LAMPIRAN B

DATA PENGAMATAN

B.1 Data Ruang

Tabel B.1 Data Keadaan Ruang
Hari ke-1 Hari ke-2
Parameter
Awal Akhir Awal Akhir
Temperatur ( C) o
27 27.2 26.8 27.2
Tekanan (mbar) 958 957 958 956
B.2 Data Percobaan
B.2.1 Kalibrasi Termometer
Tabel B.2 Kalibrasi Termometer
Termometer Titik Beku (oC) Titik Didih (oC)
Termometer Raksa 110 oC 0 98
Termometer Raksa 110 C o
0 98
Termometer Raksa 250 C o
0 98
Termometer Raksa 250 C o
0 98
Termometer Raksa 360 oC 0 98

B.2.2 Kalibrasi Piknometer

Tabel B.3 Kalibrasi Piknometer
Pengukuran Massa (gram)
Piknometer kosong 11.775 11.775 11.775
Piknometer + aquadest 17.1468
Piknometer + metanol teknis 15.9632

B.2.3 Kalibrasi Refraktometer

Tabel B.4 Kalibrasi Refraktometer
Indeks Bias
Bahan
1 2 3
Benzene 1.495 1.486 1.497
Aquadest 1.334 1.334 1.334

B.2.4 Kalibrasi Pompa Diafragma

Tabel B.5 Kalibrasi Pompa Diafragma
Volume (mL)
Skala Pompa Waktu (s)
1 2 3
10 30 85 90 80
20 30 120 130 110
30 30 150 160 140
40 30 190 200 220
50 30 200 220 210
 60 30 240 250 230
70 30 260 270 250
80 30 280 280 270
90 30 300 290 300
100 30 310 320 330

B.2.5 Penentuan Kurva Indeks Bias dengan Fraksi Mol Metanol

Tabel B.6 Penentuan Kurva Indeks Bias dengan Fraksi Mol Metanol

Massa botol
Massa Botol Massa botol + + aquadest + Indeks Bias
Botol ke- Kosong (gram) aquadest (gram) metanol
(gram)
1
1 9.4034 14.1959 14.1959 1.335025
2 9.6195 13.8802 14.2323 1.33702
3 9.6297 13.3199 13.947 1.338035
4 9.5054 12.6601 13.7657 1.34106
5 9.1342 11.8179 13.2519 1.342065
6 9.614 11.8654 13.6427 1.34307
7 9.659 11.3451 13.5677 1.342065
8 9.4999 10.7057 13.2513 1.341
9 9.3913 10.1205 13.2731 1.33602
10 10.5812 11.1296 14.5542 1.33401
11 9.5062 9.5062 13.3099 1.329

B.2.6 Distilasi Kontinyu Refluks Parsial

Tabel B.7 Distilasi Kontinyu Refluks Parsial
Keterangan Pengukuran
Indeks Bias Metanol teknis 1.32907 1.32907
Volume Metanol 1024
Volume Aquadest 803
Volume Total Umpan 1827
Indeks Bias Umpan 1.34302 1.34302
Suhu Umpan 28
Massa Bottol Bottom Kosong 28
Indeks Bias Produk Bottom 1.33601 1.33601
Massa Botol Kosong + Bottom 908
Tinggi Kolom 96
Jumlah Tetesan Ke Kolom 23
Jumlah Tetesan ke distilat 9
Suhu Distilat Akhir
Indeks Bias Produk Vakum
Massa Botol Produk Vakum Kosong 0
Massa Botol Kosong + Produk Vakum 97

B.2.7 Data Distilasi dengan Refluks Parsial

B.2.7.1 Data Distilasi dengan Refluks Parsial pada Kolom 3
Tabel B.8 Data Distilasi Pada Kolom 3

Massa Botol Massa Botol + Indeks Bias

Waktu (menit) Suhu (oC)
Kosong (gram) Sampel (gram)
1
10 9.4533 9.5423 55 1.34206
20 9.4733 9.8231 52 1.34206
30 9.3502 10.5995 59 1.34206
40 9.287 10.7099 50 1.34005
50 9.1349 10.919 54 1.342055
60 9.6044 10.318 48 1.342055
70 6.3319 11.3796 56 1.342055
80 6.487 8.341 53 1.342055
90 13.432 13.6723 56 1.342055
100 13.3135 13.5325 57 1.342055
110 11.7383 12.7757 60 1.342055
120 11.8468 11.9725 57 1.342055
130 11.8235 12.1235 60 1.342055
140 13.3134 13.8321 52 1.342055
150 12.1983 12.9235 56 1.342055

