RH ±- 5% RH.
surface against ink surface.
Bad adhesion cannot be detected with this method as long
as scratch or rub resistance is good. The specific resistances preparation and procedure
must be elicited with different methods, e.g. FTM 21. In
difficult cases bad adherence and bad rub resistance can 1. Remove one label from the master reel sample.
occur together. 2. Cut of a short piece of blank substrate from the reel
in the size of the rubber bed on the right hand side of
This test procedure can be handled by lab personnel of a the Ink Rub Tester.
printing factory or a pressman / production manager who 3. Adhere blank substrate to the rubber bed on the right
is instructed to the Ink Rub Tester equipment. hand side of the Ink Rub Tester and adhere the printed
label to the rubber of the 2 lbs* weight. It is important
that the sample on the 2 lbs weight is covered with
definition ink all over the test area.
4. Place the 2 lbs weight completely with label onto the
Normally rub resistance is a question of through curing retaining clip. Both printed label and substrate should
or reactivity of an ink film. Rubbing off or scratching off be facing each other ink side to substrate surface.
describes the damage of an ink surface by mechanical 5. Set up the machine to 100 moves per minute
influence, e.g. two labelled bottles rubbing against each 6. Set the machine to 25 cycles and press start
other during transport. 7. At the end of the cycles, observe the labels for ink rub
Scratch or rub resistance describes the mechanical of or scratch of.
resistance of an ink or varnish surface. 8. If ink rub of or scratch of is present, repeat the test
after the following improvement trials using fresh
printed labels for every trial:
test equipment • decrease printing speed or
• add suitable photo initiator to the UV ink if
Ink Rub Tester by Testing Machines Inc. available
www.testingmachines.com • choose an anilox roll with less volume as long as
colour shade is still sufficient or
Heating cabinet. • add 5% of blending varnish as long as colour
shade is still sufficient
• replace UV bulb
• clean up UV lamp reflector
56
results remark
To give an impression of good and bad test results please For sure the ink surface will be scratched by this test
look at the following pictures. method also if there is a proper curing (Level 1). But it
should not be scratched of (please view picture 3)! Level 1
is always that one to be achieved.
Depending on the substrate quality also this can be
scratched by this test method (please view picture 4).
If the ink should be peeled of by this test than ink adhesion
is an issue together with poor reactivity (picture 5).
silicone in inks
If inks consist of silicone this migrates to the surface and
Picture 3: Slightly scratched ink surface: sufficient result works like a lubrication. Then a rub resistance test can
end in a “faked” good result. Silicone residues should be
carefully wiped of with a 70% isopropyl alcohol before
starting this test.
note
This test is to be repeated with ink side to ink side if
required. Then also the sample on the rubber bed should
have an ink coverage all over the test area.
If wet rub resistance shall be checked repeat the test with
Picture 4: Substrate in comparison: surface is scratched a drop of water applied onto the sample mounted on the
rubber bed on the right hand side of the Ink Rub Tester.
combination printing
In cases of combining water born inks with a UV Flexo
overprint varnish it is reasonable to set up the test as a
wet rub resistance test. Then beside damage of the varnish
surface ink bleeding can be the indicator for bad curing of
the overprint varnish. If ink bleeding occurs not only the
curing of the overprint varnish might be insufficient but also
Picture 5: Bad rub resistance caused by bad ink reactivity or through the curing/drying of the waterborne ink. Then the curing of
curing. Ink can be scratched and rubbed easily. ink and varnish should be checked individually.
Level 2: Scratched of ink film or rubbed of ink film, • L abels und substrate as described on page two in
< 10% substrate visible chapter “test pieces”
Level 3: Scratched of ink film or rubbed of ink film,
10 - 30% substrate visible * 1 lb = 453.6 g
Level 4: Scratched of ink film or rubbed of ink film, Issued October 2008
30 - 60% substrate visible
Level 5: Scratched of ink film or rubbed of ink film,
> 60% substrate visible
57
FTM28 evaluation of bleeding through paper
scope procedure
This procedure describes the spectrometric assessment Ageing:
of the migration of a label adhesive through the paper • Place the strip (sample B) to be tested in oven, by
substrate at elevated temperature. piling up the strips of samples on top of the other with
polyester films between the samples.
• Do the same for sample C.
test equipment • Take the samples out of the oven after 2 weeks ageing.
Allow to cool to room temperature.
Ventilated ovens.
Testing:
Paper cutter. Differences between aged samples (B) and references
(A and C) can be observed either visually or measured with
Substrate: Label paper, release liner as appropriate, and a spectrophotometer.
polyester film.
1 - Visual comparison:
Reflectance Spectrophotometer Example: Hunterlab
Ultrascan XE. The aged samples are compared to reference A, to detect
any bleed through.
The samples are either ranked on bleed through
test pieces characteristics or on their non acceptance if any bleeding
occurs.
These should be strips from representative samples of label
material. (e.g. of the 3 layers: label paper, adhesive and 2 - Use of a spectrophotometer
release paper)
Reference sample:
For each sample being evaluated, and for each temperature
at which the test will be done, prepare 3 strips of samples • Place the center of sample A or C at the reflectance
of about 5 cm x 20 cm, cut in the machine coated direction. port, with the label paper facing the transmittance port.
• Set the spectrophotometer as follows:
Prepare following samples: • Scale: CIELAB
• Illuminant: C
Sample A: label laminate • Observer: 2°
(face paper ± adhesive ±release paper) • Area view: Large
Sample B: label laminate • Selected Indices: WI E313-98
Sample C: non coated face paper
• Measure whiteness index (according to ASTM E 313) in
the middle of each of the three samples which have
test conditions been prepared.
notes
Detailed information on how to use the Hunterlab
Ultrascan XE spectrophotometer are provided in the
Hunterlab operating manual.
http://www.hunterlab.com/manuals/appendixa2_5.pdf
59
FTM29
scratch resistance of an uv ink
film on different print materials
scope
This test method describes how to test the scratch resistance
of a UV ink film applied to different printed surfaces.
For this test to give reliable results it is important that the
ink has been cured to a sufficient level, and this can be
checked in advance using FTM. 2, or as a quick check a
thumb smear test can be used.
The tip of the Scleromteter consists of a tool with a 0,75 Preparation of Sclerometer
mm (0,03“) diameter tungsten carbide tip. This is moved Loosen the knurled screw and slide of the collar off the
over the specimen with different preset spring force. Sclerometer. Select the appropriate spring and insert into
the Sclerometer. Always choose the natural sprint as the
weakest to begin. Refit the collar. Find the scale on the
FINAT TECHNICAL HANDBOOK 2014 |
Procedure
1. Place the Sclerometer perpendicular to the surface
being tested and apply sufficient downwards force to
compress the spring by approx. 2 mm. Do not allow
the bottom of the Sclerometer (other than the tip), to
Picture 1: Elcometer 3092 Sclerometer Hardness Tester touch the surface being tested.
