Beruflich Dokumente
Kultur Dokumente
Wear
journal homepage: www.elsevier.com/locate/wear
a r t i c l e i n f o a b s t r a c t
Article history: The raw materials industry is faced with severe challenges due to ever changing heterogeneous mix-
Received 2 November 2009 tures and thus each industrial comminution system needs to be analyzed one by one. This study is aimed
Received in revised form 14 March 2011 at identifying the most common degradation mechanisms occurring in closed circuit high stress com-
Accepted 25 March 2011
minution equipment such as vertical roller mills. Both a macroscopic and a microscopic analysis of the
Available online 27 April 2011
wear parts has been conducted. A laboratory scale vertical roller mill with a transparent roller/table has
been developed to further understand the material movements during grinding. The development of
Keywords:
a simple wear test apparatus has verified the type of wear mechanism dominating the process. Optical
Vertical roller mills
Quartz
microscopy revealed that strain incompatibility resulted in fracture and decohesion of the carbides below
Wear mechanisms the worn surface. The emphasis of this work are wear related issues and thus detailed rock mechanical
considerations have been omitted and are not within the scope of this study.
© 2011 Elsevier B.V. All rights reserved.
1. Introduction ferent minerals (for instance limestone, clay, quartz) with different
cohesion, particle size distributions (PSD) and hardness properties:
One of the most well known abrasion resistant high chromium Due to the mineralogical differences the power consumption will
alloys is Ni-Hard 4, which has been studied closely as a wear part range between approx. 3 and 11 kWh/t.
material in the mining industry [1]. However, for this study an abra- Due to the advantageous centrifugal forces, the VRMs are nor-
sion resistant heat treated high chromium white cast iron similar to mally operated at 20–40 rpm depending on the VRM size and this
21988/JN/HBW555XCr21 was investigated [2]. The chemical com- will yield a maximum tangential speed of approx. 7 m/s in large
positions of such abrasion resistant wear parts are given in Table 1. VRMs. The table is driven by an electrical motor and the rollers
These high chromium alloys are used in closed circuit dry grinding rotate due to the frictional force established in the grinding bed.
vertical roller mills (VRM) as wear liner on both table and rollers The grinding force is made up of the net weight of the rollers and
(Fig. 1). The heat treatment (hardening and tempering) results in a an additional hydraulic force (Fig. 1). In the VRM, several separation
macro hardness of approx. 750 HV [2]. processes controlled by the air flows will change the mineralogical
composition of the grinding bed.
1.1. Vertical roller mills VRMs are mainly used in the cement and coal industry as a
3-in-1 machine (grinding, separation and drying). However, if labo-
The VRM is a commonly known grinding unit in the cement ratory measurements indicate wear rates significantly above 10 g/t,
industry. The VRM sizes range from approx. 2 to 6 m in table a ball mill (tube mill) will be chosen as the most economical solu-
diameter, and depending on the VRM size, the feed material will tion: Experience shows that wear rates exceeding 10 g/t will result
vary between pebble sized rocks in small VRMs and Ø150 mm in unsatisfying production rates and the maintenance costs will
fragments in large VRMs. The final product will typically be clas- become excessively large. It has been reported that raw material
sified/separated at 12% + 90 m. Contrary to clinker VRMs the VRM wear parts need servicing at intervals between 4 months and
mineralogy of raw materials varies significantly making the pro- 10 years [4].
cess difficult to predict and control. The grinding process is highly
heterogeneous as the raw mix on average is made up of 3 very dif-
2. Roller kinetics
∗ Corresponding author. Fax: +45 36182647. The stresses acting on a towed or driven wheel in loose sand/soil
E-mail address: lje@flsmidth.com (L.R.D. Jensen). has been studied intensively [5–8]. These setups are characterized
0043-1648/$ – see front matter © 2011 Elsevier B.V. All rights reserved.
doi:10.1016/j.wear.2011.03.018
2708 L.R.D. Jensen et al. / Wear 271 (2011) 2707–2719
Table 1
Chemical compositions of abrasion resistant wear part materials. A material similar to 21988/JN/HBW555XCr21 is commonly used in VRMs. G-X 300 CrNiSi 9 5 2 (Ni-Hard
4) is less abrasion resistant than the former [3].
