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The document describes an experiment to analyze an unknown salt sample to identify its cation and anion. Through a series of tests including analyzing color, solubility, and reactions with reagents like dilute sulfuric acid, silver nitrate, and ammonium chloride, the salt was found to contain bromide (Br-) as the anion and aluminum (Al3+) as the cation. Therefore, the unknown salt was determined to be aluminum bromide (AlBr3).
The document describes an experiment to analyze an unknown salt sample to identify its cation and anion. Through a series of tests including analyzing color, solubility, and reactions with reagents like dilute sulfuric acid, silver nitrate, and ammonium chloride, the salt was found to contain bromide (Br-) as the anion and aluminum (Al3+) as the cation. Therefore, the unknown salt was determined to be aluminum bromide (AlBr3).
The document describes an experiment to analyze an unknown salt sample to identify its cation and anion. Through a series of tests including analyzing color, solubility, and reactions with reagents like dilute sulfuric acid, silver nitrate, and ammonium chloride, the salt was found to contain bromide (Br-) as the anion and aluminum (Al3+) as the cation. Therefore, the unknown salt was determined to be aluminum bromide (AlBr3).
Aim: To analyze the given salt and identify the anion and cation present in it.
S.N EXPERIMENT OBSERVATION INFERENCE
O Preliminary Test 1. COLOUR White Absence of copper, The Colour of given cobalt,iron,nickel, salt is noted. manganese. 2. APPEARANCE Crystalline Absence of carbonate The appearance of the given salt is noted 3. SOLUBILITY IN WATER A little of the given salt is dissolved in distilled Soluble Absence of Carbonate water in a test tube 4. ODOUR No characteristic Absence of acetate odour and ammonium salts. ANION ANALYSIS 5. ACTION OF DIL.SULPHURIC ACID To a little of the substance No characteristic Absence of taken in a test tube a few reaction Carbonate,sulphite,nit drops of dil. Sulphuric acid rite and sulphide. is added . 6. ACTION OF Reddish brown May be nitrate or CONC.SULPHURIC ACID vapors are bromide. To a little of the substance evolved. NO3--, Br- taken in a test tube a few drops of conc. Sulphuric acid is added and warmed. 7. SILVER NITRATE TEST A pale yellow ppt Presence of Bromide To salt solution add dil nitric partially soluble is confirmed. acid and silver nitrate solution. in NH4OH is Br- obtained 8. To the salt add 1ml of CHCl3 Brown/orange Presence of Bromide and 2ml of chlorine water and layer is formed. is confirmed. shake well. Br- CATION ANALYSIS Original solution is prepared by dissolving the salt in water 9. ZEROGROUP(AMMONIU M) No characteristic Absence of To a little of the salt sodium reaction ammonium hydroxide solution is added Salts and heated NH4+ 10 I GROUP (LEAD) To a little of the original No characteristic Absence of I group solution dil. HCI is added. reaction Pb2+ 11. II GROUP (COPPER) To a little of the original No characteristic Absence of II group solution dil. HCI and reaction Cu2+ Hydrogen sulphide are added. 12. III GROUP (ALUMINIUM, IRON) To a little of the original Gelatinous white Presence of III solution ammonium chloride ppt is obtained. group(may be Al3+) and ammonium hydroxide are added. 13. CONFIRMATORY TEST White ppt soluble To the salt Solution add in excess sodium Presence of sodium hydroxide solution. hydroxide is aluminium is obtained. . confirmed. Al3+ 14. To the salt solution add blue Blue ppt floating Presence of litmus followed by ammonium in colorless aluminium is hydroxide solution. solution is seen. confirmed. Al3+ Result: The anion present in the given salt is bromide (Br-) and cation is Al+3.
The salt is Aluminium bromide AlBr3.
(Please note below equations for cations and anion to be written on the blank page of the journal with pencil.)