60
2. Move the Sclerometer to produce a linear scratch of Level 3: Ink film is scratched off; surface of printing
approximately 20 mm in length material is visible
3. Inspect the tested surface of the sample for any sign
of damage.
remarks
If the ink surface is not damaged set the spring
compression to the next required force position and repeat There will nearly always be some slight distortion of the
steps 1 – 3. ink surface depending on the selected spring force, even if
the curing of the ink is excellent (level 1 on the scale), but
Once a scratch becomes visible it should be examined the ink film should not be so scratched that the printing
using a magnifying glass, to determine whether there has material surface becomes visible (see image 3 on page 4).
only been a deformation on the ink surface or whether The target should always be to achieve a “Level 1” result.
the ink has been scratched away from the surface. If it
is confirmed that the ink has been scratched from the The wide range of printing materials and printing inks
surface then it is important to identify whether it is only available in the market means that it is not possible to
the upper layers of ink that have been removed (indicating specify a single spring force that can be applied for all
cohesive failure within the ink), or whether the ink has testing. This has to be evaluated for each print sample
been removed down to the printing material. Both the individually. The target should be to identify the highest
level of curing of the ink and the spring force used for possible spring force at which a “level 1” result can still be
the Sclerometer will have an impact on this result. This achieved for that print material and then use this is as a
investigation is important to create comparable test results. minimum for the final printed product using that material.
Picture 3: Distorted ink surface alongside scratched ink surface silicone and wax in printing inks
Silicone and waxes inside the ink intend to migrate to
the surface after curing. Waxes also have the function of
increasing scratch resistance. These migratory materials
can be pushed aside with increasing spring force, but these
inks can still be tested by this method.
combination printing
FINAT TECHNICAL HANDBOOK 2014 |
Picture 4: Substrate in comparison: the surface is distorted above Where ink is applied in several layers using different
the blue line printing techniques on the same line, it is important to
measure each ink layer separately directly on the printing
The scratch appearance as described in the “procedure” material. This does not mean however that overprinting ink
leads to the following rating scale: layers are not also tested, as it is important to understand
adhesion between different ink layers. This is especially the
Level 1: distorted surface; no ink scratched off; only case if printed using different print processes. The skilled
the ink surface distorted knowledge of the ink supplier is then important.
Level 2: Scratched ink surface; ink has been removed
from surface but surface of printing material is not visible Issued September 2013
61
It is important that a join in a self-adhesive laminate should be
made in such a way that it will minimize problems
joinswhen
2.1
recommended in
converted into roll labels. The join should
self be angled
-adhesive so that the
laminates
feed-in is gradual, the width of facing tapelabels
and backing tape
SECTION for roll
should differ so that there is not too great a step in increased
thickness and the total thickness of the join should be kept to a
minimum in order to avoid damage to or misplacement of the
cutters.
conversion
The following specification is recommended:
a) The angle of the join should be 10° - 30° from the cross
It is important that a join in a self-adhesive laminate should be
made in suchdirection.
a way that it will minimize problems when
converted into roll labels. The join should be angled so that
b.
a smaller tape, at least < 20 mm.
The width of tape on the facing paper should be at
least > 30 mm.
e) The tapes should have a thickness of no more than
c.
0.063mm inclusive of adhesive.
The width of tape on the backing paper should be
g. Where applicable the tapes should withstand the
broader than the tape of the face material > 36 mm.
temperatures involved in label printing processes.
tape for ease of identification but the tape on the Revised faceOctober 2008
should be a smaller tape, at least < 20 mm. Revised March 1999
e. material
The tapes should have can either
a thickness bethan
of no more a colored tape for a similar reason, or
a white printable tape for use with laminates which are to be
0.063 mm inclusive of adhesive.
f. converted
The tape to paper
used on the backing security
should beor
a sequentially numbered labels, i.e.
coloredwhen alloflabels
tape for ease must
identification but thebe
tape accounted
on for.
the face material can either be a colored tape for a
similar reason, or a white printable tape for use with
g) Where applicable the tapes should withstand the
laminates which are to be converted to security or
temperatures involved in label printing processes.
sequentially numbered labels, i.e. when all labels must
be accounted for.
Tape
Adhesive
Adhesive
Tape
Silicone
Adhesive
Backing paper
Tape
62
processing recommendations
SECTION 2.2
roll stock
1. Generally, self-adhesive paper roll stock can be 10. With UV cured inks, always check the cure before
considered as normal paper with respect to ink choice proceeding. Checks should be made at regular
etc. synthetics, filmic and foil roll stock, however often intervals on UV output of the lamps . It is advisable to
need special materials involving consultation with ink keep the web temperature on re-wind under 24°C.
suppliers.
11. It is advisable to use an antistatic bar at the point
2. Corona treatment is required for filmic face stock of matrix de-lamination for easy matrix removal
to enhance the ink adhesion. When the substrate by neutralizing the generated static charge by de-
is corona pre-treated, it is advisable to refresh the lamination. This prevents matrix break.
corona treatment on press.
12. Avoid excessive tension in reels of finished labels. This
3. Chemically top coated filmic face stock substrates will prevent bleeding and label shifting.
should not be corona treated on press without prior
contact with the supplier. 13. Wind finished labels on to cores of an appropriate size.
Large labels should not be wound on to small cores. It
4. Always check with the Supplier if his material is therefore advisable to use 6” core instead of 3” core
can withstand the intended process conditions, to prevent the label curling.
particularly if excessive temperatures or unusual web
feed patterns are involved. 14. Finished work should be shrouded in polythene prior
to packing.
5. Do not change the winding direction of the roll prior to
conversion, as this will alter the release properties and 15. Wherever possible, the manufacturer’s batch/order
could affect curl problems. references should be retained in case of complaints.
6. Always use the correct die for the product. Therefore 16. To take dust out of the roll stock it is advisable to use
it is advisable to mention to die manufacturer the type a web cleaner on un-wind section.
of face stock substrate.
17. To reduce the static electricity mainly from the filmic
7. Labels should be designed with matrix stripping in roll stock it is advisable to use antistatic devices
mind. Refer to the supplier if complex shapes are between the printing units and before web rewinding.
involved. Wherever possible, use round corners for
labels and avoid narrow matrices. Revised May 2001
Revised October 2008
8. Check the depth of die-cutting before proceeding with
any lengthy run.
Excessive die pressure will cause weakening of
the backing paper / liner and should be avoided
in products intended for high speed automatic
application. Check also the dimensional size of the
label because on filmic you can have a retraction
of the material generally on wide press or during
FINAT TECHNICAL HANDBOOK 2014 |
processing.
63
SECTION 2.2 processing recommendations
1. Check that the ink is compatible with the product to 1. Self-Adhesive paper sheet stock can be considered
be used and is approved or recommended by the ink as normal paper with respect to ink type, dryers,
supplier. retarders, etc.
