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a r t i c l e i n f o a b s t r a c t
Article history: Because energy efficiency in buildings will be evaluated not only based upon heating demand, but also
Received 14 January 2011 according to the primary energy demand, the ecological properties of the building materials for the
Received in revised form 5 May 2011 whole assessment has become essential. The demand for green building materials is rising sharply, espe-
Accepted 12 June 2011
cially insulating materials from renewable resources. The application of natural materials has become
increasingly important as a consequence of the increasing need to conserve energy, use natural materi-
Keywords:
als, incorporate architecture and construction into sustainable development processes, and the recently
Thermal insulating material
promulgated discussions on appropriate disposal of used insulation materials such as polystyrene (EPS).
Jute
Flax
Due to the fact that natural materials are more sensitive to moisture, decomposition factors such as
Hemp temperature, material moisture content, attacks by microorganisms, and possible decomposition of the
material or shorter durability, it is necessary to evaluate the degradation rate of built-in materials and
also determine their real in situ hygrothermal properties according to their moisture content, and volume
changes.
This paper describes the results of a research project carried out at the Vienna University of Technology
and Brno University of Technology. The objective is to use jute, flax, and hemp to develop a new insulating
material from renewable resources with comparable building physics and mechanical properties to com-
monly used insulations materials. All input components are varied in the tests. The impact of moisture
content changes in relation to the rate of change of other properties was the focus of the investigation.
The tests results show that the correct combination of natural materials is absolutely comparable with
convectional materials.
© 2011 Elsevier B.V. All rights reserved.
0378-7788/$ – see front matter © 2011 Elsevier B.V. All rights reserved.
doi:10.1016/j.enbuild.2011.06.012
A. Korjenic et al. / Energy and Buildings 43 (2011) 2518–2523 2519
hemp concrete can decrease the daily indoor relative humidity vari- sibility of rapid drying must be ensured when materials get wet.
ations and reduction of 45% in energy consumption can be reached Problems with moisture in walls should not occur if the building is
compared to cellular concrete. Also, systematic measurements of properly designed.
several important variables in a built house with straw bale walls Thermal insulating properties deteriorate due to humidity and
in Germany shows excellent properties to provide excellent living moisture. The thermal conductivity coefficient of a damp material
conditions [5]. is defined by the thermal conductivity of the fixed matrix, fluid
By using natural building materials in structures, human health phases, gas phases and their quantities, phase variations and spa-
can also be positively influenced [6]. Natural building materials reg- tial arrangement of the individual phases. The thermal conductivity
ulate internal air humidity well and their characteristic odor acts coefficient is generally increasing with higher humidity. A very
on the human psyche beneficially. International research focusing high open porosity value has a dominant influence on thermal and
on studying the effects of buildings on human health studies the moisture behaviour of organic insulating materials, and is a very
relationship between psyche and building material odors. It takes important factor of natural thermal insulating materials.
several trends; we rank the following among the most important Finally, poor fire resistance ranks among the negative proper-
ones: ties of natural building materials. However, fire resistance can be
effectively improved by fire retardants and by building these nat-
- IAP (Indoor Air Pollution) deals with negative health effects of ural materials into structures with fireproof finishings (plaster or
harmful physical, chemical and biological substances, facing).
- SBS (Sick Building Syndrome)- deals with the negative influence
of the indoor environment on human health without demonstra-
ble origin and continuity, 3. Heat and moisture transfer in a porous environment
• natural fibres (jute, flax, technical hemp), • The determination of bulk density was carried out on test
• shives,
specimens dried at 105 ◦ C by the gravimetric method. Exact
• binder (bicomponent fibres).
dimensions of test specimens were measured with accuracy to
0.1 mm. The weight was determined using a laboratory balance
In Fig. 1, the hemp fibres with bicomponent fibres is pictured. with 0.01 g accuracy. The determination of bulk density was car-
Table 1 indicates individual percentages of individual compo- ried out according to EN 1602 [11].
nents in the six specimen sets. The dosing of different materials • Determination of mechanical properties
was controlled by volume with a given density.
Table 1
Percentages of various components in the test sets.
1 Jute 68 20 12
2 Flax 68 20 12
3 Technical hemp 48 20 32
4 Technical hemp 64 20 16
5 Technical hemp 48 20 32
6 Technical hemp 64 20 16 Fig. 2. Testing samples.
A. Korjenic et al. / Energy and Buildings 43 (2011) 2518–2523 2521
Fig. 3. Device for measuring the thermal conductivity, Holometrix Lambda 2300.
in the climatic chamber at Faculty of Building in Brno at a tem-
◦ The stress at 10% deformation was determined on test spec- perature of 23 ◦ C and relative humidity of 93% and in compliance
imens 200 mm × 200 mm slabs. The test was carried out with EN 12086 “Thermal insulating products for application on
according to EN 826 “Thermal insulating products for building building industry – determination of water vapour transmission
applications – Compression test”. properties” [14].
During the determination of mechanical properties, the
test specimens were loaded by test equipment (a pressing The absorption properties were determined using test specimens
machine). The applied pressure and related proportional defor- at an ambient temperature of 23 ◦ C and relative humidity in the
mation of the test specimen was read at specific intervals for range from 0% to 92%. The values measured were used for plotting
the purpose of plotting the stress–strain diagram. the absorption isotherms represented in Diagram 3. Knowledge of
the absorption properties is crucial for determining the moisture
F10 content in the material after its used for building.