Alloy C Mn Si Cr Mo Ni Cu
Piston
Particle bed
Wear plate
Support
Fig. 5. The main components of the wear test apparatus is a polished wear plate
specimen, a small grinding bed and a piston. First, a force is applied to the bed
by means of a spring and the shown piston. Next, the sample holder is displaced
horizontally for a distance of approx. 20 mm. During this operation the abrasive
particles abrade the surface.
digital video camera was used for recording the bed movements.
Each experiment consists of 1 table revolution: The compaction of
the bed will change the bed properties and further roller passings
will not reflect the correct conditions.
Fig. 3. Experimental VRM with a single transparent roller designed for investigating
the particle bed movement during operation. 3.3. Wear apparatus
Fv
A
Top plate
Metal strip
Bed
Base plate
Fv
B
Fh
h1
C Fv
Fh
h2
Fig. 6. Shear analysis. (A) Shear test assembly. A bed of particles is compressed
between two steel plates and a thin steel strip is used as an indicator to show the
degree of shear. (B) Low pressure situation: The angled strip indicates that internal
shear occurs (interface > bed ). (C) High pressure situation: The particles interlock
and shear occurs in the bed/metal interface (interface < bed ).
Prior to the standard microstructural analysis, the specimens Fig. 7. Theoretical illustration of grinding bed behavior during operation where the
table is driven while the roller is towed resulting in a slip of constant magnitude
were sampled from a large cast segment by means of water jet
[9]. (A) Resultant shear on roller surface where the horizontal -line indicates the
cutting (Section 3.4). Subsequently the specimens were prepared interfacial roller/bed friction factor. (B) Diagram showing approx. pressure and shear
by a traditional preparation method (Struers Discotom, Struers profile on roller surface. (C) Diagram showing approx. pressure and shear profile
Prontopress-2 and Struers TegraSystem with the final step of 1 m on table surface. (D) Resultant shear on table surface where the horizontal -line
diamond). For optical analysis the specimen was etched 1 sec- indicates the interfacial table/bed friction factor.
A B C
50
0
100 100
Nominal speed [%] Nominal speed [%] Friction factor [−]
Fig. 8. Relative grinding bed speeds. (A) In the compression zone, the bed is transported slipless on the table but with slip on the roller. (B) In the last part of the relaxation
zone, the bed is extruded out of the gap resulting in slip on both the table and the roller. On the roller the two slips are superimposed. (C) Using smooth wear parts, the
friction is larger within the grinding bed resulting in shearless grinding.
property is highly dependent on PSD, moisture and cohesion. If the factor is highly dependent on PSD, surface roughness, moisture, etc.
vertical force, F , is at a relatively low setting, the bed height will but as an average estimate it can be set to approx. 0.5.
be h1. When a horizontal force, Fh , is applied to the upper steel If the interfacial friction is assumed to be constant, the tangen-
plate, the steel strip will angle itself and indicate internal shear. tial/radial pressure ratio plotted in a diagram will show where slip
If F is increased, the two steel plates approach further indicating occurs (Fig. 7A and D): Slip will not occur in the entire compressive
increased compression (h2). A horizontal force, Fh , is applied, but zone and the first part of the relaxation zone. However, slip will
compared to the low pressure experiment, this force needs to be of occur in the last part of the relaxation zone just before leaving the
greater intensity. In this high pressure situation only the top plate gap (Fig. 8). The slip occurring in the last part of the relaxation zone
will move horizontally and the metal strip will stay vertical. The can be regarded as extrusion. In the last part of the relaxation zone
increased vertical forces will compress the bed to a solid and fully (where slip is present) the radial pressure has decreased substan-
interlock all particles and objects in the bed. Thus the bed internal tially and it is believed that the extrusion effect will not contribute
friction coefficient is highly pressure dependent. In the high pres- much to the wear.
sure experiment the internal friction has surpassed the metal/bed As mentioned above, the VRM experiences a second type of
interfacial friction. slip which originates from the fact that only the table is driven
and the roller is towed in a grinding bed [5–8]. This slip is con-
5. Experimental VRM analysis stant and acts in one direction only on the entire bed/roller surface
(Fig. 8A). It is believed that this slip will contribute substantially to
5.1. General the wear.
It can thus be concluded that all tangential stresses are trans-
The analysis of the experimental VRM grinding bed movements mitted in the bed/roller and the bed/table interface. Consequently
are in close accordance with the results presented in an earlier no internal shear occurs within the grinding bed between the nip
study [9]. It has been shown that the VRM experiences two types angle and the outlet gap space: The internal friction in the grinding
of slip (Fig. 7): bed is higher than the friction in the interface resulting in excessive
wear (Section 4).
