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1.E-01 1.E-01
JO/L%U JO/L%U
1.E-02 1.E-02

1.E-03 1.E-03
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1.E-04 1.E-04

1.E-05 1.E-05

1.E-06 1.E-06

1.E-07 1.E-07
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1.E-08 50º C 1.E-08 50º C
75º C 75º C
1.E-09 1.E-09
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JO/L%U JO/L%U
1.E-02 1.E-02

1.E-03 1.E-03

1.E-04 1.E-04
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|i|/A cm-2
1.E-05 1.E-05

1.E-06 1.E-06

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1.E-08 75º C 1.E-08 75º C
100º C 100º C
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1.E-02 1.E-02

1.E-03 1.E-03
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1.E-04 1.E-04

1.E-05 1.E-05

1.E-06 1.E-06

1.E-07 25º C 1.E-07 25º C

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1.E-08 75º C 1.E-08 75º C
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1.E-05 1.E-05

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1.E-06 100 1.E-06 100
125 125
150 150
1.E-07 1.E-07
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E vs (Ag/AgCl)/V E vs (Ag/AgCl)/V
 
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0.2  -400 0.2  -400

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0.08 0.08
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0.16 25ºC-75ºC 0.16 25ºC-75ºC
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0.12 0.12
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0.04 0.04

0.00 0.00

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0.70 75º C-100º C 0.70 75º C-100º C
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0.60 0.60

0.50 0.50
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0.40 0.40

0.30 0.30

0.20 0.20

0.10 0.10

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150

100 100

50 50
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
0 0

-50 -50

-100 -100

-150 -150

25ºC-25ºC 25ºC-25ºC
-200 25ºC-50ºC
-200 25ºC-50ºC
25ºC-75ºC 25ºC-75ºC
-250 -250
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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-50 -50
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
-100 -100

-150 -150

-200 -200

-250 -250
25ºC-25ºC 25ºC-25ºC
-300 25ºC-50ºC -300 25ºC-50ºC
25ºC-75ºC 25ºC-75ºC
25ºC-100ºC 25ºC-100ºC
-350 -350
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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25ºC-25ºC 25ºC-25ºC
25ºC-50ºC 25ºC-50ºC
25ºC-75ºC 25ºC-75ºC
-50 25ºC-100ºC -50 25ºC-100ºC
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
-100 -100

-150 -150

-200 -200

-250 -250
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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250 250
200 200
150 150
100 100
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
50 50
0 0
-50 -50
-100 -100
-150 -150
-200 -200
-250 -250
75º C-75º C 75º C-75º C
-300 -300
75º C-100º C 75º C-100º C
-350 75º C-125º C -350 75º C-125º C
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-450 -450
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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100 100
y = 2.83x - 169.91 y = 2.83x - 169.91
50 R = 0.915 50 R = 0.915

y = 2.93x - 111.14 y = 2.93x - 111.14

0 R = 0.998 0 R = 0.998
y = 3.086x - 221.03 y = 3.086x - 221.03
Eth vs (Ag/AgCl)/mV

Eth vs (Ag/AgCl)/mV
R = 0.995 R = 0.995
-50 -50

-100 -100

-150 -150

-200 -200
y = 2.6526x - 254.58 400 g/l LiBr y = 2.6526x - 254.58 400 g/l LiBr
-250 R = 0.997 700 g/l LiBr -250 R = 0.997 700 g/l LiBr
992 g/l LiBr 992 g/l LiBr
-300 -300
1080 g/l LiBr 1080 g/l LiBr
Li l (1080 /l Li l (1080 /l
-350 -350
0 25 50 75 100 0 25 50 75 100
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-400  -90 -400  -90

D  -80
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Ángulo de fase (grados)

Ángulo de fase (grados)

-300 -70 -300 -70
 
-60 -60
Z''/kΩ cm2

Z''/kΩ cm2
-200
 -50
-200
 -50

 -40
 -40

-30 -30
-100  -100 
Electrodos frío y caliente (AAT) -20 Electrodos frío y caliente (AAT) -20
Electrodos frío y caliente (AAT) Electrodos frío y caliente (AAT)
 
Electrodo frío (DAT) Electrodo frío (DAT)
Electrodo caliente (DAT) -10 Electrodo frío (DAT) Electrodo caliente (DAT) -10 Electrodo frío (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT)
0 0
 0 100 200 300 400
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 0 100 200 300 400
0
0.01 0.1 1 10 100 1000 10000 100000

 Ω cm2
Z'/kΩ Frecuencia (Hz)  Ω cm2
Z'/kΩ Frecuencia (Hz)

-400  -90 -400  -90

E 
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Ángulo de fase (grados)

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-300 -300
-60 -60
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2
Z''/kΩ cm

Z''/kΩ cm
 -50  -50
-200 -200
-40 -40
 
-30 -30

-100
 -20 -100
 -20
Electrodo frío (AAT) Electrodo frío (AAT)

