ORGANIC

CHEMISTRY

A. EQUIPMENTS AND MATERIALS

EQUIPMENTS :
1) Beaker glass 100 mL 2 pieces
2) Beaker glass 250 mL 1 piece
3) Test Tube 6 pieces
4) Graduated cylinder 10 mL 1 piece
5) Graduated cylinder 25 mL 1 piece
6) Erlenmeyer 250 mL 2 pieces
7) Burette 50 mL 2 pieces
8) Reflux 1 piece
9) Stative and clamps 2 set
10) Bunsen burner 1 piece
11) Gauze 1 piece
12) Hot plate 1 piece
13) Pipette Sufficiently
14) Container of soap 6 pieces
15) Analitical Balance 1 piece
16) Tripod 1 piece
17) Thermometer 1 piece
18) Boling stone 1 piece
19) Stopwatch 1 piece
20) Plastic pipe sufficiently
MATERIALS :
1) Coconut oil 17 mL
2) Palm oil 17 mL
3) Bulk oil 17 mL
4) KOH 0.1 N sufficiently
5) Olive oil 3 mL
6) NaOH solid 5.2 gam
7) Stearic acid 3 gram
8) Alcohol 48 mL
9) Glycerin 12 gram

1 Soap Making
 ORGANIC
CHEMISTRY

10) PP indicator sufficiently

11) Ethanol 75 mL
12) KOH alcoholic 0,5 N 75 mL
13) HCl 0,5 N sufficiently
14) Dye and parfume sufficiently
15) Aquades sufficiently

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 ORGANIC
CHEMISTRY

B. LANES WORK
1. Soap Making
 Making of NaOH solution
1,4 grams NaOH crystal

1. Entered into test tube

2. Dissolved in 3,3 ml of aquadest

NaOH solution
 Soap making
10 grams of oils (Palm, Coconut and Bulk)

1. Add 1 gram of steric acid.

2. Heat untl 70°C and all of stearic acid melts.
3. Let miture until 50°C .
4. Add NaOH solution.
5. Stir it.
6. Add 12 gram of alcohol and 4 gram of glycerin.
7. Heat and stear it ntul the solution become coloeless.
8. Let tehmixture become cooler.
9. Add 1 mL of olive oil.
10. Add dye and parfume .
11. Pour into the mold.

Solid Soap

2. Emulsion properties of soap

3 mL of aquades

1. Add 5 drops of oil.

2. Add 2 mL of soap soution (0,1 – 0,2 gram soap which
dissolved in 6 - 8 mL of hot water)
3. Shake it strongky.
4. Wait a minute
5. Record the time
Solution become 2 layers

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 ORGANIC
CHEMISTRY

3 mL of aquades

1. Add 5 drops of oil.

2. Shake it strongky.
3. Wait a minute
4. Record the time

Solution become 2 layers

3. Acid number
5 gram of oils (Palm, Coconut and Bulk)

1. Add 25 mL of ethanol.
2. Add 5 drops of PP indicator.
3. Titrated with KOH 0,1 N as a standart solution.
4. Repeat it to 3 types of oils.

Volume of KOH

5. Calculated the acid number

Acid Number

4. Saponification number
2 gram of oils (Palm, Coconut and Bulk)

1. Add 25 mL of KOH alcoholic 0,5 N.

2. Refluxed for 30 minutes.
3. Cooled.
4. Add 5 drops of PP indicator.
5. Titrated with HCl 0,5 N as a standart solution.
6. Repeat it to 3 types of oils.
Volume of HCl

7. Calculated the saponification number

Sapponification Number

4 Soap Making