2. Allow sufficient unprinted edge trim on the screen to 2. When using self-adhesive sheet stock in offset litho
prevent edge lift due to shrinkage. printing, however the following points should be
noted:
3. Avoid excessive amounts of thinners or retarders to
prevent shrinkage. a) Reset the impression nip between the
blanket and plate cylinder to allow for the extra
4. Ensure that all machinery in the vicinity of solvent thickness. This will reduce problems of tail edge
fumes is fitted with anti-static devices and solvent creasing, misregister etc.
extractors where possible. b) The double sheet trip should always be used to
prevent any damage to plates, etc.
5. Use a minimum of heat to dry the ink in order to avoid c) Always use minimum of damping to prevent
sheet curl. edge waving, etc.
d) To prevent edge curl, always shroud sheets in
6. When using a jet drier for multi-colour runs, shroud polyethylene between colors if multi-colour
the sheets in polythene between runs to prevent machines are not being used.
sheet curl.
3. Finished work should be shrouded in polyethylene
7. When rack drying, avoid changes in temperature or until cut and boxed.
humidity between runs to prevent sheet curl.
4. The Manufacturer’s recommendations on guillotining
8. Always allow sufficient time between passes for each and slitting should be used.
colour to dry. This is of particular importance in the
case of flood coating. 5. Wherever possible, retain the Manufacturer’s batch/
order references in case of complaint.
9. Print successive close-register colors as soon as
possible after each other. Printing separate colors Issued May 1987
under different atmospheric conditions will cause
difficulties with register.
64
surfaces requiring caution
SECTION 2.3
Caution should be exercised when labeling surfaces listed Ageing
below. In many cases products are available which will Surfaces where adhesive may be significantly exposed
overcome the problems of application and you are strongly over time to severe environmental conditions resulting
recommended to contact your material supplier. in eventual breakdown and failure of the adhesive, e.g.
drum labeling, exposure to salt water, and or high levels of
surfaces where damage can be caused by application or sunlight.
removal of self-adhesive products
Weaker bonded surface finishes e.g. (plasticized/soft) Applications where specific advice should be sought
PVC, flock coated fabric, acrylic vehicle paint, paper, card. Direct food labeling, toy labeling, any medical or
Animal skins and natural fibres, e.g. suede, leather wool. pharmaceutical applications, e.g. direct skin contact,
Tarnishable metal surfaces, e.g. copper, brass, silver. blood bags, phials, items requiring sterilization processes.
Some coated glass surfaces e.g. self cleaning, and optical Apparel and fabric labeling, leather, luxury goods, extreme
lenses. environment exposures e.g. temperatures 80°C or -20°C,
direct/continuous exposure to sunlight, UV, seawater or
Surfaces to which it is difficult to obtain satisfactory chemicals.
adhesion
Low energy surfaces where ‘wetting’ is difficult e.g. See also Section 2.6 Qualitative Adhesion testing
PT.F.E., untreated polyolefins, silicone treated or
contaminated surfaces, surfaces chemically treated for Issued March 1987
corrosion resistance, waxed surfaces, printed polyethylene Revised May 2001
(polyamide inks), greasy surfaces. Surface energy changes Revised October 2008
due to migration or loss of effectiveness of pre-treatment.
65
safety guide for users of
storage fire
Normal storage principles should be applied when storing The laminates will burn in the event of contact with a
and stacking laminate rolls. See also section 2.5. flame, smoky fumes being given off by the adhesive itself.
Materials involved are generally flammable and therefore Fires may be extinguished with water provided that live
should be stored away from all sources of heat and electrical equipment is not in the vicinity. Otherwise
ignition. powder or C02 should be used. The advice of your Fire
Officer should be initially sought having regard for the
Consideration should be given to listing types of material layout of your premises and the particular operations
stored to assist the Fire Brigade in the event of fire. involved. The following extra precautions are applicable to
the products stated.
usage 1. Films
Plastic films pass through a melt stage and will
1. Handling therefore drip before burning - this may cause severe
Safe methods of roll and pallet handling should be burns if skin contact is made. In the event of a fire,
applied. During un-banding pallets, care should be the use of self contained breathing apparatus is
exercised to avoid whiplash when banding is cut – recommended during fire-fighting.
eye protection and gloves are recommended. It is
important to remember that the outside wrappers, or 2. PVC (vinyl)
laps, of a roll are for protection only and should not During combustion, hydrochloric acid gas is evolved,
be relied upon to support the roll if excessive stresses as well as dense smoke and other acrid fumes which
are applied. Ideally, lifting and movement should be can have a corrosive and irritant effect. Self contained
conducted in a safe horizontal manner using centre positive-air breathing equipment should be readily
core support where possible. available for fire fighting and rescue work.
Operators should be forewarned that self-adhesive
laminate rolls show a greater tendency to
telescope than rolls of plain paper and therefore health and safety
greater care should be exercised.
Under normal conditions of handling, no hazards are
2. Conversion anticipated, but good industrial hygiene should always
Care should be taken to avoid cuts from exposed be observed. For specialized applications e.g. food, toy
paper or laminate edges during handling. During or surgical labeling, advice should be sought from the
the conversion of pressure sensitive laminates static individual supplier.
build-up may occur. Therefore, conversion equipment
should be adequately earthed. In situations where
highly flammable solvents or inks are being used,
specialist recommendations on static elimination may
be necessary.
FINAT TECHNICAL HANDBOOK 2014 |
66
waste disposal
Waste laminate is usually classified in most countries as
“non-hazardous” but local and national regulations must
be examined and complied with.
FINAT Solutions
While research and development efforts continue towards
material recycling solutions, FINAT has arranged a disposal
system for release liners in a number of countries.
other information
67
2.5
handling and storage of
label stock throughout
Store in a cool and dry place. Wrap in polythene and pack flat in boxes or on pallets to
Ideal storage conditions are 20-25°C and 40-50% RH. give protection during transport and further handling.
Store finished coils on end (vertical storage), ideally use Take care, if banding, to avoid pressure marking.
two-side silicone release coated interleaving sheets
between the coils. Issued April 1987
Wrap in polythene and pack in boxes or on pallets to give Revised March 1999
protection during transport and further Revised October 2008
handling.
68
qualitative adhesion testing
SECTION 2.6
recommended adhesion test surfaces to be labeled
1. Cut out several labels, same size and in the same 1. Surfaces may not be what they appear to be. For
machine direction as the proposed printed label. example glass may have a protective coating or
antiscuff agent on the surface. There is no substitute
2. Peel off backing and apply to object to be labelled in for a test carried out on the actual object to be
the same position as the eventual requirement. Rub labeled.
down lightly with fingers or a rubber pad.
2. Test for adhesion under conditions which are as close
3. Ideally, prepare several samples and place one in a dry as possible to the end application. This should take
atmosphere and one in high humidity or other specific into consideration temperature and humidity.
conditions simulating potential end applications.