 
Electrodo frío (AAT) Electrodo caliente (AAT) Electrodo frío (AAT) Electrodo caliente (AAT)
Electrodo caliente (AAT) -10 Electrodo frío (DAT) Electrodo caliente (AAT) -10 Electrodo frío (DAT)
Electrodo frío (DAT) Electrodo caliente (DAT) Electrodo frío (DAT) Electrodo caliente (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT)
0 0
0  0.01 0.1 1 10 100 1000 10000 100000
0  0.01 0.1 1 10 100 1000 10000 100000
0 100 200 300 400 0 100 200 300 400
 Ω cm
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Z'/kΩ
2
Frecuencia (Hz)

 
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 -90
 -90

F -80
F -80
 
Ángulo de fase (grados)

Ángulo de fase (grados)

-300 -70 -300 -70

 -60  -60
Z''/kΩ cm2

Z''/kΩ cm2
-200  -50
-200  -50

-40 -40
 -30
 -30
-100  Electrodo frío (AAT)
-20 Electrodo frío (AAT)
-100  Electrodo frío (AAT)
-20 Electrodo frío (AAT)
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 -10

Electrodo frío (DAT) Electrodo frío (DAT) Electrodo frío (DAT) -10 Electrodo frío (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT)
0 0 0 0

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Frecuencia (Hz) Frecuencia (Hz)

 
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Ángulo de fase (grados)

-70 -70

 
-60 -60
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Z''/kΩ cm2
-50 -50
-200 -200
 -40  -40

-30 -30
 -100 -20
 -100 -20
Electrodos frío y caliente (AAT) Electrodos frío y caliente (AAT) Electrodos frío y caliente (AAT) Electrodos frío y caliente (AAT)

 
Electrodo frío (DAT) -10 Electrodo frío (DAT) Electrodo frío (DAT) -10 Electrodo frío (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT)
0 0 0 0

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Ω cm
Z'/kΩ Ω cm
Z'/kΩ
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-300 -70 -300 -70

 -60  -60
2

2
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-50 -50
 
Z''/kΩ

Z''/kΩ
-200 -200
-40 -40

 -30
 -30
-100 Electrodo frío (AAT) -20 -100 Electrodo frío (AAT) -20
Electrodo frío (AAT) Electrodo frío (AAT)
 Electrodo caliente (AAT)
Electrodo frío (DAT) -10
Electrodo caliente (AAT)
Electrodo frío (DAT)
 Electrodo caliente (AAT)
Electrodo frío (DAT) -10
Electrodo caliente (AAT)
Electrodo frío (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT)

 0
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0
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0 100 200 300 400
0
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 -400
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-90
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-300 -70 -300 -70

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-50 -50
-200 -200
-40 -40

 -30  -30
-100 -20 -100 -20
 Electrodo frío (AAT)
Electrodo caliente (AAT)
Electrodo frío (DAT) -10
Electrodo frío (AAT)
Electrodo caliente (AAT)
Electrodo frío (DAT)
 Electrodo frío (AAT)
Electrodo caliente (AAT)
Electrodo frío (DAT) -10
Electrodo frío (AAT)
Electrodo caliente (AAT)
Electrodo frío (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT)

 0 0
0.01 0.1 1 10 100 1000 10000 100000
 0 0
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0 100 200 300 400 0 100 200 300 400

 -400
Ω cm
Z'/kΩ
2 Frecuencia (Hz)
 -400
Ω cm
Z'/kΩ
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-90 -90

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Ángulo de fase (grado)

 
-300 -300
-60 -60
2

2
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Ω cm
 -50
 -50
Z''/kΩ

Z''/kΩ
-200 -200
-40 -40

 -30  -30
-100 -100
 
-20 -20
Electrodo frío (AAT) Electrodo frío (AAT) Electrodo frío (AAT) Electrodo frío (AAT)
Electrodo caliente (AAT) Electrodo caliente (AAT)
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Electrodo frío (DAT) Electrodo frío (DAT)
0 0 0 0
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0 100 200
 300
Frecuencia (Hz)
400 0 100 200
 300
Frecuencia (Hz)
400

 
2 2
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Ángulo de fase (grados)

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-300 -70 -300 -70

 -60
 -60
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2
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Ω cm
-50 -50
Z''/kΩ

Z''/kΩ
 -200 -40  -200 -40

 -100  -100
-30 -30

-20 -20
Electrodos frío y caliente (AAT) Electrodos frío y caliente (AAT)

 
Electrodos frío y caliente (AAT) Electrodos frío y caliente (AAT)
Electrodo frío (AAT) -10 Electrodo frío (DAT) Electrodo frío (AAT) -10 Electrodo frío (DAT)
Electrodo caliente (AAT) Electrodo caliente (DAT) Electrodo caliente (AAT) Electrodo caliente (DAT)
0 0 0 0
 0 100 200 300 400 0.01 0.1 1 10 100 1000 10000 100000  0 100 200 300 400 0.01 0.1 1 10 100 1000 10000 100000

2 Frecuencia (Hz) 2 Frecuencia (Hz)

Ω cm Ω cm
 -400 Z'/kΩ
-90
 -400 Z'/kΩ
-90

E  Ángulo de fase (grados)

-80 E  -80

Ángulo de fase (grados)

-300 -70 -300 -70
 -60  -60
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2
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Ω cm
 -200 -50
 -200 -50
Z''/kΩ

