RLK+01 KAN+requirement+for+Calibration+Laboratory+ (EN)

KAN-R-LK 01
KAN REQUIREMENT ON
IMPLEMENTATION OF
ISO/IEC 17025 FOR CALIBRATION
LABORATORY
Issue Number : 2
January 2008
Komite Akreditasi Nasional

National Accreditation Body of Indonesia
Gedung Manggala Wanabakti, Blok IV, Lt. 4
Jl. Jend. Gatot Subroto, Senayan, Jakarta 10270 – Indonesia
Tel. : 62 21 5747043, 5747044
Fax. : 62 21 57902948, 5747045
Email : laboratorium@bsn.or.id
Website : http://www.bsn.or.id
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KAN-R-LK 01 Issue Number : 2 January 2008
LIST OF AMANDMENT
Part
Part number
No. Date Brief description of changes revision
revised
number
1.
ii

KAN REQUIREMENTS ON IMPLEMENTATION OF ISO/IEC 17025 FOR

CALIBRATION LABORATORY
1. Introduction
1.1. This document is an integral part of KAN laboratory accreditation system based on
the ISO/IEC 17025 : 2005
1.2. This document provides requirements on the specific interpretatio n to the technical
requirements of ISO/IEC 17025 : 2005, those shall be met by KAN accredited
calibration laboratory and used by KAN assessor to assess competence of
calibration laboratories
1.3. KAN has provided general interpretation of ISO/IEC 17025: 2005 i n the KAN Guide
on the Interpretation of ISO/IEC 17025: 2005)
1.4. KAN accreditted laboratories shall meet ISO/IEC 17025: 2005 requirements, and if
applicable KAN Guide on the Interpretation of ISO/IEC 17025: 2005 shall be used
as a reference to implement ISO/ IEC 17025: 2005 in the laboratory
1.5. Implementation of ISO/IEC 17025: 2005 in the calibration laboratories need specific
interpretation, especially for implementation of its technical requirements. This
document provides that specific interpretations to impr ove harmonization,
effectivness and efficiency of calibration laboratory’s management system
2. Scope of Accreditation
2.1. An applicant calibration laboratory shall fill ‘Accreditation Application Checklist

(FPA 03.02b) and Proposed scope of Accreditation Fo rm (Annex of FPA 03.01b
for calibration laboratory), which includes, calibration or measurement fields, type
of item to be calibrated, measurement range, best measurement capabilty, as well
as method and/or specification used by the laboratory to provide i ts calibration
services
2.2. Calibration laboratory accreditation is not restricted only to high level of accuracy.
Accreditation may be granted to the lower accuracy level, provided with larger
BMC, as appropriate with the uncertainty of measurement achieved by the
laboratory in more or less routine calibrations.
2.3. Classification of the scope of KAN accreditation for calibration laboratories is

shown in Annex A of this documents
3. Personnel
3.1. .Laboratories shall equipped with appropriately competence person nel to cover all
calibration included in its accreditation scopes and of sufficient number to cover
volume of calibration works. Personnel responsible for technical operation of the
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laboratory shall have adequate knowledge on the calibration principles (in cluding
evaluation of measurement uncertainty) and having skill to make critical evaluation
of calibration results)
3.2. Competence of laboratory personnel shall be objectively assessed based on their

ability to apply their knowledge in the scope of activities they responsible for,
Education, training and experiences record of personnel in the specific field of
calibration may support their competence. However those records may not enough
to meet competency requirements if objective evidence to apply their know ledge is
not provided.
3.3. Laboratory shall establish scope of competency of each laboratory’s technical

personnel, including authority and responsibility to execute calibration work in its
accreditation scope.
3.4. When, more than one personnel are authorized to execute similar calibration work
of equivalence accuracy, laboratory shall provide objective evidence shows their
ability to achieve an equal accuracy level. If there is no objective evidence showing
an equal competency level of technical personnel, labor atory shall document the
accuracy level that may be achieved by individual laboratory personnel.
4. Accomodation and Environmental Conditions
4.1. Accommodation and environmental conditions needed by the calibration

laboratories will depend on the type of c alibration and/or measurement and BMC
claimed in its scope.
4.2. Accommodation and environmental conditions shall be monitored and controlled in

such way that function and accuracy of all standards and equipment used by the
laboratory is assured. Attention may be given to temperature, temperature
gradient, relative humidity, vibration, dust, cleanliness, electromagetic disturbance,
interferences, lighting and other factors affecting validity of calibration results.
4.3. Limits of environmental condition shall be es tablished by the laboratory based on

requirements of standards, methods, specification, operating conditions of
standards and equipment, and/or other existing information including experimental
data showing the effect of environmental condition to the achi eved measurement
uncertainty. Laboratory shall be able to provide an evidence that the established
limits is achieved in day-to-day operation.
4.4. When on-site calibration is included in management system of the laboratory, it

shall equipped with a mobile or portable environmental monitoring system needed
to monitor an environmental paramater that may be affect the on -site work.
4.5. When environmental condition significantly affect validity of calibration results in

such way that contributes significantly to mea surement uncertainty, that condition
shall be monitored and recorded continuously.
4
4.6. When correction caused by environmental conditions is applied to calibration

results, those original and corrected measurement data shall be recorded.
5. Measurement Uncertainty
5.1. Procedure for evaluation of measurement uncertainty shall be based on KAN

