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OISD STANDARD - 144

FIRST EDITION
APRIL 1994

FOR RESTRICTED
CIRCULATION ONLY

LIQUEFIED PETROLEUM GAS (LPG)

BOTTLING PLANT OPERATIONS

VOLUME-1
DESIGN PHILOSOPHIES

Prepared by

FUNCTIONAL COMMITTEE ON LIQUEFIED PETROLEUM GAS (LPG)

OIL INDUSTRY SAFETY DIRECTORATE


2nd Floor, ‘KAILASH’
26, KASTURBA GANDHI MARG,
NEW DELHI-110001
LIQUEFIED PETROLEUM GAS (LPG)

BOTTLING PLANT OPERATIONS

CONTENTS

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CHAPTER DESCRIPTION PAGE
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INTRODUCTION

SCOPE

VOLUME 1 : DESIGN PHILOSOPHIES

1. Physical Properties & Characteristics of LPG

2. Statutory Rules and Regulations

3. Plant Layout

4. Plant Design Criteria

5. LPG Cylinders and Valves

VOLUME II : OPERATING PRACTICES

6. Storage and Handling of Bulk LPG

7. Bottling Operations

VOLUME III : INSPECTION & MAINTENANCE PRACTICES

8. Plant Equipment

9. Statutory Testing of Cylinders

VOLUME IV : SAFETY & FIRE PROTECTION

10. Fire Protection Facilities

11. Emergency Management

12. Safety Audit

GLOSSARY OF TERMS

APPENDIX
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CHAPTER 1

PHYSICAL PROPERTIES AND CHARACTERISTICS OF LPG


1.1 LIQUEFIED PETROLEUM GAS (LPG)
(c) The LPG pumping facility is neither to be
LPG is a mixture of commercial butane and provided below ground level nor beneath the
commercial propane having both saturated and storage vessel in order to avoid the accumulation
unsaturated hydrocarbons. LPG marketed in of LPG.
India shall be governed by Indian Stnadard
Code IS-4576 (Refer Table 1.0) and the test 1.2.2 VAPOUR PRESSURE
methods by IS-1448.
The pressure inside a LPG storage vessel/
LPG is inherently dangerous on account of fire, cylinder will be equal to the vapour pressure
explosion and other hazards. This calls for corresponding to the temperature of LPG in the
special attention on the manner in which it is storage vessel. The restriction on vapour
bottled, transported or used. These hazards can pressure is stipulated by IS-4576 which in turn
have an impact on both the plants and the regulates the lighter ends of hydrocarbons and
public. As a consequence of this special this governs the design parameters for storage
emphasis has been placed on the safety vessels.
regulations in its handling,system design, etc.
The vapour pressure is dependent on
1.2 PHYSICAL PROPERTIES AND temperature as well as on the ratio of mixture of
CHARACTERISTICS hydrocarbons. At liquid full condition any
further expansion of the liquid, the cylinder
1.2.1 DENSITY pressure will rise by approx. 14 to 15 kg./sq.cm.
for each degree centigrade. This clearly explains
LPG at atmospheric pressure and temperature is the hazardous situation that could arise due to
a gas which is 1.5 to 2.0 times heavier than air. overfilling of cylinders.
It is readily liquefied under moderate pressures.
The density of the liquid is approximately half 1.2.3 FLAMMABILITY
that of water and ranges from 0.525 to 0.580 @
15 deg. C. LPG has an explosive range of 1.8% to 9.5%
volume of gas in air. This is considerably
Since LPG vapour is heavier than air, it would narrower than other common gaseous fuels.
normally settle down at ground level/ low lying This gives an indication of hazard of LPG
places, and accumulate in depressions. Under vapour accumulated in low lying area in the
still conditions the dissipation of accumulated eventuality of the leakage or spillage.
vapour can be slow. This accumulation of LPG
vapour gives rise to potential fire and explosion The auto-ignition temperature of LPG is around
hazard. Some of the areas requiring careful 410-580 deg. C and hence it will not ignite on
consideration of this hazard in order to prevent its own at normal temperature.
and control fire and explosion are as given
below : Entrapped air in the vapour is hazardous in an
unpurged vessel/ cylinder during pumping/
(a) Terrain and natural drainage must slope filling-in operation. In view of this it is not
away from process units, buildings or other advisable to use air pressure to unload LPG
plant facilities, storage vessels, property lines cargos or tankers.
bordering community establishments and
roadways, navigable or inhabited streams, and 1.2.4 COMBUSTION
towards low incident areas.
The combustion reaction of LPG increases the
(b) There shall be no low spots under or near volume of products in addition to the generation
the base of the container where spillage could of heat. LPG requires upto 50 times its own
accumulate and the container can get engulfed volume of air for complete combustion and at
in a fire pot. For the same reasons it is the same time yields 3 or 4 times its own volume
advisable to compact/ concrete beneath the of carbon-dioxide yielding approx. 10,900 kcal
storage vessels with a slope to avoid wetting of heat per kg.
soil and to eliminate vegetation. This will also
facilitate evacuation/ channeling, and washing Thus it is essential that adequate ventilation is
out the spillage so that it can be trapped or provided when LPG is burnt in enclosed spaces
allowed to burn at a safe location. otherwise asphyxiation due to depletion of
oxygen apart from the formation of carbon- can give violent concussion in explosion than in
dioxide can occur. case of hydrogen, due to faster flame
propagation.
1.2.5 VOLATILITY
1.2.8 CUBICAL EXPANSION
The restriction on the evaporation temperature
to 2 degree C for 95% by volume at 760 mm Hg Liquid phase LPG expands considerably when
pressure imposes regulation on the quantity of its temperature increases exceeding most of the
hydrocarbons heavier than butane. This ensures petroleum products. The coefficient of expansion
that when the container is nearly empty, the is around 0.00237 per deg. C. The high rate of
liquid does not have an unacceptably low vapour expansion has to be taken into account when
pressure to let in air and to form an explosive specifying the maximum quantity of LPG
mixture. permited to be filled into any pressure vessel.

When pressure is released, LPG vapourizes The maximum permissible liquid volume of any
rapidly lowering the surrounding temperature. container is that quantity which will assure that
This may lead to frost burns by contact of LPG the container will have a minimum vapour space
with the skin. Protective clothing such as gloves of 5% for cylinders and bulk containers, when
and goggles shall therefore be worn when there the liquid is at the highest anticipated
is any possibility of contact with LPG. temperature. These temperatures have been
considered as 55 deg. C for bulk containers and
Auto refrigeration effect of the vapourisation of 65 deg. C for cylinders. The safe filling ratio for
LPG freezes the water vapour in the atmosphere, cylinders/ storage vessels shall be in accordance
which makes the escaping LPG vapour visible as with Gas Cylinders Rules and SMPV Rules
a whitish cloud. Even if this cloud disappears, it respectively.
is not a sign that the inflammable gas/ air
mixture has been dispersed. Because the filling ratio precautions takenin
storage system cannot be extended to the
Leaking liquid phase LPG will rapidly expand connected piping network, relief valves are
around 250 times its own volume thereby provided in all areas where LPG can be trapped
creating a greater risk than would occur with a between closed valves in order to protect these
similar sized vapour leakage. Sufficient ullage parts of the system.
space for the expansion of liquid when the
temperature rises must therefore be left in all 1.2.9 ODOUR
storage/ transport containers.
LPG has only a very faint smell, and
1.2.6 EFFECT OF WATER IN LPG consequently, it is necessary to add some
odorant, so that any escaping gas can easily be
Because of a very low solubility of LPG in water detected.
the identification of minor leakage in water is
after and easier. Ethyl Mercaptan is normally used as stenching
agent for this purpose. The amount to be added
Water present in LPG may cause rust and should be sufficient to allow detection in
corrosion and freeze-up of valves, drain valves, atmosphere 1/5 of lower limit of flammability or
excess-flow check valves, cylinder valves and odour level 2 as per IS : 4576.
regulators. Ice-formation may prevent the
closure of drain valves, bleeders in LPG vessels 1.2.10 COLOUR
and lines, self closing valves, etc. and result in
leakage of LPG. Ice crystals formed at the LPG is colourless both in liquid and vapour
regulator orifice may lead to plugging of the phase. During leakage the vapourisation of
orifice and thus stopping the flow of gas. Ice liquid cools the atmosphere and condenses the
crystals may also make the linkages in a water vapour contained in them to form a
regulator inoperable. whitish fog which may make it possible to see
an escape of LPG.
1.2.7 FLAME PROPATION
1.2.11 VISCOSITY
LPG liquid released will form a vapour which
will travel long distance. The vapours of LPG
LPG liquid has low viscosity of around 0.3 CS aluminium alloys. Hence stipulating absence of
@ 45 deg. C and can leak when other petroleum caustic is essential in addition to IS-4576
products normally cannot, thus demanding a specification.
very high integrity in the pressurised system to
avoid leakage. It is also a poor lubricant and 1.2.15 PUVCE AND BLEVE'S
leaks are therefore likely to occur at pump seals PHENOMENA
and glands. In view of this a special attention to
the given, for example to the selection of The hazards associated with the release to
mechanical seals for pumps and also seals at the atmosphere of a boiling flammable liquid show
carousel centre column. themselves disproportionately where large
quantities are involved - they can give rise to
1.2.12 PYROFORIC IRON two phenomena which are highly hazardous ;
(a) Unconfined Vapour Cloud Explosion
Pyrophoric Iron sulphide is a highly (UVCE) and (b) Boiling Liquid Expanding
inflammable compound formed due to the Vapour Explosion (BLEVE).
reaction of sulphur and its compounds with the
loose iron/ iron oxide on a ferrous surface. Thus Vapour cloud can ignite and burn as
the pyrophoric Iron Sulphide can be controlled deflagrations or fire balls causing lot of damage
by totally eliminating highly corrosive hydrogen by radiation starting secondary fires at some
sulphide, limiting the total volatile sulphur to distance. Vapour cloud ignites and explodes
0.02% by mass reducing the loose iron oxide by causing high over pressures and very heavy
thoroughly cleaning the storage vessels damage. The later is termed as `percussive
internally during the outage. unconfined vapour cloud explosion' i.e. PUVCE
in short. Even though large quantities of LPG
Pyrophoric Iron Sulphide will not ignite emission is necessary, only a fraction of this
spontaneously in a sphere/ cylinder containing a contributes to the percussive effect ( more
concentration of vapour of gas as long as the reactive molecules such as ethylene in much
concentration is above the upper flammable smaller quantities). Rare though PUVCE may
range limit. When these vessels are aired to be, their damage is large and sometimes
(during opening to atmosphere or air entrapped enormous.
condition) within or below the range, it will
ignite spontaneously, unless water or steam is The boiling liquid expanding vapour explosion
used to cut the sulphur iron reaction. The most (BLEVE) is due to holding a pressurised
effective extinguishing agent is water spray of flammable liquid above its boiling point. This
fog. Similar type of precaution is warranted may result from inadequate vapour space for
while opening of LPG pump strainers and any temperature expansion of the contents or high
location where loose iron oxide is expected. temperature due to radiation heat from the
adjacent vessel fires or due to any mechanical
1.2.13 TOXICITY damage. BLEVE even though not as serious as
PUVCE, its potential for spreading fire over a
LPG even though slightly toxic, is not poisonous wide area makes them significant in terms of
in vapour phase, but can, however, suffocate both life and property damage.
when in large concentrations due to the fact that Ejection of boiling liquid produces reaction
it displaces oxygen. In view of this the vapour rupturing the vessel causing the rocket
posses mild anaesthetic properties. projectioning of dish ends. The released liquid
flashes and atomizes immediately, often
1.2.14 CAUSTIC RESIDUE resulting in a large fire ball. Although the fire
ball lasts only a few seconds, its effect can be
Caustic soda treatment employed for the devastating due to flame contact and thermal
removal of hydrogen sulphide could leave traces radiation.
of caustic in LPG. This may lead to corrosion on
the storage vessel and other LPG handling
equipment with predominant effect on

TABLE 1.0

LPG SPECIFICATIONS
Salient Features as per IS:4576
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S.No. Characteristic Requirement for commercial Method of Test Ref. to
Butane-Propane Mixture Page(P) of IS:1448
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1. Vapour pressure at 16.87 Max. P:71


65 deg. C kgf/cm.g.

2. Volatility: evaporation 2 P:72


temperature in deg.C,
for 95 per cent by
volume at 760 mm Hg
pressure, Max.

3. Total volatile sulphur 0.02 P:34


percent by mass, Max.

4. Copper strip corrosion Not worse P:15


at 38 deg.C for 1 hour than No.1

5. Hydrogen Sulphide Absent P:73

6. Dryness No free entertained P:74


water

7. Odour Level 2 P:75

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CHAPTER 2

STATUTORY RULES / REGULATIONS

2.1 STATUTORY RULES/ REGULATION & b) Air (Prevention & Control of Pollution)
OTHER RECOMMENDED Act- 1981 (Amended upto 1988)
GUIDELINES : c) The Environment (Protection) Act -
1986
Construction and operation of LPG bottling
plants, storage, transportation and d) Manufacture, storage & import of
distribution of LPG are required to be Hazardous chemicals Rules - 1989.
carried out in accordance with various
prevailing national statutory rules and e) Guidelines for Environmental clearance
regulations. This section covers the salient of new projects - 1981.
features in brief w.r.t. following regulations
which are in force. For complete details 2.3 RECOMMENDATION OF
with regard to the various provisions, COMMITTEES :
original notifications/ documents may be
referred to. In addition to the above Statutory regulations,
there are various recommended guidelines
2.2 STATUTORY RULES/ REGULATIONS emerging out of the various Committees set up
by the Govt. of India from time to time for
i) Gas Cyliinders Rules, 1981 (under streamlining/ improving the safety standards of
Indian Explosives Act,1884) LPG Bottling/ Distribution:

ii) Static & Mobile Pressure Vessels I) Vasudevan Committee - 1983 Ministry
(unfired) Rules-1981 (Under Indian of Energy (Department of Petroleum).
Explosives Act 1884).
ii) Expert Committee Review of Safety
iii) The Factories Act, 1948 (Amended in and Operating Procedures in LPG
1987). facilities - 1986, Ministry of Petroleum
& Natural Gas (Department of
iv) Electrical Installation under Indian Petroleum).
Electricity Rules - With Latest
Amendments. iii) Sudha Joshi Committee for better
services to LPG users - 1987 (Ministry
v) a) The Standards of Weight & of Petroleum & Natural Gas).
Measures Rules - 1987 Under Weight &
Measures Act - 1976. N.B. : The summary of the recommendations of
the above committees is covered in this section.
b) The Standards of Weight & Measures For further details the original documents may
(Packaged Commodities Rules-1977) be referred to.
Licence to import Gas Cylinders in
Form D issued with latest amendments. 2.4 SALIENT FEATURES OF VARIOUS
RULES/ REGULATIONS :
vi) Liquefied Petroleum Gas (Regulation of
supply and distribution Order - 1993). I) Gas Cylinder Rules - 1981 :

vii) The Motor Vehicles Act - 1988. These rules have been framed under the Indian
Explosives Act,1884 to regulate the possession,
viii) Environmental Regulations : delivery, storage, handling and examination/
testing of gas cylinders limited upto capacity of
a) Water (Prevention & Control of 1000 litres.
Pollution) Act, 1974 (Amended upto
1988). Under these rules, prior approval from Chief
Controller of Explosives (CCE) is required to be
taken before constructing any new facility or
altering the existing facility for filling cylinders in bulk issued be submitted in
and storage area etc. Before commissioning/ in Form-III : in Form -1
operating of LPG bottling plant following (under rules 49, 54
licences are required to be obtained from CCE & 55).
after furnishing the details in specified formats :

Licence to import cylinder in Form D: Licence to transport Application is to


Application is to be submitted in Form B(under LPG in bulk issued be submitted in
Rules 57and 61) in Form -IV : in FORM- II
(under rules
Licence to fill/ possess Cylinders in Form E & 49&54)
F : Application is to be submitted in Form C
under Rules 57,61&62)
1. Approval of initial location or expansion of
Generally licence for import of cylinders (form existing installation by the site appraisal
D) is valid upto one year (maximum) whereas committee constituted by the State Govt.
other licences in Form E and F granted or
reviewed remain in force till 31st March of the 2. Approval of the plan, speficiations/
year subject to validity of maximum 3 years. drawings for construction of the Factory/
Application for renewal must reach CCE, Installation by the Chief Factory Inspector
Nagpur at least 30 days prior to expiry of the and also registration/ licence for operating
current licence. factory. Licence is to be renewed every year
or as specified.
Cylinders should conform to specified design,
fittings, markings, identification colour and
should have approved from CCE before use of The granted licences which remain in force till
the same. 31st March of the year are generally valid for
period of 3 years (max.). Application for renewal
Cylinders in use are required to be inspected and must reach CCE, Nagpur at least 30 days prior
hydrostatically tested as specified in the BIS to expiry of the current licence.
code as per or procedure/ frequency approved by
CCE. Rejected cylinders are to be destroyed by Inspection/ hydrotesting of vessels is required to
flattening/ cutting into pieces. be carried out once in 5 years or as specified by
a competent agency duly approved by CCE.
II) STATIC & MOBILE PRESSURE Frequency of inspection/ testing of safety valve
VESSELS (UNFIRED) RULES - is once a year. (Refer OISD-STD No.128 - on
1981 Inspection of Pressure Vessels).

These rules in conjunction with Gas Cylinders N.B. : The above rules do not apply to transport
Rules have been framed under the Indian compressed gases filled in vessels by Railways
Explosives Act to regulate the construction, Administration who follow their own RDSO
fitment, storage, loading/ transport and regulations.
inspection of unfired vessels in service of
compressed gas like LPG with capacity III) FACTORIES ACT - 1948
exceeding 1000 litres. (AMENDED AS FACTORIES
(AMENDMENT) ACT, 1987)
As per these rules it is obligatory to obtain
approval and licences from CCE prior to The act aims at regulating working conditions in
construction/ alteration and commissioning/ the factories and lays down minimum
operation of any LPG storage vessel and allied requirements for ensuring the safety, health and
facilities. Vessels are required to be designed, welfare of the workmen. It is applicable to all
constructed and tested in accordance with BIS - establishments/ factories employing more than
2825 as amended from time to time or such 10 employees.
code/ standard as approved by CCE.
As per the First Schedule of the amended Act
Application/ licences under these rules are : (1987), installations handling highly flammable
liquids and gases come under Hazardous
Licence to store LPG Application is to process/ operations. Salient provisions to be
complied with rules framed by the State Govts. The installation must be inspected and approved
under the Factories Act are given below : by Electrical Inspector of the State Government
before commissioning. Subsequent inspection/
- Approval of initial location or expansion of testing shall be required at intervals not
existing installation by the site appraisal exceeding five years or as specified. Only
committee constituted by the State Govt. licenced contractors/ agencies holding the
certificate of competency should be engaged for
- Approval of the plan, specifications/ any installation work.
drawings for construction of the Factory/
Installation by the Chief Factory Inspector All earthing system in the installation shall
and also registration/ licence for operating require to be tested for resistance during the dry
factory. Licence is to be renewed every year season not less than once a year or as specified
or as specified. by the authorities. Record of every earth test
shall be maintained by the occupier incharge of
- Disclosure of information by the occupier the installation and shall be produced as
regarding hazards/ dangers including health required before the inspector or authorised
hazards and measures to overcome such officer. (Refer OISD STD 137 for earthing test
hazards to workmen and general public frequencies).
living in the vicinity of the factory.
Suitable fire extinguishers for dealing with
- Declaration of written safety policy w.r.t. electrical fire like Co2, DCP type extinguishers
health and safety of workmen. should be placed in electrical installations.

- Ensuring proper fencing/ provision of safety Note :


guards on equipment/ machinery. Fire/
accident prevention faciities etc. i) For appropriate area classification,
guidelines contained in IS:5572 (part 1)
- Examination/ testing of machinery/ vessels/ 1978 should be followed.
tools/ tackles etc. at specified frequency.
ii) For selection of electrical equipment,
- Maintenance of uptodate Disaster guidelines contained in IS:5571-1979
Management Plan. & IS:9570-1980 as revised from time to
time should be followed.
- Specific responsibility of the occupier in
relation to - V) (A) STANDRDS OF WEIGHTS &
MEASURES ACT -1976 :
a) Maintenance of health records of person (WEIGHTS & MEASURES RULES-
likely to be exposed to harmful toxic 1987)
substances.
Approval/ certification of Measuring
b) Deployment of qualified persons to handle Appliances: Weighing equipment like
hazardous substances/ equipment. weight scales, weigh bridges etc. before
installation shall have approval and
c) Appointment of Safety Officer. certification by the Regional Director/
designated authority of Weights &
IV) STATUTORY REQUIREMENTS OF Measures. in case, the equipment is
LECTRICAL INSTALLATIONS : imported, the same shall have
(INDIAN ELECTRICITY RULES certification of appropriate authority of
MARCH, 1980: AMENDED UPTO the country where it is manufactured in
1988) accordance with recommendations of
International Organisation of Legal
For supply of power, licence is required from the Meterology. Such models shall be
designated authority of the State Government tested, if required, and shall be duly
after submitting the application with details of certified by the Indian authorities to
premises, drawing/ maps of the proposed area of verify the accuracy.
supply, electrical installation, nature and amount
of supply etc. Verification/ stamping : Weighing
equipment shall require re-verification
by the designated Inspector at Declared Maximum
prescribed intervals. Certificates in Quantity permissible error
prescribed form shall be obtained or in excess or in deficiency
stamping indicating therein the
particulars of verified measures shall be gm or ml % gm or ml
made. Test weights used for regular
checking the accuracy of weighing 1000-10000 1.5 --
equipment shall also require stamping 1000
of Weights & Measures. 1001 10000-15000 -- 150

Bulk Meters : Bulk meters used for more than 15000 1.0 --
measuring Liquid petroleum products
shall be of positive displacement type. VI) THE LIQUEFIED PETROLEUM
These meters can be fitted with GAS (REGULATION OF SUPPLY &
automatic or manually operated DISTRIBUTION ORDER), 1993
temperature compensating devices. For AND AMENDMENT ORDER, 1994
flow accuracy, these shall be correctly
installed as per recommended This order was brought into force w.e.f.
procedure and protected by a strainer August 1993 by the Ministry of Petroleum
filter and air eliminators. & Natural Gas, Salient features are outlined
below :
All meters shall be tested under
conditions which duplicate normal Restriction on possession & consumption
operating conditions in respect of flow of LPG :
and product involved. The error shall
not exceed +/- 0,1% for any quantity No person shall be granted by an oil
discharged. Every meters shall be company more than one gas connection and
provided with suitable scaling the same shall not be used for purposes
arrangement to receive the stamp or other than cooking unless specified by a
seal of the verification authority. general or special order for such other
purposes it may specify in that order.
Site Inspection : Weights & Measure
Authorities within their area of No transporter or delivery person shall
jurisdiction can visit the premises, for deliver LPG gas either in cylinders or bulk
inspection/ testing of any measuring to any person other than the authorised
equipment in use apart from checking consumer.
the relevant records/ documents.
No person shall fill cylinder with LPG or
(B) THE STANDARDS OF WEIGHTS & transfer from one container to other without
MEASURES (PACKED permission of Chief Controller of
COMMODITIES) RULES AND Explosives.
AMENDMENT RULES, 1991.
Regulation of weight ;
LPG shall be marketed/ sold on weight
basis in packaged form i.e. cylinder of The weight of the LPG contained in a
approved design. cylinder shall not vary by a difference of
1.5% of the net weight of the respective
Declaration shall be required on every cylinder as indicated on it by the Govt. oil
cylinder about name/ address of company.
Manufacturer/ packer, common or generic
name of the commodity, net quantity in Restriction on storage & transportation :
terms of standards weight, size/
dimensional details of the containers etc. No person shall use cylinder, pressure
regulator and gas cylinder valve other than
Maximum permissible errors on net those specified in schedules "A" and "B".
quantities declared by weight or by volume
shall be as below : Storage place should be cool, dry, well
ventilated, easily accessible, place under
cover being away from open flames/ steam competence certificate,minimum driving
pipes or other source of heat. experience etc.

Possession, supply or sale of LPG Registered laden weight/ axle weight as per
equipment : notification for particular model should not
exceed the permissible value.
a) No person shall supply or sell filled or
empty cylinders, gas cylinder valves Use of `TREM CARD' or other safety
and pressure regulators to any person guidelines issued for particular hazardous
other than a Govt. oil company or a commodity as prescribed by Central/ State
parallel marketeer. Govt. authorities. This covers specified
arrangement of maintenance/ repairs,
b) Unless authorised by a Govt. oil emergency handling procedures in case of
company or a parallel marketeer, road accidents.
supply or sell empty cylinder, gas
cylinder valve and pressure regulator to Certificate of fitness/ age limit as specified
any person other than a consumer. in rules of Central/ State Govt.

c) Possess filed or empty cylinder, gas VIII) ENVIRONMENTAL


cylinder valve or pressure regulator REGULATIONS
unless he is a consumer and the same
has been supplied by a distributor, a A) Water (Prevention & Control of
Govt. oil company or a parallel Pollution) Act, 1974 (with latest
marketeer. amendment) :

Restriction on Disposal of Discarded Under the main provision of this Act :


Cylinder/ Equipment
Prior consent of State Pollution Control
Every manufacturer of cylinder, gas Board by applying in prescribed format is
cylinder valves and pressure regulators required for :
shall dispose off the items which do not
conform to respective BIS Establishing any industry, operation or
specifications after deshaping/ crushing process or any treatment and disposal
such items. system or any extension or addition thereto
which is likely to discharge sewage or
Power of Entry, Search & Seizure : effluent into a stream or on land.

