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CERTIFICATE OF CALIBRATION

ISSUED BY Redstone Calibration Service


DATE OF ISSUE 10 August 2017 CERTIFICATE NUMBER 12345 0574

Redstone Calibration Services APPROVED SIGNATORIES


The Freelands W Lewis √
51 Main Road, Kempsey B Lewis
Worcester
WR5 3NB
Calibration Engineer Will Lewis
Tel: 01905 821911 E-mail: info@redstonecal.co.uk
Web: www.redstonecalibration.co.uk PAGE 1 OF 5 PAGES

Calibration / Verification: Direct Verification of a Rockwell Hardness


Testing machine to ASTM E18-17
Machine: Wilson
Model Number: 574R
Serial Number: 999999
Calibrated for: Redstone Calibration Services
51 The Freelands
Main Road, Kempsey
Worcester, WR5 3NB

Date calibrated: 10 August 2017 Load Cell No: 200263A


Customer Order Number: Calibration standard: ASTM E74-06 Class A

SUMMARY OF CALIBRATION / VERIFICATION RESULTS


Force Pre Load Full Load Maximum
Allowed Error ± 2.0% ± 1.0 % Uncertainty
Maximum 1.80% 0.10% ± 0.4%

Depth Measuring System


Maximum Error 0.19 µm Maximum Uncertainty ± 0.37 µm

Time cycle Pre Load = 1.916 Secs Application Time = 2.298 Secs. Dwell Time = 3.337 Secs.
o o
The temperature during the calibration ranged from 25.6 C to 26.1 C
o
with a rate of change less than 2 C per hour

METHOD OF CALIBRATION / VERIFICATION


The Direct verification of the machine detailed above was made using calibrated force, linear
glass scale and a stopwatch with a calibrated time base. The series of measurements was in accordance
with the standards given above to a proceedure agreed by UKAS.

The reported uncertainties of measurement are based on a standard uncertainty multiplied by a


coverage factor k, providing a level of confidance of approximately 95%.
The Uncertainty evaluation has been carried out in accordance with UKAS requirements.
This certificate is issued in accordance with the laboratory accredition requirements of the
United Kingdom Accreditation Service. It provides traceabilty of measurement to the SI system
of units and/or to units of measurement realised at the National Physical Laboratory or
other recognised national metrology institutes. This certificate may not be reproduced other
than in full, except with the prior written approval of the issuing laboratory.
CERTIFICATE OF CALIBRATION
UKAS ACCREDITATION CALIBRATION LABORATORY No. CERTIFICATE NUMBER
12345
UKAS ACCREDITATION CALIBRATION LABORATORY No. 0574B
PAGE 2 OF 5 PAGES

RESULTS OF FORCE VERIFICATION k(95%) = 2

Decreasing loads Increasing loads Decreasing loads


Force (kgf) 0 Degrees (kgf) 0 Degrees (kgf) 180 Degrees (kgf) Mean (kgf) Bias (kgf) Unc (kgf) % Error
3 10 9.836 9.885 9.887 9.8693 -0.1307 0.0396 -1.32% ###
150 150.153 150.183 150.136 150.1573 0.1573 0.3265 0.10%
10 9.823 9.823 9.823 9.8230 -0.1770 0.0213 -1.80%

## -0.013 0.001191911 -0
Force Readings during indentation of Reference Blocks
Block 0 Degrees (kgf) 0 Degrees (kgf) 180 Degrees (kgf) Mean (kgf) Bias (kgf) Unc (kgf) % Error
Hard Block 150.184 150.163 150.190 150.1790 0.1790 0.3258 0.12%
Soft Block 150.200 150.146 150.140 150.1620 0.1620 0.3275 0.11%

RESULTS OF DEPTH MEASURING SYSTEM VERIFCATION

Block Depth Machine Depth Bias (µm) Unc (µm) Veff


33.52 33.56 0.13 0.10 4
51.80 52.12 -1.58 0.35 4
73.50 73.16 -0.63 0.26 4
112.80 113.00 0.19 0.15 4
146.30 147.24 -1.12 0.37 4
0.00%

INDENTER INFORMATION (FROM CALIBRATION CERTIFICATE)

Calibration Laboratory Euro Products Indenter Angle α 120.05 °

UKAS laboratory No 0441 Uncertainty (k=2) 0.030 °

Diamond Serial Number 999999 Indenter Radius 0.1940 mm

Certificate Number 999999 Uncertainty (k=2) 0.00094 mm

Date of calibration 10-Aug-17


####

COMMENTS
Hysterisis
Average of the last three readings performed = 99.73
CERTIFICATE OF CALIBRATION
CERTIFICATE NUMBER
12345
UKAS ACCREDITATION CALIBRATION LABORATORY No. 0574
PAGE 3 OF 5 PAGES

