Beruflich Dokumente
Kultur Dokumente
Smart Accessories
sampling tools
for Thermo Scientific
Nicolet FT-IR Systems
Smart Accessories
Speed Sample Preparation and Improve the Results in your Laboratory
2
How does it work?
An Overview of Basic FT-IR Sampling Techniques
3
How to Choose the Right Accessory
olids
s
ble S
s
uids
ting
udie
als
ids
ng
ype
s
ders
uids
s
Samples marked with “왖” are well suited for the indicated Smart Accessory.
mer
ders
Met
mer
rinda
s Liq
rofili
Coa
Liqu
n St
ls
le T
Pow
ic Liq
Poly
gica
lysts
Pow
Poly
bers
s on
th P
ace
eou
le/G
ctio
stic
tes
p
rs
Biolo
Sam
Hard
Hard
Cata
Acid
Gels
T YPE A CCESSORY P AGE D ISTINGUISHING F EATURES / A PPLICATIONS
Fibe
Surf
Aqu
Dep
Soft
Soft
Film
Britt
Cau
Rea
Rub
Pas
Smart ARK ™
pg.6 Research and analytical test laboratory environment
High energy throughput/high level quantitative and
qualitative analyses
12 reflection ZnSe crystal 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖
Mu lti-Bou n c e HAT R
Smart Multi-Bounce HATR pg.7 10 reflection ZnSe crystal; optional Ge crystal, and
Si crystal
왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖
Smart Golden Gate™ pg.11 Industrial strength ATR with diamond crystal with up to
80 lbs of force available to achieve good sample-to-crystal
contact of even the hardest sample
Single reflection type IIa diamond crystal 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖
Sing le Bo u n c e HAT R
Smart Performer™ pg.12 Small crystal area (2mm) in flat and trough formats
Single reflection with 4 crystal configurations: ZnSe,
Ge, AMTIR, Si
왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖
Smart OMNI-Sampler ™ pg.14 Resilient crystal allows for measuring of acids and
bases from pH 1 to 14
Capable of measuring a spot on a sample of 2 mm
왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖
diameter or less
Single reflection Germanium crystal
4
olids
s
ble S
s
uids
ting
udie
als
ids
ng
ype
s
ders
uids
s
mer
ders
Met
mer
rinda
s Liq
rofili
Coa
Liqu
Samples marked with “왖” are well suited for the indicated Smart Accessory.
n St
ls
le T
Pow
ic Liq
Poly
gica
lysts
Pow
Poly
bers
s on
th P
ace
eou
le/G
ctio
stic
tes
p
rs
Biolo
Sam
Hard
Hard
Cata
Acid
Gels
Fibe
Surf
T YPE A CCESSORY P AGE D ISTINGUISHING F EATURES / A PPLICATIONS
Aqu
Dep
Soft
Soft
Film
Britt
Cau
Rea
Rub
Pas
Smart SAGA ™
pg.15 All gold reflecting optics; unique internal dual masking
Sp e c u la r Re fle cta nc e
Smart Diffuse Reflectance pg.16 Convenient sample slides with storage space in the
accessory cover
Includes Si-Carb™ sampling tool, for analyzing solid materials
such as paint chips 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖
Smart NIR Integrating Sphere pg.17 Optimal solution for near-infrared diffuse reflectance of
powders and many solid samples
Includes dedicated room temperature InGaAs detector
Diffuse
왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖 왖
Optional sample spinner to average variations in your sample
Smart Transmission pg.19 Enclosed design provides excellent purge and is chemically
resistant, protecting the spectrometer from contamination
and spillage
Tra nsmission
5
Smart ARK
For Research Grade, Multiple-Reflection ATR Analysis
The Thermo Scientific Smart ARK is a stable, rugged, high energy Smart ARK is available with the widest variety of crystal plates in
throughput HATR. The Smart ARK™ is the ideal choice for both different materials and angles including 30, 40, 50, 55, 60, and 70
research and analytical test laboratories. degrees (dependent on material). There is a crystal material for
It is well suited for high level accurate almost any pH sample and a suitable crystal angle that results in a
quantitative and qualitative analyses pathlength from 0.6 to 45 micrometers.