Notified officers of Central Govt./State Using any new or altered outlet for
Govt. (Deptt of Food & Civil Supplies) discharge of sewage or effluent.
or Sales Officer of a Govt. oil company
are authorised to inspect Distributor's Application for renewal of consent, which is
premises or transport vehicle to ensure generally valid for one year should be made
the compliance with provision of this at least one month in advance. Occupier has
order. to ensure the compliance of the directions or
stipulations laid down by the Board while
VII) THE MOTOR VEHICLE ACT, 1988 granting the consent. Returns for the
amount of water consumed alongwith
Some relevant features w.r.t. safety payment of cess must be submitted in
provisions in Motor Vehicles Act revised in manner as prescribed in the Water
1988 are as below (Prevention & Control of Pollution) Cess
Act, 1977.
Grant of driving licence for transport
vehicle used for hazardous goods like LPG b) Air (Prevention & Control of
and other petroleum products is restricted. Pollution) Act-1981 (with latest
The person must have some minimum amendments)
educational qualification as prescribed by
Central/ State Govt. apart from other The objective of this act is to provide for
conditions like medical fitness, driving prevention, control and abatement of air
pollution" caused by any operation or environment due to hazardous chemicals.
process. These rules are applicable to all
installations which store/ handle threshold
Under the main provision of this Act, prior quantity of 200 MT or more.
consent of the State Pollution Control Board
is required regarding discharge or emission Salient provisions to be complied with are -
of air pollutants for operation of an industry
as specified in schedule which includes An occupier who has control of operations
Petroleum Industry Installation. shall identify the major accidents likely to
occur and shall take adequate steps to
Strict compliance with standards/ prevent such accidents and to limit their
conditions laid down by the Board or consequences to persons and environment.
specified in the consent order must be
ensured. State Pollution Control Board/ Factory
Inspectorate shall be informed immediately
Application for renewal of consent must be in case of any major accident followed by a
submitted at least one month prior to expiry report in the prescribed format.
of the current consent order which is
generally valid for one year. Detailed safety report containing the
information as specified is to be submitted
c) The Environment (Protection) Act- to the concerned authorities.
1986 :
An uptodate on-site emergency plan has to
The Water Act-1974 and Air Act-1981 deal be maintained for dealing with any major
specifically with water and air pollution accident or disaster situation likely to affect
while this act deals with environment as a the environment. Off-site emergency in
whole including prevention of hazards to coordination with all industry
human beings, other living creatures, soil, establishments.
plants and property.
Occupier shall take appropriate steps to
This act empowers Central/ State inform persons outside the installation
Government to take all such measures it either directly or through District
may deem fit for protecting and improving Emergency Authorities, who are likely to be
the quality of environment. in area which may be affected by major
accidents about
*(Air pollution means presence in the
atmosphere, of any solid, liquid or gaseous i) the nature of major accident hazards
substances including noise in such ii ) the safety measures required to be
concentration/ intensity that may be adopted ( Do's & Dont's)
injurious to human being or other living
creatures or plant or property or e) Environmental Clearance for New
environment.). LPG Bottling Plants :

Several rules for the specific areas have A. Guidelines for Siting Industry
been/ are in the process of being notified
under this Act. This also includes issuance Ministry of Environment have laid down
of various standards for effluent water, certain guidelines for sitting of industries
atmospheric emissions/ air quality, storage/ which includes LPG installation. While
handling of hazardous chemicals, solid selecting a site, enough care should be taken
waste etc. to minimise the adverse impact of the
operations in neighbourhood and natural
d) Manufacture/ Storage and Import of life sustaining systems.
Hazardous Chemicals Rules-1989
Letter of intent of the industry can be
These rules have been framed by the converted to the Industrial Licence only
Ministry of Environment and Forests under after the following conditions are fulfilled :
the provision of E.P. Act, 1986 for
prevention/ mitigating pollution of
The State Director of Industry confirms that under Water Pollution Control Act, 1974
the site of the project has been approved and Air Pollution Act, 1981.
from the environmental angle by the
concerned state authorities. 2.5 SUMMARY OF
RECOMMENDATIONS OF VARIOUS
The Project Authorities commit to State and COMMITTEES ON LPG SAFETY :
Central Governments to install the
appropriate equipment and implement the 1) Vasudevan Committee - 1983 (MOP&C)
measures prescribed for prevention and
control of environmental pollution. Ministry of Petroleum & Chemicals had set
up a high level commitee in May, 1983
B. Procedure for obtaining headed by Shri R. Vasudevan, the then Joint
Environmental Clearance : Secretary, Deptt. of Petroleum to review all
safety and operational procedures adopted
Firstly, No Objection Certificate (NOC) has in LPG filling plants, transportation of LPG
to be obtained from concerned State by rail/ road, and in the distribution/
Pollution Control Board by submitting delivery of LPG cylinders. Several
application in the prescribed form recommendations for improvements in
alongwith detailed project report. operations/ systems were made by the
committee for adoption/ implementation by
Final clearance from environmental angle is the oil industry. Gist of key points
to be obtained from Department of pertaining to the recommendations are
Environment Govt. of India. The following given below :
documents will have to be submitted for
obtaining clearance : 1.0 LPG BOTTLING PLANT

- Detailed Project Report (DPR) i) Location - Should not adjoin


- Response to questionaire (Prepared by residential areas
DOEn.) ii) Size - Desirable to restrict to 25000
MTPA on 2 shift basis.
- No objection Certificate (NOC) from
State Pollution Control Board. iii) Layout - Provision of 80 M wide green
belt beyond perimeter wall, access
- Detailed Environmental Impact roads etc.
Assessment (EIA)
- Risk Analysis Study Reports iv) Cylinder Filling - 100% cross
- Disaster Management Plan schecking of weighments on manual
- Master Rehabilitation Plan, duly scale.
approved by State Govt. (where
required) v) Cylinder Testing - Use of compact valve
- Green belt Development Plan. tester, water bath check for leaks.
- Safety Manual/Code.
vi) Cylinder Handling - Conveyor system,
The Department of Environment, after loading/ unloading at 15 M distance
considering these documents and from shed.
presentation by the industry member will
give clearance with/without special vii) Evacuation of leaky cylinders - Use of
conditions to be complied with. A six proper evacuation system and recovery
monthly report on the progress of the of LPG, gas freeing prior to repairs/
facilities being provided for pollution replacements of valve.
control is to be submitted to Department of
Environment till the completion of the viii) Cylinder Storage - Vertical stacking in
report. small lots with min. separation distance
of 1 metre seggregated storage for
Finally, before commissioning of the plant, empty and filled cylinders, mastic
consent has to be obtained from the State flooring in the shed.
Pollution Control Board for the discharge of
liquid effluent and atmospheric emission
ix) Other Safety features/ practices - Fail- iv) Customer Education - Audio Visual
safe shut-off valves, extraction of gas/ aids/ films on TV , booklets on LPG
air mixtures, adequate communication safety emergency complaint cells etc.
facilities etc. One designated Safety
Officer for each plant. v) Control and Supervision - System of
periodic inspection to oversee and
x) Manpower & Training - LPG plants to control the working of the distributors
be headed by Sr. Officers. Structured by oil companies.
training/ refresher courses for staff and
officers on LPG operations, emergency
handling etc. No contract labour on I) EXPERT COMMITTEE (POST
shop floor for LPG operations. REVIEW OF VSC) -1986
(MOP&C) :
xi) Fire Prevention/ Fire Fighting - Strict
security check prevention of smoking, 4. An expert committee was set up in May,
Gas detection/ alarms, automatic Fire 1986 by Ministry of Petroleum & Chemicals
Water deluge/ sprinkler system. to review the safety and operating
Automatic starting of Fire Water procedures in LPG filling, transportation
Pumps, fire drills etc. and distribution in light of the experience
gained by oil companies and also the safety
1.0 CYLINDERS/ VALVES/ REGULATORS practices followed by International
Organisations.
3. Standardisation and strict quality control in
manufacture of cylinder and fittings, 5. Summary of recommendations is given as
industry inspection system for quality below
assurance etc.
A) LPG BOTTLING PLANT :
2.0 TRANSPORTATION OF LPG :
i) Layout - Typical layout showing the
i) Bulk by Rail - LPG movement in bulk safety distances have been specified for
rake of 68 wagons, unloading/ loading 12500 MTPA bottling plants. Concept
in lot of 34 (500 MT) wagons. of 80M green belt/ buffer zone around
Provision of remote operated water LPG bottling plant as recommended by
sprinklers at Gantries. Vasudevan Committee has been
replaced by min. 92 M safety distance
ii) Bulk by Road - Safety training of of LPG sphere (600MT) from property
Driver/ Attendant, special safety wall.
precautions during loading/ unloading
LPG. ii) LPG Storage - No. of storage vessels :
as per OCC norms -
iii) Cylinders by Road - Vertifical stacking,
gradual switchover to palletisation. a) 25,000 MTPA Rail - fed plant 4x600 MT
spheres.
3.0 LPG DISTRIBUTION :
b) 25,000 MTPA Road - fed plant 2x600
i) Distributor's godown - Properly MT spheres +1x100 MT bullets.
designed distributor godowns with
mastic covered flooring, fire fighting c) 12,500 MTPA- Road fed plant 5x100
equipment etc. MT bullets

ii) Delivery Equipment - Standardisation iii) Bottling Plant Shed - Single shed for
approach with cage design, use of 3 empty/filled cylinder-cum-filling plus
wheeler scooters/ delivery van. one cold repair shed.

iii) Training of delivery boys/ mechanics - iv) Cylinder Filling & other equipment - A
suitable training programme by oil Carousel Machine with 12 filling heads
companies with certification scheme. for 12,500 MTPA plant/ 24 filling
heads for 25000 MTPA plant. Other
facilities should include automatic Deluge sprinkler system for 2.5 times the
check scales, test bath. CVT, on-line surface area of one sphere where 4 NOs. of
cylinder evacuation and purging spheres are installed with 10 LPM/ Sq.M.
facilities, Off & On screwer, telescopic water denstiy.
conveyor for cylinder loading, cylinder
washing and drying unit etc. b) Spray system for 3 segments at a time with
10 LPM/ Sq.M. water density + 200
v) Empty & cylinder storage - Cu.M/hr. for operation of 2 nos. of turrets.

a) No. of empty cylinder : one and a half days vi) Min. of 2 Nos. of diesel driven water pumps
& to provide 100% requirement plus one no.
b) No. of filled cylinder : one and a half days. of electric motor pump (50% requirement as
standby).
vi) LPG vapor extraction blower - This
needs to be provided to cater to LPG vii) Water storage min. 4 hours aggregate
accumulation in filling/ cylinder pumping capacity.
storage shed particularly in low lying
areas. (III) SUDHA JOSHI COMMITTEE - 1987 :

vii) Other Safety Features - Remote control Ministry of Petroleum & Natural Gas in 1986
valves on LPG lines, excess flow had set up a committee headed by Mrs. Sudha
valves, safety valves, pop off valves, Joshi, the then M.P. and Marketing Directors of
Gas detection system etc. as specified Oil Companies as members with a view to
by VSC also. provide better services to LPG users with due
regard to safety.
(B) BULK LOADING/ UNLOADING:
Brief summary of important recommendations
2.0 Nos. & 6 Nos. truck unloading points w.r.t. safety aspects are outlined below :
for 12,500 MTPA and 25000 MTPA
plant respectively.  Streamlining of registration/ release of LPG
connections, issuing booklet like ration card
6. 2 Rail spurs for unloading of 34 wagons at a to each consumer etc.
time with use of suitable compressors.
 Use of auto-driven vehicles to be
(C) FIRE PROTECTION FACILITIES : encouraged for delivery of refills.

i) Hydrant system around LPG plant/  Consumers to use only BIS marked hot
equipment. plates.

ii) Remote manually operated water spray  Distributors to check weight of at least 10%
for LPG shed dividing area into 13 of cylinders before accepting deliveries. Oil
Mx40 M zones/ segments. companies to ensure pre-delivery
checks by the Distributors.
iii) Remote manually operated water
deluge/ sprinkler for LPG vessels/  Caging of trucks carrying filled LPG
spheres. cylinders.

iv) Water turrets for LPG pumps/  - Oil companies to use only
compressors, bulk loading/ unloading aluminimum/ PVC seals with different
area. colour code of filling plant embossed.

v) Pumping requirement shall be based on  Periodic safety inspection of equipment at


the maximum of the following : consumer premises.

a) Deluge/ spray system for total in case of 2  Regular training of delivery boys by the oil
spheres with water density of 10 LPM/ Sq. companies.
M.
OR
 Emergency and complaint cells to be
operated by oil companies in LPG marketed
towns.

 Consumer education in LPG SAFETY


THROUGH TV media and curriculam to
high school.

 - Oil companies to strengthen the


inspection system of LPG bottling plants
and working of the Distributors.

 Establishment of more bottling plants near


the consuming centre to the extent possible.
CHAPTER 3

PLANT LAYOUT

3.1 GENERAL (f) Predominant direction of wind and velocity


shall be considered.
The general layout principles of LPG storage,
bottling and bulk handling facilities have been (g) Longitudinal axis of horizontal vessels
detailed in the chapter, which also conform to (bullets) shall not be pointed towards other
OISD Standard-118 on layout. The various vessels, vital process equipment and control
facilities within LPG storage and bottling room.
premises shall be located based on Table-I and
Table-II. (h) Storage vessels shall be located downwind
of process units, important buildings and
3.2 LOCATION & SAFETY DISTANCES : facilities.

3.2.1 LOCATION : (i) Storage vessels shall not be located within


the same dykes where other flammable
While assessing the suitability of any site for liquid hydrocarbons are stored.
location of LPG storage facilities, the following
aspects shall be considered : (j) Storage vessels shall be laid out in single
row both in case of the spheres and bullets
(a) In addition to the requirements for safety within a group. Spheres and bullets shall
distances as given in Table I & II, the not be grouped together and will be
location of residential quarters, other provided with separate piping manifold.
industries, public railways, public roads,
public waterways, overhead power lines, (k) Storage vessels shall not be located one
working areas etc. based on risk analysis above the other.
study of the proposed site should be taken
into account as required by the 3.2.2 SAFETY DISTANCES :
Statutory/State Govt. regulations.
The safety distances as given in Table- I & II are
(b) Adequate availability of water from a nearby the distances in plane between the nearest point
reliable source of water should be ensured. on a vessel other than the filling/ discharge line
and a specified feature, e.g. adjacent vessel, site
(c) The topographical nature of the site with boundary etc.
special reference to its effect on the disposal
of escaping LPG shall be considered. 3.3 TYPE OF STORAGE VESSELS :

(d) The access of mobile fire fighting equipment 3.3.1 HORIZONTAL CYLINDRICAL
to the storage vessels under all foreseen VESSELS:
circumstances, preferably from two sides
and upwind (prevailing wind) is an Horizontal bullets with volumetric capacity up to
important parameter. 400 Cu.M each shall be used for storing LPG.

(e) The availability of space for future extension 3.3.2 SPHERICAL VESSELS :
of LPG facilities which will still comply
with the safety standards shall be taken into Spheres are the most economical form of storage
account. for capacities of more than 400 Cu.M of each
vessel.
3.4 LAYOUT: Top surfaces of all the vessels installed in a
group shall be on the same plane so that the
The following aspects shall be considered while safety blowout from them do not affect each
establishing layout of LPG storage vessels. A other.
typical layout of LPG storage vessels is shown in
Annexure-I. It is preferable to provide separate manifolds
with independent pumping facilities for bullets
3.4.1 LPG STORAGE FACILITIES: and spheres so as to avoid any chances of
overfilling of adjacent vessels due to gravitation.
(a) CONFINEMENT/ GRADING - Kerb wall
shall be provided around sites of the storage A typical layout plan of LPG sphere area with
vessel with concrete flooring of the ground major safety requirement of distances, drawing
under vessel and extending upto minimum sump, pump location etc. is enclosed at
distance of D/2 or 5M whichever is higher and Annexure-I for general guidance.
atleast 5 M(min.) from the edge of the Horton
Spheres with a slope of 1:100 (min.). Grading of 3.5 LPG BULK HANDLING FACILITIES :
the ground underneath should be levelled so as
to direct spillage from the fourth side to a 3.5.1 LPG tank lorry loading/ unloading
shallow sump away from the storage vessel and gantry shall be covered and located in a
kerb wall height shall be minimum 30 cm but separate block and shall not be grouped
shall not exceed 60 cm otherwise evaporation of with other petroleum products.
spilled LPG may get affected.
3.5.2 LPG loading/ unloading rail gantries
(b) SPILLS AND LEAKS - Spillage shall have separate rail spur and be
collection shallow sump shall be located at a grouped separately from other rail
distance where the flames from sump fire will shunting facilities by minimum
not impinge on the vessel. This distance shall distance of 50M.
not be less than the diameter of the nearest
vessel or 15M whichever is higher. The 3.5.3 Space for turning with minimum radius
capacity of the collection sump shall be based as of 20M for tank lorries shall be
per drawing enclosed (Annexure-I). This provided commensurate with the
drawing is valid for 2 spheres or more. In case capacities of the tank trucks.
of one sphere, the sump size shall be equal to
layout of 2 spheres. 3.5.4 LPG tank wagon loading/ unloading
shall be restricted to a maximum of half
(c) PIPING - Only piping associated with the rake, present capacity of which is 500
storage vessels shall be located within the tonnes. If full rake loading/ unloading
storage areas or between the storage area and the is envisaged this shall be done on two
manifold system. separate rail gantries separated by a
minimum distance of 50M. In case of
(d) SURFACE DRAINAGE - In order to 8-wheeler wagons half rake unloading
prevent the escape of spillage into the main capacity shall be 600 tonnes.
drainage system, surface water from the storage
area and from the manifold area shall be 3.5.5 Maximum number of LPG tank lorry
directed to the main drainage through a water bays shall be restricted to 8 in one
seal to avoid the spread of hydrocarbon. group. The bays should be designed in
such a way that the drivers cabin will
(e) GROUPING - Vessels shall be arranged be facing the exit direction, and shall
into groups, each having a maximum of six have no other obstructions. Safety
vessels. Capacity of each group shall be limited distance between the two groups shall
to 15000 Cu.M. There shall be minimum not be less than 50 M.
spacing as specified in Table-I between adjacent
vessels. 3.5.6 Adequate permanent protection for tank
lorry discharge pipeline island shall be
(f) Spheres and bullets shall be treated as provided. The minimum width of such
separate groups with minimum 30 M safety pipeline island shall be 1 M.
distance between two groups.
3.6 LPG BOTTLING FACILITIES ;
3.6.8 Escape routes shall be specified in LPG
3.6.1 LPG bottling facilities should be sheds for evacuation of employees in
located at a safe distance from other emergency.
facilities with minimum ingress of
trucking traffic and upwind direction 3.6.9 There shall not be any trapping of
with respect to bulk storage. personnel in LPG sheds by conveyors,
cylinders and other facilities. If such
There shall not be any deep distances in trapping cannot be eliminated, it should
the surrounding areas to avoid LPG be kept to the minimum. In such places
vapour settling. sufficient arrangements for escape
routes to be provided.
3.6.2 Bottling section shall be of single storey
having asbestos roofing and open from 3.6.10 All steps forming part of the escape
all sides for adequate ventilation so that routes shall be minimum 1.2 M with
leaked gas can drift away from the treads 30 cms (Min.) and maximum
shed. RCC roofing shall not be used. rise of 15 cms.
Antistatic mastic flooring conforming
to IS-8374 shall be provided in the LPG 3.7 PROTECTION OF FACILITIES :
filling shed/ cylinder storage including
cold repair shed to avoid frictional 3.7.1 There shall be road all around the
sparks. Fire-proofing upto full height various facilities within the bottling
of structural columns and Antistatic plant area for accessibility of fire
mastic coating upto 1.5 (Min.) shall be fighting operations.
done of the supporting columns of the
shed. 3.7.2 There shall be proper industry type
boundary wall atleast 3 M high with
3.6.3 3 Sheds, 1 for storage of empty 0.6M barbed wire overhand all around
cylinders and filling, 1 for filled bottling plant including buffer zone
cylinders storage and 1 for cold repairs (green belt) unless the bottling plant is
of defective cylinders shall be provided otherwise protected as a part of refinery
(Annexure-II). Empty cylinders complex.
storage area shall be properly
segregated from filling machines by 5 3.7.3 Emergency escape exit with proper gate
M (Min.). Cylinders shall always be shall be provided in the earmarked
stacked vertically in two lines. For zone.
details of cylinder stacking pattern refer
Annexure-I of chapter 7. 3.7.4 Provision for green belt development of
minimum 30M width within the
3.6.4 LPG cylinder filling machines and boundary wall shall be made and
other related testing facilities shall be segregated from hazardous/ licensed
organised in sequential manner as area by 1.0M high brick masonary wall
shown in line diagram (Annexure-II of with 0.6M high barbed wire fencing as
Chapter 7). shown in the typical layout (Annexure-
II).
3.6.5 A separate shed shall be provided for
carrying out cold repairs/ degassing of 3.7.5 LPG lorry parking area (Bulk/Packed)
defective cylinders. shall be located in a secured area with
proper hydrant coverage.
3.6.6 Cylinder storage shall be kept on or
above grade and never below grade in 3.8 UTILITIES :
cellar or basement.
Utilities consisting of fire water pumps, admin.
3.6.7 Filled cylinders shall not be stored in building, canteen, motor control centre, DG
the vicinity of cylinders containing room, air compressors, driers etc. shall be
other gases or hazardous substances. separated from other LPG facilities and located
as per the area classification as specified in
Table-I (Annexure-III).
ANNEXURE III
TABLE - I
INTERDISTANCES FOR LPG FACILITEIS
---------------------------------------------------------------------------------------------------------------------------
1 2 3 4 5 6 7
---------------------------------------------------------------------------------------------------------------------------

1. LPG Storage vessels * T-II 30 30 30 15 60

2. Boundary/property line/ T-II - 30 30 30 30 -


group of bldgs. not associated
with LPG plant

3. Shed-LPG 30 30 15 30 30 15 60

4. Tank wagon/Tank truck 30 30 30 50 50 30 60


gantry-LPG

5. LPG/other rail spurs 30 30 30 50 50 30 60

6. Pump house/Comp.house 15 30 15 30 30 - 60
(LPG)

7. Fire Pump House 60 ** 60 60 60 60 -


---------------------------------------------------------------------------------------------------------------------------
Notes :
1. All distances are in Metres.
2. Notation :
T-II - Refer Table - II
 1/4 of sum of diameters of adjacent vessels OR Half the diameter of the larger of the
two adjacent vessels, whichever is greater.
** Any distance for operational convenience.

3. Distance of stabling line shall be as per minimum Railway Standards.


4. Provisions of 30M green belt is over and above the safety distances from property line as given in
Table-I and II.
TABLE - II

DISTANCE BETWEEN LPG STORAGE VESSELS AND BOUNDARY/ PROPERTY


LINE/GROUP OF BUILDINGS NOT ASSCIATED WITH LPG PLANT
---------------------------------------------------------------------------------------------------------------------------
Capacity of each Distance
vessel (Cu.Mt. of water)
---------------------------------------------------------------------------------------------------------------------------
10-20 15
21-40 20
41-350 30
351-450 40
451-750 60
751-3000 90
--------------------------------------------------------------------------------------------------------------------
Note : All distances are in Metres

CHAPTER 4

DESIGN CRITERIA FOR LPG BOTTLING PLANTS


b) Bullets are recommended for Micro and
4.1 GENERAL Mini plants. For Major and Mega plants,
spheres are recommended.
This section describes the broad process design
and safety features required in a typical LPG c) Recommended maximum water capacity of
bottling plant. For design details about the plant a sphere (based on 18 meters diameter
layout reference should be made to Chapter 3 of maximum) is approx 3,000 cubic meters.
this standard. For bullets the maximum recommended
water capacity is 400 cubic meters.
4.2 DESIGN BASIS
4.2.3 LPG LOADING/ UNLOADING
4.2.1 PLANT CATEGORIES FACILITIES

Based on operation, maintenance and safety For Micro and Mini plants only truck loading/
considerations, the plants are classified into the unloading facilities are recommended. For Mega
following four categories depending upon their and Major plants both rail and road tanker
capacities. loading/ unloading facilities are recommended.

Category Capacity Remarks To reduce the risk of accidental LPG release


(MTPA) during product transfer, excess flow check
valves shall be provided in LPG loading/
Micro Below 6000 Single shift/ unloading lines.
(small) stationary machine
4.2.4 CYLINDER FILLING FACILITIES
Mini 6000 and below Double shift/
22,000 stationary machines A. FILLING MACHINES AND WEIGHING

Major 22,000 and Double shift/single I) The filling machines shall be provided with
below 68,000 carousel auto cut-off system so that the liquid and
gas supply is cut off when the desired
Mega 68,000 and Double shift/ multi quantity of product has been filled in the
above carousel cylinders. The filling pressure shall not be
more than the design pressure of the
The filling capacities, per carousel on a two shift cylinders i.e. 16.9 kg/sq.cm. gauge.
basis are given below :
ii) Filling machines in a carousel/stationary
No. of filling Capacity Facilities filling machines shall not have a weighment
machines per (MTPA) error of more than +1% of the net quantity
carousel of the LPG filled in the cylinder, with a
capacity of 14.2/19 kg.
12 22,000 1CS 1 DCVT 1 in-line bath
18 34,000 2 CS 2DCVT " iii) It is recommended that in-line check weigh
24 44,000 2 CS 2DCVT " scales with a minimum of 50 gms.
36 68,000 3 CS 3DCVT 2 in-line baths graduation be installed so that all the
cylinders can be check weighed after filling.
CS - Check Scale
DCVT - Double Compact Valve Tester B. LAYOUT AND SAFETY

4.2.2 STORAGE CAPACITY i) The cylinder filling area shall be completely


open type and covered from top with
a) The designed storage capacity in bottling asbestos roof designed to ensure good
plants shall be as per the OCC guidelines. natural ventilation, RCC roofing shall not
It is preferable to divide the storage to be used.
minimum number of vessels. However for
convenience of operation, maintenance and The filling area will not be on upper floors
inspection, 3 vessels are required as of building or in cellars.
minimum.
ii) As far as possible, the floor area shall not compressor running is envisaged, 50% standby
have any channels or pits. Where these are capacity shall be provided.
necessary for conveyors or other equipment
like weigh machine etc., suitable gas (B) Service Water
detection system shall be provided.
Additionally they shall be ventilated Service water is required for the cylinder
through ducts fitted with blowers to outside washing equipment and leak check bath,
of the shed at safe location. The whole of compressor cooling and in hose stations for
the LPG filling shed flooring shall be washing etc.
provided with bitumenistic mastic flooring.
Water shall be provided at a pressure of about 3
iii) Adequate lighting shall be provided in the Kg/sq.cm.g. If one pump is envisaged to run
cylinder filling area. Additionally normally, another pump with 100% capacity
emergency lighting shall also be provided at shallbe provided as a standby. Where more than
critical places. one pump running is envisaged, 50% capacity as
standby shall be provided.
iv) Water drains from the cylinder filling area
where they enter an outside drainage i) Water Quality
system, shall be provided with vapour seals.
Water shall be of potable quality conforming to
v) Fixed water spray system shall be installed IS-10500-1983 (Indian Standard Specification
for fire fighting inside the cylinder filling for Drinking Water). Suitable treatment facility
area as described in section 4.4. Besides (Softener or demineraliser) shall be provided
this, access shall be made available for other whenever required to meet the above
fire fighting systems. specifications, depending upon the quality of
available water.
4.2.5 CYLINDER STORAGE
ii) Water Cooling Systems
Maximum cylinder storage of empty and filled
cylinders combined shall be restricted to a total These can be either closed circuit or once
of 3 days bottling capacity of the plant. Storage through to drain type. Control of water quality
area requirement shall be based on the stacking is better, in closed circuit system. This in turn
pattern of filled and empty cylinders described leads to much less downtime for cleaning.
in section 7.2. Closed circuit water circulation system
circulating inhibited potable water can be
4.2.6 UTILITIES provided. Following shall be the concentration
of inhibitors.
(A) Compressed air
Zinc as Zn 5 ppm
The quality of instrument air shall conform to
the following specifications : PH 7-8

Pressure 7 kg/sq.cm.g The circulating water heat to be dissipated


Moisture Dew Point, -15 deg.C at through exchangers (not by evaporation).
7 kg/sq.cm.g
Quality Oil free Alternately, if the once through to drain system
is provided, it requires to be periodically cleaned
For the plant air/ service air, the specifications by chemical cleaning. Accordingly the design
are given below : should have provisions to hook up some portable
type of chemical cleaning kit which may contain
Pressure 7 kg/ sq.cm.g tank, pump etc. for circulation. During this
Moisture No free moisture operation the equipment is taken out of service
Quality Oil free and put back into service after the heat transfer
surfaces are cleaned. Normally the cleaning
If one compressor is envisaged to run normally, consists of degreasing, followed by circulation of
another standby compressor of 100% capacity inhinbited hydrochloric acid solution and finally
shall be provided. When more than one passivation using trisodium phosphate.
(C) Emergency Power Kg/Sq.cm.g at 65 Deg C temperature. LPGs
with higher vapour pressure are not expected to
The plant shall be provided with diesel be stored in bottling installations.
generating set for operating the essential
systems such as the instrumentation and safety
systems (gas detectors, automatic fire water This (IS:4576) LPG will have a vapour pressure
sprinkler system) and minimum lighting during (depending on composition) of around 13-14
the grid power failure. (max.) Kg/Sq.cm.g at 55 Deg C.

4.3 LPG STORAGE VESSELS This forms the basis of 14 Kg/sq.cm.g as design
pressure for IS:4576 LPG storage at bottling
Following are recommended : installations.