1. Slip at the gap outlet based on classical flat rolling theory and
verified in roller presses [9].
5.2. Rolling point
2. Constant slip because the table is driven and the roller is towed
in a grinding bed. This slip acts on the entire bed/roller surface.
The rolling point is a point where the table tangential speed
vector and the roller tangential speed vector have the same magni-
The slip originating from the compression of the grinding bed tude (Fig. 9). In an ideal system the rolling point will always settle in
needs to be treated without the superimposed constant slip (simi- the center of gravity of the high pressure zone. Experimentally, the
lar to a situation where both the table and roller is driven): The slip rolling point is determined by simultaneously counting the revolu-
in the inlet zone (where particles are rearranged and air is squeezed tions of both the roller and the table for a predetermined amount
out) is evident but has no effect due to negligible radial (normal) of time or radians. The following equation is used:
pressures. As soon as the particles reach the nip angle, the radial
pressure will rapidly increase to a maximum value. In this compres- N1 r1 = N2 r2
sive zone the tangential stresses on the roller counteract the rolling
direction (Fig. 7B). If sufficient force has been applied to the roller, a
where N1 is the number of revolutions of the table, r1 is the radius
relaxation zone emerges and the grinding bed acts elastically with
to the common velocity vector (unknown), N2 is the number of
a hysteresis loss. After the smallest gap space, the radial pressure
revolutions of the roller and r2 is the total radius of the roller.
rapidly decreases and at the same time the tangential stress shifts
In a VRM the high pressure zone forms towards the outer periph-
and acts in the rotational direction.
ery of the table due to the sloped grinding bed (Figs. 10 and 11).
Slip will only occur if the tangential stress exceeds the bed/roller
As discussed in Section 5.1 a constant slip occurs when operating
interfacial friction. Thus the tangential/radial stress ratio has to
VRMs. This statement has been verified to be correct, and as a result
exceed the interfacial friction coefficient:
the roller rotates slower positioning the rolling point closer to the
center of the VRM. Mostly, the rolling point is positioned right at
=
the edge of the high pressure grinding zone (Fig. 11). This conflicts
where is the tangential stress (shear stress), is the radial stress with the classical belief on rolling point positions on a VRM grinding
(normal stress) and is the friction factor. The interfacial friction table (Fig. 9).
2712 L.R.D. Jensen et al. / Wear 271 (2011) 2707–2719
OD ID
Fig. 11. Location of high pressure grinding zone with rolling point indicated as a
Fig. 9. Classical interpretation of rolling point. The cylindrical roller involves a set red line. It is observed that the rolling point is positioned off center very close to the
of relative velocity vectors which will govern shear under certain conditions. In this edge of the high pressure zone. (For interpretation of the references to color in this
particular case the rolling point is shown as being in the middle of the roller. In most figure legend, the reader is referred to the web version of the article.)
cases however, the rolling point will settle towards the outer diameter (OD) of the
roller due to the geometric bed configuration.
CL
Roller 90
Pressure profile
Material flow
Rolling point [% roller width OD−>ID]
80
Grinding bed
Table
70
60
B 50
40
Roller
Pressure profile
Grinding bed 30
Table
20
10
20 40 60 80
Fig. 10. (A) Due to the centrifugal forces the grinding bed will try to form a parabola.
If the roller was non-existing, the combined full and dotted line show this behavior. Nominal pressure [%]
As the roller is lowered onto the grinding bed an uneven pressure profile forms. (B)
As a result of choke feeding a bead forms in front of the roller and a non-uniform Fig. 12. Rolling point as function of grinding pressure. The table speed and grinding
pressure profile builds up. bed thickness is kept constant.