Z''/kΩ
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 -30  -30
-100 -20 -100 -20
 Electrodo frío (AAT)
Electrodo caliente (AAT)
-10
Electrodo
Electrodo
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Electrodo caliente (AAT)
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Electrodo
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Electrodo frío (DAT) Electrodo frío (DAT) Electrodo frío (DAT) Electrodo frío (DAT)
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 0 0
0.01 0.1 1 10 100 1000 10000 100000
 0 0
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 -400
Ω cm
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Ω cm
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-90 -90

F  -80
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-70 -70
 
-300 -300
-60 -60
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2
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Ω cm
 -50
 -50
Z''/kΩ

Z''/kΩ
-200 -200
-40 -40
 -30  -30
-100 -100
 Electrodo frío (AAT)
Electrodo caliente (AAT)
-20 Electrodo frío (AAT)
Electrodo caliente (AAT)
 Electrodo frío (AAT)
Electrodo caliente (AAT)
-20 Electrodo frío (AAT)
Electrodo caliente (AAT)
Electrodo frío (DAT) -10 Electrodo frío (DAT) Electrodo frío (DAT) -10 Electrodo frío (DAT)

 
Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT) Electrodo caliente (DAT)
0 0 0 0
0 100 200 300 400 0.01 0.1 1 10 100 1000 10000 100000 0 100 200 300 400 0.01 0.1 1 10 100 1000 10000 100000

 Ω cm
Z'/kΩ
2 Frecuencia (Hz)  Ω cm
Z'/kΩ
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-60 -60
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2
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 -50  -50
Z''/kΩ

Z''/kΩ
-200 -200
-40 -40
 -30
 -30

 -100
Electrodo frío (AAT)
Electrodo caliente (AAT)
-20 Electrodo frío (AAT)
Electrodo caliente (AAT)
 -100
Electrodo frío (AAT)
Electrodo caliente (AAT)
-20 Electrodo frío (AAT)
Electrodo caliente (AAT)
Electrodo frío (DAT) -10 Electrodo frío (DAT) Electrodo frío (DAT) -10 Electrodo frío (DAT)

 
Electrodo caliente (DAT) Electrodo caliente (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT)
0 0 0 0
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25ºC-25ºC - 400 g/l LiBr 25ºC-25ºC - 400 g/l LiBr

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0.080 0.080
25ºC-50ºC - 400-992 g/l LiBr 25ºC-50ºC - 400-992 g/l LiBr
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-2

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0.040 0.040

0.000 0.000

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0.200 0.200
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E 25ºC-50ºC - 700 g/l LiBr
25ºC-75ºC - 700 g/l LiBr
0.160 25ºC-100ºC - 700 g/l LiBr 0.160 25ºC-100ºC - 700 g/l LiBr
25ºC-25ºC - 700-992 g/l LiBr 25ºC-25ºC - 700-992 g/l LiBr
25ºC-50ºC - 700-992 g/l LiBr 25ºC-50ºC - 700-992 g/l LiBr
25ºC-75ºC - 700-992 g/l LiBr 25ºC-75ºC - 700-992 g/l LiBr
0.120 25ºC-100ºC - 700-992 g/l LiBr 0.120 25ºC-100ºC - 700-992 g/l LiBr
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-2
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0.080 0.080

0.040 0.040

0.000 0.000

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150 150
D D
25ºC-25ºC - 400 g/l LiBr 25ºC-25ºC - 400 g/l LiBr
100 25ºC-50ºC - 400 g/l LiBr 100 25ºC-50ºC - 400 g/l LiBr
25ºC-75ºC - 400 g/l LiBr 25ºC-75ºC - 400 g/l LiBr
25ºC-25ºC - 400-992 g/l LiBr 25ºC-25ºC - 400-992 g/l LiBr
50 25ºC-50ºC - 400-992 g/l LiBr
50 25ºC-50ºC - 400-992 g/l LiBr
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
25ºC-75ºC - 400-992 g/l LiBr 25ºC-75ºC - 400-992 g/l LiBr
0 0

-50 -50

-100 -100

-150 -150

-200 -200

-250 -250

-300 -300

-350 -350
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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25ºC-25ºC - 700 g/l LiBr 25ºC-25ºC - 700 g/l LiBr
E 0
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25ºC-75ºC - 700 g/l LiBr
E 0
25ºC-50ºC - 700 g/l LiBr
25ºC-75ºC - 700 g/l LiBr
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25ºC-25ºC - 700-992 g/l LiBr 25ºC-25ºC - 700-992 g/l LiBr
-50 25ºC-50ºC - 700-992 g/l LiBr -50 25ºC-50ºC - 700-992 g/l LiBr
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
25ºC-75ºC - 700-992 g/l LiBr 25ºC-75ºC - 700-992 g/l LiBr
25ºC-100ºC - 700-992 g/l LiBr 25ºC-100ºC - 700-992 g/l LiBr
-100 -100

-150 -150

-200 -200

-250 -250

-300 -300

-350 -350
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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100 100