4.3.1 MECHANICAL DESIGN The recommended design pressure and


temperature shall be treated as MINIMUM
The mechanical design of storage vessel shall be requirement and other design consideration and
based on following considerations : Statutory requirements may call for something
additional.
a) Design Code : ASME SEC. VIII or IS-2825
or BS - 5500 or equivalent duly approved by e) Other Considerations
CCE.
Corrossion Allowance : 1.5 mm (minimum)
Design shall take into account the Static and
Mobile Pressure Vessels (Unfired) Rules 1981 Radiography : Full
also. (A single code shall be adopted for design,
fabrication, inspection and testing), i.e. ASTM Stress Relieving : 100% irrespective of
and BS shall not be combined. thickness.

b) Material: Micro-alloyed steel containing Ni, Wind pressure : as per IS: 875
Mb, Va shall not be considered.
Earthquake pressure : as per IS:1893
Since H2S presence cannot be completely ruled
out in the Refinery LPG storages, high stress Hydrotest pressure : As per Design Code
material shall not be used as it is prone to
Hydrogen induced stress corrosion cracking. 4.3.2 FITTINGS

c) Recommended maximum tensile stress shall Spheres/ bullets shall have a single nozzle at the
be below 80,000 PSI. bottom for inlet as well as outlet. The nozzle
shall be full welded pipe, stress relieved along
d) Recommended material of construction for with th vessel and shall extend minimum 3
sphere/ bullet : meters from the shadow of the sphere/ bullet. A
remote operated shutdown value (ROV) shall be
i) For Refinery service : ASTM A516 Gr. provided on this bottom nozzle at a distance of
60 (BS-5500 shall not be used for the above). atleast 3 meters from the shadow of sphere/
bullet. The nozzle pipe shall have a slope of 1.5
Code and Material used should be the same. Deg.

ii) For marketing installation : Where H2S is There shall not be any other flanges, manhole,
not present ASTM A 516 Gr. 70 or A 537 instrument tapping on this nozzle upto the ROV
CLASS 1. or on sphere/ bullet bottom. In order to avoid
stress on the nozzle due to relative settling of
iii) Design temperture : -27 o C to +55 Deg C. support and sphere, supporting the bottom
nozzle from the vessel support legs should be
iv) Design Pressure : 14 Kg/ Sq.cm.g Vapour considered.
pressure of LPG (as per IS: 4576) at 55 Deg C.
The top vapour zone of the vessel shall be
Marketable LPG conforming to IS: 4576 can provided with nozzles for vapour outlet and
have a maximum vapour pressure of 16.87
recirculation, which shall also be provided with vertically upwards to atmosphere at an elevation
fire-safe ROVs. of 3 meter (minimum) from the top of the
highest platform in a radius of 50 metre for
Two independent level indicators, a high level effective dispersion of hydrocarbons. In this
switch, pressure gauge and a manhole shall be case, isolation valves on down stream of PSVs
provided on top. are not required. A weephole with a nipple at
low point shall be provided on the vent pipe in
Each vessel shall have atleast two safety relief order to drain the rain water which may get
valves, each set at not more than 110% of design accumulated otherwise. Weephole nipples shall
pressure of the vessel and having the relieving be so oriented that in case of safety valve lifting
capacity adequate for limiting the pressure build and consequent fire, the flame resulting from
up in the vessel not more than 120% of design LPG coming out from weephole does not
pressure. impinge on the sphere or structure. A loose
fitting rain cap with a chain (non sparking)
All the fittings shall be suitable for use at not fitted to vent pipe shall be provided on top of
less than the design pressure of the sphere/ PSV.
bullet and for the temperatures appropriate to
the worst operating conditions. The remote 4.4 SAFETY/ SECURITY SYSTEM
operated valves on the sphere/ bullet connected
lines shall be fire-safe type. The flange joints of The features of safety/ security system for the
these valves shall either have spiral wound different areas in the LPG bottling plants shall
metallic gaskets or ring joints. Plain asbestos be as follows :
sheet gaskets shall not be used.
4.4.1 AUTOMATIC FIRE PROTECTION
Flange connections shall be a minimum of SYSTEM
ANSI-300 lb flange class. All fittings shall be a
minimum of 20 MM. Automatic fire protection (Fixed) system based
on heat detection through thermal fuses/ quartz
4.3.3 INSTRUMENTS bulbs/ EP detectors shall be employed. Sensors
shall be installed at all critical places described
i) The storage vessel shall have minimum below :
two different type of level indicators and one
independent high level switch. One level (A) LPG STORAGE AREA
indicator shall be float type and the other may be
differential pressure type in case of spheres. DP In storage area these detectors shall be provided
type level transmitter shall either be sealant encircling each vessel, equispaced with a
filled type or LP side tubing heat traced. maximum spacing of 1 meter at an elevation of
Magnetic float type gauge is recommended for about 1.5 to 2.0 meter from bottom of vessel.
bullets in place of differential pressure type. Also minimum 2 nos. detectors shall be
High level alarms shall be set at not more than provided at the top of the vessel and atleast one
85% level of the volumetric capacity of the near the liquid line ROV to take care of failure
vessel. Audio visual indication shall be at local of flanges. In case of an automatic thermal fuse
panel & control room. based fire protection system the instrument air
supply pressure to thermal fuses shall be
ii) The relieving load for the safety valves, maintained through a pressure control valve and
(minimum 2 nos. installed, each having 100% a restriction orifice.
relieving capapcity) shall be based on fire
condition and no credit shal lbe takne for fire The thermal fuses shall be designed to blow at
proofing on the vessel. 79 deg C temperature (max). Instrument air
will start leaking as a result of thermal fuse
For safety reasons, the discharge of safety valves blowing. The capacity of the restriction orifice
shall be connected to flare system wherever is such that the discharge of air through even
available. In this case PSVs shall have lock open one thermal fuse will depressurise the
(or car seal open) type isolation valves on both downstream side of the restriction orifice to
sides of Pressure Safety Valves (PSVs). below set point of the pressure switch.

In case of non availability of flare system, the The actuation of pressure switch on any one of
discharge from safety valve shall be vented the vessels shall initiate the following :
draining/ sampling are done on a routine basis.
- an audio visual alarm at the local/ main Audio visual alarms showing the location of gas
control panel and fire water station, leakage shall be provided on the control panel.
indicating the vessel on fire. First level alarm can be set at 20% LEL and
second level alarm at 60^ LEL.
- the Remove Operated Valve (ROV) on liquid
inlet/ outlet line to the affected vessel will
close.
4.4.3 GAS EXTRACTION SYSTEM
- the ROVs on vapour balance line and liquid
return line of the affected vessel will close. A gas extraction system having suction points at
critical places where gas concentration is high
- LPG pumps and compressors in LPG storage like carousel, evacuation, valve change shed etc.
area will trip. shall be provided.

- the deluge valves on fire water supply lines to 4.5 OTHER EQUIPMENT/ SYSTEM
that vessel will open.
4.5.1 BOTTLING PUMPS
Additionally push buttons for initiating all the
above actions shall be provided on remote There shall be a minimum of two pumps,
operating panel and also in field at safe location including one standby. Pumps shall be provided
for enabling manual actuation of a trip by with suction and discharge pressure gauges, a
operator. In the field, manual bypass valves of high point vent to safe height or flare, and a
fire water deluge valves shall also be provided. suction strainer. Mechanical seal shall be
Arrangement to routinely test the security provided (double mechanical seal with seal
system shall also be provided. failure alarms is preferred). A pressure switch
actuating a low pressure alarm in control room
(B) OTHER AREAS shall be provided, taken from pump discharge.
Pumps shall be designed to build a discharge
Detectors shall be placed at critical locations in pressure such that the pressure at the carousel
LPG sheds (filling, cylinder storage, testing, filling machine is at least 5.0 kg/sq.cm.g. above
evacuation, etc.) loading/ unloading gantries, the vapour pressure at the operating
LPG compressor house, piping manifold, repair temperature.
sheds etc. Opon actuation there shall be alarm
in central panel, LPG pumps and compressors Typical sketch of a bottling pump installation is
would trip, ROVs (wherever provided) on LPG enclosed as Annexure-1.
supply and return lines would trip and the
deluge valves on fire water sprinkler system will 4.5.2 LPG COMPRESSOR
get actuated.
Gear driven compressor shall preferably by used.
The fire water deluge valves shall be kept However belt driven compressors can also be
outside the kerb wall at a safe distance in case of used provided the belts used are antistatic type &
sphere/ bullet, and located 15 M away from fire resistant.
limits of other sheds or shadows of spheres. A
fire wall shall be provided for the protection of There shall be a minimum of two compressors
the deluge valve and for personal protection of including one as a standby.
the operator.
The operating parameters shall be decided on a
4.4.2 GAS DETECTION SYSTEM case to case basis. However, typical operating
conditions may be as follows:
Suitable gas detectors shall be placed at
identified critical locations in the LPG storage, Suction pressure 10.0 kg/sq.cm.g abs
compressor house, pump house, filling shed, (max.)during unloading
cylinder storage area, evacuation/ testing area, 2-11.8 kg/sq.cm.g abs
LPG loading/ unloading area. during vapour recovery.

This shall include the area described in 4.2.4B Discharge pressure 13.0 kg/sq.cm.g. abs
and shall also include places where water, during unloading.
11.5 kg/sq.cm.g. abs
during vapour recovery. - Pressure gauges
- Level gauges and high level alarm
Compressor shall be provided with the following switches
features as a minimum :
- Pressure relief valves and vent valves
- Pressure gauges in suction and discharging to safe height.
discharge.
- Other trims like drain valve, utility
- Temperature gauge in discharge connection.

- Discharge safety valve and a vent valve, Typical sketch of cylinder evacuation facility is
their outlets leading to flare/ safe height enclosed as Annexure-III .
outside the shed.
4.5.4 PURGING OF NEW CYLINDERS/
- Suction and discharge block valves TANKERS
(lock open type)
(a) The new LPG cylinders containing air shall
- Suction strainer be evacuated with a vacuum pump. The vacuum
pump shall be water/ oil cooled type. The
- Check valve in discharge evacuation facility shall consist of :

- A discharge to suction recycle valve for - Purging manifold


achieving capacity turndown during
startup. - Vacuum receiver fitted with vacuum
gauge, vent and drain.
Besides these, other indications/ protections can
also be provided along with those recommended - LPG vapour heaader
by compressor vendor. Typical sketch of
compressor installation is enclosed as Annexure- - Purging adaptors
II.
- Portable oxygen analyser
4.5.3 EVACUATION FACILITY FOR
SICK/ LEAKY CYLINDERS - Nitrogen cylinder manifold

The cylinder evacuation facility shall consist of : - Vacuum pump with suction strainer

- Cylinder emptying vessels (2 nos. with - Pressure regulator, relief valves etc.
attachments given below) Typical sketch of new cylinder purging/
evacuation system is enclosed as
- Compressor (1 no.) as per 4.5.2. Annexure-IV.

- Four way valves (b) Purging of tankers/ vessels shall be done


using either Nitrogen or by filling water and
- Cylinder rack, header to be provided displacing with LPG vapours.
with pressure gauge and a strainer with
isolation valves. 4.5.5 ELECTRICAL AREA
CLASSIFICATION
- The LPG line exit cylinder evacuation
area to be provided with a non-return All electrical fittings/ equipments to be of
valve before joining the main LPG Flame-proof type in vulnerable areas.
return header.
For electrical area classification refer to IS-
- Independent earthing connections shall 5571, IS-5572 (Part-1) and OISD Standard
be provided. No.113.

Each of cylinder emptying vessels mentioned 4.6 DESIGN DEVELOPMENTS


above shall be equipped with the following :
Some recent developments in equipment designs connections, a nozzle can be provided
and safety systems have taken place. These may on the common liquid inlet/ outlet line
be considered in future installations: outside the ROV, or a line to the top of
storage, to supply water and flood the
a) Systems are now available for on-line bottom portion inside the sphere with
evacuation of leaky cylinders. These water. Repairing of small leakages
would reduce the risk involved in would be easier under conditions of
handling leaky cylinders. water leakage than in the case of LPG
leakage.
b) In the event of leakage of LPG from
any of the sphere bottom area
CHAPTER 5

DESIGN OF CYLINDERS AND VALVES

5.1 CYLINDERS : IS:6240-1976 or IS:10787-1984 as amended


from time to time.
5.1.1 Since the cylinders and valves remain
in customer's premises for a longer time than in b) Bungs or Valve Pad - The bund shall
any other location, the quality of the cylinders conform to IS:3196 (Part-1):1992. It shall be
must receive utmost attention and importance. hot forged from rolled steel conforming to class
1-A of IS:1875-1978 OR IS:226-1975. The
5.1.2 The various capacities of cylinders used bung machined from such forgings shall be free
in our country for marketing LPG and the from surface defects such as fissures, surface
applicable IS code is given in the table below. cracks, porosity, lamination and pin holes etc.
The cylinders are designed, manufactured and
tested as per applicable IS codes and in c) Backing Strips; The material used for
accordance with Indian Gas Cylinders Rules, Backing Strips shall conform to IS:226-1975 Or
1981. IS:2062-1969 or steel of equivalent or superior
quality.
S.No. Water Capacity Net Weight IS Code
(in litres) (in kg.) d) Foot Rings: The foot Rings, where fitted as
a fixture to the bottom end of the cylinder, shall
1. 10.0 4.2 3196 be at least 20mm away from the circumferential
weld. The thickness of sheet from which the foot
2. 26.4 11.2 3196 ring is made shall not be less than 2.4 mm. The
foot ring may be intermittently welded and its
3. 33.3 14.2 3196 bottom edge shall be curled inwards to facilities
safe handling. It shall be provided with holes
4. 44.5 19.0 3196 for ventilation, as well as draining holes to avoid
corrosion. The maximum permissible deviation
5. 110.0 50.0 3196 from the vertical shall not exceed 1 degree. The
foot ring shall be sufficiently strong and made
NOTE : out of steel compatible with that of the steel
prescribed in IS:1079-1973 or of other steel
Bureau of Indian Standards specifications as per having equivalent properties. The bottom of the
IS:3196-(part 1) 1992 covers the design, foot ring shall not be less than 8 mm below the
fabrication and testing of welded low carbon outside bottom of the cylinder shell for cylinders
steel cylinders intended for storage and upto 34 litres water capacity. For cylinders of
transportation of low pressure liquefiable gases, more than 34 litres water capacity this value
other than toxic gases, of nominal water shall be minimum 25 mm.
capacity above 5 litres and upto and including
250 litres water capacity. The cylinders below 5
litres water capacity are covered by IS:7142- 5.1.4 CONSTRUCTION :
1974.
a) The minimum wall thickness of
Since maximum number of cylinders used in the cylinder body is to be calculated taking
country for domestic purpose are of nominal into account the test pressure, outer
water capacity of 33.3 litres, most of the details diameter and the minimum specified
are for this type of cylinders. For details on yields strength. The minimum agreed
other type of cylinders, relevant code and thickness, however, shall not be less
drawing may be referred to. than 2.4 mm and also calculated as per
Section 5.2.1 of IS:3196 (Part-1):1982
5.1.3 MATERIAL OF CONSTRUCTION : which ever is higher.

a) BODY: The cylinder should be fabricated b) The cylinder shall be welded by any
out of steel sheets manufactured conforming to suitable fusion welding method and
shall conform, as for welding procedure provided sufficient care is taken to
and welder's performance ensure complete fusion and penetration.
qualifications, to the requirements of
IS:2825-1969, when cylinder welding 5.1.5 MARKINGS ON THE CYLINDERS :
is required to be rediographed and to
the requirements of IS:817-1966, when The details of markings are standardised on the
the cylinder welding is not to be industry basis :
radiographed.
a) MARKING ON FOOT RING :
c) Before welding, the plates to be joined
shall be inspected and should be free Foot ring is stamped and embossed
from grease, oil and dirt or any other with Oil Company's name on one side
surface defects. and product trade name on other side.
The foot rings are provided with
d) The circumferential seam shall consist adequate no. of openings for
of butt joint in conjunction with Ventilation.
permanent backing material, or
alternatively a toggle joint may be used, b) MARKINGS ON VERTICAL STAYS :
ensuring that the external surface of the
container is smooth. A longitudinal Following markings are provided on
seam in case of LPG cylinders is not the vertical stays supporting valve protection
permitted. ring :

e) Surfaces of the plates at the seam shall Ist STAY PLATE


not be out of alignment with each other
at any point by more than 10% of the I) Manufacturers' identification mark/
plant thickness. logo
ii) S.No. followed by source of steel (S-
f) Welds shall not be dressed without SAIL, T-TISCO, I-IMPORTED).
approval of the inspecting authority. iii) Tare weight
The weld surfaces shall have a smooth iv) Maximum gross weight.
contour and there shall be no
undercutting. 2nd STAY PLATE

g) All welding of the shell and I) IS-No. and BIS logo


attachments shall be completed before the final ii) Water Capacity
heat treatment. iii) Maximum working pressure
iv) Test pressure
h) Welds shall have an even finish and
shall merge into the parent material 3rd STAY PLATE
without undercutting or abrupt
irregularity. i) Test dates

i) Welding electrodes used shall be such In addition test date due with appropriate colour
that the desired properties of the weld code to be provided on the inside portion of the
are obtained and the physical values of stay plat by stencilling.
the welded metal are not lower than
specified values of the parent metal, as c) MARKINGS ON BUNG :
certified by BIS.
i) Serial number of the cylinder
j) The chemical composition of the weld
material shall be compatible with that of the ii) Manufacturer's identification mark
parent metal.
iii) Tare weight
k) All welded joints shall be double
welded butt joints. In case where iv) Month and year of manufacture.
second side welding is not possible,
single welded butt joint may be used,
5.1.6 CYLINDER TESTING/ INSPECTION The maximum deviation of the shell
DURING MANUFACTURE : from a straight line shall not exceed
0.3% of the cylindrical length.
A) BEFORE CLOSING-IN OPERATIONS :
g) VALVE CONNECTIONS :
Each cylinder shall be examined for
wall thickness before the closing-in The valve connection shall consist of a
operation, circularity of the cylindrical welded pad or bung and shall be
shell and skirt portion of the ends, threaded to suit the type of valve
external and internal surface defects, specified as per IS:8737 (Part II) -
profile regularity of the ends, offset at 1978.
the joints and straightness. The
manufacturers shall assure themselves h) VALVE PROTECTION RING (VP RING)
that the wall thickness is not less than
the agreed finished thickness at any The cylinder shall have the valve
point. protected against damage by the
provision of a stout V.P. Ring welded
with the help of 3 stay plates on the
b) ROUNDNESS : body of the cylinder. The height of the
V.P. Ring from the body of the cylinder
The out-of roundness of the cylindrical shall be 122+/-3mm. The diameter of
shell shall be limited to such a value tht the V.P. Ring tube shall be 21 mm and
the difference between the max. and the should be provided with a vent hole.
min. outside diameter in same cross
section is not more than 1% of the I) HEAT TREATMENT :
mean of these diameters.
All cylinders shall be efficiently
normalised or stress, relieved in
c) SURFACE DEFECTS : accordance with the steel maker's
recommendations, after manufacture
The internal and external surfaces of and completion of all welding and
the cylinder shall be free from defects before subjecting to hydrostatic test. A
which will adversely affect the safe complete record of heat treatment cycle
working of the cylinders. shall be maintained.

d) PROFILE REGULARITY : 5.1.7 RADIOGRAPHIC EXAMINATION :

The inner surface of the end shall not Radiographic examination when
deviate from the prescribed shape by required shall conform to the
more than 1.25% of the nominal techniques and acceptability criteria set
diameter of the head skit. Such forth in the relevant Indian Standards.
deviations shall not have abrupt A reference may be made to IS:1182-
changes. 1967, IS:2595-1978, IS:3657-1978,
IS:4853-1968 and 8.7 of IS:2825-1969.
e) OFFSET AT THE JOINT : The Radiographic techniques used shall
be sufficiently sensitive to reveal the
The misalignment measure at the defect having thickness equal to 2% of
surface at the plates shall not exceed the combined thickness of the weld and
10% of the nominal plate thickness. backing strip.
Where the thickness of the ends
exceeds the shell thickness by more One out of each batch of 50 cylinders,
than 25%, the abutting edges shall be or less shall be taken for spot
reduced by smooth taper extending for radiography of the seam weld i.e. the
a distance of 4 times the offset between sample taken for Acceptance Tests as
the abutting edges. per IS:3196 (Part-1) should also be
radiographed before destructive testing.
f) STRAIGHTNESS :
5.1.8 INSPECTION OF FNISHED
CYLINDERS : e) ACCEPTANCE TEST :

a) CHECK OF WATER CAPACITY : One cylinder at random shall be taken


out from each batch of 202 or less and
The water capacity of each cylinder the acceptance test for the parent metal
shall be checked. This shall be done by and weld joint shall be carried out in
weighing, by filling the cylinder with a accordance with section 17 of IS:3196
calibrated volume of liquid or by other (Part -1)-1982 for tensile strengths
means approved by the inspecting yield strength and root bend test.
authority in order to ensure compliance
with the required specified water f) PAINTING AND FINISHING :
capacity. The tolerance for water
capacity shall be +3-0%. As per BIS code, each cylinder shall be
shot blasted for cleaning the scales, rust
b) HYDROSTATIC TEST : etc. and should be subjected to
metalising with zinc to prevent against
Each heat treated cylinder shall be corrosion. The thickness of the metal
subjected to hydrostatic test. During the film should be minimum 37 microns.
hydrostatic test, the pressure shall be After metalising the cylinder shall be
increased gradually till the required test applied with one coat of zinc chromate
pressure is reached i.e. 25.35 primer and one coat of enamel paint.
kgf/sq.cm. After the test pressure is The total dry film thickness of the paint
reached, it shall be retained for a period and metal spray thickness of the paint
of not less than 30 seconds. Any and metal spray should not be less than
reduction in pressure noticed during 67 microns.
this retention period or any leakage or
visible bulge or deformation shall be g) OVERALL DIMENSIONS OF
treated as the case of failure in the test. CYLINDER

c) PNEUMATIC LEAKAGE TEST : The following are the important


dimensions of a 33.3 Lts. Water capacity
Subsequent to the Hydrostatic test, each cylinder :
cylinder after it has been dried shall be
tested for leakage by subjecting to air I) Overall height - 625 +/-5mm
pressure of not less than 10 kgf/sq.cm
for a period of one minute while ii) Height of shroud - 143 +/-3mm
immersed in water and shall show no
leakage. iii) Internal diameter - 314.4+1%,-0%

d) BURSTING TEST : iv) Height of foot ring - 44 mm

One cylinder taken at random from v) Outer dia of foot - 265 +/-3mm
each batch of 403 cylinders or less shall ring
be subjected to an internal hydrostatic
pressure till it bursts, as stipulated in
IS:3196-1982. 5.2 VALVES :

The normal hoop stress corresponding The LPG cylinder valve shall be
to the pressure at which destruction manufactured conforming to IS:8737
occurs shall be calculated as per (Part II)-1978 and as per Kosan
Section 16.1.1 of IS:3196-1982. The Technova (Denmark) Technology.
cylinder shall burst without
fragmentation. The fracture should not 5.2.1 MATERIAL :
occur in the weld in the direction of
seam nor parallel to the weld within 10 All components used in valve
mm of the weld in the direction parallel construction shall be made out of
to the weld. material compatible with LPG and with
material of cylinder. The material of the
valve body shall have properties as All the dimensions,
described here under : threadings, material
specifications, etc. shall be in
The valve body shall be forged from accordance with the
wrought or extruded sections. Implementation Report on
Import of Technology for self-
5.2.2. MARKINGS ON THE VALVES : closing type LPG cylinder
valves of March, 1985.
a) The specification of the valve
& name of product. 5.2.4 TESTS :

b) Quarter/ Year of manufacture a) Representative samples of


machined valve bodies shall be
c) ISI Monogram subjected to a hydrostatic test
at 1.5 times the maximum
d) Maximum working pressure working pressure i.e. 25.35
(WP) kgf/sq.cm as per IS:8737 (Part
II)-1978.
e) Batch No.
b) Each assembled valve shall be
f) Manufacturer's symbol subjected to a pneumatic
pressure of 17 kgf/sq.cm. in
5.2.3 PHYSICAL PROPERTIES : both, open and closed position.

a) The tensile strength and c) The valve shall perform


elongation of the material of satisfactorily at not less than
valve body determined 5000 cycles of opening and
according to IS:1608-1972, closing operations. After the
IS;1816-1961 and IS:2654- tests, the valve shall be
1977 shall be respectively subjected to a pneumatic test at
atleast 40 kgf/sq.mm and 18% 17 kgf/sq.cm. pressure.
measured on a gauge length of
5.65/50 mm, 50 being the d) For carrying out all other tests,
original area of cross section the scheme of testing and
in mm. inspection as prescribed by
IS:8737 (Part II)-1978 shall be
b) IMPACT STRENGTH referred to.

The Izod impact strength of


the material of valve body 5.2.5 SAFETY CAPS :
determined according to
IS:1598-1977 shall not be less The safety caps for the valves have been
than 2.2 kgf/sq.m for brass. standardised. This being an important
component for valve protection as well
Test samples of tensile and as stopping leakage in case of
Izod impact test shall, where emergency, should be tested for
practicable, be taken from material and also operation at 17
valve body bland, where this is kgf/sq.cm. The tests and the inspection
not practicable, the test sample scheme adopted should be as per
shall be made from the same inspection scheme prescribed below.
raw material giving the same The material of the caps shall be acetal
outside shape as to valve body homopolymer/ co-polymer.
blanks it represents. The scale
of sampling and criteria for 5.2.6 JOINT PACKING :
conformity shall be in
accordance with Section 2.5 of The joint packing or the`O' Ring of the
IS:8737 (Part II)-1978. valve is highly critical component of
the valve, as it is the main component design and dimensions of the `O' Ring
which prevents leakage between valve must be strictly adhered to.
and Regulator assembly. Therefore, the
quality control checks on the material,
ANNEXURE

INSPECTION FORMAT FOR SAFETY CAPTS


TEST CRITERIA : f) 1.4 + 0.2
- 0.0
1. Fitment on SC valves g) 37.5 + 0.1
2. Pneumatic test - 0.2
a) 5 kgf/sq.cm h) 18.8 + 0.3
b) 17 kgf/sq.cm 4. Spring wire dia 1.35 mm

3. Dimensions : 5. Strap length 275 +/-5mm


(All dimensions in mm)
6. Performance with AL Seal
a) 26 + 0.2 O.K./NOT O.K.
- 0.2
7. Marking a) Marketing Co. symbol
b) 11.5 + 0.1 b) Arrow
- 0.05 c) Patent No.
d) Cavity No.
c) 6.5 + 0.2
- 0.2 8. Weight of caps 7.5 gms.

d) 29.5 + 0.1 9. General Workmanship


- 0.2 O.K/ NOT O.K.
e) 3.5 + 0.0
- 0.2
GLOSSARY OF TERMS

1. Area Classification
5. Cylinders
It is method of classifying an area zone wise/
group wise based on the presence of explosive A portable container upto 1000 litres water
gas/ vapour - air mixture vis-a-vis the capacity used for both domestic and industrial
requirement of precautions for construction and purposes.
use of electrical apparatus.
6. Explosive mixture
2. Bulk Vessels
It is a mixture of combustion agent (oxidising
A pressure vessel used for more than 1000 litres product-gas, vapour, liquid or solid) and a fuel
water capacity for storage or transportation. (oxidisable product - gas, liquid or solid) in such
proportions that it could give rise to a very rapid
3. Bullet and lively oxidisation reaction liberating more
energy than is dissipated through conduction
A horizontal pressure vessel used for storage or and convection.
transportation by rail/ road.
7. Earthing & Bonding
4. Compressed Gas
Earthing is the provision of a safe path of
Any permanent gas, liquefiable gas or gas electrical current to ground, in order to protect
dissolved in liquid under pressure or gas mixture structures, plant and equipment from the effects
which in a closed container exercises a pressure of stray electrical current, and electrostatis
either exceeding 2.5 kg/sq.cm. abs @ 15 Deg C discharge.
or a pressure exceeding 3.0 kg/Sq.cm. abs @ 50
Deg C or both.
Bonding is the process of connecting the
equipment/ system to be earthed to the ground A wall of appropriate height and size
by the bond wire to prevent sparking between constructed of suitable material and designed to
two conducting bodies. contain the LPG spillage and to direct it to a
safe location around the storage vessel.
8. Filling Ratio
16. Liquefied Petroleum Gas (LPG)
It is the ratio of weight of LPG in a container to
the weight of water the same container can hold The term applies to a mixture of certain light
at 15 deg. C. hydrocarbon C2 to C5, derived from petroleum
which are gaseous at ambient temperature and
9. Fire safe pressure test may be condensed to a liquid state
at normal ambient temperature by the
As applied to valves, it is the concept of application of moderate pressure.
controlling the leakage to an acceptable level
after damage encountered during and after the 17. Purging
fire achieved by dual seating.
It is the act of replacing the atmosphere within a
10. Fire proofed container by an inert substance in such a manner
as to prevent the formation of explosive mixture.
It is a passive concept of exposure protection of
structures, vessel surface or cables that could be (A) Purging into Service : is the replacement
exposed to direct flame impingement, free of air in a closed system by an inert substance
burning plus pressure torching conditions, and/ and replacement of the later by combustible gas,
or prolonged periods of high intensity radiant vapour, or liquid.
heat fluxes by the application of coating with a
specified rating. (B) Purging out of service : is the replacement
of normal combustible content of a closed
11. Flammability system by an inert substance, and replacement of
the later by air.
It is the percentage of volume of any flammable
vapour in air-vapour mixtures capable to form 18. Reid Vapour Pressure
an explosive mixture.
Reid Vapour Pressure is the vapour pressure in
12. Flammable ( or Inflammable) pounds per square inch (psi) at 100 Deg F as
determined by Reid apparatus.
Any substance which when tested in a specified
manner will ignite when mixed with air on 19. Spheres
contact with a flame and will support
combustion. A spherical pressure vessel used for storage.