10 = 103 · (1)
A0
F10 is the force corresponding to 10% of compressive strain [N]; 6. Measurement results and discussion
A0 is the initial cross-section of test specimen [mm2 ].
◦ The tensile strength perpendicular to the plane of the slab was Test specimens of organic thermal insulating materials were
determined on 200 mm × 200 mm slab test specimens. The test subject to individual tests as presented in Section 5.
was conducted conforming to EN 1607 “Thermal insulating
products for building applications – determination of tensile 6.1. Determination of physical and mechanical properties
strength perpendicular to faces”.
The test specimens were fixed between two stiff boards and The resulting measurements of physical and mechanical prop-
installed in the test equipment to determine the tensile test erties of individual test specimen sets are presented in Table 2.
and they were subsequently pulled apart from each other with The data acquired from the measurements were used as a resource
a given velocity. The maximum tensile force was registered and for a part of further research work, i.e. the assessment of heat
the tensile strength of the test sample was calculated. and moisture propagation in engineering structures and materials
using calculation software.
Fm Fm
mt = = (2)
A l×b • Bulk density values of individual test specimen sets were within
Fm is the maximum tensile force [kN]; A is the sectional area the range of 26.1–33.1 kg m−3 . The value of 82.1 kg m−3 , which
[m2 ]; l, b is the length, test specimen width [m] is significantly higher for test specimens in set 6, was caused by
• The determination of the thermal conductivity coefficient was stronger consolidation of input raw materials.
carried out in a steady state using the slab method. Measure- • The most favourable thermal conductivity coefficient was deter-
ments were made using the Lambda 2300 measuring device, by mined in specimen set 6 from hemp, the average thickness of
Holometrix Micromet Inc., USA, operating on the principle of the which was 40.2 mm and the average bulk volume was 82.1 mm.
stationary slab method at a mean temperature of +10 ◦ C and tem- • The diffusion resistance factor in individual sets varied in the
perature gradient of 10 K. The measuring instrument is presented range of 2.1–4. The minimum diffusion resistance was deter-
in Fig. 3. mined in specimen set 1 made of flax.
Test specimens – 300 mm × 300 mm slabs – were dried at 65 ◦ C • As it is apparent from the above given tabular values, the stress
prior to testing and were then tested at 105 ◦ C. The thermal con- at 10% deformation and the tensile stress perpendicular to slab
ductivity coefficient was determined according to ISO 8301 [12]. faces that the hemp insulation made obtain very good mechani-
Measurements were taken using the device operating on the sta- cal properties relative to their bulk densities. The test specimen
tionary slab principle at the mean temperature of +10 ◦ C and sets made of natural raw material resources (jute, flax) reached
temperature gradient of 10 K [13]. significantly lower values of tensile strength perpendicular to the
faces of the slab.
T
q = − · (3)
x
6.2. Determination of balanced humidity absorption
q is the heat flux density [W m−2 ]; is the thermal conductivity
[W m−1 K−1 ]; T/x is the temperature gradient [K m−1 ]. The moisture behaviour of newly developed materials was
• The water vapour permeability was determined using 100 mm assessed based on the test results. Frequent moisture formation in
diameter circular test specimens (Fig. 4). The test was carried out buildings may result in faults; the increased moisture on wall and
2522 A. Korjenic et al. / Energy and Buildings 43 (2011) 2518–2523
Table 2
Physical and mechanical properties of investigated samples.
Set of samples Thickness Density Thermal Factor of diffuse Tension at 10% Tensile strength
[mm] [kg m−3 ] conductivity, dry resistance [–] deformation [kPa] [kPa]
[W m−1 K−1 ]
6.3. Determination of the moisture dependence of whereas Fm represents the moisture conversion factor:
thermal-moisture characteristics
Fm = efu (u1 −u2 ) (5)
In order to determine the moisture dependence of thermal
conductivity coefficient values for individual test specimens, test where u is the mass moisture [kg kg−1 ]; fu is the conversion factor
specimens were measured with different moisture contents within for mass moisture [kg kg−1 ],
the range of detected absorption moistures (see above). The defined According to EN ISO 10456, Tab. 4, the conversion coefficient for
amount of moisture was always installed in the test specimens mass moistures fu = 0.5 kg kg−1 is also tabulated.
before the measurement. Particularly, there were several moisture Based on the measured values a back-calculation of coefficient
levels, from 0% to 14%. The specimens got desiccated or moistened for mass moistures f u for function was performed (6). The results
so that their moisture approximates to the values of the selected are presented in Table 3 and Fig. 7.
moisture as much as possible. Subsequently, the specimens were The comparison of moisture dependence of thermal conduc-
wrapped in foil in order to prevent the moisture from escaping. tivity for “Set of samples 1 between measured, simulated, and
The specimens were weighed before and after the measurements in standard values is shown in Fig. 8.
order to compute the change of moisture during the measurement.
The test results are presented in Fig. 6.
Fig. 5. Illustration of stable balanced moisture absorption properties’ behaviour for Fig. 6. The moisture dependence of thermal conductivity coefficient values in indi-
individual test specimens at 23 ◦ C. vidual test specimens.
A. Korjenic et al. / Energy and Buildings 43 (2011) 2518–2523 2523
Acknowledgements
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With respect to the development of science and technology, it
can be said that thermal insulations made from natural raw mate-