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Indian Standard
METHOD FOR DETERMINATION OF WAX
CONTENT IN BITUMEN—SPECIFICATION
(First Revision)
ICS 75.140
GBIS2003
J(/niimy 2003
Price Group 4
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Bitumen Tar and Their Products Sectional Committee, PCD 6
FOREWORD
This Indian Standard (First Revision) was adopted by the Bureau of Indian Standards, after the draft finalized by
the Bitumen Tar and Their Products Sectional Committee had been approved by the Petroleum, Coal and Related
Products Division Council.
This standard was published in 1983, which was largely based on UOP 46-64. Since the present method is having
the following disadvantages the Committee decided to revise the standard to align the same with DIN 52015:1980
‘Determination of paraffin wax content in bitumen’ in order to over come the disadvantages:
a) The method is not specific to ‘Paraffin wax content’ only but specifies the wax content which includes wax
and micro-crystalline wax,
b) The method does not mention the purity of ‘fullers earth’,
c) There is no mention of ‘Reproducibility’ in the method,
d) Fullers earth having the particle size within the range 10-35 p, is not available indigenously,
e) There is no mention about the availability of fullers earth,
f) The sieves required to check the particle size of fullers earth are not available indigenously, and
g) The wax content value varies with the quality of fullers earth.
The composition of the Committee responsible for formulation of this standard is given in Annex A.
In reporting the results of a test or analysis made in accordance with this standard, if the final value, observed or
calculated, is to be rounded off, it shall be done in accordance with IS 2: 1960 ‘Rules for rounding off numerical
values (revised)’.
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1S 10512:2003
Indian Standard
METHOD FOR DETERMINATION OF WAX
CONTENT IN BITUMEN—SPECIFICATION
(First Revision)
1 SCOPE 4.2 Steam Bath
This standard prescribes a method used for determining 4.3 Heating Cabinet (Oven), for temperature at least
the paraffin wax content of bitumen. The method is 150”C.
applicable to bitumens having paraffin wax with
melting point above 25”C. 4.4 Bunsen Burner
NOTE —Paraffhr waxes include only those hydrocarbons 4.5 Thermometers, having least count at least 0.5°C.
crystal 1izing in an ether/ethanol mixture at temperatures down
to –20”C, obtained by a specified process and having a melting 4.6 Distillation Flask, as shown in Fig. 1, fitted with
point of above 25°C. cork stopper.
334:2002 Glossary of terms relating to 4.12 Test Tube, fitted with ground socket and a wash
bitumen and tar (third revision) bottle head fitted with ground cone (see Fig. 4).
For the purpose of this standard, the definitions given 4.14 Vacuum Pump
in IS 334 shall apply.
4.15 Evaporating Dish
4 APPARATUS NOTE— The apparatus for determining the paratlh wax content
is available with M/s Petrotest Instruments GmbH & Co KG,
4.1 Balance, readable and accurate to+ 0.5 mg. Ludwig-Erhard-Ring 13, D-15827, Dahlewitz.
16*10
30
FIG. 1 DISTILLATION
FLASK
1
. 7.-
1
IS 10512:2003
OPENING
CONNECTOR FOR
FILTER FIASK 2200
,
OPENING FOR
INSERTION OF
WRBO N DIOXIDE
1 \/-&..
OPENING FOR
INSERTION OF
THERMOMETER /
FIG.2 COOLINGBATH
-, *L,...-
7-
IS 10512:2003
GUARD RING
ICE WATER
r- !
TEST TUBE
FlllED WITH
TEST TUBE
SPOUT AND
BORED CORK FITTED WITH
II WASH BOTTLE
STOPPER ::
~’ n < *
FILTRATION
FIG. 4 SCHEMATICDIAGRAMOFFILTRATION
ARRANGEMENT
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IS 10512:2003
4
IS 10512:2003
7 CALCULATION all the three values and repeat the test on two further
test portions.
7.1 For each test portion, calculate the paraffin wax
content, expressed as a percentage by mass, using the 7.4 Express the paraffh wax content as a percentage
following equation: by mass; rounded to the nearest 0.1.
(MBx A’Q 8 PRECAUTION
paraffin wax, percent~= ~MAXMc) x 100
Never evaporate petroleum spirit on naked flame or on
where a hot plate. Steam bath shduld invariably be used.
MA = initial massofbitumen, ing;
9 PRECISION
MB = mass ofdistillate received, ing;
Mc = initial massofdistillate taken up fortest, ing; 9.1 Repeatability
and
IfWo results are obtained by one and the same operator
MD = final mass of paraffin wax, in g.
under repeatability conditions, they are considered to
7.2 If the values measured for both test portions do not be acceptable and in accordance with the specifications
differ by more than 0.3 percent by mass, determine the of this standard if they do not differ by more than 0.3
mean of the two values. Otherwise, carry out a percent by mass.
determination on a third test portion of 25 g and take
the mean of the two values being the closest together. 9.2 Reproducibility
These values, however, shall not differ by more than If two single and independent results are obtained in
0.3 percent by mass. If the first two values are two different laboratories under comparable conditions,
equidistant from the third, specify the third value.
they are considered to be acceptable and in accordance
7.3 If it is not possible to obtain a mean value from with the specifications of this standard if they do not
these three values under the specified conditions, reject differ by more than 1.0 percent by mass.
5
1S 10512:2003
ANNEX A
(Foreword)
COMMITTEE COMPOSITION
Bitumen, Tar and Their Products Sectional Committee, PCD 6
Organization Representative(s)
(Continued on page 7)
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IS 10512:2003
(Confinuedfrom page 6)
Organization Representative(s)
Regional Research Laboratory, Jorhat DRR. C. BARUAH
SIP Limited, Kolkata SHRJT. K. ROY
SHRJS. BHANUSEKHAR (Alternate)
University of Roorkee, Roorkee PROFH..C. MEHNOIRATTA
INS Directorate General SHRJANIANKAR,Director & Head (PCD)
[Representing Director General (Ex-oficio)]
Member Secretary
DR(SHRJMATI) WJAYMALJK
Director (PCD), BIS
Methods of Test for Bitumen Tar and Their Products Subcommittee, PCD 6:1
7
.
Bureau of Indian Sti[ndar(ls
B1S is a statutory institution established under the Bureau of Indian S~undards Act, 1986 to promote harmonious
development of the activities of standardization, marking and quality certification of goods and attending to
connected matters in the country.
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without the prior permission in writing of BIS. This does not preclude the free use, in the course of implementing
ti~cstandard, of necessary details, such as symbols and sizes, type or grade designations. Enquiries relating to
copyright be addressed to the Director (Publication), BIS.
Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed
periodically: a standard a!ong with amendments is reti]rmed when such review indicates that no changes are
needed: if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards
should a.scerli]in that they are in possession of the latest amendments or edition by referring to the latest issue of
‘BIS Ci]t:lloglle’ iind ‘Standards: Monthly Additions’.
This Indian Standard has been developed from Dot: No. PCD 6 (1974).