13. Gas-Free 20. Tare Weight

It means the concentration of flammable or toxic It is the weight of the cylinder together with any
gases or both in a pressure vessel or pipeline is fitting permanently attached to them and
within the safe limits specified for persons to includes the weight of valve.
enter and carryout hot work in such vessels/
pipelines. 21. Working Pressure

14. Hot Work It is saturated vapour pressure at 65 Deg. C.

It is an activity which may produce enough heat 22. Water Capacity


to ignite a flammable air-hydrocarbon mixture
or a flammable substance. The volume of water in litres that the container
can hold at 15 Deg. C.
15. Kerb Wall
CHAPTER 6

STORAGE AND HANDLING OF BULK LPG

6.1 GENERAL 6.3 PROCEDURE FOR UNLOADING


TANK TRUCKS
This section is recommended as a guide to safe
practices and provisions applying to unloading 6.3.1 Checks essential for plant safety shall be
of bulk LPG and storage of bulk LPG at plants. carried out for each Tank Truck before its
This section cover - entry to the licensed area as per
Annuexre-I.
- Unloading of bulk Tank Truck and Tank
Wagon 6.3.2 Tank pressure, temperature and weight of
filled tank truck shall be recorded.
- Storage of bulk LPG
6.3.3 Tank shall be placed in drive out position
6.2 UNLOADING OF BULK LPG TANK with entire tank truck consisting of bullet
TRUCK & TANK WAGONS and engine covered by sprinklers.

Bulk LPG is transported through Rail Tank 6.3.4 After placement, engine as well as master
wagon, Road Tank Trucks. Currently various control switch shall be switched off and
capacities of Tank wagons and Tank-trucks are minimum two wooden chokes shall be
in use. placed under wheels.

Rail tank wagons - 5,10,12,13,15,37 MT 6.3.5 Following shall be connected -

Road tank trucks - 6-18 MT - Chassis and bullets both are to be earthed
independently for which bare metal cleats to
Unloading of bulk T/Ts and T/Ws shall be be provided.
carried out only at location as approved by
CCOE and under the supervision of a - Liquid and vapour hoses to tank trucks after
responsible person. All safety precautions shall examining the integrity of gaskets and using
be observed : proper studs. Bolts and nuts are not be
used.
- All electrical equipment/ lighting are of
flameproof type - Earthing lines to tank bare metal or
earthing point to tank.
- Vapour vent line should be for individual
bay at 1.5 M height above the eaves of the - Liquid and vapour hoses to tank trucks.
shed fitted with flame cap. ( applicable
where flare system are not available or not 6.3.6 The tank truck valves shall be crack
used for venting). opened and ensured there are no leaks.

- Extinguishers as referred in Chapter 10, 6.3.7 After the above, unloading should be
shall be positioned as an immediate aid to done preferably with LPG compressor by
fight fire. differential pressure method.
6.3.8 Pressure and level in the tank truck shall
- No hot work/ cold work is carried out in the be monitored at regular intervals so that it
vicinity of unloading operation. does not exceed safe limits. After
- decanting all liquid LPG, close the valve
- Checks shall be carried out for each T/T and of liquid line of the bay. Thereafter, LPG
T/W prior to unloading of LPG as per check vapour should be recovered such that
list given in Annexure I and II respectively. vapour pressure in the tank truck is
brought down to 1.5 kg/cm2 minimum
but not below atmospheric pressure.
6.3.9 On completion of unloading, following 6.4.9 Clear the track for movement of wagons.
operations shall be done in sequence :
6.5 STORAGE OF BULK LPG
a) Isolate rigid liquid and vapour lines of
bay by closing the valves and stop LPG LPG is stored in liquid and vapour form under
compressor. pressure in specially designed tanks known as
Pressure Vessels (Unfired). For details of design,
b) Close the valves of liquid/ vapour lines of facilities etc. refer to Chapter 3 on Plant Layout
the tank truck. Depressurise the hose & Chapter 4 on Design criteria.
through high vent - close vent valve.
The bulk storage of LPG shall be governed by
c) Remove hose connections, electrical SMPV (U) Rules, 1981.
bonding wires.
Precautions for storage of LPG in bulk :
d) Cap the vapour/ liquid outlet lines of tank
trucks. a) Filling shall not exceed safe permissible
filling ration.
e) Remove chokes placed under wheels.
b) Vessel shall be inspected daily for any LPG
6.3.10 Record the weight of empty tank truck leakages and corrective action taken.
along with rotogauge, pressure gauge and
temperature gauge readings. Storage vessel should be drained regularly for its
water content, sediments, caustic contents etc.
6.4 PROCEDURE FOR UNLOADING OF Draining operation should be carried out under
TANKWAGONS the supervision of a responsible person.

6.4.1 Checks shall be carried out as given in Following precaution should be observed :
Annexure-II.
The valve closest to the Pressure vessel must be
6.4.2 The tank shall be placed in position and fully opened first. The draw off rate as required,
secured against any movement. The hand to be adjusted by operating the lower valve. This
brakes must be put on and hand brake is to ensure that valve near to the Pressure vessel
lever secured in "ON" position. remain free from freezing, blockage.

6.4.3 After placement, the points leading to the c) All gauges, viz. High level alarm,
track/ lines on which the tank to be measuring gauges, pressure gauges,
unloaded shall be set and pad locked so as temperature gauges should be kept in
to isolate it from other track/ lines. operating condition at all times and be
checked daily.
6.4.4 The siding site shall be properly protected
to prevent any Wagons dashing against
the tank wagons. Caution sign be
exhibited at suitable distance away from
tanks on both ends as applicable.
6.4.5 Tank pressure, temperature and dips of
filled wagons shall be recorded. Record
weighments wherever weighbridge is
provided.

6.4.6 Procedure enumerated from 6.3.5 to 6.3.8


& 6.3.9 (a,b,c,d) shall be followed.

6.4.7 Release hand brakes, remove caution sign


and pad locks.

6.4.8 Weight the empty wagon, wherever


weighbridge is provided.
ANNEXURE - 1

CHECK LIST FOR BULK LPG TANK TRUCKS AT UNLOADING LOCATION

1. CHECKS REQUIRED TO BE - Fuel tank is protected by means of stout


CARRIED OUT BEFORE ALLOWING guard and fuel tank cap is locked.
ENTRY OF TT INSIDE LICENCED
AREA - Paint of bullet is not peeling off.

TANK TRUCK : GENERAL

- has suitable spark arrestor of make and - First aid kit is available.
design approved by CCE, Nagpur properly
fixed to exahust.
3. CHECKS REQUIRED TO BE
- carries 2 nos. 10 kg. DCP extinguishers in CARRIED OUT ON RANDOM BASIS -
easily accessible and removable position MINIMUM ONE DAY, ONCE IN A
with Truck No. date of checking and MONTH :
charging painted on it.
TANK TRUCK :
- quick closing manifold valve with lever
indicating close and open status. - Internals of fire extinguishers in good
condition
- No visible dent on the bullet.
- Carries TREM CARD, instructions booklet
ELECTRICALS : detailing instructions on handling
emergencies en route.
- All junction boxes are properly sealed
- Carries route map
- Any loose electrical wiring/ terminal
- Carries TREM card
- Electrical wiring is insulated and provided
with suitable over current protection. - Has valid CCE licence and authenticated
copy of drawing
- Truck is self starting
- Carries RTO permits
- Readily accessible master switch for
switching off the engine is provided inside - RLW-ULW> Licenced capacity
the cabin.
- HAZCHEM sign, name of contractor with
address and telephone No. displayed
TANK FITTINGS : prominently.

- Leakage from any fittings or joints. - Bullet has no sign of extern corrosion.

2. CHECKS REQUIRED TO BE
CARRIED OUT BEFORE ISSUING TANK FITTINGS :
LOADING MEMO (DURING THE
COURSE OF UNLOADING - Excess flow check valves are functioning.
OPERTIONS)
- Liquid / vapour lines are adequately
TANK TRUCK anchored and are well protected by means
of stout steel guard.
- Height barrier provided as per specifications
- Liquid/ vapour pipe lines are in single piece
from excess flow check valve to discharge - Tools for all fittings
valves - Safety fittings viz., safety valve,
roto-gauge, pressure gauge and temperature - 4 Nos. caution sign board with luminous
gauge are adequately protected. paint for stopping traffic in case of any
emergency.
- Operative fittings like roto gauge, pressure
gauge and temperature gauge are Based on the nature of defects either all the
operational. deficiencies should be got corrected at the
unloading location itself or the tanker should be
allowed to get the repairs done en route and
GENERAL : submit the details at loading location.

Following are available in Tank Truck :

ANNEXUR -II

CHECKLIST AT UNLOADING LOCATION FOR BULK LPG TANKWAGONS

VISUAL EXAMINATION OF WAGON FOR

- POH/ ROH OVERDUE : FOR BARREL Y/N

- FOR UNDERFRAME Y/N

- Damage to Tank Barrel Y/N

- Damage/ missing tank fittings Y/N

- Leakage from dome fittings Y/N

- Seal intact Y/N

- All valves, fittings are in working order Y/N

- The surface is free from rust. Y/N


The paint on the barrel is in good
condition and has not lost its
reflecting characteristics.

The matter regarding tank wagon not complying with any of above checks shall be taken up with loading
location for corrective action.
CHAPTER 7

BOTTLING OPERATIONS

7.1 GENERAL
- Cylinder is free of air.
This section covers the safe practice of LPG
filling plants dealing with cylinders fit for - `O' Ring (joint packing) is present and
filling, having cylinder capacities as referred in there is no apparent damage to valve.
Chapter 5.
- Tare weight is legible.
Activity on bottling line including valve change,
shall be carried out by trained company's (b) Filling operation - All cylinders shall be
personnel and shall be carried out in an area filled on gross weight basis on filling
approved by CCE and filling shall be governed machine.
as per -
Maximum permissible errors on net
- Gas Cylinder Rules, 1981 (under Indian quantity declared by weight shall be in
Explosives Act,1884) accordance with the Standards of Weights &
Measures ( Packaged Commodities) Rules
- The Standards of Weights and Measure 1977 and Amendment Rules, 1992. The
Rules, 1987 (under Weights & Measures filling pressure should not exceed working
Act, 1976) pressure of cylinder i.e. 16.9 kgf/sq.cm at
65 deg.C.
- The LPG Regulation of Supply &
Distribution Order, 1993. (c) Post Filling Operation - Cylinder shall be
counter weighed with check scale for
accuracy of weight. Variation of net weight.
7.2 BOTTLING OPERATIONS Variation of net weight shall not exceed
1.5%. All under-filled/ over-filled cylinders
The Bottling Operations can be classified under should be corrected on adjustment scale.
following heads :
Cylinder shall be checked for `O" ring
I) Receipt of LPG cylinders condition and for valve leak by means of
Compact valve Tester (CVT).
ii) Filling of LPG Cylinders
CVT should be calibrated so as to detect
iii) Handling & storage of LPG cylinders leakage beyond 0.5 gm/hr. For cylinders
found with `O' ring defect, the `O' ring shall
iv) Auxilliary Operations be replaced with a new one and the same
should be rechecked for `O' ring condition
with CVT.
I) Receipt of LPG cylinders
Cylinder shall be checked for body leak and
Cylinders shall be received in capped condition. bung leak by dipping in water test bath.
Cylinder shall conform to IS:3196. Cylinder shall be capped prior to dipping in
test bath water.

II) Filling of LPG cylinders Only those cylinders found passing all
above checks shall be processed further for
(a) Pre-filling operation Cylinder before filling sealing.
shall be checked for following :
Cylinders shall be sealed with PVC seal or
- Visually inspected as per IS:5845 Aluminium seal. Seal shall have
identification mark of oil company,
- Cylinder surface is clean
preferably name of plant and period of space shall be properly marked/ painted on
filling. the flooring.

For typical layout of filling shed with For typical stacking arrangement refer
carousel refer to Annexure-I. Annexure-II.

III) Handling & Storage of LPG Cylinders in Empty and filled cylinders shall be
cylinder filling and cylinder storage shed : demarcated clearly.

Handling and storage of LPG cylinders shall be Minimum distance of 15 metres from
governed by Gas Cylinders Rules, 1981. cylinder loading area and minimum
distance of 10 metres from filling point
Following safe practices shall be observed : shall be observed for all filled cylinders
stack.
a) Handling of LPG Cylinders - LPG
cylinders shall not be dropped, rolled on
sides and shall not be subjected to any IV) Auxilliary Operations
violent contact with any other cylinder or
object cylinder shall be moved by rolling on a) Cylinder requiring valve removal and
its foot ring or on conveyors or hand valve fixing
trolleys.
Cylinder having defective valve and with
b) Defective filled cylinders - Any cylinder bung leak shall have to undergo valve
having body leak, bung leak, bulge, fire removal and valve refixing operation.
ravaged or spurious shall be evacuated
immediately. Following safe procedures shall be observed
for the operation :
Any cylinder with valve leak shall be
immediately capped and thereafter - Cylinder shall be evacuated of its product
evacuated immediately. upto pressure, 1.5 kg/cm2 or less, thereafter
depressurised to near atmospheric pressure
Cylinders requiring repairs other than valve through cold flare before opening the
leak/ Bung leak shall be degassed for defective valve.
repairs.
- Cylinder having bung leak, same valve be
All above cylinders shall be clearly used. Cylinder having defect in valve shall
identified, with markers, to their nature of be replaced with good valve.
defects and shall be kept capped during
storage. - Cylinder bung shall be cleaned with 3/4"
NGT tap and cylinder bung threads checked
c) LPG cylinder storage - All cylinders shall with L1 and L9 gauge.
be stacked vertically (with valve in upright
position) in not more than 2 stack high. - Only cylinders passing above tests shall be
taken up for valve change operation.
Cylinders of different capacity and type - Good valve shall be fixed using a torque
shall be stacked separately. wrench. The torque shall not exceed 20 +/-
2kg.m. Before fixing the valve suitable
All cylinders shall be capped during jointing compound shall be used. Jointing
storage. compound shall be used. Jointing
compound shall be compatible with LPG,
The cylinders shall be stacked in small lots water and metallurgy of cylinders and
of 4 rows and 25 cylinders length. A valves. Teflon tape/ paste of suitable valve
minimum access path of 1 mtrs. must be joining material are recommended as
maintained on both sides of 4 rows and 2 jointing material.
metres after every 5 such lots. After each
length of 25 cylinders, there must be a b) Purging of cylinders
passage of 2 metres. The cylinder storage
- New cylinders and cylinders degassed for Degassing shall be carried out as follows :
repairs shall be purged of air prior to be
taken up for refilling with LPG. Following Cylinders shall be evacuated and depressurised
safe procedure shall be observed for purging to near atmospheric pressure. The residual LPG
of LPG cylinders : in the cylinder should be cold flared in the
atmosphere at a vent outside the shed at 1.0M
- Connect the cylinder valve to vacuum pump height above the roof of the shed.
and evacuate air so that the pressure in
cylinder is brought down to maximum 0.35 Valve shall be removed with suitable torque
kg/cm2 absolute. Inject LPG vapour in the wrench. Cylinders shall be filled with water
cylinder so that pressure is minimum 1 fully and water should be allowed to over flow.
kg/cm2 and not above working pressure of Thereafter cylinders shall be emptied out of
cylinder i.e. 16.9 kgf/cm2 at 65 degree C. water and checked with explosimeter for
degassing. Not more than 6 cylinders shall be
c) Degassing of Cylinders : degassed at a time.
CHAPTER 8

PLANT EQUIPMENT

8.1 GENERAL : responsible for this in service stress corrosion


cracking of welds. LPG vessels made from
8.1.1 SERVICEABILITY OF PLANT : microalloyed high tensile steels have shown
greater susceptibility to such cracking. Wet
The serviceability and safety of LPG plant Fluoroscent Magnetic Particle Testing
equipments, especially in the long term, are (WFMPT) is considered the most reliable test
affected by the standard of maintenance and method for detecting these microcracks.
inspection carried-out. WFMPT should be carried out prior to hydraulic
test wherever cracks are found, their depths
8.1.2 MAINTENANCE SCHEDLES : should be assessed by ultrasonic testing. All
cracks having depths less than corrosion
To facilitate the maintenance service to be allowance may be removed by grinding, edges
rendered in a planned manner, a preventive smoothered and areas left as such after final
maintenance schedule covering the necessary WFMPT check. Weld build up of grooves so
work to be done, mentioning the periodicity i.e. formed is essential wherever depths of groove is
daily, weekly, monthly, half yearly and yearly more than corrosion allowance.
schedules, must be worked out. While basic
recommendations given by the manufacturers b) SHUT-OFF VALVES, CONTROL
should be considered and modified bearing in VALVES, NON-RETURN VALVES, EXCESS
mind the local conditions (See Annexure I-III). CHECK VALVES, PIPELINES, VALVES
AND FITTINGS :
8.1.PERSONALPROTECTION
EQUIPMENT : OISD Standard No. OISD-130 on "Inspection of
Pipes and Valves and Fittings" shall be followed.
Necessary personal protection equipments such
as Hand gloves, Safety shoes, Helmets, Safety c) HOSE AND FLEXIBLE CONNECTION :
belts, Safety goggles etc. shall be used (Ref.
OISD STD-155). OISD Standard No. OISD-135 on "Inspection of
Loading and Unloading Hoses for petroleum
8.2 WORK PERMIT SYSTEM : products" shall be followed.

No Maintenance/ Inspection work shall be d) STRAINERS AND FILTERS :


carried out without following the OISD
Standard OISD-105 on "Work Permit System" Shall be inspected and cleaned as per following
and Section 4 of OISD-137 for electrical frequency, unless sluggish operation warrants
maintenance purpose. earlier inspection :

8.3 INSPECTION & MAINTENANCE OF


VARIOUS FACILITIES IN LPG BOTTLING
PLANTS :

8.3.1 STATIC EQUIPMENTS :

a) PRESSURE VESSELS & STORAGE TYPE / LOCATION FREQUENCY


FACILITIES :
Air filters Weekly
OISD Standard Nos. OISD-128 on "Inspection Strainers on evacuation Weekly
of Pressure Vessels and OISD-129 on line
"Inspection of Tankages" shall be followed. Pump Suction Quarterly
Up stream of filling Quarterly
Weld cracking has been experienced in the lower carousel
half portions of LPG vessels. Small amounts of up stream of PD-Meter Quarterly
wet H2S present in LPG is supposed to be
e) SAFETY RELIEF VALVES :
e) Cylinder Test Bath
OISD Standard No. OISD-132 on
"Inspection of Pressure Relieving f) General
Devices" shall be followed.
8.3.4 INSTRUMENTATION :
8.3.2 ROTARY EQUIPMENT :
a) TEMPERATURE INDICATING
a) COMPRESSORS : OISD Standard No. DEVICES
OISD-120 on "Inspection of
Compressors" shall be followed. In Shall be checked daily for its proper
addition, periodic maintenance checks, as functioning and shall be calibrated once in
detailed in Annexure-I to be followed. 6 months.

b) PUMPS : OISD Standard No. OISD-110 b) LEVEL GUAGING DEVICES :


on "Inspection of Pumps" shall be
followed. In addition, periodic checks as The gauging devices shall be checked daily for
detailed in Annexure-II to be followed. proper functioning. Zero level check and
calibration shall be carried out monthly
c) DIESEL ENGINES: OISD Standard No. and quarter as applicable.
OISD-123 on "Inspection and
Maintenance of Rotating Equipment c) PRESSURE GAUGES :
components shall be followed.
Shall be checked daily for its proper functioning
8.3.3 FILLING EQUIPMENT : and shall be calibrated once in 6 months.

It shall be ensured that the equipment is d) FLOW MEASURING DEVICES :


in good working condition to ensure quality
output and also safe operation. Specimen Shall be checked daily for proper functioning
inspection checks are serving schedule given and calibration shall be carried out
at Annexure --- for ready reference for the monthly and quarterly as applicable.
following equipments:
8.3.5 FIRE FIGHTING EQUIPMENT :
a) CAROUSEL
OISD Standard No. OISD-142 on "Inspection of
i) Drive units Fire Fighting Equipments" shall be
ii) Centre column followed.
iii) Running Rail
iv) Introduction and Ejection devices 8.3.6 ELECTRICAL EQUIPMENT
v) Filling machines
vi) Check Weigh Scales OISD Standard No. OISD-137 on
"Inspection of Electrical Equipment"
b) Chain/ Roller conveyor shall be followed.
c) Drive Units for Conveyors

d) CVT-leak detector

ANNEXURE -I
MAINTENANCE SCHEDULE

COMPRESSORS
--------------------------------------------------------------------------------------------------------------------------------
Sr. Equipment Checks PERIODICITY
--------------------------------------------------------------------------------------------------------------------------------
Daily Weekly Monthly Qrtly Half Annually
Yrly
(1) (2) (3) (4) (5) (6) (7) (8)
--------------------------------------------------------------------------------------------------------------------------------
1. Check Lub. Oil Level of plunger *
pump unit & top up if necessary.

2. Check the oil level in the crank *


case & top up if necessary.

3. Before start check flow of cylinder *


cylinder jacket cooling water.

4. Check oil flow from plunger pump to *


gland packing assembly.& compressor
cylinder.

5. Check for flow rate from plunger pump *

6. Drain water from receiver/ liquid trap. *

7. Check belt tension and adjust *


if necessary. *

8. Ensure tightness of foundation bolts. *

9. Flush out lube oil system : *


a) Crank case
b) Pump chamber and fill fresh oil.

10. Flush jacket water cooling system. *

11. Check alignment of compressor & motor pullies. *

12. Change lube oil filter and clean LPG Suction filter. *

13. Clean oil strainer *

14. Clean Breather *

15. Open and inspect suction and discharge valves. *

16. Check instrumentation calibrate if necessary. *

17. Check safety release valve. *

18. Complete over-haul. *


ANNEXURE -II

MAINTENANCE SCHEDULE

CENTTRIFUGAL PUMP

--------------------------------------------------------------------------------------------------------------------------------
Sr. Equipment Checks PERIODICITY
--------------------------------------------------------------------------------------------------------------------------------
Daily Weekly Monthly Qrtly Half Annually
Yrly
(1) (2) (3) (4) (5) (6) (7) (8)
--------------------------------------------------------------------------------------------------------------------------------

1. Check lub oil & top up level *


if necessary.

2. Check cooling water flow *


(where provided).

3. Check mechanical seal/ gland leakage. *

4. Check the "AMPS" are within limits. *

5. Change lube oil every 800 running *


hours.

6. Check coupling and coupling bolts *


and replace worn out parts.

7. Check tightness of foundation bolts. *

8. Clean suction strainer of : *


a) Product pumps
b) Other pumps

9. Check alignment of pump and motor. *

10. Overhaul. *

11. Greasing of Bearings. *

--------------------------------------------------------------------------------------------------------------------------------
ANNEXURE-III

MAINTENANCE SCHEDULE

FILLING EQUIPMENTS
--------------------------------------------------------------------------------------------------------------------------------
Sr. Equipment Checks PERIODICITY
--------------------------------------------------------------------------------------------------------------------------------
Daily Weekly Monthly Qrtly Half Annually
Yrly
(1) (2) (3) (4) (5) (6) (7) (8)
--------------------------------------------------------------------------------------------------------------------------------

I. CAROUSEL :
(A) DRIVE UNIT :

1. Check oil level & top up if required. *

2. Check oil pressure. *

3. Put oil drop in orifice of cut-off valve. *

4. Grease guide rollers. *

5. Check & adjust drive belt. *

6. Unscrew magnetic plug and clean. *

7. Change hydraulic oil &clean filter. *

8. Clean hydraulic oil tank. *

9. Inspect gears for wear and tear. *

10. Check electric motor & grease motor bearing. *

11. Complete overhaul of the drive unit. *

(B) CENTRAL COLUMN

1. Check air & gas joints for leakage. *

2 Grease bearing. *

(C) RUNNING RAIL :

1. Clean & apply graphite. *

2. Lubricate rail wheels. *

3. Check rail levels. *

--------------------------------------------------------------------------------------------------------------------------------
(1) (2) (3) (4) (5) (6) (7) (8)
--------------------------------------------------------------------------------------------------------------------------------

(D) INTRODUCTION AND EJECTION DEVICES:

1. Blow the air filter free of water & dirt. *

2. Check & top up oil in air lubricator. *

3. Oil the introduction arms. *

4. Check functioning & adjust if required. *

5. Greasing all grease points. *

6. Tighten guide rollers. *

7. Check & repair leaks. *

8. Inspect for wear and tear. *

9. Overhaul the unit. *

(E) FILLING MACHINES:

1. Thoroughly cleaning by using *


dry air.
2. Checking & adjustment of auto *
cut off device.

3. Check operation of filling head *


by supplying air.

4. Check leakage of LPG and repair. *

5. Check condition of LPG filling hoses. *

6. Check oil level in air lubricators. *

7. Lubricate pullies holding filling guns. *

8. Carry out calibration and adjust- ment. *

9. Suspension system bearings & knife *


edges to be thoroughly cleaned.

10. Inspect knife edges for wear & tear *


and repair where required.

11. Complete overhauling. *

--------------------------------------------------------------------------------------------------------------------------------
(1) (2) (3) (4) (5) (6) (7) (8)
--------------------------------------------------------------------------------------------------------------------------------

(F) CHECK SCALE :

1. Thorough cleaning by using dry air. *


2. Air Filter :
a) Blow-out dir t & condensate. *
b) Clean. *

3. Check oil level in lubricator *


and its functioning.

4. Calibrate with standard weights. *

5. Greasing of cylinder stop unit. *

6. Clean suspension system bearings *


knife edges etc.

7. Check for wear & tear of knife edges *


& replace if necessary.

8. Complete overhauling. *

II. CHAIN CONVEYOR :

1. Top up soap solution trays. *

2. Check position of tension roller *


of chain and adjust if required.

3. Lubricate tension rollers & wheels. *

4. Clean soap solution tray. *

5. Grease the bearing *

6. Check foundation bolts of conveyor *


frame for tight- ness.

III. DRIVE UNIT OF CONVEYORS :

1. Check & top up oil level. *

2. Check coupling bolts & rubber *


bushings. Replace the cracked
or worn out bushings.

3. Check alignment of gear box & *


orrect if necessary.
--------------------------------------------------------------------------------------------------------------------------------
(1) (2) (3) (4) (5) (6) (7) (8)
--------------------------------------------------------------------------------------------------------------------------------

4. Clean & lubricate chain. *

5. Tighten foundation bolts. *

6. Drain & change oil. *

7. Inspect for wear & tear. *


IV. CVT/ DCVT LEAK DETECTOR :

1. Check for proper functioning. *

2. Top up kerosene Every shift


chamber.

3. Check leakage rate thru verifier. *

4. Dismantle/ clean the interiors & *


apply silicon grease to "O" ring.

V. CYLINDER TEST BATH:

1. Fill with clean water. *

2. Lubricate moving parts. *

3. Clean tank walls from inside. *

4. Check & lubricate pneumatic *


circuitory of all equipments.

5. Check all fasteners and tighten. *

6. Paint tank walls from inside. *


--------------------------------------------------------------------------------------------------------------------------------

DIESEL ENGINES

MAINTENANCE STEPS

1. KEEP THE DIRT OUT OF THE ENGINE.

2. MAINTAIN A LUBRICATING FILM ON ALL BEARING SURFACES.

3. REGULATE THE ENGINE'S FUEL.

4. CONTROL OPERATING TEMPERATURES.

5. GUARD AGAINST CORROSION.


6. LET THE ENGINE BREATHE.

7. PREVENT OVERSPEEDING.

8. KNOW YOUR ENGINE'S CONDITION.

9. CORRECT TROUBLES WHILE THEY ARE SIMPLE.

10. SCHEDULE AND CONTROL YOUR MAINTENANCE.


DIESEL ENGINES

"A" CHECK EVERY DAY

----------------------------------------------------------------------------------------------------------------------------
MAINTENANCE STEPS REMARKS
----------------------------------------------------------------------------------------------------------------------------

1. CHECK PREVIOUS DAY'S 1A CORRECT AS REQUIRED


ENGINE LOG BOOK.