B.2.7.2 Data Distilasi dengan Refluks Parsial pada Kolom 5

Tabel B.9 Data Distilasi pada Kolom 5

Massa Botol Massa Botol + Indeks Bias

Waktu (menit) Suhu (oC)
Kosong (gram) Sampel (gram)
1
10 9.5318 10.4135 53 1.341
20 9.2102 9.7924 49 1.34008
30 10.5523 10.7012 55 1.33904
40 9.4352 9.6943 50 1.341
50 9.3196 9.5213 48 1.341
 60 9.2886 10.2428 48 1.33904
70 9.1527 9.994 53 1.33904
80 9.3691 9.5431 45 1.33904
90 9.5218 9.7182 51 1.33904
100 13.4801 17.8586 50 1.33904
110 13.5504 14.5132 55 1.33904
120 11.8749 12.8184 51 1.33904
130 13.4703 13.5348 50 1.33904
140 13.3905 14.1981 48 1.33904
150 13.2518 13.7923 50 1.33904

B.2.7.3 Data Distilasi dengan Refluks Parsial pada Kolom 8

Tabel B.10 Data Distilasi Pada Kolom 8

Massa Botol Massa Botol + Indeks Bias

Waktu (menit) Suhu (oC)
Kosong (gram) Sampel (gram)
1
10 9.4613 12.0576 51 1.338035
20 9.5882 10.894 43 1.33804
30 9.6188 13.5628 55 1.33703
40 9.7234 11.5868 49 1.338055
50 9.4897 12.4612 45 1.33808
60 9.6608 13.9374 45 1.33803
70 9.8725 11.2156 49 1.33803
80 9.1142 11.1072 42 1.33803
90 11.755 12.3219 46 1.33803
100 13.2284 13.9106 40 1.33805
110 11.8393 11.9234 49 1.33805
120 11.8875 11.8905 43 1.33805
130 11.7491 11.8599 42 1.33803
140 11.9412 11.9821 43 1.33803
150 11.8747 11.8795 42 1.33803
B.2.7.4 Data Distilasi dengan Refluks Parsial pada bottom
Tabel B.11 Data Distilasi pada bottom

Massa Botol Massa Botol + Indeks Bias

Waktu (menit) Suhu (oC)
Kosong (gram) Sampel (gram)
1
10 9.2686 11.4821 72 1.33904
20 9.3597 12.5174 70 1.34206
30 9.3506 14.6506 66 1.341055
40 9.1532 11.6757 70 1.34206
50 8.9539 12.338 76 1.34206
60 9.2837 11.4126 70 1.34106
70 9.7165 12.8894 69 1.34104
80 9.5217 13.9076 76 1.34206
90 13.2337 16.2156 76 1.34106
100 13.4369 18.386 70 1.33904
110 11.7547 14.887 79 1.339055
120 11.626 14.0235 70 1.341055
130 11.6826 14.1376 70 1.33904
140 1.3896 14.2151 72 1.33904
150 13.2751 13.0572 70 1.33904

B.2.7.5 Data Distilasi dengan Refluks Parsial pada Distilat

Tabel B.12 Data Distilasi pada Distilat

Massa Botol Massa Botol + Indeks Bias

Waktu (menit) Suhu (oC)
Kosong (gram) Sampel (gram)
1
10 9.2156 11.4821 42 1.333
20 9.6988 15.2619 42 1.333
30 9.1984 19.2896 42 1.332
40 9.4239 11.2373 40 1.332
50 6.4422 9.1657 40 1.334005
60 6.4239 20.785 42 1.332
70 6.1984 15.0879 40 1.332
80 6.467 15.4065 42 1.332
90 6.4437 14.3577 42 1.332
100 6.487 12.4646 42 1.333
110 6.0775 11.5323 42 1.333
120 6.112 13.4728 42 1.333
130 6.3319 13.1739 42 1.333
140 11.6826 22.1219 42 1.333
150 13.3896 23.2547 42 1.334005
tanol