L.R.D. Jensen et al. / Wear 271 (2011) 2707–2719 2713
the rollers and the table. The wear will inevitable result in a thicker
grinding bed and consequently the grinding pressure will decrease
70
if the force stays the same. For optimum performance the grinding
force needs to be increased as long as the mechanical components
60
can withstand the extra stress.
50
5.3. PSD vs bed thickness
40
From the investigations it is concluded that the bed thickness
and thus the production rate is dependent on the PSD. This has
30
been verified by testing monodisperse and polydisperse mixtures
on the experimental VRM. A monodisperse mixture results in a thin
20
grinding bed as the material is ploughed in front of the roller and
cannot be gripped: The particles roll and interlocking is suppressed.
10
A polydisperse mixture results in a bed which is easily packed and
the result is a thick grinding bed. From a comminution point of view
20 40 60 80 a monodisperse mixture governs the best conditions for an effective
Nominal velocity [%] grinding process (large compaction ratio, single particle breakage)
whereas a polydisperse mixture is unfavorable (small compaction
Fig. 13. Rolling point as function of table speed. Pressure and bed height is kept ratio).
constant.
CL
Roller
Pressure profile
90 Material flow
Grinding bed
Table
Rolling point [% roller width OD−>ID]
80
70
60
50
B
40
CL
30
20
Inner dam ring
10
20 40 60 80
Nominal bed tickness [%] Fig. 15. Two principal/illustrative figures showing the bed behavior at constant
speed, pressure and bed height. (A) A normal setup where the pressure profile is
Fig. 14. Rolling point as function of bed thickness. Grinding pressure and table speed close to OD. (B) A special setup where an inner dam ring constraints the inward
is kept constant. material flow.
2714 L.R.D. Jensen et al. / Wear 271 (2011) 2707–2719
A
B
C
Fig. 17. (A) Rock fragments in the new feed are often three times larger than the
grinding bed thickness. (B) For a fraction of time, the rock fragment is wedged
between the roller and the table. (C) The rock fragment is crushed resulting in a
vertical movement of the roller.
Fig. 16. Roller shown horizontally with waves in aluminum foil indicating slip. The
slip acts in the rotational direction. The red arrow indicates the calculated rolling the grinding bed thickness (Fig. 17). Just before the compressive
point which is 20 mm from the outer edge (top side of photograph), the roller having
crushing takes place, the rock fragment might be wedged between
a total width of 70 mm. The lower part of the photograph shows that radial pres-
sures are non-existing from the rolling point towards ID. (For interpretation of the the roller and the table and the result is visible gouging (Section 6.1).
references to color in this figure legend, the reader is referred to the web version of Mostly the rock fragments are limestones with very low abrasive
the article.) contents not resulting in any gouging, however it is assumed that
loose abrasives can be squeezed between the rock and the roller as
necessary grinding pressure is decreasing. However, this effect is it is wedged.
counteracted because the abrading effect is reduced as the grinding
bed becomes thicker and more quartz particles are hidden within
the bed.
Fig. 18. Wear part macroscopical analysis (roller segment): (a) top view of surface
5.5.2. Fragment movements
from the high stress abrasion zone. The wear mechanism is characterized as gouging.
The large fragments have a secondary function in the grinding (b) The wear part has a width of approx. 700 mm. The yellow ruler indicates the
bed behavior and cannot be explained by the discussions outlined in original wear part cross section. The maximum wear depth is approx. 100 mm. Note
Section 5.1. The large fragment movements have also been analyzed that the lefthand edge of the roller has been severely abraded resulting in a large
using adhesive tape and aluminum foil as an indicator. By analyzing gap.
(a) Stereo photograph of roller surface.
the material flows in the grinding bed, it is observed that a bead
(b) Cross sectional view of worn roller wear part (width 700 mm). (For interpretation
forms in front of the roller (Fig. 10). Furthermore, the new feed in of the references to color in this figure legend, the reader is referred to the web
a VRM consists of rock fragments having a size up to three times version of the article.)
L.R.D. Jensen et al. / Wear 271 (2011) 2707–2719 2715
A Constrained movement
of rotactitioon
n
Dire
Unconstained movement
B Unworn profile
Worn profile
Abrasive vectors
C
Direction
of rotation
Area of
reduced wear
Fig. 19. Visual characterization of wear regions (roller segment). (A) The pressure
profile will intensify the material removal in the segment towards the periphery of
the roller. (B) Cross sectional view shows how a worn segment compares to a new
segment. (C) A detailed top view of a wear segment shows three regions of interest.
