PELAKSANAAN CEK ANTARA STANDAR UKURAN

LABORATORIUM MASSA DI BSML REGIONAL II

Disampaikan oleh Arif Nurjaya, ST

Bimbingan Teknis Pengelolaan Laboratorium Dan Standar Ukuran Di Bidang Metrologi Legal
Hotel Grand Zuri Malioboro Yogyakarta
 Check standard is a standard that is used as part of
measurement assurance program to provide check on the
standard and process to ensure that the standards,
measurement results, and measurement processes are
within acceptable statistical limits.

–KAN G-06 Guide On Measurement Assurance

The Ministry of Trade of the Republic of Indonesia

CHECK STANDARD

Check standard

?
E2 F1 Artifact

Calibration
 The concept of statistical process control is based on
comparing how measurement process is performing today
(often a single measurement) to how it has performed in
the best (a database of measurement results).

–KAN G-06 Guide On Measurement Assurance

The Ministry of Trade of the Republic of Indonesia

STATISTICAL PROCESS CONTROL

Today The Best

(initial data)

The Ministry of Trade of the Republic of Indonesia

5
1 DATA =
1 SERI

ABBA
Massa
A B B A ABBA
ABBA
Konv.

AT Standar

123.00
1
O

AT Dikalibrasi
N
O
FF
10
3
2
20
Control chart is a graphical tool used to visualize data
when monitoring, evaluating and improving a
measurement process

–KAN G-06 Guide On Measurement Assurance

The Ministry of Trade of the Republic of Indonesia

CONTROL CHART
10 is good number of data points to use as the baseline for our
The Best initial control measurements. Be sure to gather data over a period
of time, with not more than 1 measurement from the same day.
(initial data)

Data 1 Upper
UWL = mean + (2 x deviation)
Data 2 Statistical Warning Limits
Data 3
Data 4
Lower LWL = mean - (2 x deviation)

Data 5 MEAN
Data 6 DEVIATION
Data 7
Data 8
Upper
UAL = mean + (3 x deviation)

Statistical Action Limits

Data 9
Data 10
Lower LAL = mean - (3 x deviation)

The Ministry of Trade of the Republic of Indonesia

8
CHECK STANDARD
Description : 3 point control chart
Balance used : XP26C / 0.001 mg
Load : 0.002 g
Unit :g
Check Standar : F1 OIML class
Serial Number : 15885

LIMIT
Date Data Correction Mean Std Dev
UWL LWL UAL LAL
4-Feb-13 0.0020017 0.0017
5-Feb-13 0.0020007 0.0007
6-Feb-13 0.0020002 0.0002
7-Feb-13 0.0020012 0.0012
8-Feb-13 0.0019987 -0.0013
0.00005 0.0010
9-Feb-13 0.0019997 -0.0003
10-Feb-13 0.0019987 -0.0013 0.0021 -0.0020 0.0031 -0.0030
11-Feb-13 0.0020007 0.0007
12-Feb-13 0.0019992 -0.0008
13-Feb-13 0.0019997 -0.0003
7-Jul-13 0.0020035 0.0035
8-Jul-13 0.0020025 0.0025 0.00157 0.0025
9-Jul-13 0.0019987 -0.0013

The Ministry of Trade of the Republic of Indonesia

9
CHECK STANDARD
Description : 3 point control chart
Balance used : XP26C / 0.001 mg
Load : 0.002 g
Unit :g
Check Standar : F1 OIML class
Serial Number : 15885

Control Chart
0,004

0,003 UAL

0,002 UWL
Mass Correction (mg)

0,001

0,000

-0,001

-0,002 LWL

-0,003 LWL

-0,004
4-13 Feb 2013 Date 7-9 Juli 2013

The Ministry of Trade of the Republic of Indonesia

10
− Recalibration of the standard
− Validate calculation software
− Validate check standard calculation

Out of Control? What next???