2. DRAIN WATER AND SEDIMENT 2A BEFORE STARTING ENGINE.


FROM FUEL TANK AND FUEL
FILTER THROUGH DRAIN COCK.

3. CHECK ENGINE OIL LEVEL 3A MUST BE SLIGHTLY LESS THAN


AND TOP UP IF NECESSARY OR EQUAL TO "H" MARK ON DIP
STICK WHEN ENGINE IS STOPPED
AND HAS STOOD FOR 20 MINUTES
OR MORE (MUST BE MEASURED
AFTER ALL OIL IS DRAINED
BACK INTO OIL PAN).

4. CHECK FOR FUEL,OIL,WATER 4A CORRECT IF LEAKING.

5. FILL RADIATOR/SURGE TANK 5A RADIATOR CAP MUST BE FIRMLY


WITH TREATED WATER TIGHTENED BACK INTO THE
(CHROMATE CONCENTRATION RADIATOR/SURGE TANK NECK,
3500 PPM). ENGINE MUST NOT BE OPERATED
WITHOUT THE RADIATOR CAP
SINCE THIS WILL CAUSE
AERATION AND OVERHEATING
OF THE COOLANT.

6. CHECK AIR CLEANER OIL 6A USE CLEAN ENGINE OIL.


LEVEL AND CHANGE OIL, IF
REQUIRED (IF OIL BATH
TYPE) CLEAN DUST PAN AND
PRECLEANER OF DAY TYPE
AIR CLEANER.

7. CHECK AIR LINE CONNECTIONS 7A CORRECT AS REQUIRED


FOR LEAKS.

8. REMOVE AND CLEAN AIR COM- 8A FILL WITH CLEAN OIL, UPTO
PRESSOR BREATHER, IF MARK.
EQUIPPED.

9. DRAIN AIR RECEIVER TANK 9A


AT THE BEGINNING OF EACH
SHIFT AND THEN CLOSE THE
DRAIN COCK.
DIESEL ENGINES

"A" CHECK EVERY DAY


----------------------------------------------------------------------------------------------------------------------------
MAINTENANCE STEPS REMARKS
----------------------------------------------------------------------------------------------------------------------------

10. CLEAN CRANKCASE BREATHER 10A DISCARD PAPER TYPE ELEMENT,


IF CLOGGED.

11. CHECK OIL LEVEL IN 11A CHECK FOR LEAKS, USE SPECI-
HYDRAULIC GOVERNOR,IF FIED ENGINE OIL FOR TOPPING
PROVIDED. UP.

12. START THE ENGINE AND NOTE 12A IF THERE IS A CHANGE IN OIL
THE OIL PRESSURE BOTH AT PRESSURE FROM THAT RECORDED
IDLING AND MAXIMUM SPEED. IN THE LONG BOOK ON EARLIER
OCCASION THEN STOP ENGINE
AND CHECK THROUGH TROUBLE
SHOOTING TECHNIQUE THE CAUSE
FOR OIL PRESSURE CHANGE AND
CORRECT IF NECESSARY (FOR
ASSISTANCE IN DIAGNOSING THE
CHANGE IN OIL PRESSURE
CALL YOUR SERVICE
REPRESENTATIVE IF NECESSARY.

13. RECORD OIL PRESSURE 13A REFER O&M MANUAL FOR LUB.
OIL PRESSURE LIMITS.

14. FILL FUEL TANK AT THE 14A USE CLEAN FUEL AND A STRAI-
END OF THE SHIFT. NER. ALSO CLEAN THE CAP AND
SURROUNDING AREA BEFORE
OPENING THE FILLER CAP.
--------------------------------------------------------------------------------------------------------------------------

"B" CHECK EVERY 250 HOURS

----------------------------------------------------------------------------------------------------------------------------
MAINTENANCE STEPS REMARKS
----------------------------------------------------------------------------------------------------------------------------

1. REPEAT ALL MAINTENANCE 1B


STEPS OF CHECK "A" 1 TO 14.

2. CHANGE ENGINE OIL 2B WHEN LUB. OIL IS EXAMINED


THROUGH LUB. OIL ANALYSIS IN
LABORATORY. OIL CHANGE PERIOD
MAY BE EXTENDED IN SUCH CASES
(REFER TO YOUR SERVICE REP.)

DIESEL ENGINES

"B" CHECK EVERY 250 HOURS


----------------------------------------------------------------------------------------------------------------------------
MAINTENANCE STEPS REMARKS
----------------------------------------------------------------------------------------------------------------------------

3. FIT NEW LUBRICATING OIL 3B INSPECT THE CHANGED FILTER


FULL FLOW FILTER ELEMENT ELEMENTS AND CHECK FOR METAL
PARTICLES AND OIL SLUGING/
OXIDATION.

4. REMOVE CLEAN AND INSPECT 4B BLOW OUT DUST WITH COMPRESSED


DRY TYPE AIR CLEANER AIR IN THE OPPOSITE DIRECTION
ELEMENT, REMOVE AND CLEAN OF THE NORMAL AIR FLOW, IF
DUST PAN. INSPECT FOR HOLES VERY DIRTY WITH OIL AND
AND TEARS, CHECK GASKETS CARBON WASH IN SOLUTION OF
AND "O" RINGS FOR DAMAGE WARM WATER (120-140 DEG F)
AND NON-SLUDGING DETERGENT
ALLOW IT TO DRY FIRST, THEN
USE COMPRESSED AIR. REPLACE
IF WASHED TWO TIMES. CAUTION
EXCESS AIR PRESSURE WILL
DAMAGE PAPER. AIR NOZZLE
MUST BE KEPT AT LEAST 20 cm
FROM THE ELEMENT. MUST NOT
BE USED IF EVEN ONE PIN HOLE
EXISTS. DISCARD ELEMENT IF
PUNCTURED AND ALSO CHANGE
GASKET ALONG WITH
ELEMENT.

5. CLEAN OIL BATH AIR CLEANER 5B


TRAY SCREEN

6. CHANGE LUBRICATING OIL 6B RECORD OIL PRESSURE.


BY-PASS FILTER ELEMENT
AND GASKET, IF PROVIDED.

7. CLEAN FLOAT TANK AND/OR 7B


MAIN FUEL TANK BREATHER.

8. CHECK COOLANT PH VALUE- 8B CHANGE CORROSION PRESISTER


CONCENTRATION OF DCA/ ELEMENT IF PH VALUE IS BELOW
CHROMATE CONCENTRATION NORMAL RANGE 8.5-10.5. CHECK
(3500 PPM). CHROMATE CONCENTRATION AT
3500 PPM. FOR DCA REFER O&M
MANUAL.

9. CHECK MAGNESIUM PLATE 9B CHECK MAGNESIUM PLATE FOR


IN ASSEMBLY CORROSION PITTING OR BEING EATEN AWAY
REGISTER CHANGE WATER CHANGE IF MORE THAN 50% OF

DIESEL ENGINES

"B" CHECK EVERY 250 HOURS

----------------------------------------------------------------------------------------------------------------------------
MAINTENANCE STEPS REMARKS
----------------------------------------------------------------------------------------------------------------------------

FILTER ELEMENT. OF AREA IS LOST. USE DCA


SERVICE ELEMENT OR CHROMATE
ELEMENT OR CHROMATE ELEMENT
BAGS (AR95679) IF CONCEN-
TRATION IS LOW.

10. CHANGE FUEL FILTER ELE 10B CLEAN SHELL FUEL FILTER
MENT WASHER AND "O" RING CHANGE ELEMENT WHEN RESTRI-
ON MOUNTING BOLT. CTION EXCEEDS VACUUM 200MM
OR MERCURY.

11. CHECK OIL IN ANEROID 11B USE SAME OIL AS USED IN OIL
CONTROL, IF REQUIRED. PAN.

12. CHECK & ADJUST BELTS.NEW 12B TIGHTEN BELT TENSION REFER
BELTS WILL STRETCH WITHIN MAINTENANCE MANUAL.
ONE HOUR OR USE THEY MUST
BE READJUSTED.

13. TIGHTEN FOUNCTION BOLTS AND 13B


FLEXIBLE COUPLING BOLTS OF
ENGINE AND ALTERNATOR.

14. CHECK ALL AIR CLEANER CON- 14B CORRECT AS REQUIRED.


NECTIONS FOR CRACKS.
CHAFING ETC. TIGHTEN ALL
AIR INTAKE CONNECTIONS.

15. CHECK FAN HUB AND DRIVE. 15B USE SPECIAL TOOL FOR
TIGHTENING THE FAN HUB NUT.

16. CLEAN/CHANGE AIR COMPRE- 16B CHANGE ELEMENT FOR NATURALLY


SSOR BREATHER ELEMENT. ASPIRATED ENGINE CLEAN SCREEN
FOR TURBO ENGINE.

17. CHECK THROTTLE LINKAGE. 17B


DIESEL ENGINES

"C" CHECK EVERY 1500 HOURS

----------------------------------------------------------------------------------------------------------------------------
MAINTENANCE STEPS REMARKS
----------------------------------------------------------------------------------------------------------------------------

1. REPEAT ALL MAINTENANCE


STEPS OF CHECKS "A" & "B".

2. CHECK THERMOSTATE OPERATION 2C IT SHOULD START OPENING AND


OPEN FULLY WITHIN RANGE 165
DEG. F. OR 170 DEG. F. DISCARD
AND FIT NEW THERMOSTATE
IF OPERATION IS NOT
SATISFACTORY.

3. CHECK FAN HUB AND DRIVE 3C CHECK MOUNTING BOLTS AND


BEARING END PLAY.

4. CHECK IMPLELLER WATER PUMP 4C CORRECT IF NECESSARY.


FOR PLAY.

5. CHECK FOR TURBOCHARGER 5C CORRECT AS REQUIRED.


OIL LEAKS.

6. TIGHTEN TURBOCHARGER 6C TIGHTEN TO THE SPECIFIED TORQUE


MOUNTING NUTS. DO NOT TIGHTEN WHEN ENGINE IS
HOT.

7. CHECK INLET AIR RESTRICTION 7C CHECK AFTER CLEANING DRY TYPE


AIR CLEANER ELEMENT. IF
RESTRICTION IN
EXCESS OF 1000 MM WATER A NEW
ELEMENT MUST BE FITTED.

8. CLEAN OIL BATH AIR CLEANER 8C REMOVE COMPLETE ASSEMBLY AND


CLEAN INCLUSIVE OF FIXED
SCREENS.

9. CLEAN AND TIGHTEN ALL ELEC- 9C


TRICAL CONNECTIONS.

10. CHECK GENERATOR BRUSHES AND 10C REPLACE AND CLEAN AS REQUIRED.
COMMUTATOR.

11. CLEAN ENTIRE ENGINE 11C HIGH PRESSURE AND SOAP WATER
MIXTURE PREFERRED AFTER
SPRAYING ENGINE WITH
CLEANSER

DIESEL ENGINES

"C" CHECK EVERY 1500 HOURS


----------------------------------------------------------------------------------------------------------------------------
MAINTENANCE STEPS REMARKS
----------------------------------------------------------------------------------------------------------------------------

TAKING CARE OF PROTECTING


ELECTRICAL SYSTEM.

12. TIGHTEN ALL MOUNTING BOLTS 12C TIGHTEN AS REQUIRED. OVER TIGHTEN-
AND NUTS. NING MAY RESULT IN DISTORTION OR
DAMAGE.

13. CLEAN ANEROID AIR BREATHER. 13C REPLACE BREATHER IF NECESSARY.

14. CHECK SEA WATER PUMP 14C CHECK FOR LEAKS/ OPERATION/
(MARINE APPLICATION ONLY) PERFORMANCE.

15. CHECK HEAT EXCHANGER ELEMENT 15C CLEAN ELEMENT TUBES/CHANGE


ZINC PLUG (MARINE APPLICATION) PLUGS.

16. CHECK EXHAUST AND INLET MANI- 16C


FOLD NUTS AND CAPSCREWS.

17. CHECK ENGINE BLOWER. 17C READINGS IN EXCESS OF RECOMMENDED


LIMITS. CORRECTIVE ACTION MUST BE
TAKEN. THOROUGH ANALYSIS WITH THE
HELP OF TROUBLE SHOOTING CHART.

18. CLEAN RADIATOR 18C BLOW AIR THROUGH THE RADIATOR CORE
IN OPPOSITE DIRECTION TO THE NORMAL
FLOW OF AIR, IF WORKING UNDER
DUSTRY/ DIRTY CONDITIONS.
(REVERSE FLUSHING OPERATION)

19. CHECK AIR COMPRESSOR 19C CHECK SHAFT END CLEARANCE.

20. ADJUST INJECTORS AND VALVES. 20C FINAL ADJUSTMENTS MUST BE CARRIED
OUT WITH ENGINE HOT AND WITH
CORRECT TORQUE AS SPECIFIED
(REFR O&M MANUAL).

21. CLEAN FUEL INLET CONNECTIONS. 21C

22. CHANGE HYDRAULIC GOVERNOR 22C USE ENGINE LUBRICATING OIL.


OIL/ ANEROID OIL.

23. CHECK VIBRATION DAMPER. 23C CHECK WOBBLE AND ECCENTRICITY


ALIGNMENT MARKS ON RUBBER TYPE.
DISCARD DAMPER IF MISALIGNMENT
IF MORE THAN 1/16 IN.
DIESEL ENGINES

"D" CHECK EVERY 4500 HOURS

----------------------------------------------------------------------------------------------------------------------------
MAINTENANCE STEPS REMARKS
----------------------------------------------------------------------------------------------------------------------------
1. REPEAT ALL MAINTENANCE STEPS 1D
OF CHECKS "A", "B" & "C".

2. CHECK EXHAUST AND INLET 2D


MANIFOLD NUTS AND CAPSCREWS.

3. TIGHTEN ALL MOUNTING BOLTS 3D


AND NUTS.

4. CLEAN TURBOCHARGER DIFFUSER 4D


AND IMPELLER AND CHECK END
FLOAT.

5. CHECK TURBOCHARGER REARING 5D ONLY END FLOT ON SEMI FLOATING


CLEARANCES BEARINGS IF IN EXCESS OF LIMITS,
REPLACE.

6. CHECK CRANKSHAFT END FLOAT 6D IF IN EXCESS OF RECOMMENDED LIMITS.


CORRECTIVE ACTION IS INDICATED.

7. CLEAN INJECTOR INLET SCREENS.

8. CLEAN AND CALIBRATE ALL MUST BE DONE ONLY IF A PERFORMANCE


INJECTORS. DETERIORATION IS EVIDENT.
SOME OF THE INDICATIONS FOR
PERFORMANCE DETERIORATION
ARE:

9. CHECK FUEL PUMP CALIBRATION 1 BLACK SMOKE.


2 CHANGE IN FUEL MANIFOLD PRESSURE
10. REPLACE ANEROID BELLOWS AND 3 LOSS OF POWER
CALIBRATE ANEROID. 4 MALFUNCTION OF ANEROID.

11. REPLACE FUEL PUMP FILTER


SCREEN AND MAGNET.

12. STEAM CLEAN ENGINE 12D IF STEAM IS NOT AVAILABLE, THEN


USE CLEAN SOAP WATER SOLUTION
AS OUTLINED IN "C" CHECK ITEM-11C.

`E' CHECK EVERY 8000 HOURS

1. REPEAT ALL MAINTENANCE STEPS OF CHECK `A', `B', `C' & `D'.

2. THE `E' MAINTENANCE CHECK IS NECESSARY ONLY WHEN THE ENGINE OPERATING
CONDITIONS SIGNIFY DETERIORATION IN PERFORMANCE AS CAN BE ASCERTAINED
BY THE SYMPTOMS :

(1) HEAVY SMOKE (2) LOSS OF POWER (3) HIGH OIL TEMPERATURE HIGH WATER
TEMPERATURE (4) LOSS OF LUB. OIL PRESSURE (5) UNUSUAL NOISE & VIBRATIONS.
THE `E' MAINTENANCE CHECK IS A METHODOLOGY FOR INSPECTION OF WEAR OR
ASSEMBLY DETRIORATION OF PARTS AND ASSEMBLIES, AND SHOULD BE RESORTED
TO ONLY WHEN TROUBLE SHOOTING IN ADDITION TO PERFORMING A,B,C AND D
MAINTENANCE CHECKS, WHICH MAY ELIMINATE THE ENGINE PERFORMANCE
PROBLEM AND BRING THE ENGINE BACK TO NORMAL OPERATING CONDITIONS. IT
IS ANTICIPATED THAT GOOD OPERATING AND MAINTENANCE PRACTICES AS
PRESCRIBED THROUGH A,B, C & D CHECKS WILL ENSURE THAT THE ENGINE WILL
PERFORM BEYOND 25000 HOURS BEFORE THAT THE ENGINE MUST BE DISMANTLED
FOR INSPECTION PRELUDE TO A MAJOR OVERHAUL. THE TIME INTERNAL OF 8000
HOURS IS A PERIOD AT WHICH THE ENGINE MAY DEVELOP SYMPTOMS ASCRIBED
ABOVE 1-5 AND ARE INDICATIVE OF PERFORMANCE DETERIORATION DUE TO
INADEQUATE A,B,C & D CHECKS AND FAILURE TO IDENTITY PERFORMANCE
DETERIORATION. THIS FIGURE HAS BEEN ARRIVED AT ON THE BASIS OF CURRENT
MAINTENANCE PRACTICES AND SHOULD NOT BE TREATED AS AN ABSOLUTE FOR
MAKING AN `E' CHECK. HOWEVER, IT IS ESSENTIAL THAT THE ABOVE ROUTINE
ANALYSING ENGINE PERFORMANCE BE STRICTLY FOLLOWED IN ORDER TO
PREVENT DISMANTLING OF ENGINE WHOSE PERFORMANCE CAN BE SIMPLY
CORRECTED BY TROUBLE SHOOTING AND ROUTINE MAINTENANCE CHECKS.

3. THE `E' MAINTENANCE CHECK IS OFTEN REFERRED TO AS "IN FRAME INSPECTION"


WHERE SOME KEY PARTS, SUCH AS BEARINGS, ARE CHECKED FOR WEAR TO
DETERMINE IF THE ENGINE MAY BE OPERATED FOR ANOTHER SERVICE PERIOD.
LIKEWISE, OIL CONSUMPTION, OIL PRESSURE AND OTHER SIGNS OF WEAR SHOULD
BE ANALYSED DURING THE CHECK WEAR LIMITS AND OTHER INFORMATIONIS
AVAILABLE FROM DISTRIBUTOR AND DEALERS. (IT MUST BE CLEARLY UNDERSTOOD
THAT THE DECISION TO INSPECT KEY PARTS MUST BE ARRIVED THROUGH ROUTINE
OUTLINED IN POINT TWO ABOVE).
CHAPTER 9

STATUTORY TESTING OF LPG CYLINDERS

9.0 All cylinders used for filling LPG are


required to be tested periodically to ensure a) The detailed visual inspection of the
fitness of the cylinders for further service. cylinder body shall be carried out as per
First retesting is required to be done after 7 IS:5845.
years and subsequent retesting after every
5 years interval. Such tests are to be b) Depending upon the visual inspection,
conducted by the CCE approved parties cylinders are segregated for scrapping, for
only. cold repairs and for hot repairs in case
required.
9.1 TESTING PROCEDURE
c) The interior of the cylinder shall be
9.1.1 DEGASSING OF LPG CYLINDERS examined by means of infra low voltage
All the LPG cylinders are depressurised in FLP lamp. The internal examination shall
the approved premises by opening valves be carried out as per IS:5845.
by means of suitable adaptors to ensure
that the internal cylinder pressure is d) LPG cylinders selected at random may be
reduced to atmospheric pressure. Only cut into two holes for assessing internal
after depressurising the cylinder, cylinder corrosion.
valve is removed and LPG cylinder is
taken up for water filling and water is e) In case of dented/ buckled cylinders, visual
overflown and retained in the cylinder for inspection of welds needs to be done more
not less than one hour to remove any traces carefully since the welds are more
of LPG. Degassing can also be achieved by susceptible to cracking. Denting or buckling
stripping, Nitrogen purging, etc. by more than nominal plate thickness may
be attended by repairs/ replacement.
9.1.2 SURFACE CLEANING :
9.1.5 HYDROSTATIC TESTING :
a) After depressurising the cylinder and
emptying out the water, the same is kept in a) All the LPG cylinders shall be taken up for
inverted position and stroked gently with a hydrostatic test at an interval of 7 years for
non-sparking hammer such as wooden first testing and subsequent testing after
mallet to remove any dust, rust or any every 5 years in accordance with IS:8868.
loose remnants in the cylinders. Only water should be used as a medium for
hydrostatic testing and the pressure to be
b) The depressurized cylinder bung is applied should be the test pressure marked
plugged and is takne up for surface on the cylinder body (25.35 kg/sq.cm) and
cleaning by immersing the cylinder in the the same should be retained for a minimum
caustic soda bath and soap water and the period of 30 seconds. Any reduction in
same is then rinsed with water. pressure noticed during the test, any
leakage, visible bulge or deformation should
9.1.3 CHECKING TARE WEIGHT : be treated as a case of failure. Such
cylinders should be properly marked,
All the LPG cylinders shall be weighed observation recorded and segregated for
and if the loss in tare weight is more scrapping and disposal.
than 5% of original weight such
cylinders shall be segregated and b) Pressure Gauges shall be calibrated at least
scrapped. At the time of weighing the once a week and the Pressure Gauges used
weight of valve is also accounted. for verification should be tested once in
every three months.
9.1.4 VISUAL INSPECTION :
9.1.6 VALVE FIXING : 9.1.9 CHECKING MARKING THE TARE
WEIGHTS
a) Before commencing the fitting of valve
operation, all the water inside the cylinder a) Tare Weight of the cylinder should be
should be drained and the cylinder should ascertained and if in variance with the
be made dry with the use of hot air jet. original tare weight (this could be as a
Before refitting the valve, internal threads result of change of cylinder valves ) the
of the cylinder bung should be cleaned with observed tare - weight should be punched as
3/4" NGT thread tap and checked against close to the original tare weight marking as
thread damage. In case old valves are being recorded in the register maintained.
refitted the same should be tested by
compressed air at 7 kg/sq.cm for leakage b) The observe tare weight should be stencilled
from seat. with paint on the shoulder and as well as on
inside of one of the vertical stay.
b) Teflon paste/ suitable sealing compound
should be used as a sealing material for c) Gross weight punched/ stencilled on the
tightening the valve and the torque of 20+/- cylinder should be changed in case of
2 kg. m. should be applied. In no case change of tare weight.
spanners and ordinary wrenches be used for
tightening the valves. d) Weighing machines used for checking the
tare weight should be duly certified by
9.1.7 PNEUMATIC TEST : Weights & Measures Authority. The
machine should be tested daily with the
a) The Pneumatic test should be applied to the standard weights to verify accuracy. The
cylinder at a pressure of 7 kg/sq.cm. for a test used for checking should be tested
minimum of 60 seconds as per IS:3196. against standard weights and the same must
This is basically to check the tightness of be stamped periodically by Weights and
the valve cylinder joints. Measures Authority. The minimum
graduations of 50 gms. must be available.
b) With the cylinder under pressure, a soap
solution should be applied to the cylinder e) Weighing scale error should not be greater
valve bung joint to ensure that there is no than 1.0%.
leak. The same can be checked by dipping
the cylinders in water bath. Depressurise f) The tare weight should be recorded with an
the cylinders. All the Pressure Gauges used accuracy of +/-50 gms. and rounded off as
for Pneumatic test shall be calibrated at per IS:2.
least once in 3 weeks and the Pressure
Gauge used for verification should be tested 9.1.10 PUNCHING OF MARKS :
once in every three months.
In addition to punching of revised tare
9.1.8 PAINTING OPERATIONS : weight/ gross weight wherever applicable,
following details should also be punched
a) To enhance the life of the cylinder and to on the cylinder body as close to the
project a better image to the customers, previous markings as practicable :
maintaining a well painted surface of
cylinder is most desirable. a) Date of retest

b) All LPG cylinders are painted with one coat b) Code marking for the Test Plant/
of zinc chromate primer and a coat of super Repairer.
synthetic enamel paint of signal red colour
(IS:2932 shade 575). Special care should be c) Tare weight of the cylinder should be
taken to paint the cylinders in vulnerable stencilled with black paint within the
areas like undermeath the foot ring. V.P. Ring circle diameter at 3 places for
easy identification by filling operators.
c) The valve should be protected while The recommended lettering size is 25
painting the cylinder. mm and the thickness of the numerals
is 6-7 mm.
d) It is also recommended that the net without going through the test date of
weight of LPG to be filled should be manufacturing dates punched on each and every
stencilled on the body of the cylinders cylinder. Currently, the following colour codes
outside the V.P. Ring diameter. The size have been selected for easy identification of
of the lettering recommended is 18 mm cylinders and the same shall be repeated after
and the thickness of the numerals is 4-5 every five/ seven years cycle. Colour coding is
mm. done on the inside of one of the Stay Plates and
the same is given below:
9.1.11 COLOUR CODING OF CYLINDER :

This is done primarily to facilitate easy


segregation of cylinders for repairs at plants

COLOUR CODING SCHEME

--------------------------------------------------------------------------------------------------------------------------------
Cylinder Cylinder Next Background Shade as Lettering
Manufactured retested/hot Retesting colour IS:5 colour
in the repaired Date
year in the year
-------------------------------------------------------------------------------------------------------------------------------

1989 1991 1996 Sea Green 217 Black

1990 1992 1997 Dove grey 694 Black

1991 1993 1998 Aircraft Blue 108 White

1992 1994 1999 Salmon Pink 443 Black

1993 1995 2000 Black 521 White

1994 1996 2001 Yellow 355 Black

1995 1997 2002 White 127 Black

--------------------------------------------------------------------------------------------------------------------------------

c) Serial number of cylinder &


9.1.12 CERTIFICATION : name of manufacturer

A detailed record of each cylinder tested d) Month and year of test


at the plant or at the repairer's premises
should be maintained. The record e) Weight of cylinder
should include the minimum following
details : f) Punched on cylinder

a) Running serial number g) Observed weight

b) Date of testing h) Whether satisfactory/ rejected


- Quarter/ year of retest punched on the
i) Visual defects cylinder

j) Internal - Stencilling/ colour coding for age


profile
k) External
- Relevant test certificate number
l) Whether passed/ rejected
REMARKS :
9.1.13 HYDROSTATIC TEST/
HYDROSTATIC STRETCH TEST : (The Remarks columns should indicate whether
the cylinder has been finally passed or rejected
- Whether passed/ rejected besides any other relevant details not covered
above).
- Condition of bung threads (internal)
The test certificate issued by the Plant or by the
- Whether satisfactory/ rejected Repairers should include :
Pneumatic Test
- Running Serial Number of cylinder
- Whether passed/ rejected - Cylinder Serial Number
- Date of testing
ANNEXURE

SEQUENCE OF OPERATIONS FOR STATUTORY

PRESSURE TESTING OF LPG CYLINDERS

1. Receipt of Cylinders

2. Depressurising

3. Recording details
(like Sr.No., Test Dates, Tare weight, Manufacturer's name)

4. Valve Removal

5. Degassing

6. External surface cleaning

7. Internal cleaning and internal inspections

8. Visual Inspections of external surface and bung threads


by L-1 and L-9 plug gauges

9. Tare weight checking

10. Hydrostatic testing

11. Internal cleaning and checking

12. Primer coating

13. Signal red painting

14. Punching of new test date and repairer's identification mark

15. Tare weighing

16. Colour code painting to indicate ownership of cylinders,


stencilling new tare weight, new weight and next test date

17. Tapping the bung thread, cleaning the same by brass wire
brush and checking the bung threads by L-1 & L-9 plug gauges.