because sample preparation is not The following table shows the angle of incidence (q), number of
necessary. The Smart ARK’s high reflections, the refractive index of the crystal (R.I.), the calculated
performance is a result of high optical depth of penetration (dp), the calculated effective pathlength (EPL)
collection efficiency and unique patented in micrometers for three common materials (other materials available
crystal design. This crystal design allows upon request). The experimental sampling depth is 2 to 3 times the
the user to change crystal angles and calculated depth of penetration.
materials without optical realignment. Θ # OF REFL. ZNSE (R.I. = 2.4) GE (R.I. = 4) AMTIR (R.I. = 2.5)
The multi-reflection crystal design is dp EPL(µm) dp EPL(µm) dp EPL(µm)
extremely well-suited for analyzing 30 21 NA NA 1.2 17.68 NA NA
lower concentration samples and where 40 14 4.4 45.64 0.763 4.24 2.76 38.75
high sensitivity is necessary. It is good 45 12 2.0 12.12 0.664 2.59 1.70 9.68
for samples that require consistent, 50 10 1.5 5.82 0.596 1.62 1.34 4.93
precise analysis or when different 55 8 1.25 3.11 0.547 .992 1.14 2.71
pathlengths are required to analyze a 60 7 1.11 1.94 0.510 .672 1.02 1.72
sampling system.
Critical Angle 38.68 22.02 36.87
Example Applications
• Liquids Both trough and flat plate style crystal plates are available to
• Solids suit the specific sample analysis. The trough plate version is optimized
• Semi-solids for use with liquids, pastes, and gels. The flat plate version is
• Powders optimized for use with solid films. All crystal plates are Teflon® coated
• Quantitative and qualitative measurements to improve chemical resistivity and prevent discoloration of the plate
surface. The pressure device has been optimized to reduce breakage
Unique Features of the crystals that can be caused by too much or uneven pressure.
To facilitate changing crystal angles or material (and subsequently
Specifications
the depth of penetration into a sample or effective pathlength) our
Crystal Material: Zinc Selenide (standard),
patented crystal design ensures high energy throughput without the
Germanium (optional), Silicon (optional),
need for mechanical or manual optical alignment of the accessory. Zinc Sulfide (optional), AMTIR (optional)
It is extremely easy to change crystal plates and angles; there is no Angle of Incidence: 45 degree (standard), optional 30, 40, 50, 55, 60,
need to worry about moving mirrors and mechanical parts failing. 70-depending on material
The crystal design ensures reproducibility and reliability with every Number of Reflections: 12 (standard) see chart above for
measurement, which is especially critical when transferring analytical additional information
methods between laboratories with multiple spectrometers. The Pathlength: Approximately 12 micrometers
Sample Volume (trough): 1.0 milliliters
Heated Option: Allows thermal studies from ambient to 100 °C
Ordering Information
Accessory Part Number
XX = 99 for Nicolet ™ iS10, Nicolet iS50, Nicolet x700, and Nicolet Nexus™
XX = 97 for Nicolet 380 and Avatar ™
Spectra of vegetable oil using 40° (top), 45° (middle) and 60° (bottom) ZnSe
crystals on the Smart ARK
6
Smart Multi-Bounce HATR
For Multiple-Reflection ATR Analysis
The Thermo Scientific Smart Multi-Bounce HATR crystal has a Multi-Bounce HATR Flat Plate Kit
pathlength of 10 micrometers, while the smallest pathlength of a The flat plate kit is useful for analyzing films and coatings on flat
typical transmission cell is 15 micrometers. This short pathlength samples. Flat plates are configured with
makes the Smart Multi-Bounce HATR suitable for samples that the crystal ‘flush’ with the surface of the
absorb strongly and yields better results than transmission. In plate. The pressure device included with
addition, the Smart Multi-Bounce HATR is well suited for providing the flat plate kit ensures reproducible
information about the surface properties of a material. pressure and uniform optical contact
between the sample and crystal.