Guide on the Evaluation and Expression of Uncertainty and/or other equivalent
documents based on the ISO Guide to the Expression of Uncertainty in
Measurement.
5.2. Calibration laboratory shall have documented procedure for the evaluation of
uncertainty covering important stages in the evaluation of measurement
uncertainty and the estimate of contribution summarizing in the uncertainty budget.
(guidance is given in the Annex C o f this document.
6. Best Measurement Capability (BMC)
6.1. Best measurement Capability is simply defined as smallest uncertainty that the
laboratory can achieve in more or less routine calibration of nearly ideal devices
that can be calibrated aginst labora tory’s calibration system, which is stated as
expanded uncertainty at 95% in the scope of accreditation.
6.2. Best Measurement Capability should be routinely achieved by the laboratory when
calibrates unit under test having equivalent characteristic with those used as the
basis of their claimed BMC
6.3. In the framework of KAN calibration laboratory accreditation system, the claimed
BMC shall be supported by an appropriate uncertainty budget and experimental
evidence showing that the laboratory is capable to achiev e their BMCs
7. Measurement Standards and Measuring Equipments

7.1. All measurement standards and equipments including ancilliary equipments used
by the laboratory shall meet requirements of the calibration method claimed by the
laboratory and shall support their claimed BMC
7.2. Measurement standards and/or measuring instruments shall be only used by as

the reference standards when the laboratory has procedures needed to verified
their accuracy, including their long term variability. If applicable, laboratory s hall
have a documented procedure for the verification of their measurement standards
and/or measuring instruments
7.3. Note: procedures and records of the verification of standard’s accuracy may
be integrated with the internal quality control system of the lab oratory
5
7.4. Laboratory shall have a list of all measurement standards, measuring equipments,
including any ancilliary equipment needed for all calibration in its scope, as well as
establishing the functions as a reference standards, working standards,
comparators, calibration media, ancilliary equipement (e.g measuring instruments
for environmental condition, etc)
7.5. Laboratory shall establih acceptance criteria of each measurement standards and
equipments and shall ensure that all of them meet that established acceptance
criteria. Record of verification againts acceptance criteria shall be documented.
7.6. Calibration of measurement standards and equipments is not the only

responsibility of calibration laboratory, to ensure their compliance with the
established acceptance criteria, the laboratory shall appropriately choose, install,
maintain, check, operate and store them.
7.7. When measurement standards and measuring equipments those significantly

affect the calibration results is used outside of laboratory’s permanent facility
(including when they are sent for calibration), the laboratory shall appropriately
checks their performance immediately before and after sent them out of
permanent facility to ensure that their performance is not significantly changed as
such affect their ability to achieve the claimed BMC.
7.8. All measurement standards and measuring equipment shall be labelled, coded or
otherwise identified to indicate their calibration status, i.e. the date of last
calibration and the next calibration date. Any lim itation of calibration or restriction
of use shall be clearly indicated on the equipment.
7.9. When neither labelling nor coding is practicable, or is not considered essential for
control purposes, other procedures shall be established to ensure conformance to
these requirements
7.10. Access to adjustable devices on measurement standards and measuring

equipment, which are fixed at the time of calibration, shall be sealed or otherwise
safeguarded to prevent tampering by unauthorised personnel. Seals shall be
designed so that tampering will destroy them.
NOTE: This requirement does not apply to adjustable devices that are intended to
be set by the user without needing external references.
8. Measurement Traceability
8.1. All quantitative measuring equipments and measure ment standards having
significant effect to calibration results shall be calibrated before used by the
laboratory.
8.2. Measuring equipments and measurement standards shall be calibrated with an

appropriate interval based on its stability, its intended use, en vironment, and
frequency of use.
6
8.3. Calibration interval for each equipments and standards shall provide confidence
that specification limits defined by the laboratory is not breached between its
subsequent calibrations.
8.4. Calibration interval should not exce ed maximum recommended interval in the
Annex B of this document.
8.5. Laboratory may establish longer calibration interval if objective evidence provided
that extension of calibration interval will not affect its capability to achieve claimed
BMC
8.6. Extension of calibration interval shall only be done based on the evaluation of at
least 3 (three) subsequent calibration certificates, or based on IQC records having
more than 50 (fifty) QC periodic measurements.
8.7. Laboratory shall established shorter calibration int erval If evaluation on previous
calibration certificates and/or IQC records show that drift or instability of standards
and equipments between periodic calibration are not support its claimed BMC
8.8. Change of calibration interval shall be an integral part of laboratory’s quality

management system and a planned action based on provision of objective
evidence that is not adversely affect laboratory performance.
8.9. Change of calibration interval will affect an estimate compensation for drift or
stability of standards and equipments those may affect BMC granted in its scope
of accreditation.
8.10. Calibration laboratories shall fulfill KAN Policy on Traceability of Measurement
9. Computerized Calibration System