Fig. 20. SEM micrographs showing wear part surfaces of 21988/JN/HBW555XCr21.
(a) A gouging scratch cuts almost horizontally through the material disobeying the
hardness differences between matrix and chromium carbides. The white spots are
6. Macroscopic wear analysis remaining limestone particles. (b) Surface appearance after 10 repeated high stress
displacements in the wear test apparatus.
The observed grinding bed movements (Section 5) have been (a) Industrial VRM wear part surface (from high stress zone).
(b) Experimental VRM wear part surface.
verified by examining industrial roller wear parts. The surface of
the worn roller wear parts show two distinct properties:
6.1. Gouging
• A rough surface with deep scratches resembling gouging
(Fig. 18a). As a counter intuitive fact, it has been observed that the wear
• A pronounced change of surface geometry (Figs. 18b and 19). scratches mainly cut in the opposite direction of rotation (Fig. 19).
This phenomena can be verified by studying the wear scratches,
Because the VRM is performing a continuous crushing of parti- their starting points and end points. The main reason for this obser-
cles, the rocks (and granular material) will flow in the directions vation is due to the large rock fragments which are scattered evenly
of least resistance. When analyzing the macroscopic wear profile, throughout the grinding bed (Section 5.5.2, Fig. 17). Gouging is the
three different regions can be identified: result of the wedged rock fragments, however it is believed that this
phenomena will not contribute substantially to the pronounced
• A high stress abrasion (gouging) region with large wear marks geometrical change of the wear part surfaces. It is believed that
tangential to the rolling direction showing a distinct anisotropic the gouging wear increases the interfacial friction enabling a larger
wear mode (constrained movement). This region is formed nip angle.
towards the outer periphery due to the sloped grinding bed and
the subsequent high stress region (Figs. 10 and 11). 6.2. Abrasion
• A high stress abrasion (gouging) region with anisotropic wear
marks radially to the rolling direction (unconstrained move- Besides the counter rotational wear scratches, 2-body abrasive
ment). This region is formed at the outermost edge of the wear based primarily on slip and extrusion acts in the direction of
roller. The grinding pressure quickly decreases at the edge and rotation (Section 5.1). As a result of the sloped grinding bed which
as a result the rocks/particles extrude radially towards the forms during operation, a high stress region appears towards the
dam ring. outer periphery of the table resulting in accelerated abrasion in the
• A low stress abrasion region with reduced wear with tiny wear same region (Figs. 10 and 19). It is believed that this slip rotational
marks showing an isotropic wear mode (unconstrained move- wear is the primary source for the geometrical changes observed on
ment). This region is located towards the center of the VRM and the roller surfaces. The abrasive wear scratches based on rotational
stays almost unaffected because no radial pressures are acting in slip cannot readily be identified as they are camouflaged by the
this region. counter rotational wear scratches (gouging).
2716 L.R.D. Jensen et al. / Wear 271 (2011) 2707–2719
Fig. 21. SEM micrographs of 21988/JN/HBW555XCr21 as a cross sectional view in Fig. 22. SEM micrographs of 21988/JN/HBW555XCr21 as a cross sectional view
the vicinity of the surface experiencing abrasive wear. Sample is etched with Nital. in the vicinity of the surface experiencing abrasive wear. Sample is polished with
(a) Micro cracks more than 200 m below the surface. cerium oxide.
(b) Heavy plastic deformation at the surface going from left to right. Furthermore, (a) Micro crack formation below surface in chromium carbides. Note the delamina-
horizontal cracks in the chromium carbide. The matrix stays unaffected. tion at the proximity to the surface. The matrix stays unaffected.
(b) Finely dispersed secondary chromium carbide (Cr3 C2 ) in the matrix. The areas
close to the coarse primary carbides (Cr7 C3 ) are depleted from Cr3 C2 .