50 50

0 0
Eth vs (Ag/AgCl)/mV

Eth vs (Ag/AgCl)/mV
-50 -50
y = 1.87x - 190.5 y = 1.87x - 190.5
-100 R = 0.992 -100 R = 0.992

y = 1.64x - 238.18 y = 1.64x - 238.18

-150 R = 0.997
-150 R = 0.997

-200 -200

-250 -250
400-992 g/l LiBr 400-992 g/l LiBr
-300 -300
700-992 g/l LiBr 700-992 g/l LiBr
-350 -350
0 25 50 75 100 0 25 50 75 100
ΔT ΔT
 
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1.E-06 1.E-06

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1.E-09 1.E-09
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1.E-02 1.E-02

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1.E-05 1.E-05

1.E-06 1.E-06

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-330 -330

-340 -340

-350 -350
Eth vs (Ag/AgCl)/mV

Eth vs (Ag/AgCl)/mV
-360 -360

-370 -370

-380 -380

-390 -390

-400 -400

-410 25ºC-25ºC -410 25ºC-25ºC

25ºC-50ºC 25ºC-50ºC
-420 25ºC-75ºC -420 25ºC-75ºC

-430 -430
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
t/h t/h
 
D D
-380 -380

-390 -390

-400 -400
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
-410 -410

-420 -420

-430 -430

-440 -440

-450 -450
25ºC-25ºC 25ºC-25ºC
-460 25ºC-50ºC
-460 25ºC-50ºC
25ºC-75ºC 25ºC-75ºC
-470 -470
25ºC-100ºC 25ºC-100ºC
-480 -480
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
t/h t/h
 
E E
 
 
 
 
 

   
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-420 -420

-430 -430

-440 -440
Eth vs (Ag/AgCl)/mV

Eth vs (Ag/AgCl)/mV
-450 -450

-460 -460

-470 -470

-480 -480

-490 -490

-500 25ºC-25ºC -500 25ºC-25ºC

25ºC-50ºC 25ºC-50ºC
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25ºC-100ºC 25ºC-100ºC
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0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
t/h t/h
 
F F

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75ºC-100ºC 75ºC-100ºC
75ºC-125ºC 75ºC-125ºC
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Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
-470 -470

-490 -490

-510 -510

-530 -530

-550 -550
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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400 g/l LiBr 400 g/l LiBr
700 g/l LiBr 700 g/l LiBr
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1080 g/l LiBr 1080 g/l LiBr
Eth vs (Ag/AgCl)/mV

Eth vs (Ag/AgCl)/mV
y = -0.867x - 338.79 y = -0.867x - 338.79
R = 0.978 R = 0.978
-400 -400

y = -0.417x - 414.15 y = -0.417x - 414.15

-450 R = 0.962 -450 R = 0.962

y = -0.621x - 445.69 y = -0.621x - 445.69

-500 R = 0.932 -500 R = 0.932

y = -0.7283x - 483.87 y = -0.7283x - 483.87

R = 0.893 R = 0.893
-550 -550
0 25 50 75 100 0 25 50 75 100

ΔT/ºC ΔT/ºC
 
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-700 -60  -700 -60 

D -600 Electrodos frío y caliente (AAT)
Electrodo frío (DAT) D -600 Electrodos frío y caliente (AAT)
Electrodo frío (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT)
-50 -50

Ángulo de fase (grados)

Ángulo de fase (grados)

-500  -500 
-40 -40
-400  -400 
2

2
Z''/Ω cm

Z''/Ω cm
-30 -30
-300 -300
-20 -20
-200  -200 
 Electrodo frío (DAT)
-100 -10 Electrodos frío y caliente (AAT)
-100 -10 Electrodos frío y caliente (AAT)
Electrodo frío (DAT)
Electrodo caliente (DAT) Electrodo caliente (DAT)
0 0
0.01
 0.1 1 10 100 1000 10000 100000
0 0
0.01
 0.1 1 10 100 1000 10000 100000
0 100 200 300 400 500 600 700 0 100 200 300 400 500 600 700

Ω cm
Z'/Ω
2  Frecuencia (Hz) Ω cm
Z'/Ω
2  Frecuencia (Hz)

 
-700 -70 -700 -70
E -600 Electrodo frío (AAT)
Electrodo caliente (AAT)
 Electrodo frío (AAT) E -600 Electrodo frío (AAT)
Electrodo caliente (AAT)
 Electrodo frío (AAT)
-60 Electrodo caliente (AAT) -60 Electrodo caliente (AAT)
Electrodo frío (DAT) Electrodo frío (DAT)
Electrodo caliente (DAT)  Electrodo frío (DAT)
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Ángulo de fase (grados)

Ángulo de fase (grados)

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-500 -50 -500 -50
 
Z''/Ω cm2

Z''/Ω cm2
-400 -40 -400 -40
 
-300 -30 -300 -30

-200
 -200

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-100  -100 
-10 -10

0 0
 0 0

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 0.1 1 10 100 1000 10000 100000 0.01
 0.1 1 10 100 1000 10000 100000

Ω cm2
Z'/Ω Frecuencia (Hz) Ω cm2
Z'/Ω Frecuencia (Hz)
 
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Ángulo de fase (grados)

Ángulo de fase (grados)

Electrodo caliente (DAT) Electrodo caliente (DAT)
-500 -50  -500 -50 
F F
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-400 Electrodo caliente (DAT) -400 Electrodo caliente (DAT)

Ángulo de fase (grados)