3. Do not carry out the test on a flat, empty plastic bag
4. Leave for 24 hours minimum before assessment of when the end user is labeling one filled with product.
adhesion.
4. Check whether the label is to be applied to a plain or a
printed part of the pack.
69
SECTION 2.7 adhesives
Pressure sensitive adhesives were first developed in the mid nineteenth century for self-adhesive bandages. However, it
was only ninety years later that the idea was used to make self-adhesive labels.
At that time the adhesive used was made from natural rubber and applied by coating from a solvent solution. Today
solvents are not very popular any more, and alternative self-adhesive materials are available. Acrylic adhesives which are
also available as water-based emulsions, have excellent ageing properties. They are easy to coat and clearly eliminate the
hazards linked with solvent coating.
Hot melt adhesives can be coated at very high coating weights, because there is no drying or curing process involved.
Due to modern coating and drying technology both types of adhesives are able to be applied at high machine speeds.
• Wash-off
• Recycling friendly • Other
An adhesive which is designed to be less harmful to
paper recycling; already used in N.A. for self-adhesive 4. Additional significant properties, e.g. “direct food
stamps these adhesives support the trend of trouble contact according to FDA 175.125”
free recycling of self-adhesive materials. or for pharmaceutical purposes.
70
unwind roll chart
SECTION 2.8
indicate unwind direction by number as follows
Extract from TLMI Manual of Recommended Standards (where the chart has 16 positions).
71
2.9
recommendations
regarding static electricity
SECTION
72
problems and elimination neutralize each other or be dissipated to earth. However
with the presence of a nearby static charged surface an
of static electricity ion will be attracted to an opposite charge on the surface
of the substrate and the surface will be completely
Problems neutralized.
Static charges result in electrostatic attraction to the
substrate surface, of dirt and airborne particles present
around the press and converting machines. Web speeds measuring the static charge
complicate this process, because the faster the web speed
the higher the static charge level. This problem affects all There is a variety of measuring instruments for static
printers and converters, especially when converting filmic electricity available in the market.
substrates. In the label printing industry dust attraction Some instruments are calibrated to measure the field at
decreases the print quality. a given distance. The surface voltage and the polarity are
then displayed on the screen. Other instruments indicate
Material misbehavior is another type of electrostatic the electrical field strength in kV/m. To calculate the surface
attraction. This can be noticed on a sheeter, stacker, voltage, the reading has to be multiplied by the distance
conveyer, where the sheets would stick to themselves or between instrument and surface.
will be misrouted or repelled each other on the equipment,
Elimination glossary
The basic principle for neutralization of static charges is
the same whatever the technique used: one should re- Coulomb: The unit of measure of electrical charges.
establish the electrical neutrality of the surface by adding (Symbol : C)
or removing the electrons which create the imbalance of
the surface charge. As previously mentioned the moisture Electron: A small atomic particle with a negative
in the press room has an impact on static charge, therefore charge (1.6x10ˉ19 coulombs).
it makes sense to control the moisture. We suggest to
maintain the relative humidity at 50-65% and the room Ion: A molecule or atom with an electrical
temperature at about 22-24°C. imbalance (a negative ion has an excess of
electrons, a positive ion has a deficit
Passive ionisation of electrons)
Carbon or stainless steel fibre earthed brushes placed
closely over the surface of the web of a press or a Resistance: The higher the resistance of a material,
converting machine will leach away the static charges the harder it is for a charge to flow through
down to earth. Passive eliminators are thus useful for it. Insulators e.g. all polymeric substances
reducing very high level of static charges, say tens of kV’s (plastics) are very resistive.
down to medium high levels of a few kV’s. However by
their very nature, they are not able to completely neutralize Unit: Ohm (Ω)
the surface electricity, therefore residual charges remains
on the substrate surface. Capacitance: A measure of the ability of a substrate to
hold the charge. Unit: farad (F)
Active ionisation
By using high voltage AC or DC bars over the web of a Issued October 2008
press or converting machine, ionized air can be produced
FINAT TECHNICAL HANDBOOK 2014 |
73
2.10
advices about light fastness of
printing inks and light exposition
SECTION
• In the case of mixed inks the ink with the lowest light
fastness is decisive because it governs the earliest time
of fade-out.
• M
ixed inks are frequently mixed in very different ratios.
As a result of the mixing an ink could be very intensively
thinned, thereby losing its original light fastness. (For
example, a certain orange could be comprised of 1
74
part red and 20 parts yellow. Thinned by a factor of
20 the inherently good light fastness of the unmixed
red exhibits a significantly poorer light fastness. When
exposed to light, the orange quickly becomes yellow.)
75
SECTION 3 test equipment (manufacturers)
Specifications
Diameter of roll: mm 85 ± 2.5
Roll cover: rubber to hardness scale Shore A 80 ± 5
Width of roll: mm 50 ± 1
Weight of roller: kg 2 ± 0.05
Rollers made to the earlier specifications
92 – 98 mm diameter are still acceptable.
Technical data
Roller speed 3 levels 5, 10, 200 (± 1 %) mm/s
Length of roll area adjustable max 300mm Mains connection 220 V/50 or 110V/60
Roll data
Diameter: mm 85 ± 2.5
Width: mm 50 ± 1
Weight: kg 2 ± 0.05
Hardness of rubber surface: Shore A 80 ± 5
Thickness of rubber layer: mm 6 ± 0.5
Rolls can be supplied to other standards
Atlas Material testing Technology UK, USA textile testing machines 84,86
Brookfield Viscometers United Kingdom viscometers 84
Brookfield Engineering Laboratories Vertriebs GmbH Germany, India, USA viscometers 79,82,86
BRK Instruments India India viscometers 82
Büro Mayr Germany standard test rollers 79
Cheminstruments USA 86
Datacolor Switzerland colour measurement 83
Elcometer Belgium, France, Germany
Japan, Netherlands scratch resistance 78,79,82
76
Company Country Test equipment Page
77
SECTION 3.3 test equipment manufacturers
austria
belgium
china
SDL Atlas China 1/F (South East) & 2/F Textile testing machines
Shenjian Mansion Shirlestain
Central District (West) Hi-Tech Park
Nanshan, Shenzhen 518057
Tel.: +86-755-26711168
Fax: +86-755-26711337
E-mail: info@sdlatlas.com.cn
canada
78
france
MTS Systems 58, Rue Auguste Perret, Europarc Tensile testers for release,
F-94200 Creteil tack and peel
Tel.: +33-1-58439000 Specimen cutters, rollers
Fax: +33-1-58439001
E-mail: contact.ance@mts.com
URL: www.mts.com
germany
germany
81
SECTION 3.3 test equipment manufacturers
india
japan
netherlands
Sneep Industries BV P.O. Box 5726 Shear testers, hot melt/holding power
NL-3290 AA Strijen at elevated temperature
Tel.: +31 – 78 – 6107690 High and low speed peel and release
Fax: +31 – 78 – 6107691 testers
E-mail: info@sneepindustries.com Hand rollers, testplates of stainless
URL: www.sneepindustries.com steel and glass
Automatic roll down machine
Custom built testers
FTM 1, 2, 3,4, 5, 8, 9
82
netherlands
singapore
Sheen Instruments 3A International Business Park #08-02 Instruments for use in coating
ICON@IPB, Tower A and paint industry, incl. Abrasion,
Singapore 609935 coating thickness, colour match,
Tel.: +65-69337680 gloss, hardness, moisture
E-mail: info@sheeninstruments.com measuring
URL: www.sheeninstruments.com
switzerland
com
URL: www.testingmachines.com
83
SECTION 3.3 test equipment manufacturers
sweden
united kingdom
Adhesive Technical Services Beacon Hill Industrial Estate Adhesive, label and tape testing
PO Box 51, Botany Way according to FINAT, AFERA, PSTC,
Purfleet, Essex RM19 1SY PSMA and ASTM.