Indeks Bias

2 3
1.33502 1.33502
1.33701 1.33608
1.338035 1.338035
1.34106 1.34106
1.34206 1.34206
1.34307 1.34307
1.34206 1.34206
1.341 1.341
1.33602 1.336015
1.33401 1.33401
1.328 1.329

1.32907
mL
mL
mL
1.34302
C
o

gram
1.33601
gram
cm

C
o
 gram
gram

Indeks Bias

2 3
1.34206 1.34206
1.34206 1.34206
1.34206 1.34206
1.34005 1.34005
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206
1.342055 1.34206

Indeks Bias

2 3
1.341 1.341
1.34008 1.34008
1.33904 1.33904
1.341 1.341
1.341 1.341
 1.33904 1.33904
1.33904 1.33904
1.33904 1.33904
1.33904 1.33904
1.33904 1.33904
1.33904 1.33904
1.33904 1.33904
1.33904 1.33904
1.33904 1.33904
1.33904 1.33904

Indeks Bias

2 3
1.338035 1.33804
1.33804 1.33804
1.33703 1.33703
1.338055 1.33806
1.33808 1.33808
1.33803 1.33803
1.33803 1.33803
1.33803 1.33803
1.33803 1.33803
1.33805 1.33805
1.33805 1.33805
1.33805 1.33805
1.33803 1.33803
1.33803 1.33803
1.33803 1.33803
Indeks Bias

2 3
1.33904 1.33904
1.34206 1.34206
1.34106 1.34106
1.34206 1.34206
1.34206 1.34206
1.34106 1.34106
1.34104 1.34104
1.34206 1.34206
1.34106 1.34106
1.33904 1.33904
1.339055 1.33906
1.341055 1.34106
1.33904 1.33904
1.33904 1.33904
1.33904 1.33904

Indeks Bias

2 3
1.333 1.333
1.333 1.333
1.332 1.332
1.332 1.332
1.334005 1.33401
1.332 1.332
1.332 1.332
1.332 1.332
1.332 1.332
1.333 1.333
 1.333 1.333
1.333 1.333
1.333 1.333
1.333 1.333
1.334005 1.33401
1 Kalibrasi Termometer

Percobaan Literatur
Termometer Tekanan
Tb (˚C) Td (˚C) Tb (˚C) Td (˚C)
rata-rata
Termometer Raksa 110 oC 0 98 0 98.41
Termometer Raksa 110 oC 0 98 0 98.41 Tekanan
Termometer Raksa 250 oC 0 98 0 98.41 955
Termometer Raksa 250 oC 0 98 0 98.41 960
Termometer Raksa 360 oC 0 98 0 98.41

a Termometer Raksa 110 oC

Termometer Raksa 110 oC

Slope
120
1.0042
100
f(x) = 1.0041836735x - 2.00971834711523E-14
80
Tliteratur

60

40

20

0
0 20 40 60 80 100 120
Tpercobaan (°C)

b Termometer Raksa 110 oC

Termometer Raksa 110 oC

Slope
120
1.0042
100
f(x) = 1.0041836735x - 2.00971834711523E-14
80
Tliteratur (°C)

60

40

20

0
0 20 40 60 80 100 120
Tpercobaan (°C)

c Termometer Raksa 250 oC

Termometer Raksa 250 oC

120

100
f(x) = 1.0041836735x - 2.00971834711523E-14
 Termometer Raksa 250 oC
Slope
120
1.0042
100
f(x) = 1.0041836735x - 2.00971834711523E-14
Tliteratur (°C) 80

60

40

20

0
0 20 40 60 80 100 120
Tpercobaan (°C)

d Termometer Raksa 250 oC

Termometer Raksa 250 oC

Slope
120
1.0042
100
f(x) = 1.0041836735x - 2.00971834711523E-14
80
Tliteratur (°C)

60

40

20

0
0 20 40 60 80 100 120
Tpercobaan (°C)

e Termometer Raksa 360 oC

Termometer Raksa 360 oC

Slope
120
1.0042
100
f(x) = 1.0041836735x - 2.00971834711523E-14
80
Tliteratur (°C)