18. Valve fixing

19. Pneumatic test

20. Certification and despatches.

GLOSSARY OF TERMS

1. Area Classification It is method of classifying an area zone wise/


group wise based on the presence of explosive
gas/ vapour - air mixture vis-a-vis the 9. Fire safe
requirement of precautions for construction and
use of electrical apparatus. As applied to valves, it is the concept of
controlling the leakage to an acceptable level
2. Bulk Vessels after damage encountered during and after the
fire achieved by dual seating.
A pressure vessel used for more than 1000 litres
water capacity for storage or transportation. 10. Fire proofed

3. Bullet It is a passive concept of explosure protection of


structures, vessel surface or cables that could be
A horizontal pressure vessel used for storage or exposed to direct flame impingement, free
transportation by rail/ road. burning plus pressure torching conditions, and/
or prolonged periods of high intensity radiant
4. Compressed Gas heat fluxes by the application of coating with a
specified rating.
Any permanent gas, liquefiable gas or gas
dissolved in liquid under pressure or gas mixture 11. Flammability
which in a closed container exercises a pressure
either exceeding 2.5 kg/sq.cm. abs @ 15 Deg C It is the percentage of volume of any flammable
or a pressure exceeding 3.0 kg/Sq.cm. abs @ 50 vapour in air-vapour mixtures capable to form
Deg C or both. an explosive mixture.

5. Cylinders 12. Flamable ( or Inflammable)

A portable container upto 1000 litres water Any substance which when tested in a specified
capacity used for both domestic and industrial manner will ignite when mixed with air on
purposes. contact with a flame and will support
combustion.
6. Explosive mixture
13. Gas-Free
It is a mixture of combustion agent (oxidising
product-gas, vapour, liquid or solid) and a fuel It means the concentration of flammable or toxic
(oxidisable product - gas, liquid or solid) in such gases or both in a pressure vessel or pipeline is
proportions that it could give rise to a very rapid within the safe limits specified for persons to
and lively oxidisation reaction liberating more enter and carryout hotwork in such vessels/
energy than is dissipated through conduction pipelines.
and convection.

7. Earthing & Bonding


14. Hot Work
Earthing is the provision of a safe path of
electrical current to ground, in order to protect It is an activity which may produce enough heat
structures, plant and equipment from the effects to ignite a flammable air-hydrocarbon mixture
of stray electrical current, and electrostatis or a flammable substance.
discharge.
15. Kerb Wall
Bonding is the process of connecting the
equipment/ system to be earthed to the ground A wall of appropriate height and size
by the bond wire to prevent sparking between constructed of suitable material and designed to
two conducting bodies. contain the LPG spillage and to direct it to a
safe location around the storage vessel.
8. Filling Ratio
16. Liquefied Petroleum Gas (LPG)
It is the ratio of weight of LPG in a container to
the weight of water the same container can hold The term applies to a mixture of certain light
at 15 deg. C. hydrocarbon C2 to C5, derived from petroleum
which are gaseous at ambient temperature and
pressure test may be condensed to a liquid state Reid Vapour Pressure is the vapour pressure in
at normal ambient temperature by the pounds per square inch (psi) at 100 Deg F as
application of moderate pressure. determined by Reid apparatus.

17. Purging 19. Spheres

It is the act of replacing the atmosphere within a A spherical pressure vessel used for storage.
container by an inert substance in such a manner
as to prevent the formation of explosive mixture. 20. Tare Weight

(A) Purging into Service : is the replacement It is the weight of the cylinder together with any
of air in a closed system by an inert substance fitting permanently attached to them and
and replacement of the later by combustible gas, includes the weight of valve.
vapour, or liquid.
21. Working Pressure
(B) Purging out of service : is the replacement
of normal combustible content of a closed It is saturated vapour pressure at 65 Deg. C.
system by an inert substance, and replacement of
the later by air. 22. Water Capacity

18. Reid Vapour Pressure The volume of water in litres that the container
can hold at 15 Deg. C.
CHAPTER 10

FIRE PROTECTION FACILITIES

10.1 GENERAL
v) Detection of fire for automatic actuation of
LPG Bottling Plants are generally located away medium velocity water sprinkler system
from populated areas in view of hazardous shall be provided at all critical places like
nature of product. With the passage of time LPG Bulk Storage, Tank Truck/ Tank
these plants get surrounded by settlements/ Wagon Gantry, near Carousal, LPG pump/
residential localities in the absence of any Compressor House, Evacuation, Valve
statutory regulations prohibiting their Change Shed etc.
construction.
10.4 FIRE WATER SYSTEM
Due to large quantities of highly inflammable
product stored in the Bottling Plants these pose Water is used for fire extinguishment, fire
safety risk to the plant as well as to the control, cooling of vessels/ equipment and
surrounding environment. Therefore, it is very exposure protection of equipment and personnel
much essential that elaborate in-built Fire from heat radiation.
Protection Facilities are installed at the LPG
Bottling Plants. 10.4.1 COMPONENTS OF FIRE WATER
SYSTEM
10.2 APPLICATION
The main components of the system are :
i) This standard lays down the minimum
requirements of Fire Protection Facilities - Fire Water Storage
at LPG Bottling Plants.
- Fire Water Pumps
ii) For LPG bottling Plants located within the
Refineries the OISD Standard No. 116 - - Fire Hydrant/ Monitor distribution piping
Fire Protection Facilities for Refineries, network.
Gas Processing Plants shall also be
referred. - Water Sprinkler/ Deluge system.

10.3 DESIGN CRITERIA 10.4.2 FLOW RATE DESIGN

i) Facilities shall be preferably designed on The Fire Water pumping requirement shall be
the basis that the city fire water supply is calculated based on minimum spray density as
snot available. under :

ii) The single largest fire risk shall be Storage Vessels - 10 LPM/Sq.M
considered. LPG Shed - 10 LPM/Sq.M
LPG Pump/compressor - 20 LPM/Sq.M.
iii) All LPG storage Vessels, Cylinder Storage/ House
Filling/ Repair Sheds, LPG Pump Houses, LPG Loading racks - 10 LPM/Sq.M.
Bulk Lorry and Tank Wagon Gantries shall
be fully covered by medium velocity water
spray system.

iv) Fire Protection Facilities shall have fire a) Storage Vessels


fighting access, means of escape in case of
fire and also segregation of facilities so that In case of Bulk Storage of LPG, automatic
the adjacent facilities are not endangered detection of heat for automatic actuation of
during the fire. The layout shall permit medium velocity (MV) sprinkler system having
access from atleast two directions. remote/ local operated deluge valve with spray
density of 10 LPM/Sq.M. of surface area shall be
provided. For water flow calculations adjoining 10.4.3 FIRE WATER SYSTEM DESIGN
vessels within distance of R+30 Mts. (Where R
is the Radius of the LPG vessel and 30 Mts. i) The Fire Water pressure system shall be
shall be measured from the periphery of the LPG designed for a minimum residual pressure
vessel), water density for cooling shall be of 7.0 kgs/ Sq.cm g at the remotest place of
considered at the rate of 10 LPM/Sq.M. surface application in the plant.
area.
ii) A fire water ring main shall be provided all
b) Sheds around perimeter of the LPG Plant facilities
with hydrants/ monitors spaced at 30 M
MV sprinkler system having remote operated centre to centre. Fire hydrants and monitors
deluge valve and at critical places like near shall not be installed within 15 Meters from
carousal, evacuation, valve chang eshed, the facilities/ equipment to be protected.
automatic detection of heat for automatic
operation of sprinkler system with spray density iii) Fire hydrant network shall be in closed
10 LPM/Sq.M. shall be provided. The shed has loops to ensure multidirectional flow in the
to be divided into suitable number of zones, each system. Isolation valves shall be provided to
served by independent deluge system. The enable isolation of any section of the
adjacent zones are required to be operative network without affecting the flow in the
around the zone under fire and the same shall be rest. The isolation valves shall be located
considered as a single risk. normally near the loop junction. Additional
isolation valves shall be provided in the
c) LPG Pump House segments where, the length of the segment
exceeds 300 Mts.
MV sprinkler system with automatic heat
detection having remote/ local operated Deluge 10.4.4 FIRE WATER STORAGE
valve with spray density of Max. 20 LPM/Sq.M
shall be provided. i) Water for the hydrant service shall be stored
in any easily accessible surface of
d) Tank Lorry Gantry underground concrete reservoir or above
ground tank of steel or concrete. However,
In case of Tank Lorry Gantry, automatic above ground tanks shall be preferred in
detection of heat for automatic actuation of MV view of the availability of flooded suction
sprinkler system having remote/ local operated condition for easy start of fire water
deluge valve with spray density 10 LPM/Sq.M of engines. The effective storage capacity
surface area shall be provided. A maximum of 7 shall be not less than 4 Hrs. aggregate
bays shall be considered as single risk area. working capacity of Fire Water pumps.

e) Tank Wagon Gantry ii) Storage tank/ reservoir shall be in two inter
connected compartments to facilitate
MV sprinkler system with automatic heat cleaning and repairs. In case of steel tanks
detection having remote/ local operated deluge there shall be a minimum of two tanks.
valve with effective spray density of 10
LPM/Sq.M shall be provided. A minimum of
one gantry (600 MTs) shall be considered as 10.4.5 FIRE WATER PUMPS
single risk. The spray system shall cover tank
wagons surface on either side of tank wagon i) Centrifugal type fire water pumps shall be
gantry as well as the associated LPG pipelines in installed to meet the designed fire water
the gantry. The Zoning concept can be adopted flow rate and head. These pumps
as described in 10.4.2(b). prerferably should have a flooded suction.

The fire water system in the plant shall be ii) There shall be a Jockey pump of capacity not
designed to meet the highest fire water flow less than 10 Cu.M./Hr. per 100 Hydrant
requirement of a single largest risk of any of the Point. (1 Monitor is equivalent to 4 Hydrant
above cases at a time plus 288 Cu.M/Hr. for Points). The system pressure has to be
operating 2 Nos. Fire water Monitors/ maintained at 7 kg/cm2g with the help of
Supplementary Hose requirements. Jockey Pump operating automatically.
The Jockey Pump shall be quick auto start- a) Road crossings.
stop type with the help of pressure switches.
b) Places where above ground piping is likely
A standby jockey pump shall be provided if to cause obstruction to operation and vehicle
the number of hydrant points are more than movement.
100.
c) Places where above ground piping is likely
iii) The fire water pump(s) including the stand to get damaged mechanically, particularly in
by pump(s) shall be of diesel engine driven the lPG storage area where water supply
type. The pumps shall be capable of lines are laid for feeding sprinkler deluge
discharging 150% of its rated discharge at a system.
minimum of 65% of the rated head. Each
engine shall have an independent fuel tank d) Where Frost conditions warrant and
of suitable size for 6 Hrs. continuous ambient temperature is likely to fall below
running. zero deg. centigrade underground piping at
least 1 meter below the ground level should
iv) No. of stand by pumps shall be provided as be provided.
per following criteria :
iii) If Fire water ring main laid underground the
a) Minimum 1 no. following precautions shall be taken :

b) 50% upto 4 Nos. of Main pumps. a) The Ring main shall have at least one meter
earth cushion in open ground and 1.2
c) For 4 and above, minimum 2 Nos. meters cushion under the road crossings.

v) Fire water pump house/ Fire water tanks or b) The Ring main shall be provided with
reservoir shall be located atleast 60 M protection against soil corrosion by suitable
(minimum) away from LPG facilities. coatings/ wrappings.

vi) Fire water pumps shall be exclusively used c) In case of poor soil conditions it may be
for Fire Fighting purpose only. necessary to provide concrete/ masonary
supports under the pipe line.
10.4.6 FIRE HYDRANT NETWORK
iv) Fire water ring main shall be sized for 120%
i) Fire hydrant ring main should be normally of the design water rate. Design flow rates
laid above ground. Following prcautions shall be distributed at nodal points to give
should be taken if fire water ring main laid the most realistic way of water requirements
above ground : in an emergency.

a) Pipe line shall be laid at a height of 300 v) The fire water network shall be kept
mm to 400mm above finished ground level. pressurised to a pressure of about 7
kg/sq.cm.g with the help of one or more
b) The mains shall be supported at regular Jockey pumps.
intervals not exceeding 6 meters.
vi) Hydrants/ monitors shall be located bearing
c) The system for above ground portion shall in mind the fire hazards at different sections
be analysed for flexibility against thermal of the premises to be protected and to give
expansion and necessary expansion loops most effective service.
where called for shall be provided.
vii) Hydrant/ monitors shall be provided for
d) The portion of fire water hydrant above every 30 meters in case of hazardous areas
ground and within 15 M of the LPG storage and may be spaced 45 meters in other areas.
vessels shall be provided with suitable fire
retardant coating. viii) Connections for fire water monitors shall be
provided with independent isolation valves.
ii) However the ring main shall be laid
underground at the following places :
ix) Hose boxes with 2 nos. hoses and a nozzle the discharge of air through one Quartzoid
shall be provided between the hydrant Bulb will depressurise the down stream side
points. of the restriction orifice.

x) Considering radiation levels in the event of iii) The Electro pneumatic (E.P) heat detectors
a fire hydrants/ Monitors/ Control valves can be provided in the sheds and they work
shall be located at a safe distance (minimum on the following principle :
distance of 15 mts.) and from hazardous
equipment/ buildings. a) Rate of rise - 10 deg. C/
of temp. Minute.
xi) The deluge valves shall be located out side
the kerb wall at a safe distance in case of b) At 79 deg. C(max.)
LPG spheres/ bullets and 15 meters away
from the limits of LPG cylinder sheds. A The EP detectors are divided into groups
fire wall shall be provided for the protection and alternate detectors are connected in one
of deluge valve and for operating personnel. circuit. Two detectors from two different
groups shall function/ operate for actuation
10.4.7 MATERIAL SPECIFICATIONS of sprinkler system.

All the materials used in fire water system using iv) The actuation of detectors shall initiate the
fresh water shall be of approved type as following :
indicated below.
a) Opening of deluge valve.
In case of sea water service, the fire water main
pipes shall be concrete mortar lined internally. b) Audio-visual alarm at the fire pump
house/ control panel.
i) Pipes CS as per
IS:3589/IS:1239 c) Fire siren.
ii) Isolation Valves Cast iron/ Cast Steel
iii) Deluge valves Cast iron/ Cast steel d) The diesel pump will start based on their set
iv) Hydrant pressure to supplement/ to maintain the fire
Standpost C.S. water pressure in the ring main.
Outlet valves Gunmetal/ Aluminium
v) Monitors C.S. ROV's of Fire-safe type shall be provided.
vi) In case of underground mains the isolation
valves shall be located in RCC/ brick The following areas shall be covered with
masonary chamber. the medium velocity spray system in the
LPG Bottling Plants :
vii) The above ground fire water main and the
fire hydrant standpost shall be painted with a) LPG Storage Area :
corrosion resistant "Fire Red" paint.
Automatic detection of heat for automatic
viii) Water monitor and hose box shall be actuation of MV sprinkler system having
painted "Luminous Yellow'. remote/ local operated deluge valve shall be
provided.
10.4.8 MEDIUM VELOCITY SPRAY
SPRINKLER SYSTEM b) Tank Wagon Loading/ Unloading Area :

i) Medium velocity sprinkler system based on MV sprinkler system having remote/ local
heat and other detection shall be employed. operated deluge valves shall be provided. Tank
wagon loading/ unloading area shall be divided
ii) Quartzoid Bulb protection can be provided in into six zones and one deluge valve shall cover
open areas or in the sheds. The Quartzoid 12 LPG tank wagons at a time (60 Meters long
Bulbs are designed to blow at 79 deg. on each spur).
centigrade (max.) and Quartzoid Bulb
network shall be maintained with plant air c) Tank Lorry Loading/ Unloading Area :
at a pressure of about 3.5 kgs/sq.cm.g
through a restriction orifice and is such that
Detection of heat for automatic actuation of MV unloading gantries Extinguisher for every
sprinkler system having remote/ local operated 15/20 meters of
deluge valve shall be provided. One deluge gantry.
valve shall be provided for a maximum of 4
bays. Other Pump Houses 2 Nos. 10 kg DCP
Extinguisher
d) LPG Sheds:
Office/Canteen/ At least 2 Nos. 10 kg.
MV sprinkler system having remote/ local Stores DCP extinguishers in
operated deluge valve and at critical places like each building
carousal, evacuation, valve change shed,
automatic detection of heat for automatic MCC/DG Room/HT At least 2 nos. 4.5
operation of sprinkler system shall be provided. Room KG Co2
extinguishers in each
e) LPG Pump/Compressor House : room or for floor area
of about 100 Sq.m.
Based on heat detection automatic MV sprinkler & 4 sand buckets & a
system having remote/ local operated deluge stand shall be
valves shall be provided. provided in MCC/DG
Room.
10.5 FIRST AID FIRE FIGHTING
EQUIPMENT v) 100% spre CO2 cartridges and 50% (Min)
spare DCP bags (as per Fire Extinguisher
10.5.1 PORTABLE FIRE EXTINGUISHERS Capacities) shall be stored in the LPG plant.

i) Portable fire extinguishers shall be located 10.5.2 WHEELED/ MOBILE FIRE


at convenient locations and shall at all times FIGHTING EQUIPMENT
be readily accessible and clearly visible.
i) One No. Mobile 75 Kg DCP fire
ii) The maximum running distance to locate an extinguisher shall be provided in filling
extinguisher in working areas shall not shed, LPG storage vessels/ LPG Pump
exceed 15 meters. House area, Tank truck loading/ unloading
gantry area & tank wagon loading/
iii) The top surface of the extinguisher shall not unloading gantry area.
be more than 1.5 meter high.
ii) The Dry chemical powder used in the
iv) The fire extinguishers shall be provided at extinguishers shall be Potassium/ Urea
various locations as under : based or Sodium Bicarbonate as per
IS:4308. Nitrogen/ Carbon Dioxide shall be
Area Portable Fire Extinguisher used as expellent gas.

LPG Storage 2 Nos. 10 kg DCP iii) Considering the large area, and no. of
Vessel(Each) extinguisher. operations involved in Mega LPG Plants,
special fire fighting facilities like DCP fire
LPG cylinder 2 Nos. 10 kg DCP tenders should preferably be provided.
sheds extinguisher per 200
Sq.M.Area. iv) A trolley with suitable first aid fire protective
accessories shall be readily available in the
LPG Pump 2 Nos. 10 kg. DCP LPG plant.
houses extinguisher per 50
Sq.m. Area. 10.5.3 HOSES, NOZZLES AND
ACCESSOREIS
Tank Truck loading/ 1 No. 10 kg. DCP
loading gantries Extinguisher i) Reinforced rubber lined hoses (63mm)
in each bay. conforming to IS:636 (type A or B) shall be
provided.
Tank Wagon loading/ 1 No. 10 kg DCP
ii) The hoses shall be of 15 Meters standard with one spare cyl.
length and shall be provided with Gun (Cap. 30 minutes)
metal/ Aluminium alloy male & female
couplings of instantaneous pattern. 15. Water jet blankets Min. 2 nos.

iii) 50% spare Hoses shall be stored in the LPG 16. Unitised type gas Min. 2 Nos.
plant. detector

iv) In addition to the nozzles provided in the The above are guidelines and minimum
hose boxes there shall be at least 2 Nos. requirements of each item and can be
spare nozzles in each category viz. Jet increased depending upon the scale of
Nozzles with branch pipes, Fog Nozzles, operations, statutory/ mandatory
universal Nozzles, water curtain Nozzles, requirement of local bodies/ State
Spray Nozzles and Tripple purpose nozzles Governments or any other expert body.
in the plant.
10.6 FIRE/ ALARM/ COMMUNICATION
v) The following accessories/ first aid items SYSTEM
shall be provided in the plant :

1. Fire hoses 100% of no. of 10.6.1 FIRE ALARM SYSTEM


hydrant points.
i) Sufficient No. of Manual call points shall be
2. Safety helmets As required ( Min. provided in the plant.
10 Nos.) 1 no. for
each. ii) Electricity operated Fire Siren shall be
audible to the farthest distance in the plant
3. Hose Boxes alternate hydrant (1 K.M. from the periphery of the plant).
point.
iii) Manually operated fire sirens shall be
4. Stretcher with Min. 2 Nos. each provided at strategic places.
blankets.
iv) For fire condition the siren shall be walling
5. First aid Box Min. 2 nos. sound for minimum `2 minutes and for all
clear signal it shall be straight run siren for
6. Rubber hand gloves Min. 2 pairs 2 minutes.
for electrical (BIS approved)
purpose. v) For Disaster condition the wailing sound
given shall be repeated thrice with a
7. Low temperature 4 pairs minimum 10 seconds gap.
rubber hand gloves
for LPG emergency. 10.6.2 COMMUNICATION SYSTEM

8. Low tem. protective Min. 2 sets i) Communication system like telephone/ PA


clothing for LPG or paging or walkie-talkie shall be provided.
emergency.
ii) In the hazardous areas flame-proof
9. Explosimeter Min. 2 Nos. telephones shall be provided.

10. Fire proximity suit Min. 1 No. iii) Wherever possible Hot line connection
between City Fire Brigade/ near by major
11. Fire entry suit Min. 1 no. Industries shall be provided.

12. Resuscitator Min. 2 Nos. iv) Plant shall have a ` Mutual Aid' arrangement
with near by industries.
13. Red/Green Flags As required
10.7 SPECIAL FIRE PROTECTION
14. Self contained Min. 1 No.
breathing apparatus
The most hazardous situation in LPG vessel is
the possibility of BLEEVE. This usually takes The fire fighting system shall be periodically
place when the vessel is subjected to external tested for proper functioning and logged for
fire. record and corrective actions. In addition to
routine daily checks/ maintenance the following
The unwetted (vapour space) portion of the shell periodic inspection/ testing shall be ensured.
gets overheated and fails even at the operating
pressure. As such, it is important that metal 10.8.1 FIRE WATER PUMPS
temperature in the vapour space is protected
from overheating by some measures. A passive i) Every Pump shall be in test run for atleast
measure like fire proofing/ insulation or fire 10 min. twice in a week at the rated
retardant coating will provide protection in the conditions.
initial period of fire which is very crucial. This
will give some breathing time for activating ii) Once in a month each pump shall be checked
other fire fighting measures like starting of and tested and the shut-off pressure
pumps, organising people, opening of valves etc. observed and logged. Also the pump
This will also take care of automation failure performance shall be ascertained.
wherever it is provided.
iii) The Jockey pump operation shall be checked
In the event of exposure of LPG vessel to fire it periodically. Frequent start/ stop condition
is recommended that fire proofing provided on of Jockey pump indicates that there are
the vessel and supporting legs shall be adequate water leaks in the system.
to protect the shell material from overheating
and consequent failure. The material provided 10.8.2 FIRE WATER RING MAIN
for fire proofing purpose shall be good enough
to provide this protection for the initial 30-60 i) The ring main shall be kept pressurised at 7
minutes. Based on this it is recommended to kg/sq.cm.g with the help of one or more
provide the minimum rating for fire proofing as jockey pumps.
follows :
ii) The ring main shall be inspected for any
LPG storage vessel & connected 1 hour visual leaks, detects, damage and corrosion.
lines upto the fire safe ROVs
iii) All valves on the ring main/ hydrant/
Supporting legs of all above 2 hour monitor valves shall be checked for leaks/
operation and lubricated once in a month.
Before fire-proofing application, protected metal
surfaces shall be prepared through such means 10.8.3 FIRE WATER SPRINKLER
as sand-blasting and corrosion-protective SYSTEM
primers. Particular attention shall be given to
the top junction of the fire-proofing with the i) All deluge valves and sprinkler system shall
protected metal to prevent water ingress. be operated and checked once in a quarter
for correct remote operation performance of
Fire water line to each sphere should be so each nozzle and effectiveness of system in
routed that it is not exposed to direct fire. This total.
is to protect it from failure in the initial period
when water flow has not commenced. It is ii) The sprinkler system in the sheds shall be
recommended that riser should be located away tested by closing the outlet of the deluge
from bottom ROV. The horizontal run of the valve for correct remote operation once in a
Fire Water line may be buried if fire engulfment quarter.
cannot be avoided otherwise. Fire proofing shall
include connected LPG lines and pipe supports iii) The strainers provided in the Fire water
within 15 M of a storage vessel or in the sprinkler system shall be cleaned once in a
drainage paths. quarter and records maintained.

10.8 INSPECTION AND TESTING 10.8.4 FIRE WATER RESERVOIR

The fire protection equipment shall be kept in In case of a Reservoir the same shall be cleaned
good operating condition all the time. once in 6 months or earlier as and when needed
so that there shall not be any foreign particles/ Facilities to make up water during fire fighting
fungus/ vegetation in the reservoir. shall be provided.

10.9 MAKE UP WATER :


CHAPTER 11

EMERGENCY MANAGEMENT PLAN

11.1 GENERAL a) Through water drain valve while


draining.
11.1 The best way to manage any emergency is
to prevent it. Following guidelines for b) Leaking sample valve.
emergency prevention shall be followed :
c) Breakage of glass on Sight Flow Indicator
Ensure : on the pipeline.

a) Sound engineering practice in the d) Opening of pot-off valve, gland/ packing


design, fabrication, installation and etc.
maintenance of facilities.
e) Leakage through LPG compressor/ pump.
b) Careful selection and correct use of
equipment. f) Leakage due to bursting/ rupture of hose
or through sviwel joints of body arms.
c) Observance of safety and security
regulations. g) Leakage from the filling guns.

d) Proper and constant training and h) Escape of liquid/ vapour LPG during
guidance to all pesonnel working in maintenance/ repairs.
the Plant, with particular reference to
product knowledge and maintenance 11.1.4 BEWARE OF COMMON CAUSES
practices. OF FIRE, SOME OF WHICH ARE:

e) Good House-keeping. (a) ELECTRICAL :

f) Constant supervision and alertness. i) Short circuiting due to loose wiring


including that of automobile moving
in the area.
11.1.2 EMERGENCY PLANS :
ii) Use of non-flame proof fittings such
Plant Manager shall ensure that suitable as lights, torch, motors, fan,
instructions are issued to both Corporation's and telephone, temporary lighting etc.
contractor's personnel identifying the action to (Note : Flameproof fittings become
be taken by each one in an emergency. This non-flame proof due to poor
should be achieved by display of organisation maintenance e.g. increase in gap in
chart/ posters not only for fire-fighting but also junction boxes, due to missing nuts
for other likely emergencies. Likewise, for and bolts or improper glands used for
emergencies of large magnitude Emergency connection to junction box, or sealing
Response Plan (or Disaster Management Plan) compound not used in junction boxes
to be drawn out in coordination with related etc.)
outside agencies, such as local administration,
Police authorities, Fire Brigade, hospital iii) Static electricity as result of improper
authorities, home guards, neighbouring bonding/ grounding to tanks,
industries etc. Periodic mock drills for all such conveyor system, tank truck, tank
plans to be conducted, and plans to be updated/ wagon etc.
modified based on experience gained during
such drills.
(b) VEHICLE :
11.1.3 BEWARE OF LPG LEAKAGE AT
PLANTS, THESE ARE : i) Exhaust of vehicle, if effective spark
arrestors are not provided.
ii) Operation of non-FLP electrical switches f) Plant personnel without specific duties
such as vehicle ignition. should assemble at the nominated place.

iii) Spark from the loose contact on vehicle g) All vehicles except those required for
batteries. emergency use should be moved away
from the operating area, in an orderly
iv) Spark from exhaust of railway engine. manner at pre-nominated route.

v) Cinders from the steam locomotives. h) Electrical system except for control
supplies, utilities, lighting and fire
(c) OTHERS fighting system, should be isolated.

i) Landing of crackers (flying type ) in i) If the feed to the fire cannot be cut off, the
hazardous areas. fire must be controlled and not
extinguished.
ii) Chiselling/ hammering.
j) Start water spray system at areas involved
iii) Spark from studed shoes, with steel button in or exposed to fire risks.
by friction against ground/ metal.
k) In case of leakage of LPG without fire
iv) Lighted agarbatti in a truck. and inability to stop the flow, take all
precautions to avoid source of ignition.
v) Excessive release of vapour beyond safe
limit and fire due to outside source of l) Block all roads in the adjacent area and
ignition. enlist Police support for the purpose if
warranted.
vi) Lighting
11.2.2 Fire Fighting Operations :
vii) Smoking.
a) Enlist support of local fire brigade and
11.2 BASIC ACTION IN EMERGENCIES : neighbouring industries.

