I.

Lanes Work
1. Experiment-1

0,3 gram of NaNO2

- Mixed with 10 mL H2O

- Entered into distilated flask
- Connected with separated funnel
that have been filled with NH4Cl
(0,3 grams in 10 mL H20)
- Heated flask
- Opened tape of separated funnel
- carrefully
Connected the destilate flask with
reversed measure glassthat filled
water using pipe

Bubbles is appeared

- Do the flame test with incandescent wood

The flame gas out

Reactions :

- NaNO2 (s) + H2O (l) →NaNO2(aq)

- NH4Cl (s) +H2O (aq) → NH4Cl (aq)
- NaNO2 (aq) + NH4Cl(aq) →NaCl (aq) +2H2O (l) + N2(g)

2. Experiment-2

0,25 grams of NaNO2

Test tube 1 Test tube 2

- Added 2-5 drops of - Diluted 4 times with H2O

H SO 1 M
 Reactions:

- 2 NaNO2 (aq) + H2SO4 (aq) → Na2SO4 (aq) + 2HNO2 (aq)

- NaNO2 (s) + H2O (l) → NaNO2 (aq)
- 2NaNO2 (aq) + 2KI (aq) + 2H2SO4 (aq) → I2 (aq) + 2NO (g) + 2K2SO4 (aq) +Na2SO4 (aq)
+ 2H2O (l)

-
3. Experiment-3

1 mL HNO3 (aq)

- Entered into test tube

- Added H2SO4 (l) 1 mL
- Cooled
- Added 0,5 mL FeSO4 0,2M from other
tube carefully through tube was
Brown ring is appeared
 Reactions :
- HNO3 (aq) + 2H2SO4 (aq) → 4NO (g) + H2O (l)+ 2H2SO4 (aq)
- 2NO3- (aq) + 4 H2SO4 (aq) + 6Fe2+ (aq) →6Fe3+ (aq) +2NO (g) + 4SO42- + H2O (l)
- Fe2+ (aq) + NO (g) → [Fe(NO3)]2+

4. Experiment-4

1 mL NH4OH 2M

- Flow H2S
- Added 1 mL ammonium 0,1 M
- Shaked with sulphur and
filter

Residue The color of solution

change

- Added HCl carrefully

Precipitate
Reactions:

- FeS (s) + 2HCl (aq) → H2S (g) + FeCl2 (aq)

- 2(NH4)OH (aq) + H2S (g) → (NH4)S (aq) + 2H2O (l)
- (NH4)2S (aq) + S(s) →(NH4)2S2(aq)
- (NH4)2S2(aq) + HCl (aq) → S (S) + NH4Cl (aq) NH4SH(aq)

5. Experiment-5
 2 mL NH4Cl 4M

- Entered into test tube

- Added ½ spoon Ca(OH)2
- Heated carrefully

Formed gas

- Placed with litmus paper on the mouth of test tube

- Observed the gas

The color of limus paper changed

- Entered spatula that have been entered HCl (l)

- Observed the gas

Formed gas

Reactions :

- 2NH4Cl (aq) + Ca(OH)2 (s) → CaCl3(aq) + 2H2O (l) + NH3(g)

- NH3(g) +HCl (aq) → NNH4Cl (g)

6. Experiment-6

5 mL NH4OH (l)

- Entered into erlenmeyer

- Heated carrefully

Formed gas

- Placed the gas in the test tube that been concentrated

by using rubber lid
- Tested by using spatula that have been entered into HCl (l)
- Entered gas into beaker glass that contain water through pipe
that contain water
- Added 2 drops of PP indicator into beaker glass

The color of limus paper changed