60

40

20

0
0 20 40 60 80 100 120
Tpercobaan (°C)
2 Kalibrasi Piknometer
Massa Pikno rata-rata (gram) 11.7750 Suhu ρA (kg/m3) ρA (g/mL)
Massa Aquadest (gram) 5.3718 25 996.836 0.9968
Massa Jenis Aquadest (g/mL) 0.9968 26 996.568 0.9966
Volume Piknometer (mL) 5.3889 27 996.29 0.9963
28 996.003 0.9960
Massa Metanol (gram) 4.1882
Massa Jenis Metanol (g/mL) 0.7772

3 Kalibrasi Refraktometer
Indeks bias Aquadest Benzene
1 1.3340 1.4950
2 1.3340 1.4860
3 1.3340 1.4970
Rata-rata 1.3340 1.4927
Literatur 1.3314 1.4896

Kalibrasi Refraktometer
1.5500
Slope
0.9966
1.5000
f(x) = 0.9966113445x + 0.0019414664
1.4500
ɳliteratur

1.4000

1.3500

1.3000

1.2500
1.3200 1.3400 1.3600 1.3800 1.4000 1.4200 1.4400 1.4600 1.4800 1.5000 1.5200
ɳpercobaan

4 Kalibrasi Pompa Diafragma

%Bukaan Volume rata- Q (mL/s)
rata (mL)
10 85 2.833333
20 120 4
30 150 5
40 203.33333333 6.777778
50 210 7
60 240 8
 70 260 8.666667
80 276.66666667 9.222222
90 296.66666667 9.888889
100 320 10.66667

Kalibrasi Pompa Diafragma Slope

12 0.0845

10 f(x) = 0.0845454545x + 2.5555555556

8
Q (mL/s)

0
0 20 40 60 80 100 120
%Bukaan Pompa

5 Kalibrasi Indeks Bias Terhadap Fraksi Mol Metanol

Mr (gr/mol)
Aquadest 18
Methanol 32

Massa Massa Mol Mol Mol Total Fraksi

Botol Aquadest Metanol Aquadest Metanol (mol) Metanol
(gram) (gram) (mol) (mol)

1 4.7925 0 0.26625 0 0.26625 0

2 4.2607 0.3521 0.236706 0.011003 0.2477087 0.04442
3 3.6902 0.6271 0.205011 0.019597 0.224608 0.087249
4 3.1547 1.1056 0.175261 0.03455 0.2098111 0.164672
5 2.6837 1.434 0.149094 0.044813 0.1939069 0.231103
6 2.2514 1.7773 0.125078 0.055541 0.1806184 0.307503
7 1.6861 2.2226 0.093672 0.069456 0.1631285 0.425776
8 1.2058 2.5456 0.066989 0.07955 0.1465389 0.542859
9 0.7292 3.1526 0.040511 0.098519 0.1390299 0.708616
10 0.5484 3.4246 0.030467 0.107019 0.1374854 0.778401
11 0 3.8037 0 0.118866 0.1188656 1

Kalibrasi Indeks Bias Terhadap Fraksi Mol Metanol

1.345

1.34
f(x) = 1.3337887388
f(x) = 0.04164446x^4 -0.0015072066 x^-0.0011324298
l n(x) +- 0.0569185559x^2
- 0.0365664862x^3 1.3338007527 + 0.0456663037x + 1.332225536
1.335
Indeks Bias (ɳ)

1.33

1.325
 1.345

1.34
f(x) = 1.3337887388
f(x) = 0.04164446x^4 -0.0015072066 x^-0.0011324298
l n(x) +- 0.0569185559x^2
- 0.0365664862x^3 1.3338007527 + 0.0456663037x + 1.332225536
1.335

Indeks Bias (ɳ)

1.33

1.325 x4
0.0416
1.32

1.315
0 0.2 0.4 0.6 0.8 1 1.2
Fraksi Mol Metanol (x)

5 Perhitungan Umpan
Fraksi Umpan 0.36
Massa Umpan (gram) 1700

Mr Campuran umpan (gr/mol) 23.04

Mol Campuran Umpan (mol) 73.784722222

Mol Metanol Umpan (mol) 26.5625

Mol Aquadest Umpan (mol) 47.222222222

Indeks Bias Metanol Teknis 1.32907

Indeks Bias Metanol Teknis
Terkoreksi 1.326451162
Fraksi Metanol Teknis (dibaca
dari kurva) 0.93