11.2.1 Immediate action is the most important b) If escaping vapour cannot be stopped, jets
factor in emergency control because the of water should be directed at the point of
first few seconds count, as LPG fires leakage to assist controlled release of
develop and spread very quickly unless vapour and in between water fog should
prompt and efficient action is taken. In be used for dilution and rapid disperson
the event of fire/ gas leak within LPG of vapour cloud.
Plant the following action shall be taken
as quickly as possible: c) Fire Fighting personnel working in or
close to unignited vapour clouds or close
a) Take immediate steps to stop LPG to fire must wear protective clothing and
leakage/ fire and raise alarm equipment including safety harness and
simultaneously. manned life line. They must be protected
continuously by water sprays. Water
b) Initiate action as per Fire Organisation protection for fire fighters should never
Plan or Disaster Management Plan, based be shut off even though the flames appear
on gravity of the emergency. to have been extinguished until all
personnel are safely out of the danger
c) Stop all operations and ensure closure of area.
all ROVs and isolation valves.
d) Exercise care to ensure that static charge
d) All out effort should be made to contain is not generated in LPG vapour cloud. For
the spread of leakage/ fire. this purpose solid jets of water must be
avoided, instead fog nozzles should be
e) Saving of human life shall get priority in used.
comparison to stocks/ assets.
e) Fire fighters should advance towards a
fire down wind if possible. d) Exercise care to ensure that static charge
is not generated in LPG vapour cloud.
f) Cylinder fire should be approached using For this purpose solid jets of water must
proper barricades/ protection to avoid be avoided, instead fog nozzles should be
direct hit from flying cylinders. used.

g) If the only valve that can be used to stop e) Fire Fighters should advance towards a
the leakage is surrounded by fire, it may fire down wind if possible.
be possible to close it manually. The
attempt should be directed by trained f) Cylinder fire should be approached using
persons only. The person attempting the proper barricades/ protection to avoid
closure should be continuously protected direct hit from flying cylinders.
by means of water spraying (through fog
nozzles), fire entry suit, water jel blanket g) If the only valve that can be used to stop
or any other approved equipment. The the leakage is surrounded by fire, it may
person must be equipped with a safety be possible to close it manually. The
harness and manned life line. attempt should be directed by trained
persons only. The person attempting the
h) Any rapid increase in pressure or noise closure should be continuously protected
level of product discharged through safety by means of water spraying (through fog
relief valve of the vessel/ pipeline should nozzles), fire entry suit, water jel blanket
be treated as a warning of over or any other approved equipment. The
pressurisation. In such cases all personnel person must be equipped with a safety
should be evacuated immediately. harness and manned life line.

i) As in case of any emergency situation, it h) Any rapid increase in pressure or noise


is of paramount importance to avoid level of product discharged through safety
endangering human life in the event of relief valve of the vessel/ pipeline should
fire involving or seriously exposing LPG be treated as a warning of over
equipment or serious leakage of LPG pressurisation. In such cases all
without the fire. personnel should be evacuated
immediately.
11.2.3 Action in the event of LPG leakage
without fire : i) As in case of any emergency situation, it
is of paramount importance to avoid
a) Take basic action as detailed in 11.2.1 endangering human life in the event of
above. fire involving a seriously exposing LPG
equipment or serious leakage of LPG
b) If escaping LPG is not on fire, close any without the fire.
valve which will stop the flow.
11.2.3 Action in the event of LPG leakage
c) In some cases like the leakage from a without fire :
pressure vessel without a fire (such as
leak from tank truck bullet or a) Take basic action as detailed in 11.2.1
overturning) it may be desirable to move above.
the vessel to some remote area such as
block of isolated roadway or open field b) If escaping LPG is not on fire, close any
where it can be allowed to leak safely valve which will stop the flow.
without a source of ignition nearby.
However, if this is to be done, the vessel c) In some cases like the leakage from a
must be moved in an upright position. pressure vessel without a fire (such as
Never drag the vessel in a manner which leak from tank truck bullet or
might damage valve or pipeline. Any overturning), it may be desirable to move
attempt to turn a vessel back upright to the vessel to some remote area such as
move it to some remote location should be block of isolated raodway or open field
done carefully to avoid damage to valve where it can be allowed to leak safely
and pipelines. without a source of ignition nearby.
However, if this is to be done, the vessel (ii) Fire on storage vessel : If a pressure
must be moved in an upright position. vessel is exposed to radiant heat from
Never drag the vessel in a manner which external fire, it should be kept cool by
might damage valve or pipeline. Any water sprays to prevent excessive pressure
attempt to turn a vessel back upright to rise in the vessel. Cooling water sprays
move it to some remote location should be must be applied without delay to the heat
done carefully to avoid damage to valve affected area using fixed water sprinkler
and pipelines. system or equivalent spray water
coverage, through fixed monitors or other
11.2.4 Action in the event of LPG fire : equipment. Cooling the vessel with water
sprays reduces the heat input to the vessel
a) Take basic action as detailed in 11.2.1 and thereby reduces the pressure, thus,
above. reducing the rate of discharge from the
relief valves.
b) Extinguishing Fires - A small fire at the
point of leakage should be extinguished (iii) Leakage of LPG burning at the outlet of a
by enveloping with a water spray or a cylinder valve: Extinguish the fire by
suitable smoothering agent such as means of a portable fire extinguisher, or
carbon dioxide or dry chemical powder. smoothering with a thick non-synhetic
However, it is again stressed that LPG fire cloth (preferably wet) or sand/ earth etc.
should not; except in special
circumstances explained earlier; be Fix safety cap on the valve to prevent
extinguished until the escape of product further leakage.
has been stopped.
After the fire is extinguished, if the
c) Fire fighting procedure - Fire fighting leakage cannot be stopped the cylinder
procedures would vary depending upon should be moved carefully to a safe
various factors such as nature, sources, location to vent out the contents under
size, location, etc. of fire. Basic fire controlled conditions.
fighting techniques have been explained
earlier in section 11.2.2. However, for the (iv) Fire of LPG vapour escaping from a
purpose of guidelines, fire fighting damaged vessel fitting ( flame not
techniques for few common cases are as playing on vessel) :
follows :
Allow fire to continue till exhaustion.
(i) Cylinder Fire : If a filled cylinder is
involved in fire, internal pressure may Spray vessel with water to cool it, if vessel is
start rising and if not relieved the built up being heated by radiation from the flame or if
pressure could rise above 70 kgf/sq.cm.g flame is endangering other plant equipment.
and ultimately rupture the container.
Ignition of the escaping gas would Cool adjacent vessels and structures.
aggravate the fire but the release of
pressure would reduce the possibility of (v) Fire at Safety Relief Valves of vessels
rupture of the container. No attempt exposed to adjacent fire.
should be made to extinguish the burning
gas. Bus the container and other (vi) Fire in Oil storage area adjacent to
containers in the vicinity should be kept LPG storage :
cool by water sprays until the contents of
the container have burnt away. If the gas Start water sprays only on those LPG
leakage does not ignite, the container vessels exposed to fire/ heat.
should be approached from upwind (if in
the open air) and be removed to a place of Isolate affected vessels and run out fire
safety remote from sources of ignition. water hoses in case hose stream cooling
Cylinders not directly involved in the fire becomes necessary.
should be moved away from heat
exposure, while applying cooling water Water pressure in LPG vessels.
sprays on cylinders directly involved.
If LPG vessel's SRVs have started personnel. It shall include the following
blowing vapour, take no further action functions, expanded to suit the location
(apart from cooling) unless vessel facilities/ requirement:-
pressure continues to rise.
(i) Sounding the emergency (fire) alarm.
If fire enters LPG storage area,
concentrate available cooling water on (ii) Shutting off the LPG supply to any leakage
LPG vessels, most affected. point/ fire.

Do not try to empty LPG vessels exposed (iii) Summoning the fire brigade/ police.
to fire. They become more vulnerable to
overheating as their liquid content (iv) Fire control, with first aid, fire fighting
decreases. equipment.

(v) LPG vapour dispersal.


11.2.5 Fire Fighting Organisation Plan :
(vi) Operation of LPG vessel's fixed water
(a) A plan of action for use in the event of a sprinkler system, starting of fire pump (s)
major LPG product leakage with a fire or and application of water hose jets/ sprays
risk of fire is essential. Such a plan must for containing/ extinguishing fires.
be carefully prepared for each plant. It
should be fully understood by all LPG (vii) Cooling of vessels/ cylinders and other
plant supervisory personnel and other equipment/ facilities.
personnel responsible for action as per
plan. It shall be based on the following : (viii) Closing down all operations in the plant
including closure of valves and stopping
(i) Plant personnel shall be fully trained for of pumps.
the specialized techniques necessary for
combating LPG leakages and LPG fires. (ix) Preventing all sources of ignition in case of
LPG leakage.
(ii) If leakage and/ or fire occures, all
personnel should use the equipment (x) Evacuation of vehicles.
provided and to carry out their allotted
tasks as detailed in the fire fighting (xi) Evacuation and mustering of personnel.
organisation plan.
(xii) Establishing an emergency fire-control
(iii) All personnel should be conversant with centre.
fire control equipment and also its
location. (xiii) Traffic control.

(iv) LPG plant personnel should know the (xiv) Stations and duties of all personnel.
position and method of operation of all
Remove Operation valves (ROVs) in the (xv) Policing of affected areas.
plant.
(xvi) Any other specialised duties.
(v) Plant personnel should be familiar with
the standard recognition markings of fire (xvii) Display of fire brigade, ambulance, Police
control, first aid and all safety equipment, telephone numbers etc.
must know the location of emergency
exits, and they should know the location (xviii) All clear signal by competent person.
of water hydrant points/ monitors and
must be familiar with the sound of the (c) Liaison with local fire brigade :
emergency (fire) alarm.
Close co-operation with the local fire authorities
(b) The Fire Fighting Organisation Plan is essential and shall take the following form :
together with layout of fire fighting and
safety devices shall be displayed at (i) The fire brigade should be made familiar
prominent places and explained to all with the layout of the plant and the
location of important equipment/ facilities g) The local fire brigade should be
provided, and their method of use. Mock encouraged to participate in fire drills
fire drills/ exercise jointly by plant periodically.
personnel and local fire brigades shall be
planned. h) Any shortcoming, noticed during the drill
shall be rectified.
(ii) Fire fighting equipment at the plant shall
be compatible with the fire brigade 11.2.6 Disaster Management Plan : ON-
equipment, otherwise adaptors shall be SITE
kept ready for hoses, hydrants etc.
a) It is basically a pre-plan to handle any
(iii) The fire brigade shall be aware of the emergency situation of a higher
plant's fire fighting organisation plan and magnitude arising out of factors listed
the views held at the plan regarding the below:
most effective LPG fire control methods.
(i) Major fire/ explosions
(iv) In the event of an emergency/ fire, the
plant manager and/ or his representative (ii) Uncontrollable leakage of LPG
shall advise the Fire Officer about
particular or potential hazards that may (iii) Lightning
be present e.g. stocks of filled cylinders at
that particular point of time. (iv) Heavy floods

(d) Fire Drills & Training : (v) Earthquakes/ land slides

a) Drills for all Plant personnel, making use (vi) Sabotage/ terrorist outrage
of the "Fire fighting Organisation Plan"
and practicing the specialised techniques (vii) War situation
required for fighting LPG fires or
dispensing/ diluting LPG vapour clouds The objective of the plan shall be to reduce the
shall be held minimum once in a month. probability of serious loss/ damage to general
stock, plant and machinery, documents etc.
b) The drills should cover various types of utilizing combined resources of the location
incidents, e.g. major spillage, LPG bulk itself and the outside agencies. In order to have
lorry fire, cylinder fire etc. an effective organisation, preliminary meeting
shall be conducted with the representatives from
c) Extinguishers due for recharging/ due for local fire services, police authorities, voluntary
hydrotesting shall be discharged during organisations like ambulance service/ Govt.
drills and replenished subsequently 50% medical service/ contractors and even Home
(Min.) stock of refills as replenishment Guards and defence personnel. In the course of
for FEs should be maintained. the meeting, there should be exchange of
knowledge, training and plans for development
d) The fire pump should be run, sprinkler of expertise and skills to gain knowledge about
system activated, emergency systems the plant layout/ facilities, potential of likely
tested, water hoses run out and spray/ set hazards/ risks, likely emergencies that may
techniques practiced during drills. arise. This group should draw out modalities of
the exercises in the given situation and arrive at
e) Fire alarms shall be sounded/ tested an agreed action plan which should be updated
(neighbouring plants/ factories and the from time to time and put to test in the form of
fire brigade shall be warned in advance of periodical mock drills.
this test).
(b) Due to varying risk potentials and also
f) Protective clothing, breathing apparatus varying hazards at/ around each location
and any other specialised safety `Disaster Management Plan' for each
equipment available shall be tried out location shall be drawn up individually
during drills to train all concerned in based on the outline given below:
their application.
(i) Identify Disaster scenario i.e. the situation higher authorities within the
under which the plan would become organisation.
operational. Plan for the worst possible
scenario. (viii) Mock drills to be conducted minimum
once a year.
(ii) Identify resources required from each of
the outside agencies. (ix) Modify the plan based on the experience
gained through mock drills and try out
(iii) Establish outside agencies, role of each the modified plan through subsequent
agency and obtain their commitment for mock drills.
rendering the assistance in crisis situation
as per the agreed plan. (x) The plan shall be updated as and when the
changes recorded in the plan occur and
(iv) Establish organogram for Disaster communication sent to all concerned.
Management based on available
manpower in various groups and identify (c) Communication organogram :
the leader and alternative leader for each
for the groups and the role to be played by As a part of Disaster Management Plan,
each team in various likely crisis communication organogram shall be drawn up
situations. giving flow of communication from the
originating location to various local agencies
(v) Identify Disaster control room/ group. and also to Statutory Authorities and upwards
within the organisation to mobilise support and
(vi) Furnish detailed data and drawings to consider alternatives for maintaining essential
relevant for the crisis management. supplies.

(vii) Establish channel of communication at the


local level to Statutory Authorities and
CHAPTER 12

SAFETY AUDIT

12.1 GENERAL: These check lists can be further supplemented


and modified suitably to meet the specific
Safety audit is a well recognised tool to improve requirements of individual plant.
the effectiveness of safety programme and loss Recommended minimum safety audits at
prevention measures by carrying out systematic different levels, their frequencies and broad
and critical appraisal of potential safety hazards check lists to be used are indicated below :-
involving personnel, plants and equipments.
Daily audit essentially shall cover the
For a structured and systematic safety audit of compliance of recommended operating
any plant/ facility, check lists are the most procedures/ safety practices. Reports of audit
important prerequisite. Check lists should cover shall be reviewed by the Plant Manager on daily
all the operational areas, major equipments, basis and corrective action be undertaken on
operating/ maintenance procedures, safety priority wherever required.
practices, fire prevention/ protection systems etc.
Observations/ recommendations of safety audit In case of external safety audit, following areas
team should be presented in the form of a besides the points given in check list of
formal report and action plan for corrective Annexure III shall be covered.
measures should be prepared and subsequently
monitored for implementation. 1. Safety Organisation

General guidelines on safety audit 2. Security System


methodologies and techniques are also given in
OISD - GDN- 145. 3. Fire prevention/ protection system

12.2 TYPE OF SAFETY AUDIT AND 4. Preparedness to handle any emergency


PERIODICITY : --Disaster control plan and mock drills.

In view of the high hazard potential of LPG, 5. Skill level and training needs for HRD.
safety audits at frequent intervals by the teams/
personnel of various levels are advocated, Broad 6. Operating manual/ instructions, display
check lists for different recommended safety of Do's/ Dont's etc.
audits are given in the Annexure I, II, III, IV.

S.No. Type of Safety By Frequency Checklist


Audit (Annexure)
-----------------------------------------------------------------------------------------------------------------------------
1 2 3 4 5
-----------------------------------------------------------------------------------------------------------------------------

1. Inspection Safety LPG Plant Daily I


audit of LPG Bottling Safety
Plant. Officer

2. Electrical audit of Expert Annual II


LPG Bottling plants personnel
from electrical
discipline

3. Detailed safety audit Multi disciplinary Annual III


of LPG Bottling Plants team of region/
corporate level

4. Inspection and Expert Annual IV


maintenance audit of personnel of
LPG Bottling plants Inspection/ Maintenance

5. External safety audit Panel As decided Based on


of LPG Bottling plants constituted by OISD observations

by OISD and OISD

Checklist

--------------------------------------------------------------------------------------------------------------------------------
ANNEXURE - I

DAILY SAFETY AUDIT - CHECKLIST


FOR LPG BOTTLING PLANTS

LOCATION ______________

Audit/ Inspection by _________________

--------------------------------------------------------------------------------------------------------------------------------
S.No. Item Description Observation Corrective Action Remarks
1 2 3 4 5
--------------------------------------------------------------------------------------------------------------------------------

A. SAFETY/ FIRE PROTECTION SYSTEM

A-01 Water level in static Yes/No


water tank is satisfactory.

A-02 Hydrant pressure Yes/No


maintained with jockey pump.
Record Pressure.

A-03 Fire water pumps/engines Yes/No

a) Are the batteries in good condition.

b) Are the diesel tanks full

c) Start one pump, record pressure developed.

d) Whether auto start system working.

A-04 Fire alarm/ Yes/No


communication system in working order.

A-05 Automatic Gas Detection Yes/No


system operating.

A-06 Vapour Extraction Unit operating Yes/No

A-07 Any unsafe condition of Yes/No


S&FP system observed
(specify in brief under remarks column).

A-08 Any signs of beedi/ Yes/No


cigarette butts/ used matches
observed in the area- particularly at toilets.

A-09 Regular surprise checks/ testing Yes/No


being done at gate/ at the plant.
--------------------------------------------------------------------------------------------------------------------------------
S.No. Item Description Observation Corrective Action Remarks
1 2 3 4 5
--------------------------------------------------------------------------------------------------------------------------------
A-10 Caution signs displayed Yes/No
at appropriate places.

A-11 Direction of wind Yes/No


(specify in remarks column by
observing wind sock).

B. BULK STORAGE AREA

B-01 Whether water draining Yes/No


sampling done under constant
supervision.

B-02 Earthing connection Yes/No


apparently sound.

a) Whether level instruments are working.

b) High level alarm in working condition (test check).

B-04 Portable fire Yes/No


extinguishers in position.

B-05 Water spray/ sprinkler Yes/No


system apparently O.K.

B-06 Housekeeping is in order Yes/No

B-07 Gas detection system working Yes/No

C. TANK WAGON UNLOADING

C-01 Any visible sign of LPG leakage Yes/No

C-02 Earthing connection apparently sound Yes/No

C-03 a) Whether hose condition/ Yes/No


connections are proper

b) Are these properly Yes/No


plugged if not in use.

C-04 House keeping in order. Yes/No

D. BULK TRUCK UNLOADING


--------------------------------------------------------------------------------------------------------------------------------
S.No. Item Description Observation Corrective Action Remarks
1 2 3 4 5
--------------------------------------------------------------------------------------------------------------------------------

D-01 Are all vehicles allowed in licensedYes/No


area permanently fitted with CCE
approved spark arrestors on exhaust
pipe (Random check)

D-02 Is the vehicle engine and master Yes/No


switch being shut off during
unloading bulk LPG (site check)

D-03 Are the earthing connection Yes/No


properly made before connecting
hoses to tank trucks.

D-04 Rotogauge, Fixed level instrument Yes/No


in working order (Random check.
Record TT No)

D-05 Any visible sign of LPG leakage Yes/No

D-06 Random safety check of Yes/No


tank truck No.

a) CCE licence available/ valid Yes/No

b) Fittings as per CCE Yes/No

c) 2 Nos. of fire extinguishers Yes/No


available in good condition/
easily accessible.
(physical check)

d) Safety instruction booklet Yes/No


TREMCARD available. Record
any abnormality/discrepancies observed.

e) Wheel choke used Yes/No

D-07 a) Portable extinguisher Yes/No


available in nominated places.

b) Sprinkler system in Yes/No


working condition.

D-08 House keeping in order Yes/No

D-09 Bonding of flange connection given Yes/No


E. PUMP HOUSE/ COMPRESSOR ROOM

--------------------------------------------------------------------------------------------------------------------------------
S.No. Item Description Observation Corrective Action Remarks
1 2 3 4 5
--------------------------------------------------------------------------------------------------------------------------------

E-01 Electrical connections apparently sound Yes/No

E-02 Earthing apparently proper Yes/No

E-03 Gauges on pumps/compressor Yes/No


in working condition, record pressure.
E-04 Drain/ vent connection cap in position. Yes/No

E-05 Safety guards in position Yes/No

E-06 Abnormal vibration/ excessive noise. Yes/No

E-07 Portable fire extinguisher in position Yes/No

E-08 Any visible sign of LPG leak or any Yes/No


unsafe conditions observed (record
under remarks column).

E-09 Housekeeping in order. Yes/No

E-10 Gas detection system working. Yes/No

F. FILLING SHED
F-01 No ignition sources visible in operating Yes/No
areas or area in vicinity.

F-02 Are the LPG cylinders empty or empty Yes/No


or filled, properly loaded/ unloaded and
handled to avoid impact, falling, horizontal
rolling etc.

F-3 Are earthing connection on filling Yes/No


carousel properly made.

F-04 Are the cylinder chain conveyors adequately Yes/No


lubricated to avoid metallic rubbing and friction.

F-05 Water in test bath is clean and maintained Yes/No


upto the required level.

F-06 Any sign of leakage of unsafe condition Yes/No


None of the filling guns or adaptors used
for cylinder filling/emptying are leaking.

--------------------------------------------------------------------------------------------------------------------------------
S.No. Item Description Observation Corrective Action Remarks
1 2 3 4 5
--------------------------------------------------------------------------------------------------------------------------------

F-07 Are all the fire extinguishers available Yes/No


in accessible location.

F-08 All electrical connection apparently Yes/No


intact & safe.

F-09 Is the concentration level of gas checked Yes/No


with explosimeter twice a day in the filling
area in filled and empty cylinder area, pump/
compressor room. Record reading for sample
check.
F-10 Sprinkler system in working condition Yes/No
(physical check).

F-11 Housekeeping is in order. Yes/No

F-12 Rotary equipment/ coupling etc Yes/No


properly graded.

F-13 Gas detection system working. Yes/No

G. CYLINDER STORAGE/ HANDLING


G-01 Are cylinders stacked properly in Yes/No
demarcated areas. (filled/empty/
defectives).

G-02 Any leaky overfilled cylinder kept at Yes/No


the end of the day. Record No. if any,
of the leaky unevacuated cylinder.

G-03 Safety cap fixed on cylinders in stock. Yes/No

G-04 Explosimeter/ portable lead gas detector Yes/No


used to detect gas leaks periodically in
stacking area.

G-05 Cylinders loaded in to trucks through Yes/No


conveyors.

G-06 Rubber mats are used for unloading Yes/No


empty cylinders from tank trucks and
are in good condition.
ANNEXURE - II.

ELECTRICAL AUDIT OF LPG BOTTLING PLANTS

LOCATION _____________ Dated ____________

AUDIT/ INSPECTION BY ______________________

--------------------------------------------------------------------------------------------------------------------------------
S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------

A. ELECTRICAL SUBSTATION/ SWITCH ROOM

A-01 Is painted line diagram of power/ lighting distribution provided.

A-02 Is the equipment easily accessible for operation, inspection & maintenance.

A-03 MCC Panel condition :

a) Doors okay and closed

b) Dust/soot/ cobwebs not existed

c) Lugs existing at each cable, termination not loose.

d) Visual condition of switch contact fuse etc. O.K.

e) Control wiring condition satisfactory.

f) Jumper condition between bus and distribution okay.

g) Grounding OK

h) Alarm/ trip circuit working.

A-04 Live parts of equipment made inaccessible by barriers/ shrouds.

A-05 No temporary electrical connection existing.

A-06 Condition of cable duct

a) Cables are on rack

b) Cable deck clear

c) Sealing of duct

d) Cable identification tags.

--------------------------------------------------------------------------------------------------------------------------------
S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------
A-07 Rubber mats (with ISI mark) existing are enough in number.

A-08 Protective relays set at recommended values.

A-09 All fuses are of proper type and rating as specified in single line diagram.

A-10 Fire extinguishers are of proper type and are in working condition.

A-11 Lighting condition OK (fixtures/ tubes/ wtiches etc.)

A-12 Emergency lighting system in order.

A-13 All energised equipment provided with caution boards.

A-14 Condition of transformer :

a) Grounding OK

b) No oil leak

c) Silica gel OK

d) Oil level OK

e) Terminal box earthing OK

f) Oil/winding temp. OK

g) Periodic oil quality test conducted.

A-15 Whether location/type of transformer in conformity with area classification drawings.

A-16 Housekeeping is good.

B. MOTORS IN PUMP HOUSE/ COMPRESSOR


ROOM/ FILLING & STORAGE SHED ETC.

B-01 Is double independent earthing connection for all motors provided.

B-02 Is grounding wire OK (not loose).

B-03 a) Is terminal box and gland OK


Flame proofness maintained and not tampered.

b) Existing cable termination are proper

B-04 a) Is push button earthed properly and flame proof condition not tampered.
b) General condition of push button good.

B-05 Ground resistance at motor/ push button measured and found okay.

B-06 No motor abnormality

- Vibration/ bearing condition, faulty guard, fan condition,


excessive noise, high body temperature.
B-07 Existing preventive maintenance schedule OK.

B-08 a) Earthing resistance test schedules/ records satisfactory.

b) Earthing pit condition OK

B-09 i) Carousel machine frame to filling gun earthing continuity maintained.

ii) Carousel machine frame to central column earthing continuity OK.

B-10 Conveyor system bonding and earthing maintained.

B-11 First-aid chart for treating electrical shocks displayed prominently in MCC room.

C. UNIT LIGHTING

C-01 All lighting fixture flame proof as per area classification.

C-02 Whether flame proof condition of fixtures ensured ?

C-03 Whether proper earthing of fixture provided ?

C-04 Condition of wiring good.

C-05 Does water enter and accumulate in fixture distribution boxes etc ?

C-06 Whether lighting DB, switches, MCB well maintained ?

C-07 Any other unsafe point observed.

D. MAST LIGHTS (AREA LIGHTING)

D-01 Whether grounding of mast OK ?

D-02 Condition of junction boxes, switch board, fuses etc. OK

D-03 Approach to electrical installation and ladder good and safe.

D-04 Condition of flood lights :

a) Is gasket present ?

b) Is glass cover in good condition ?

c) Is control gear condition OK


--------------------------------------------------------------------------------------------------------------------------------
S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------

D-05 Is earthing electrode of mast OK and its


connnection with mast proper ?

E. TANKAGE AREA, PIPELINES, LOADING/


UNLOADING GANTRY
E-01 Are LPG pipelines provided with flange earth jumper connection
for electrical continuity?

E-02 Are earthing provision on LPG storage vessel well maintained ?

E-03 Condition of grounding electrode OK

E-04 Continuity of location, hoses maintained.

E-05 Grounding resistance at inlet of grounding connection checked/ date (for vessels etc.)

E-06 Connection of earth-bonding of railway track OK.

F. GENERAL

F-01 a) Area classification drawings duly approved by CCE, Nagpur?

b) Conditions if any, specified by CCE for electrical substation, switch


room etc. and their compliance.

F-02 Certificate in respect of FLP for each electrical equipment- records maintained.

F-03 Earthing network diagram available and site checks done from time to time.

F-04 Records for electrical testing/ checks maintained upto date.

F-05 Work permit system is effective and records are maintained.

Note : For developing a detailed check list refer OISD-GDN-145-09 document on safety audit check list
for electrical system.
ANNEXURE - III

DETAILED SAFETY AUDIT OF LPG BOTTLING PLANTS

LOCATION _____________ Dated ____________

AUDIT/ INSPECTION BY ______________________

--------------------------------------------------------------------------------------------------------------------------------
S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------

A. BULK STORAGE AREA

A-01 Area under the sphere is having concrete pavement with proper
slope leading to shallow sumps.

A-02 a) Water drain chamber provided away from shadow of sphere.

b) Double valves on water drain line provided: the first one


(near to chamber) of quick shut off type and the other are
throttle type (Globe valve).

c) Safety instructions for draining operations displayed prominently


and water draining is done under supervision.

A-03 a) Relief valves provided with isolation valves.

b) Isolation valves in locked open condition.

A-04 Last safety valve test done as per statutory requirement and record maintained.

A-05 Remote operated valves provided on liquid inlet/outlet lines with push
buttons/ indication control and located at safe distance.