9.1. The equipment shall be satisfactory for its intended p urpose. The adequacy of the
equipment will be determined by the accuracy and speed of making the reading
9.2. The system shall be satisfactory calibrated. If the measuring equipment cannot be
isolated from the data processing system, the system as a whole shal l be
calibrated either statically or dynamically. If the measuring equipment can be
isolated from the data processing system, the equipment can be calibrated in the
conventional manner and a separate verification of the data processing system
can be undertaken.
9.3. The data processing system shall allow for the detection of errors in data input
and the monitoring of the progress of the calibration.
9.4. data processing system shall maintain the original integrity of the measured data.
The limiting factor on the pr ecision of the numbers which the data processing
system can handle must be taken into account.
.
7
9.5. The system shall be capable of being checked for error -free operation with
respect to data capture, data processing and freedom from sources of external
interference. This check shall be determined by manual check or by a set of
artefact data, etc
10. Assuring Quality of Calibration Results

10.1. Laboratory shall implement internal quality control system and have external
quality control program through participatio n in relevant proficiency testing
activites. The type of Proficiency Testing Programme those may be accepted
within KAN accreditation system for calibration laboratory are proficiency testing
schemes in accordance with ISO Guide 43, bilateral proficiency t esting, and/or
other interlaboratory comparisons program designed for other purposes.
10.2. Laboratory’s internal quality control system shall be designed in such way that
short term and long term random variability and bias of the measurement system,
measurement standards, and all relevant resources will be monitored continuously
to assure validity of calibration results
10.3. Quality control data may be analyzed using a relevant control chart, or other
statistical analysis based on measurement data from calibration of reference
standards, calibration of working standards and supporting equipment,
intermediate check, calibration of customer items or other sources of data as
relevant with type and volume of laboratory acitivities
10.4. Degree of rigour of laboratory’s qual ity control system will depend on their
claimend BMC. Smaller claimed BMC will need more rigorous quality control,
while larger claimed BMC may need the only simple quality control system
10.5. To implement quality control programme, laboratory may refer to KAN Guide on
Measurement Assurance
10.6. Applicant laboratory shall, at least participates 1 (one) proficiency testing

programme for 1 (one) of calibration fields covered in the proposed scope of
accreditation.
10.7. Calibration laboratory shall establish a program fo r its participation in proficiency

testing to ensure that each calibration field is verified by 1 (one) proficiency testing
activities per 4 (four) years.
10.8. Accredited calibration laboratories were obliged to participate in Proficiency

Testing Activities and/or Measurement Audit conducted by KAN for their relevant
scope of accreditation
10.9. Laboratory may arrange a bilateral calibration proficiency testing and/or other
interlaboratory comparison programmes with the other accredited calibration
laboratories having similar scope of accreditation and submit the results of those
program to KAN secretariat as an evidence for their participation in proficiency
testing programmes
8
10.10. In case of bilateral interlaboratory comparison, laboratory should chose the other
laboratory that has been participated in national/regional/international
interlaboratory comparison programmes and having smaller BMC than their own
claimed BMC
10.11. Laboratory shall follow-up any outliers results in proficiency testing in accordance
with KAN Policy on Proficiency Testing Activity
9
ANNEX A
Classification of Accreditation Scope for Calibration Laboratory
Calibration fields Instruments to be calibrated
1. Temperature 1.1 Liquid-in glass thermomter
1.2. Temperature sensor with display unit :

1.2.1 thermocouple sensor with display unit
1.2.2 resistance thermometer sensor with display
unit
1.3. Temperature Indicator (without sensor) :

1.3.1 for thermocouple sensor
1.3.2 for Resistance thermometer sensor
1.4. Resistance thermometer sensor
1.5. Themocouple sensor

1.5.1 T – type
1.5.2 J - type
1.5.3 E – type
1.5.4 K – type
1.5.5 S and R - type
1.5.6 B - type
1. Temperature 1.6. Radiation thermometer

(cont’d) 1.6.1 Infrared photodetector
1.6.2 Visible-light photodetector
1.7. Optical pyrometer 1 diminishing filament pyrometer
1.8. Hygrometer, hygrograph
1.9. Thermohygrometer, Thermohygrograph
1.10. Temperature enclosure

1.10.1 Oven
1.10.2 Furnace
1.10.3 Bath
1.10.4 Incubator
1.10.5 Refrigerator
1.11. Humidity Chamber
2. Mass 2.1 Conventional Mass (mass standards, weights)
10
2.2 Balances
1.2.1 Electronic Balance
1.2.2 Mechanical Balance
1.2.3 Equal Arm Balance
1.2.4 Batching Plant
3. Volumetric 3.1 Volumetric proving measures

3.2 Volumetric glassware (buret / pipet / labu ukur /
etc)
4. Pressure
4.1 Dead Weight Tester (DWT – Pressure Balance)
4.2 Pressure Test Gauge (used for calibration fo r
pressure gauge)
4.3 Pressure Gauge
4.4 Electromechanical manometer (indicated pressure
transducer, pressure transmitter, digital
manometer)
4.5. Vacuum gauge (gauge or absolute indication)
4.6 Barometer
5. Force 5.1 Load cell

5.2 Tension force testing machines
5.3 Compression force tersting machines
5.4 Universal force testing machine
5.5 Hydraulic Jack
5.6 Force gauge / proving ring
5.7 Impact Testing Machine
6. Torque 6.1 Torque meter
7. Hardness 7.1 Hardness testing machines
8. Flow 8.1 Flowmeter
9. Length 9.1 Length standards