Example Applications
• Aqueous solutions Smart Multi-Bounce HATR
• Solvents Combination Plate Kit
• Flexible films The combination plate kit is ideal when
• Gels a variety of liquid and solid samples are
• Soft powders analyzed. This kit includes both trough
and flat plates, and the following
Unique Features sampling tools:
The horizontal sampling surface is ideally suited for obtaining high- • Volatile liquid cover
quality infrared spectra – without the need for sample preparation. • Powder press
There are convenient storage spaces within the cover of the accessory • Pressure device
which accommodate the accessory’s sampling tools, such as a
powder press and volatile liquid cover. Crystal Materials
The Smart Multi-Bounce HATR uses crystals mounted in plates The standard crystal material is zinc selenide (ZnSe), with a 45 degree
that are pinned in place on the accessory. This allows you to change angle of incidence. This material is well suited for almost all routine
plates by simply lifting one off and placing another on. All of the sampling. Zinc selenide is fairly hard, and is utilized for neutral
Smart Multi-Bounce plates are Teflon coated to improve chemical pH solutions.
resistivity and prevent discoloration. Once measurements have The optional Germanium crystal has a high refractive index
been made, the crystal may be wiped clean or if necessary the with a shallow depth of penetration into the sample, making it well
whole plate can be simply lifted off and removed for rapid cleaning. suited for measuring samples with a high refractive index, such as
carbon-filled polymers. Although germanium has a limited spectral
Plate and Crystal Choices range, it offers good chemical resistivity to both acids and bases.
Multi-Bounce HATR Trough Plate Kit
The trough plate kit is useful for analyzing liquids, powders, pastes,
Specifications
and gels. The ATR crystal is recessed and mounted into a trough Crystal Material: Zinc Selenide, standard; (4000 – 650 cm-1)
Germanium, optional; (4000 – 800 cm-1)
shaped, leak-proof sampling plate. The ATR crystal sample plate Silicon, optional; (4000 – 1500 cm-1)
restricts catastrophic liquid spills from damaging the accessory in Number of Reflections: 10
any way. Also included is a volatile liquid cover that eliminates Crystal Angle: 45°
solvent evaporation and a powder press to ensure good contact Pathlength: Approximately 10 micrometers
between powdered samples and the crystal. Sample Volume (trough): 0.5 milliliters
Ordering Information
Accessory Part Number
XX = 99 for Nicolet iS10, Nicolet iS50, Nicolet x700, and Nicolet Nexus
XX = 97 for Nicolet 380 and Avatar
Xylene mixture with 45° ZnSe trough with Smart Multi-Bounce HATR
7
Smart iTR
For Multi-purpose ATR Sampling
Ten replicated PET spectra collected from different locations on the same sample
using a Nicolet iS10 spectrometer with the Smart iTR
8
Choice of ATR Crystal Materials Specifications
The Smart iTR accessory can be ordered with three common Diamond ATR Crystal: Diamond is one of the most rugged optical
ATR crystals fixed in stainless steel as standard: diamond, ZnSe materials available.
and germanium. Each crystal performs strongly under specific • Low wavenumber cutoff 650 cm-1 (due to ZnSe lens)
circumstances. • Depth of penetration 2.03 micrometers at 1000 cm-1
• Refractive index 2.4
The diamond crystal is excellent for the analysis of hard,
• Useful pH range 1–14
abrasive, reactive, caustic or corrosive materials, since it is
• Incident angle 42
inert and robust. It is also a multi-purpose ATR with a depth of
penetration of over 2 microns at 1000 cm-1 and is used with a wide ZnSe ATR Crystal: ZnSe is the most common ATR crystal. It has limited
uses with strong acids, alkalis. The surface can be scratched by hard
variety of samples. Its disadvantage is the intrinsic absorbtion from
materials, which will eventually reduce sensitivity. Complexing agents
approximately 2300 to 1800 cm-1. (EDTA and ammonium) will also attack the crystal surface.