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-50 -50

-300  -300 
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-40 -40

-30
 -30

-200 -200

-20  -20 
-100 -100
  Electrodo
Electrodos frío y caliente (AAT) Electrodos frío y caliente (AAT)
-10 -10
Electrodo frío (DAT) frío (DAT)
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Ω cm2 Ω cm2
-500
Z'/Ω
-70
 Frecuencia (Hz)
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-20
 -20

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Ω cm2
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Ω cm
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-50 -50
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-750 Electrodo caliente (DAT)
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Ángulo de fase (grados)

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-50 -50
-600 -600
-40
 -40

2

2
Z''/Ω cm

Z''/Ω cm
-450 -450

 
-30 -30
-300 -300
-20 -20

-150 -10
 Electrodos frío y caliente (AAT) -150 -10
 Electrodos frío y caliente (AAT)
Electrodo frío (DAT) Electrodo frío (DAT)

0 0  Electrodo caliente (DAT)

0 0  Electrodo caliente (DAT)

0 150 300 450 600 750 900 0.01 0.1 1 10 100 1000 10000 100000 0 150 300 450 600 750 900 0.01 0.1 1 10 100 1000 10000 100000

2  2 
Ω cm
Z'/Ω Frecuencia (Hz) Ω cm
Z'/Ω Frecuencia (Hz)

E
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Electrodo frío (AAT)
-70
 E
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Electrodo frío (AAT)
-70

Electrodo caliente (AAT) Electrodo caliente (AAT)
-750 Electrodo frío (DAT) -60 -750 Electrodo frío (DAT) -60
Electrodo caliente (DAT)  Electrodo caliente (DAT) 
Ángulo de fase (grados)

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-50 -50
-600 -600
2

2
 
Ω cm

Ω cm
-40 -40
Z''/Ω

Z''/Ω
-450 -450
-30  -30 
-300 -300
-20
 -20

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-10 Electrodo caliente (AAT) -10 Electrodo caliente (AAT)

0
 Electrodo frío (DAT)
Electrodo caliente (DAT) 0
 Electrodo frío (DAT)
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0 150 300 450 600 750 900 0.01
 0.1 1 10 100 1000 10000 100000 0 150 300 450 600 750 900 0.01
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Ω cm2
Z'/Ω Frecuencia (Hz) Ω cm2
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-900 -70  -900 -70 
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-50 -50
 
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2 2
Ω cm
Z'/Ω Frecuencia (Hz) Ω cm
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Ω cm
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50 50
25ºC-25ºC - 400 g/l LiBr 25ºC-25ºC - 400 g/l LiBr
D 25ºC-50ºC - 400 g/l LiBr
25ºC-75ºC - 400 g/l LiBr
25ºC-25ºC - 400-992 g/l LiBr
25 25ºC-50ºC - 400-992 g/l LiBr
25ºC-75ºC - 400-992 g/l LiBr
-2
D 25ºC-50ºC - 400 g/l LiBr
25ºC-75ºC - 400 g/l LiBr
25ºC-25ºC - 400-992 g/l LiBr
25 25ºC-50ºC - 400-992 g/l LiBr
25ºC-75ºC - 400-992 g/l LiBr

-2
0 0
ithm/μA cm

ithm/μA cm
-25 -25

-50 -50

-75 -75
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
t/h t/h
 

100 100
E 25ºC-25ºC - 700 g/l LiBr
25ºC-50ºC - 700 g/l LiBr
75 25ºC-75ºC - 700 g/l LiBr
25ºC-100ºC - 700 g/l LiBr
25ºC-25ºC - 700-992 g/l LiBr
50 25ºC-50ºC - 700-992 g/l LiBr
25ºC-75ºC - 700-992 g/l LiBr
25ºC-100ºC - 700-992 g/l LiBr
25
-2
E 25ºC-25ºC - 700 g/l LiBr
25ºC-50ºC - 700 g/l LiBr
75 25ºC-75ºC - 700 g/l LiBr
25ºC-100ºC - 700 g/l LiBr
25ºC-25ºC - 700-992 g/l LiBr
50 25ºC-50ºC - 700-992 g/l LiBr
25ºC-75ºC - 700-992 g/l LiBr
25ºC-100ºC - 700-992 g/l LiBr
25

-2
0 0
ithm/μA cm

ithm/μA cm
-25 -25

-50 -50

-75 -75

-100 -100

-125 -125

-150 -150
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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-320 -320

D -340 D -340

-360 -360
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
-380 -380

-400 -400

-420 -420

-440 -440
25ºC-25ºC - 400 g/l LiBr 25ºC-25ºC - 400 g/l LiBr
-460 25ºC-50ºC - 400 g/l LiBr -460 25ºC-50ºC - 400 g/l LiBr
25ºC-75ºC - 400 g/l LiBr 25ºC-75ºC - 400 g/l LiBr
25ºC-25ºC - 400-992 g/l LiBr 25ºC-25ºC - 400-992 g/l LiBr
-480 25ºC-50ºC - 400-992 g/l LiBr -480 25ºC-50ºC - 400-992 g/l LiBr
25ºC-75ºC - 400-992 g/l LiBr 25ºC-75ºC - 400-992 g/l LiBr
-500 -500
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
t/h t/h
 