Tel.: +44–1708–867355 Agents for Cheminstruments
Fax: +44–1708–869804
E-mail: sales@adhtechnical.com
URL: www.adhtechnical.com
Atlas Material Testing 2 New Star Road Textile testing machines Shirlestain
Leicester LE4 9JD
Technology Ltd. Tel.: +44-116-2462957
E-mail atlas.service@ametek.co.uk
URL: www.atlas-mts.co.uk
M.C. TEC England P.O. Box 1067 Hand rollers, Rolling ball track
FINAT TECHNICAL HANDBOOK 2014 |
Stable Micro Systems Ltd. Vienna Court, Lammas Road Tensile/compression equipment
Godalming, Surrey GU7 1YL FTM 1, 2, 3, 5, 6, 9, 18, 22
Tel.: +44 - 1483 - 427345
Fax: +44 - 1483 - 427600
E-mail: stable@stablemicrosystems.com
URL: www.stablemicrosystems.com
The Testometric Unit 1, Lincoln Business Park Tensile, compression, loop tack,
Company Ltd. Lincoln Close, Rochdale probe tack, 90 & 180 degree
Lancashire OL11 NR peels, friction, dynamic shear and
Tel.: +44 - 1706 - 654039 adhesion/peel tests, conducted
Fax: +44 - 1706 - 646089 at cryogenic and elevated
E-mai:l info@testometric.co.uk temperatures
URL: www.testometric.co.uk
3M United Kingdom Plc 3M Centre TTapes 810 magic TM tape FTM 21,
Cain road 22
Bracknell, Berkshire RG12 8HT
Tel.: +44-8705-360036
URL: www.3direct.co.uk
www.3m.com
FINAT TECHNICAL HANDBOOK 2014 |
85
SECTION 3.3 test equipment manufacturers
usa
ChemInstruments, Inc. 510 Commercial Drive FTM 1, 2, 3, 4, 5, 7, 8 9, 10, 11, 13, 14,
Fairfield OH 45014 15,18, 21, 24
Tel. +1-513-8601598 Chemsultants International
Fax +1-513-8601597 Network is a source for contract
URL www.chemsultants.com research, laboratory testing,
pilot coating, consulting, test
instruments and hands-on
Chemsultants, Inc. Chemsultants, Inc. seminars.
9079 Tyler bvd
Mentor OH 44060
Tel. +1-440-9743080
Fax +1-440-9743081
URL www.chemsultants.com
Hunter Associates 11491 Sunset Hills Road Colour measurement FTM 20, 22
Reston, VA 20190-5280
Laboratory Inc. Tel.: +1 - 703 - 4716870
Fax: +1 - 703 - 4714237
E-mail: info@hunterlab.com
URL: www.hunterlab.com
Sheen Instruments 5856 Corporate Ave, Instruments for use in the coating
Suite 220, Cypress, and paint industry, incl. abrasion,
CA 90630 coating thickness, colour match,
Tel.: +1-760-3433650 gloss, hardness, moisture
Email: info@sheeninstruments.com measuring
URL: www.sheeninstruments.com
This is a list of independent testing laboratories/institutes that can carry out specific tests in relation to packaging, food
contact (migration) and other industry areas. Except for IGT-Netherlands and SGS France (= FINAT members) FINAT does
not have any business relations or agreement with them.
belgium
CELABOR, Research and Mr David Berck, M.Sc. All FTMs except for 4, 7 and 19.
(Dept. Manager, Packaging – Raw
Testing Centre materials)
Avenue du Parc 38
B-4650 Herve
Tel. +32-87-322456
Fax +32 -87-341387
E-mail david.berck@celabor.be
URL www.celabor.be
china
Shanghai Rubber Product Mr Jiang Honggui All FTMs except for 4, 7 and 19.
381, PanYu Road
Research Institute 200052 Shanghai
Tel. +86-21–62815008
Fax +86–21-62816790
E-mail webmaster@china-sirp.com
URL www.china-sirp.com
denmark
Eurofins Product Testing Smedeskovvej 38 All FTMs except for 4, 7 and 19.
DK-84y64 Galten
Denmark A.S. Tel. +45-70-224276
Fax +45-70-224275
E-mail product-testing@eurofins.dk
URL www.eurofins.dk
www.dti.dk/
services/#p=23739
(English version)
finland
88
finland
france
SGS - CTS Bat 8, Parc du Golf FTM 1, 2, 3, 5, 6, 7, 8, 10, 11, 12 13, 14,
F-13594 Aix-en-Provence Cedex 3 15, 16, 17, 18, 20 21, 22, 23 25
Tel. +33-4-42977213
Mob. +33-4-11738138
E-mail fabien.mille@sgs.com
URL www.sgsgroup.fr
89
SECTION 3.4 testing institutes
germany
PTS Papiertechische Stiftung Hessstr. 134 PTS conducts materials tests and
(The Paper Technology Specialists) D-80797 München analyses in:
Tel. +49-89-121460 (switchboard) Pulps and recovered paper, coating
URL www.ptspaper.de pigments, process additives; Paper,
paperboard, Adhesives, films,
Pirnaer Straße 37 composites and coatings; Paper
01809 Heidenau converting products and paper coating
Tel. +49-352-955160 products; Food microbiological and
Fax +49-352-9551899 food chemistry testing, environmental
E-mail irene.pollex@ptspaper.de compatibility; Water/effluents, sludge,
URL www.ptspaper.de solid wastes/waste
japan
Fax +81-3-27281710
URL www.chemitox.co.jp/eng/
DJK Corporation 5376-1, Shimo-shinjuku, Kimagase, Peel adhesion, release force, coat
Noda-shi, Chiba 270-0222 weight, chemical resistance
Tel +81-4-71984111
Fax +81-4-71983358
E-mail info@djklab.com
URL www.djkrc.co.jp
91
SECTION 3.4 testing institutes
japan
IGT Testing Systems K.K. 1229-1, Mawatashi, Sakura-shi, Printability testing, maintenance &
Chiba-ken 285-0804 calibration
Tel. +81-43-3087302
Fax +81-43-3087304
E-mail japan@igt.nl
URL www.igt.nl
netherlands
Hechtingsinstituut Delft Kluyverweg 1 Adhesive bonding tests
2629 HS Delft
Tel +31-015-2785353
Fax +31-015-2787151
E-mail: info@hechtingsinstituut.nl :
URL www.hechtingsinstituut.nl
singapore
IGT Testing Systems Pte. Ltd. Blk. 3 Ang Mo Kio Printability testing, maintenance &
Ind. Park 2A calibration
#05-11 AMK Tech 1
Singapore 568050
Tel. +65 6481 8993
Fax: +65 6481 9685
URL www.igt.nl
spain
sweden
Adhesive Technical Services Beacon Hill Industrial Estate Adhesive, label and tape testing
PO Box 51, Botany Way according to FINAT, AFERA, PSTC,
Purfleet, Essex RM19 1SY PSMA and ASTM.