The ZnSe crystal offers similarly outstanding throughput and a • Low wavenumber cutoff 650 cm-1
depth of penetration similar to diamond. It can be used for a wide • Depth of penetration 2.03 micrometers at 1000 cm-1
variety of samples, but over time it can be etched by acids and • Refractive index 2.4
scratched by hard samples. ZnSe is soft and not as chemically inert • Useful pH range 5– 9
as the other crystals, but provides an excellent performing, lower • Incident angle 42
cost option for general analyses. Germanium ATR Crystal: Ge is a hard ATR crystal with a high refractive
A five-year warranty is provided with the diamond ATR crystal. index. This makes it useful for strong absorbers or samples with a high
Both the diamond and ZnSe configurations can be validated. refractive index. The novel germanium design provides enormous
through-put over an extended range.
Germanium is also hard and inert (although not as robust
• Low wavenumber cutoff 700 cm-1
as diamond). Germanium provides a much shallower depth of
• Depth of penetration 0.67 micrometers at 1000 cm-1
penetration, making it ideal for highly absorbing or scattering • Refractive index 4.0
samples such as carbon-black containing rubbers. The exclusive • Useful pH range 1– 14
germanium crystal used in the Smart iTR provides huge performance • Incident angle 42
through the mid-IR range, with upwards of 50% transmittance.
Silicon ATR Crystal: Si is a very hard ATR crystal with a high refractive index.
Germanium has a limited range, but offers good chemical
• Low wavenumber cutoff 700 cm-1
resistivity to both acids and bases. • Depth of penetration 0.84 micrometers at 1000 cm-1
An additional ATR crystal that can be added to any of the • Refractive index 3.4
accessories is silicon. Silicon is a very hard ATR crystal with a high • Useful pH range 1– 12
refractive index. This makes it useful for strong absorbers or abra- • Incident angle 42
sive samples. Silicon withstands thermal shock, so it is suitable for Active Sample Area: The ATR active sample area is 1.5 mm for the single
temperature studies. Silicon is typically absorbing below 1500 cm-1, bounce ATR and 6 mm for the 3 bounce ATR.
but the composite design results in a much broader range. Specular Plate: Spectral range dependent on spectrometer. Incident angle
is 45 degrees.
Ordering Information
Accessory Part Number
9
Smart Orbit
For single-reflection, diamond ATR analysis
The Smart Orbit accessory provides spectral results from a variety of samples
such as small fibers, hard polymers, and more
10
Smart Golden Gate
For single-reflection, diamond ATR analysis
The Thermo Scientific Smart Golden Gate Single Reflection Example Applications
Diamond ATR accessory analyzes sample types from hard solids to • Polymer pellets
corrosive liquids. This versatile infrared sampling instrument is • Intractable or opaque solids
fast, sensitive, and robust. Excellent sensitivity is achieved using • Single fibers
high pressure contact against a Type IIa diamond, selected for its • Corrosive liquids
unparalleled sensitivity as a single-reflection ATR element together • Geochemical samples
with its unique physical and chemical stability. The accessory can • Powders
be used to analyze a range of samples from single particles and • Coated wires
fibers to corrosive liquids, and the large working area sample plat- • Air sensitive samples
form is ideal for macro sampling. The diamond is high temperature • Hazardous materials/toxic compounds
bonded into its tungsten carbide mount giving performance and
strength to withstand the high pressures required for maximum Unique Features
optical contact with hard samples. • 45° single reflection Type IIa diamond
Because of the robust design of the Smart Golden Gate™ • Brazed tungsten carbide diamond
accessory and the ability to apply very high pressures to the mount
sample, this accessory can be used for almost any sample type • Fully enclosed beam condensing
in any research or QA environment. Little or no sample preparation lens system
is needed, the only requirement is that the sample is in optical • Sapphire anvil for high pressure
contact with the diamond. With up to 80 pounds* available to contact
achieve this, good spectra can be run from even the hardest rocks • Reproducible pressure control to
80 pounds
and powders. Special anvils are available to hold polymer pellets,
• Thermal, cryogenic, and super critical fluid options available
to seal in and run air/moisture sensitive samples, and to analyze
• Fully enclosed sample anvil available for dangerous or sensitive