9.1.1 Gauge blok / end gauge / slip gauge
9.1.2 Step gauge - Vernier caliper cheker, inside
checker, chek master.
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9.2 Micrometer
9.2.1 Outside micrometer
9.2.2 Inside micrometer
9.2.3 Micrometer head
9.2.4 3-point inside micrometer
9.2.5 Depth micrometer
9.2.6 indicating micrometer
9.2.7 Mikrometer roda gigi
9.3 Calliper
9.3.1 Vernier caliper
9.3.2 Height gauge
9.3.3 Depth caliper
9.4 Dial Gauge

9.4.1 Dial indicator
9.4.2 Mechanic dial comparator
9.4.3 Electronic dial comparator
9.4.4 Dial Test indikator
9.4.5 Linear scale / LVDT
9.4.6 Bore gauge
9.5 Gauges
9.5.1 Feeler gauge
9.5.2 Pin gauge
9.5.3 Straight edge
9.5.4 Plug gauge
9.5.5 Ring gauge
9.6 Angle measuring devices

9.6.1 Bevel Protactor
9.6.2 Waterpass / Spirit level / bubble / clinometer
9.6.3 Theodolite
9.6.4 Telescope
9.6.5 Square
9.6.6 Sine bar
9.7 Meeasuring Machine

9.7.1 Profile projector
9.7.2 Roughness meter
9.7.3 Coordinate Measuring Machine
9.7.4 Microskop
9.7.5 Roundnessmeter
9.7.7 Dial gauge tester
9.7.8 Digital mu checker
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9. Length (Cont’d) 9.8.Miscellaneous

9.8.1Thickness gauge
9.8.2 Surface plate
9.8.3 Height master
9.8.4 Electronic distance meter
9.8.5 Walking measurer
9.8.6 Planimeter
9.8.7 Tape measure
9.8.8 Steel ruler
9.8.9 V-blok
10. Electrical 10.1 . Current

10.1.1 AC/DC Current source
10.1.2 AC/DC Ampere meter
10.1.3 AC/DC current recorder
10.1.4 Current transducer
10.2. Voltage
10.2.1 AC/DC Voltage source
10.2.2 AC/DC Voltmeter
10.2.3 AC/DC voltage recorder
10.2.4 AC/DC voltage devider)
10.2.5 AC/DC voltage transducer
10.3. Resistance
10.3.1 Resistor
10.3.2 Decade resistor
10.3.3 Hammond resistor
10.3.4 Current shunt
10.3.5 Ohmmeter
10.3.6 Resistance bridge
10.4. Capacitance
10.4.1 Capasitor
10.4.2 Decade capacitor
10.4.3 Capacitance bridge
10.4.4 Capacitance meter
10.5. Inductance
10.5.1 lnductor
10.5.2 Decade capacitor
10.5.3 Inductance bridge
10.5.4 Inductance meter
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10.6. Electric Power and Phase
10.6.1 Power meter
10.6.2 Cos  meter
10.6.3 Energy meter
10.6.4 Power transducer
11. Time and 11.1 Time

Frequency 11.1.1 Stopwatch
11.1.2 Tirner
11.2. Frequency
11.2.1 Frequency standard
11.2.1.1 Rubidium frequency standard
11.2.1.2 X'tal frequency standard
11.2.2 Counter
11.2.2.1 Frequency counter
11.2.2.2 Frequency meter
11.2.2.3 Microwave frequency counter
11.2.2.4 Universal time counter
11.2.3 Frequency converter
11.2.4 Down converter
11.2.5 RPM converter
11.2.5.1 Optical
11.2.5.2 Electromagnetic
11.2.5.3 Mechanical
11.3. AF & RF signal

11.3.1 AF signal
11.3.1.1 AF oscillator
11.3.1.2 Function generator
11.3.1.3 Pulse generator
11.3.2 RF Signal
11.3.2.1 Synthesized signal generator
11.3.2.2 Synthesized sweeper
11.3.2.3 AM / FM signal generator
11.4. RF Power & Attenuation

11.4.1 RF Power meter
11.4.2 RF attenuator
11.4.3 Power divider / coupler
11.4.4 RF Amplifier
14
11.5 AF / RF Analyzer
11.5.1 Analyzer
11.5.1.1 Distortion analyzer / distortion
meter
11.5.1.2 Modulation analyzer / modulation
meter
11.5.1.3 Spectrum analyzer
11.5.1,4 Impedance analyzer
11.5.1.5 Audio analyzer
11.5.1.6 Network analyzer
11.5.2 Osiloskop
11.5.2.1 Oscilloscope
11.5.2.2 Digitizing oscilloscope
11.5.2.3 Storage oscilloscope
11.5.2.4 Plug-in-type oscilloscope
11.5.3 Measuring receiver / signal analyzer
11.5.4 Other measuring equipment
12. Accoustics and 12.1 Accoustics
Vibration
12. 1.1 Sound level meter
12. 1.2 Microphone
12.2 Vibration
12.2.1 Accelerometer
12.2.2 Displacement
12.2.3 Vibratiometer / Vibrometer
13. Analytical 13.1 Spectro-photometry