Tel. +44–1708–867355 Agents for Cheminstruments
Fax +44–1708–869804
E-mail sales@adhtechnical.com
URL www.adhtechnical.com
usa
FINAT TECHNICAL HANDBOOK 2014 |
Adherent Laboratories Inc. 3804 Dunlap Street North Product development, consulting
Saint Paul, MN 55112 and testing laboratory specialising
Tel. +1- 651-4821264 in adhesives, sealants, coating and
E-mail info@adherentlabs.com material science.
URL www.adherentlabs.com
93
SECTION 3.4 testing institutes
usa
ChemInstruments, Inc. 510 Commercial Drive FTM 1, 2, 3, 4, 5, 7, 8 9, 10, 11, 13, 14,
Fairfield OH 45014 15,18, 21, 24
Tel. +1-513-8601598 Chemsultants International
Fax +1-513-8601597 Network is a source for contract
URL www.chemsultants.com research, laboratory testing,
pilot coating, consulting, test
instruments and hands-on
Chemsultants, Inc. Chemsultants, Inc. seminars.
9079 Tyler bvd
Mentor OH 44060
Tel. +1-440-9743080
Fax +1-440-9743081
URL www.chemsultants.com
94
3.5
tesa test tapes product information
and worldwide addresses
SECTION
Productinformation Productinformation
tesa® 4104 is a premium packaging tesa® 7475 and 7476 are especially
tape based on a PVC-film backing designed for the characterisation of
and a natural rubber adhesive It silicone coated liners.
shows excellent performance on A typical test method represents
all kind of cardboards and secures FINAT 10 and FINAT 11.
a safe closure. The natural rubber For a comprehensive characterisation
adhesive system is designed to of release properties it is
show best results for applications recommended to use both tapes.
on different kind of surfaces.
tesa® 7475 features a typical modified a crylic adhesive to
Main Application record the interaction of a silicone and an acrylic adhesive.
• sealing small boxes (card-board or plastic) Additionally it shows a significant interaction with SiH
• sealing tins and bags Groups for measurement of the grade of curing of a silicone
• sealing of cartons of medium to heavy-range weight. by measuring the subsequent adhesion according FINAT 11.
Technical Data
tesa® 7475 pv2 • Backing material - cotton cloth
• Type of adhesive - natural rubber
Productinformation • Type of liner - glassine
tesa® 7475 has been successfully • Shelf life time - 12 months
deployed for many years, both when
it comes to assessing the release
properties of silicone coatings
(FINAT 10 or similar) and testing the latest information
curing of silicone coatings (FINAT
11 or similar). For a comprehensive tesa® 4104 - http://l.tesa.com/?ip=04104
characterization of release properties tesa® 7475 - http://l.tesa.com/?ip=07475
it is recommended to use both tesa® tesa® 7476 - http://l.tesa.com/?ip=07476
7475 (acrylic adhesive) and tesa®
FINAT TECHNICAL HANDBOOK 2014 |
Main Application
• Characterization of silicone coatings
Technical Data
• Backing material - PET film
• Type of adhesive - acrylic
• Type of liner - glassine For the latest information on these
• Shelf life time - 24 months test tapes visit www.tesa.com
95
3.5
tesa test tapes product information
and worldwide addresses
SECTION
AFGHANISTAN BRAZIL CHINA CROATIA
tesa Export tesa Brasil Ltda. - Curitiba tesa tape (Guangzhou) Co., Ltd. tesa tape Kft.
Quickbornstraße 24 Ave. João Gualberto, No. 1259 - 18th Floor Room 1002-03, Zhongzhou Trading Representative Office
20253 Hamburg Centro Empresarial Lais Peretti Center, No. 1008, Xin Gang East Road, Tijardoviceva 8
Germany Alto da Gloria Haizhu District, Huangzhou 510335 10.000 Zagreb
Phone: +49 (40) 49094095 80030-000 Phone: +86 (20) 89300200 Phone: +385 (1) 3882929
Fax: +49 (40) 49092265 Curitiba-PR Fax: +86 (20) 89300201 Fax: +385 (1) 3882929
Manager: Jakob Ravn Phone: +55 (41) 30218100 Manager: Dick Li Manager: Gyula Behumi
Fax: +55 (41) 30218110
www.tesatape.com.br
Manager: Antonia Marques
ALL AFRICAN COUNTRIES CHINA CZECH REP.
tesa Export tesa tape (Hong Kong) Ltd. tesa tape s.r.o.