-370 -370
E E
-390 -390

-410 -410
Ethm vs (Ag/AgCl)/mV

Ethm vs (Ag/AgCl)/mV
-430 -430

-450 -450

-470 -470

-490 -490

-510 -510
25ºC-25ºC - 700 g/l LiBr 25ºC-25ºC - 700 g/l LiBr
25ºC-50ºC - 700 g/l LiBr 25ºC-50ºC - 700 g/l LiBr
-530 25ºC-75ºC - 700 g/l LiBr -530 25ºC-75ºC - 700 g/l LiBr
25ºC-100ºC - 700 g/l LiBr 25ºC-100ºC - 700 g/l LiBr
25ºC-25ºC - 700-992 g/l LiBr 25ºC-25ºC - 700-992 g/l LiBr
25ºC-50ºC - 700-992 g/l LiBr 25ºC-50ºC - 700-992 g/l LiBr
-550 25ºC-75ºC - 700-992 g/l LiBr -550 25ºC-75ºC - 700-992 g/l LiBr
25ºC-100ºC - 700-992 g/l LiBr 25ºC-100ºC - 700-992 g/l LiBr
-570 -570
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
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-200 -200
400-992 g/l LiBr 400-992 g/l LiBr
-250 700-992 g/l LiBr -250 700-992 g/l LiBr

-300 -300
Eth vs (Ag/AgCl)/mV

Eth vs (Ag/AgCl)/mV
-350 -350

-400 -400

y = -0.9237x - 384.47 y = -0.9237x - 384.47

-450 R2 = 0.976
-450 R2 = 0.976

-500 -500
y = -0.9244x - 428.32 y = -0.9244x - 428.32
2 2
R = 0.994 R = 0.994
-550 -550

-600 -600
0 25 50 75 100 0 25 50 75 100
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1.E-03 1.E-03
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1.E-04 1.E-04

1.E-05 1.E-05

1.E-06 1.E-06
1.15 M 1.15 M
1.E-07 4.61 M 1.E-07 4.61 M
8.06 M 8.06 M
1.E-08 11.42 M 1.E-08 11.42 M

1.E-09 1.E-09
-0.9 -0.6 -0.3 0 0.3 0.6 0.9 1.2 -0.9 -0.6 -0.3 0 0.3 0.6 0.9 1.2
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1.E-06 1.E-06
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1.E-09 1.E-09
-0.9 -0.6 -0.3 0 0.3 0.6 0.9 1.2 -0.9 -0.6 -0.3 0 0.3 0.6 0.9 1.2
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1.E-09 1.E-09
-0.9 -0.6 -0.3 0 0.3 0.6 0.9 1.2 -0.9 -0.6 -0.3 0 0.3 0.6 0.9 1.2
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1.E-08 1.E-08

1.E-09 1.E-09
-0.9 -0.6 -0.3 0 0.3 0.6 0.9 1.2 -0.9 -0.6 -0.3 0 0.3 0.6 0.9 1.2
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0.3 0.3

0.2 25º C 0.2 25º C

50º C 50º C
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1.4 1.4

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1 1
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0.6 0.6
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100 ºC 100 ºC
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 & =  ([ = / )   & =  ([ = / ) 
 
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10  10 10  10
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2
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2
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Ω cm

Ω cm

Ω cm
Ω cm

Ω cm

Ω cm

Ω cm
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 0.01 0.01
 0.01

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 0.001 0.001
 0.001

 
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Ángulo de fase/grados

Ángulo de fase/grados
-70 -70
-500  -500 
2

2
Z''/kΩ cm

Z''/kΩ cm
-60 -60
-400 -400
-50  -50 
-300 -40 -300 -40
-30
 -30

-200 Experimental 25º C
-200 Experimental 25º C
Experimental 25º C
Circuito Fig. 6.1a
-20  Circuito Fig. 6.1a
Experimental 25º C
Circuito Fig. 6.1a
-20  Circuito Fig. 6.1a
-100 Circuito Fig. 6.1b (ec. 6.26) -10 Circuito Fig. 6.1b (ec. 6.26) -100 Circuito Fig. 6.1b (ec. 6.26) -10 Circuito Fig. 6.1b (ec. 6.26)

0  0 
Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30)
0 0
0 100 200 300 400 500 600 700 0.01
 0.1 1 10 100 1000 10000 100000 0 100 200 300 400 500 600 700 0.01
 0.1 1 10 100 1000 10000 100000
Ω cm
Z'/kΩ
2
D Frecuencia/Hz Ω cm
Z'/kΩ
2
D Frecuencia/Hz
-250  -250 
-90 -90
-80  -80 
Ángulo de fase/grados

Ángulo de fase/grados
-200 -200
-70 -70
 
2

2
Z''/kΩ cm

Z''/kΩ cm
-60 -60
-150 -150
-50  -50 
-100 -40 -100 -40
-30
 -30

-50
Experimental 50º C
Circuito Fig. 6.1a
-20  Experimental 50º C
Circuito Fig. 6.1a
-50
Experimental 50º C
Circuito Fig. 6.1a
-20  Experimental 50º C
Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26) -10 Circuito Fig. 6.1b (ec. 6.26) Circuito Fig. 6.1b (ec. 6.26) -10 Circuito Fig. 6.1b (ec. 6.26)