Instruments
13.1.1 UV - Vis Spectrophotometer
13.2 Chemical testing Instruments

13.2.1 PH meter
13.2.2 Viscometer
14. Optical 14.1 Optical Power Meter

14.2 Optical Time Domain Reflectometer
14.3 Optical Light Source
14.4 Optical Attenuator
15
Appendix B
Recommended Calibration Interval
The following table sets out nominal maximum periods between successive
calibrations for a number of reference standards and measuring instruments. It
must be stressed that these periods are generally considered to be the maximum
appropriate in each case providing that the other criteria as specified below are met:
 That the equipment is of good quality and proven adequate stability, and
 That the laboratory has both the equipment capability and staff expertise to
perform adequate intermediate checks, and
 That if any suspicion or indication of overloading or mishandling arises the

equipment will be checked immediately and thereafter at fairly frequent
intervals until it can be shown that stability has not been impaired.
 Where the above criteria cannot be met appropriately, shorter intervals shall
be specified.
The list of standards and measuring instruments is by no means exhaustive, and

will be updated periodically.
No Type of instruments Maximum calibration intervals

Temperature
1 Calibration bath and Furnace Initial spatial and temporal surveys should
be carried out
Check temperature distribution at one
temperature every five years
2 Thermocouple
Rare metal, reference for 100 hours use or three years
use below 1000 0 C
Rare metal,reference for u se 10 hours use or three years
above 1000 0C
Rare metal, working 100 hours use or three years
standard
Base metal, working Calibration interval to suit particular
standard application
16

3 Thermometer:
Liquid in glass (reference Check ice point or other suitable reference
thermometer) point each time of use or at interval of one
to two months, whichever is the sooner
until the secular change is less than half
the uncertainty of calibration. Then check
every six months. Recalibrate every five
years when reference point changes by five
or more scale divisions
Liquid in glass (working Compare working thermometer with
thermometer) reference thermometer at two points in the
working range every six months.
Recalibrate every five years or when a
change of five or more scale division is
noted
Resistance – temperature Check ice point before use or at least every
thermometer six months Recalibrate every five years or
when ice point change by more than the
equivalent of five times the uncertainty of
calibration
4 Psychrometers Check thermometer ice point every six
months. Calibrate thermometers every five
years or when ice point changes by more
than five scale divisions
5 Pyrometers 1 year
6 Strip lamps 100 hours use or five years
7 Hygrometer 1 year
Mass and Related Quantities

1 Mass standards
Reference standards 3 years
Working standards 1 year
2 Balances
Electronic, mechanic 1 year
With monthly single point check at full
scale
Mass comparator Repeatability check every 6 months
3 Dead Weight Tester
(Pressure Balance)
Accuracy < 0.01% 3 years, with spin-rate examination anually
Accuracy > 0.01% 5 years, with spin-rate examination anually
4 Pressure Test Gauge for 1 year
calibrating pressure gauge
17

6 Manometer :
Reference std (liquid) 10 years, with checking the cleanliness of
the fluid every 36 months
Working std (liquid) 5 years, with checking the cleanliness of
fluid every 36 months
Electronic 1 year
7 Barometer:
Fortin Initial, with one point check using transfer
instrument every 5 years
Aneroid 1 year
8 Load Cell 2 years
9 Torque:
Standard – beam and 4 years than 8 years subsequent
masses
Transducer 1 years
10 Force Testing Machine:

Dead Weight 5 year
Elastic Dynamometer 2 year
Hydraulic, Pneumatic 2 year
11 Hydrometer:
Reference 5 years
Working - glass Check against reference hydrometer or in
newly prepared solutions of known density
every 1 year
Working - metal Check against reference hydrometer or in
newly prepared solutions of known de nsity
every 6 months
12 Density Bottles 2 years then 5 years subsequent
13 Volumetric Glassware initial
14 Orifice Plates Initial, with visual check for wear and
damage every 6 months
Length, Angle and Dimensional

1 Gauge Block:
Reference standard 3 years
Working standard 1 year
2 Angle Gauge:
Working standard 2 years
3 Comparator 3 years
18

4 Height setting micrometer 3 years with annual performance checks
and Riser Blocks
5 Setting rings and plugs:

Working standard 1 year
6 Autocollimator 6 years
7 Dividing Head and Rotary 5 years
Tables
8 Callipers 2 years
9 Dial Gauges 2 years
10 Alignment Telescopes 6 years
11 Surface plates:
Cast iron 1 years
Granite 3 years
12 Measuring Machine (Other
than CMC):
Precision scale 10 years
Geometric Test 5 years
Micrometer Heads 3 years
13 Optical flats/parallels Three years
14 Linear transducer 1 year, with performance check before use
15 Micrometers 5 years, with annual zero, one point check

(against gauge block) and condition of anvil
16 Length bar:
Reference 4 years
Working 2 years
17 Precision Level 4 years
18 Precision Linear scale 5 years
19 Micrometer setting gauge 3 years
20 Optical projectors 5 years
21 Pitch Diameter reference 4 years
disc
22 Precision Polygon 5 years
23 Rollers and Balls 4 years
24 Roundness standard 5 years
25 Roughness standards:
Metal 4 years, with annnual microscopic
inspection
Glass Initial, with annual microscopic inspe ction
26 Screw check for ring gauge 3 years
19