7. Wear apparatus
particles at approx. 90 m (Section 1.1). With this microstructure
During operation, the grinding bed is drawn underneath the there is a strong possibility that quartz particles will wash out the
roller and compressed to a very hard and dense press cake (high chromium carbides.
pressure zone). Since the particles are fully interlocked in this com- The VRM can be regarded as a bearing system with the grind-
pressed bed, not being able to rotate, a 2-body anisotropic abrasion ing bed acting as a cushioning media between the table and the
wear mechanism is expected. The system can be thought of as lime- roller. The forces are transmitted through the bed which will act as
stone particles acting as glue and thereby keeping the abrasive a pressed solid in the high stress zone. The geometrical setup of the
particles fixed (grit paper system). VRM requires the table to turn faster in the high stress region and
The SEM micrographs of both the industrial worn parts and the the result is slip on the roller surface (Section 5.1). The slip (similar
worn sample specimen, show coinciding results (Fig. 20a and b). to heavy squeezing) combined with the rolling action will result in
The wear test apparatus developed for this study seems to imitate a strain gradient perpendicular to the worn surface.
the abrasive wear mechanism observed in industrial VRMs. Conse- In the proximity to the surface a shattering and even a delam-
quently, this result has revealed that the major material removal ination of carbides from the surrounding matrix is present. This
process is governed by 2-body abrasion. is mainly due to the direct contact with hard particles and frag-
ments to be ground. The strain gradient combined with the soft
8. Microscopic wear analysis and hard phases in the microstructure result in a strain incompati-
bility in the subsurface region. The strain results in micro cracks in
Along with the macroscopical analysis, the SEM was used the chromium carbides alone and reach depths of 200 m below
to investigate the subsurface microstructure. The worn surface surface (Fig. 21a). Also, a visual decohesion of the carbides from the
texture and the subsurface microstructure show similarities to surrounding matrix is present in many regions. The cracks are only
observations made in a previous study where jaw crushers were present approx. parallel to the surface in the elongated chromium
investigated [16]. The wear part material consists mainly of a carbides and thus explains that the matrix easily transmits shear
matrix and elongated chromium carbides with sizes of approx. stresses well below the surface (Fig. 21b). When closely analyzing
10–200 m. When examining the microstructure it becomes evi- the SEM micrographs it also becomes evident that some carbide
dent that the distance between the hard chromium carbides and fragments are displaced from their mother fragments (strong deco-
soft matrix is unfavorable when the surface is in contact with quartz hesion) indicating that heavy plastic deformation is present in
L.R.D. Jensen et al. / Wear 271 (2011) 2707–2719 2717
Table 2
Result from OES analysis of wear part material [%].
21988/JN/HBW555XCr21 75 2.7 0.62 1.98 16.1 0.12 1.3 0.63 1.13 0.42
this reason a micro hardness value of 1200–1600 HV has been 10. Conclusion
adopted [18]. The results from the micro hardness measure-
ments of the tempered martensitic matrix showed variations in This study is based on dry grinding bed investigations on VRM
the hardness as function of depth below surface (Fig. 25). The wear part geometries. The wear part material is a heat treated
micro hardness values show a strain hardening behavior close 21988/JN/HBW555XCr21 with Cr7 C3 and Cr3 C2 phases embed-
to the surface, but micro hardness results are generally very dif- ded in a tempered martensitic matrix. No residual austenite is
ficult to measure and should be interpreted with great caution present.
[19,20]. Depending on PSDs, particle shapes, moisture, etc., a grind-
ing bed will only show internal shear if pressures are low.
At high pressures the bed interlocks and becomes like a
solid: As a result the size reduction in VRMs is domi-
nated by the mechanism of compression alone. Size reduction
a by shear is insignificant and applies to low pressure areas
800 alone. Size reduction by abrasion/attrition is also insignifi-
cant.
Rock fragments govern visible counter rotational wear scratches
(gouging) and small particles govern rotational wear scratches
750 (high stress abrasion). The main wear removal process is con-
trolled by 2-body abrasion in the high stress compaction
zone.
HV0.025
Fig. 25. Micro hardness measurement of tempered martensite (21988/ The authors would like to thank associated professor Knud Aage
JN/HBW555XCr21).
Thorsen and senior metallographer Steffen Sonne Munch for their
(a) General micro hardness measurements.
(b) Close up view of (a). support.
L.R.D. Jensen et al. / Wear 271 (2011) 2707–2719 2719
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