coatings on wires. The Smart Golden Gate accessory is particularly samples
suitable for samples which may polymerize or set on the crystal
since they can be cleaned off with a knife or abrasive pads without Specifications
causing any damage to the unit. Crystal Material: Type IIa diamond
The demountable top plate is a valuable accessory for the Spectral Wavelength Range: 5000 to 650 cm-1 ZnSe optics, 5000 to
preparation of toxic compounds (such as anti-cancer drugs). The 400 cm-1 KRS-5 optics
sample can be prepared in a glove box, sealed, and then measured
with higher protection to the operator than when using other Ordering Information
sampling methods. Accessory Part Number
* Applied load across the diamond surface. Smart Golden Gate – ZnSe/Diamond 840-081500
Smart Golden Gate – KRS-5/Diamond 840-081600
Xylene mixture with 45° ZnSe trough with Smart Multi-Bounce HATR
11
Smart Performer
For single-reflection ATR analysis
12
Smart DuraSamplIR and Smart DuraScope
For single-reflection, diamond ATR analysis
Example Applications
• Liquids ranging in pH from 1 to 14
• Rigid, intractable materials
• Abrasive powders Specifications
• Painted metal panels Crystal Material: Diamond or Silicon
• Fibers Spectral Range: Standard to 650 cm-1; Optional to 230 cm-1
• Inclusions and contaminants down to 200 microns Sampling Area: 1 reflection: 500 micrometers
(DuraScope only) 3 reflection: 1.5 millimeters
9 reflection: 3 millimeters (DuraSamplIR only)
Unique Features Depth of Penetration: 2 µm at 1000 cm-1
• 1, 3, or 9-bounce crystal options Useful pH Range: 1 – 14
• Hastelloy plate available for extra chemical resistivity Sample Volume: 1 reflection: 1 microliters
• DuraScope video capability option 3 reflection: 2 microliters
• DuraScope magnification up to 100X 9 reflection: 5 microliters (DuraSamplIR only)
Ordering Information
Accessory Part Number
Smart DuraSamplIR, 1 bounce 840-091600
Smart DuraSamplIR, 3 bounce 840-091500
Smart DuraSamplIR, 9 bounce 840-091400
Smart DuraScope, 1 bounce 869-091700
Smart DuraScope, 3 bounce 869-091800
13
Smart OMNI-Sampler
For Single-Reflection ATR Analysis
XX = 99 for Nicolet iS10, Nicolet iS50, Nicolet x700, and Nicolet Nexus
XX = 97 for Nicolet 380 and Avatar
14
Smart SAGA
For Research Performance Grazing Angle Reflectance Studies
The Thermo Scientific Smart SAGA (Specular Apertured Grazing Unique Features
Angle) is ideal for grazing incidence analysis of sub-micron films on In addition to the all of the advantages of the Thermo Scientific
metallic substrates. Grazing angle reflectance is the technique of Smart Accessories, the Smart
choice for analyzing thin coatings or deposits because the high SAGA™ features a unique internal
angle of incidence increases pathlength of the infrared beam sliding aperture assembly to quickly
through the material of interest, significantly enhancing sensitivity. provide sampling areas of different
This accessory samples an average angle of 80 degrees from the sizes. The aperture is set by simply
normal. Analysis of films from 10 Angstroms to 0.5 microns is pos- rotating a calibrated thumb wheel
sible. A permanently mounted polarizer minimizes the ‘S’ polarized on the front of the assembly. It
light which does not contribute to spectral data at the surface, defines the infrared beam area
increasing sensitivity and sampling speed. Samples are analyzed both before and after reaching the
conveniently by placing them on a horizontal sampling surface and sample surface, using a revolution-
masked using a unique sliding aperture assembly. ary double-pass beam path. The
This is an extremely easy accessory to use for grazing angle design eliminates the need to “soot”
studies, yet it delivers superior performance and great sample area apertures to reduce unwanted
discrimination. Simply lay the sample flat on the horizontal sampling reflections, and allows accurate
surface, position it using the laser-engraved grid if desired, turn sample definition localized studies. The integrated polarizer allows
the wheel to set the aperture size, and scan. Monolayer sensitivity the best possible sensitivity and signal-to-noise ratio.
is achievable due to the high angle of incidence and selective The sample stage features a laser-engraved linear measurement
polarization. grid that allows reproducible sample positioning for localized studies
of larger samples. These markings provide spatial information
Example Applications about where data was collected on a sample that can be recorded
• Ultra-thin coatings for future reference.