27 Screw pitch reference 3 years
standard
28 Screw thread measurement Initial, with annual visual inspection
cylinder and vee pieces
29 Setting cylinder 3 years
30 Sine bars, centres and 3 years
tables
31 Squareness testers 3 years
32 Squares:
Try squares 2 years
Block squares 4 years
Steel / cast iron Straight 3 years
Edges
Granites 4 years
33 Tape measures, Rules:
Tape measures Initial, wiht check at maximum length
every 2 to 5 months dpendi ng on use and
accuracy required
Steel rules Initial, wiht check at maximum length
every 2 to 5 months dpending on use and
accuracy required
Electrical
1 Electronic standard cells 1 year
2 Digital meters 1 year, compare every sixth month
3 Analog meters 2 years, compare every sixth months
4 Resistors 3 years, compare anually
5 Capacitor 3 years, compare anually
6 Standard cell, Weston 2 years, compare at least sixt monthly
7 AC-DC Transfer standards 2 years, compare immediately after
calibration
8 Bridges 3 years (full calibration), check against
laboratory standard anually
9 Potentiometer 3 years, compare anually
Time and Frequency

1 Signal Generator 1 year
2 Attenuator 3 years (frequency response)
resistance check anually where appropriate
3 RF Power Meter 1 year
4 Stop watches, clock 1 year
20

Photometry
1 Luminous intensity lamps 1 year
2 Luminous flux lamps 1 year
3 Illuminance (lux) meter 1 year
4 Luminance meter 1 year
Radiometry
1 Spectral irradiance lamps 100 hours burning time or three years,
whichever is earlier
2 UV irradiance meters 6 months (heavy usage)
1 year (light usage)
3 Laser/optical power meter 1 year
4 Fibre optic power meter 1 year
5 Laser wavelength (fiber 1 year
optic)
Spectrophotometry
1 Wavelength standard filters 1 year
2 Transmittance standard 1 year
filters
3 Reflectance standards 1 year
21
ANNEX C (Indonesian Only)

Guide on writing procedure for the evaluation of
Uncertainty in Measurement for Calibration Laboratories
Evaluasi ketidakpastian pengukuran merupakan bagian dari kegiatan kalibrasi atau

pengukuran. Sebagaimana halnya dengan metode kalibrasi/pengujian yang harus
diuraikan dalam dokumen instruksi kerja, begitu pula metode atau prosedur evaluasi
ketidakpastian harus diuraikan dalam sua tu dokumen instruksi kerja evaluasi
ketidakpastian pengukuran. Instruksi kerja tersebut harus dibuat agar jelas dan mudah
dipahami, sehingga dapat diterapkan tanpa keraguan oleh operator kalibrasi dan dapat
diverifikasi oleh asesor dengan mudah. Untuk dapa t membuat instruksi kerja yang efektif
itulah perlu diperhatikan beberapa langkah yang diuraikan dalam pedoman ini.
Untuk memudahkan verifikasi instruksi kerja, sebaiknya instruksi kerja tersebut disajikan
dengan format yang terdiri atas:
1) mathematical model
2) uncertainty equation,
3) description of uncertainty sources, and
4) uncertainty budget table.
Komponen-komponen ini akan diuraikan dalam bagian berikut:
Model Matematis
Model matematis menyatakan hubungan matematis antara measurand (besaran ya ng
diukur) dengan besaran-besaran yang mempengaruhi. Jika suatu besaran dianggap
mempengaruhi hasil pengukuran, maka variabel yang melambangkan besaran tersebut
harus ada dalam model matematis. Sebaliknya, jika suatu besaran dianggap tidak
berpengaruh, maka tidak perlu ada variabel yang mewakilinya dalam model matematis.
Model matematis dapat dimodifikasi dengan penye derhanaan atau pendekatan yang
logis untuk mempermudah evaluasinya.
Persamaan Ketidakpastian
Persamaan ketidakpastian pada dasarnya adalah e laborasi dari rumus ketidakpastian
baku gabungan (ISO GUM):
uc2 = ∑ (ci2·ui2) = c12·u12 + c22·u22 + c32·u32 + … [1]
Untuk setiap variabel x i dalam model matematis, akan ada komponen ketidakpastian
baku ui dan koefisien sensitivitas c i. Perlu diperhatikan bahwa nilai (atau rumus) koefisien
sensitivitas sangat bergantung pada bentuk persamaan dalam model matematis, karena
itulah penentuan model matematis harus tepat dan jelas.
Deskripsi Sumber-Sumber Ketidakpastian

Persamaan ketidakpastian akan mempunyai dua macam komponen: komponen
ketidakpastian (u i) dan komponen konstanta (c i). Kedua macam komponen ini nilainya
harus ditentukan; baik dengan diestimasi maupun diturunkan dari data lain. Untuk itu
perlu ada uraian yang jelas mengenai cara menentukan nilai -nilai ini. Uraian ini meliputi:
 cara menentukan atau mengestimasi ketidakpastian terentang (expanded
uncertainty) setiap sumber ketidakpastian;
22
 jenis distribusi dan faktor pembagi yang sesuai;

 penentuan nilai konstanta yang menjadi faktor dalam koefisien sensitivitas
Tanpa adanya suatu uraian yang jelas, budget ketidakpastian menjadi sulit diverifikasi,
bahkan bisa dikatakan meaningless (tidak berarti).
Tabel Anggaran Ketidakpastian