Quickbornstraße 24 The gate way tower 2, Suite 712, Pekarská 14
20253 Hamburg BULGARIA 25 Canton Road, Tsim Sha Tsui Kowloon, 155 00 Praha 5
Germany tesa tape A.E. Hongkong Phone: +420 (296) 824546
Phone: +49 (40) 49094095 Representative Office Phone: +852 (2) 25839980 Fax: +420 (296) 824549
Fax: +49 (40) 49092265 2, Agiou Nektariou Str. Fax: +852 (2) 25839244 www.tesa-tape.cz
Manager: Jakob Ravn GR-153 44 Gerakas / Attiki Manager: Dick Li Manager: Tomas Kuska
Phone: +30 (210) 6600290
Fax: +30 (210) 6610657
Manager: Kostas Theodoropoulos
ARGENTINA CHINA DENMARK
tesa tape Argentina S.R.L. tesa tape (Shanghai) Co., Ltd tesa A/S
Av. Del Libertador 6966 5° B No.1, 2500 Lane Xiu Pu Road, Klintehøj Vaenge 12
(C1429BMP) CHILE Pudong Shanghai 3460 Birkerød
Ciudad Autonoma de Buenos Aires tesa tape Chile S.A. Phone: +86 (27) 68183110 Phone: +45 (45) 998200
Argentina Av. Presidente Riesco 5561. Oficina 1104 Fax: +86 (27) 68183860 Fax: +45 (45) 810145
Phone: +54 (11) 47811846 Las Condes, Santiago Manager: Dick Li www.tesa.dk
Fax: +54 (11) 47869107 Phone: +56 (2) 3693600 Manager: Steve Plastow
www.tesatape.com.br Fax: +56 (2) 3693699
Manager: Antonio Marques www.tesa.cl
Manager: David Paz CHINA
tesa tape (Shenzhen) Co., Ltd ESTONIA
Room 11f, Jingyun Century tesa A/S Estonia
AUSTRALIA Mansion , No.6033 Shennan Street, Sepise 1
tesa tape Australia Pty. Ltd. CHINA Futian District, Shenzhen 518040 11415 Tallinn
Unit 8, 2 Southridge Street, tesa (Suzhou) Co., Ltd Phone: +86 (755) 33958620 Phone: +372 (640) 1366
Eastern Creek NSW 2766, Room 1716, Century Fiernancial Tower, Fax: +86 (755) 33958621 Fax: +372 (640) 1359
Sydney No.1 West Suzhoudadao, Suzhou Manager: Dick Li www.tesa.dk
Phone: +61 (2) 98303929 Industrial Park, Jiangsu 215021 Manager: Sergei Pljassunov
Fax: +61 (2) 98303928 Phone: +86 (512) 62965613
Manager: Gary Robinson Fax: +86 (512) 62965693
Manager: Mr. Dick Li CHINA
tesa Tape (Tianjin) Co., Ltd FINLAND
Room 11D1 Building A, DaAn Mansion, tesa Oy
AUSTRIA No.41, Friendship Road, HeXi Dist, Puutarhakatu 53
tesa GmbH CHINA Tianjin 300211 20100 Turku
Laxenburger Str. 151 tesa tape (Beijing) Co. Ltd. Phone: +86 (22) 28362660 Phone: +358 (2) 2103400
1100 Wien Room A704, Zhengjia Mansion, Fax: +86 (22) 28361990 Fax: +358 (2) 4103291
Phone: +43 (1) 614000 No.7, Jian Guo Road, Chaoyang Manager: Dick Li www.tesa.dk
Fax: +43 (1) 61400455 District, Beijing, 100024 Manager: Steve Plastow
www.tesa.at Phone: +86 (10) 85931022
Manager: Gabriele Kosar Fax: +86 (10) 85931021
Manager: Dick Li CHINA
tesa Tape (Wuhan) Co., Ltd FRANCE
Room 710, 7/F New World Centre, tesa s.a.s.
BAHRAIN Tower A, Hangkong Road, Jiefang La Croix du Sud - ZAC CARRE SENART
tesa Export CHINA Avenue, Wuhan 430022 2 Allée de la Mixité
Quickbornstraße 24 tesa tape (Changchun) Co. Ltd. Phone: +86 (27) 68838713 77127 Lieusaint
20253 Hamburg Room 1101, Fax: +86 (27) 68838710 Phone: +33 (1) 78482000
Germany ZhongTian Mansion No. 2066, Manager: Dick Li Fax: +33 (1) 78482001
Phone: +49 (40) 49094095 Puyang Street, Lvyuan Dist, www.tesa.fr
Fax: +49 (40) 4909 2265 Changchun 130062 Manager: Bruno Derouet
FINAT TECHNICAL HANDBOOK 2014 |
96
GUATEMALA ITALY JORDAN MEXICO
tesa tape Centro América S.A. tesa SpA tesa Export tesa tape México
Diagonal 6, 10-50 Zona 10 Via L. Cadorna 69 Quickbornstraße 24 Av. Santa Fe No. 170
Edificio Interamericas WFC 20090 Vimodrone (Milano) 20253 Hamburg German Centre P 6-3-3
Torre Norte nivel 12, oficina 1202 Phone: +39 (02) 25010811 Germany Col. Lomas de Santa Fe
Guatemala, C.A. Fax: +39 (02) 25010841 Phone: +49 (40) 49094095 D.F. C.P. 01210
Phone: +502 (2) 2449100 Manager: Matteo Martinelli Fax: +49 (40) 49092265 Phone: +52 (55) 52926978
Fax: +502 (2) 2449191 Manager: Jakob Ravn www.tesatape.com
Manager: Carlos Blanco Manager: Fernando Cruz
JAPAN
tesa tape K.K. KOREA
HUNGARY 8F, Shirokanetakanawa Station Bldg. tesa tape Korea Ltd. NETHERLANDS
tesa tape Kft. 1-27-6 Shirokane, Minato-ku City Air Tower 159-9, Room 1805 tesa BV
2040 Budaörs Tokyo 108-0072 Samseong-dong, Gangnam-gu Stationsplein 3-1
Szabadság út 117. Phone: +81 (3) 68332300 Seoul 135-973 1211 EX Hilversum
Phone: +36 (23) 814154 Fax: +81 (3) 34737440 Korea Phone: +31 (35) 6250200
Fax: +36 (23) 814160 www.tesa.jp Phone: +822 (569) 8451 Fax: +31 (35) 6250240
www.tesa.hu Manager: Andreas Walkembach Fax: +822 (569) 8455 www.tesa.nl
Manager: Gyula Behumi Manager: Detlev Radloff Manager: Ferdy Denie
JAPAN
INDIA tesa tape K.K. (Nagoya) KUWAIT NEW ZEALAND
tesa Tapes (India) Pvt. Ltd. 7F, arex Bldg, tesa Export tesa tape New Zealand Ltd.