Mr Campuran Metanol Teknis

(gr/mol) 31.02
Mol Metanol Teknis (mol) 28.561827957
Mol Aquadest (mol) 1.999327957
Mol Aquadest yang dibutuhkan
(mol) 45.222894265

Massa Aquadest yang

dibutuhkan (gram) 814.01209677
Massa Metanol yang
dibutuhkan (gram) 885.98790323
Massa Total (gram) 1700

Volume Aquadest yang

dibutuhkan (mL) 816.5958059
Volume Metanol yang
dibutuhkan (mL) 1139.9780808
 957

Td literatur
98.35
98.5

Intersep
0

Intersep
0
Intersep
0

Intersep
0

Intersep
0
Intersep
0.0019
 Intersep
2.5556

Indeks Bias Indeks Bias

Rata-rata Terkoreksi

1.33502167 1.33238259
1.33670333 1.33405854
1.338035 1.33538568
1.34106 1.3384004
1.34206167 1.33939866
1.34307 1.34040356
1.34206167 1.33939866
1.341 1.3383406
1.33601833 1.33337587
1.33401 1.33137437
1.32866667 1.3260492
x3 x2 x
-0.0366 -0.0569 0.0457 1.322
 Indeks Bias
Umpan
L 23 1 1.34302
D 9 2 1.34302
R 2.555556 3 1.34302
Rata-rata 1.34302
Terkoreksi 1.340353732

Fraksi Mol
Umpan (dari 0.34
kurva)

Data pada Kolom 3 Data pada Kolom 5

Suhu Massa Fraksi mol Suhu

Koreksi Indeks Bias Indeks Bias metanol Koreksi
Menit Sampel Menit
Rata-Rata Terkoreksi (dari
(°C) (gram) (°C)
kurva)

10 55.231 0.089 1.34206 1.339396996 0.44 10 53.2226

20 52.2184 0.3498 1.34206 1.339396996 0.44 20 49.2058
30 59.2478 1.2493 1.34206 1.339396996 0.44 30 55.231
40 50.21 1.4229 1.34005 1.33739383 0.54 40 50.21
50 54.2268 1.7841 1.342055 1.339392013 0.44 50 48.2016
60 48.2016 0.7136 1.342055 1.339392013 0.44 60 48.2016
70 56.2352 5.0477 1.342055 1.339392013 0.44 70 53.2226
80 53.2226 1.854 1.342055 1.339392013 0.44 80 45.189
90 56.2352 0.2403 1.342055 1.339392013 0.44 90 51.2142
100 57.2394 0.219 1.342055 1.339392013 0.44 100 50.21
110 60.252 1.0374 1.342055 1.339392013 0.44 110 55.231
120 57.2394 0.1257 1.342055 1.339392013 0.44 120 51.2142
130 60.252 0.3 1.342055 1.339392013 0.44 130 50.21
140 52.2184 0.5187 1.342055 1.339392013 0.44 140 48.2016
150 56.2352 0.7252 1.342055 1.339392013 0.44 150 50.21
0 0 0 0 0.0019 0 0
0 0 0 0 0.0019 0 0
0 0 0 0 0.0019 0 0
0 0 0 0 0.0019 0 0
0 0 0 0 0.0019 0 0

Massa Massa
Total Fraksi Mol Rata- Total
(gram) 15.6767 Rata 0.446667 (gram)

Massa Massa
Kontinyu Kontinyu
(gram) (gram)
 Massa Massa
Batch Batch
(gram) (gram)

Komposisi yang didapat

Xb 0.168
Xd 0.849333

Produk Vakum Bottom (Final) Distilat (Final)

Massa Massa
Produk Massa Bottom Distilat
Vakum 97 Final 880 Final

Mr
Indeks Bias Indeks Bias Rata- Campura
Rata-Rata 0 Rata 1.33601 n Distilat

Indeks Bias Indeks Bias Mol

Terkoreksi 0.0019 Terkoreksi 1.333368 Distilat

Fraksi Mol Fraksi Mol

Metanol Metanol (dari
(dari kurva) kurva) 0.168
pada Kolom 5 Data pada Kolom 8

Massa Indeks Indeks Fraksi mol Suhu Massa Indeks Indeks

metanol Koreksi
Sampel Bias Rata- Bias Menit Sampel Bias Rata- Bias
(dari
(gram) Rata Terkoreksi kurva) (°C) (gram) Rata Terkoreksi