Tabel budget ketidakpastian berisi nilai -nilai ketidakpastian dari tiap -tiap sumber
ketidakpastian beserta variabel -variabel lainnya (faktor pembagi, koefisien sensitivitas,
derajat kebebasan). Budget ketidakpastian dibuat dalam format yang sedemikian rupa
untuk memudahkan penghitungan ketidakpastian baku tiap -tiap sumber, ketidakpastian
baku gabungan, derajat kebebasan efektif dan faktor cakupan (jika diperlukan) serta nilai
ketidakpastian terentang (expanded uncertainty). Bentuk ini sangat sesuai untuk
digunakan dalam program spreadsheet sehingga penghitungan secara otomatis dapat
dilakukan dengan mudah.
Catantan: Notasi Ketidakpastian Baku dan Ketidakpastian Bentangan

To avoid misunderstanding, notation for the standard uncertainty and expanded
uncertainty shall be considered:
 standard uncertainty is stated as u (non -capital letter)
 expanded uncertainty is stated as U (capita l letter)
 standard uncertainty of variable Xi is stated as u(Xi).
Formula Baku dan Konsep Dasar

Rumus-rumus baku serta konsep-konsep dasar dari ISO GUM tidak perlu dicantumkan
lagi dalam instruksi kerja, karena diasumsikan bahwa pengguna instruksi kerja sudah
memahami konsep-konsep dasar ISO GUM. Rumus -rumus yang bisa dianggap baku
misalnya rumus rerata, simpangan baku, ketidakpastian gabungan, derajat kebebasan
efektif (rumus Welch-Satterthwaite).
Example : Kalibrasi Gauge Block dengan Metode Pembandin gan Mekanik
Model matematis
Model dasar yang meliputi besaran -besaran yang utama atau dominan diturunkan
sebagai berikut:
L = Ls + d [2]
dengan: L = panjang balok tes
Ls = panjang balok acuan
d = penunjukan komparator
Untuk memperhitungkan pengaruh besaran-besaran lain yang berpengaruh, model
tersebut dielaborasi menjadi sebagai berikut:
L(1 + ·) = Ls(1 + s·s) + d + L drift [3]
dengan:  = koefisien muai panjang balok tes
 = suhu balok tes
s = koefisien muai panjang balok acuan
s = suhu balok acuan
23
Ldrift = perubahan panjang balok acuan akibat drift

Dengan manipulasi matematis [ISO GUM H.1], persamaan [ 3] dapat disederhanakan
untuk mempermudah evaluasi ketidakpastian, men jadi seperti berikut:
L = Ls + Ls(·s + ·s) + d + L drift [4]
dengan:  = selisih antara koefisien muai panjang balok tes dan balok acuan
 = selisih antara suhu balok tes dan balok acuan
Persamaan [4] selanjutnya akan dipakai sebagai model matematis untuk kalibrasi gauge
block dengan metode perbandingan.
Persamaan ketidakpastian
Setelah menurunkan koefisien sensitivitas untuk tiap -tiap komponen ketidakpastian,
maka persamaan ketidakpastian u ntuk kalibrasi gauge block dengan metode
perbandingan dapat diturunkan dari Persamaan [ 4] sebagai berikut:
u2(L) = u2(Ls) + (·s + ·s)2·u2(Ls) + Ls2·s2·u2() + Ls2·s2·u2() + Ls2·2·u2(s) +
Ls2·2·u2(s) + u2(d) + u 2(Ldrift) [5]
Karena  dan  masing-masing mempunyai nilai taksiran nol, maka Persamaan [ 5]
dapat dipersingkat menjadi
u2(L) = u2(Ls) + Ls2·s2·u2() + Ls2·s2·u2() + u2(d) + u 2(Ldrift) [6]
Persamaan [6] merupakan persamaan ketidakpastian kalibrasi gauge block metode
perbandingan.
Deskripsi Sumber-Sumber Ketidakpastian

Persamaan [6] mempunyai beberapa input ketidakpastian yaitu u(L s), u(), u(), u(d),
u(Ldrift); serta beberapa konstanta yaitu L s, s, s.
Tiap-tiap input ketidakpastian mempunyai sumber -sumber ketidakpastian yang diuraikan
dalam tabel berikut, berikut cara m engevaluasi nilai dan distribusinya.
Tabel 1. Deskripsi Sumber -Sumber Ketidakpastian

Input/ Deskripsi Sumber Penentuan nilai ketidakpastian
variabel ketidakpastian terentang dan pembaginya
u(Ls) Ketidakpastian 1. Kalibrasi balok 1. Dari sertifikat kalibrasi, dibagi k
nilai balok acuan acuan
u(d) Ketidakpastian 1. Daya baca 1. Setengah dari resolusi komparator,
penunjukan atau 2. Repeatability dibagi √3
pembacaan 3. Kalibrasi komparator 2. Simpangan baku, dibagi √n
komparator 3. Dari sertifikat kalibrasi, dibagi k
u(Ldrift) Ketidakpastian 1. Estimasi nilai drift 1. Nilai maximum permissible secular
drift balok acuan change (ISO3650) (dianggap sebaran
persegi), dibagi √3
* kecuali ada acuan lain
u() Ketidakpastian 1. Estimasi nilai selisih 1. Jika kedua balok dari bahan yang sama,
selisih koefisien sepersepuluh dari nilai  nominal (mis.
muai kedua  = 11,5e-6 °C–1 untuk baja) (dianggap
balok sebaran persegi), dibagi √3
u() Ketidakpastian 1. Estimasi nilai selisih 1. Jika kedua balok telah dikondisikan
selisih suhu cukup lama dalam suhu lab, 0,05 °C
kedua balok (dianggap sebaran persegi), dibagi √3
24
The values of constants used in the uncertainty equation may be eva luated as follows:
Tabel 2. Deskripsi Konstanta yang Digunakan