• Adsorbed species on metal substrates
• 80 degree fixed angle of incidence
• Lubricants
• All gold reflecting optics
• Surface contaminants
• Unique internal aperture sliding assembly providing four
• Residues different shapes and sizes of sample definition.
• Molecular monolayers • Integrated polarizer to eliminate the ‘S’ polarized light and
enhance the “P” polarized light component. The integrated
design also protects the polarizer from contamination
• A laser engraved grid on the sampling plate to facilitate
reproducible sample positioning and masking when performing
quantitative analysis
Specifications
Angle of Incidence: Average 80° fixed
Sampling Area: Two circular active areas: 5mm, and 8mm; one oval active
area of 16mm x 8mm, and open beam
Optics: Gold reflective
Sample Positioning: Laser-engraved measurement grid on sample stage
Polarizer: Germanium
Ordering Information
Cadmium arachidate monolayer on a gold substrate analyzed with a Smart SAGA
Accessory Part Number
XX = 99 for Nicolet iS10, Nicolet iS50, Nicolet x700, and Nicolet Nexus
XX = 97 for Nicolet 380 and Avatar
15
Smart Diffuse Reflectance
For Mid-infrared Diffuse Analysis
Example Applications
• Hard and soft powders
• Organic and inorganic materials
Ninhydrin 1% in KBr collected using the Smart Diffuse Reflectance
• Paint chips
• Inflexible sample that can be abraded
with silicon carbide paper The second holder is intended for use with the Si-Carb
measuring system and has an integral gold mirror that can be
Unique Features used as a background reference. A blank Si-Carb disk can also be
The Smart Diffuse Reflectance accessory comes complete with two used as a background reference. This sample slide also has a slot
sample slides. One holder has two integral sample cups within it. that holds the Si-Carb disk. The Si-Carb kit includes the adhesive-
Typically, one of the positions is loaded with the sample and the backed silicon carbide paper that is used to abrade the surface to
other is loaded with a reference material, such as KBr. The integral be analyzed, plus a handle and sample plate to hold the paper.
sample cups eliminate the need to worry about easily lost small This technique transfers a small amount of sample to the disk.
parts, and are easy to load without the inconvenience of handling An infrared spectrum is obtained of the material clinging to the
small sample cups. If KBr is needed to dilute a sample for analysis, surface of the silicon carbide disk.
the convenient KBr Powder Packets can be used. Each of the KBr
Powder Packets contains a convenient, pre-measured quantity of Specifications
dry KBr for dispersing a sample. Sample Cup Volume: 0.25 gram
Dual Sample Slide Holders: Si-Carb holder
and powder sampler holder
KBr Packets: 0.5 gram packets (25)
Silicon Carbide Disks: 320 grit Si-Carb disks (100);
400 grit Si-Carb disks (100)
Ordering Information
Accessory Part Number
Smart Diffuse Reflectance 0028-4XX
XX = 99 for Nicolet iS10, Nicolet iS50, Nicolet x700, and Nicolet Nexus
XX = 97 for Nicolet 380 and Avatar
16
Smart NIR Integrating Sphere
For Near-infrared Diffuse Reflectance
The Thermo Scientific Smart NIR integrating sphere provides the The diameters of the sphere, detector, and sample window
best method of analysis of diffuse reflection. This leads to easier size have been carefully optimized to make collection even more
sample handling and increased throughput. The integrating sphere efficient. The scattered near-
enhances the near-infrared capabilities of Thermo Scientific Nicolet infrared energy is collected with
FT-IR spectrometers. greater than 95% efficiency.