0.8817 1.341 1.338341 0.5 10 51.2142 2.5963 1.338035 1.335386

0.5822 1.34008 1.337424 0.54 20 43.1806 1.3058 1.33804 1.335391
0.1489 1.33904 1.336387 0.57 30 55.231 3.944 1.33703 1.334384
0.2591 1.341 1.338341 0.5 40 49.2058 1.8634 1.338055 1.335406
0.2017 1.341 1.338341 0.5 50 45.189 2.9715 1.33808 1.335431
0.9542 1.33904 1.336387 0.56 60 45.189 4.2766 1.33803 1.335381
0.8413 1.33904 1.336387 0.56 70 49.2058 1.3431 1.33803 1.335381
0.174 1.33904 1.336387 0.56 80 42.1764 1.993 1.33803 1.335381
0.1964 1.33904 1.336387 0.56 90 46.1932 0.5669 1.33803 1.335381
4.3785 1.33904 1.336387 0.56 100 40.168 0.6822 1.33805 1.335401
0.9628 1.33904 1.336387 0.56 110 49.2058 0.0841 1.33805 1.335401
0.9435 1.33904 1.336387 0.56 120 43.1806 0.003 1.33805 1.335401
0.0645 1.33904 1.336387 0.56 130 42.1764 0.1108 1.33803 1.335381
0.8076 1.33904 1.336387 0.56 140 43.1806 0.0409 1.33803 1.335381
0.5405 1.33904 1.336387 0.56 150 42.1764 0.0048 1.33803 1.335381
0 0 0.0019 0 0 0 0 0.0019
0 0 0.0019 0 0 0 0 0.0019
0 0 0.0019 0 0 0 0 0.0019
0 0 0.0019 0 0 0 0 0.0019
0 0 0.0019 0 0 0 0 0.0019

Fraksi Massa Fraksi

Mol Rata- Total Mol Rata-
11.9369 Rata 0.547333 (gram) 21.7864 Rata

Massa
Kontinyu
(gram)
 Massa
Batch
(gram)

Distilat (Final)

108.5014

20.352

5.33124
 Data pada Bottom Data pada Distilat
Fraksi mol Suhu Massa Indeks Indeks Fraksi mol
metanol Koreksi metanol
Menit Sampel Bias Rata- Bias Menit
(dari (dari
(°C) (gram) Rata Terkoreksi kurva)
kurva)

0.62 10 72.3024 2.2135 1.33904 1.336387 0.12 10

0.62 20 70.294 3.1577 1.34206 1.339397 0.23 20
0.63 30 66.2772 5.3 1.341055 1.338395 0.18 30
0.62 40 70.294 2.5225 1.34206 1.339397 0.23 40
0.62 50 76.3192 3.3841 1.34206 1.339397 0.23 50
0.62 60 70.294 2.1289 1.34106 1.3384 0.18 60
0.62 70 69.2898 3.1729 1.34104 1.33838 0.18 70
0.62 80 76.3192 4.3859 1.34206 1.339397 0.23 80
0.62 90 76.3192 2.9819 1.34106 1.3384 0.18 90
0.62 100 70.294 4.9491 1.33904 1.336387 0.11 100
0.62 110 79.3318 3.1323 1.339055 1.336402 0.11 110
0.62 120 70.294 2.3975 1.341055 1.338395 0.18 120
0.62 130 70.294 2.455 1.33904 1.336387 0.12 130
0.62 140 72.3024 12.8255 1.33904 1.336387 0.12 140
0.62 150 70.294 -0.2179 1.33904 1.336387 0.12 150
0 0 0 0 0.0019 0
0 0 0 0 0.0019 0
0 0 0 0 0.0019 0
0 0 0 0 0.0019 0
0 0 0 0 0.0019 0

Massa Fraksi
Total Mol Rata-
0.620667 (gram) 54.7889 Rata 0.168

Massa
Kontinyu
(gram)
Massa
Batch
(gram)
Data pada Distilat

Suhu Massa Indeks Indeks Fraksi mol

Koreksi metanol
Sampel Bias Rata- Bias (dari
(°C) (gram) Rata Terkoreksi kurva)