0
Circuito Fig. 6.1b (ec. 6.30)
0
 Circuito Fig. 6.1b (ec. 6.30)
0
Circuito Fig. 6.1b (ec. 6.30)
0
 Circuito Fig. 6.1b (ec. 6.30)

0 50 100 150 200 250 

0.01 0.1 1 10 100 1000 10000 100000 0 50 100 150 200 250 
0.01 0.1 1 10 100 1000 10000 100000
2 2
Ω cm
Z'/kΩ E
Frecuencia/Hz Ω cm
Z'/kΩ E
Frecuencia/Hz
-200
 -200

-90 -90
-80  -80 
Ángulo de fase/grados

Ángulo de fase/grados
-150 -70
 -150 -70

2

2
Z''/kΩ cm

Z''/kΩ cm
-60 -60
 -50  -50
-100 -100
 -40
 -40
-30 -30
 -50 Experimental 75º C -20 Experimental 75º C  -50 Experimental 75º C -20 Experimental 75º C
Circuito Fig. 6.1a Circuito Fig. 6.1a Circuito Fig. 6.1a Circuito Fig. 6.1a
-10 -10
 
Circuito Fig. 6.1b (ec. 6.26) Circuito Fig. 6.1b (ec. 6.26) Circuito Fig. 6.1b (ec. 6.26) Circuito Fig. 6.1b (ec. 6.26)
Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30)
0 0 0 0
 0 50 100 150 200 0.01 0.1 1 10 100 1000 10000 100000  0 50 100 150 200 0.01 0.1 1 10 100 1000 10000 100000
Ω cm
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-700 -90 -700 -90
-600
 -80 -600
 -80

Ángulo de fase/grados

Ángulo de fase/grados
 
-500
-70
 D -500

-70
D
Z''/kΩ cm2

Z''/kΩ cm2
-60 -60
-400 -50  -400 -50 
-300 -40  -300 -40 
-200 -30  -200 -30 
 Experimental  Experimental
Experimental 25º C -20 25º C Experimental 25º C -20 25º C
Circuito Fig. 6.1a Circuito Fig. 6.1a Circuito Fig. 6.1a Circuito Fig. 6.1a
-100 -100
Circuito Fig. 6.1b (ec. 6.26) -10 Circuito Fig. 6.1b (ec. 6.26) Circuito Fig. 6.1b (ec. 6.26) -10 Circuito Fig. 6.1b (ec. 6.26)
0
Circuito Fig. 6.1b (ec. 6.30)  Circuito Fig. 6.1b (ec. 6.30) 0
Circuito Fig. 6.1b (ec. 6.30)  Circuito Fig. 6.1b (ec. 6.30)
0 0
0 100 200 300 400 500 600 700 0.01  0.1 1 10 100 1000 10000 100000 0 100 200 300 400 500 600 700 0.01  0.1 1 10 100 1000 10000 100000
Z'/kΩ Ω cm
2  Frecuencia/Hz Z'/kΩ Ω cm
2  Frecuencia/Hz
-500  -500 
-90 -90
-80
 -80

Ángulo de fase/grados

Ángulo de fase/grados
-400  -400 
-70
E -70
E
Z''/kΩ cm2

Z''/kΩ cm2
-60  -60 
-300 -300
-50  -50 
-200 -40  -200 -40 
Experimental 50º C
-30  Experimental 50º C
-30 
-100 Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
-20
 Experimental 50º C
Circuito Fig. 6.1a
-100 Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
-20
 Experimental 50º C
Circuito Fig. 6.1a
-10 Circuito Fig. 6.1b (ec. 6.26) -10 Circuito Fig. 6.1b (ec. 6.26)
0
Circuito Fig. 6.1b (ec. 6.30)
0
 Circuito Fig. 6.1b (ec. 6.30)
0
Circuito Fig. 6.1b (ec. 6.30)
0
 Circuito Fig. 6.1b (ec. 6.30)

0 100 200 300 400 500 0.01  0.1 1 10 100 1000 10000 100000 0 100 200 300 400 500 0.01  0.1 1 10 100 1000 10000 100000
Z'/kΩ Ω cm
2  Frecuencia/Hz Z'/kΩ Ω cm
2  Frecuencia/Hz
-250 -90
 -250 -90

-80
 -80

Ángulo de fase/grados

Ángulo de fase/grados
-200  -200 
-70
F -70
F
Z''/kΩ cm2

Z''/kΩ cm2
-150
-60  -150
-60 
-50  -50 
-100 -40  -100 -40 
Experimental 75º C
-30
 Experimental 75º C Experimental 75º C
-30
 Experimental 75º C
-50 Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
-20
 Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
-50 Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
-20
 Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
-10 -10
0
Circuito Fig. 6.1b (ec. 6.30)
0
 Circuito Fig. 6.1b (ec. 6.30)
0
Circuito Fig. 6.1b (ec. 6.30)
0
 Circuito Fig. 6.1b (ec. 6.30)