− Obtain service or repair for balance

− Get new staff trained as soon as possible
− Fix environmental control as soon as possible

The Ministry of Trade of the Republic of Indonesia

STATISTICAL EVALUATION

Today The Best

(initial data)

Mean Mean t - test

F - test Deviation Deviation

The Ministry of Trade of the Republic of Indonesia

12
F – test

F – test is used to evaluate two processes have equivalent standard

deviations
2
𝑠𝑜𝑙𝑑
𝐹𝑣𝑎𝑙𝑢𝑒 = 2
𝑠𝑛𝑒𝑤
Our measurement system is considered to be “out of control” if we meet the
following conditions:
2 2
𝐹𝑣𝑎𝑙𝑢𝑒 > 𝐹∝,𝑣𝑛𝑒𝑤 ,𝑣𝑜𝑙𝑑 ; if 𝑠𝑜𝑙𝑑 >𝑠𝑛𝑒𝑤
2 2
𝐹𝑣𝑎𝑙𝑢𝑒 < 𝐹1−∝,𝑣𝑛𝑒𝑤 ,𝑣𝑜𝑙𝑑 ; if 𝑠𝑜𝑙𝑑 <𝑠𝑛𝑒𝑤

Possible action steps:

− Obtain service or repair for balance
− Get new staff trained as soon as possible
− Fix environmental control as soon as possible
The Ministry of Trade of the Republic of Indonesia

13
F – test

OIML R111-1:2004 Annex D

The Ministry of Trade of the Republic of Indonesia

14
t - test
t – test is used to evaluate the means of two processes
𝑥𝑜𝑙𝑑 − 𝑥𝑛𝑒𝑤
𝑡𝑣𝑎𝑙𝑢𝑒 =
2 2
𝑠𝑜𝑙𝑑 𝑠𝑛𝑒𝑤
+
𝑛𝑜𝑙𝑑 𝑛𝑛𝑒𝑤
Our measurement system is considered to be “out of control” if we meet the
collowing conditions:
2
𝑠2 𝑠2
𝑜𝑙𝑑+ 𝑛𝑒𝑤
𝑛𝑜𝑙𝑑 𝑛𝑛𝑒𝑤
𝑡𝑣𝑎𝑙𝑢𝑒 < 𝑡𝑐𝑟𝑖𝑡𝑖𝑐𝑎𝑙 ; 𝑣 = 𝑠2
𝑜𝑙𝑑 𝑠2
𝑛𝑒𝑤
𝑛𝑜𝑙𝑑 𝑛𝑛𝑒𝑤
+
𝑛𝑜𝑙𝑑 −1 𝑛𝑛𝑒𝑤 −1

Possible action steps:

− Recalibration or get maintenance of the standard
− Validate calculation software
− Validate check standard calculation
The Ministry of Trade of the Republic of Indonesia

15
t - test

OIML R111-1:2004 Annex D

The Ministry of Trade of the Republic of Indonesia

16
ANALYZE DATA

• Process degradation
• Process improvement
Control • Process compared to • Possible assignable
specification / tolerances causes
Chart • Shift in values of standard • Possible action steps
• Drift of values of standard
• Outliers

The Ministry of Trade of the Republic of Indonesia

17
PROCESS IMPROVEMENT
We obtained service for your balance
We have a new calibration officer who has many years of previous experience
Our environmental controls were repaired or improved
We have been practicing in balance operation

18
SHIFT IN VALUES OF STANDARD
Our standard is damage
Our check standard is damage
We are using calculation software
that has not been validated
We have errors in entering data
Our equation for the correction due to environmental
condition were drifted and correction changed
Our standard was recalibrated and a new value was
assigned without starting a new control chart
19
DRIFT OF VALUES OF STANDARD
Our working standard worn from use
Our check standard getting dirty
Our standards are not stable enough for this process

20
OUTLIERS
Balance not exercised normally / properly
We do not allow adequate thermal equilibrium to the standard prior to begin calibration
We have data entry error or miscalculation
Our environmental system is out of control
Our standard was recently damaged

21
PROCESS DEGRADATION
Our balance need service
We have calibration officer in the laboratory who needs training
Our environmental controls stopped working properly

22
PROCESS COMPARED TO SPECIFICATION / TOLERANCES

Our process is not achieving the requirements needed to meet the tolerances
because our balances has degraded and can not reach its normal performance

23
 Laboratorium
Panjang

Laboratorium
Laboratorium
Gaya dan
Massa
Tekanan

Laboratorium
Suhu

Laboratorium
Volume

The Ministry of Trade of the Republic of Indonesia

24
a r i f. n u r j a y a @ k e m e n d a g . g o . i d

25