42.1764 2.2665 1.333 1.330368 0.84

42.1764 5.5631 1.333 1.330368 0.84
42.1764 10.0912 1.332 1.329371 0.88
40.168 1.8134 1.332 1.329371 0.88
40.168 2.7235 1.334005 1.331369 0.79
42.1764 14.3611 1.332 1.329371 0.88
40.168 8.8895 1.332 1.329371 0.88
42.1764 8.9395 1.332 1.329371 0.88
42.1764 7.914 1.332 1.329371 0.88
42.1764 5.9776 1.333 1.330368 0.84
42.1764 5.4548 1.333 1.330368 0.84
42.1764 7.3608 1.333 1.330368 0.84
42.1764 6.842 1.333 1.330368 0.84
42.1764 10.4393 1.333 1.330368 0.84
42.1764 9.8651 1.334005 1.331369 0.79
0 0 0 0.0019
0 0 0 0.0019
0 0 0 0.0019
0 0 0 0.0019
0 0 0 0.0019

Massa Fraksi
Total Mol Rata-
(gram) 108.5014 Rata 0.849333

Massa
Kontinyu
(gram)
Massa
Batch
(gram)
1 Memisahkan Metanol-Aquadest dengan Distilasi Kontinyu

2 Menentukan Jumlah Tahap pada Distilasi Kontinyu

Xb 0.168
Xf 0.34
Xd 0.8493333
R 2.5555556
Intersep 0.238875

Kurva Kesetimbangan
A B C P (mbar) P(kPa) T (°C)

Metanol 16.5785 3638.27 239.5 957 95.7 63.25316

Water 16.3872 3885.7 230.17 957 95.7 98.40314

P˚ P˚
T (˚C) x α y
Metanol Aquadest 1

63.2531591885 95.7 23.209245 1 4.1233569 1

66.7681577664 109.85255 27.148186 0.8288778139 4.0464049 0.9514560402
0.9
70.2831563443 125.70399 31.639361 0.6810279 3.9730257 0.8945446889
73.7981549221 143.40836 36.743194 0.5527278409 3.9029911 0.828273691
77.3131535 163.12857 42.524692 0.4409087608 3.8360906 0.7515654857
0.8
80.8281520779 185.03658 49.053598 0.3430311696 3.7721307 0.6632530296
84.3431506557 209.31345 56.404541 0.2569860723 3.7109325 0.5620756568
87.8581492336 236.14943 64.65718 0.1810158796 3.6523311 0.4466749915
0.7
91.3731478115 265.74406 73.896333 0.1136509027 3.5961738 0.315590928
94.8881463893 298.30615 84.212106 0.0536581673 3.542319 0.1672576926
98.4031449672 334.05385 95.7 4.17345826E-16 3.4906358 1.4568023E-15
0.6

0.5

Jumlah Tahap 4
0.4

0.3

0.2

0.1
 0.3

0.2

3 Menentukan HETP pada Distilasi Kontinyu

0.1

Jumlah Tahap
Teoritis 4
0
Tinggi Kolom 0 0.1
(cm) 96
HETP (cm) 24

4 Menentukan Efisiensi Tahap (ɳ)

Jumlah Tahap
Teoritis 4
Jumlah Tahap
Sebenarnya 8

Efisiensi Tahap 0.5

5 Menentukan %Recovery Metanol

Mol Metanol
Umpan (mol) 26.5625

Mol Metanol
Distilat (mol) 5.3312402
%Recovery 20.070551

6 Menentukan Neraca Massa

Teoritis
Umpan
Massa (gram) 1700

Bottom
Massa (gram) 880
Massa Masuk 1700
Massa Keluar 988.5014
Distilat
Massa (gram) 108.5014
Percobaan
Umpan 1700
Kolom 3 15.6767 Massa Masuk 1700
Kolom 5 11.9369 Massa Keluar 1134.9014
Kolom 8 21.7864
Bottom 880
Produk Vakum 97
Distilat 108.5014
 mbar to kPa
0.1

3.514999

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1
0.3

0.2

0.1

0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9
0.8 0.9 1