Konstanta Deskripsi Penentuan nilai konstanta
Ls Panjang balok acuan Untuk tiap rentang ukur, ambil nilai yang terbesar (mis.
untuk rentang 0~1 mm, maka L = 1 mm atau 1000 µm)
s Koefisien muai balok Estimasi berdasarkan bahan balok, atau informasi dari
acuan pembuat. Mis. untuk baja,  = 11,5 e-6 °C-1
s Deviasi suhu balok Selisih antara suhu balok acuan dengan 20 °C. Mis. jika
acuan suhu = 20,1 °C, maka s = 0,1 °C.
Tabel Anggaran Ketidakpastian
Uncertainty sources Unit Distribution Symbol Expanded Cov.erage Degrees of Standard. Sensitivity ci.ui (ci.ui)2 (ci.ui)4/vi
uncertainty Factor freedom Uncertainty Coefficiients
(U) (k) (vi) (ui) (ci)
1 Reference block µm Normal u(Ls)

value
2 Readability of µm Rect u(d1)
instrument
3 Repeatability of µm Rect u(d2)
measurement
4 Instrument µm Normal u(d3)
correction
5 Reference block µm Rect u(Ldrift)
drift
6 Difference /°C Rect u()
between α and
αs
7 Temperature °C Rect u()
gradient
between blocks
Sums
Combined
uncert, uc
Eff. Deg of
freedom, v eff
Cov. Factor for
95% CL
Expanded
uncertainty,
U95
25

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KAN REQUIREMENTS ON IMPLEMENTATION OF ISO/IEC 17025 FOR

2.1. An applicant calibration laboratory shall fill ‘Accreditation Application Checklist

2.3. Classification of the scope of KAN accreditation for calibration laboratories is

3.2. Competence of laboratory personnel shall be objectively assessed based on their

3.3. Laboratory shall establish scope of competency of each laboratory’s technical

4. Accomodation and Environmental Conditions

4.1. Accommodation and environmental conditions needed by the calibration

4.2. Accommodation and environmental conditions shall be monitored and controlled in

4.3. Limits of environmental condition shall be es tablished by the laboratory based on

4.4. When on-site calibration is included in management system of the laboratory, it

4.5. When environmental condition significantly affect validity of calibration results in

4.6. When correction caused by environmental conditions is applied to calibration

5.1. Procedure for evaluation of measurement uncertainty shall be based on KAN

6. Best Measurement Capability (BMC)

7. Measurement Standards and Measuring Equipments

7.2. Measurement standards and/or measuring instruments shall be only used by as

7.6. Calibration of measurement standards and equipments is not the only

7.7. When measurement standards and measuring equipments those significantly

7.10. Access to adjustable devices on measurement standards and measuring

8.2. Measuring equipments and measurement standards shall be calibrated with an

8.8. Change of calibration interval shall be an integral part of laboratory’s quality

8.10. Calibration laboratories shall fulfill KAN Policy on Traceability of Measurement

9. Computerized Calibration System

10. Assuring Quality of Calibration Results

10.6. Applicant laboratory shall, at least participates 1 (one) proficiency testing

10.7. Calibration laboratory shall establish a program fo r its participation in proficiency

10.8. Accredited calibration laboratories were obliged to participate in Proficiency

Classification of Accreditation Scope for Calibration Laboratory

Calibration fields Instruments to be calibrated

1. Temperature 1.1 Liquid-in glass thermomter

1.2. Temperature sensor with display unit :

1.3. Temperature Indicator (without sensor) :

1.4. Resistance thermometer sensor

1.5. Themocouple sensor

1. Temperature 1.6. Radiation thermometer

1.7. Optical pyrometer 1 diminishing filament pyrometer

1.8. Hygrometer, hygrograph

1.9. Thermohygrometer, Thermohygrograph

1.10. Temperature enclosure

1.11. Humidity Chamber

2. Mass 2.1 Conventional Mass (mass standards, weights)

Calibration fields Instruments to be calibrated

3. Volumetric 3.1 Volumetric proving measures

5. Force 5.1 Load cell

6. Torque 6.1 Torque meter

7. Hardness 7.1 Hardness testing machines

8. Flow 8.1 Flowmeter

9. Length 9.1 Length standards

Calibration fields Instruments to be calibrated

9.4 Dial Gauge

9.6 Angle measuring devices

9.7 Meeasuring Machine

Calibration fields Instruments to be calibrated

9. Length (Cont’d) 9.8.Miscellaneous

10. Electrical 10.1 . Current

Calibration fields Instruments to be calibrated

11. Time and 11.1 Time

11.3. AF & RF signal

11.4. RF Power & Attenuation