301, 3rd Floor, Lakhani Centrium, 1-4-12, Marunouchi, Naka-ku, Nagoya- Quickbornstraße 24 PO Box 33-121
Plot No 27, Sec 15, CBD Belapur, shi, 20253 Hamburg Takapuna, 0740
Navi Mumbai - 400614 Aichi-ken 460-0002 Germany Auckland
Maharashtra Phone: +81 (52) 2234511 Phone: +49 (40) 49094095 Phone: +64 (0800) 837269
Phone: +91 (22) 47419200 Fax: +81 (52) 2234512 Fax: +49 (40) 49092265 Fax: +64 (0800) 837267
Fax: +91 (22) 47419299 www.tesa.jp Manager: Jakob Ravn Manager: Gary Robinson
Manager: Venkatesh Inamdar Manager: Andreas Walkembach
LATVIA NORWAY
INDONESIA JAPAN tesa A/S tesa AS
tesa tape Asia Pacific Pte. Ltd. tesa tape K.K. (Osaka) Vienibas gatve 109 Karihaugveien 89
11th Floor, Suite A, Perwata Tower 4F, Risoshinosaka Bldg, 4-3-7-Miyahara, LV 1058, Riga 1086 Oslo
CBD Pluit, Jl Pluit Selatan Raya Yodogawa-ku. Osaka-shi, Phone: +371 (679) 30180 Phone: +47 (22) 907979
Jakarta Utara 14440 Osaka-fu 532-0003 Fax: +371 (679) 30179 Fax: +47 (22) 300376
Phone: +62 (21) 66672978 Phone: +81 (6) 63965811 www.tesa.dk www.tesa.dk
Fax: +62 (21) 66672985 Fax: +81 (6) 63967648 Manager: Andris Kranevskis Manager: Steve Plastow
Manager: Tanaka Takafumi www.tesa.jp
Manager: Andreas Walkembach
LEBANON OMAN
IRAN tesa Export tesa Export
tesa Export JAPAN Quickbornstraße 24 Quickbornstraße 24
Quickbornstraße 24 tesa tape K.K. 20253 Hamburg 20253 Hamburg
20253 Hamburg Technical Center (tTC) Germany Germany
Germany 10F, Shirokanetakanawa Station Bldg Phone: +49 (40) 49094095 Phone: +49 (40) 49094095
Phone: +49 (40) 49094095 1-27-6 Shirokane, Minato-ku Fax: +49 (40) 49092265 Fax: +49 (40) 49092265
Fax: +49 (40) 49092265 Tokyo 108-0072 Manager: Jakob Ravn Manager: Jakob Ravn
Manager: Jakob Ravn Phone: +81 (3) 68332321
Fax: +81 (3) 54235753
www.tesa.jp
Manager: Andreas Walkembach LITHUANIA PAKISTAN
IRAQ tesa A/S tesa Export
tesa Export V.Gerulaicio str.1 Quickbornstraße 24
Quickbornstraße 24 08200 Vilnius 20253 Hamburg
20253 Hamburg JAPAN Lithuania Germany
Germany tesa tape K.K. Warehouse Phone: +370 (5) 2191555 Phone: +49 (40) 49094095
Phone: +49 (40) 49094095 C/O Japan transcity Corp, Fax: +370 (5) 2191554 Fax: +49 (40) 49092265
Fax: +49 (40) 49092265 1221 Minamibansyu, Mitsubuchi, www.tesa.dk Manager: Jakob Ravn
FINAT TECHNICAL HANDBOOK 2014 |
97
3.5
tesa test tapes product information
and worldwide addresses
SECTION
POLAND SLOVENIA TAIWAN UNITED ARAB EMIRATES
tesa tape Sp. z o.o. tesa tape d.o.o. tesa tape (Hong Kong) Ltd. - tesa Middle East
ul. Gnieznienska 32 Pot k sejmiscu 30 Taiwan Branch Office No.: LOB 15-604C
61-021 Poznan 1231 Lj.-Crnuce 9F-1, 3, Sec 1 Min Sheng Road Jebel Ali Free Zone,
Phone: +48 (61) 8746147 Phone: +386 (1) 5602409 Panchiao 220, Taipei Hsien PO Box 261534
Fax: +48 (61) 8746019 Fax: +386 (1) 5602415 22069 Taiwan Dubai, United Arab Emirates
www.tesa.pl www.tesa.si Phone: +886 (2) 29579662 Phone: +971 (4) 8808933
Manager: Tomasz Badyda Manager: Gylua Behumi Fax: +886 (2) 29579433 Mobile: +971 (5) 54056706
Manager: Dick Li Manager: Richard Dunn
SPAIN
QATAR tesa tape S.A. THAILAND USA
tesa Export Ctra. de Mataró a Granollers, P. Km. 5,4 tesa tape Thailand Limited tesa tape inc.
Quickbornstraße 24 08310 Argentona 1858/80, 17th Floor, Nation Tower 800 W. El Camino Real - Suite 180
20253 Hamburg Phone: +34 (93) 7583300 Bangna-Trad Road, Bangna Bangna Mountain View, CA 94040
Germany Fax: +34 (93) 7583444 Bangkok 10260 electronics.tesa.com
Phone: +49 (40) 49094095 www.tesatape.es Phone: +66 (2) 751 4025 to 4029
Fax: +49 (40) 49092265 Manager: Jordi Senespleda Fax: +66 (2) 7514030
Manager: Jakob Ravn Manager: Tanaka Takafumi
VIETNAM
tesa tape Asia Pacific Pte Ltd.
SRI LANKA Unit 705A, 7th Floor, Me Linh Point Tower
ROMANIA tesa Export TURKEY No. 2 Ngo Duc Ke Street
tesa tape SRL Quickbornstraße 24 tesa Bant Sanayi ve Ticaret A.S. District 1
str.Observatorului , nr.113A, etaj 1, 20253 Hamburg Merdivenköy Mah. Bora Sokak No:1 Ho Chi Minh City
Cluj-Napoca, 400363 Germany Nida Kule Göztepe K:4 Phone: +84 (8) 823 7850 Ext 2805 &
Romania Phone: +49 (40) 49094095 34732 Kadıköy İstanbul 2806
Phone: +40 (364) 401140 Fax: +49 (40) 49092265 Phone: +90 (216) 5789000 Fax: +84 (8) 8237840
Fax: +40 (364) 401141 Manager: Jakob Ravn Fax: +90 (216) 5789001 Manager: Tanaka Takafumi
www.tesatape.ro www.tesabant.com.tr
Manager: Magnus Becker Manager: Mete Konuralp
SWEDEN VIETNAM
tesa AB tesa tape Asia Pacific Pte Ltd.
RUSSIA Box 10275 TURKEY Unit 210, 2nd Floor, V-Tower
tesa tape OOO 434 23 Kungsbacka tesa scribos Turkey 649 Kim Ma Street, BaDinh District
Shabolovka 10, Building 2 Phone: +46 (300) 55350 Merdivenköy Mah. Bora Sokak No:1 Hanoi
119049 Moscow Fax: +46 (300) 19494 Nida Kule Göztepe K:4 Phone: +84 (4) 7667800
Phone: +7 (495) 2584024 www.tesa.dk 34732 Kadıköy İstanbul Fax: +84 (4) 7667801
Fax: +7 (495) 7923245 Manager: Steve Plastow Phone: +90 (216) 5789000 Manager: Tanaka Takafumi
www.tesatape.ru Fax: +90 (216) 5789001
Manager: Audrius Petryla www.tesa-scribos.com
Manager: Ms. Tuba Olak
SWITZERLAND YEMEN
tesa tape Schweiz AG tesa Export
SAUDI ARABIA Industriestr. 19 Quickbornstraße 24
tesa Export 8962 Bergdietikon UKRAINE 20253 Hamburg
Quickbornstraße 24 Phone: +41 (44) 7443444 Representative Office Germany
20253 Hamburg Fax: +41 (44) 7412672 tesa tape KFT Phone: +49 (40) 49094095
Germany www.tesa.ch 104 Saksaganskogo street Fax: +49 (40) 49092265
Phone: +49 (40) 49094095 Manager: Claus Grobe Office 4 Manager: Jakob Ravn
Fax: +49 (40) 49092265 Kyiv 01032
FINAT TECHNICAL HANDBOOK 2014 |
98
World-wide Association for self-adhesive labels and related products
P.O. Box 85612
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The Netherlands
Tel.: +31 (70) 312 39 10
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