0 50 100 150 200 250 0.01  0.1 1 10 100 1000 10000 100000 0 50 100 150 200 250 0.01  0.1 1 10 100 1000 10000 100000
Z'/kΩ Ω cm
2  Frecuencia/Hz Z'/kΩ Ω cm
2  Frecuencia/Hz
-150 -90
 -150 -90

-80  -80 
Ángulo de fase/grados

Ángulo de fase/grados
 
-70
G -70
G
Z''/kΩ cm2

Z''/kΩ cm2
-100 -60  -100 -60 
-50  -50 
-40  -40 
-50 -50
Experimental 100º C
-30
 Experimental 100º C Experimental 100º C
-30
 Experimental 100º C
-20 -20
Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
 Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
 Circuito Fig. 6.1a
Circuito Fig. 6.1b (ec. 6.26)
-10 -10
0
Circuito Fig. 6.1b (ec. 6.30)
0
 Circuito Fig. 6.1b (ec. 6.30)
0
Circuito Fig. 6.1b (ec. 6.30)
0
 Circuito Fig. 6.1b (ec. 6.30)

0 50 100 150 0.01  0.1 1 10 100 1000 10000 100000 0 50 100 150 0.01  0.1 1 10 100 1000 10000 100000
Z'/kΩ Ω cm
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 Frecuencia/Hz Z'/kΩ Ω cm
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Circuito Fig. 6.1a
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Circuito Fig. 6.1a
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Circuito Fig. 6.1a
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Circuito Fig. 6.1a
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Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30)
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Z'/kΩ Ω cm 2  Frecuencia/Hz Z'/kΩ Ω cm 2  Frecuencia/Hz
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Ángulo de fase/grados

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Circuito Fig. 6.1a -20  Experimental 50º C
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Experimental 50º C
Circuito Fig. 6.1a -20  Experimental 50º C
Circuito Fig. 6.1a
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Ángulo de fase/grados

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Circuito Fig. 6.1a -20  Experimental 75º C
Circuito Fig. 6.1a Circuito Fig. 6.1a
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Circuito Fig. 6.1b (ec. 6.30) Circuito Fig. 6.1b (ec. 6.30)
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Circuito Fig. 6.1b (ec. 6.30) -10  Circuito Fig. 6.1b (ec. 6.26)
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0.8 0.8
1000  0.7
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0.5 0.5
600  0.4
600  0.4
400  25º C
0.3 400  25º C
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200  75º C
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 E vs (Ag/AgCl)/mV E vs (Ag/AgCl)/mV  E vs (Ag/AgCl)/mV E vs (Ag/AgCl)/mV
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600
 0.7 600
 0.7

0.6 0.6
500
 500

0.5 0.5
400
 400

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0.4 0.4
300
 0.3
300
 0.3
200  25º C 0.2
200  25º C 0.2
50º C 50º C
100  75º C 0.1 75º C 100  75º C 0.1 75º C
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 E vs (Ag/AgCl)/mV
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 1400
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600 600
 400
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 12  12

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C1 /μF cm-2

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 8  8

 6  6

 4  4
25º C 25º C
 2 50º C  2 50º C
75º C 75º C
 0  0
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 16 E  16 E
 14  14
12 12
 
C1 /μF cm-2

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8 8
 6  6
 4
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50º C
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50º C

 
2 75º C 2 75º C
100º C 100º C
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15 15
 
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100º C 100º C
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3500  9 3500  9
50º C 50º C
3000  8
75º C 3000  8
75º C
7 7
2500
 6
2500
 6
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2000 2000
 5  5
1500 4 1500 4
 3
 3
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500
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75º C
2
500
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2
1 1
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 E vs (Ag/AgCl)/mV
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 E vs (Ag/AgCl)/mV
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1800 3 1800 3
1600
 75º C
1600
 75º C
2.5 100º C 2.5 100º C
1400  1400 
1200 2 1200 2
 
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RW /kΩ cm2

RW /kΩ cm2
1000 1000
1.5 1.5
800  800 
600 1 600 1

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25º C
400 50º C 400 50º C
0.5 0.5
200 
75º C
100º C
200 
75º C
100º C
0 0 0 0
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 8
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3000 3000

25º C
50º C
7 
25º C
50º C
7
2500 2500
75º C 75º C

100º C
6

100º C
6
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2000 2000
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5 5
 
1500 4 1500 4
 3  3
1000 1000
 2  2
500 500
1 100º C 1 100º C
 
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600 600
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200 200
 
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 300
 300
 
200 200
 
100 100
 75º C  75º C
100º C 100º C
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 500
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 400
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 200  200

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250 250
 
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150 150
 
100 100
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 0
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 -350 -250 -150 -50 50 150  -350 -250 -150 -50 50 150
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70 70
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50 50
 
C2 /μF cm-2

C2 /μF cm-2
40 40
 
 30  30

 20  20

 10 75º C  10 75º C
100º C 100º C
 0  0
-350 -250 -150 -50 50 150 -350 -250 -150 -50 50 150
 
E vs (Ag/AgCl)/mV E vs (Ag/AgCl)/mV
 
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 60  60

 50  50
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C2 /μF cm-2
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 30  30

 20  20
 10
 10
100º C 100º C
 
0 0
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E vs (Ag/AgCl)/mV 
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