RESULTS OF TIME VERIFICATION @ 150Kg FORCE

Summary of Time Graph Results


Force Measured Time Specified time

Pre Load: 1.916 seconds 0.1 to 4 seconds

Load Application: 2.298 seconds 1 to 8 seconds

Full Load: 3.337 seconds 2 to 6 seconds

Final Load: 2.578 seconds 0.2 to 5 seconds


CERTIFICATE OF CALIBRATION
CERTIFICATE NUMBER
12345
UKAS ACCREDITATION CALIBRATION LABORATORY No. 0574
PAGE 4 OF 5 PAGES

RESULTS OF INDENTER CONTACT VELOCITY VERIFICATION

Summary of Time Graph Results


Depth Measured Time Specified Velocity

Maximum µm 606.800 <=999 µm per second

Minimum µm 0.000 Measured Velocity

Range µm 606.800 3.79 Seconds 160.11 µm per second


CERTIFICATE OF CALIBRATION
CERTIFICATE NUMBER
12345
UKAS ACCREDITATION CALIBRATION LABORATORY No. 0574
PAGE 5 OF 5 PAGES

RESULTS OF INDENTER CONTACT VELOCITY VERIFICATION

Summary of Time Graph Results


Depth Measured Time Specified Velocity

Maximum µm 705.270 <=999 µm per second

Minimum µm 0.000 Measured Velocity

Range µm 705.270 2.11 Seconds 334.25 µm per second


CERTIFICATE OF CALIBRATION
ISSUED BY Redstone Calibration Service
DATE OF ISSUE 10 August 2017 CERTIFICATE NUMBER 123456 0574

Redstone Calibration Services APPROVED SIGNATORIES


The Freelands W Lewis √
51 Main Road, Kempsey B Lewis
Worcester
WR5 3NB
Calibration Engineer John Lewis
Tel: 01905 821911 E-mail: info@redstonecal.co.uk
Web: www.redstonecalibration.co.uk PAGE 1 OF 2 PAGES

Calibration / Verification: Indirect Verification of a Rockwell Hardness


Testing machine to ASTM E18-17
Machine: Wilson Start Temp. 23.0 °C
Model Number: 574R End Temp. 23.2 °C
Serial Number: 999999
Calibrated for: Redstone Calibration Services Indenter Serail No.: 999999
51 The Freelands
Main Road, Kempsey Indenter Certificate: 999999
Worcester, WR5 3NB
Date of Calibration: 10-Aug-17
Date calibrated: 10-Aug-17
Customer Order Number:

METHOD OF CALIBRATION / VERIFICATION

The above Rockwell hardness testing machine has been indirectly verified to the standard requirements of
ASTM E18.

The hardness tests were made using certified indenters. Certified hardness reference blocks were also
used. The serial numbers and assigned hardness values of the reference blocks together with the
measurements obtained are given in the table on page 2 of this certificate.

A direct verification was carried out to ASTM E18. Reference certificate number 12345
Dated :- 10 August 2017

Note! This indirect certificate becomes invalid if an indenter other than one certified by a BS EN ISO 17025
accedited laboratory is used.

The reported uncertainties of measurement are based on a standard uncertainty multiplied by a


coverage factor k, providing a level of confidance of approximately 95%.
The Uncertainty evaluation has been carried out in accordance with UKAS requirements.
This certificate is issued in accordance with the laboratory accredition requirements of the
United Kingdom Accreditation Service. It provides traceabilty of measurement to the SI system
of units and/or to units of measurement realised at the National Physical Laboratory or
other recognised national metrology institutes. This certificate may not be reproduced other
than in full, except with the prior written approval of the issuing laboratory.
CERTIFICATE OF CALIBRATION
UKAS ACCREDITATION CALIBRATION LABORATORY CERTIFICATE NUMBER
123456
UKAS ACCREDITATION CALIBRATION LABORATORY
PAGE 2 OF 2 PAGES 200

RESULTS OF REFERENCE BLOCK VERIFICATION

Repeatability
Mean of Uncertainty

Allowed error
Block Scale Serial Reading Reading Reading Reading Reading

Error
the of the Mean k
& Value Number 1 2 3 4 5
readings Readings
3

Max Unc

64.5 HRC EP17193754 64.7 64.6 64.7 64.7 64.8 64.70 0.36 2.00 -0.20 0.20 0.5
45.3 HRC EP17193751 45.2 45.5 45.5 45.6 45.7 45.50 0.30 2.00 -0.20 0.50 1.0
24.8 HRC EP17193750 24.5 24.8 24.8 24.9 25.1 24.82 0.30 2.16 -0.02 0.60 1.0
Max Unc

#REF!
Note! The readings above have not been corrected for the BIAS of the machine obtained during the direct verification.

INDENTER INFORMATION (FROM CALIBRATION CERTIFICATE)

Diamond Indentor Ball Indentor


Ball
Calibration Indenter Calibration
Euro Products 120.05º 0 Certificate 12879
Laboratory Angle α Laboratory
Number
UKAS
UKAS laboratory Uncertainty Date of
0441 0.03º laboratory 0 00-Jan-00
Number (k=2) Calibration
Number
Ball holder
Diamond Serial Indenter
999999 0.194 mm Serial 12879 Ball Diameter 0.0625 Inch
Number Radius
Number
Uncertainty Certificate Uncertainty
Certificate Number 999999 0.00094 mm 12879 0.000026 Inch
(k=2) Number (k=2)

Date of Date of
10-Aug-17 00-Jan-00
Calibration Calibration

COMMENTS
0

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