17
Smart NIR UpDRIFT
For near-infrared diffuse analysis
Ordering Information
Accessory Part Number
Smart Near-IR UpDRIFT 0027-0XX
18
Smart Transmission
For Transmission Analysis
The Thermo Scientific Smart Transmission is ideal when you need reach environmental equilibrium, while with the standard sample
to make fast and accurate measurements of liquids, solids, or compartment holder it can take up to 11 minutes. The Quick-Purge
gases that are mounted in cells or cell holders and mounts. The feature eliminates atmospheric water
Smart Transmission optimizes the ease and speed with which basic vapor and carbon dioxide that can
transmission measurements are made. The accessory features one obscure peaks of interest and complicate
step, snap-in-place installation and automatically seals the sample spectral subtractions. Once a cell has
compartment with its Quick-Purge feature. This capability drastically been placed in the sample card/cell
reduces the length of time between sample analyses and is holder tray, a plastic insert can be
extremely advantageous when analyzing a large number of samples installed to complete the purge features.
in succession. Purging the sample environment during infrared The Smart Transmission accessory
analysis eliminates atmospheric water vapor and carbon dioxide that has sample positions that accommodate
can obscure peaks of interest and complicated spectral subtractions. most KBr Pellet holders, Precision
Typically, purging the main instrument sample compartment without Pathlength liquid cells, infrared cards,
a Smart Accessory can take up to five times longer to reach film holders, gas cells and many other
environmental equilibrium than with the Smart Transmission accessory. transmission tools. Each position is for
The accessory has an enclosed design which is chemically resistant optimizing the IR beam focus through
and will protect the instrument from contamination and spillage. different cells.
When using corrosive or caustic materials, the Smart Transmission Smart Transmission 0028-1XX
accessory protects the spectrometer from potential accidental spillage. XX = 99 for Nicolet iS10, Nicolet iS50, Nicolet x700, and Nicolet Nexus
To obtain faster results and higher quality spectral information, XX = 97 for Nicolet 380 and Avatar
the Smart Transmission accessory should be used to enhance
transmission infrared analyses. The Quick-Purge feature dramatically
decreases the time necessary between samples. With the Smart
Transmission accessory it takes two minutes or less to
19
SAMPLE
SET UP
A N A LY Z E
Success R E P O RT
www.thermoscientific.com
©2010-2012 Thermo Fisher Scientific Inc. All rights reserved. ISO is a trademark of the International Standards Organization.
Windows is a registered trademark of Microsoft Corporation. Golden Gate is a trademark of Specac Limited. DuraSamplIR,
DuraScope and DuraVision are trademarks of SensIR Technologies, now a part of Smith's Detection. Spectralon is a registered
trademark of Labsphere, Inc. All other trademarks are the property of Thermo Fisher Scientific Inc. and its subsidiaries. This information Thermo Electron Scientific
Instruments LLC, Madison, WI USA
is presented as an example of the capabilities of Thermo Fisher Scientific Inc. products. It is not intended to encourage use of
is ISO Certified.
these products in any manners that might infringe the intellectual property rights of others. Specifications, terms and pricing are
subject to change. Not all products are available in all countries. Please consult your local sales representative for details
Africa +27 11 822 4120 Denmark +45 70 23 62 60 India +91 22 6742 9434 New Zealand +64 9 980 6700
Australia +61 3 9757 4300 Europe-Other +43 1 333 50 34 0 Italy +39 02 950 591 Russia/CIS +43 1 333 50 34 0
Austria +43 1 333 50 34 0 Finland/Norway/Sweden Japan +81 45 453 9100 Spain +34 914 845 965
Belgium +32 53 73 42 41 +46 8 556 468 00 Latin America +1 561 688 8700 Switzerland +41 61 716 77 00
Canada +1 800 530 8447 France +33 1 60 92 48 00 Middle East +43 1 333 50 34 0 UK +44 1442 233555
China +86 10 8419 3588 Germany +49 6103 408 1014 Netherlands +31 76 579 55 55 USA +1 800 532 4752
CT51044_E 07/12M