A-06 Two independent level instruments and high level alarm provided in
storage vessels and are in working condition.

A-07 All leg supports of Horton spheres/ vessels encased in concrete with
fire proof coating/ motar.

A-08 a) Sprinkler system provided on all vessels and are in working condition.

b) Deluge valve is remote operated and is located at safe distance from storage vessels.

A-09 Gas detection system provided and in good working condition (To be checked).

A-10 a) All flame-proof electricl fittings provided.

b) Earthing connections properly maintained.


--------------------------------------------------------------------------------------------------------------------------------
S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------
A-11 Statutory inspection/ hydro test records maintained.

B. PUMPS/ COMPRESSORS AREA

B-01 a) All electrical motors/ push buttons properly earthed and flame proofness maintained.

b) Flame proof light fittings provided.

c) Earthing resistance test conducted periodically and record maintained.

B-02 Venting through high rise vents or flare systems only.

B-03 a) No leakage from mechanical seals.

b) Double seal provided to minimise chances of leakage.

c) No abnormal sound and vibration from motor and bearings condition OK.

d) Coupling guards in position.

B-04 Drain points/ vent points/ sample points capped when not in use.

B-05 Operating instructions Do's and Dont's displayed.

B-06 Long range monitors/ fixed water spray with proper throw/ sprinkler system
installed and in good condition.

C. CYLINDER FILLING/ STORAGE AREA

C-01 LPG bottling facilities located at safe distance from other facilities with
minimum ingress to trucking traffic.

C-02 Facilities provided for positioning of trucks 15 m away from storage shed
for receipt/ loading of cylinders.

C-03 Transfer of cylinders from truck to conveyor.

- Telescopic conveyor

- Trolley use

C-04 Proper purging facilities provided for new/ retested/ reconditioned cylinders

C-05 a) Inspection/ visual checks followed for spurious/ defective cylinders and
record maintained.

b) Segregated storage marked for -

i) Spurious

ii) Hot repairs

iii) 5/7 years testing due cylinders

iv) Other defects


C-06 Gross weight filling :

- Auto cut off after completion of filling

C-07 Hoses are of approved quality and periodically tested.

C-08 Vapour extraction system provided for carousel and system is working satisfactorily.

C-09 100% weight checking facilities provided and in use.

C-10 Accuracy of check scales being checked daily and records maintained.

C-11 CVT checks done for `O' ring defects.

C-12 Check facilities provided for valve seat leakage and working satisfactorily.

- CVT with verifier

- Electronic

C-13 Proper facilities/ correction conveyor loops are provided for defective cylinders
(`O' ring & weight correction).

C-14 Bung leak/ body leak check are done through in-line water bath with caps in position.

C-15 Capping/ Pilfer proof sealing facilities provided.

- Aluminium foil

- PVC sealing

C-16 Neck label being put

- Plastic

- Paper

C-17 Quality control checks (SQC) carried out/ records maintained.

C-18 Proper facilities provided for evacuation of defective cylinders and working satisfactorily.

C-19 Cold repairs facilities evacuation for evacuated depressurized cylinders.

- Valve removal/ replacement by use of torque wrench with proper settings.


--------------------------------------------------------------------------------------------------------------------------------
S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------
- PTFE tape/ paste or other suitable sealing compound used.

C-20 Movement of cylinders for cold repairs through floor conveyors/ use of trolleys.

C-21 Mastic flooring provided on the floor storage area to avoid accidental sparks.

C-22 a) Cylinders stacked in vertical position

b) Stacking discipline with small lots of 4 rows and 25 cylinder lengths


followed, a minimum access path of 1M maintenance on both sides of 4 rows.

C-23 Cylinders are inspected for leakage with explosimeter or portable leak detector.

C-24 Sprinkler system provided in the storage shed and in working condition.

D. BULK LPG UNLOADING FACILITIES

D-01 Whether the location and layout of the facilities meet statutory distances/ design guidelines.

D-02 Effective earthing system provided and working satisfactorily.

D-03 a) Hoses used are of approved quality standard.

b) They are periodically tested and replaced after prolonged use.

D-04 Hose contents after unloading are released to high vent located at safe distance.

D-05 Blocked hoses/ pipelines provided with TSVs.

D-06 a) Sprinkler system provided on the railway siding/ tank truck loading/
unloading area are and working satisfactorily.

b) Fire hydrant/ long range monitors provided.

D-07 Remote operated valves provided on liquid loading headers.

D-08 a) Weigh bridge provided on liquid loading headers.

b) Calibration certificate obtained from Weights & Measures Authorities available.

D-09 a) Vehicles are properly checked for any sign of leak, proper fittings and
other valid documents.

b) 2 Nos. of fire extinguishers (DCP type).

c) Explosive licence, safety certificate, fitness certificate.

d) Proper earthing cable with clamps.

D-10 Loading/ unloading procedures along with safety precautions prominently displayed.
--------------------------------------------------------------------------------------------------------------------------------
S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------

E. SAFETY/ FIRE PROTECTION SYSTEM

E-01 Fire organisation chart prepared, updated and displayed.

E-02 Contigency plan updated for tackling major emergencies.

E-03 Important telephone Nos. of State Fire Services, Police, District Admn./
other offices etc. displayed.

E-04 Are fire emergency mock drills conducted periodically and records maintained.

E-05 Work permit system for repairs/ hot jobs etc. followed and records maintained.
E-06 a) Fire water network (layout displayed)

- above ground/ under ground

- corrosion protection

- material of construction

b) Pressure at farthest end and flow

c) Condition of hydrants, long range monitors. Maintenance and inspection schedules


followed and records maintained.

d) Provision of sprinkler system and testing schedules for checking :

- Adequate water distribution : spray nozzle are clean.

- Defective nozzles to be identified for replacement.

- Deluge valve operation satisfactory.

e) Strainers provided at inlet of deluge/ sprinkler water supply main piping. Strainers are
cleaned periodically and records maintained.

E-07 Fire Water Pumps :

- Adequacy of capacity, nos. discharge pressure etc.

- Auto starting (system security logic) provided.

- Working jockey pump operting para meters maintained.

E-08 Static water storage tank -

- capacity and adequacy

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S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------

- Source of water supply and rate of replenishment.

E-09 a) Fire vehicles well maintained.

b) Mutual aid scheme with neighbouring industries/ district


authorities existing.

E-10 a) Fire extinguishers - type, make, capacity, location, provision of


tamper seals on retainer clips.

b) Maintenance procedures/ records of fire extinguishers.

E-11 a) Fire alarm and communication system working satisfactorily.

b) Testing schedule/ maintenance.


E-12 Protective clothing :

- Availability of special fire fighting suits (Aluminised suits)

- Breathing apparatus & its upkeep

- Water jel blankets.

- Use of nylon clothes prohibited.

E-13 Automatic Gas Detection System :

- Working satisfactorily

- Regularly tested.

E-14 No smoking cautions/ signs in Hindi/ English local languages displayed at prominent places.

E-15 First aid facilities maintained.

E-16 a) Emergency lighting system provided in strategic locations and system working satisfactorily.

b) Flame-proof torches available

F. MANPOWER AND TRAINING

F-01 Supervisory/ managerial cadre staff fully trained in all aspects of LPG plant
operations, Disaster control/ emergency handling.

F-02 Safety officer available in each shift and his detailed responsibility/ accountability is drawn.

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S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------

F-03 Training programmes are organised periodically in LPG operations;


fire fighting/ emergency handling etc. for

a) Regular staff

b) Contractor workmen

c) Security staff

d) Tank truck operators/ drivers

F-04 All activities are effectively supervised with available manpower.

F-05 a) Operating manuals and standing instructions provided to working personnel.

b) Small handy safety booklets distributed to all including contractor employees


in English/ Hindi/ Local language.

F-06 Important Do's and Dont's displayed prominently in operation areas.


G. GENERAL

G-01 a) Plant approach/ access roads well maintained and at least two emergency
exits are there.

b) Fencing/ wall around the plant is in proper condition.

c) Segregated parking area for LPG trucks outside the plant.

d) Adequate escape route available for operational facilities.

G-02 a) Strict security checks employed for compliance to safety regulations.

b) Spot checks being done.

G-03 a) Valid CCE licences available for :

- Storage of LPG

- Storage of LPG cylinders

- Filling of LPG cylinders

- Storage of HSD in tanks for running DG sets/ fire water engines.

- Layout plan approved by CCE(layout plan updated and approved by CCE).

G-04 Accident records maintained and updated.


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S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------
G-06 Hot work permit/ clearance issued - proper procedures followed and
documents maintained.

G-07 Following manual/ documents available:

a) LPG operating manual.

b) Safety and Fire Prevention manual

c) Emergency/ disaster control plan

d) Operation/ Inspection manual of equipment supplied by vendors.

e) Gas Cylinders Rules, 1981, SMPV Rules 1981 and other relevant
BIS Standards with latest amendments.

G-08 a) Records of periodic testing of hoses/ replacement.

b) Testing records of Pn relief valves/ pop action valves.

c) Inspection records of underground pipelines etc.

d) Weights & Measures certificates.

G-09 Updated P&I Diagrams, drawing of layout and other facilities available.
G-10 Records of "Daily Safety Audits" reviewed. Corrective action taken.

G-11 General housekeeping standards : area/ facility wise.

G-12 Pipeline colour code system maintained.


ANNEXURE - IV

INSPECTION & MAINTENANCE SYSTEM AUDIT

LOCAL _______________ DATED: _________

AUDIT/ INSPECTION BY ________________

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S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
--------------------------------------------------------------------------------------------------------------------------------

A. GENERAL

A-01 Whether standard system of inspection/ maintenance schedule


developed and followed and records maintained.

A-02 Whether equipment documents supplied by vendors are readily


available and recommended maintenance procedures are strictly
adhered to.

A-03 Whether spare parts for different equipment/ machinery are maintained.

A-04 Whether data card/ history records of static and rotary equipment are
maintained (as per OISD Std.127/28).

A-05 Whether proper work permit system is followed for maintenance jobs and
records maintained.

A-06 Whether personnel protective equipment such as hand gloves, safety shoes,
safety helmet etc. provided to the concerned workmen and their use is ensured
(OISD Std.-155).

A-07 Fire fighting equipment and portable fire extinguishers periodically checked /
tested as per maintenance schedules & records maintained (OISD Std.-142).

A-08 Fire alarm/ communication system scheduled testing & maintenance ensured.

A-09 Whether Explosimeters are periodically checked and calibrated.

A-10 Whether continuous monitoring devices are periodically checked and calibrated.

A-11 Whether exhaust fans and other ventilation devices are properly maintained and
regularly used.

A-12 Whether inspection/ testing of pressure vessels carried out periodically as per statutory
requirements and records maintained.

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S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
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B. BULK STORAGE HANDLING FACILITIES

B-01 Whether design of pressure storage vessels conform to relevant


BIS/BS/ASME code with standard engineering practices. All
required fittings/ instruments/ safety valves have been provided.

B-02 Whether inspection/ test certificate at the time of original fabrication


available and subsequent inspection/ hydraulic test carried out as per
SMPV Rules 1981 of CCE and records maintained. Guidelines of
OISD Standard-128 followed for detailed inspection of pressure vessels.

B-03 Annual inspection and testing of safety valves carried out at proper set
pressure and records maintained.

B-04 All instruments, level indicators, pressure and temperature gauges, ROVs
are maintained in working condition following daily scheduled checks,
periodic calibration and preventing maintenance schedule.

B-05 Regular operation checks are carried out on pumps/ compressors


(condition of bearings/ mechanical seal/ abnormal sound etc. as
per OISD STD-119, 120).

B-06 Preventive maintenance and servicing schedules for pumps and


compressors for daily/ weekly/ monthly/ yearly are checked and
records maintained.

B-07 Gas detection system is checked and calibrated periodically. Audio


visual alarm/ security logic system maintained in working condition.

B-08 Fire water system & sprinkler spray system checked/ tested periodically
and maintenance jobs carried out and records maintained.

B-09 LPG bullets/ spheres having fire proofing are periodically checked for cracks,
spalling/ bulging and suspected area are further inspected for presence of corrosion
etc. and corrective steps taken.

B-10 Earthing connections are periodically checked and good electrical contact is maintained.
Records of resistance testing as outlined in OISD Std-137 maintained.

B-11 Foundation/ Anchor bolts, ladders, stairways, platforms/ structurals checked periodically
for any corrosion/damage etc.

B-12 Annual testing of chain pulley blocks and other tool tackles is carried out by certified agency.

B-13 Weigh bridges calibration and certification done once in a year.

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S.No. ITEM DESCRIPTION AUDITORS REMARKS
1 2 3
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C. CYLINDER FILLING

C-01 LPG filling carousel - Drive unit, central column, running rails, etc.
are daily checked, scheduled maintenance (weekly, monthly, quarterly,
annual) are carried out and records maintained.
C-02 Introduction/ Ejection devices and filling machines are checked daily and
scheduled maintenance/ overhaul work carried out.

C-03 Checking of pin travel done regularly and records maintained.

C-04 Check scales are well maintained and calibrations carried out on daily basis
with standard weights.

C-05 Calibration of CVT/DCVT detectors being done regularly and maintenance


schedule followed.
GLOSSARY OF TERMS

1. Area Classification by the bond wire to prevent sparking between


two conducting bodies.
It is method of classifying an area zone wise/
group wise based on the presence of explosive 8. Filling Ratio
gas/ vapour - air mixture vis-a-vis the
requirement of precautions for construction and It is the ratio of weight of LPG in a container to
use of electrical apparatus. the weight of water the same container can hold
at 15 deg. C.
2. Bulk Vessels
9. Fire safe
A pressure vessel used for more than 1000 litres
water capacity for storage or transportation. As applied to valves, it is the concept of
controlling the leakage to an acceptable level
3. Bullet after damage encountered during and after the
fire achieved by dual seating.
A horizontal pressure vessel used for storage or
transportation by rail/ road. 10. Fire proofed

4. Compressed Gas It is a passive concept of explosure protection of


structures, vessel surface or cables that could be
Any permanent gas, liquefiable gas or gas exposed to direct flame impingement, free
dissolved in liquid under pressure or gas mixture burning plus pressure torching conditions, and/
which in a closed container exercises a pressure or prolonged periods of high intensity radiant
either exceeding 2.5 kg/sq.cm. abs @ 15 Deg C heat fluxes by the application of coating with a
or a pressure exceeding 3.0 kg/Sq.cm. abs @ 50 specified rating.
Deg C or both.
11. Flammability
5. Cylinders
It is the percentage of volume of any flammable
A portable container upto 1000 litres water vapour in air-vapour mixtures capable to form
capacity used for both domestic and industrial an explosive mixture.
purposes.
12. Flamable ( or Inflammable)
6. Explosive mixture
Any substance which when tested in a specified
It is a mixture of combustion agent (oxidising manner will ignite when mixed with air on
product-gas, vapour, liquid or solid) and a fuel contact with a flame and will support
(oxidisable product - gas, liquid or solid) in such combustion.
proportions that it could give rise to a very rapid
and lively oxidisation reaction liberating more 13. Gas-Free
energy than is dissipated through conduction
and convection. It means the concentration of flammable or toxic
gases or both in a pressure vessel or pipeline is
7. Earthing & Bonding within the safe limits specified for persons to
enter and carryout hotwork in such vessels/
Earthing is the provision of a safe path of pipelines.
electrical current to ground, in order to protect
structures, plant and equipment from the effects 14. Hot Work
of stray electrical current, and electrostatis
discharge. It is an activity which may produce enough heat
to ignite a flammable air-hydrocarbon mixture
Bonding is the process of connecting the or a flammable substance.
equipment/ system to be earthed to the ground
15. Kerb Wall system by an inert substance, and replacement of
the later by air.
A wall of appropriate height and size
constructed of suitable material and designed to 18. Reid Vapour Pressure
contain the LPG spillage and to direct it to a
safe location around the storage vessel. Reid Vapour Pressure is the vapour pressure in
pounds per square inch (psi) at 100 Deg F as
16. Liquefied Petroleum Gas (LPG) determined by Reid apparatus.

The term applies to a mixture of certain light 19. Spheres


hydrocarbon C2 to C5, derived from petroleum
which are gaseous at ambient temperature and A spherical pressure vessel used for storage.
pressure test may be condensed to a liquid state
at normal ambient temperature by the 20. Tare Weight
application of moderate pressure.
It is the weight of the cylinder together with any
17. Purging fitting permanently attached to them and
includes the weight of valve.
It is the act of replacing the atmosphere within a
container by an inert substance in such a manner 21. Working Pressure
as to prevent the formation of explosive mixture.
It is saturated vapour pressure at 65 Deg. C.
(A) Purging into Service : is the replacement
of air in a closed system by an inert substance 22. Water Capacity
and replacement of the later by combustible gas,
vapour, or liquid. The volume of water in litres that the container
can hold at 15 Deg. C.
(B) Purging out of service : is the replacement
of normal combustible content of a closed

APPENDIX

BIS CODES PERTAINING TO LPG OPERATIONS

--------------------------------------------------------------------------------------------------------------------------------
CODE NO. NAME
--------------------------------------------------------------------------------------------------------------------------------
IS:2-1960 - RULES FOR ROUNDING OFF NUMERICAL VALUES

IS:5-1978 - COLOURS FOR READY MIXED PAINTS & ENAMELS

IS:1196-1978 - CODE OF PRACTICE FOR LAYING BITUMEN MASTIC


FLOORING

IS:1432-1959 - GENERAL REQUIREMENTS FOR WEIGHING


INSTRUMENTS

IS:1435-1991 - PLATFORM WEIGHING MACHINE

IS:1436-1991 - WEIGHBRIDGES

IS:1437-1967 - AUTOMATIC WEIGHING MACHINES

IS:1448(P:70-1968) - RESIDUE IN LPG

IS:1448(P:71-1979) - VAPOUR PRESSURE OF LPG

IS:1448(P:72-1968) - VOLATILITY OF LPG

IS:1448(P:73-1968) - HYDROGEN SULPHIDE IN LPG

IS:1448(P:74-1968) - DRYNESS OF LPG

IS:1448(P:75-1968) - ODOUR OF LPG

IS:1448(P:76-1968) - DENSITY OF LPG

IS:1448(P:111-1983) - ANALYSIS OF LPG AND PROPYLENE


CONCENTRATES BY GAS
CHROMATOGRAPHY

IS:2148-1981 - FLAMEPROOF ENCLOSURES FOR ELECTRICAL


APPRATUS

IS:2206 - FLAME PROOF ELECTRIC LIGHT FITTINGS

IS:2206(PART 1)-1984 - WELL GLASS AND BULKHEAD TYPES

IS:2206(PART 2)-1976 - FITTINGS USING GLASS TUBES

IS:2808-1964 - METHOD FOR COMPUTATION OF CAPACITY TABLES


FOR PRESSURIZED STORAGE TANKS

BIS CODES PERTAINING TO LPG OPERATIONS

--------------------------------------------------------------------------------------------------------------------------------
CODE NO. NAME
--------------------------------------------------------------------------------------------------------------------------------

IS:2825-1969 - CODE FOR UNFIRED PRESSURE VESSELS

IS:2827-1976 - METHODS FOR CALIBRATION OF PRESSURIZED


STORAGE TANKS
IS:3196(PART 1)-1992 - WELDED LOW CARBON STEEL GAS CYLINDER
EXCEEDING 5 LITRE WATER CAPACITY FOR
LOW PRESSURE LIQUEFIABLE GASES CYLINDERS
FOR LPG.

IS:3465-1966 - JOINTING COMPOUND FOR USE IN LPG APPLIANCES


AND INSTALLATIONS

IS:3710-1978 - FILLING RATIOS FOR LOW PRESSURE LIQUEFIABLE


GAS.

IS:4093-1981 - NON-REFILLABLE LPG CONTAINERS

IS:4246-1984 - SPECIFICATION FOR DOMESTIC GAS STOVES FOR


USE WITH LIQUEFIED PETROLEUM GASES

IS:4379-1981 - IDENTIFICATION OF CONTENTS OF INDUSTRIAL GAS


CYLINDERS

IS:4576-1978 - SPECIFICATION FOR LIQUEFIED PETROLEUM GASES

IS:4784-1968 - LOW PRESSURE REGULATORS FOR USE WITH


BUTANE GASES

IS:4785-1968 - LOW PRESSURE REGULATORS FOR USE WITH


PROPANE GAS

IS:4786-1968 - VARIABLE HIGH PRESSURE REGULATORS FOR USE


WITH LPG

IS:4991-1968 - CRITERIA FOR BLAST RESISTANT DESIGN OF


STRUCTURES FOR EXPLOSIONS ABOVE GROUND

IS:5116-1985 - GENERAL REQUIREMENT FOR DOMESTIC AND


COMMERCIAL EQUIPMENT FOR USE WITH
LPG

IS:5571-1979 - GUIDE FOR SELECTION OF ELECTRICAL EQUIPMENT


FOR HAZARDOUS AREAS

IS:5572 - CLASSIFICATION OF HAZARDOUS AREAS (OTHER


THAN MINES) FOR ELECTRICAL
INSTALLATIONS

BIS CODES PERTAINING TO LPG OPERATIONS

--------------------------------------------------------------------------------------------------------------------------------
CODE NO. NAME
--------------------------------------------------------------------------------------------------------------------------------

IS:5572(PART 1)-1978 - AREAS HAVING FLAMMABLE GASES AND VAPOURS

IS:5844-1970 - RECOMMENDATIONS FOR HYDROSTATIC STRETCH


TESTING OF COMPRESSED GAS CYLINDERS

IS:5845-1984 - CODE OF PRACTICE FOR VISUAL INSPECTION OF


LOW PRESSURE WELDED STEEL GAS
CYLINDERS IN USE
IS:5903-1970 - RECOMMENDATIONS FOR SAFETY DEVICES FOR
GAS CYLINDERS

IS:6044 - CODE OF PRACTICE FOR LPG TORAGE


INSTALLATIONS

IS:6044(PART 1)-1971 - COMMERCIAL AND INDUSTRIAL CYLINDER


INSTALLATIONS

IS:6044(PART 2)-1972 - INDUSTRIAL, COMMERCIAL AND DOMESTIC BULK


STORAGE INSTALLATIONS

IS:6539-1972 - INSTRINSICALLY SAFE MAGNETO TELEPHONES FOR


USE IN HAZARDOUS ATMOSPHERES

IS:6665-1972 - CODE OF PRACTICE FOR INDUSTRIAL LIGHTING

IS:7142-1974 - WELDED LOW CARBON STEEL GAS CYLINDER FOR


LOW PRESSURE LIQUEFIABLE GASES, NOT
EXCEEDING 5 LT WATER CAPACITY

IS:7145-1973 - TECHNICAL SUPPLY CONDITION FOR TORQUE


WRENCHES

IS:7241-1981 - GLOSSARY OF TERMS USED IN GAS CYLINDER


TECHNOLOGY

IS:8198(PART 5)-1984 - CODE OF PRACTICE FOR STEEL CYLINDERS FOR


COMPRESSED GASES ; LIQUEFIED
PETROLEUM GAS (LPG)

IS:8374-1977 - SPECIFICATION FOR BITUMEN MASTIC, ANTI STATIC


ELECTRICALLY CONDUCTING GRADE

IS:8451-1984 - CODE OF PRACTICE FOR VISUAL INSPECTION OF


HIGH PRESSURE GAS CYLINDERS

BIS CODES PERTAINING TO LPG OPERATIONS

--------------------------------------------------------------------------------------------------------------------------------
CODE NO. NAME
--------------------------------------------------------------------------------------------------------------------------------
IS:8737 - VALUE FITTINGS FOR USE WITH LPG CYLINDERS OF
MORE THAN 5 LIT. WATER CAPACITY

IS:8737(PART 1)-1979 - VALVE FITTINGS FOR REPLACEMENT PURPOSES

IS:8737(PART 2)-1978 - VALVE FITTINGS FOR NEWLY MANUFACTURED LPG


CYLINDERS

IS:8776-1988 - VALVE FITTINGS FOR USE WITH LIQUEFIED


PETROLEUM GAS (LPG) CYL. UPTO AND
INCLUDING 5 LIT WATER CAPACITY
IS:8790 - GENERAL REQUIREMENTS OF POWERED
INDUSTRIAL TRUCKS WORKING IN
HAZARDOUS AREAS

IS:8790(PART 1)-1978 - INTERNAL COMBUSTION ENGINES POWERED


TRUCKS

IS:8790(PART 2)-1979 - ELECTRIC BATTERY POWERED INDL. TRUCKS

IS:8867-1987 - SATURATED VAPOUR PRESSURE AND TEST


PRESSURE FOR LOW PRESSURE LIQUEFIABLE
GASES CONTAINED IN GAS CYLINDERS

IS:8868-1988 - PERIODICAL INSPECTION INTERVAL OF GAS


CYLINDERS IN USE

IS:9121-1979 - INSPECTION GAUGES FOR CHECKING TYPE 1 (SIZE 2)


TAPER THREADS OF GAS CYLINDER VALVES, TAPER
1 IN 16

IS:9122-1979 - INSPECTION GAUGES FOR CHECKING TYPE 2 TAPER


THREADS OF GAS CYLINDER VALVES, TAPER
3 IN 25

IS:9199-1979 - INSPECTION GAUGES FOR CHECKING TAPER


THREADS OF GAS CYL. VALVES, TAPER 60
DEGREE INCLUDED ANGEL

IS:9200-1979 - METHOD OF DISPOSALS OF UNSERVICEABLE


COMPRESSED GAS CYLINDERS

IS:9281 - ELECTRONIC WEIGHING SYSTEMS

IS:9281(PART 1)-1979 - TERMS AND DEFINITIONS

IS:9281(PART 2)-1979 - METHODS OF MEASUREMENTS


BIS CODES PERTAINING TO LPG OPERATIONS

--------------------------------------------------------------------------------------------------------------------------------
CODE NO. NAME
--------------------------------------------------------------------------------------------------------------------------------

IS:9281(PART 3)-1981 - REQUIREMENTS

IS:9281(PART 4)-1983 - CODE OF PRACTICE FOR USE &


INSTALLATION

IS:9583-1981 - EMERGENCY LIGHTING UNITS

IS:9639-1980 - CODE OF PRACTICE FOR VISUAL INSPECTION


OF LOW PRESSURE WELDED STEEL GAS
CYLINDERS IN USE

IS:9777-1981 - DATA SHEET FOR SELECTION OF


WEIGHBRIDGES FOR BULK
HANDLING EQUIPMENT
IS:9798-1981 - LOW PRESSURE REGULATORS FOR USE WITH
LPG

IS:9902-1982 - RECOMMENDED PRACTICE FOR LEAK


TESTING

IS:9975 - `O' RINGS

IS:9975(PART 1)-1981 - DIMENSIONS

IS:9975(PART 2)-1984 - MATERIAL SELECTION & QUALITY


ACCEPTANCE CRITERIA

IS:9975(PART 3)-1984 - SEAL HOUSING DIMENSIONS AND


TOLERENCES

IS:9975(PART 4)-1984 - TERMINOLOGY AND DEFINITIONS OF TERMS

IS:10733-1983 - ELECTRICALLY BONDED ROAD AND RAIL


TANKER HOSE OF RUBBER,
RESISTANT TO PETROLEUM PRODUCTS

IS:10908-1991 - FLEXIBLE RUBBER TUBING FOR LPG

IS:11498-1985 - LEVER TYPE DIA GAUGES

IS:12936-1990 - CODE FOR BASIC REQUIREMENTS FOR


DELIVERY PERSONS ENGAGED IN
THE DELIVERY OF LPG CYLINDERS

BIS CODES PERTAINING TO LPG OPERATIONS

--------------------------------------------------------------------------------------------------------------------------------
CODE NO. NAME
--------------------------------------------------------------------------------------------------------------------------------
IS:13258-1991 - WELDED LOW CARBON STEEL CYLINDERS
EXCEEDING 5 LT WATER CAPACITY
FOR LOW PRESSURE LIQUEFIED
PETROLEUM GAS CODE OF PRACTICE FOR
INSPECTION AND RECONDITIONING OF
USED LPG CYLINDERS

IS:13432(PART 1)-1992 - GAS LEAK DETECTOR FOR USE WITH LOW


PRESSURE LIQUEFIED PETROLEUM
GAS BURNING APPLIANCES
SPECIFICATION

PART I – MECHANICAL TYPE

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